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Transcript of SNS Experimental FacilitiesOak Ridge X0000910/arb Neutron Detectors for Materials Research T.E....
SNS Experimental Facilities Oak RidgeX0000910/arb
Neutron Detectors for Materials Research
T.E. Mason
Experimental Facilities Division
Spallation Neutron SourceAcknowledgements: Kent Crawford & Ron Cooper
SNS Experimental Facilities Oak RidgeX0000910/arb
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Neutron Detectors
• What does it mean to “detect” a neutron? – Need to produce some sort of measurable quantitative (countable)
electrical signal
– Can’t directly “detect” slow neutrons
• Need to use nuclear reactions to “convert” neutrons into charged particles
• Then we can use one of the many types of charged particle detectors– Gas proportional counters and ionization chambers
– Scintillation detectors
– Semiconductor detectors
SNS Experimental Facilities Oak RidgeX0000910/arb
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Nuclear Reactions for Neutron Detectors
• n + 3He 3H + 1H + 0.764 MeV
• n + 6Li 4He + 3H + 4.79 MeV
• n + 10B 7Li* + 4He7Li + 4He + 0.48 MeV +2.3 MeV(93%)
7Li + 4He +2.8 MeV( 7%)
• n + 155Gd Gd* -ray spectrum conversion electron spectrum
• n + 157Gd Gd* -ray spectrum conversion electron spectrum
• n + 235U fission fragments + ~160 MeV
• n + 239Pu fission fragments + ~160 MeV
SNS Experimental Facilities Oak RidgeX0000910/arb
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Gas Detectors
n He H H MeV 3 3 1 0 76.
533318.
barns
~25,000 ions and electrons produced per neutron (~410-15 coulomb)
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Gas Detectors – cont’d
• Ionization Mode– electrons drift to anode, producing a charge pulse
• Proportional Mode– if voltage is high enough, electron collisions ionize gas atoms
producing even more electrons- gas amplification- gas gains of up to a few thousand are possible
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MAPS Detector Bank
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Scintillation Detectors
n Li He H MeV 6 4 3 4 79.
barns8.1
940
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Some Common Scintillators for Neutron Detectors
Li glass (Ce) 1.751022 0.45 % 395 nm ~7,000
LiI (Eu) 1.831022 2.8 % 470 ~51,000
ZnS (Ag) - LiF 1.181022 9.2 % 450 ~160,000
Material
Density of6Li atoms
(cm-3)
Scintillationefficiency
Photonwavelength
(nm)
Photons per neutron
SNS Experimental Facilities Oak RidgeX0000910/arb
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GEM Detector Module
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Anger camera
2000-03449/arb
• Prototype scintillator-based area-position-sensitive neutron detector
• Designed to allow easy expansion into a 7x7 photomultiplier array with a 15x15 cm2 active scintillator area.
• Resolution is expected to be ~1.5x1.5 mm2
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Semiconductor Detectors
n Li He H MeV 6 4 3 4 79.
barns8.1
940
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Semiconductor Detectors cont’d
• ~1,500,000 holes and electrons produced per neutron (~2.410-13 coulomb)– This can be detected directly without further amplification
– But . . . standard device semiconductors do not contain enough neutron-absorbing nuclei to give reasonable neutron detection efficiency
- put neutron absorber on surface of semiconductor?- develop boron phosphide semiconductor devices?
