NARRATIVE - GC/MS ANALYSIS OCTOBER, 1987 · NARRATIVE - GC/MS ANALYSIS ROX P. WESTON - UPSHUR...

B, S, Slluji, P.E,Prttldint

1258 Qreonbrlsr StrutChirlailon, WV 25311

304.348-0725

teshcNARRATIVE - GC/MS ANALYSIS

ROX P. WESTON - UPSHUR COUNTY 4-H TARPIT PROJECT

OCTOBER, 1987

1. Since only two liters of sample L01 (H3895) were available,one liter was used for sample analysis and the second literwas split in hali for the matrix spike/matrix spikeduplicate,

2. TTL's high level surrogate spiking solution contains <~J 16%toluene in order to increase the soluability of terphenyl.This is the source of the toluene peak in the soil/sludgeextracts.

3, The high level soil procedure was used for the soil/sludgesamples based on initial screening results. The fined volumeof extract was 10 ml and was not further reduced. For thepurposes of calculation this is recorded as a 1 to 10dilution.

4. Total ion chromatograms are included for each sample extract.Surrogate:! are labled "SRG" and internal standards are labled"IS". Any reported priority pollutants are also labled.Several additional peaks were searched (NBS) and thatinformation is also provided.

5. NaiJjthtlena was tentatively identified in two samples. Aspectrum could not be obtained due to apparent

tlon of a substituted phenol.

6. Staple 8pT4 contained a trace amount of 2,4-Dimethyl phenol ata concentration below our method detection limit. The valuereported is an estimated value.

RRIOOOQ2

Consulting Antlyiti ind EnglnMra, Sampling ind Anilyilt of Witir, Coal, Sollr, ind Huirdoui Wilt*

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'3 H H H HH in « N m r4 «K 3 3 3 33 W U UU1WUHSin m m 10 in o g 01 r> oo u> mcncnffi fj\ o\ o D o^cn o\ o\ o\oooooooo ojoo en > 0300000000

1RI00007

TECHNICAL TEBTINO LABORATORIES, INC » !PFTPP TUNXNQ RECORDi 625-624

'.

I ^ ' ' . • . " '*JS, TUNE'- UNUORMAIilZED ''.:!.'!.' ,. ,,. ••N-. . '. •• •vi .rj-w. >"'••••' '• ' ; '• •, /Wrtj . • '.'• :;:i: Ji './:-- ••;.;•' ' , • :':'1,' flali J.73ug/ml DFWP RT fi Tf tw. AREA ' o)j73ft fs

DATE FILENAME ' TIME RANGE OF AVERAGE SPECTRUM

•f'f.•«MASS EPA CRITERIA , TTfCRITERIA IABD. PASS

51 130-401 of 198] . I.!.v!..'}! ^ ' ^

68 l< 21 of 198] .••'•(>.;'.t V, J :' •• * I

69. I .''-.' *] ' '•''':({!( l''11"'?!! - '•''.. '' 1 pi ___:' '•'' ' • I'-'?-'1 \ni;Sl '('r ~7!—~~ *;.70 .. [< 21 of 198] . ( '• ;;>il -;;>, ) •: I ,___

'•J •'.'" l P60l of 198] '••'.irT'il ' •' ^ ———

^97 (. l< It of 198] I .-•-'' I ^f ___

'199 '^ .[5-91 of 198] . . [ ; • ] ' "

275 110-301 of 198] , l''r;.-]

365 (> 1% of 198] I y> ] >,W __NR_1 ' ' ' i

441 (preaent but < 443] ;: ' 1° ^

442 ' ' [40-106* of 198] • ' l,,"V/') ' ...ZL_ _*'——

443 •' 117-23* of 442] I1'',..'! , 7/ )7 ^

ANALYST

"'f)(?

ANALYST

flvaraao of 9.582 to 9,694 mln. fron DflTfl:30FTPKI8,DIUL DFTPP.50 UG/ML

n/z abund. n/: abund. n/z abund. n/z abund.

39.00 4 92,00 I 148.00 2 211,00 I48.00 5 93.00 5 149.00 I 217.00 541,00 I 99,00 3 155,00 I 219.00 944.00 4 99,00 3 156.00 2 221.00 850,00 13 100,00 I 161.00 I 223.00 I

SI. 00_____Jfi_ 101,00 2 165.00 I 224,00 II52.00 2 103,00 I 166,00 I 225,00 355,00 I 104,00 I 167.00 4 227.00 356.00 I 105.00 I 168.00 2 244.00 957.00 4 107.00 12 174.00 I 245.00 K

•V63.00 2 108,00 2 175,00 1 246,00 It64,00 I 110,00 28 177.00 I 255.00 39'65.00 I 111,00 4 179.00 3 256.00 6BJ.00_____72 116.00 I 180.00 2 258.00 273,00 I 117,00 6 181.00 I 273.00 I

74.00 4 123.00 I 185.00 I 274.00 375,00 8 127.08_____44_ 186.00 12 275.00_____L3_76,00 2 128,00 3 167,00 3 276.00 277.00 45 129,00 19 192.00 I 277.00 I78.00 3 130,00 I 193.00 I 296.00 4

79.00 3 131.00 B 196.00 4 323.00 I80.00 ' 2 135.00 i 198.00 iaa jss.BB81.00 3 136.00 I 199.00_____6__423.0083.09. .<-.,•' 1 137,00 I 204.00 2 441.00,

M7.00 i 207.00 3 444.00

93,0»::ij|iifeji'i!;l(. 141.00 2 205.00 S 442.00____TL.

142,00 I 206.00 59 443.00_____13

AfllOQO!

kt.ullll ,LV,<ti, 1L.JA..IU IjllUbMUUUIVliliJ

CONTINUING CALIBRATION AND SVSTEM RESPONSE.CHECKGC/HS EXTRACTA8LES

• IN

TODAY'S DATE l|- 1$ '^FILENAME IcCjftlf HSD0 ? CONC OF STANDARD &° »g/ml

INITIAL CALIBRATION PATE \I-I1-ll ANALYSTJ

CONT1NIUNG CALIBRATION CIIECKMCCC)

PARAMETER

PHENOL

1,4-DICIILOROBENZEN.E

2-NlTRQPHENOL

2,4-DiClPHENOL

HEXACHLOROBUTADIENE

4-Cl-3-MePHENOL

2,4,6-TRICHLOROPHENOL

ACENAPHTHENE

n-NITROSODIPHENYL|AHINE '

1

01-n-OCTYLPH.THALATE

BENZO[a]PYRENE '> i • . , • '

MEAN RF**.

/(^/>0

1,110

O. 2"?«»W2./V . '

0,160p.nii •|.lo»

0.1*10,110

1.066'2.HS'O, $06"

RfAAA

\.6TS1.2.11

Q.Wo.uoO.iirfa3\0.1 »l.i»i/*) '34 4

0.IUl-fitl

/, Uf •o.f'K

XUi££

2.3 il.o I

<i.n1.1 1li'l iI/. 2*in1.21

' /</. 2 ilO.oi

ttlMl/i.'n

ACCEPT

25%

25X

25%

25*

25%

25%

25%

25%

25%

252

—— 25* ———

25*

—— 25? ———

OK

•

^

^

"

-

-

u-

>

•iis

^'^

SKSTEM PERFORMANCE CHECKMSPCJ

PARAMETER . . P.F*** Mlnlmuu RF .

— •— ' """ , 0.050n-NITROSODIPROPYLAMINi 0. J f

HEXACHLOROC^IHHTDIEt g^rf ' : , M5°'• 'iKi >'<•>;' n nin

2,4-DINITRO||lWOL ^/^^ .U>USU . ,.

4-NITROPHENOL . ', . , °'05?, . ..

OK

.« ' '

^

(S

^

•

ASH-846,3RD ED.** Mean RF from Initial calibration'*** RF from today's runRF-AREAstd/AREAlsACONCisACONCatd AR I 000 I 2

. TTL8707.1 •

TECHNICAL TESTING LABORATORIES, INC,DFTPP TUNING RECORDi 625-624 'MS TUNE - UNNORMALUED

•.T .1,' .luli rtfug/ml DFTPP RT /MMmL AREft

•'•:'• DATE FILENAME TIME RANGE OF AVERAGE SPECTRUM." |i • i ..-.if. ocr,

I

MASS' EPA CRITERIA . TTlT CRITERIA tABD. PASS

51 . 130-40% of 198] , l/,Ci»X'l S{° ' *..

68 [< 21 of 198] . . lV. J. ' C/ *

441 [present but < 443]

442 " [40-106* of 198] I

443 [in*?! of 442] [

69 i - -i ;; i;-:.M - •' -JA.'»', '

21 of 198] [>..<, }' ''•''•'.'

127 ' I<$p60t of 1981 [ '' ]'• ,1

•,197 [< It of 1981 I - 1•„, v . .;.'' 199 . [5-9t of 1981 I • 1

•,:: 275 [10-30* of 198] , I1'.' -1 —13.—— ————• r • n • " ^

..'•"},>. 365 I > It'of 1981 I •' 1 BS—— ——NR—

'ANALYST

... ,; COR^ECWVE .ACT10N4

;•;,•' ,'•• / 'AR10001 If

ANALYST

TUNE Version 3.1.1 7-Mer-flfiTune parameters rear* from file «JSTUME,U

Tune parameters stored In file iJSTUME.U

(Vierag* of 9.971 to 18.156 nln. from QftTftiDFTPJ2B.QIUL DFTPP,59 US/ML

nit abund. m/z abund. n/z ahund, m/z abund.

36.ee 7 83.aa i U2.ae i 2ii.ee i37,aa i 84.aa 6 U7.aa i 217.ea 538.80 3 85.ea 2 148,90 Z 22l.ee 639,ae 6 86.ee s ts3.ee t 223.aa i48.0a 2 9i.aa i iss.ea i 224.aa 104i,ea 2 92.aa i isa.aa i 225.ee 242,ea i 93.ee s lee.ee i 227.ee 443.ee 2 98.ae 4 isi.aa i 22a.ee i44.ea is 99.aa 3 iss.ea i 229.ee i45.aa i iea.ee i iBB.aa i 244.ea a

iei.ee 2 I67.eo 4 245,ae iia3.ee i i68.ee i 246.aa i184.ae i 174.ea i 255.ee 39ies.ee' i 175.aa i 256,aa sia7,ee 12 wa.ae i 258.ee 2

2 177,09 I 265.B9 134 179.09 3 273.BO 14 iae.ee 2 274,aa 3i iai.aa i 275.ae___197 185.aa i 276.ae 2

188.08 11 277.ae i187,08 3 298.aa 4189.aa i 297,aa192.aa i 323.ae i193,08 i 334.ea i

, i24,aaaa / 125,ea

73, ee 2 i27_.ae ___ «a i^B.aa 3 36S.ee 274.ee s I28,ao 3 igg.aa ___ IBB L372.aa i75. aa , a 129, ea 20 i99,aa ____ j_ 423jpfc . 377. ae /' 53 139. ea 2 204, ea 3 4Z4?78, aa--1' 4 131. aa i 2as.ea 3 44i.ae79. 0a ' 4 135, aa i 2a6.«a 19 442 ,ae ___ et88,89 3 136,90 I 207.98 '3 443. ea _____ IIai.ae n i37.ee i zea.aa i 444. ea i82, aa I 141,89 2

I,,, '' • '. CONTINUINa CALIBRATION AND SY8TBHI MBPOMSB(, CHECK,.

rf'v,'" '••' • . ': .v'v'(i'''' S?£|S|.;.....i,., .TODAY'S DAIEOCfZMlg? FILEHAHB J.CCCTa.1 MBDl j COMO. OMIAMDARD k'O ug/ml,

\. ' IHITIALjOAlIBiAWiyK h- y MIM.W''"'J

1

j

••

r . '

PARAMETER

PHENOL

M-DICHLOROBENZENE

'2-NITROPHENOL

2,4-DlClPHENOL '

HEXACHLOROBUTADIENE

4-Cl-3-MePHENOL

2,4,.6-TRICHLOROPHENOL

ACENAPHTHENE

n-NITROSODIPHRUYLlAMINE

PENTACHLOROPHENOL

7LOURAHTHEHE "•"" \

Pi-n-OCTYLPHTHALATE

BENZO(a]PYRENE '' ' i ',' ' . , ' . '

MEAN RF **.

/'?/?

//9o6, 00

o-Wtcv/83t , '0'A.t/o,if!3 ')• Xo/*'*/y5"a,/7W

/, 045-7,

a.'A»%7•. OJ-..

, RfMft

/;<?o9'/1IM73iasis0-3-/30

o,/Woisrs-oo( fA.

U33IC(V777

Mff?

o,S?H

a,lb?3 •0,9*1?

nut

9,0. 'J/,l

, 75:-

n,i0,4

ffift

a.QkSU'7,3

C D)f,T^fair

ACCEPT '

1 25X

25X

25X

25X

25X

25* '

—— DX ———— 25iE ———

—— 25! ———

—— 251 ——— '

25% ' '

— zsit ———— BX ——

SYSTEM. PERFORMANCE CHECK* (SPC) .

PARAMETER , , M*** Minimum RF . OK

n-NITAOSODIPROPYLAMIHI 0,317?" °'°50 • ^

HEXACHLOROCj||)fHTDIBlA{l«f3r"': , ,0|05° . .

2,4-DINITRc||ioL gltllfr ;9.W , ,, •

'A-NITROPHENOL o,»«r . , ', .. °'° r,.,.,. -^ '

OK

^

•

•

•

^

^

•^

vfm^>M>\\iia,"tU«||pI/

I/

K

.

