SCOPE OF ACCREDITATION SGS Philippines, Inc. Multi-Laboratory

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SCOPE OF ACCREDITATION

SGS Philippines, Inc. – Multi-Laboratory 2229 Chino Roces Avenue, Makati City

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Philippine Accreditation Bureau

Chemical Testing

Classification of Scopes Specific tests or Measurements

Standard Method/ Reference Standard

Metallic coatings and treatment solutions

Plating Solution Cu Direct Measurement, AAS

Fe

Pb

Ni

Sn

Zn

Ores and Minerals

Nickel Ores Ag (Silver) In-house Method-

Al (Aluminum) Mixed Acid Digestion,

As (Arsenic) ML-REF-114

Ca (Calcium)

Cd (Cadmium)

Co (Cobalt)

Cr (Chromium)

Cu (Copper)

K (Potassium)

Mg (Magnesium)

Mn (Manganese)

Mo (Molybdenum)

Na (Sodium)

Pb (Lead)

Ti (Titanium)

Zn (Zinc)

V (Vanadium)

Ni (Nickel) In-house Method Acid Digestion, MIN-REF-0692

Fe (Iron) In-house Method Acid Digestion, MIN-REF- 0692; Mixed Acid Digestion, ML-REF-114

P (Phosphorus) Mixed Acid Digestion,

S (Sulfur) ML-REF-114

Geochemical samples Arsenic (As) Hydride AAS/ ICP for trace elements USEPA 3050B Manual

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Mercury (Hg) USEPA 7471B Cold- Vapor AAS

Boron (B) ICP-OES, USEPA 3050B

Strontium (Sr)

Thallium (Tl)

Vanadium (V)

Beryllium (Be)

Molybdenum (Mo)

Sulfur (S)

Silver (Ag) USEPA 3050B AAS/ICP

Calcium (Ca)

Copper (Cu)

Cobalt (Co)

Iron (Fe)

Potassium (K)

Magnesium (Mg)

Manganese (Mn)

Sodium (Na)

Zinc (Zn)

Barium (Ba)

Aluminum (Al)

Cadmium (Cd)

Chromium (Cr)

Nickel (Ni)

Lead (Pb)

Antimony (Sb)

Silicon (Si)

Tin (Sn)

Titanium (Ti)

Fuels

Coals and Coke Sample preparation ASTM D2013

Air drying Loss & Total Moisture ASTM D3302

Proximate Analysis Gravimetry/ ASTM D3173

Moisture Gravimetry/ ASTM D3173

Ash Gravimetry/ ASTM D3174

Volatile Matter Gravimetry/ ASTM D3175; ISO 562

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Fixed Carbon ASTM D3172

Gross Calorific Value (in BTU/lb Bomb Calorimetry / or kcal/kg) ASTM D5865

Total Sulfur (S) Sulphur Analyzer/ ASTM D4239

Hardgrove Grindability Index ASTM D409-D4239

Solvents

Chemical Tests Assay/ Purity of Alcohols Gas Chromatography (Ethanol, Methanol, In-house method Isopropyl Alcohol) QLY-LAB-1159

Inks, Dyes and Pigments

Chemical Tests Cr VI Analysis Non-metal: RSTS-E&E-004 (US EPA 3060A & US EPA 7196) Metal: RSTS-E&E-103 (ISO 3613); RSTS-E&E-104 (EC 62321)

Lead, Cadmium, Mercury and RSTS-E&E-003 Chromium (US EPA 3051A, US EPA 3152 &EC 62321

Lead RSTS-E&E-001 (US EPA:3050B) ASTM E 1645-16 16 CFR Part 1303 RSTS-CHEM-109-1 ASTM E1613 CPSC-CH-E-1003-09.1 ASTM F963-17 Clause 4.3.5.1

Cadmium RSTS-E&E-002 (EN 1122)

PBB/ PBDE RSTS-E&E-005 (US EPA 3540C; 3541; 3550C; 3600C; SW-846 8270C; 8082; 8081); RSTS-E&E-

007 (IEC 62321)

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Migration of eight elements ISO 8124-3: 1997; ASTM F973- 03 / US CPSC Part 3- 2003 – Lead only / 16 CFR 1303; EN 71: 2013 Part 3; Canadian Hazardous Products Acts Regulation Ch. 42 Sec 1

Paper, paperboard and pulp

Paper, paper board and pulp Lead, Cadmium, Mercury and RSTS-E&E-003 (US Chromium EPA 3051A, US EPA 3052 & IEC 62321)

Lead RSTS-E&E-001 (US EPA: 3050B) ASTM E 1645-16; 16 CFR Part 1303 RSTS- CHEM-109-1; ASTM E1613; CPSC-CH- E1003-09.1; ASTM F963-17 Clause 4.3.5.1

Cadmium RSTS-E&E-002 (EN 1122)

Foods and Beverages

Cereal products Proximate Analysis for:

Protein Kjeldahl Method, QLY-LAB- 1201/ AOAC 945.18, 992.23 21stEd., 2019

Dietary Fiber Enzymatic-Gravimetric Method, QLY-LAB-1208/ AOAC 985.29 21st Ed., 2019

Ash Gravimetric Method, QLY-LAB-1153/ AOAC 923.03 21st Ed., 2019

Fat Ether Extraction, Roese- Gottlieb/Acid Hydrolysis, QLY- LAB-1147/ AOAC 950.54, 922.06, 925.18, 963.15, 933.05, 989.05 21st Ed., 2019/

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AOCS Ba 3-38

Moisture Air-Oven Method, QLY-LAB-1202/ AOAC 925.10 21st Ed., 2019/ GAFTA No. 130 (2003)/ Toluene Distillation/ AOCS Ca 2a-45

Carbohydrate By computation/ Based on FNRI Phil. Food Composition Tables 1997

Salt as NaCl Titrimetric Method, QLY-LAB-1211/ AOAC 937.09 21st Ed., 2019

Starch Polarimetry/ GAFTA No. 130 Method 28:1 (2003)

Free Fatty Acids Titrimetric Method, AOCS Official Method Ca 5a- 40, 7th Ed., 2017

Peroxide value Titrimetric Method, AOCS Official Method Cd 8b- 90, 7th Ed., 2017

pH pH electrode method/ AOAC, 21st Ed., 2019

Iodine in food ICP-MS, QLY-LAB-1149

Total sugars as invert Lane-Eynon Method, AOAC, 21st Ed., 2019/Pearson's Composition and Analysis of Foods, 9th Ed.

Sucrose Computation/ Handbook of Phil. Sugarcane Ind. (1992)

Calories from fat By computation/FNRI Calories from protein Phil Food Composition tables Calories from carbohydrates 1997

Sugar Profile – Fructose, glucose, HPLC-RI, QLY-LAB-1148 lactose, maltose and sucrose

Label Drafting USNLEA/ RENI

Trace Elements (Aluminum, In-house method/

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Antimony, Arsenic, Barium, AAS/ ICP-OES Cadmium, Calcium, Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Phosphorus, Potassium, Selenium, Sodium, Thallium, Tin, Zinc)

Fatty Acids profile: Gas Chromatography/

Omega-3 In-house method,

Saturated Fatty acid QLY-LAB-1134

Trans Fatty acid

Mono-unsaturated fatty acid Poly-unsaturated fatty acid

Cholesterol Gas Chromatography/ In-house method QLY-LAB-1133

Propionic acid HPLC/ In-house Method, QLY-LAB-1161

Broken & defective Physical Test NFA Standard rice kernels Specification for Milled Broken and damaged Rice (2nd Version)

kernels (shelled corns) TRED_SQAD No. 2; 1980; US DA GIPSA

Nuts and nuts products Proximate

Protein Kjeldahl Method, QLY-LAB-1201/ AOAC 950.48 21st Ed., 2019


Ash Gravimetric Method, AOAC950.49 21st Ed., 2019

Fat Ether Extraction/ Roese-Gottlieb/Acid Hydrolysis/ AOCS Ba 3-38/ AOAC948.22 21st Ed., 2019

Moisture Air-oven Method,

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GAFTA No. 130 (2003)/ AOAC925.40 21st Ed., 2019; Toluene Distillation/ AOCS Ca 2a-45

Carbohydrates By computation/ Based on FNRI Phil. Food Composition Tables 1997

Salt as NaCl Titrimetric Method, QLY-LAB-1211/ AOAC 937.09 21st Ed., 2019

Calories from fat By computation/FNRI

Calories from protein Phil Food

Calories from Carbohydrates Composition tables 1997

Sugar profile – fructose, glucose, HPLC-RI, QLY-LAB-1148 lactose, maltose and sucrose