SNS Experimental Facilities Oak RidgeX0000910/arb
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Coating with Neutron Absorber
• Layer must be thin (a few microns) for charged particles to reach detector – detection efficiency is low
• Most of the deposited energy doesn’t reach detector – poor pulse height discrimination
SNS Experimental Facilities Oak RidgeX0000910/arb
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Detection Efficiency
• Full expression: 1 e N t
• Approximate expression for low efficiency:
tN• Where:
= absorption cross-section
N = number density of absorber
t = thickness
N = 2.71019 cm-3 atm-1 for a gas
For 1-cm thick 3He at 1 atm and 1.8 Å,
= 0.13
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Pulse Height Discrimination
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Pulse Height Discrimination cont’d
• Can set discriminator levels to reject undesired events (fast neutrons, gammas, electronic noise)
• Pulse-height discrimination can make a large improvement in background
• Discrimination capabilities are an important criterion in the choice of detectors ( 3He gas detectors are very good)
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Position Encoding
• Discrete - One electrode per position – Discrete detectors – Multi-wire proportional counters (MWPC)– Fiber-optic encoded scintillators (e.g. GEM detectors)
• Weighted Network (e.g. MAPS LPSDs)– Rise-time encoding – Charge-division encoding – Anger camera
• Integrating – Photographic film – TV – CCD
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Multi-Wire Proportional Counter
• Array of discrete detectors
• Remove walls to get multi-wire counter
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MWPC cont’d
• Segment the cathode to get x-y position
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Resistive Encoding of a Multi-wire Detector
• Instead of reading every cathode strip individually, the strips can be resistively coupled (cheaper & slower)
• Position of the event can be determined from the fraction of the charge reaching each end of the resistive network (charge-division encoding) – Used on the GLAD and SAND linear PSDs
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Resistive Encoding of a Multi-wire Detector cont’d
• Position of the event can also be determined from the relative time of arrival of the pulse at the two ends of the resistive network (rise-time encoding) – Used on the POSY1,
POSY2, SAD, and SAND PSDs
• There is a pressurized gas mixture around the electrodes
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Anger camera detector on SCD
• Photomultiplier outputs are resistively encoded to give x and y coordinates
• Entire assembly is in a light-tight box
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Micro-Strip Gas Counter
• Electrodes printed lithgraphically– Small features – high spacial resolution, high field gradients – charge
localization and fast recovery
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Crossed-Fiber Scintillation Detector Design Parameters (ORNL I&C)
• Size: 25-cm x 25-cm
• Thickness: 2-mm
• Number of fibers: 48 for each axis
• Multi-anode photomultiplier tube: Phillips XP1704
• Coincidence tube: Hamamastu 1924
• Resolution: < 5-mm
• Shaping time: 300 nsec
• Count rate capability: ~ 1 MHz
• Time-of-Flight Resolution: 1 sec
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The scintillator screen for this 2-D detector consists of a mixtureof 6LiF and silver-activated ZnS powder in an epoxy binder. Neutrons incident on the screen react with the 6Li to produce a triton and an alpha particle. Collisions with these charged particles cause the ZnS(Ag) to scintillate at a wavelength of approximately 450 nm. The 450 nm photons are absorbed in the wavelength-shifting fibers where they converted to 520 nm photons emitted in modes that propagate out the ends of the fibers. The optimum mass ratio of 6LiF:ZnS(Ag) was determined to be 1:3. The screen is made by mixing the powders with uncured epoxy and pouring the mix into a mold. The powder then settles to the bottom of the mold before the binder cures. After curing the clear epoxy above the settled powder mix is removed by machining. A mixture containing 40 mg/cm2 of 6LiF and 120 mg/cm2 of ZnS(Ag) is used in this screen design. This mixture has a measured neutron conversion efficiency of over 90%.
Neutron Detector Screen Design
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0
2000
4000
6000
8000
10000
0 5 10 15
GAUSSIAN FIT-FWHM = 5.41 mmDATA POINTS
FIBER NUMBER
CO
UN
TS
/10
SE
C
Neutron Beam
Coincidence tube
2-D tube
Scintillator Screen
Clear Fiber
Wavelength-shifting fiberAluminum wire
16-element WAND Prototype Schematic and Results
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Principle of Crossed-Fiber Position-Sensitive Scintillation Detector
Outputs to multi-anode photomultiplier tube
Outputs to coincidence single-anode photomultiplier tube
1-mm Square Wavelength-shifting fibers
Scintillator screen
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0
10
20
30
40
500
10
20
30
40
50
X-Axis
Y-Axis
1.40
1.05
0.70
0.35
0.00
-0.35
-0.70
-1.05
-1.40
Counts
Scattering Data from Germanium Crystal
• Normalized scattering from 1-cm high germanium crystal
• En ~ 0.056 eV• Detector 50-cm from
crystal
Neutron Scattering from Germanium Crystal Using Crossed-fiber Detector
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All fibers installed and connected to multi-anode photomultiplier mount