ASH-846,3RD ED.** Mean RF from Initial calibration.M* » (ton today's rimRF-AREAatd/AREAlB*CONCl8*CONCatd

TTL8707.1 •"''

TECHNICAL TESTINQ LABORATORIES, INC, ' '. .PFTPP TUNING RECORD! 625-624 ' .. .."• ',*JS, TUNE'-^NORMALIZED '•/.:..;> ;' ... ,

•!( 1.,'fJuli >2Pug/ml DFTPP RT *?/dSf 'hL. AREA ' j73.9 ./<{

;.'• DATE FILENAME TIME RANGE OF AVERAGE SPECTRUM

• , , •.,';,•MASS' EPA CRITERIA , TTL~ CRITERIA tABD. PASS

51 [30-aO! o£ 198] , I !..•„';)

6B l< 21 oJ 198) , ';..•', I £*> 1

.69 , i . /. •] •:' !'; |f i!;!'t:hif; i >i |"'

•70 [< 2t of 198) Jil ., ]

~\ll ' I r60l of 198] lO;;l

197 , [< II of 198] (.- ' ]

199 [5-9» of 198] I • )

275 [10-301 of 198] , l':\.-1

365 [> It of 198]

141

442 " '

443 ' '

'0/5

ANALYST

flvaraga of 9. 578 to 9.724 nln. fron QftTA:3DFTPKI9.D

n/z abund, n/z atmnd, m/z abund. pi/z abund,

39,00 s 99.ee 3 iE7.ee 3 229, ee i41.8'} i iee,ee 2 iB8.ee z 243.ee i43.ee i iei.ee 2 i7s.ee i S44.ee s44, ee z ie4.ee i i76.ee i S4S.ee ise.ee M ies.ee i i77.ee i 24S.ee i5j.e.g ___ 54 ie7.oe 12 179. e0 3 25B.ee 39sz.ee 2 ies.ee 2 iee.ee 2 sss.ee sss.ee i ne.ee 29 isi.ee i zss.ee 256.00 z iii.ee 4 iss.ee i 265,00 i57.ee 4 iia.ee i i8B.ee n 273.ee i;si.ee i ii7, ee 7 I87.ee 3 Z74.ee 362.00 I 123.00 I 189.00 I 275.00 _____ 2J_63.00 2 124.00 I 191.00 I 276.00 365.00 I 127,00 44 193.00 I Z77.00 I.Ea afl ___ Z2_J28,00 3 196. ee 4 296. ee b74.ee s I29.ee 19 i98.ea ___ L22_ 297.007S.ee 8 i30.ee 2 lauaa ___ B__303.0e77.ee se i3i.ee 3 204.ee 3 216.0078.00 3 i35.ee 2 zes.ee 4 323.0079.00 3 I3B.00 I Z0B.ee 19 334,00

80.00 3 137.00 I 207.00 3 354.00 I81.00 4 141.00 2 211.00 1 365.00 _____ 2_82. 00 I 142.00 I 217.00 5 372.ee I83,00 I I47.e0 I 219,00 5 423.00 485,0e : i M8.ee 2 22i.ee B 424.00 i

.,'>•• £1

86.00 'fj;. I 155.00 I 223.0B I 441.00 _____ LL91.00 w | 156. B0 2 224.00 10 442. B0 _____ B3_32,00 i i6i.ee i 2zs, 00 3 443.00 ___ ia_93.00 5 IB5.ee I 227.ee 4 444.00 I98,00 3

............. .„„,»„„ 1,/ujuHrtlUHUSCONTINUING CALIBRATION AMU SYSTEM RESPONSE.CHECK

. . GC/tIS EXTRACTAJJLES

TODAY'S DATE iMfylln. FILENAME .CC3KI1 HSDlT? CONC OF STANDARD 6& lie/nil

INITIAL CALIBRATION DATE ll-f>-%7 ANALYST^

CONTINUING CALIBRATION CHECK*(CCC)

.

..,..,

.

i

PARAMETER

PHENOL 1

M-DICHLOROBENZEN.E

2-NlTROPHENOL

2,4-UiClPHENOL '

HEXACHLOROBUTADIENE

4-Cl-3-MePHENOL

2,4,.6-TRICHLOROPHENOL

ACENAPHTHENE

n-NITROSODIPHENYLAMINE

tEHTACIlLOROPIItHOL

t'LUUHAHTIIEHE :

pi-n-OCTYLPH-THALATE

BENZO(aJPYRENE 'i i .' ' , • , • '

PARAMETER .

MEAN RF**.

;,//>°1.1100. 1'el0.111

0'iil •'0.160&.mi •1.%0\O.Hil0,lio1.066'l.lts'ow&<

lifAAA

/,l?//.aj3o./nio.as»<v«.ifj»ei 2,300Wltf/,/ai«.Wa«,MJlift4»SV .

fl,jf56

'Milt

/•i8

•H,1 .• ~f,7-11-u,r-us"\,l-t,fc'-/?,-*-3,|H,t-8,1H.).

ACCEPT

25%

25%

25%

25%

25%

25%

25%

25%

25%

25%

25%

25X

25%

SYSTEM. PERFORHANCE CHECK* (SPC) .

•',

n-NITROSODIPROPYLAMIHI

IIEXACIlLOROCYCi>INTDIEh

2,1-DINITROPHiNOL

4-NITROPHENOL

RF***

t.XlSi

0, 911

t>,l3lf

0,'jLlfO

Mlnimun RF .

U.U50

U.U5U

0.05U

. U.050, 1 . 1 . . t . -,

OK

.1 ' '

•

VI/

OK

•

»/

•"

•

•

•

<

tf

•

V

Vi/s

•

.... .6,3RD EU.AA Mean RF from initial calibration*** RF from today's run flft | OflOPn

, RF"AREAatd/ARBAi8ACONCiB*CONCatd utU*w< •'

*—' TTL8707.1

LABORATORY ANALYSIS REPORT

ROY F. HEfJTOfl, ..TPC. ___________ LAB. NO.

Rqlph MPKPPI __________ DATE SAMPLED 10/7/1907

IJpghur County 4-H Oamp Tarpifr- DATE RECEIVED

Field Blank _____________ DATE ANALYZED _liU2fiZ12JLZ

AK.A.V.T HL/JER

NOTK; AH. RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < a LESS THANBASE/NEUTRAL EXI'RACTABLES

PAGE 1

Method Detection IPARAMETERS Reaulta (m;/l) __Limit (ug/1)N-Nitrosodimethylamine ND 50Bia(2-chloroethyl)ether ND 101,3-Dichlorobenzene ND 101,4-Dichlorobenzene ND 101,2-Dichlorobenzene ND -10Bi3(2-chloroiaopropyl)ether ND 10N-Nitrosodi-n-propylamine ND 20Nitrobenzene . ND 10Hexachlorobutadiene ND 101,2,4-Trichlorobenzene ND 10laophorone ND 10Naphthalene ND 10Bis(2-Chloroethoxy)methane ND 10Hexachlorocyclopentadiene ND 102-C.hloronaphthalene ND 10Acenaphthylene ND 10Acenaphthene ND 10Diniethylphthalate ND 102,6-Dinittotoluene ND 10Fluorene ND 104-Chlorophujylphenylether ND 102,4-DinitriMiluana ND 10Hexachlordlulina ND 10MPLI HBtho^D«t«ction LimitNDi Not detected at a concentration equal to or greater than the MDL

RESPECTFULLY SUBMITTEDiJk:

1256 GREENBRIER STREET CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 304 346-0725


ROY F. WESTQN, INC. _________ LAB, NO, H3894

Attn; Ralph_HcKeen ________ DATE SAMPLED 10/7/19B7

Upahur County 4-H Camp Tarpit 0/ 75 RECEIVED 10/10/1987

_ Piqld Blank __________________ DATE ANALYZED 12/li/liiZ.

Water __________________ ANALYST

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < = LESS THANBASE/NEUTRAL EXTRACTABLES

PAGE 2

Method DetectionPARAMETERS Results (ug/1) Limit (uq/1)

Diethylphthalate ND 10N-Nitroaodiphenylamihe ND 20Hexachlorobenzene ND 104-Bromophenylphenylether ND 10Phenanthrene ND 10Anthracene ND 10Dibutylphthalate ND 10Fluoranthene ND 10Pyrene ND 10Benzidine ND 50Butylbenzylphthalate ND 10Bis(2-ethylhexyl)phthalate ND 10Chrysene ND 10Benzol a) anthracene ND 103,3'-Dichlorobenzidine ND SODi-n-octylphthalate ND 10Benzo(b)fluoranthene ND 10Benzo(k)fluoranthene ND 10Benzo(a) Pyrene ND 10Indeno(l,2,,3-c,d)pyrene ND 20Dihenzo(a,trt»nthracene ND 20Benzo( ghi)«rylene ND 20

MDLi MethodTDataction LimitNDi Not detected at a concentration equal to or greater than the MDL

ARI00022. ' RESPECTFULLY SUBMITTED:



ROY F. WESTON. INC. _________ Ua N0, H3B04

Attnt Ralph HcKeen ________ DATE SAMPLED 10/7/19R7

Upahur County 4-H Camp Tarpit DATE RECEIVED 10/10/1987Technical__ IJSU Blank —————————————— DATE ANALYZED _U/IiZI987' Inc.

Water _________________ ANALYST

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < = LESS THAN

ACID EXTRACTABLES

Method DetectionPARAMETERS Reaulta (uq/1)

Phenol ND 102-Chlorophenol ND 102-Nitrophenol ND 102,4-Dimethylphenol ND 102,4-Dichlorophenol ND 104~Chloro-3-methylphenol ND 102,4,6-Trichlorophenol ND , 102,4-Dinitrophenol ND SO4-Nitrophenol . ND 502-Methyl-4,6-dinitrophenol ND 5CPentachlorophenol ND 50

•*Ejfr'*'t ••MDLi H»mia* Dttection Limit.

NofBiiittpted «t a concentration equal to or greater than the MDL.

Ml 00023RESPECTFULLY SUBMITTED;..].;*


TIC of DnTA!RW3B94ft.O

") a-

K-

/**•.».-P-

End of plot. Tine • 3,23 to 25.53 minutes Chart speed * 0,89 cpi/nln

II r.2 of OATAIRM3894B.D

"

Ci-

6i-

Sfilr-

ffi-s-

)tl(r

.IS

.£».,.-

sJ

End of plot. Tine - 3.23 to 48.02 ninutea Chart 9peed - 0.99 cn/nin


ROY P. WEpTOH, INC. ___________ LAB, NQ H3B95

Attn! Ralph MpKf»en __________ DATE SAMPLED 1Q/7/19B7

Ilpahur County 4-H Camp Tarpih DATE RECEIVED 10/10/1987Technical.... W —————————————————— DATE ANALYZED

Inc Water _________ ANAUYSTNOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, <= LESS THAN

BASE/NEUTRAL EXTRACTABLESPAGE 1

Method DetectionPARAMETERS Resulta (ug/1) Limit (uq/1)

N-Nitrosodimethylamine ND 50Bis(2-chloroethyl)ether ND 101,3-DichJ.orobenzene ND 101,4-Diohlorobenzene ND 101,2-Dichlorobenzene ND 10Bis(2-chloroisopropyl)ether ND 10N-Nitrosodi-n-propylamine ND 20Nitrobenzene . ND 10Hexachlorobutadiene ND 101,2,4-Tri.chlorobenzene ND 10Isophorone ND 10Naphthalene ND 10Bia(2-Chloroethoxy (methane ND 10Hexachlorocyclopentadiene ND 102-Chloronaphthalene ND 1,0Acenaphthylene ND 10Acenaphthene ND 10Dimethylphthalate ND 102,6-Dinitrotoluene ND 10Pluorene ' ND 104-Chlorophfnylphenylether ND 102,4-Dinitritoluene ND 10Hexachloroithano ND 10

W - •''MDLi Method' Detection LimitND: Not detected at a concentration equal to or greater than the MDL

RESPECTFULLY SUBMITTED:



ROY F. WESTON, INC. _____ , ___ LAB| NO, H389S

Attn; Ralph McKeen ________ DATE SAMPLED 10/7/1987

Upahur County 4-H Camp Tarpit DATE RECEIVED 1Q/1Q/19B7

UJ,__ _________________ DATE ANALYZED 10/26/1987,

Water __________________ ANALYST

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < => LESS THANBASE/NEUTRAL EXTRACTABLES

PAGE 2

Method DetectionPARAMETERS Results (ug/1) Limit (uq/l)

Diethylphthalate ND ' 10N-Nitrosodiphenylamine ND 20Hexachlorobenzene ND 104-Bromophenylphenylether ND 10Phenanthrene ND 10Anthracene ND 10Dibutylphthalate ND 10Fluoranthene ND 10Pyrene ND 10Benzidine ND 50Butylbenzylphthalate ND 10Bis(2-ethylhexyl)phthalate 12 10Chryaene ND 10Benzo(a)anthracene Ni'/ 103,3'-Dichlorobenzidine ND 50Di-n-octylphthalate ND 10Benzo(b)£luoranthene ND 10Benzo(k)fluoranthene ND 10Benzo(a)Pyrene ND 10Indeno(l,2,,3-c,d)pyrene ND 20Dibenzo(a,»«nthracene ND 20Benzol ghi)(jjt[ryl«ne ND 20

•j&i '' '•HDD Method "t>ot«ction LimitNDt Not detected at a concentration equal to or greater than the MDL

RESPECTFULLY SUBMITTED!



ROY F. WESTON, INC._________ LAB, NO. H3895

Attn; Ralph McKeen________ DATE SAMPLED 10/7/1987

— - Upahur County 4-H Camp Tarpit DATE RECEIVED 10/10/1987

&*n- _Mi___________________ DATE ANALYZED 11/18/1987sine Water_________________ ANALYST WL/JER

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < ~ LESS THAN

ACID EXTRACTABLES

Method DetectionPARAMETERS Results (ug/1) Limit (ug/1)

Phenol ND 102-Chlorophenol ND 102-Nitrophenol ND J.O2,4-Dimethylphenol 200 Iff2,4-Dichlorophenol ND 104-Chloro-3-methylphenol ND 102,4,6-Trichlorophenol ND . 102,4-Dinitrophenol ND 504-Nitrophenol ND 502-Methyl-4,6-dinitrophenol ND 50Pentachlorophenol ND 50

MDLi Mtttod Detection Limit.ND; Nolr'attacted at a concentration equal to or greater than the MDL.


1256 GREENBRIER STREET CHARLESTON, WEST VIRGINIA 2S311 - TELEPHONE 304 346-0725

|i TIC of QnTfl!RW3B95fl,Q

^100030

End of plot, Tine - 3,23 to 27,64 ninutea Chart speed - 0.62 cn/nin

Bc«n SB? (11.899 m n) ul QnrRiRNafl93fl. Q 1IBBBB"BOBBBDOB'•IBBBSBBB

u D'

tt

," '[iLh, /•'• ••'

KnnS 1 RQQQ '

K BDBB'BBBB'1BDB'EBOB'

IhMtlllHimH,,,,) mih,.«M *, .h

,P,'

<h ,

2S

141 SI9

u c/

•10BBB'QPBB•RBBB'1QDB•SDBB0

»S1 Phunpl, e, 4-riim»chyl - (9CI)

1

39 ,7

il9Q

a? ^ •10QBD

'BCBD

•fiDBD•4QBD•BOBBf\

IDB I5B EBBMa s i / Ch • r i) •

Is Scan 5?Q (11.191 nin) of DZi 1IC of DfllRiRHW^.O

EKCHflNCE dotie Ys 184 Phfn«l, 8,4-r"«lhyl-Xi S««ii 53? 111.2?? ,i) cf D

UBRIWY SEIWCH RESUltS

Scan 8IP (15.618 din) of [fllfl:RH-89511.UHJ895101 R r NKTON tC«>t.O«l hi CIPIS I1CID

0library file; NBSJBE.Llibrary ami NflS MflSS SPECIRfil MTflBflSE

CHS II Library HatchIndex I turn lily

li Phenol, 8,e-<liii»lh«y (8CI7CI) ?IIOI 7968 ?35I2i Phenol, 3,1-diiwllK><y I8CI?CI) 2033698 im 91813s Btnsene, l-nelhoxyl-liwlhyllhio)- (?CI) 187916? 7?CO 881741 Btiusno, l-mlhoxyMiMlhyllhiol-WI) 23887)0 7981 85395i Phenol, 2,3-diMlhoxy-, icstale (8CI7CI) 27257085 I473C 8163(i: Phenol, 2,4-<liiwlhc-xy, M«lile (8CI9CI) 27257071 11735 63937: Phenol, 2,(i-(lii<ielhoxy, n;e|g|e (8CI9CI) 711990 1170? 830081 Phenol, 2,5-diiwlhoxy, scolal* (6CI9CI) 27257(«3 11731 8I7I9i Phenol, 3,1-diwlhoxy, «c«U!e (8CI9CI) 72031C5 11728 8151ID: D-erylhrc.-,alpha,"[i-qalnclo-0'cU'pyrnriCui l?057600 31960 7K5