Aflatoxin Rapid screening/ RIDASCREEN FAST Aflatoxin Manual

Elements (Aluminum, Antimony, AAS/ ICP-OES, Arsenic, Barium, Cadmium, In-house method Calcium, Chromium, Cobalt, QLY-LAB-1213 Copper, Iron, Lead, QLY-LAB-2143 Magnesium, Manganese, QLY-LAB-2145 Mercury, Phosphorus, Potassium,

Selenium,

Sodium, Thallium, Tin, Zinc)

Fatty Acids profile: Gas Chromatography/ Omega-3 In-house method Saturated Fatty acid QLY-LAB-1134 Trans Fatty acid Mono-unsaturated fatty acid Poly-unsaturated fatty acid

Cholesterol Gas Chromatography/ In-house method, QLY-LAB-1133

Propionic acid HPLC/ in-house Method, QLY-LAB-1161

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Dairy Products Proximate Analysis for:

Protein Kjeldahl Method, QLY-LAB-1201/ AOAC 991.20 21st Ed., 2019

Dietary Fiber Enzymatic-Gravimetric Method,

QLY-LAB-1208/

AOAC985.29 21st Ed., 2019

Ash Gravimetric Method/ AOAC945.46, 21st Ed., 2019

Fat Ether Extraction/ Roese-Gottlieb/Acid Hydrolysis/ AOCS Ba 3-38/ AOAC933.05,

989.05 21st Ed., 2019

Moisture Air-oven Method, GAFTA No. 130 (2003)/ AOAC925.23 21st Ed., 2019; Toluene Distillation/ AOCS Ca 2a-45


Lactose Lane-Eynon Method/ AOAC935.65A 21st Ed., 2019

Iodine in food In-house method ICP-MS, QLY-LAB-1149

Calories from fat By computation/FNRI

Calories from protein Phil Food

Calories from Carbohydrates Composition tables 1997

Sugar profile – fructose, glucose, HPLC-RI, QLY-LAB-1148/ lactose, maltose and sucrose AOAC, 20th Ed., 2016

Acidity Titrimetric Method, AOAC947.05, 21st Ed., 2019

Label drafting USNLEA/RENI

Trace Elements (Aluminum, AAS/ ICP-OES, Antimony, Arsenic, Barium, In-house method Boron, Cadmium, Calcium, Chromium, QLY-LAB-1213

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Cobalt, Copper, Iron, Lead, QLY-LAB-2143 Magnesium, Manganese, QLY-LAB-2145 Mercury, Phosphorus, Potassium, Selenium, Sodium, Sulfur, Tin, Titanium, Vanadium, Zinc

Fatty Acids profile: Gas Chromatography/ Omega-3 In-house method Saturated Fatty acid QLY-LAB-1134 Trans Fatty acid Mono-unsaturated fatty acid Poly-unsaturated fatty acid

Cholesterol Gas Chromatography/ In-house method

QLY-LAB-1133

Propionic acid HPLC/ in-house

Method, QLY-LAB-1161

Meat, poultry and Proximate

derived products Protein Kjeldahl Method, QLY-LAB-1201/ AOAC981.10 21st Ed., 2019

Moisture Air-oven method, AOAC950.46B, 21st Ed., 2019

Dietary Fiber Enzymatic-Gravimetric Method, QLY-LAB-1208/ AOAC 985.29 21st

Ed., 2019

Fat Ether Extraction/ AOAC960.39 21st Ed., 2019


Salt as NaCl Volumetric Method/AOAC 937.09 21st Ed., 2019

Nitrites Colorimetric, AOAC, 973.31 21st Ed., 2019

Nitrates + Nitrites Spectrophotometry, AOAC935.48 21st Ed., 2019

Sulfur dioxide Direct Titration, AOAC, 21st Ed., 2019/ Pearson's Composition and Analysis of

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Foods 9th Ed.

Elements (Aluminum, Antimony, AAS/ ICP-OES, Arsenic, Barium, Cadmium, In-house method Calcium, Chromium, Cobalt, QLY-LAB-1213 Copper, Iron, Lead, Magnesium, QLY-LAB-2143 Manganese, Mercury, QLY-LAB-2145 Phosphorus, Potassium, Selenium, Sodium, Thallium, Tin, Zinc)

Fatty acid profile: Gas Chromatography/ In- Saturated Fatty acid house method, QLY-LAB-1134 Trans Fatty acid

Mono-unsaturated fatty acid Poly-unsaturated fatty acid

Cholesterol Gas Chromatography/ In- house method, QLY-LAB-1133

Sugar Profile - Fructose, Glucose, HPLC-RI, QLY-LAB-1148 Lactose, Maltose and Sucrose

Fish, crustaceans, and Proximate

mollusks and derived Kjeldahl Method, products Protein AOAC981.10 21st Ed., 2019

Air-oven method, Moisture AOAC952.08 21st Ed., 2019

Fat Ether Extraction, AOAC948.15 21st Ed., 2019

Ash Gravimetric,

AOAC938.08 21st Ed., 2019


QLY-LAB-1208/

AOAC 985.29 21st Ed., 2019

Histamine Fluorometry,

AOAC977.13 21st Ed., 2019

Total Volatile N Distillation with MgO/

Acid Hydrolysis/ AOAC, 21st

Ed., 2019/95/149/EC: Official

Journal of the European

Communities L 097 29/04/1995

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Salt as NaCl Volumetric Method, AOAC937.09 21st Ed., 2019

Total Solids Gravimetric method, AOAC952.08 21st Ed., 2019

Saturated Fat Gas Chromatography, QLY- LAB-1134

Cholesterol Gas Chromatography, QLY-LAB-1133

Sugar Profile – Fructose, glucose, HPLC-RI, QLY-LAB-1148 lactose, maltose and sucrose AAS/ ICP-OES, In-house method


Sugar and Sugar products Proximate

Confectionary Protein Kjeldahl Method, QLY-LAB-1201/ AOAC945.23 21st Ed., 2019

Moisture Air-oven method, AOAC, 21st Ed., 2019

Fat Ether Extraction, AOAC922.06 21st Ed., 2019

Ash Gravimetric, PNS 1097/1098/ Handbook of Philippine Ind. (1992)/AOAC, 21st Ed., 2019


Color Spectrophotometric/ PNS 1097/1098/ Handbook of Phil Sugarcane Ind. (1992)/ICUMSA Method GS1/3-7 (2002)

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Invert/Reducing Sugars Titrimetric/ PNS 1097/ 1098/ Handbook of Phil Sugarcane Ind. (1992)

Moisture Gravimetric/ PNS 1097/ 1098/ Handbook of Phil Sugarcane Ind. (1992)/ICUMSA Method GS2/1/3/9-15 (2007)

Brix Hydrometer Method/ Handbook of Phil Sugarcane Ind. (1992)

Moisture (Molasses) Gravimetric/ AOAC, 20th Ed., 2016/Handbook of Phil Sugarcane Ind. (1992)

Polarization Polarimetry/ Handbook of Phil Sugarcane Ind. (1992)/ICUMSA Method GS1/2/3/9-1 (2007)


Fatty acid profile: Gas Chromatography/ Omega-3 In-house method Saturated Fatty acid QLY-LAB-1134 Trans Fatty acid Mono-unsaturated fatty acid Poly-unsaturated fatty acid


Propionic acid HPLC/ In-house method, QLY-LAB-1161

Fruits, jams and other Proximate

fruit products Protein Kjeldahl Method, AOAC945.23

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21st Ed., 2019



Fat Ether Extraction/ Roese- Gottlieb/Acid Hydrolysis/ AOCS

Ba 3-38/ AOAC950.54, 922.06, 925.18, 963.15, 933.05, 989.05 21st Ed., 2019

Moisture Vacuum-oven Method, GAFTA No. 130 (2003)/ AOAC934.06 21st Ed., 2019; Toluene Distillation, AOCS Ca 2a-45

Carbohydrate By Computation/ FNRI Phil Food Composition Tables 1997

Soluble Solids Refractometer Method, AOAC932.12 21st Ed., 2019

Calories from fat By computation/FNRI Phil Food

Calories from protein Composition tables

Calories from Carbohydrates 1997

Water Activity AOAC 978.18 21st Ed., 2019

Viscosity Viscometer

Sulfur Dioxide Direct Titration, AOAC, 21st Ed., 2019/Pearson's Composition and Analysis of Foods, 9th Ed.

