Telene (1620 , 1650 and 1651 grades) Fire behavior · D45 1333 - Peugeot Method 1333 - Renault BL...

TELENE SAS 4, Rue Marie Curie

59910 Bondues - France www.telene.com [email protected]

Disclaimer : Telene has made reasonable efforts in preparing this document, but makes no warranties or representations whatsoever regarding the quality, content, completeness, suitability, adequacy, or accuracy of the information and data contained herein. Telene accepts no liability for any loss or damage (including, without limitation, indirect or consequential loss or damage) arising out of or in connection with the use or misuse of, or the reliance on, the information or data contained herein.

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Telene® (1620 , 1650 and 1651 grades) Fire behavior

Ref : VA – WM – 2015/02

Fire tests general conditions The fire resistance behaviour can be classified into two types:

1. Flame tests The flame is applied directly on a vertical or horizontal sample, on one of its edges or on a surface. Then, the flame propagation speed or the persistence time after the flame removal is measured as well as a post-combustion time (sample still lurid) or a sample ignition facility. Then, the materials are classified as non-flammable, self-extinguishing or burning.

2. Tests with a radiant source or an incandescent w ire In the first case, a radiant source is applied at a certain distance of the sample surface; an incandescent wire can also be applied directly on the sample. The temperatures reach 600 to 700°C for the radiant sources and 960°C for the incandescent wires. In the radiant source test, the inflammation is driven through a pilot flame which inflames the pyrolysis gases and propagates the flame to the sample. Although there is no direct contact with the flame, these tests are always very difficult. Remarks - The fumes emission quantity and their nature are not considered in those two tests. - Generally, the tests are more severe as the thickness decreases. - Some other tests combine the fire and fumes reactions of the materials. These tests are not suggested to be done on Telene® while the fumes emission quantities are very important.

Telene classifications

1. ISO 3795 Road transportation, tractors and agricultural and forestry equipment. British Leyland internal norm corresponding but non equivalent norm: BLS 30 MS 302. The test consists in the measurement of the material combustion speed. The inflammation starts on one edge of a horizontal sample in a small cabin submitted to a controlled air flow.




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Results Sample’s thickness: 5mm - Extinguishing since the flame removal - Combustion speed = 0 mm/min Sample’s thickness: 4mm - The flame remains but goes out before getting to the mark (reference mark from which the propagation speed is

measured) Burning rate of the samples 0 mm/min (self-extinguishable). Telene® passed this standard and is rated not combustible. Tests reports are available.

2. EN 95/28 Burning behaviour of materials used in interior constructions of certain categories of motor vehicle. Annex 4: to determine the horizontal burning rate of materials. The burning rate was tested for 4 samples according to Directive 95/28 WE Annex 4.

Results The flame died out after cutting off the gas. The flame did not reach the first measuring point or the end of the sample. Burning rate of the samples 0 mm/min (self-extinguishable). Telene® passed this standard and is rated not combustible. Test reports are available.

3. ECE-R 118: UNIFORM TECHNICAL PRESCRIPTIONS CONCERNING THE BURN ING BEHAVIOUR OF MATERIALS USED IN THE INTERIOR CONSTRU CTION OF CERTAIN CATEGORIES OF MOTOR VEHICLES Telene® passed the requirement of Annex 6 -Test to determine the horizontal burning rate of materials - by equivalence to ISO 3795.

4. Other burning rate standards Horizontal samples: FMVSS 302 - (USA) D45 1333 - Peugeot Method 1333 - Renault BL 30 MS 302 - British Leyland CMVSS 302 - (Canada) 832GS302 - Mack Trucks Telene® passed these standards and is rated not combustible.




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5. UL 94

HB Classification - Sample bar in a horizontal position - Application of an 18 mm flame on the bar end - The material is classified if the combustion speed is lower than: - 40 mm/mn if 3mm < thickness < 13 mm - 75 mm/mn if thickness < 3 mm The propagation speed is 25mm/mn on a 5mm thick Telene® sample HB classified

V0-V1-V2 classification - Sample bar in a vertical position - Application of an 18 mm flame; 2 successive inflammations during 10s.

