VHG Labs, Inc. - Choice Analytical Standards... · VHG Labs, Inc. Standards and ... ASTM D2386...

VHG Labs, Inc.Standards and Supplies for Spectrochemical Oil Analysis

Section 1

Petroleum

Standards

Multi-Element Coolant Standard

Fuel Dilution Standards

Coolant StandardThe following standard is intended for use in the analysis of metals in ethylene glycol or other coolants.

It can be diluted 1:1 with ethylene glycol (for matrix matching) or in dilute nitric acid.

Matrix: 1% HNO3, tr. HF.

Volume (mL) Product No.

500 GLYCOLSTD-500

Element Conc. (µg/mL) Element Conc. (µg/mL)

Al 50 Mo 500

B 1,000 Na 1,000

Ca 50 P 2,500

Cu 50 Pb 50

Fe 50 Si 500

K 1,000 Zn 50

Mg 50

Custom single element or multi-element standards are available (please inquire).

Fuel Dilution StandardsThese standards are intended for use in the determination of fuel (diesel fuel or gasoline in motor oil) by fuel

dilution meter (fuel sniffer), IR, GC analyzer or flash point. They are prepared gravimetrically from high purity

fuels added to high purity motor oil and certified by GC-FID in accordance with ASTM Methods D3524 and

D3525.

Description Application Product No.

5% Virgin Diesel Fuel in 15W40 Motor Oil Fuel Dilution Meter DSL5%VIR-100

5% Devolatilized Diesel Fuel in 15W40 Motor Oil GC or IR DSL5%DEV-100

5% Virgin Gasoline in 10W30 Motor Oil Fuel Dilution Meter GAS5%VIR-100

5% Devolatilized Gasoline in 10W30 Motor Oil GC or IR GAS5%DEV-100

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Petroleum

Standards

Crackle Test References

Nominal Water Concentration (% ) Volume (mL) Product No.

Blank 250 CT-BLK-250

0.1% 250 CT-0.1%-250

0.5% 250 CT-0.5%-250

1.0% 250 CT-1.0%-250

Nominal Water Concentration (% ) Volume (mL) Product No.

Blank 100 KF-BLK-100

0.1 100 KF-0.1%-100

0.5 100 KF-0.5%-100

1.0 100 KF-1.0%-100

Nominal Soot Content Range (% ) Volume (mL) Product Number

Blank 50 SOOT-BLK-50

0.5-2 50 SOOT-A-50

2-4 50 SOOT-B-50

4-6 50 SOOT-C-50

6-9 50 SOOT-D-50

9-12 50 SOOT-E-50

Set of all 6 6 x 50 SOOT-SET

Standards for Used Oil

Analysis

Wear Metals

Coolant

Fuel Dilution

Water in Oil

Soot

Standards for S, N, Cl and

Metals

Petroleum Physical Test

Standards

“Crackle Test” references for determining water in oil (all values nominal). The crackle test is a visu-

al test performed by placing a small drop of oil onto a hot plate (usually around 300º C). The

amount of water present in oil samples is estimated by comparison to these standards. All values

certified by gravimetric preparation.

Soot Content Standards

Reference standards for use in the determination of soot content in 15W40 diesel motor oil by

infrared spectroscopy or other technique. All values certifed by thermogravimetric analysis (TGA).

Karl Fischer Titration CertifiedReference Standards

Karl Fischer Titration certified reference standards for determining water in motor oil (all values certi-

fied by Karl Fischer Titration). This test determines the amount of water present in the oil and is the

most commonly-used test for this type of determination, with a high degree of accuracy. For use

with ASTM D6304.

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Section 1

Petroleum

Standards

Polysulfide Oil Standards

Sulfur QC Samples, Drift Monitors andCalibration Standards Made fromPolysulfide oil

VHG Labs' polysulfide oils have been formulated

for long shelf life and optimal stability even when

exposed to x-rays from modern high wattage

XRF spectrometers. In addition, our polysulfide

oil products offer high purity, low volatility, and

minimal diffusion through sample films.