Nhich Mlch (I lo 10):

Scan BIB (I3.B4B m i n i of QFirfl: RN3B95R. QIQBQB-BBBB-BBBB'4BBB-SBBB'•

M B

139 1

39 B? 96

LlLl-,lL.jLj,, „„„„.,„„

I31

•IBBBB•BBBB•BOBB4QBB•EBBBQc

KV I796B Ph«no), 2, B-rii muthoxy- (BCI9CI)M QQQQ .j:it BBBB'

BBBQ'4BBB-2BBB-

Q'

139 ,39 ? \/ ¥ /

/

\\-

I34

n,^ IBD IS'B eda

•IBBBB

•BBBB•GBBB•4BBQ-ZBBB

•fl

**||.;'-'.- Is null.Zi 1IC of HflIRiRH3895fl.O

EXCIKHKE dono Y; 17966 Phenol, 2,6-dinelhoK[HS2J Xi Scan 8IC (15.618 mn) of D

LIBRARY SEARCH RESULTS

Scan 611 (I2.1« »in> rf MlAiRH.>89SA.tiH3895 L01 R r WSTDN IL'>|,Oil I'l CIPIS ACID

Library f i l e i NBS.REVE.LLibrary naiie: MBS HASS SPECTRAL DATABASE

CASH library Hatchlnd?< I Wily

li Bentenc, l,4-di«elhMy (9CI) I50787 5250 W72i 1,3-Benwnedianin*, 4-Mlhoxy (9CI) 615054 5233 92163i t.S'Btnwnediol, i-elhyl- (9CI) C8W08 5257 88764i 1,3-Bensenediol, 1,5-diiwlhyl- (9CI) 527559 5252 80075s 1-Penlanom, l-bicyclot4,l,0)hept-7-yl- S1764599 12311 8701PS 1-BulanMie, l-chlord-l-d-fluorcphenyl)- .'674512 15353 86317s Elhanone, l-(l-flucroplienyl)- (9CI) 103129 5276 81598: Beiwnesulfemc acid, nelhyl- (9CI) 72317638 5530 78969i l-Bulanwe, l-d-fluor^phMyl)- (9CI) 58C832 98!0 7895IPi 2,5-Hept«(li«n-1-pn(i, 2,P-di»«lhyl- (8CI9 50«0! 5C62 7811

Htiich Midi (1 to 10);

Scan Bit (IB.4HB «iln) of PRrRl RH3B95B. QIQBQQ-BOBB-6BBB-4QQQ-EBBB': a-

1

BP 93

T ( (isa

,163 £19

•IBBBD•BBBQ•6BOB•4BBQ'5BBBQ

nB •9293 1 . 9nBBn iftnad I >n I na . 4-nftt hnx v« <9CI)•JIBBQO-

« BBBQ-

6BQB'4BBB'8BOB'

i,-j*i

M af/ /1 iv i i i

\sa •IOBBB

6BBB6QBQ'40BB-SQBB~n

ai(Kf ' ' IB'Q IJ'Q EBBnfv' IUii/'Ch»i'Ol*H' ' Ts 15250 Beniend, 1,1-dimilho

Zi TIC of WlfliRHJ895fl.DEXCHANGE dmi Y; 15233 l,3-Bm<msdii«ine,[MS21 Xi Scan 611 02, W «in) of D

/IRI00033

11 WARY SEARCH RESULTS (j/

Scan 413 (9.85$ iin) of PATAiRH3895A,Dmm LOI R r HESTON IL«>I.O«I i<i CLPIS AGIOLibrary filei NBJiEVE.l.Library nano: IBS HASS SPECTRA DATABASE

CAS I library HatchIndM » duality

I: Hyclopenlen-l-wts, 2,3,1-lriiwlhyl- (8 26790865 3S90 95572: 2-Cyclfpenlon-l-ond, 3,1,5-lriiwlhyl- (9 5568J2II 3299 91333: 2-Cyolopenlen-l-one, 3,1,1-lrinelhyl- 18 30131652 3291 89561: 2-Cycl(,penlefl-l-ono, 3,5,5-lrinolhyl- (8 21156951 3288 89175s S-OctyH-ww, 2,2,7,7-l8lra«slhyl- (8CI 28881891 12305 86746; Haphlhaleneiolhanol, l,1,1«,5,6,7,8,fl« I9078376 I8552 81197: l-Propanone, l-d-cycU-hexen-l-yl)- fBCI 1655031 5289 81828: flepictefrncliniM-J'carbwylic «cid, nelh 559513 30113 79909s 3,5-Hepladien-2-one, 6-«elhyl-, (E)- (6C 16617011 3S86 7969

IOs Phenol, 2-iwlhoxy, acolal* (9CI) 613707 ID097 7830

Nnich Mlch (I lo 10);

Scan 443 (9.656 mln) of QRTRi RW3B93R. 0IBBBQ"BQBQ-BBB0-4BBB-SBBD1! a-

V '33

„„ -t ,

39 •;*

L , 1 , ,

•IBBBB•BBQB•BBBB•4BBBEDBBfl

nSJIBBOO'

I BBBB'BBBB'4BBB'JBBB'

3B9B S-Cycl optnon-

a; ,

asQili, 1

•l-on«, 8, 3, 4-trl m«th)'l - (B

Q9 124•IBBBD

•BBOB

•BBBB4BBBEBBB

S*Btt'*i. , IBB I3B SQQ•X,.1'! Mau/Ch»rBi..m®&', • T; Scan Gil (12.142 iin) of D"'W ' ' Zi TIC of WTA:RH38?5A,D

EXCHANGE dont Yi I3ZW 2-Cycl»p«nl(n-l-«n,(HS21 X: Son 443 (9.856 nin) of DA

ARI0003it

It TIC of OftTftiRWJflaSB.D

OS-

a-

ISXI-

J®V£, y<;.v*> .,, ",'.

ARI00036

End of plot, Tine " 3.23 to 48,01 minutes Chart speed • B.99 cn/nin

LIBRARY SEllRCH RESULTS

Scan 171 (6,391 tin) of DATA:RH3895fl,[iIUL nLIH38?5,ROY F. HESi'OH.LOl HATER.B/II,

Library file; NBS.REVE.LLibrary naioi NBS HASS SPECTRAL DATABASE

CDS I Library hatchIndex I duality

li 2-Cyckprnilen-l-ono, 2-»«lhyl- (6CI9CI) 1120736 940 90802i Cyclopropane, Mlhylmslhylene- (6CI9CI) 10631810 16? 66523l Cyclopenttne, ethylidcne- (8CI9CI) 2116374 961 6C071i 2-CyclopwlwM-e.ne, 3-wlhyl- (8CI9CI) 2758181 942 85825i 1,3-Penladiene (6CI9CI) 501609 178 616261 Cyclopenlent (8CI9CI) I1S290 176 61557; Cyck'ptnlene, t-elhyl- (8CI9CI) 2116585 965 61208s l,3-P«nladiene, (Z)- (8CI9CI) I5J14IO 167 8J519i l,3-Pentadi«n«, (E)- (8CI9CI) 2001708 188 8257I0i 2-Penlenenilril«, 5-hydooKy, (Z)- (9CI) 53778555 1002 8147

Hhich mitch (I to Id):

Scan 174IBBBBBBBB

EXCHANGE don*[MS21 Xi Scan 174 (6,394 nin) of OA

LIBRARY SEARCH RESULTS \l)

Scan 239 17,581 tin) of DATAiRH3B?5B,H111 miH3695,ROY F, HESTOH.LOI HftTER.B/H,

Library filoi NBS.REVE.LLibrary nanei N8S HASS SPECTRA DATABASE

COS I Library MatchIndex I Quality

l! 2-Cyclcpenlen-Hne, 3-iwlhyl- (6CI9CI) £758181 9'I2 91872i 2-Cyclopenlen-l-one, 2-mlhyl- (8CI9CI) IU'0736 910 61663i 2,3-ttexadiene, 2-uslhyl- (6CI9CI) 29212097 985 79791i 1,4-Butanediol, 2,3-bis(«olhylene)- (9CI 50521501 2i66 79165s 3,4-Hepladien« (8CI9CI) 2151311 969 79106: Spirohexan-5-ono (8CI9CI) 20061227 910 77837i 2,4-H«adienal, (E,E)- (9CI) 1168186 911 77558! l,3-Pentadi«ie(8CI9CI) 501609 178 7428?i l,3-Penladi«ne, 2,4-dinelhyl- (BCI9CI) (OtW B 957 7383I0i l,3-Buladii;no, 2-methyl- (9CI) 78795 175 7325

Htiich Bitch (I lo 10);

Spun 839 C7.3BI mm) of BRTRl RH3B93B. QIBBQQ-BBBQ-BBBQ4QQQ-BBBQ

39

li

;

1 in

k3 1? 9B

Bl

I2B\

•IBBQB•BBBB•BBBB•4BBQ•2BBB

c'nDJJIBBQB'

ff BBBB'

BBBQ'

4BBB'BOBO'

*948 S-C>T 1 op»n tin-l -pn« , a-mthyX

9B53 B/

39f

lr:m 1>*'*1

ai

1

r

1 - (BCI9CI)•IBQBB

•BQBB•BQBB

•4BBBEBOBn

4aftLl,« . BB ?0 BB 90 IBB IIQ 1EBJBSV. Mafi/Chargi

Zs TIC of WTAiRH38?5B,DEXCHANGE dwio Yi 1912 2-Cyclopenlen-l-ona,[HS21 Xi Scan 23? (7,561 Kin) of DA

ARI00038

LIBRARY SEARCH RESULTS (^/

Scan DO (9.262 lin) of DflTFliRHTOB.DIUL TTLIH3895,WY F, HESTON.L01 HDTER.B/II,

Library filei NBS.REVE.LLibrary name! NBS MASS SPECTRAL DATABASE

CAS I Library Hatchln<lo« I Quality

li Cyclopenlent, 3-propyl- (8CI9CI) 31067759 1952 89862: 1,4-Penladieno, 3-nelhyl- (OCI9CI) IIIS080 115 88803; CycI open lane, (l-nelhylolhylidwie)- (9CI 765833 I9I8 806!i! Cycltponlene, l-(l-methylolhyl)- (9CI) 1162073 I925 87875i Cyclopropane, l,2-di«elhyl-3-iwlhylen«-, 5070008 156 B76061 Cyclopropane, l,2-dinielhyl-3-i«elhylene', 1866551 457 87117: Cyclopenlane, 1,3-didiloro-, Irano- (8CI 2666Q506 5210 873?61 Cyolopentene, 3-iwlhyl- (8CI9CI) H2C'62i 147 8691?! CyclopenUtte, olhylideng- (OCI9CI) 2116374 961 6G87I0i Cyclopenlana, (l-inelhylelhenyl)- (9CI) 5566I024 1961 8676

Nhich match (I l» 10);

Son 330 Ca.SBa min) of QRTR|RN3B93B, QIBBBB-BBQB'BBBB'4QQQ'8QOB

M 0.

99/

JI .....Ihllh, ..„.,!

\?

(ID

ni /

•IBBQB•OBBB•BUBB•4BBQ'SDBB0

Crt* 11919 C>'d npuntun.n, ( l-nnthyl mhyl IrtunJi )- (9CI•JI QQBB 'aOC BBBB'

BBBQ'4QQB'8BBB'

41

.Jii ! ''''I''-

\93

.I I Q

n I /n i :II [ 1

•IQBEB

'BBBB•BBBB'4BBBSBBBn

4B(tK .\ > BD BO IC1B I2B

••.' •''•• Zi TIC of PATA!RH3995B,0EXCHANGE don* V; I|9|Q Cyclopentine, (l-tel[HS2J Ki Scan 330 (9,262 >ln) ol liA

LIUh'IIKY 'ilillKUl IOLIS

Scan 1128 (25,069 lint of OAIA:RH!B95B.UUH. TTLIH3895.ROY F, IIESTOII.LOI HATER.D/II,

Library film NBS.REVE.LLibrary nanui HBS HASS SPECTRAL DATABASE

[AS I library MatchIndex I duality

Is 1,13-Tolradgcadieno (6CI9CI) 21961198 I4473 99252i I.IMiodecwiediol (8CI9CI) 5675514 I5705 9B713i CycloprC'paneoclanolc acid, 2-t(2-penlylc 56667673 20963 9f68H 9,l2-Octad«adlcnoieacid(Z,Z)- (9CI) 60333 25W 95595; I,l2-Tridecadiene (8CI9CI) 2I964487 I2329 95IB6: l.ll-DodtCRdleno (BCI9CI) 5876679 9963 94I27i 11,11-Eiconadlenoic acid, methyl colcr ( 2163027 28955 9309Oi l,IHi«c«nediol'(8CI9CI) 112170 11291 93629i IO-Undec?n-l-ol (PCI9CI) 112136 I0725 9311

I in Cyclopentane, I, !'•(!, 1-bulaniliyDbiv ( 2980703 11170 9300

Nhich match (I lo 10);

IDBBB-jBBBQ'BBBB'40BQ'BBBQ'

u 0-

£ BBBB'BBBB'4BBB'8BB9'

Q-

Be

|

„,,!