Sugar profile – fructose, HPLC-RI, QLY-LAB-1148 glucose, lactose, maltose and sucrose

Fatty acid profile Gas Chromatography/ Omega-3 In-house method, QLY-LAB- Saturated Fatty acid 1134 Trans Fatty acid Mono-unsaturated fatty acid Poly-unsaturated fatty acid

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Elements (Aluminum, AAS/ ICP-OES, Antimony,

Arsenic, Barium, Cadmium, In-house method Calcium, Chromium, Cobalt, QLY-LAB-1213

Copper, Iron, Lead, QLY-LAB-2143

Magnesium,

Manganese, Mercury, QLY-LAB-2145

Phosphorus, Potassium, Selenium, Sodium, Thallium, Tin, Zinc)

Vegetables and vegetable Proximate

products Protein Kjeldahl Method, QLY-LAB- 1201/AOAC 920.152 21st Ed., 2019



Fat Ether Extraction, Roese-Gottlieb/ Acid Hydrolysis/ AOCS Ba 3-38/ AOAC 922.06, 925.18, 963.15, 933.05, 989.05 21st Ed., 2019

Air-oven Method, GAFTA No. Moisture 130 (2003)/ AOAC964.22 21st Ed., 2019; Toluene Distillation/ AOCS Ca 2a-45

By computation/ FNRI Carbohydrate Phil. Food Composition Tables 1997

Calories from fat By computation/FNRI Phil Calories from protein Food Composition tables Calories from Carbohydrates 1997



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Sugar profile – fructose, HPLC-RI, QLY-LAB-1148

glucose, lactose, maltose and sucrose

Label drafting USNLEA/ RENI

Trace Elements (Aluminum, AAS/ ICP-OES, Antimony, Arsenic, Barium, In-house method Cadmium, Calcium, Chromium, QLY-LAB-1213 Cobalt, Copper, Iron, Lead, QLY-LAB-2143 Magnesium, Manganese, QLY-LAB-2145 Mercury, Phosphorus, Potassium, Selenium, Sodium, Thallium, Tin, Zinc)

Fatty acid profile Gas Chromatography/ Omega-3 In-house method Saturated Fatty acid QLY-LAB-1134 Trans Fatty acid Mono-unsaturated fatty acid Poly-unsaturated fatty acid


Alcoholic Beverages Caffeine Anhydrous HPLC/In-House Method QLY-LAB-1162

Ethanol (Assay) Gas Chromatography/

Methanol (Assay) In-house method

Iso-Propyl Alcohol (Assay) QLY-LAB-1159

Fatty acid profile Gas Chromatography/ Saturated Fatty acid In-house method Trans Fatty acid QLY-LAB-1134 Mono-unsaturated fatty acid Poly-unsaturated fatty acid


Trace Elements (Aluminum, AAS/ ICP-OES, Arsenic, Cadmium, Chromium, In-house method Copper, Iron, Lead, Mercury, QLY-LAB-1213 Magnesium, Manganese, QLY-LAB-2143

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Phosphorus, Potassium, Sodium, Zinc)

QLY-LAB-2145

Softdrinks and cordial Caffeine Anhydrous HPLC, QLY-LAB-1162

Ethanol (Assay) Gas Chromatography/

Methanol (Assay) In-house method QLY-LAB-1159




Fruit juices, drinks and Total soluble solid as °Brix Refractometer Method, concentrates AOAC932.12 21st Ed., 2019

Total Titratable Acidity Titrimetric, AOAC942.15 21st Ed., 2019

Proximate

Kjeldahl Method/QLY-LAB- Protein 1201/AOAC 920.152 21st Ed., 2019

Dietary Fiber Enzymatic-Gravimetric Method, QLY-LAB-1208/AOAC 985.29 21st Ed., 2019


Fat Ether Extraction, Roese-Gottlieb/ Acid Hydrolysis/ QLY-LAB-1147/

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AOAC 950.54, 922.06, 925.18, 963.15,933.05, 989.05 21st Ed., 2019/AOCS Ba 3-38/

Air-oven Method, GAFTA No. Moisture 130 (2003)/ AOAC, 21stEd., 2019; Toluene Distillation, AOCS Ca 2a-45

By computation/ Based Carbohydrate on FNRI Phil. Food Composition Tables 1997

Total Sugars as Invert Lane-Eynon Method, AOAC923.09 21st Ed., 2019



Calories from fat By computation/FNRI Phil Food

Calories from protein Composition tables 1997

Calories from Carbohydrates

Sugar profile – fructose, glucose, HPLC-RI, QLY-LAB-1148 lactose, maltose and sucrose

Ethanol (assay) Gas Chromatography, In-house Methanol (assay) method/ QLY-LAB-1159



Edible fats and oils Free Fatty Acid/Acid Value AOCS Official Method Ca 5a-40,

7th Ed., 2017

Peroxide Value AOCS Official Method Cd 8b-90,

7th Ed., 2017

Saponification Value AOCS Official Method Cc 9a-48,

7th Ed., 2017

Melting Point AOCS Official Method Cc 1-25,

7th Ed., 2017

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Iodine Value AOCS Official Method Cd 1d-92, 7th Ed., 2017

Moisture Toluene Distillation, AOCS Official Method Ca 2a-45, 7th Ed., 2017

Moisture and Volatile Matter AOCS Official Method Ca 2c-25, 7th Ed., 2017

Insoluble Impurities AOCS Official Method Ca 3a-46, 7th Ed., 2017

Unsaponifiable Matter AOCS Official Method Ca 6a-40, 7th Ed., 2017

Total Fatty Matter By Computation Based on FOSFA Method

Smoke Point AOCS Official Method Cc 9a-48, 7th Ed., 2017

Color AOCS Official Method Cc 13e-92, 7th Ed., 2017

Anisidine Value AOCS Official Method Cd 18-90, 7th Ed., 2017


Fatty Acids Gas Chromatography, QLY-LAB-1134

Saturated Fat Gas Chromatography, QLY-LAB-1134

Cholesterol Gas Chromatography QLY-LAB-1133

BHA Gas Chromatography/ In-house Method QLY-LAB-1160

BHT Gas Chromatography/ In-house Method QLY-LAB-1160

TBHQ Gas Chromatography/ In-house Method QLY-LAB-1160

Margarine Proximate

Protein Kjeldahl Method, QLY-LAB-1201/AOAC 991.20 21st Ed., 2019

Dietary Fiber Enzymatic-Gravimetric Method, QLY-LAB-1208/AOAC 985.29AOAC

21st Ed., 2019

Ash Gravimetric Method, AOAC,

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21st Ed., 2019

Fat Ether Extraction,Roese-Gottlieb/Acid Hydrolysis/AOAC 950.54, 922.06,925.18,963.15,933.05,989.05

21st Ed., 2019/AOCS Ba 3-38

Moisture Air Oven Method, AOAC 925.23 21st Ed., 2019/GAFTA No. 130 (2003)


Calories from fat By computation/FNRI Phil

Calories from protein Food Composition tables






Eggs and eggs products Proximate

Protein Kjeldahl Method, QLY-LAB- 1201/AOAC 981.10 21st Ed., 2019

Dietary Fiber Enzymatic-Gravimetric Method, QLY-LAB-1208/ AOAC 985.29 21st

Ed., 2019

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Ash Gravimetric Method, QLY-LAB-1153/ AOAC 938.08 21st Ed., 2019

Fat Ether Extraction, Roese-Gottlieb/ Acid Hydrolysis/AOAC 925.32, 950.54, 922.06, 925.18, 963.15, 933.05, 989.05 21st Ed., 2019/AOCS Ba 3-38/

Moisture Air-oven Method, GAFTA No. 130 (2003)/ AOAC, 21st Ed., 2019










Pet foods Proximate

AOAC954.01

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Protein and 2001.11/21st Ed., 2019

Conventional, GAFTA Fiber No. 10.0 (2003)/ AOAC 978.10 21st Ed., 2019


Fat Ether Extraction, Rose- Gottlieb/Acid Hydrolysis/ AOCS Ba 3-38/ AOAC950.54, 922.06,925.18,963.15,933.05, 989.05 21st Ed., 2019

Moisture Air-oven Method, GAFTA No. 130 (2003)/ 934.01 AOAC934.01 21st Ed., 2019





Elements: Aluminum, Arsenic, AAS/ ICP-OES, Cadmium, Calcium, Chromium In-house method Cobalt Copper, Iron, Lead, QLY-LAB-1213 Mercury, Magnesium, QLY-LAB-2143 Manganese, Phosphorus, QLY-LAB-2145 Potassium, Selenium, Sodium, Tin, Zinc

Antioxidants in foods BHT Gas Chromatography,

BHA In-house Method

TBHQ QLY-LAB-1160

Colorant in foods Elements: AAS/ ICP-OES, Aluminum (Al) In-house method Arsenic (As) QLY-LAB-1213 Cadmium (Cd) QLY-LAB-2143 Lead (Pb) QLY-LAB-2145