These standards are well suited to ultra low

level sulfur analysis, quality control, drift correction, blank measurement and calibration standards

for XRF and other sulfur analysis techniques. Our polysulfide oil standards are intended for use in

accordance with the newly revised ASTM D2622, D4294, D5453, D7039, D7212, D7220 and

others.

Description Product No.

QC Samples

Sulfur @ 5µg/g, Polysulfide oil, 1L X3SPS-5-1L



Drift Monitors




Sulfur @ 1,000µg/g, Polysulfide oil, 1L X3SPS-1000-1L

Blank

Polysulfide Oil Blank X3SPS-BLK-1L

Calibration Sets

Sulfur Standard Set (low concentrations). X3SPS-SET1-13X50mL

Set of 13 Calibration Standards with

Sulfur @ 0, 1, 2.5, 5, 10, 25, 50,

75, 100, 250, 500, 750, 1000µg/g,

made from high purity polysulfide oil,

50mL each

Sulfur Standard Set (high concentrations). X3SPS-SET2-12X50mL

Set of 12 Calibration Standards with

Sulfur @ 0, 0.1, 0.5, 1, 1.5, 2,

2.5, 3, 3.5, 4, 4.5 and 5wt%,

made from high purity polysulfide oil,

50mL each

Sulfur Standard Set (low concentrations). X3SPS-SET3A-6X50mL

Set of 6 Calibration Standards with Sulfur

@ 0, 10, 25, 50, 100 and 250µg/g, made

from high-purity polysulfide oil, 50mL each

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Petroleum

Standards


Analysis


Metals

Sulfur-Free Metallo-

Organics

Nitrogen

Sulfur and Metals

Sulfur

Chlorine

Lead in Gas


Standards

Flash Point

Viscosity

Petroleum Physical Test Standards

Flash Point Reference Materials VHG Labs Flash Point Reference materials are intended for use with and certified by the appropriate ASTM

methods [ASTM D56, D92, D93]. Each standard is supplied with a full Certificate of Analysis (COA).

Volume: 250mL

Specification Apparatus Nominal Temp. °C Product No.

ASTM D93 (Flash Point) Pensky-Martens 27 FP27-250

Closed-Cup Tester 60 FPPM60-250

75 FP75-250

93 FP93-250

ASTM D92 Cleveland Open Cup 200 FP200-250

(Flash and Fire Point) 230 FP230-250

ASTM D56 (Flash Point) Tag Closed Tester 42 FP40-250

55 FP55-250

60 FPTC60-250

67 FP68-250

Flash Point Certified Reference MaterialsVHG Labs Flash Point Reference materials are intended for use in accordance with ASTM methods [ASTM D56,

D92, D93]. These certified reference materials are stable, pure hydrocarbons with a method specific flash point

determined by an inter-laboratory study. Each standard is supplied with a full Certificate of Analysis (COA).

Volume: 250mL

Nominal Viscosity @ 40º (cSt) Nominal Viscosity @ 100º (cSt) Product Number

9.5 2.8 VISC10-500

30 5.3 VISC30-500

54 7.3 VISC60-500

102 15.3 VISC100-500

110 16.8 VISC110-500

130 20 VISC130-500

300 47 VISC300-500

520 57 VISC500-500

920 84 VISC900-500

ASTM Test Hydrocarbon Nominal Flash Point °C Product No.

D93 Flash Point N-Decane 54°C FP53-250

Pensky-Martens N-Undecane 70°C FP70-250

Closed Cup Tester N-Tetradecane 114°C FP114-250

N-Hexadecane 134°C FP134-250

D92 Flash & Fire Point N-Tetradecane 116°C FP115-250

Cleveland Open Cup N-Hexadecane 140°C FP138-250

D56 Flash Point N-Decane 50°C FP51-250

Tag Closed Tester N-Undecane 67°C FP67-250

Viscosity Reference StandardsVHG Labs provides viscosity reference standards, intended for use in accordance with standard methods [e.g.