:

an II8B (83.BBB nin) nf OFirftt RHJKDSB. P

a BJ

[J ill

»!447aI3 B»

.-•J

S*HWt

EXCKW-E dofll

rS i

I . t

138 ^* 22? 230

1 , IS-TntrartncaitHnn (BCI9CI)

BB I5B tOO 23BMm ^Churai

r IBBBB'BBQB'BBBB•4BBRtBQDM

•IBBUB'BBBB•BBBB•4BBB'BBBB

fl

Ti 128963 CyclfpropmcoclanolZl TIC of fAIAtRHi8?5B,PYi 111173 I,l3-Titr«d4cidlefl«

IHS2) Xi Scan II2Q (25,089 nln) of

flRIOOOliO


LAD, NO,

, ,ilcalMtflJ — liftllilUlcKflOU ———————— DATE SAMPLED JJi£ZZI221,

DATE RECEIVED

ling , , _aJtJL_jB..AMflJ ——————————— DATE ANALYZED~ tes Inclligh Loyol. Sgj,l^Procpj\irq ____ _ ANALYST , tyI.i/JER/IS8

All Raaults arc on nn nn Rocoivad Dnnin,NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED^ < H LESS THAN

PftSB/^EUTRftji^lXTRftCTftnLES lPf\QE 1-1 , Mointura 42.5Dilution Pnotor 50

Method DatoationPftRftMBTBR3 Ko mil tin |»q/gl Umib_

ppm ppmN-NitroHodimnthylnmina ND 1250Uia(2~chlocoebhyl)Qbhor ND 250l,3-Di,cl\).ocobuna«n«i ND 250l,4-l)iclUoroben»ano ND 250l,2~lHc|Uoroben*ana ND 250Di3(2~chloroiBopcopyl)othor ND ;>' ' 250N-tUtroaodi-n-propyinmina ND 500Nitrobenxane ND 250||Qxachlorobut«dlana ND 2001,2,4-Trichl.orQbanzQna ND 250Isophorona ND 250Naphthalene ND 250lUaU-ChloroethoxylmatlmnQ ND 250lloxnahiococyalopentndiono ND 2502-Chloroni\phth«lana ND 250Aconnphthylene ND 250ftcennphthana ND 250l)lmothylptith*l«ta ND 2502,6-LHnitrotoln«n« ND 250Pluorana -i. • - • ND 250

ND 2!ioND 250ND 250

MDlii Method Mtcotlon MmitNO i Nob dataotad «t A aonoantrntion oqunl to or grostar thnn t:!m MD^

f l R I O O O i j I ,.RESPECTFULLY .SUBMITTED" %>

t?5« onEENoniEn aTneer CMAniESTON, WEST vmaiNiA ssai i - TELEPHONE ,104 3


mjJL...HBaam-j:UC, ________ LAB. NO._AUUU — QttlBlUlcKccn ————————— DATE SAMPLED JMULH&L

£Bit —— DATE RECEIVED

_flgl...fl..,Ar>iO ———————————— DATE ANALYZED JO/llUaaZ

J|ioh Lcvol_jQil J?rociidurti ANALYST

NOTE; ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < B LESS THAN

n.A8_E/jjEUTRM4_EXTRftCTA_Bt<BB I PAOP, 2)

PARAMETERS HonuUfl [uq/ql _ Ufntt (ij'i/gppm ppm

Diebhylphthalate HP 250N-Nitronodiphanylamina HP 500HaxaolUorobenzono MD 2504-|)romophonylphonylathar IIP 290Phennnthrana tin JJOAnthraoana HP 290Dlbutylphthalato HD '/'inFluocanthane IIP 290Pyrann HP 290Donzldtno HP 1290IHitylbonzylphthalate HP ^0llin(2-othylhoxyl)phthalata HP 290Chryaona HP 290Wonzolalanthrnoana HP 2903,:)'"PiQhlQrobflnfli,<Un« HP 1290Ri-n-oatylphth«lnto HP 290nonzo(b)(luor«nthana HP 250nanzoJKiCluocanthana HP 250nanxo(a)Pyrt^« HP 290lndano|l,a^p,d)pyr<in« HP 900Pibanxo(iJBfetl\r«a«n« HP 900nanxo(c)hi)H|«n« HI) 900MR!/1 M«tho*!6t«atlon ItimitNDi Hot d«t«at«d At A aonaanhrntlon oqunl to or grantor thnn thn HP(<

A R I O O O l » 8RESPECTFULLY SUBMIHED;__±

1250 QnEENBfllEn STHEET CHAHLiiBTON, WEST VIMQINIA 35311 - TEL8PHON0 904 340.0/38

OMLOJ'.'L M I.-Y5I5 I'Cf'Of'f

_.«// f, HWHiH, inc., im if, iu»n

I/Y M Irv*Irt'/Ht

'Jl>flli'.lt '.'-ititit.f 1 /( t.ntti, 'tntfit- hi It Hfft/Ht

l,n Hi 1,1 nit i >,l

(<M tin nil nil f*A/i«f'Mttf.//(fl/t. WWM WMW7/IM M

/IK XO//4-l!||lfif'f?''l-'((l«ihll/l((!l«ll«! UK X1//

(III IXOf/UK IX OH

MUM HflfcIIIH llnl; flaifmflMrt A); A IIIIIIM«II|;|-«| IHII «IJM«| ho «t yr»«h»f hh«ti felm

'" »RCTPUI.I,Y 'lllllMITTItoUi /l .

IHn<HIMIWIMMIf!H»ll!W! ftlM.III XNII'/ll, WMH VIMHI/IIA Will M WKir'lrVlfM I

. ANALYSIS. REPORT.

LAB. NO. -H3fl96

PATE SAMPLED 1Q/07/19B7.

F-im _ PATE RECEIVED JLO/ULUilZ,

PATEANALYZEO U/l7/19B7it(11/247X987

ANALYST HS

J-1UU;.ALL jttoULIiijy.t'tl "" IN MrV- "H!- S PTHJUWISE DESIGNATED. < * LESS THAN

H MIHHH-3-Ji

H, I _i!

Fflllrl

Mi I';

IWHMIIltlWIlH1

„.?'

f l d l f l f l Q i i i i

» HHWI-IH(IW|-I«IIH M i^HiWlHl^/i KB euEMnprt In m whUmMpn1*1 .NHi 'Ul- MMH W^ fe/HIIWFW flftllfl WlftNj ?nfl MM f a


ROY F. WESTON. INC._________ LAB_ Na n3p96

Attn; Ralph HcKeen________ DATE SAMPLED 10/7/1987

Upahur County 4-H Camp Tarpit DATE RECEIVED 10/10/1987

Sfll s. Ai-pa 1____________, DATE ANALYZED JLLO1/1M1 tc |11/24/1987

—————————————————————— ANALYST . .Dft/JS,,,.

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < ~ LESS THAN

PESTICIDES

• • • • • • • • Method Detection|PARAMETERS Results, ug/1 Lbiiit, ug/1

gamma-BBC [Lindane] ND 6.1Heptachlor ND ' 0.1Heptachlor epoxide ND 0.1Endrin ND 0.5Chlordane MD 0.5Toxaphene ND 1.0Methoxychlor ND 1.02,4-D ND 52,4,5-TP [Silvex] ND 5

.TfNDi Not detected at a concentration equal to or greater than

the Method Detection Limit.

RRIOOIU5•-'' RESPECTFULLY SUBMITTED:_Jll


LABORATORY/

1|>V NO.Duplicate,10/07/193,7,

i ... — LJ&VA ji- ^ l'Q/10/1987TechnicalfeSlInQ sfl-l——£.,—A,i-. ,,-li—— •• •—— '-WfEVWACYZE'D U/17/1987,'iSboratoriesInc ————— -...-.—

E. P. TOXICITX*

Contaminant

_ -LeadMercurySelenium,Silver

• Determinations for. .SM-846, Test Methcda fqr,

————— - ——— -- •'ANAL'YST Ms

NOTE.' ALL RESULTS EXPRESSED JH;Mgfl1y!ii!pi_ Ei .

Sample Phase

Suspended

} ' WRESPEGTRUliUY/SUBMIilffiBOi!_3k^Ata.-,

I: TIC of QflTfl:DI3096SW.D S? « i t - > f t x

0001*7

fllt/ft.vS/4

•J ,

End of plot. Tina • 3.23 to 47.33 nlnutea Chart apaad » 1.01 cn/nin

UBRflRY SEflRCH RESULTS

Sc«n55?(ll.3Wiin>of OnTfl:013896SH.[»H3896 R F «STW 581 2.0368g/IO»l 1/5 OIL MCLPIS

Library file: POUUTE.LLibrary naiwi PRIORITY POLLUTflNTS

CHS II Library HatchIndex I Quality

Is Phenol, 2,1-diiwlhyl- (9CI) 105679 21 95392i Phenol, 4-chloro-3-«elhyl- (9CI) 59507 37 44943s Phenol, 2,1-dinitro- (8CI9CI) 5I285 59 21591: Benzene, nilro- (8CI9CI) 98953 25 18785i Phenol, f-nethyl-1,6-dinitro- (9C1) 534521 63 1785Pi Benzene, ethyl" (8CI9CI) 100111 17 If227; e,7;3,6"OiiTOllmo[mphtli[S,3-b]w;irciie, 3 00571 97 1367es Benzene, 2-i»«lhyl-l,3-(linilri>- (9CI) 606202 56 12309i Helhane, oxybislchlwp- (9CI) 512881 21 121610l Benzene (8CI9CI) 7I43Z 7 1162 /K'l!'-!/r/j/

Uhich natch (1 \o 10);

Scan 999 (11.339 m i n i of QRTfi: QI 3B96SH. QIBBBB-BDBB'BBBB'4BBB-2BBB'

U Q>

39 7

f \\h nlll lll,iM HI) iCn•ajjlBBBB'« BB0B'

BBQB'•IBBB'BBBB'

124 Phi

lifB 'SiBfc'1''. ••i RSt'*'

Ji III

I07 22

1 1

•IBBBB•BDBB•BDBB•4B0B'2BBBQ

not , 2 ,

0?

-cMmothy-l- (9CI). -IBQBB32 •BBBB

'BBBB4BBB•8BBBj.

100 I9B EBBMass/Chai'Dit

T: Scan 677 (I3.M8 din) of 0Zi TIC of OHTRSDI3B96SH.D

EXCHWIGE done V: 124 Phenol, 2,1-dinelhyl-[HS21 Xs Scan 559 (11.33? Kiln) of D


ROY P. HESTON. INC.__________ LAB N0 H3B97

Attn; Ralph HoKeen_________ DATE SAMPLED 10/7/1987

Upshur County 4-H Camp Tarpit D/^ RECEIVED 10/10/1987Technical_Sgj,,S. Areaj———————————— DATE ANALYZED JLl/IiZIiB?

High Level Soil Procedure_____ ANALYST WL/JER/ISS

All Results are on an as Received Basis.NOTE; ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < a LESS THAN

BASE/NEUTRAL EXTRACTABIES [PAGE 1] % Moisture 32 7Dilution Factor 50

Method DetectionPARAMETERS Results [uq/ql _Limit [uq/q]

ppm ppmN-Nitrosodimethylamine ND 1250Bia(2-chloroethyl)ether ND 2501,3-Dichlorobenzene ND 2601,4-Dichlorobenzene ND . 2501,2-Dichlorobenzene ND ''- 250Bi3(2-chloroiaopropyl)ether ND ; 250N-Nitroaodi-n-propylamine ND 500Nitrobenzene ND 250Hexachlorobutadiene ND 2501,2,4-Trichlorobenzene ND 250Isophorone ND 250Naphthalene 360* 250Bia(2-Chloroethoxy(methane ND 250Hexaohlorocyolopentadiene ND . 2502-Chloronaphthalene ND 250Acenaphthylene ND 250Acenaphthene ND 250Dimethylphthalate ND 2502,6-Dinitrotoluene ND 250Fluorena . ND 2504-ChlorophMylphenylather ND 2502,4-Dinitnnbiuene ND 250Hexachloc<MM«M ND 250

MDtii Method Detection LimitND: Not detected at a concentration equal to or greater than the MDL* Tentative Identification.

A R I DRESPECTFULLY SUBMITTED;



ROY F. WESTONf INq,,__________ LAB, NO, H3897

Afctni Ralph HaKean_________ DATE SAMPLED 10/7/19p7

Upphur County 4-H Camp Tarpit DATE RECEIVED 10/10/1987

. Sg.?, „ S. ftgea 2_______________ DATE ANALYZER 11/19/1987

High Level Soil Procedure_____ ANALYST WT</JER/ISS

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < a LESS THAN

BASE/NEUTRAL EXTRACTABLES [PAGE 2]

Method DetectionPARAMETERS Results [uq/q] Limit [uq/ql

ppm ppmDiethylphthalate ND 250N-Nitrosodiphenylamine ND 500Hexachlorobenzene ND 2504-Bromophenylphenylether ND 250Phenanthrene ND 250Anthracene ND 250Dibutylphthalate ND 250Fluoranthene ND 250

• Pyrene ND 250Benzidine ND 1250Butylbenzylphthalate ND 250Bis(2-ethylhexyl)phthalate ND 250Chrysene ND 250Benzol a(anthracene ND 2503,3'-Diohlorobenzidine ND 1250Di-n-octylphthalate ND 250Benzo(b)fluoranthene ND 250Benzol Mfluoranthene ND 250Benzoja)Pyrana ND 250Indeno(l,2^-q,d)pyrene ND 500DibenzoUiBnthraccine ND 500Benzo(ghiJ»-Jlene ND 500

MDL; MethoaflSittction LimitNDt Not da'tacted at a concentration equal to or greater than the MDL

flRIOOOS'J •-'' RESPECTFULLY SUBMITTED;^



ROY F. WESTQN, INC.___________ LAB, NO, H3897

1 Atfcn! Ralph MoKppn___________ DATE SAMPLED 10/7/1987

Upahur County 4-H Camp Tarpit DATE RECEIVED 10/10/1987

,.502 ,-S. Area 2——————————— DATE ANALYZED 11/19/1987High Level Soil Procedure_____ ANALYST WL/JER/ISE

All Results are on an as Received Basis.NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < - LESS THAN

ACID EXTRACTABLES , .^ 32.?Dilution Factor 50

Method DetectionPARAMETERS Reaulta tug/ql Limit [ug/gj

Ppm ppm ,13Phenol 2800 250 S

2-Chlorophenol ND 2502-Nitrophenol ND 2502,4-Dimethylphenol 5200 2502,4-Dichlorophenol ND 2504-Chloro-3-methylphenol ND 2502,4,6-Trichlorophenol ND 2502,4-Dinitrophenol ND 12504-Nitroph-nol ND 12502-Methyl-4,6-dinitrophenol ND 1250Pentachlorophenol ND 1250

MDLt Malpppatection Limit.ND: Not datected at a concentration equal to or greater than the MDL.

AR100052RESPECTFULLY SUBMITTED-

1258 GREENBRIER STREET CHARLESTON. WEST VIRGINIA 25311 - TELEPHONE 304 346-0725

II TIC of DATfl!QX3897SW.D -"

,J '00053

w —

3-

ORIGIN^(Bed)

End of plot, Tine - 3.23 to 48.82 nlnutos Chart opead • 0,99 cn/nln

UBRfWY SEflRCH RESULTS

Scan 285 (7.377 iin) of DflTfliM3897SII,DH36?7 F R HESTON 502 2.059VIO»I I'I CLPIS £H

Library filei POUUTE.I.LibrirynMH PRIORITY POUUTflWS

CflS I Llbrwy Hutch;.,:iix I Quality

Is Phenol (BCI9CI) ICB952 II 976?2i Helhini, btm- (BCHCI) 74839 10 40713: UiS.B-PiKBlhanonaphlhaleno, 1,2,3,4,10 309002 95 20204i Phenol, 4-nilro- CTCI) 100027 35 258B5: Propane, 1,2-dichloro- (8CI9CI) 78875 19 16446! 1-Propeno, 1,2-dichloro- (9CI) 563512 18 13247: Elhune, 1,1-dichloro- (BCI9CI) 75313 II 11188: Elhene, lelmchlor.o- (9CI) 127181 17 10819i Phenol, 2-i«lliyl-4,6-(linilro-(9CI) 531521 63 105710; Mrazino, 1,2-diphenyl- (9CI) 122667 58 1054

Which match (1 to 10):

Scan 2B3 (7.377 mln) of DRTR! QX3B97SN.DIBBBB'BBBB'BBBB'4BBB'2BBB'•

u 0J

X94

Ll. >3 >" "^ 3=, 4BB, , r , i i . .' .''

