769_2004_843sss
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Transcript of 769_2004_843sss
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CCQM Workshop on Comparability & TraceabilityCCQM Workshop on Comparability & Traceability
in Food Analysis - 18-19 Noember !""#in Food Analysis - 18-19 Noember !""#$%M' ()res *aris+ France$%M' ()res *aris+ France
The Australia PerspectiveThe Australia Perspective
,r Terry (pencer,r Terry (pencer
Astralian .oernment AnalystAstralian .oernment Analyst
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CCQM presentation - 18 November 20032
reamblereamble
/ er0ormance-based approacher0ormance-based approach AstralianAstralian
%nternational%nternational
/ Astralian 0ood re2latory systemAstralian 0ood re2latory system impacts on approach to 0ood analysisimpacts on approach to 0ood analysis
case stdies relatin2 to measrement issescase stdies relatin2 to measrement isses
/ Aailability o0 re0erence materialsAailability o0 re0erence materials/ ro0iciency testin2ro0iciency testin2
/ The ne3t steps - isses to be addressedThe ne3t steps - isses to be addressed
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Astralian approach to 0ood analysisAstralian approach to 0ood analysis
/ er0ormance-based' non-prescriptieer0ormance-based' non-prescriptie
/ Accreditation to %(415"!6 - NATAAccreditation to %(415"!6 - NATA
/ 7ess emphasis on method7ess emphasis on method
/ More emphasis onMore emphasis on systemssystems
technical competence o0 laboratoriestechnical competence o0 laboratories
technical competence o0 analyststechnical competence o0 analysts
howeverhowever
/ 3ceptions to the rle3ceptions to the rle
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CCQM presentation - 18 November 20034
Astralia and Code3Astralia and Code3
/ (tron2 (pporter(tron2 (pporter 0ondation member0ondation member
host CCF%C(host CCF%C(
/ roponent o0roponent o0 criteria approachcriteria approach
sin2le laboratory method alidationsin2le laboratory method alidation
/ Acceptance o0 Code3 methodsAcceptance o0 Code3 methods as one alternatieas one alternatie 0it 0or prpose0it 0or prpose
/ Mtal promotion o0 the concept o0 e:ialenceMtal promotion o0 the concept o0 e:ialence
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CCQM presentation - 18 November 20035
Food re2lation in AstraliaFood re2lation in Astralia
/ rior to 199!rior to 199! ; states
/ ost 199!ost 199! stablishment o0 National Food Athoritystablishment o0 National Food Athority
/ 199;199; Astralia Ne= >ealand Food AthorityAstralia Ne= >ealand Food Athority
/ !""!!""! Food (tandards Astralia Ne= >ealandFood (tandards Astralia Ne= >ealand
/ (tattory Athority(tattory Athority independentindependent
e3pert bodye3pert body
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CCQM presentation - 18 November 20036
Food (tandards Astralia Ne= >ealandFood (tandards Astralia Ne= >ealand
/ ?esponsibilities?esponsibilities deelopin2' aryin2' reie=in2 standardsdeelopin2' aryin2' reie=in2 standards
/ 0ood sa0ety0ood sa0ety
/ ma3imm reside limitsma3imm reside limits
/ compositioncomposition
/ labellin2' etclabellin2' etc
deelopin2 codes o0 practicedeelopin2 codes o0 practice
deelopin2 primary prodction standardsdeelopin2 primary prodction standards coordinatin2 0ood sreillance & recallscoordinatin2 0ood sreillance & recalls
condctin2 researchcondctin2 research
assessin2 policiesassessin2 policies
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(tandards settin2(tandards settin2
/ AN> Food ?e2lation Ministerial Concil *AN>F?MC+AN> Food ?e2lation Ministerial Concil *AN>F?MC+- deelops policy- deelops policy
/ F(AN> - deelops standard*s+F(AN> - deelops standard*s+ conslation =ith stakeholdersconslation =ith stakeholders
/ F(AN> $oard - approes standard*s+F(AN> $oard - approes standard*s+
/ AN>F?MC - approes standard*s+AN>F?MC - approes standard*s+
inclded in the Food (tandards Codeinclded in the Food (tandards Code
adopted by re0erence intoadopted by re0erence into
/ stateealand le2islation
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Methods 0or 0ood analysisMethods 0or 0ood analysis
/ Astralia has no process *& no need+ 0or approal o0 methods sed inAstralia has no process *& no need+ 0or approal o0 methods sed in0ood analysis0ood analysis
e2 @ealth Canada and $Ae2 @ealth Canada and $ABBsystemsystem
/ rescriptie methods remoed 0rom the Food (tandards Code drin2rescriptie methods remoed 0rom the Food (tandards Code drin2reie= in !"""reie= in !"""