Magnesium (Mg) Manganese (Mn)

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Mercury (Hg)

Food additives Potassium Sorbate/ Sorbic Acid HPLC,

(Preservatives, Sodium Benzoate/ Benzoic Acid In-House Method QLY-LAB-1135

sweeteners, color Fatty acid profile: Gas Chromatography, additives, flavour Omega-3 QLY-LAB-1134 enhancers, emulsifiers, Saturated Fatty acid stabilizers/thickeners/ Trans Fatty acid binders, leaving agents and

Mono-unsaturated fatty acid

enzyme preparations) Poly-unsaturated fatty acid


Propionic acid HPLC, In-house method QLY-LAB-1161

Food products Proximate

(food processing, Protein Kjeldahl Method, processed AOAC945.18, 950.48, 991.20, foods and finished 981.10, 945.23 21st Ed., 2019

products) Dietary Fiber Enzymatic-Gravimetric Method, AOAC 985.29 21st Ed., 2019

Ash Gravimetric Method/ AOAC942.05 21st Ed., 2019

Fat Ether Extraction/ Roese- Gottlieb/Acid Hydrolysis/ AOCS Ba 3-38/ AOAC950.54, 922.06,925.18,963.15,933.05, 989.05 21st Ed., 2019

Moisture Air-oven Method, GAFTA No. 130 (2003)/ AOAC925.10 21st Ed., 2019



Calories from fat By Computation/

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Calories from Protein FNRI Phil. Food

Calories from Carbohydrates Composition Tables 1997

Viscosity Direct Measurement, use of Viscometer


Sugar Profile - Fructose, Glucose, HPLC-RI, Lactose, Maltose and Sucrose QLY-LAB-1148

Ethanol (Assay) Gas Chromatography,

Methanol (Assay) In-house method

Iso-Propyl Alcohol (Assay) QLY-LAB-1159

Fatty acid profile Gas Chromatography, Omega-3 QLY-LAB-1134 Saturated Fatty acid Trans Fatty acid Mono-unsaturated fatty acid Poly-unsaturated fatty acid


Propionic acid HPLC, In-house method QLY-LAB-1161

Iodine in Food ICP-MS/QLY-LAB-1149

Sulfur Dioxide Direct Titration, AOAC, 21st Ed., 2019/Pearson's Composition and Analysis of Foods, 9th Edition

Trace Elements: Aluminum, AAS/ ICP-OES, Arsenic, Cadmium, Calcium, In-house method Chromium QLY-LAB-1213 Cobalt Copper, Iron, Lead, QLY-LAB-2143 Mercury, Magnesium, QLY-LAB-2145 Manganese, Phosphorus, Potassium, Selenium, Sodium, Tin, Zinc

Vitamins in Foods Vitamin A (Retinol) HPLC,

Retinyl Acetate QLY-LAB-1131

Retinyl Palmitate

Vitamin A Precursor (Beta-Carotene)

In-House Method QLY-LAB-1143

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Vitamin B1 HPLC/

Vitamin B2 In-House Method

Vitamin B6 QLY-LAB-1142

Vitamin C HPLC, QLY-LAB-1144

Vitamin D3 HPLC, QLY-LAB-1132

Vitamin E HPLC, QLY-LAB-1151

Vitamin B3 (Niacin, Niacinamide) HPLC, QLY-LAB-1142

Folic Acid HPLC, QLY-LAB-1166

Calcium Panthothenate HPLC, QLY-LAB-1163

Biotin HPLC, QLY-LAB-1165

Vitamin B12 HPLC, QLY-LAB-1164

Sauce, spices and Proximate

condiments Kjeldahl Method, Protein AOAC945.18, 950.48, 991.20, 981.10, 945.23 21st Ed., 2019


QLY-LAB-1208/ AOAC 985.29 21st Ed., 2019

Ash Gravimetric Method, AOAC, 21st Ed., 2019

Fat Ether Extraction/ Rose- Gottlieb/Acid Hydrolysis/ AOCS Ba 3-38/ AOAC950.54, 922.06,925.18,963.15,933.05, 989.05 21st Ed., 2019

Moisture Air-oven Method, GAFTA No. 130 (2003)/ AOAC964.22, 968.11,925.10 21st Ed., 2019; Toluene Distillation/ AOCS Ca 2a-45


Lane-Eynon Method, Total Sugars as Invert AOAC923.09 21st Ed., 2019

Salt as NaCl Titrimetric Method, AOAC 937.09 21st Ed., 2019

pH pH electrode method,

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AOAC, 21st Ed., 2019

Iodine in Food ICP-MS/ QLY-LAB-1149



Calories from fat By Computation/ FNRI Phil

Calories from Protein Food Composition Tables





Sugar Profile - Fructose, Glucose, HPLC-RI, Lactose, Maltose and Sucrose QLY-LAB-1148

Capsaicin, SHU HPLC, QLY-LAB-1168

Food Supplement and/or Proximate

Dietary supplement Kjeldahl Method, Protein AOAC945.18, 950.48, 991.20, 981.10, 945.23 21st Ed., 2019


Ash Gravimetric Method/ AOAC, 21st Ed., 2019

Ether Extraction/ Roese- Fat Gottlieb/Acid Hydrolysis/ AOCS Ba 3-38/ AOAC950.54,

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922.06,925.18,963.15,933.05,989.05 21st Ed., 2019

Air-oven Method, GAFTA Moisture No. 130 (2003)/ AOAC, 20th Ed., 2016; Toluene Distillation/ AOCS Ca 2a-45



Salt as NaCl Titrimetric Method, AOAC937.09 21st Ed., 2019

pH pH electrode method, AOAC, 21st Ed., 2019



Calories from fat By Computation/ FNRI

Calories from Protein Phil Food Composition

Calories from Carbohydrates Tables 1997



Vitamin A (Retinol) HPLC,


Retinyl Palmitate

Vitamin A Precursor HPLC, QLY-LAB-1143 (Beta-carotene)




Vitamin C In-house method,

HPLC(QLY-LAB-1144)

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Residues in foods and agricultural materials

Elements Antimony (Sb) AAS/ ICP-OES, Arsenic (As) In-house method Barium (Ba) QLY-LAB-1213 Beryllium (Be) QLY-LAB-2143 Boron (B) QLY-LAB-2145 Cadmium (Cd) Calcium (Ca) Chromium (Cr) Cobalt (Co) Copper (Cu) Iron (Fe) Lead (Pb) Magnesium (Mg) Manganese (Mn) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Phosphorus (P) Potassium (K) Selenium (Se) Silicon (Si) Sodium (Na) Strontium (Sr)

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Sulfur (S) Thallium (Tl) Tin (Sn) Titanium (Ti) Vanadium (V) Zinc (Zn)

Pesticides Alpha-BHC Gas Chromatography, Beta-BHC QLY-LAB-1150 Lindane Dieldrin Endrin Heptachlor Heptachlor Epoxide Chlordane Endosulfan I Endosulfan II DDT DDD DDE Methoxychlor Organophosphorus Multi-Residue Analysis Organophosphorus Pesticides Determined Ethion Azinophos Methyl Disulpoton Naled Diazinon Malathion Phorate Any Multi-residue or Individual Pesticide Residue Analysis PCBs

Antibiotics Chloramphenicol HPLC, QLY-LAB-1140

Chlortetracycline Hydrochloride HPLC, QLY-LAB-1139

Oxytetracycline HPLC, QLY-LAB-1139

Sulfamethazine HPLC, QLY-LAB-1141

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Ivermectin HPLC/ USP 31

Antibiotics Seafood (Shrimp/ Milkfish)

Chloramphenicol LC-MS/MS, QLY-LAB-1136

Nitrofurans LC-MS/MS, QLY-LAB-1152

Malachite Green LC-MS/MS, QLY-LAB-1167

Leucomalachite Green LC-MS/MS, QLY-LAB-1167

Other residues Chloramphenicol HPLC, QLY-LAB-1140

Chlortetracycline Hydrochloride HPLC,

Oxytetracycline QLY-LAB-1139


Ivermectin HPLC, QLY-LAB-1138

Drugs and pharmaceuticals

Drugs Chlortetracycline Hydrochloride HPLC,

Oxytetracycline Hydrochloride QLY-LAB-1139



Herbal products Proximate

Protein Kjeldahl Method, AOAC945.18, 950.48, 991.20, 981.10, 945.23 21st Ed., 2019