•IBBBB'BBBB•BBBB•4BBB2BBBQ

rt* tit Phinnl (BCI9CI)JJIBBBB-S. BBBB'

BBBD'4BBB'2BBB'

/94

li,ik^.-.-.-

IBBBB'BBBBBBBB

'4BBB•2BBB

'.'in it, IB'B ado IB'B''•SBF 'V ': ' M»«t/Chir(ii•*!$/">'?. . Ti 121 Ptienol, 2,4-dlmlhyl-'"• ' ' ,: I; TIC of DflTfl:M3B97SH.D

EXCNWCE dwio Yi 111 Ptienol (8CI9CI)CHS21 X: Scan 285 (7.377 Kin) of DA

IIBRRRY SEflRCH RESULTS

Scan 555 (11.338 •In) of DflTfiiDX3897$H.D113897 F R HESTON-S02 2.0599g/tOsl I'l CLPIS SH

Library fi lei WUUTE.llibrary namei PRIORITY POUUTWTS

CRS II library hitchIndent Quo lily

h Phenol, 2,4-dinolhyl- (9CI) IC'5679 21 96612i Phenol, l-chlpro-3-nelhyl- (9CI) 59507 37 17983i Phenol, 2,4-dinitrp- (BCI9CI) 51285 59 25334: Benzene, nitro- (6CI9CI) 98953 25 23725: Phenol, 2-nelhyl-4,Hinilro- (9CI) 5J1521 63 19526: Benzene, ethyl- (8CI9CI) 100111 17 I6597: Benzene, l-bronw-1-phenoxy- (9CI) 101553 72 15538: Benzene (6CI9CI) 71432 7 12559i Benzene, 2-»elhyl-l,3-dinilro- (9CI) 606202 56 123310) Benzene, nelhyl- (9CI) 108883 9 1196

Which Mlch (1 to 10):

Scan J33 (IIIBBBB-BBBB'BBBB'iooa2BBB'

a Bf

as "

L*. it *(-.,-, L ,„c

,aaa ntn> of QRrRiDxaaarsN.D

,,*

\ 1?«B7

tH ,

r

219

i ,. 7B \

•IBBBB•BBBB•BBBB•400B'20B0Q

11 t84 Phtnnl, g.4-itlmithrl- (9CI>SlBBBBi« BBBB'

BBBB'4BBB'8BBB'

39

/ . 7it* I° 3»*.'V______ /jHjjyjv

U-

\

07 1i22

•IBBBB•BBBBBBBB•4BBB•2BBB

IBD I3B 2BBH«n/Ch»rg»

W**- "> T: Sun 1032 (18,101 »in) of"'W: ' It TIC of WTfl:OX3B97SH.D

EXCHflNCE done Y: 124 Phenol, 2,1-diwlnyl"(HS2) X; Scan 555 (11.338 nin) of D

Afi/00056

C».n BBO CIQ.aBil nln) «f OHT fi • R ¥ SO B? «M. ftIBBBO'BBBB'BBBB'4BBO'2BBB'

U Q'

1B91

1, 1, Ll 1,

\2B

200 32Bs;? \ v7i i i i i ,

•IBQOB•BQBD•BBBB'•IBDB'2BBB0

Crt* I2B Naphthaline (BCI9CI)Si QQQD '

3. BBBB'BBQB'40BB'2BDB-

1

attI I , i

2B•IBBBD

•BBOB•BBOB'1BBB'BBBB

a- ——— i ————— . — , —— , ——— , — . — . ——— i —— «IBB 2BO 300 4DD

Hait/ChargiTi Scan 62! (12.309 nin) of DZl TIC of DAiri;DX3897SH.D

EXCHRNCE done Y; I26 Niphlhilene (6CI9CI)thS2l Xt Scin 622 (12.324 «in) of D

LIBRARY SEflRCH RESULTS

Scan 622 (12.324 «in) of DflTn:DX3897SN.PH3897 F R HESTON S02 2,P5y?g/lOil l«l CLPIS SH

Library filoi POUUTE.lLibrary mm PffllKY PttLUTIWS

' .v ' CHS I Library Hatch' Indent Quality

I; HnphlhalerflBCI) 9I203 26 8383' 2t Phenol, Z-«(|Hi>--'(»CI) W578 27 73993) Phenol (8CI9CI)'' I08952 II 24574: Phenol, 4-nitro- (9CI) IW&27 35 20185: Naphlhilene, 2-chloro- (8CI9CI) 91567 45 16646: Ethene, (2-chloroalhoxy)" (9CI) 110758 16 15767: Hydrazine, 1,2-dlpdenyl- (9CI) 122667 58 15388: l-Propana*ine, N-nilrouo-N-propyl- (9CI) 621647 29 14419: 1,7-Helhano-IH-inttene, 1,1,5,6,7,8,8-hep 76118 96 •10i Phenol, 2-njfro- (9CI) B8755 34 A

Hhich Ritch (I to 10):

LIBRARY SEARCH RESULTS (\J

Scan 633 (12,485 tin) of tfltfi;(«3897SH,D113897 F R HESTON 502 2.0599g/|0i«l I'l CLPIS ?H

Library file: NBS.REVE.LLibrary mm: NBS MASS SPECTRAL DATABASE

C^ I Library HatchIncteK I duality

li Benzene, l,1-dinelho«y (9CI) 150787 5250 91182: 1,3-Benzenediamine, l-nelhoxy (9CI) 615051 5233 89763: 1,3-Bcnzenediol, 1-elhyl- (JCI) 2896608 5257 65604i 1-Penlnnone, l-blcyclotl.l.Olhepl-7-yl- 51761599 I23H 65315s 1,3-Benzenediol, 4,5-dinelhyl- (9CI) 527559 5252 85056: l-Biitsnmo, 1-chloro-l-d-fluorophenyD- 3874512 15353 85027: Elhanone, l-14-fluorophenyl)- (9CI) 403129 5278 79518: e.WtepUdieiH-om, 2,6-ilinelhyl- (8CI9 501201 5262 79139: Thiophene, 2-(2-bulenyl)-, (E)- (9CI) 52W8158 5269 789910: Thiophene, 3-(2-bulenyl)-, (E)- (9CI) 53966112 5270 7863

Hhich natch (I to 10):

Scan B33 (12.463 nln) of QRTRtDxaB97SW. QIQBBB'

BOOB'BBBB-

2QBD-u 0.

1

Lillil,.

\2

,

449

•IBBBB•BBBB•BBOD•4BBB'2BBBB

rt* »9E9B B«nz«n«, 1 .4-dl nithoxy- (9CI)§IBBBB'

E BBBB'BQBB'4BBB'2BBB-

i99\

1 it:J: '.

\23

'IBQBO

'BOOB•BOBB'4DBB'2BBB

'.|W» ,. 2 BO 300 4BB•%f>'i'--' Matt/ChargaWl>',«;, • T: I32'«i 2-Cyolopenlen-l-iHie,..." ' Z: TIC »f MTfl:W3897SH.D

EXCHANGE done Y: 15250 e«nzene, t,4-dmetho(HS21 X: Scan 633 (12.465 lin) of D

1R100058


Scan 757 (14.308 iin) of DATA:DX3697SH.OH3897 F R HESfW 502 2.0599(|/IO»I 1*1 CLPIS SH

Library file; NBSJEVE.LLibrary n»»ei NBS HASS SPECTRAL OATABASE

CAS I Library HatchIndent duality

li Phenol, l-elhyl-2-nelhoxy (KI9CI) 2785899 7575 96892i Elhanone, l-(2,4-dihydroxyphenyl)- (9CI) 69819 7542 95313: Pyrazine, 2-nelhoKy-3-(l-inelhylethyl)- ( 25773101 7529 91104s Benzole acid, 2-hydrony, phenylnelhyl * 6I233673 19282 93135: Benzsldehyde, 4-hydro«y, OKi*e(9CI) 699069 5062 92826: Benzeneacetic icid, ,alpha.-hydroxy3-«e 54815408 11742 91557: Acetaiide, 2-(1-hydroify3-iwlhoxyphenyl) 29I2I49I 12544 91358: Benzeneinethanol, ,alpha.-elhyl-1-»elho«y 5M96W 9BG6 90739: Silane, lrin»thyl(4-i«ethyl-3-penl«n-l-yn 62338129 7609 9071

IDi ftealdehyde, 3-hydroKy, oxinie (9CI) 22241185 5069 9b63

Hhich ialch (I l» 10):

Scan 797 (I4.3BB nln) at BRFRlQxaBBi'SN. 0IBDBD'BBBB'BBBB'4BBQ'2BBB'

u B'

/137

39 91

/ 7 / .•Mi.... AM, ...rt4tn..nil'll ....lllJl..ttthnhb,,,..llL.,. ...

192( IBB

...I , -..N

•IQDOB•BBBB•BBBB'4DBBSDBB0

SDJJIBBBB'

I BBBB'BBBB'4BBB'2BBB-

»7373 Phinol, 4-ithyl-2

137

91i .7 /iaSS'.'.'r ii I i

•mithDny- (BCI9CI)

192(

lli

•IBBBD•BBBB•BBBB'40BB'2BBBnB' —— r-jr —————— , —— , —— . —— , —— , ———— , ——————— , —— . —— , —— . —— .

9»g»:>' IBB 190 200••»*»!•'. . Man /Charm

T: Scan 633 (I2.4B5 nin) of DZi TIC of DATAiDX?897SH.D

EXCHANGE done Y; 17575 Phenol, 4-8lhyl-2-M[HS21 X: Scan 757 (14.308 nin) of D

&LIBRARY SEARCH RESULIS

Scan 459 (9.908 lin) of OATA:DX3897JM.DH3897 F R HESTON S02 2.0599j/10il 1*1 CLPIS SH

Library filei NBS.REVE.LLibrary nami NBS MASS SPECTRAL DATABASE

C(1S t Library HatchIndex t Quality

li 2-Cyclopenlen-l-one, 2,3,4-trinelhyl- (8 28790865 3290 95845i Kyclopenlen-l-wie, 3,4,5-lriiMlhyl- (9 55683211 3299 93M?l 2-Cyclipenlen-l-Mie, 3,4,1-Ifinelhyl- (8 30131C52 3291 B3711; 2-Cyclopenlen-l-one, 3,5,5-Irinelnyl- (8 21156954 3288 8825Si S-Oclyn-1-one, 2,2,7,7-lelranelhyl- (8CI 28681891 12305 Of.?If: l-NaphlhaleneiwIhano), l,1,1a,5,6,7,8,Ba 19078)76 18552 6J257: l-Propanoae, HI-cyclchexen-l-yD- (80 1655031 5289 81P38i A:pid(.fraclinine-3-carboxylic acid, »9lh 559513 3M1! 79769i 3,5-Hepl«dien-2-on8, 6-nelhyl-, (E)- (8C I6617014 3CC5 791810: Phenol, 2-nolhc.ity, acetate (9CI) 61.<707 ICW 7865

, Which latch (1 to 10);

Scan 499 (9.90B m i n i of DRTR: QX3B97BN. DIDDOB-BBOQ'BBBO'4BOB'20BB'

u D-

93

1 ll Ii.tJIl M,, J«

1

t*H M

1 a A

99

,t ,

,X

334

'" X

•IBBBB'BOOB60DB'4BBB' 2 0 .1•0crt

c *JJIBBBO-

I BBBB-BBOB'4BBO'20BB-

p. , . _ , ,.

329B 2-Cycll

1

93Lp;

9IJB&IJ.

ptntin-l -pn«, E, 3, 4 -t rl mil hyl - (BI ^~"09

1

124•IBBBD•BBBB•BBBB'4BBB•2BBB

IBB I3B 2QO 2SO 3BBijpw • ' Maii/Chargi•'lt!'.',•,:: Ti Scan 757 (14.308 tin) of 0

' •'-•'• ' Zi TIC of Wlfl:OX38975H.DEXCHANGE dona Y: 13290 2-Cycloptnlen-l-one,IHS21 X: Scan 459 (9.908 tin) of DA

ARI00060tfO


Scan 815 (15.612 lin) of tiATAiPX3897SH.il (yH3097 F R HESTON 502 2.0599<j/10ml 1*1 CLPIS 5H

Library file: N6SJEVE.LLibrary naie: N6S HflSS SPECTRAL tifllABASE

CAS I Library HatchIndex II Quality

li Phenol, 2,6-dinelhoKy (8CI9CI) 91101 79f,8 94012i Phenol, 3,1-diielhoxy (8CI9CI) 2033898 7972 90893i Benzene, l-i»elhoxy-4-(»elriyllhio)- (9CI) I879I69 7960 B70B4: Benzene, l-inelhoKy2-(»eihyllhi(.)- (9CI) 2388730 7961 81085: Phenol, 2,3-dinelhoxy, acetate (OCI9CI) 27257085 11756 83836: Phenol, 2,4-dinelhoxy, acetate (6CI9CI) 27257074 11735 82697: Phenol, 2,6-diielhoxy, acetate (8CI9CI) 944990 14709 82018: Phenol, 2,5-diielhony, acetate (8CI9CI) 27257063 14734 80649i Phenol, 3,4-dinolhoxy, acetate (6CI9CI) 7203165 I4728 803810: O-erylhro-.alpria.-D-iialacl.o-Oclopyranosi 17057680 34930 7498

Nhich natch (1 to 10)i

Scan B49 (15.618 nln) at QRrRiDX3B975N,0

IS4

39 B9 9B

,,J|. ....

167

IBBBB•BBBBBBBB4BBB2BBB

•fl

IQOBQBBBQBBBB4BBQ2BBB

" 0*rt1! »79fifl Phanol, 2, B-rtl nithoiiy- (BCZ9CI)glQBBBq f-IODBDB BBBB' 93 "-." "« 'BBBB

BBQB' / B9 / .BBBQ4BBB' I '4QBBSBBB'I I I . 'zana

-0

T: Scan 159 (9.908 »in) of DAZ: TIC of MUAiM38?7$H,D

EXCHANGE done Y: 17968 Phenol, 2,6-diiolhox[HS2] X: Scan 845 (15.612 win) of D

39

| J j£fi

— Jm

B9

139^ \

1 94

.':;.' IBB 150 2BB;V. Masi/'Chargi

ARI0006I


Scan 952 (17.207 «in) of [fllA:DX3897SH,DH3897 F R HESTOH SK 2.0599t|/IOi«l 1*1 CLPIS Stl

Library file: NBS.REVE.LLibrary name: NBS HASS SPECTRAL DATABASE

CAS I library MulchIndex I Quality

ti Benzoicacid, 1-hyrfroxy3-»elhoxy (9CI) 121346 10193 90422i Phenol, 3,5-(li»elhyl-4-(«elhyllhio)-, «e 20!2657 I8976 67563: Benztne, l,£,Hrwlhoxy (8CI9CI) 6?43f6 10519 S5571i Acelani.de, H-(1-»ethoxy2-nilrophenyl)- 1H813 I7026 61665: Naphthc.l2,l-blfiiran (8CI9CI) 232951 10130 82976: 9H-Pyrido(-l,4-b]indole (BCI9CI) 241633 103)1 BI727: li»idazo[2,l"BJi»oc|tiinoline (8CI9CI) 231708 1053d 8I678: Dibenzofuran (BCI9CI) 132619 10129 81149: Pyridine, 2-(phenyl»elhyl)- (9CI) 101826 10571 609310: Pyridine, 2-[(2-»elhoxyphenyl)r»elhylJ- ( 35851434 15323 6077

Which match (1 to 10):

Scan 992 (I7.2B7 nln) at QRTHiQX3B978N. 0IQBQQ-BOOB-BBQQ'4BQQ'2QQQ-

t

,93«o B3 129 I/ /'' ,Q7 '

1 1 1 1 i'in. ,*L . .,»i.,,,.,ilU, ...M. ,,,,..U „ ,. J,,,,n,,,..,, „ J,L, .,,, ,

'•s.IBB

,„„„„ .