Results Since the first application of the flame: - Sample inflammation after 2 to 3s - Then total sample combustion with a very large fumes emission. Telene® is not classified

Painted Telene: V0-V1-V2 classification Fireproofed paints improve perceptibly the fire behaviour of Telene. The V0 classification is hard to reach while it is difficult to correctly paint the edges of the sample. - No inflammation after the first ignition - After the second ignition, the inflammation times go from 0s to over 1mn. Telene® is classified V1

94-5VA Classification - Vertical bar - Flame height: 125 mm.

This test is more severe than the test UL 94 V0-V1-V2. Telene® is not classified

94-5VB Classification The test is carried out on one of the sample’s surfaces. Telene® is classified 94-5VB

6. FIAT 50433 classification

Principle - Sample 200mm x 50mm x 5mm tilted to 45°C. - Inflammation duration: 30s. - Flame height: 20 mm. - Bunsen burner: 9.5 localised at 10 mm from the lower edge of the sample. - Measurement of the flame propagation speed for 1mn. - Test carried out on 3 samples.




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Results Samples’ length burnt after 1 mn. - Sample n° 1: 40 mm - Sample n° 2: 30 mm - Sample n° 3: 30 mm Combustion speed: 35 mm/mn

Remarks - Sample inflammation since the first seconds of the flame application. - Maximum flame height reached during the test: 200 mm. - The propagation rate is measured according to the damaged part of the sample after the test. - Fall of inflamed drops during the test.

7. NFT 51074 - Incandescent wire test This test consists in determining the inflammation temperature of samples as well as their capacity to go out when the ignition source is over.

Principle A heated wire (550°C - 650°C - 750°C - 850°C - 960°C) is applied onto the surface of the sample for 30s.

Measurement: - Ta: Application time - T1: First inflammation time - T2: Flame extinguishing time

Tests results at 960°C - Non painted samples: - Ta = 30 s - T1 = 0 s

- T2 = > 90 s Flame extinguishing 1mn after the incandescent wire removal. Telene® doesn’t pass the test at 960°C

- Painted samples (Flame retardant paint): - Ta = 30 s - T1 = 0 s - T2 = 30 s

Extinguishing since the incandescent wire removal. Telene® passes the test

8. LOI classification - Vertical sample localised in an enclosure with a controlled oxygen ratio - Inflammation of the top of the sample with a flame propagation to the bottom. - Measurement of the minimum oxygen ratio necessary to maintain the total combustion of the sample

Results LOI: 19% (LOI: Limit Oxygen Indication)




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9. Epiradiator classification A radiant source is applied under a plate positioned at 45°. - The possible classifications are M1-M2-M3 - Test mainly used in the building industry - Measurement of the first inflamation time, the total height of the flames (measured every 30s) and of the increase

of temperature in the cabin test for 20mn

Results - Inflamation since the 2nd minute of the test - Flames elevation over 50 cm - Important fumes emission Test stopped after 5mn

Pyrolysis test - Pyrolysis combustion tests report written down by the INERIS - Nature of the emitted gas - Quantity determination of the metallic elements in the ashes




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Summary

ISO 3795

Road transportation, tractors and agricultural and forestry equipment. - Thickness 4 mm. Combustion speed: 0mm/min - Thickness 5 mm. Combustion speed: 0mm/min Telene® passes the test and is classified ISO 3795

Derivates: FMVSS 302 (USA) - D45 1333 (Peugeot) - Method 1333 (Renault) - BL 30 MS 302 (British Leyland) - CMVSS 302 (Canada ) - 832GS302 (Mack Trucks) : Classified

EN 95/28 Materials used in interior constructions of certain categories of motor vehicle