e2 7%(A 0or 2lten analysise2 7%(A 0or 2lten analysis
/ T=o maor e3ceptionsT=o maor e3ceptions Microbiolo2ical analysisMicrobiolo2ical analysis/ (tandard 1D;D1 - Microbiolo2ical 7imits 0or Food(tandard 1D;D1 - Microbiolo2ical 7imits 0or Food
,ietary 0ibre analysis,ietary 0ibre analysis
/ (tandard 1D!D8 - Ntrition %n0ormation ?e:irements(tandard 1D!D8 - Ntrition %n0ormation ?e:irements
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rescribed methods e3ceptionsrescribed methods e3ceptions
/ (tandard 1D;D1 - Microbiolo2ical 7imits 0or Food(tandard 1D;D1 - Microbiolo2ical 7imits 0or Food prescribes A( 15;; series o0 standard methodsprescribes A( 15;; series o0 standard methods
*crrently bein2 harmonised =ith %(4 e:ialents+*crrently bein2 harmonised =ith %(4 e:ialents+
alternatiely' alidate accordin2 to A( E;69 seriesalternatiely' alidate accordin2 to A( E;69 series
/ :alitatie *presence
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Measrement %ssesMeasrement %sses
Case stdy 1 - reside methodsCase stdy 1 - reside methods
/ ?e2latory methods?e2latory methods applies to chemical residesapplies to chemical resides
per0ormance-basedper0ormance-based
/ identi0y' :anti0y' determineidenti0y' :anti0y' determine
/ applicable to all reside sitations - plants' animals' 0eedapplicable to all reside sitations - plants' animals' 0eed
/ accracy' precision' repeatability' etcaccracy' precision' repeatability' etc
/ mlti-residemlti-reside
/ ?eside trials?eside trials re:ires acreditation to 4C, principles o0 .ood 7aboratory racticere:ires acreditation to 4C, principles o0 .ood 7aboratory ractice
*.7+*.7+
/ proides another paper-based leel o0 traceabilityproides another paper-based leel o0 traceability
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Measrement %ssesMeasrement %sses
Case stdy ! - analysis o0 2lten - part 1Case stdy ! - analysis o0 2lten - part 1
/ .lten - 2eneric name 0or prolamins *stora2e proteins+.lten - 2eneric name 0or prolamins *stora2e proteins+
/ Crrent 7%(As detect prolamins 0rom =heat *2liadins+' rye *secalins+'Crrent 7%(As detect prolamins 0rom =heat *2liadins+' rye *secalins+'barley *hordeins+barley *hordeins+
/ @7C needed to detect prolamins 0rom oats *aenins+@7C needed to detect prolamins 0rom oats *aenins+
/ What is the measreandGWhat is the measreandG proline-serine-2ltamine-2ltamineH and
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Measrement %ssesMeasrement %sses
Case stdy ! - analysis o0 2lten - part !Case stdy ! - analysis o0 2lten - part !
/ Gluten freeGluten freeclaimsclaims contains no detectable 2lten *& no oats or malt+contains no detectable 2lten *& no oats or malt+
de dili2ence re:iredde dili2ence re:ired
/ 0ood man0actrer - process control0ood man0actrer - process control
/ analyst - best practice analytical methodanalyst - best practice analytical method
/ Astralian Competition and Consmer Commission *consmerAstralian Competition and Consmer Commission *consmerre2lator+re2lator+
=ill not act a2ainst the descriptor I0reeJ on prodcts =here the leel o0=ill not act a2ainst the descriptor I0reeJ on prodcts =here the leel o0ntrient in the prodct is ntritionally insi2ni0icantntrient in the prodct is ntritionally insi2ni0icant
/ F(AN> *0ood re2lator+F(AN> *0ood re2lator+ has taken Ino detectable 2ltenJ to mean I2lten 0reeJhas taken Ino detectable 2ltenJ to mean I2lten 0reeJ
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Chemical re0erence materialsChemical re0erence materials
/ AKMA re:iresAKMA re:ires 1 2 pre actie constitent*s+1 2 pre actie constitent*s+
1"" 2 technical 2rade actie constitent*s+1"" 2 technical 2rade actie constitent*s+
1"" m2 analytical standard 0or all metabolites1"" m2 analytical standard 0or all metabolites
1" m2 analytical standard o0 imprities1" m2 analytical standard o0 imprities
/ rescribed material is held by A.A7rescribed material is held by A.A7 some are 0rther pri0ied
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$iolo2ical re0erence materials$iolo2ical re0erence materials
/ @2e holes in aailability@2e holes in aailability 2lten2lten
aller2ensaller2ens
2enetically modi0ied 0oods2enetically modi0ied 0oods
biolo2icals in 2eneralbiolo2icals in 2eneral
/ macromoleclesmacromolecles
/ =hole or2anisms=hole or2anisms
/ Traceability - present bt not to the (%Traceability - present bt not to the (%
/ Comparability - present bt not completeComparability - present bt not complete
/ Measrement ncertainty - present - in abndanceLMeasrement ncertainty - present - in abndanceL
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ro0iciency testin2 pro2ramsro0iciency testin2 pro2rams
/ NATA sppliedNATA spplied
/ NATA approedNATA approed %(4 .ide E#-1%(4 .ide E#-1
%(4 15"!6%(4 15"!6
%(4 9""" series%(4 9""" series
/ Mandatory participation by laboratoriesMandatory participation by laboratories
/ Aim is to assess
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The =inds that blo= The =inds that blo=
ask them' =hich lea0 o0 the tree =ill be ne3t to 2oask them' =hich lea0 o0 the tree =ill be ne3t to 2o
(oseki(oseki
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%sses to be addressed%sses to be addressed
/ Measrement-relatedMeasrement-related aailability o0 re0erence materials - pre and matri3aailability o0 re0erence materials - pre and matri3
de0inition o0 Inot detectedJ in conte3t o0 ero tolerancede0inition o0 Inot detectedJ in conte3t o0 ero tolerance
the notion o0 e:ialencethe notion o0 e:ialence
role o0 4%M7role o0 4%M7
/ ?ole o0 C%M