Fiber Conventional, GAFTA No. 10.0 (2003)/ AOAC 978.10 21st Ed., 2019

Ash Gravimetric Method, AOAC, 21st Ed., 2019

Fat Ether Extraction/ Roese- Gottlieb/Acid Hydrolysis/ AOCS Ba 3-38/ AOAC, 21st Ed., 2019

Moisture Air-oven Method/ GAFTA No. 130 (2003)/ AOAC 925.10, 964.22 21st Ed., 2019



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Carbohydrate By computation/ FNRI Phil. Food Composition

Calories from fat Tables 1997 By computation/ FNRI

Calories from Protein Phil. Food Composition

Calories from Carbohydrates Tables 1997

Ethanol (Assay) Gas Chromatography,

Methanol (Assay) In-house method QLY-LAB-

Iso-Propyl Alcohol (Assay) 1159



Vitamin A (Retinol) HPLC,


Retinyl Palmitate

Vitamin A Precursor (Beta-carotene)

HPLC, QLY-LAB-1143


Vitamin B2

Vitamin B6









Elements AAS/ ICP-OES, Aluminum (Al) In-house method Antimony (Sb) QLY-LAB-1213 Arsenic (As) QLY-LAB-2143

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Barium (Ba) QLY-LAB-2145 Beryllium (Be) Boron (B) Cadmium (Cd) Calcium (Ca) Chromium (Cr) Cobalt (Co) Copper (Cu) Iron (Fe) Lead (Pb) Magnesium (Mg) Manganese (Mn) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Phosphorus (P) Potassium (K) Selenium (Se) Silicon (Si) Sodium (Na) Strontium (Sr) Sulfur (S) Thallium (Tl) Tin (Sn) Titanium (Ti) Vanadium (V) Zinc (Zn)

Medicinal and veterinary Vitamin A (Retinol) HPLC,

preparations Retinyl Acetate QLY-LAB-1131

Retinyl Palmitate


HPLC, QLY-LAB-1143




Vitamin C HPLC, In-house method QLY-LAB-1144



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Calcium Pantothenate HPLC, QLY-LAB-1163



Elements AAS/ ICP-OES, Aluminum (Al) In-house method Antimony (Sb) QLY-LAB-1213 Arsenic (As) QLY-LAB-2143 Barium (Ba) QLY-LAB-2145 Beryllium (Be) Boron (B) Cadmium (Cd) Calcium (Ca) Chromium (Cr) Cobalt (Co) Copper (Cu) Iron (Fe) Lead (Pb) Magnesium (Mg) Manganese (Mn) Mercury (Hg) Molybdenum (Mo) Nickel (Ni) Phosphorus (P) Potassium (K) Selenium (Se) Silicon (Si) Sodium (Na) Strontium (Sr) Sulfur (S) Thallium (Tl) Tin (Sn) Titanium (Ti) Vanadium (V) Zinc (Zn)

Vitamins Vitamin A (Retinol) HPLC,


Retinyl Palmitate

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HPLC, QLY-LAB-1143













Chlortetracycline Hydrochloride HPLC, QLY-LAB-1139

Oxytetracycline Hydrochloride HPLC, QLY-LAB-1139



Raw materials used in Vitamin A (Retinol) In-house method/

compounding Retinyl Acetate HPLC(QLY-LAB-1131)

pharmaceuticals Retinyl Palmitate


HPLC, QLY-LAB-1143





Vitamin E In-house method HPLC(QLY-LAB-1151)





Elements AAS/ ICP-OES, Aluminum (Al) In-house method Antimony (Sb) QLY-LAB-1213 Arsenic (As) QLY-LAB-2143 Barium (Ba) QLY-LAB-2145

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Beryllium (Be) Boron (B) Cadmium (Cd) Calcium (Ca) Chromium (Cr) Cobalt (Co) Copper (Cu) Iron (Fe) Lead (Pb) Magnesium (Mg) Manganese (Mn) Mercury Molybdenum Nickel Phosphorus Potassium Selenium Silicon Sodium Strontium Sulfur Thallium Tin Titanium Vanadium Zinc

Cosmetics, Perfumes and essential oils

Cosmetics Heavy Metals HPLC/ ASEAN method

Heavy Metals ICP-OES/ASEAN method

Fats, Oils and Waxes

Animal sources Crude Protein (N content) Kjeldahl Method, Vegetable sources AOAC 992.23 21st Ed., 2019

Ash Gravimetric, GAFTA 130 2003/ AOAC, 21st Ed., 2019

Crude Fiber Conventional/ GAFTA 130 2003/ AOAC, 21st Ed., 2019

Sand/ silica Gravimetric/ GAFTA 130 2003/ AOAC, 21st Ed., 2019

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Aflatoxin Rapid Screening/ RIDASCREEN FAST Aflatoxin Manual/ AOAC, 21st Ed., 2019

FFA Titrimetric Method/ AOCS Ca 5a-40/ ISO 660/ AOAC, 21st Ed., 2019

Moisture Air-Oven Method, GAFTA 130 2003/AOCS 7th Ed., 2017/ AOAC, 21st Ed., 2019

Oil Content Solvent Extraction, AOCS Ba 3-38/ FOSFA Int’l Official Method

Acetyl /Hydroxyl Value Solvent Extraction, AOCS Ba 3-38/ FOSFA Int’l Official Method

Ash Gravimetry, AOAC, 21st Ed., 2019

Color, Lovibond Lovibond, AOAC, 21st Ed., 2019/AOCS 7th Ed., 2017/ISO 15305

Titrimetry, AOAC, 21st Ed., FFA/Acid Value 2019/AOCS 7th Ed., 2017/ ISO 660

Melting Point Capillary, AOAC, 21st Ed., 2019/AOCS 7th Ed., 2017

Moisture Toluene Distillation, AOAC, 21st Ed., 2019/ AOCS 7th Ed., 2017

Moisture Hot Plate Method, AOAC, 21st Ed., 2019/ AOCS 7th Ed., 2017

Moisture and Volatile Matter (MVM)

Oven Method,

AOAC, 21st Ed., 2019/ AOCS 7th Ed., 2017/ ISO 662

Peroxide Value Titrimetry, AOAC, 21st Ed.,

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2019/ AOCS 7th Ed., 2017

Saponification Value Titrimetry, AOAC, 21st Ed., 2019/ AOCS 7th Ed., 2017

Smoke Point Cleveland cup, AOAC, 21st Ed., 2019/ AOCS 7th Ed., 2017

Specific Gravity Pycnometer, AOAC, 21st Ed., 2019

Unsaponifiable Matter Gravimetry, AOAC, 21st Ed., 2019/ AOCS 7th Ed., 2017

Iodine Value Titrimetry, AOAC, 21st Ed., 2019/ AOCS 7th Ed., 2017

Insoluble Impurities Gravimetry, AOAC, 21st Ed., 2019/ AOCS 7th Ed., 2017/ISO 663

Soap in oil Extraction/ AOAC, 21st Ed., 2019/ AOCS 6th Ed., 2011/ ISO 663

Detergents and related products

Soaps Chloride content Gravimetric Method, ISO 456-1973

Moisture Titrimetric Method, ISO 457-1983

Volatile matter content Oven Method,

Total Free alkali ISO 672-1978

Total Alkali content Gravimetric Method, ISO 684-1974

Total Fatty matter content Gravimetric Method, ISO 685-1975

Agricultural products and materials

Cereal grains and by- Crude Protein Kjeldahl Method, products AOAC 945.18 21st Ed., 2019

Crude Fat Ether Extraction, GAFTA 130 Method No. 3.0(2003) / AOAC, 21st Ed., 2019

Crude Fiber Conventional Method,

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GAFTA 130 No. 10.0 (2003)/ AOAC, 21st Ed., 2019

Moisture Oven method, GAFTA No. 130/ AOAC, 21st Ed., 2019

Gravimetric, PNS 1097:1993/ Ash AOAC, 21st Ed., 2019

Acid-Insoluble Ash Gravimetric, GAFTA No. 130 Method 13.0 (2003)/ AOAC, 21st Ed., 2019

Aflatoxin Rapid Screening, RIDASCREEN FAST Aflatoxin Manual/ AOAC, 21st Ed., 2019

Brix in Molasses Hydrometer Method, Official Chemical Handbook for Phil. Sugarcane Ind. (1992)

Calcium (Ca) Permanganate/ Volumetric Method, GAFTA No. 130 Method 16:1 (2003)/ In-house method/ AAS/ICP- OES

Gross Energy Calorimetry, PARR Manual/ AOAC, 20th Ed., 2016

Hydrocyanic Acid Titrimetric Method, AOAC 970.11 21st Ed., 2019

Phosphorus (P) Molybdo-Vanadate, GAFTA No. 130 Method 9.0 (2003)/ AOAC, 20th Ed., 2016