Classified

UL 94 HB Internal tests - Thickness 5 mm. Propagation speed: 25 mm/min Classified HB

UL 94 5VB Internal tests Classified

UL 94 5VA Internal tests Non classified

UL 94 V0-V1-V2

Internal tests Non classified V0-V1-V2

Pyrolysis combustion test

Emissions T° combustion CO CO2 HC1 Pyrolysis g/g g/g µg/g 400 (1) 0.056 0.57 1080 600 (2) 0.140 0.59 1290 800 (3) 0.116 0.84 1380

LOI (Limit Oxygen Indication)

19%

FIAT 50433 Slow combustion speed: 35 mm/mn Telene® passes the test.

Epiradiator Non classified

(1) Detected CH4: 0.7% (2) Detected CH4: 2% (3) Detected CH4: 5%




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Metallic elements in the ashes - Incineration at 600 °C - Sulfuric acid attack - Sulfuric ashes ratio: 0,27%

Determinated elements in the ashes

µ g/g

Al 495

Si 115

Mo 270

Na 7

Radiant Panel (ISO 5658-2)

Test n° Max Temp (°C)

Max Flow given off (kW/m²)

Flame Progress Total Length (mm)

Ignition Time (s)

1 362 12,12 697 55

2 326 9,76 683 49

3 331 10,16 726 53

Average values 340 10,68 702 52

Incandescent wire

NFT 51074

Equivalent norms

NFC 20455 &CEI 695-2-1

Telene®

- T° 960 °C

- T1 = 0 s

- Te = 90 s

Flame persistence after heating finger removal : 60s

Telene® coated with a flame retardant paint:

- T1 = 0 s

- T2 = 30 s

Flame out after after heating finger removal

TELENE SAS – Route d’Arras – F-62320 Drocourt – Tel. +33-321 08 83 20 – Fax +33-321 49 73 61

The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy

and suitability for particular applications or the results to be obtained.

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Annex 1

Automotive Industry institute

Laboratory of material tests

Report on burning behaviour of Telene® pDCPD resin Pimot

Technician: Z. Sieniawska Employer: Kompozyty Sp. z.o.o. Date: 06-08-16 Kind of material: pDCPD resin Place: PIMOT BLM No. of investigated object: 09/08/06T Article: Covering element for motor vehicles Date of delivery by post: 06-08-04

Results

Sample Weight and

Thickness

Time of

burning

Length of

burning

Burning

rate

Observations

145.68

5.05±5.07 0 0 0

Flame length 38 mm.

245.28

5.05±5.12 0 0 0

345.72

5.10±5.15 0 0 0

The flame died out after

cutting off the gas

445.32

5.05±5.15 0 0 0

The samples did not show any specific direction.

Date 06-08-16

Signature: A. Eminger

19.08.2013

KUEXT06360-HB engl.xls

Order by: TELENE SAS Material: Telene 1650

Order No.: KUEXT06360 Test bar: ASTM Specimen

In: 2013-08-06 Color: -

Out: 2013-08-19 Conditioning: > 48h 23 ± 2°C / 50 ± 5 % r.H.

Tested by: Christina Böhm Lab Ambient: 23°C / 56% r.H.

Material Burning Rate Remarks

Thickness total beyond 25mm mark total beyond 25mm mark

(mm) (sec) (sec) (mm) (mm) (mm/min)

4,73 1 271 181 100 75 24,9 S

4,76 2 237 181 100 75 24,9 S

4,75 3 239 179 100 75 25,1 S

Flame class UL94 HB passed in 4,8 mm




3,78 1 203 153 100 75 29,4 S

3,78 2 203 156 100 75 28,8 S

3,77 3 201 151 100 75 29,8 S





2,80 1 169 126 100 75 35,7 S

2,80 2 167 125 100 75 36,0 S

2,82 3 167 128 100 75 35,2 S


Thickness (mm) Burning Rate (mm/min)

