Microstructure analysis by high quality FIB technique...Microstructure analysis by high quality FIB...

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Microstructure analysis by high quality FIB technique / Best Technical Support Contribution Award Awardee Tomoyo Nakao ( Nagoya University, Advanced Characterization Nanotechnology Platform) Overview The sample processing method using FIB is a key technology for observing microstructure. Until now, microstructural analysis of various samples has been conducted mainly by orthogonal FIB-SEM. In this presentation three topics were selected as follows; three-dimensional structure observation of biological samples using FIB-SEM Cut & See technique, cross-sectional observation of alloy particles for next-generation solder, and Ir nanopillar structure analysis. 3D observation of biological samples using FIB-SEM Cut&See technique TEM sample preparation using FIB High Voltage Electron Microscope Laboratory, Institute of Materials and Systems for Sustainability Nagoya University Tomoyo Nakao FIB, FIB - SEM, 3D, EDS, TEM, STEM TEM sample preparation using an Argon ion beam (a) (a) (b) Gaイオン方向 B A (b) (c) (d) Carbon depo. Ag Sn Cu EDS Map (e) (c)

Transcript of Microstructure analysis by high quality FIB technique...Microstructure analysis by high quality FIB...

Page 1: Microstructure analysis by high quality FIB technique...Microstructure analysis by high quality FIB technique / Best Technical Support Contribution Award Awardee Tomoyo Nakao (Nagoya

Microstructure analysis by high quality FIB technique

/ Best Technical Support Contribution Award

Awardee Tomoyo Nakao (Nagoya University, Advanced Characterization Nanotechnology Platform)

Overview

The sample processing method using FIB is a key technology for observing microstructure. Until now, microstructural analysis of various samples has been conducted mainly by orthogonal FIB-SEM. In this presentation three topics were selected as follows; three-dimensional structure observation of biological samples using FIB-SEM Cut & See technique, cross-sectional observation of alloy particles for next-generation solder, and Ir nanopillar structure analysis.

3D observation of biological samples using FIB-SEM Cut&See technique TEM sample preparation using FIB

High Voltage Electron Microscope Laboratory, Institute of Materials and Systems for SustainabilityNagoya UniversityTomoyo Nakao

FIB, FIB-SEM, 3D, EDS, TEM, STEM

TEM sample preparation using an Argon ion beam

(a)

(a) (b) Gaイオン方向

面B

面A

(b) (c) (d)Carbon depo.

Ag

Sn

Cu

EDS Map(e)

(c)