Total N Kjeldahl Method, AOAC 945.18 21st Ed., 2019

Urease Activity pH electrode, AOCS Ba 9-58/ AOAC, 21st Ed., 2019

Stockfeeds Crude Protein Kjeldahl Method, AOAC2001.11 21st Ed., 2019

Crude Fat (Non-milk based) Ether Extraction, GAFTA No. 130 Method 3.0 (2003)/ AOAC, 21st Ed., 2019

Crude Fat (milk-based) Roese-Gottlieb, AOAC

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932.06 21st Ed., 2019

Crude Fiber Conventional Method, GAFTA 130 Method 10.0/ AOAC, 21st Ed., 2019

Moisture Air-Oven method, GAFTA No. 130 (2003)/ AOAC, 21st Ed., 2019

Ash Gravimetric, GAFTA NO. 130 Method 12:0 (2003)/ AOAC, 21st Ed., 2019

Histamine Fluorometric Method/ AOAC, 21st Ed., 2019

Calcium (Ca) In-house method, AAS/ICP- OES

Permanganate Method, GAFTA No. 130 Method 16:1 (2003)

Phosphorus (P) Molybdo-Vanadate, GAFTA No. 130 Method 9:0 (2003)/ AOAC, 20th Ed., 2016

Purity of Food Supplements Food Chemicals Codex 3rd Ed. (1981); AOAC, 20th Ed., 2016

Calcium on Feed Supplements Permanganate, Volumetric/ GAFTA Procedures 2003/ AOAC, 20th Ed., 2016

Fluorine on Feed Supplements Ion-electrode, AOAC, 20th Ed., 2016

Cobalt in Cobalt Chloride, cobalt AAS/ ICP, AOAC, 20th Ed., sulphate on Feed Supplements 2016

Copper in copper sulphate on AAS/ICP-OES, In-house Feed method Supplements

Iron in Ferrous sulphate on Feed Supplements

Manganese in Manganese dioxide,

manganese sulfate on Feed

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Supplements

Potassium in potassium iodide on Feed Supplements

Selenium sodium selenite on Feed

Supplements

Zinc in Zinc oxide, zinc sulphate zinc

carbonate on Feed Supplements


Chlortetracycline Hydrochloride HPLC,

Oxytetracycline Hydrochloride QLY-LAB-1139



Vitamins and additives Vitamin A (Retinol) HPLC, QLY-LAB-1131

on stockfeeds Retinyl Acetate

Retinyl Palmitate

Vitamin A Precursor HPLC, QLY-LAB-1143 (Beta-carotene)







Vitamin B3 (Niacin, HPLC, QLY-LAB-1142 Niacinamide)





Fertilizers and liming materials

Applicable to all kinds of Nitrogen (Total) Modified Comprehensive Nitrogen fertilizers method/ AOAC 20th Ed., 2016

Metals in Fertilizer Microwave Digestion / ICP Finish, Arsenic AOAC 2006.3 Barium Cadmium

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Cobalt Chromium Lead Mercury Molybdenum Nickel Selenium

Tin

Organic Fertilizers Moisture Ash Organic Matter ASTM D2974

Not applicable in presence

Nitrogen, Ammoniacal Kjeldahl Method (Magnesium

of organic matter, calcium (N as NH4) Oxide Method), AOAC 20th Ed., cyanamide and urea 2016

Nitrogen, Nitrate Devarda Method, Based on (N as NO3) AOAC892.01 20th Ed., 2016

Sample Preparation

Phosphorus, Total Molybdovanado-phosphate (Total P2O5) (Spectrophotometry, AOAC958.01

21st Ed., 2019

Preparation of Solution

Phosphorus, Water Soluble Molybdovanado-phosphate (Water Soluble P2O5) method/ AOAC 970.01 21st Ed., 2019

Phosphorus, Citrate Soluble By Computation/ (Citrate Soluble P2O5) AOAC 960.01 21st Ed., 2019

Phosphorus Spectrophotometric (citrate insoluble) Molybdovanado-phosphate method/ AOAC 963.03 21st Ed., 2019

Phosphorus By Computation/AOAC 960.02 (available) 21st Ed., 2019

Potassium Sodium Tetraphenyl Borate (K2O) (STPB) Titration/ AOAC958.02 21st Ed., 2019

Sulfur Gravimetry/AOAC980.02a 21st Ed., 2019

Minor Nutrients: Magnesium, Cobalt,

Atomic Absorption Spectrophotometry AOAC 965.09

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Copper, Iron, Manganese, Molybdenum, Zinc) 21st Ed., 2019

(Carmine method) Boron Spectrophotometry/ Based on SMEWW, 22nd Ed., 2012

Organic Carbon Organic Matter

Black-Walkley method/ Laboratory

Manual for the analysis of Soils, Water, Fertilizers, Feeds, Plant Tissues, Sugarcane Juices and Sugars Phil. Sugarcane Commission, 1977

Not applicable in presence

Nitrogen (Ammoniacal) Magnesium Oxide Method,

of urea AOAC 920.03 21st Ed., 2019

Applicable to urea only Biuret AOAC 960.04 21st Ed., 2019

Di-Ammonium Phosphate Ammoniacal Nitrogen Kjeldahl Method (Magnesium (DAP) Oxide (MgO) Method), AOAC Mono-Ammonium 20th Ed., 2016

Phosphate Available P2O5 By Computation/AOAC 960.02 (MAP) 21st Ed., 2019

Ammonium Water Sol. P2O5 Molybdovanado-phosphate Phosphate method, AOAC 970.01

(NH4)2HPO4 21st Ed., 2019

Citrate Sol. P2O5 By Computation/ AOAC 960.01 21st Ed., 2019

Moisture Air-oven Method, AOAC 950.01 21st Ed., 2019 / GOST 20851.4-75

pH (10%) pH meter/ AOAC 20th Ed., 2016

Potassium Sulfate Volumetric Sodium Tetraphenyl (K2SO4) Total K2O Boron Method (STPB)/ AOAC 20th Ed., 2016

Sulfate Gravimetric Method, AOAC 20th Ed., 2016

Chloride Volhard Method, AOAC 20th Ed., 2016

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Moisture Air-oven Method, AOAC 950.01 21st Ed., 2019 /

GOST 20851.4-75

Potassium Nitrogen, Nitrate Devarda Method, AOAC 20th Nitrate (KNO3) Ed., 2016

Total K2O Volumetric Sodium Tetraphenyl Boron Method (STPB)/ AOAC 20th Ed., 2016

Trisodium Phosphate Total P2O5 Spectrophotometric Molybdovanado- (TSP) phosphate Method, AOAC 20th Ed., 2016

Available P2O5 AOAC 20th Ed., 2016

Water Soluble PO4 AOAC 20th Ed., 2016

Moisture Air-oven Method, AOAC 950.01 21st Ed., 2019 / GOST 20851.4-75

Ammonium Sulfate Ammoniacal Nitrogen Magnesium Oxide Method, (NH4)2SO4 AOAC 20th Ed., 2016

Free Acidity Titrimetric Method, AOAC 20th Ed., 2016

Air-oven Method, AOAC950.01 Moisture 21st Ed., 2019 / GOST 20851.4-75

Physical Form Visual/ AOAC 20th Ed., 2016

Muriate of Potash (MOP) Total K2O Volumetric Sodium Tetraphenyl Boron Method (STPB), AOAC 20th Ed., 2016

Soils Nitrogen (Total) Kjeltec Auto Analyzer or Rapid N III / Protein Analyzer/ Modified Comprehensive Nitrogen method/ AOAC 20th Ed., 2016

Minor Nutrients: Atomic Absorption Magnesium, Cobalt, Spectrophotometry/ Copper, Iron, Manganese, AOAC 20th Ed., 2016 Molybdenum, Zinc)

Phosphorus, Total (Total P2O5) Molybdovanado-phosphate (Spectrophotometry), AOAC 20th Ed., 2016

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Potassium (K2O) Sodium Tetraphenyl Borate (STPB)Titration., AOAC 20th Ed., 2016

Boron (Carmine method) Spectrophotometry, Based on SMEWW 22nd Ed., 2012

Sulfur Gravimetry, AOAC 20th Ed., 2016

Waters

Water potable and domestic

Arsenic, Total Hydride AAS, SMEWW 3114B,

purposes 23rd ed., 2017/ICP, SMEWW Drinking water 3120B, 23rd Ed., 2017

Water for irrigation and Arsenic, Dissolved Filtration, SMEWW3030B, 23rd stock Ed., 2017 and Hydride AAS, Waters for industrial and SMEWW 3114B, 23rd Ed., 2017 steam-raising purposes or ICP, SMEWW 3120B, Sewage 23rd Ed., 2017