•IQBQD•BQQQ•BOOD•4QBB•2BBBB

crtc *

K BQQQ-BBBB-40BQ-2BBB-

Q-

10493 Bincnic acirt, 4-h)'drQxy-3-«i

,93

51 *' '?5

1 , , ' ' • * '• 1 11 • bkW :' \\ \

ithoxy- (9CI)

IBB') QOOQ'BQBBBQBB40002BD00

9Br>|lf-&,'. IBB ,9Q 2QB''Wjj;.;-" . Han/Charga

T: Scan 845 (15,612 iln) of PZ: TIC of OflTfliOX3897SH.D

EXCHANGE done Y: 110193 Benzoic acid, 1-hydIrN) X: Scin 952 (17.207 «in) of P

HRIOQ062


ROY P. WESTON. TUG. ____________ LAB. N0. 113897

flttni Ralph HcKeen ——————————— DATE SAMPLED 10/07/1987.

tlpahur County A-ll Cnmn TnrplC RATE RECEIVED .10/10/1987.

s02 S. Arcn 2 _______________ DATE ANALYZED11/24/1987

ANALYST —— US ———

NOTEjjMj RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < - LESS THAN

Sample Phase __Sludge_Liquid

Suspended Solids, % <O.SX_>0.5

Sample Treatment Extracted 6 Filtered & Analyzed_Piltered & Analyzed ,

E. P. TOXlCm*

Contaminant

Aromlo •. 0.029<0.05<0.2<0.01<0.2

(fercury <0.002Selenium <0.005Silver <0.2

flRI00063RESPECTFULLY SUBMITTED:j_i_:

* Determinations for E.P.Toxicity, as outlined in EPA PublicationSH-846, Test Methods for Evaluating Solid Waste, 2nd Ed., Revised 19B41258 QREENBRIER STREET CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 304 346-0725


ROY. F. WESTON. INC._________ LAB| N0 ,,,fl07

Attni Ralph McKeen_______ MTE SAMPLED 10/7/1987

Upshur County 4-H Camp Tarpit DATE RECEIVED 10/10/1-987

.-SB2 ...S.,Ar.ea.,,2———————————— DATE ANALYZED J-LZlflZlMZ. toitorieslnc 11/24/198?—————————————————————— ANALYST

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < a LESS THAN

PESTICIDES

Method DetectionPARAMETERS Results, uq/1 Limit, uq/1

gamma-BHC [Lindane] ND b.lHeptachlor ND 0.1Heptachlor epoxide ND 0.1Endrin ND 0.5Chlordane MD 0.5Toxaphane ND 1.0Methoxychlor ND 1.02'4"D ND 12,4,5-TP [Silvex] ND i

ND» "Kot' detected at a concentration equal to or greater thanthe Method Detection Limit.

* Method Detection Limit had to be raised due to a largephenolic type interference.

flRioooe.-•'' RESPECTFULLY SUBMITTED:

1256 QREENBRIER STREET CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 304 346-0725


ROY F. pSTQH. INC. __________ y B. N0| _H3898

Attni Ralph MoKeen ________ . p/^ SAMPLED _10/7/1987

Upshur County 4-H Camp Tarpit p^g RECEIVED ,10/10/1987

.5.03 S. Area 3 ____________ DATE ANALYZED

High level Soil Procedure ____ ANALYST HL/JER/ISSAll Results are on an as Received Basis,

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < a LESS THAN

BASE/NEUTRAL EXTRACTABLES (PAGE 1] % Moisture 39 •Dilution Factor 50

Method DetectionPARAMETERS Results tuq/ql limit [uq/ql

ppm ppmN-Nitrosodimethylamine ND 1250Bi3(2-chloroethyl)ether ND 2.501,3-Dichlorobenzene ND 2501,4-Dichlorobenzene ND 2501,2-Dichlorobenzene ND !':;""i- 250Bis(2-chloroisopropyl)ether ND .... • ' 250N-Nitrosodi-n-propylamine ND 500Nitrobenzene ND 250Hexachlorobutadiene ND 2501,2,4-Trichlorobenzene ND 250laophorone ND 250Naphthalene 360* 250Bia(2-Chloroethoxy (methane ND 250Hexachlorocyclopentadiene ND . 2502-Chloronaphthalene ND 250Acenaphthylene ND 250Aaenaphthene ND 250Dimethylphthaiate ND 2502,6-Dinitrotoluena ND 250Fluorene ., ND 2504 -Chlorophffiylpheny lather ND 2502,4-Dinit8|koluene ND 250Hexachlordfchtn*! ND 250

MD_t Method Detection LimitND: Not detected at a concentration equal to or greater than the MDL* Tentative Identification.

RESPECTFULLY SUBMITTED;_Ll±



ROY F. HESTON, ING.___________ |>B, NO. _H3B9B

_A.fctn; Ralph McKeen_________ DATE SAMPLED 10/7/1997

Upshur County 4-H Camp Tarpif! DATE RECEIVED .10/10/1987

S03 5- Area 3_______________ DATEAMALV7FD 11/19/1987

High Level Soil Procedure_____ ANALYST WT./JER/ISS

NOTE; ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < a LESS THAN


Method DetectionPARAMETERS Results [uq/q] Limit Juq/ql

ppm ppmDiethylphthalate ND 250N-Nitrosodiphenylamine ND 500Hexachlorobenzene ND 2504-Bromophenylphenylether ND 250Phenanthrene ND 250Anthracene ND 250Dibutylphthalate ND 250Fluoranthene ND . 250•Pyrene ND 250Benzidine ND . 1250Butylbenzylphthalate ND 250Bis(2-ethylhexyl)phthalate ND 250Chrysene ND 250Benzo(a)anthracene ND 2503,3'-Dichlorobenzidine ND 1250Di-n-octylphthalate ND 250Benzo(b)fluoranthene ND 250Benzo(k)fluoranthene ND 250Benzol a)Pyrene ND 250Indeno(l,2f3-a,d)pyrane ND 500Dibenzo(a,rtttnthracene ND 500Benzo(ghi)||i;ylene . ND 500MDLt MathoJT!rtt«ation LimitNDi Not datacted at a concentration equal to or greater than the MDL


1256 GREENDRIER STREET CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 304 346-0725


ROY P. tyEgTON,, INC.___________ LAB, NO. H3B98_____

ftf-fn! tyalph MnKppn___________ DATE SAMPLED 10/7/1987

Upshur County 4-H Camp Tarpit DATE RECEIVED 10/10/1987

S03 S. Area 3____________ DATE ANA, V7Fn 11/19/1987

High Level Soil Procedure____ ANALYST HL/JER/IS!All Results are on an as Received Basis.

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < - LESS THAN

ACID EXTRACTABLES % Moigturfi 32.3Dilution Factor 50

Method DetectionPARAMETERS Results [ug/gl Limit [ug/g]

ppm ppm;

Phenol 4200 250 \2-Chlorophenol ND 2502-Nitrophenol ND 2502,4-Dimethylphenol 7200 2502,4-Dichlorophenol ND T?!' 69i4-Chloro-3-methylphenol ND '". 25<r2,4,6-Trichlorophenol ND "''2502,4-Dinitrophenol ND 12504-Nitrophenol ND 12502-Methyl-4,6-dinitrophenol ND 1250Pentachlorophenol ND 1250

MDLi Metlw* Datection Limit.ND: Not detected at a concentration equal to or greater than the MDL.

flfiiooos?RESPECTFULLY SUBMITTED- *


II TIC of DflTfl:DX3898SW.Q

ARI00068

-' SH

a-

MI00069

End of plot. Tine - 3.23 to 48.02 nlnutea Chart spend • B.99 cn/nin

HBRflRYSEfflCHRESUlTS

Scan 280 (7,372 iin) of OflTfoOMWBSH.Dmm R r HESTON m z-iwoj/idii I/SOIL 1*1 CLPISLibrary fik PCLLUIE.LLibrary naiwi PRIORITY POLLUTWS

CflS I Library halchIndex I Quality

li Phenol (BCI9CI) 108*52 " WBO£i Hothano, broao- (8CI9CI) 74839 10 48373: l,4:5,8-OiMllnnoniipl!lhalene, 1,2,3,4,10 305002 95 27G*4i Phentl, 4-nllre- (Kl) 100027 35 2S105s Propane, 1,2-diclilopo- (BCI9CI) 76875 19 I4MC: l-Propene, 1,2-dichlcrp- (9CI) 563512 18 12797: Elhann, 1,1-dlchlero- (6CI?CI) 75343 14 IIC6BiEtheno, lelnchlw (9CI) 127184 47 10779: Elhaim, J,l'-o«ybi.[Z-clilcf»- (9CI) 111144 36 106110! Hydrazino, 1,2-diphenyl- l?CI) 122567 58 1030

Hhich natch (I to 10);

Scin ZBB (P. 372 nln) of QRTR: DX3B9BSW. QIBQBQ-BBQB'BQBB'4BBQ'2BBD-

U B-

X94

ll7. rIBBBO•BOBQ•BODB•4BBB2BBBQ

" III Ph.nol (BCI9CI)_IBBBB-C BBBB-BBBB'4BBB-8BB0-

/94

hi 1 .**.

•IBBBB•BBBB•BBBB'•4EtBB'EBBB

"Jan- ia'a aa'a 4BB&; M.n/Chirgi

-'S-Sv . Ti Scan 545 (11.356 *in) of D. '-.- ' " Zi TIC of DflTfl!DX3898SH.D

EXCNmGEdon* Yi III Ptiwol (8CIJCI)IMS2) Xi Scan 28$ (7.372 nil,) of DA

LIBRFflY SEfflCH RESULTS

Scan 545 (11.35$ »in) of WHfliC«3B9BSH.[iH.'6'!8 R F HESTOM 503 Z.IIGOn/KM I/5UIL I'l CLPIS

Library file: POLLUTE!Library n«i»e: PRIORITY POLIUTIHITS

CHS I Library MulchIndex I duality

li Phenol, 2,4-diMlhyl- (9CI) 105679 24 97252i Phenol, l-chloro-3-nelhyl- (9CI) 59507 37 115363: Phenol, 2,1-dinitro- (8CI9CI) 5I2B5 5? 24194i Benzene, nilro- (8CI9CI) 98953 25 24065s Phenol, 2-iwlhyH,6-dinilro- (9CI) 531521 63 201661 Benzene, HroiH-phenoxy (JCI) 101553 72 15917i Benzene, ethyl- (6CI9CI) 100114 17 1589B: Benzene (6CI9CI) 7143,' 7 13169; Benzene, 2-ielhyl-l,3-dinilro- (9CI) 606202 56 1247IE): Helhane, oKybi»(chloro- (9CI) 512881 21 1139

Which Mlch (1 to 10):

Scan 949 kll.356 nin) at URTR: DX3B9aSN. QIBBBB'BBBB'BBBQ'4BBB'.BCD'

U 0.

i

771

Lull*

1B

I4B 36? 373

'IBBBB•BBBQ'BBQB'4BBBEQQBBc

H* »24 Phinpl , 2,4-rtlmthyl- C9CI)_I0BBB-

I BBBB'BBBB'4BBB-SBBB-

B'

77

[• L22

IBBBB'BBBB'BBBQ4BBQSBBB

-jit'tB .BB 3BB 4BBWJ1"'1, Hn./Chim*«f" T: Scan 600 (12.190 iln) of D•""' Z: TIC of DflTfl!PX3B98SH.O

EXCHANGE done Yi 124 Phenol, 2,4-diinelhyl-(HS21 X: Scan 545 (11.35$ iin) of D

AR100071

Scin BOB (IS. 316 mm) of DRrRi QX3B9aSN. DIQQBB-BQBQ'BOOB-4QBQ-2QBB-

u B*

7 Ii l l

iSB

I I94\s

'IDBBBBBHDBQBB'4BQQ2BBBflcil

jjlBQQQ-C BBQB'

BBBB'1BBB'.BOB'

B-. —— .- . -r—-- • ——— • -,--—-• ———— - T— — • ——— --• -,---.-»

•

91

I I , ,

SB Naphthaline (BCI9CI)

SB'IBBBDaaaa•BBBB'4BBB-2BBB

IBB 2DB 3BD 4BBMait/Chargi

T: null.Z: Ion 128.00 aw. front [iRTfli

EXCHftNGE done Yi 126 Naphthalene (8CI7CI)IHS2J Xi Scin 608 (12.316 iln) of D

flfi/00072

LIBFffiY SEfflCH RESULTS f\ \

Scan 739 (14,331 tin) of OftTfl:OX3B9BSH.DH389B R r HESTON 503 2.ll60<i/IO«il I/50IL 10 CLPIS

Library file: NBS.REVE.LLibrary nano: NBS HflSS SPEClRfil CtiTRBflSE

CHS I Library natchln<te< I duality

1: Phenol, l-elhyl-2-nelhoxy (8CI9CI) 27B5B99 757J 97112: Elhant.no, H2,4-dihyclroKyphenyl)- (9CI) 69819 7542 96313: Pyrazlne, 2-inelhoKy-3-(l-»elhylolhyl)- ( 25773101 7529 95304i Bcnwic acid, 2-hydroxy, phenylnelhyl e 61233(78 19282 93565i Benzaldehydei 4-hydroKy, mm (9CI) 679069 50F2 9285P: Benzeneacelie acid, .ulpha.-hydroxy-3-jie 51845108 14742 92177: Bensenenelhanol, .alpha,-elhyl"4-iiielh(«(y 5349600 98C6 915981 Silane, lri«ielhyl(4-iielhyl-3-penten-l-yn W?i8l29 7f09 91259; fkelamido, 2-(4-hydrt.Ky-3-netho«yph«myl) 29121491 12544 909710; Benzaldchyde, 3-hydror,y, o«iie (9CI) 22241185 5DP? 9093

Hhich natch (I \u 10):

Scan 739 (14.331 nin) of QRTR: D*3B 98 SW, QIBBBB-BQQQ-BBQQ-4BBQ'2BBD'

u B-

„<39 91> 77 X"' f i' 1A(,.,*,,lllllM .ni*Jtm»,li.Ul..iit(ltilt, , «,,iAl,,, i,,ll|lh, ,,.»>,

ise/\

•IBBBB•BBBB•BBBB•4QBB•2QBB

i ... {_,S•" (7579 Phunnl, 4-athyl -S-mntnnxx.- (BCZ9CIH.IBBBQ-I BBQB-

BBBB-4BBB-2BBB-

/137

9,

.-isr''. I li i i

,92f

,

IOBBB

'BBBB'BQBB'4BBB2BDBa

SB'Si' IQB ISB 2BD;.ijw> Maii/Charu«;*"«"»''- T: 114473 1,13-Telradecadiene

' - ' ' • Z: TlUf WTf):OX3898SH.OEXCHflNCE done Y: 17575 Phenol, 4-8lhyl-2-»eEHS2) X: Scan 739 (14.331 win) of 0

'00073

LIBRflRY SEflRCH RESULTS L\

Scan 620 (12.498 tin) of MTf):DX3B96SH.DH3898 R f NESTON 503 2.||80g/IO*l I/Sim hi CLPIS

Library file: NBSJ0E.LLibrary naine: DBS HflSS SPECTRRL ORTRBIiSE

C(1S I Library Hatchlnd*< I Quality

I: Bonzeno, l,4-dii»elhoxy (9CI) 150787 5250 89982: 1,3-Bentonedlaiiine, 4-uelhoxy (9CI) 615054 K3J 69123: l,3-B<nzenedlol, 4-elhyl- (9CI) 289f«i8 5257 BMP4i 1-Bulanone, 4-chlc.ro-HI-fluorophenyl)- 3874512 15353 81815: 1-PentMone, l-bicyclol4,l.01hepl-7-yl> 54764599 12314 61106: 1,3-Benzenediol, 4,5-diuelhyl- (9CI) 527559 5252 83537: Elhanwio, l-(l-fluorophenyl)- (9CI) 103129 5C78 79486: 2,5"Hept-die(i-4-one, 2,6-dinelhyl- (8CI9 501201 5282 79109: Tnfophmo, 2-(2-bulenyl)-, (E)- (9CI) 52003158 5269 781910: Thiophene, 3-(2-bulenyl)-, (E)- (9CI) 53966112 5270 7781

Nhich match (I to 10): ,I

Scan 62B US.49B mm) of QRTfii QX3B9BSH. 0IQQBB- ——BQBB'BQQQ-4QBQ'SQQB-

U n-

1

B7

lii-i.