ASTM D445]. Each standard is manufactured in our ISO 9001:2000 and ISO/IEC 17025:2005 facility and sup-

plied with a full Certificate of Analysis (COA) which states the Certified Viscosity as correlated to the Master

Viscometer technique and is traceable to the NIST value of 1.002 mPa-s for water at 20°C.

Volume: 500mL

Section 1

Petroleum

Standards


ASTM D97 Pour Point Certified Reference MaterialsASTM D97 method for determination of the pour point of petroleum products. Standards are packaged in

250mL bottles and are accompanied with a certificate verifying the determined value.

Volume: 250mL

Nominal Pour Point (°C): -5 -10 -15 -20 -40 -50

Product No.: P5-250 P10-250 P15-250 P20-250 P40-250 P50-250

ASTM D2500 Cloud Point Certified Reference MaterialsASTM D2500 method for determination of the cloud point of petroleum products. Standards are packaged in


Volume: 250mL

Nominal Cloud Point (°C): +5 -2 -10 -15 -20

Product No.: C5-250 C2-250 C10-250 C15-250 C20-250

ASTM D2386 Freezing Point Certified Reference MaterialsASTM D2386 method is for determination of the freezing point of aviation fuels. Standards are packaged in


Volume: 250mL

Nominal Freezing Point (°C): -50 -45

Product No.: F50-250 F45-250

Group 1 & 2 Distillation Range

IBP 129º F

10% 180º F

50% 228º F

90% 319º F

EP 368º F

ASTM D86 Group 4 Distillation StandardThe Group 4 standard is a diesel oil whose distillation range is 379º F to 700º F, (193º to 371º C) and was

verified by consensus analysis.


Synthetic Distillation Standard 0.5L D86-4-500

Group 4 Distillation Range

IBP 379º F

10% 439º F

50% 525º F

90% 639º F

EP 700º F

ASTM D86 Group 1 & 2 Synthetic Distillation StandardThe automatic distillation apparatus duplicates the distillation conditions of the manual method. The increased

reliance on electronic control requires an independent standard to verify that the apparatus is performing cor-

rectly. VHG has introduced a synthetic blend of hydrocarbons that boil in the temperature range specified in

ASTM D86 distillation groups 1 and 2.

The Group 1 and 2 standard covers the boiling range 129º F to 368º F, (54º to 187º C) and was verified by

consensus analysis with twelve refinery laboratories.


Synthetic Distillation Standard 0.5L D86-500

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Petroleum

Standards


Analysis


Metals


Standards

Flash Point

Viscosity

Pour Point

Cloud Point

Freezing Point

Distillation

TAN, TBN


Total Acid Number (TAN Reference Materials)

VHG Labs' TAN Reference materials are intended for use in the determination of Total Acid Number (TAN) in

petroleum products by potentiometric titration. Our TAN standards are intended for use in accordance with

ASTM D644 and IP177.

Matrix *Certified Value Size Product Number

(mg KOH/g) (grams)

Mineral Oil 0.1 125 TAN-0.1


Mineral Oil 1.0 125 TAN-1





Acid number is defined as the quantity of base expressed as milligrams of potassium hydroxide per gram of sample, required to

titrate a sample to a well defined inflection point as specified in ASTM D 644.

Total Base Number (TBN Reference Materials)VHG Labs’ TBN reference materials are intended for use in the determination of Total Base Number (TBN) in

petroleum products by potentiometric titration. Our TBN standards are intended for use in accordance with

ASTM D2896 and IP276 or ASTM D4739.

Matrix *Certified Value Size Product Number

(mg KOH/g) (grams)

Mineral Oil 6 50 TBN-6-50






*Base number is defined as the quantity of perchloric acid, expressed in terms of the equivalent number of milligrams of potas-

sium hydroxide that are required to titrate 1g of the sample, dissolved in the specific solvent to a well defined inflection point as

specified in ASTM D 2896.

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VHG Labs, Inc. - Choice Analytical Standards... · VHG Labs, Inc. Standards and ... ASTM D2386...

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