Industrial waste Mercury, Total Cold-Vapor AAS SMEWW Saline waters 3112B, 23rd Ed., 2017

Bore waters Mercury, Dissolved Filtration, SMEWW 3030B, 23rd Ed., 2017, and Cold-Vapor

AAS SMEWW 3112B, 23rd Ed., 2017

Metals, Total (Silver, Calcium, Nitric Acid-Hydrochloric Acid Cadmium, Cobalt, Chromium, SMEWW 3030 For Nitric Acid Copper, Iron, Potassium, Digestion SMEWW 3030E and Magnesium, Manganese, AAS Direct Air-Acetylene Flame Sodium, Method) SMEWW 311B, Nickel, Antimony, Zinc) 23rd Ed., 2017

Metals, Total (Aluminum, Barium, 3030F (Nitric Acid-Hydrochloric Silicon, Tin, Titanium) Acid or 3030E (Nitric Acid Digestion) and 3111D (AAS Direct Nitrous Oxide-Acetylene Flame Method) SMEWW, 23rd Ed., 2017

Metals, Total (Silver, Aluminum, Nitric Acid-Hydrochloric Acid Boron, Barium, Beryllium, SMEWW 3030 For Nitric Acid

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Calcium, Cadmium, Cobalt, Digestion SMEWW 3030E

Chromium, Copper, Iron, and Potassium, Magnesium, Inductively Coupled Plasma Method

Manganese, Molybdenum, SMEWW 3120B, Sodium, Nickel, Phosphorus, 23rd Ed., 2017 Sulfur, Antimony, Selenium, Silicon, Tin, Strontium, Titanium, Thallium, Vanadium, Zinc)

Metals, Dissolved Filtration, SMEWW 3030Band

(Silver, Calcium, Cadmium AAS Direct Air-Acetylene Cobalt, Chromium, Copper, Flame Method) Iron, Potassium, Magnesium, SMEWW 311B, 23rd Ed., 2017 Manganese, Sodium, Nickel, Antimony, Zinc)

Metals, Dissolved (Aluminum, Filtration, SMEWW 3030Band Barium, Molybdenum, Silicon, AAS Direct Nitrous Oxide- Tin, Titanium) Acetylene Flame Method SMEWW 3111D, 23rd Ed., 2017

Metals, Dissolved (Silver, Filtration SMEWW 3030Band Aluminum, Boron, Barium, Inductively Coupled Plasma Beryllium, Calcium, Cadmium, Method SMEWW 3120B, Cobalt, Chromium, Copper, 23rd Ed., 2017 Iron, Potassium, Magnesium, Manganese, Molybdenum, Sodium, Nickel, Phosphorus, Sulfur, Antimony, Selenium, Silicon, Tin, Strontium, Titanium, Thallium, Vanadium, Zinc)

Lead, Total Nitric Acid Digestion SMEWW 3030E and AAS Direct Air- Acetylene Flame Method SMEWW 3111B, 23rd Ed., 2017

Nitric Acid Digestion SMEWW 3030E and Inductively Coupled Plasma Method SMEWW 3120B, 23rd Ed., 2017

Lead, Dissolved Filtration SMEWW 3030B and AAS Direct Air-Acetylene Flame

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Method SMEWW 3111B, 23rd Ed., 2017

Lead, Dissolved Filtration SMEWW 3030B and 3120B Inductively Coupled Plasma Method SMEWW 3120B, 23rd Ed., 2017

Alkalinity (Total, Hydroxide, Titration Method, SMEWW Carbonate, Bicarbonate Conc., 2320B 23rd Ed., 2017 Phenolphthalein, Methyl Orange)

Acidity Titration Method, SMEWW 2310B 23rd Ed., 2017

Chloride Argentometric Method, SMEWW4500-Cl- B, 23rd Ed., 2017

Residual Chlorine SMEWW 4500-Cl Method I, 23rd Ed., 2017

Total Hardness EDTA Titrimetric Method SMEWW2340C/ 2340B or By Calculation SMEWW 2340B 23rd Ed., 2017

Calcium Hardness EDTA Titrimetric Method SMEWW 3500-Ca B or By Calculation SMEWW 2340B, 23rd Ed., 2017

Magnesium Hardness EDTA Titrimetric Method SMEWW 2340C or By Calculation SMEWW 2340B, 23rd Ed., 2017

Cyanide (Free, without distillation) Cyanide-Selective Electrode Method SMEWW 4500-CN- F, 23rd Ed., 2017

Cyanide (Free, with distillation) Cyanide-Selective Electrode Method SMEWW 4500-CN- F, 23rd Ed., 2017 and SOL85W

Cyanide (Total) Total Cyanide after Distillation SMEWW 4500-CN- C, 23rd Ed., 2017 and SOL85W

Cyanide (WAD) Weak Acid Dissociable Cyanide

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SMEWW4500-CN- I, 23rd Ed., 2017 and SOL85W

pH Electrometric Method SMEWW4500-H+ B, 23rd Ed., 2017

Conductivity SMEWW2510B, 23rd Ed., 2017

Salinity SMEWW 2520, 23rd Ed., 2017

Temperature SMEWW 2550B, 23rd Ed., 2017

Ammonia/ Ammonia as N Photometry (By Computation from Merck SQ Nova 60 Method 54)

Ammonium/ Ammonium as N Photometry (Merck SQ Nova 60 Method 54)

Nitrate / Nitrate as N Photometry (Merck SQ Nova 60 Method 60)

Fluoride Photometry Merck SQ Nova 60 Method 166

Formaldehyde Photometry (Merck SQ Nova 60 Method 91)

Hydrogen Sulfide/ Sulfide Photometry (Merck SQ Nova 60 Method 80)

Turbidity Photometry (Merck SQ Nova 60 Method 77)

Ammonia/ Ammonia as N Phenate Method SMEWW4500- NH3 F, 23rd Ed., 2017

Chromium Hexavalent Colorimetric Method, SMEWW3500-Cr B, 23rd Ed., 2017

Free Chlorine DPD Colorimetric Method, SMEWW4500-Cl G, 23rd Ed., 2017

Nitrate / Nitrate as N Colorimetric – Brucine, USEPA 352.1

Nitrite/ Nitrite as N Colorimetric, SMEWW 4500-NO2 B 23rd ed., 2017

Phosphorus/ Phosphate as P/ Vanado-molybdophosphoric Phosphate Acid Colorimetric SMEWW

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4500-P C/Stannous Chloride, SMEWW4500-P D, 23rd Ed., 2017

Silica Molybdosilicate Method SMEWW4500-SiO2 C, 23rd Ed., 2017

Sulfate Turbidimetric Method, SMEWW4500-SO4

2- E, 23rd Ed., 2017

Settleable Solids (Imhoff Cone Method) SMEWW, 23rd Ed., 2017

Total Solids Gravimetry, Dried at 103-105C SMEWW2540F, 23rd Ed., 2017

Total Dissolved Solids Gravimetry, Dried at 180C SMEWW2540C, 23rd Ed., 2017

Total Suspended Solids Gravimetry, Dried at 103-105C, SMEWW 2540D, 23rd Ed., 2017

Volatile Solids/ Volatile Gravimetry, Ignited at 550C Suspended Solids SMEWW2540E, 23rd Ed., 2017

True Color Visual Comparison, SMEWW 2120B, 23rd Ed., 2017

Apparent Color Visual Comparison, unfiltered sample, SMEWW2120B, 23rd Ed., 2017

Odor Threshold Odor Test) SMEWW2150B, 23rd Ed., 2017

Biochemical Oxygen Demand 5-day BOD Test SMEWW5210B, 23rd Ed., 2017

Chemical Oxygen Demand Open Reflux Method, SMEWW 5220B, 23rd Ed., 2017

Dissolved Oxygen (DO) Azide Modification, SMEWW4500-O C, 23rd Ed., 2017

Oil and Grease Liquid-Liquid Partition- Gravimetric Method, Petroleum Ether Extraction/ n-Hexane

Extraction, SMEWW 5520B, 23rd Ed., 2017

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Anionic Surfactants as MBAS, Surfactants SMEWW 5540C, 23rd Ed., 2017

Chloroform Extraction Method, Phenols SMEWW 5530C, 23rd Ed., 2017

Constituents of the Environment

Air (Stack/Source Emission)