I .i

3, 43<

•IBQBB•BBQQ•BBBB•4BBQ•SBQBft_

115 »9S9Q Binzina. 1 . 4 -_l nithgxy- (9CI)JJIBBQB'I BQBB-

BBQB14BBB'9QBB'

B-^i — -f ' . l . . ——— . — > — i — . — . — . — • — i — . — . — • — . — i — •— H

1

4.1

\.&l.

\S3

/'

•IQQBB•BBQB•BBBB'4BQB•2BBQ

'••mM., 2BQ 3BQ 4BBHf &••,••.. Ha.i/Charpi

•y

Hf%$!' T: 115353 l-Bulanwie, 4-chlor'!''-'': Z: TIC of Oflffl:OX3898SH.O

EXCHRNGE dona Y: 15250 Benzene, 1,4-dimetho[HS21 X: Son 620 (12,498 .in) of D

•J

L1BRRRY SERRCH RESULTS

Scan 451 (9,919 *in) of WTfliDX389B5H.il (0H3B98 R F HESTON S03 2.ll(»9/IOnil I/5DIL M CLPIS

Library file: NBSJEVE.LLibrary nano: NBS HflSS SPECTRAL LflTfiBfiSE

CHS I Libraiy Halchlnde< I duality

I: 2-Cyclopenten-l-ono, 2,3,1-Irinelhyl- (6 28790855 3290 95562: 2-Cyclopenlen-l-one, 3,4,5-lrinolhyl- (9 55683211 329? 93523: 2-Cyclopenlen-l-one, 3,1,4-Irinelhyl- (6 30434652 3291 68701: 2-Cyclopenlen-Kne, 3,5,5-lrinelhyl- (6 24156954 3268 87885: 5-Oclyn-4-one, 2,2,7,7-lelr.nethyl- (8CI 28884691 12305 8613C: l-Prcpanone, Hl-cyclohwn-l-yl)- (8CI I6KOJ4 5289 82507: Hldphlhaleneielhanol, l,4,4a,5,6,7,0,0a 19078376 18552 82428: 3,5-Hepladien-2-cne, 6-melhyl-, (E)- (8C 16647014 )266 79769: fiBpidofraclinine-J-carlwxylic acid, inelh 5595I3 30143 783110: Phenol, 2-uethoKy, acelale (9CI) 613707 10097 7752

Hhich natch (I to 10);

Scan 491 (9,919 nln) of DRTR: DX3B9BSN. QIQBQB-BQQQ-BQQQ'4QQQ'2QBQ'

jj Q-

B.I

93

iL ,!«, .in*, .a, H*«. t 1

\ U*Q9 /

I4B.s s i ai. , S '

IOBQB'BQQQ•BBBB•4QQQ'2QQQ•a

li* »3Eaa B-Cycl op«nl»n-l-nnn, S, 9, 4-trt nuthyl - (BJJIBBBB'K BBBQ'

BQBB4BBB'SQBQ'

Bl |

asii'fvi 1

iQ9^,S4

•IQBBB•BBQQ

•BQBB•4BQQ•2BQB

SjBK'VV . ."• IBB ISO EBB•'"iKXJMv !'« Man /Charm' ;W$<% ' T: Scan 620 (12.498 tin) of D

•"' •'• ">!• Zi TIC of DflTfl:DX3898SH.DEXCHANGE dona Y: 13290 2-Cyclopenlen-l-one,EHS2] X; Scin 451 (9.919 Kin) of Dfl

1R/00075

LIBRARY SEARCH RESULT

Scnn 994 (18.396 Kin) of r.'ATA:DX36'?8$H.D113698 R F HESTON S03 2.11609/IOml l/SDIl l<l CLPIS

Library fi lot NBS.REVE.LLibrary naiio: NBS IIASS SPECTRAL DATABASE

Cn; 1 Library HutchIndex II duality

1: Elhanone, l-(2,6-dihydroxy4-«elhoKyphen 7507893 12773 9W92: Benstne, l,l'-elhylidenebia- (9CI) 6 I 2000 12690 92413: Bwzeno, dilorodielhylnelhyl- (9CI) 51618003 12590 91901: 1-Penlanono, l-(2,4,6-lrihyc!roKy3-»elhy 1*583268 IB788 07895; Benzene, l-mihyl-4-(phenylinelhyl)- (9CI 620337 I2693 89856: 2,'l-llexadienedioic acid, 3-melhyH-prop 58367445 I9li85 89657: Benzene, l-*elhyl-2-(phenylnelhyl)- fl'CI 713360 12691 B87C8: 2,1-Hewdienedioic acid, 3-»elhyl-4-prcp 69796130 19088 88709: 2,1-Hexadienedioic acid, 3,4-dielhyl-, d 31545752 17075 68C910! l,r-Biphenyl,2,2'-dii«elhyl- (9CI) 605390 12E87 8959

Nhich natch (I to 10):

Scan 994 (IB.39B mm) of QRfHi QX3B9BSN, QIQBBB-BQQQ'BBBB-•IQBB'2BBB'

IB?

53 77 |Q7 |_af t j tLi.. lLi_....il. . ...liLl-. J fc.... ..!..-. _.Ji ....h,i .J._.

219x.

•IQBQC•BQQQ•6QBQ•4QDB•S0BB

c*1 *

I SBBB'BBQQ'4BQB-saaa-

IC779 Ethnnoni, 1 -( 8, B-rtl hydrony-

IB?

49 _g III

i .W.,-. ii ,1 /

4-inathi))i>>phiin•IBBBB•BBBQ•BBQBMQBB'SBBBn

'Wfe'1 IBB I5a 2QBw"A. T: 112590 Benzene, chlorwliel"'A Zi TIC of DA1A:DX3898SH.D

EXCHANGE donn Y: 112773 Elhanone, l-(2,6-diIHS2] X: Scan 994 (18.396 nin) of D

LIBNARY SEARCH RESULTS

Scan 1064 (19.547 din) of ttiTfi:DXJ898SH,P 15VH3698 R F HESTON S03 2.1180t)/IOiil I/5ML M CLPIS ^

Library file: NBSJEVE.LLibrary naie: NBS HASS SPECTRAL DATABASE

CAS II Library MulchIndex I duality

li 2,'Hlexadienedioic acid, 3-iwlhyH-prop 58367115 19085 95962i 2,1-Hexadienedioic acid, 3-ielhyl-4-prop 69796130 19083 95773: 2,1-Hexadienedioic acid, 3,1-dielhyl-, d 3I147M8 19074 95121i 2,1-Hexadienedioic acid, 3,1-dielhyl-, d 31515752 19075 95105: Benzene, l,l'-(3,3-dinielhylbulylidene)bi 57123349 20628 95(i36: Benzene, I.T-lolradecylidenebis- I9CI) 55£fW38 30936 91787: 2H-l-Benz(.pyran-2-ono, 6-(2,2-diphenylel 31231188 304 JO 91718: Benzene, l,l',rl,r"-(l,2-elhanediylid 632W8 29929 9<P9: Heptane, 1,1-diphenyl- (8CI) 1530058 22231 915510: 9H-Carbazole (9CI) 86718 10118 9419

Which natch (1 to 10):

Scan IQB4 (19.947 nln) of ORTR: DX3B9BSM. QIBBBB-BQQQ'BBBQ-HC1BB-2QBQ'•

« QJ

,23a; 7 N (;?itt. , xlfl.iirtHIm |»IH ., ,nMn ri. ...I," ..Mft . nihn IMA ., ,,,

t67

I9B^ 22 Q1 /•

1 ,«. , ,, Ih ,,

•IQBQB'OBBB•BQQB•4QQB'EQQQQ

n* tSjlBQBQ'£ BBBQ'

BBBB'4BQQ'2BBB'

I9QB9 a,4-Hi«ad unariipl c acid

91•:! \. 'P7 I3B

. .i&.A'V . ii 1 ' 1 .^ i

3-mBthyl -4 -prop\B7

'" S,?B

•IQBQBBBBQ-BBBQMQBQ•8QQB-n

9Mj|!'; . OB I5B 2QQS&aft'::' Maii/Ch»ra««p;'; -.'".• T: 120628 Benzene, I,l'-(3,3-

Z: TIC of DflTA:DX3898SH,DEXCHANGE done Y; 119065 2,1-Hexadlenedioic[HS21 X: Scan 1061 (19,547 nin) of

ARI00077


Scan 922 (17.227 iin) of DATA:OX3890SH,DH3898 R F HESTON 503 2.11803/IOinl I/5DIL M CLPIS

Library file: NBS.REVE.LLibrary nans: N8S HASS SPECTRAL DATABASE

C(1S l Library hatchIndex I duality

I: Benzoicacid, 4-hydroi(v3-i»olhoxy (9CI) 121316 10193 90892: Phenol, 3,5-di«elhyl-1-(«elhyllhio)-, IN 2M2P57 18976 86GO3: Benzene, 1,2,3-lrimelhoxy (8CI9CI) f,31iPC IOH9 85011: Rcelanide, H-(1-nelno/!v2-nilrophenyl)- Il9ij|3 17026 83715: Naphlhol2,l-b]furan (6CI9CI) 232951 10430 82076: Benzenenelhanol, 3,4-dinethoxy (9CI) 73038 10511 61147: 9H-Pyri(lol3,1-blindole(eci9CI) 211633 10331 80818: lmidazo[2,l-ali»Miuincline (6CI9C1) 231708 10330 60769i Benzoicacid, 2-(melhyllhio)- (9CI) 3724105 10187 6K6I0i Oibenzofuran (8CI9CI) 132617 I042? 8D24

Nhich natch (1 lo 10);

Scan 582 (17,227 mm) of CiRTR: DX3B9BSN, DIQQBB'BQQQ'BBBQ-4BBQ-2BBD'

U ti-

153

53 B? V" 1

I 1 ^ '°? 1III,., L»,.L...J.llj, ,M4, U, . Jlh m,,n.ll,n,

IBB

. .. ,1. .

•1QBBB•BBBB•BBBB'4BBB2BBBfl

iiB »SJIQBBQ'

I BBQQ-EBBB'

4QBQ'2BBB'

IQ493 BanzDIc acid, 4"hydrQKy--3-m

153

L I r• thaxy- OCI)

IBB•IQQBB•BBBB•BBBB•4QBB•2BBB

*£&-.' IB'Q IS'B JB'QW'J. Mais/'ChargiW'-.1 Ts 118976 Phenol, 3,5-dliwlhy

Zs TIC of DATA:DX3898SH,DEXCHANGE done Y; 110493 Benztic acid, 4-hydinS2) Xi Scan 922 (17.227 iin) of D

ARI00078


RQV P. tyESTON. TNG.__________ LAB. NO. H389B

Actni Ralph MoJCeen ___________ DATE SAMPLED 10/07/19H7

Unahur County 4-H Camn Tarpit p fE RECEIVED 10/10/1987

__ S03 S. Area 3 _______________ nATF AMAI V7Er> 11/17/1987 C

"T"'NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < a LESS THAN

Sample Phase ___Sludge_ Liquid

Suspended Solida, % <0.5

Sample Treatment x_Extracted & Filtered & Analyzed_Filtered & Analyzed

E. P. TOXlcm*

Contandnant

Arsenic .. 0.009i <1

<0.05<0.2

iun <o.oiLead',-1' ••' <0.2Mercury <0.002Selenlun <0.005Silver <0.2

RESPECTFULLY SUBMITTED;* Determinations for E.P.Toxlcity, aa outlined in EPA PublicationSH-846, Test Methods for Evaluating Solid Haste, 2nd Ed., Revised 1984

1856 OR6ENBRIER STREET CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 304 346-0725


ROYF_. WESTON. INC. __________ |_A.B N0| H3B9H

Attn;_ Ralph McKeen ________ DATE SAMPLED 10/7/1987

UPshur County 4-H Camp Tarpit pxjp pprpiypp io/in/1987,TechniOQllasting .,,303 S. Ayea j ____________ DATE ANALYZED -LLOflliaflZ tcLaboratories Inc 11/24/1937

. ——————————————————————— ANALYST . „ Dfl/JS ,

NOTE; ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < ~ LESS THAN

PESTICIDES

Method DetectiorPARAMETERS Results, ug/1 Limit, uq/1

gamma-BBC [Lindane] ND 0.1Heptachlor ND • 0.1Heptachlor epoxide ND 0.1Endrin ND 0.5Chlordane ND 0.5Toxaphene ND 1.0Methoxychlor ND 1.02,4-D ND 12,4,5-TP (Silvex] ND 1 no/1

Not detected at a concentration equal to or greater thanthe Method Detection Limit.

( /Method Detection Limit had to be raised due to a largephenolic type interfere^., Q0080

.-••' RESPECTFULLY SUBMITTED: V.



ROY P. MRqTON, TNC. _________ LAg, NQ, H3B99

at-t-n- Ralph MPKP»" ________ DATE SAMPLED 10/7/1987

Upahur County _4-H Camp Tarpit JJAJE RECEIVED 10/10/1987

. S0" S. Area 4 ———————————— DATE ANALYZED -II/IiZIM?

High Level Soil Procedure ____ _ ANALYST WL/JER/ISSAll Results are on an as Received Basis.