Passed 3 - 13 ≤ 40

< 3 ≤ 75

D= Material dripped during contact S= Smoke

DA= Material dripped after contact WG= Material burned on wire gauze

Remark:

Burning Time Damaged Length

Sam

ple

Sam

ple

Thermoplastics Testing Center

Sam

ple


UL 94 HB


L:\09-Prueftechnik\06-Brand\Brandprg\deutsch\KUEXT06360.xls Seite: 1

Customer : TELENE SAS Department: UL-TTC

File Number : KUEXT06360 TELENE SAS_1001666521

Date of receipt : 2013-08-06 00:00 032XXXXXXX-000010

Material : -

UL94V Flammability Test

material: - lot: Telene 1650 color: -

at least 48h at 23± 2°C / 50± 5% r.F. storing 168h at 70± 1°C

sample thickness t1 t2 t2 + t3 sample thickness t1 t2 t2 + t3

mm s s s mm s s s

1 2,86 >35,1 (1) 1 2,86 >35,1 (1)

2 2,88 >35,1 (1) 2 2,86 >35,1 (1)

3 2,85 >35,1 (1) 3 2,90 >35,1 (1) Flame Class

4 2,84 >35,1 (1) 4 2,85 >35,1 (1)

5 2,86 >35,1 (1) 5 2,91 >35,1 (1) V-not

total afterflaming time (t1+ t2), s: >175,5 total afterflaming time (t1+ t2), s: >175,5

date of test: operator: 38830 date of test: operator: 38830

micrometer: 123450 hood/PC: #3/KRE0975050 micrometer: 123450 hood/PC: #3/KRE0975050

remark: - remark: -

- -

- -




mm s s s mm s s s

1 3,86 >35,1 (1) 1 3,85 >35,1 (1)

2 3,86 >35,1 (1) 2 3,88 >35,1 (1)

3 3,96 >35,1 (1) 3 3,92 >35,1 (1) Flame Class

4 3,90 >35,1 (1) 4 3,90 >35,1 (1)

5 3,92 >35,1 (1) 5 3,89 >35,1 (1) V-not




remark: - remark: -

- -

- -

( 1 ) Specimen burned up to holding clamp. ( 4 ) Specimen dripped particles which ignited cotton.

( 2 ) Specimen did not drip. ( 7 ) Fumes from specimen extinguished flame-burner relit during test

( 3 ) Specimen drips

t1= afterflaming time of first flaming

t2= afterflaming time of second flaming

t3= afterglowing time


2013-08-21 06:13 2013-08-27 10:08

2013-08-21 06:25 2013-08-27 10:19

L:\09-Prueftechnik\06-Brand\Brandprg\deutsch\KUEXT06360.xls Seite: 2

Customer : TELENE SAS Department: UL-TTC

File Number : KUEXT06360 TELENE SAS_1001666521

Date of receipt : 2013-08-06 00:00 032XXXXXXX-000010

Material : -

UL94V Flammability Test




mm s s s mm s s s

1 4,78 >35,1 (1) 1 4,78 >35,1 (1)

2 4,77 >35,1 (1) 2 4,76 >35,1 (1)

3 4,82 >35,1 (1) 3 4,81 >35,1 (1) Flame Class

4 4,81 >35,1 (1) 4 4,89 >35,1 (1)

5 4,79 >35,1 (1) 5 4,79 >35,1 (1) V-not




remark: - remark: -

- -

- -

( 1 ) Specimen burned up to holding clamp. ( 4 ) Specimen dripped particles which ignited cotton.

( 2 ) Specimen did not drip. ( 7 ) Fumes from specimen extinguished flame-burner relit during test

( 3 ) Specimen drips

t1= afterflaming time of first flaming

t2= afterflaming time of second flaming

t3= afterglowing time


2013-08-21 06:38 2013-08-27 10:26

Telene (1620 , 1650 and 1651 grades) Fire behavior · D45 1333 - Peugeot Method 1333 - Renault BL...

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