Sulfur Dioxide (SO2) Barium-Thorin Titration Method,

USEPA Method 6 & 8

Nitrogen Dioxide (NO2) Phenoldisulfonic Colorimetric Method, USEPA Method 7

Particulate Matter (PM) Gravimetric Method, USEPA Method 5

Arsenic (As) AAS-Hydride Technique, ICP-OES USEPA Method 29

Mercury (Hg) AAS-Cold Vapor, USEPA Method 29

Silver AAS/ICP-OES, USEPA Copper Method 29 Cobalt Zinc Barium Cadmium Chromium Nickel Lead Antimony

Manganese

Phosphorus ICP-OES, USEPA Method 29 Selenium Thallium Vanadium Beryllium

Air (Ambient) Ammonia (NH3) Part II 401 (Indophenol Soils Method)/ Methods of Air Sediments Sampling and Analysis

Sludges Formaldehyde Part II 116 (Colorimetric Method)/ Methods of Air

Sampling and Analysis

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Hydrogen Sulfide Methylene Blue Method

Nitrate Part II 404 (Brucine Method) / Methods of Air Sampling and Analysis

Total Oxidants as Ozone Part II 411 (NBKI Method) / Methods of Air Sampling and Analysis and Philippine Standard Methods for Air and Water Analysis Volume 3 Section 4 Chapter 11

Sulfur Dioxide (SO2) Pararosaniline Method, CFR 40 Part 50 Appendix A

Nitrogen Dioxide (NO2) Part II 406 (Griess-Saltzman Reaction Method) / Methods of Air Sampling and Analysis

Suspended Particulate Matter High Volume Gravimetric Method, CFR 40 Part 50 Appendix B

Particulate Matter as PM10 Gravimetric Method, CFR 40 Part 50 Appendix J

Lead (Pb) AAS, CFR 40 Part 50 Appendix G

Moisture Gravimetric, ASTM D2216

Arsenic (As) USEPA 3050B Manual Hydride AAS / ICP

Mercury (Hg) USEPA 7471B Cold-Vapor AAS Silver AAS/ICP, USEPA 3050B Calcium Copper Cobalt Iron Potassium Magnesium Manganese Sodium Zinc Barium

Aluminum Cadmium

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Chromium Nickel Lead Antimony Silicon Tin Titanium

Boron, ICP, USEPA 3050B Phosphorus Selenium, Strontium Thallium Vanadium Beryllium Molybdenum Sulfur

Cyanide (Free, without distillation) Cyanide-Selective Electrode Method SMEWW4500-CN- A and F, 23rd Ed., 2017

Cyanide-Selective Electrode Cyanide (Free, with distillation) Method, SMEWW4500-CN-F, 23rd Ed., 2017 and SOL85W

Total Cyanide after Distillation, Cyanide (Total) SMEWW4500-CN- C, 23rd Ed., 2017, and SOL85W

Alkaline Digestion and Chromium Hexavalent Colorimetric Method, USEPA Method 3060A and 7196A

Total Solids/ Volatile Solids Gravimetry, SMEWW2540G, 23rd Ed., 2017

Phosphorus SMEWW4500-P B and C, 23rd Ed., 2017

Organic Matter Black & Walkley/ Lab Manual Organic Carbon for the Analyses of Soils, water, fertilizers, feeds, plant tissues,

sugarcane juices & sugars,

pH (1:1) AOAC 21st Ed., 2019

Workplace environments and hazards

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Nuisance Dust Total Nuisance Dust NIOSH 500

(Respirable Total Dust) Total Respirable Dust NIOSH 600

Alkaline Dusts (as NaOH) NIOSH 7401

Organic Solvents/vapours

Acetone NIOSH 1300

Acetonitrile NIOSH 1606

Ethanol Isopropyl Alcohol NIOSH 1400

Benzene,Toluene,Ethylbenzene, NIOSH 1501 Xylene (Total)

Petroleum Ether NIOSH 1550

Methylene Chloride NIOSH 1005

Formaldehyde Methods of Air Sampling and Analysis Part II Method 116

Inorganic chemical Aluminum& compounds (as Al) NIOSH 7013

Calcium and compounds NIOSH 7020

(as Ca)

Copper and compounds NIOSH 7029

(as Cu)

Lead NIOSH 7082

Aluminum NIOSH 7300, 7301, 7303

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead

Magnesium

Manganese

Molybdenum

Nickel

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Phosphorus

Potassium

Selenium

Silver

Sodium

Thallium

Tin

Titanium

Vanadium

Zinc

Other substances Ammonia Methods of Air Sampling and Analysis Part II Method 401

Nitrogen Dioxide Methods of Air Sampling and Analysis Section 4 Chapter 11

Oxidizing Substances (as Philippine Standard Methods for Ozone) Air and Water Analysis Volume 3 Section 4 Chapter 11; Methods of Air Sampling and Analysis Part II Method 411

Sulfur Dioxide CFR 40 Part 50 Appendix A; Philippine Standard Methods for Air and Water Analysis Volume 3 Section 4 Chapter 12

Carbon Black NIOSH 5000

Residues in Constituents of the Environment

Pesticides Organochlorine Pesticides Gas Chromatography, Determined: QLY-LAB-1150

Alpha-BHC QLY-LAB-1155

Beta-BHC

Lindane

Aldrin

Dieldrin

Endrin

Heptachlor

Heptachlor Epoxide

Chlordane

Endosulfan I

Endosulfan II

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DDT

DDD

DDE

Methoxychlor

Organochlorine pesticides Multi- Residue Analysis

Organophosphorus Pesticides Determined:

Methyl Parathion

Ethion

Azinophos Methyl

Disulpoton

Naled

Diazinon

Malathion

Phorate

Organophosphorus Multi-Residue Analysis

Any Multi-residue or Individual Pesticide

Residue Analysis

PCBs

Organophosphate Pesticides in Water

Organochlorine pesticides in water

Polyhalogenated biphenyls

PCBs in water GC/ SMEWW, 22nd Ed., 2012

PCBs in soil Gas Chromatography

PCBs in transformer oil Gas Chromatography, 6420, SMEWW, 22nd Ed., 2012

Phenols Phenols in water Gas Chromatography, 6420, SMEWW, 22nd Ed., 2012

Particle Sizing

Sieve Analysis: Mesh No. ASTM D359/ ASTM D501 (10/12/14/16/18/20/30/35/40/50/

60/70/80/100/120/140/200/325)

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Laboratory Reagents

Laboratory Reagents Moisture/ Loss on Drying ASTM, FCC, USP methods

Loss on Ignition ASTM, FCC, USP methods

Residue on Ignition ASTM, FCC, USP methods

Elements: AAS/ ICP-OES/ FCC/USP Aluminum Shimadzu and Ethos Manuals Antimony AAS/ ICP-OES/ FCC/USP Arsenic Shimadzu and Ethos Manuals Barium Cadmium Calcium Chromium Cobalt

Copper

Iron Lead Magnesium Manganese Mercury Molybdenum Nickel Phosphorus Potassium Selenium Silicon Sodium Strontium Thallium Tin Titanium Zinc

Miscellaneous Materials and Products

Food container / Migration Test (BFAD Packaging Requirements) Japan Food Sanitation Law's - UV Examination Specifications and Standards - Residue on Evaporation for Food and Food Additives - - Potassium Permanganate Notification No. 370 (Japan - Consumption External Trade Organization

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- Migration of Lead and Clause II) Cadmium Residue on Ignition

Migration Tests (US 21 CFR Requirements)

Aqueous Film Forming pH Measurement by the Foam use of pH meter

Concentrate (AFFF) for Specific gravity Measurement by the use of Foam Fire extinguisher pycnometer, ASTM D891-09

Density Measurement by the use of pycnometer, ASTM D3505-12

Protein Kjeltec Analyzer/ FOSS

Manual Kjeltec 8400 Analyzer/ Rapid N Protein Analyzer / AOAC, 19th Ed., 2012

Mono-Ammonium % Purity Spectrophotometric Phosphate (MAP) Molybdovanado-Mono- for Dry Chemical Ammonium phosphate Fire Extinguisher Method/ AOAC 958.01 19th Ed. 2012

Appearance Visual Inspection/ PNS 15 Part 1: 1989

Particle Size Sieve analysis by

ASTM B214-07

Legend to Reference Standards: ASTM - American Society for Testing Materials

AOAC - Association of Official Analytical Chemists PNS - Philippine National Standard

PAB ACCREDITED

TESTING LABORATORY PNS ISO/IEC 17025:2017

LA-1996-011F

JAMES E. EMPEÑO Director IV Philippine Accreditation Bureau

SCOPE OF ACCREDITATION SGS Philippines, Inc. Multi-Laboratory

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