BASE/NEUTRAL EXTRACTABLES [PAGE 1] . „ . . ,. ,*" — ' — —— ~ """" ""-•-"• — « i ^ H01StUlT6 J6 • 6Dilution Factor 10

Method DetectionPARAMETERS Results [uq/ql Limit [uq/ql

ppmN-Nitrosodimethylai,iine ND 250Bis(2-chloroethyl)ether ND :"ilj|:] i/ii 501,3-Dichlorobenzene ND r.. '"1' 501,4-Dichlorobenzene ND "''' 501,2-Dichlorobenzene ND 50Bis(2-chloroisoprop/l)ether ND 50N-Nitroaodi-n-propylamina ND 100Nitrobenzene ND 50

. Hexachlorobutadiene ND 501,2,4-Trichlorobenzene ND 50laophorone ND 50Naphthalene ND 50Bis (2-Chloroethoxy (methane ND 50Hexachlorocyclopentadiene ND 502-Chloronaphthalene ND 50Acenaphthylene ND 50Acenaphthene ND 50Dimethylphthalate ND 502,6-Dinitrotoluene ND 50Fluorene ND 504-Chloroph«0_'lphenylether ND 502,4-Dinitr||Koluene ND 50HexachloroKliane ND 50

.••v\ >*'MDLt Method Detection LimitND: Not detected at a concentration equal to or greater than the MDL

A R I O O O S bRESPECTFULLY SUBMITTED: J^—* . ' n^fnr^f^t li I \J *t ink i t*r*t*r*v\ J^r^Af ^1\ ^i A -



ROY F. WESTON, IMC.___________ LAB, NQ, H3899

ftttn! Ralph MnKegn__________ DATE SAMPLED 10/7/1987

Upshqr Cpunfcy 4-H Camp Tarpit DATE RECEIVED 10/10/1987

. S04 S. Area 4——————————___ DATE ANALYZED JI/I2ZI21Z

High Level Soil Procedure____ ANALYST - HL/JER/lSi

NOTE; ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < s LESS THAN

BASE/NEUTRAL EXTRftCTABLES [PAGE 2]

Method DetectionPARAMETERS Results [uq/gl Limit [uq/ql

ppm ppmDiethylphthalnte ND y, .-,,,,, 50N-Nitroaodiphenylamine ND ' .' ''' 100Hexachlorobenzene ND k|-''•<] 504-Broraophenylphenylether ND 50Phenanthrene ND 50Anthracene ND 50Dibutylphthalate ND 50Fluoranthene ND 50Pyrene ND 50Benzidine ND 250Butylbenzylphthalate ND 50Bia(2-ethylhexyl)phthalate ND 50Chrysene ND 50Benzol a(anthracene ND 503,3'-Dichlorobenzidine ND 250Di-n-octylphthalate ND 50Benzo(b)£luoranthene ND 50Benzo(k)fluoranthene ND 50Benzo(a)Pyrono ND 50Indeno(l,2,3-of(J)pyr«ne ND 100Dibenzo(a,,tt thracen« ND 100Benzol gnDflnjlena ND j.00MDLi MathoWiteotion LimitNDt Not detected at a concentration equal to or greater than tSe MDL

ARI0008•••'' RESPECTFULLY SUBMITTED;Jb



ROY P. WESTON, JTNC.__________ LAB. NO, _H3899

flfrtn! Ralph MoKeen_________ DATE SAMPLED .10/7/1987

typahur County 4-11 Camp Tarplfc DATE RECEIVED 10/10/1987

, S04 S. Area 4———————————— DATEANALYZED 11/19/1987

High Level Soil Procedure____ ANALYST WL/JER/ISSAll Results are on an as Received Basis.

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < ~ LESS THAN

ACID EXTRACTABLES% Moisture 36.6

Dilution Factor 10Method Detection

PARAMETERS ' Results [uq/g] Limit [uq/ajppm ppm •!.i

Phenol ND 502-Chlorophenol ND 502-Nitrophenol ND 502,4-Dimethylphenol 21* 502,4-Dichlorophenol ND 504-Chloro-3-methylphenol ND 502,4,6-Trichlorophenol ND 502,4-Dinitrophenol ND 2504-Nitrophenol ND 2502-Methyl-4,6-dinitrophenol ND 250Pentachlorophenol ND 250

.MDLi M«tJ»_"Detection Limit.ND: Not detected at a concentration equal to or greater than the MDL.* Parameter is present, result is estimated.

ARI00083RESPECTFULLY SUBMITTED: J_ki

1256 GREI-NBRIER STREET CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 304 346-0725

I! TIC of DftTfl:RW3899SW,Q ft"

t,

fln IUUU04

K-

W-

B3-

K-

t>4_IO^*

<.•!_

•r;

ARI00085

End of plot, Una « 3,23 to 47,72 nlnutea Chart apaad • 1. 00 cn/nln

IBDBQ'BBQQ'BBBB'•IBBB'2t)E)B'

H Q.C

a_ 77a /

1

X' 1 .Jn•nJJIBBBB'S. aaQQ'

BOOB'MODS'

2B0B-

a

k i ih 1! 1

T IBBBBIQ?

1

22

1 1

'BBQB'BBBB'4BQBSBBB0

»S1 Plunol , t.

7?

||

90

1 a?-rtlnithyl- (9CI), r IBBBBi

•BBRB'QQBB'•IBBB•EQBB

IQD IfB 20BM»si/Ch-rB«

T: Scon 620 (12,225 din) of DZi IIC of [ATRilWmp

EXCHflNGE done Vi <£4 Phenol, 2,4-diiMlh/l-»1S2) X: Scin 558 (11,329 niin) of D

UBRBRV SEflRCH RESULTS

Scin 559 (11,329 .in) of PflIfliRH3899SH.DH3697 R r HESTOH 2.0657(1/10*1 l» OIL HI CLPIS SH

Litforyflloi POLLUTE.LLibciry niiwi PRIORITY POLLUTANTS

CRS I Library Halchlndo« I quality

li Phenol, 2,4-dJMthyl- (9CI) 105579 21 95532i Phenol, l-chloro-3-iwlliyl- (9CI) 59507 37 43693i Phenol, 2,1-dlnllro- (8CI9CI) 51285 59 21381i Benzene, nilro- (BCI9CI) 96953 25 23725; Phenol, 2-*ethyl-4,Hinilro- (9CI) 534521 63 217561 Bmiwit, ethyl- (9CI9CI) Id0414 17 17367i Benieni, l:br«t»-i)-ptienoxy- (9CI) 101553 72 129661 Benteni,viM||l*. (HI) IC8883 9 12939i BenzMi«£|KHiyl-l,3-dlnllro- (9ei) 606202 5P 1273

lOi «iltiM«,i*S&*lofo- (9GI) 56235 11 12(2

Milch Midi (I lo IB)i

ARI00086


AOY F. WESTON. INC. __________ LAB. NO.

ACtni Raloly McKeen ___________ DATE SAMPLED -10/07/1987

Upahur County A-H Camp Tarpit DATE RECEIVED 10/10/198^

HB& S. Area A _______________ DATE ANAI Y7Ef> 1 1 / 1 7 / 1 9 8 7 t11/24/1987

AMA.VCT MS

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < a LESS THAN

Sanple Phase x_Solid__Sludge__U.quid

Suspended Solids, t <0.5X_>0.5

Sanple Treatment X Extracted * Filtered s, Analyzed ,.-..H,"Filtered & ftnalyzed '• :Q)

E. P. TOXICITO*

Contaminant

<0.005<1<0.05<0.2

roraiun <o.oi<0.2

Mercury <0.002Selenium < 0.005Silver <0.2

flRI00087RESPECTFULLY SUBMITTED:.

* Determinationn for E.P.Toxicity, as outlined in EPA PublicationSW-B46, Test Methods for Evaluating Solid Waste, 2nd Ed., Revised 19841258 GREENBfllER STREET CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 304 345-0725


ROY F. WESTON, INC._________ LAB, NO. H3B99

Attn; Ralph McKeen________ D/_jE SAMPLED _lQ/7/1987 .

Upshur County 4-H Camp Tarpit D/_,TE RECEIVED .10/10/19B7

S04 S. Area tl____________ D/^TEANALYZED.11/18/19H7 to11/24/1987

—————————————————————— ANALYST ——Dft/JS

NOTE; ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < - LESS THAN

PESTICIDES

Method DetectionPARAMETERS ' Results, uq/1 Limit, uq/1

garama-BHC [Lindane] ND 0.1Heptachlor ND 0.1Heptachlor epoxide ND 0.1Endrin ND 0.5Chlordane ND 0.5Toxaphene ND 1,0Methoxychlor ND 1.02,4-D ND 52,4,5-TP [Sllvex] ND 5

ND: Not detected at a concentration equal to or qreater thanthe Method Detection Limit.

ARI00088RESPECTFULLY SUBMITTED- % •*•



ROY P. WESTOM, INC.___________ LAB, NO. H390Q

__^hfen.i Ralph MnKppn___________ DATE SAMPLED -1Q/7/19B7

llpahur County 4-H Camp Tarpit DATE RECEIVED 10/10/1987

pflS Bapkgrrmr.fi______________. DATE ANALYZEn 10/18/1987

High Level Soil Procedure_____ ANALYST _HL/JER/ISS

All Results are on an as Received Basis.NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < = LESS THAN

BASE/NEUTRAL EXTRACTABLES [PAGE 1] % Moisture 13Dilution Factor 10

Method DetectionPARAMETERS Results [uq/q] Limit |uq/ql

ppmN-Nitrosodimethylamine ND 250Bi3|2-chloroethyl)ether ND 501,3-Dichlorobenzene ND 501,4-Dichlorobenzene ND .,,-M,,, , 501,2-Dichlorobenzene ND ' '• 'Ml. 50Bis (2-chloroiaopropyl (ether ND ".•..:; 50N-Nitrosodi-n-propylamine ND 100Nitrobenzene ND 50Hexachlorobutadiene ND 501,2,4-Trichlorobenzene ND 50Isophorone ND 50Naphthalene ND 50Bis(2-Chloroethoxy)methane ND 50Hexachlorocyclopentadiene ND 502-Chloronaphthalene ND 50Acenaphthylene ND 50Acenaphthene ND 50Dimethylphthalate ND 502,6-Dinitrotoluene ND 50Fluorene ND 504-Chloroph«nylphenylether ND 502,4-Dinitritoluene ND 50Hexachloro«y|hana ND 50

HDLi Method Detection LimitND; Not detected at a concentration equal to or greater than the MDL

ARI00089RESPECTFULLY SUBMITTED:J



pOY P. ftqfjTpNf inc._________ LAB, NO. H3900

Ahtni Ralph MrKPBn___________ DATE SAMPLED 10/7/1987

_ . , , Upshur County 4-H Camp Tarpit DATE RECEIVED 10/10/1987TechnicalBBS Background______________ DATE ANALYZED 10/18/1987

; ||"£High Level Soil Procedure_____ ANALYST WL/JER/ISE

NOTE; ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < = LESS THAN


Method DetectionPARAMETERS Results [uq/ql Limit [uq/q)

ppm ppmDiethylphthalate ND 50N-Nitrosodiphenylamine ND 100Hexachlorobenzene ND 504-Bromophenylphenylether ND , ,.-,,,,,, 50Phenanthrene ND ."""."''• 50Anthracene ND 50Dibutylphthalate ND 50Fluoranthene ND 50Pyrene ND 50Benzidine ND 250Butylbenzylphthalate ND 50Bis(2-ethylhexyl)phthalate ND 50Chrysene ND 50Benzo(a(anthracene ND 503,3'-Dlchlorobenzidine ND 250Di-n-octylphthalate ND 50Benzo(b)Cluoranthene ND 50Benzo(k)fluoranthene ND 50Benzo(a)Pyrene ND 50Indeno(l,2,3-c,d)pyrene ND 100Dibenzo( a, .anthracene ND 100Benzo(ghi)»rylane ND 100

W '"'•MDLt Methodrfttietlon LimitND; Not detected at a concentration equal to or greater than the MDL

M/00090RESPECTFULLY SUBMITTEDiJ^,



ROY F. WESTON. INC,__________ LAB, NO. H390Q

ftttn: Ralph JlcKepn_________ DATE SAMPLED 10/7/1987

Upshur County 4-H Camp Tarpit DATE RECEIVED 10/10/1987

BUS Background_____________ DATE AKIAI V7Fn 10/18/1987

High Level Soil Procedure____ ANALYST WL/JER/ISSAll Results are on an as Received Basia.

NOTE; ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED. < B LESS THAN

ACID EXTRACTABLESt Moisture' • 13.1

Dilution Factor 10Method Detection

PARAMETERS Results [uq/ql Limit [uq/qlppm ppm

Phenol ND 502-Chlorophenol ND '50 "2-Nitrophenol ND 502,4-Dimethylphenol ND 502,4-Dichlorophenol ND 504-Chloro-3-methylphenol ND 502,4,6-Trichlorophenol ND 502,4-Dinitrophenol ND 2504-Nitrophenol ND 2502~Methyl-4,6-dinitrophenol ND 250Pentachlorophenol ND 250

MDLi MetKod Detection Limit.NDi Not detected at a concentration equal to or greater than the MDL.

ARI0009RESPECTFULLY SUBMITTED:

1256 GREENBRIER STREET CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 004 34B-0725

li TIC of OflTftlRW390BSW.Q /fce/I/W-^ S ? S~

r

SRlr

-li

K-T

K~

8-

si-ia-i

/

End pf plot. Tina • 3.23 to 45,85 nlnutos Chart apaad • I.BB an/«Hn


ROY F. HBSTON. INC. ___________ LAB, NO. H3900

Attn! Ralph HeKeen ___________ , DATE SAMPLED ^10/07/1087

Unahur County A-lj Camn Tarpit DATE RECEIVED -10/10/1987

S85 Background _____________ DATE AKJALVZEn 11/17/1987 t[orleslnc

—————— i ———————————————— ANALYST - Hs

NOTE: ALL RESULTS EXPRESSED IN MG/L UNLESS OTHERWISE DESIGNATED, < = LESS THAN

Sample Phase jcjolid__Sludge_Liquid

Suspended Solids, « <0.5 ^ 'F>0.5

Sample Treatment Extracted & Filtered & Analyzed ,_Filtered & Analyzed -{

E. P. TOXICITV*

Contaminant

<o.oo5<i<o.os<0.2<0.01

Lead ; '"'•' •'"• <o.2Mercury <0-002Selenium <°-0°5Silver <°-2

RESPECTFULLY SUBMITTED;__!*__.* Deteiminatlona for E.P.Toxicity, aa outlined in EPA PublicationSH-B46, Test Methods Cor Evaluating Solid Waste, 2nd Ed., Revised 1984

1256 QREENBRIER STREET CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 304 346-0725


ROY F. WESTON, INCJ_________ LAB. NO. H3900

Attn; Ralph McKeen________ DATE SAMPLED .10/7/1987

Upshur County_4-H Camp Tarnit DATE RECEIVED .10/10/19.87.

SgS Background___________ DATE ANALYZED J-L/lfl/lSfiZ titorieslnc . 11/24/198?______———————————————— ANALYST


PESTICIDES

Method DetecticPARAMETERS Results, uq/1 Limit, uq/1

gamma-BHC [Lindane] ND 0.1Heptachlor ND ' 0.1Heptachlor epoxide ND 0.1'Endrin ND 0.5Chlordane ND 0.5Toxaphene ND 1.0Methoxychlor ND 1.02,4-D ND 52,4,5-TP [Silvex] ND 5

ND: Not detected at a concentration equal to or greater thanthe Method Detection Limit.


1256 GREENBRIER STREET CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 304 346-0725ARIQ0095

NARRATIVE - GC/MS ANALYSIS OCTOBER, 1987 · NARRATIVE - GC/MS ANALYSIS ROX P. WESTON - UPSHUR...

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Transcript of NARRATIVE - GC/MS ANALYSIS OCTOBER, 1987 · NARRATIVE - GC/MS ANALYSIS ROX P. WESTON - UPSHUR...