MEMORANDUM FROM TERRI WHITE, USEPA TO JON … · Project: 13-0162, Aberdeen Groundwater - Reported...

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division:

980 College Station Road, Athens, Georgia 30605-2700 D.A.R.T Id: 13-0162

Project: 13-0162, Aberdeen Groundwater - Reported by Terri White

4SESD-ASB

MEMORANDUM

February 22,2013

SUBJECT: FINAL Analytical Report

Project: 13-0162, Aberdeen Groundwater

Superfund Remedial

FROM: Terri White

ICS Chemist

THRU: Mike Wasko, Chief

ASB Inorganic Chemistry Section

T O : Jon Bomholm

Attached are the final results for the analytical groups listed below. These analyses were perfonned in accordance with the Analytical Support Branch's (ASB) Laboratory Operations and Quality Assurance Manual (ASB LOQAM) found at www.epa.gov/region4/sesd/asbsop. Any unique project data quality objectives specified in writing by the data requestor have also been incorporated into the data unless otherwise noted in the Report Narrative. Chemistry data have been verified based on the ASB LOQ/\M specifications and have been qualified by this laboratory if the applicable quality control criteria were not met. Verification is defined in Section 5.2 of the ASB LOQAM. For a listing of specific data qualifiers and explanations, please refer to the Data Qualifier Definitions included in this report. The reported results are accurate within the limits of the method(s) and are representative only of the samples as received by the laboratory.

Analyses Included in ihis report: Method Used: Accreditations:

Total Metals (TMTL)

Tolal Metals Tolal Metals

EPA 200.8 (Water) EPA 6010 (Water)

ISO ISO

of 18 E130310 TMTL FINAL 02 22 13 1349 2/22/13 13:49

http://www.epa.gov/region4/sesd/asbsop

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division



Sample Disposal Policy

Because of the laboratory's limited space for long term sample storage, our policy is to dispose of samples on a periodic schedule. Please note that within 60 days of this memo, the original samples and all sample extracts and/or sample digestates will be disposed of in accordance with applicable regulations. The 60-day sample disposal policy does not apply to criminal samples which are held until the laboratory is notified by the criminal investigators that case development and litigation are complete.

These samples may be held in the laboratory's custody for a longer period of time if you have a special project need. If you wish for the laboratory to hold samples beyond the 60-day period, please contact our Sample Control Coordinator, Debbie Colquitt, by e-mail at Colquitt.Debbie(a)epa.gov, and provide a reason for holding samples beyond 60 days

cc: Nardina Turner

of 18 EI30310 TMTL FINAL 02 22 13 1349 2/22/13 13:49




SAMPLES INCLUDED IN THIS REPORT


Sample ID

ACGMW26

ACGM\V27

ACGMW29

ACGMW929

GEIMW29D

CE1MW29L

Laboratory ID

El 30310-02

El 30310-03

El 30310-04

El 30310-05

El 30310-06

El 30310-07

Matrix

Groundwater

Ground waler

Groundwater

Groundwater

Groundwater

Groundwater

Date Collected Date Received

1/17/13 16:15

1/17/13 17:55

1/16/13 16:40

1/16/13 16:40

1/17/13 11:30

1/17/13 11:20

1/18/13 11:32

1/18/13 11:32

1/18/13 11:32

1/18/13 11:32

1/18/13 11:32

1/18/13 11:32

of 18 E130310 TMTL FINAL 02 22 13 1349 2/22/13 13:49




DATA Q U A L I F I E R D E F I N I T I O N S

U The analyte was not detected at or above the reporting limit.

J The identification of Ihe analyte is acceptable; the reported value is an estimate.

OL-2 Laboratory Control Spike Recovery greater than method control limits

QM-1 Matrix Spike Recovery less than method control limits

A C R O N Y M S A N D A B B R E V I A T I O N S

C A S Chemical Abstracts Service

Note; Anaiytes with no known CAS identitlers have been assigned codes beginning with "E". the EPA ID as assigned by the EPA Substance Registry System (ww\v.epa.gov/srs), or beginning with "R4-", a unique identifier assigned by the EPA Region 4 laboratory.

ISO The tesL if analyzed after June 26. 2012, is accredited under the EPA Region 4 ASB's ISO/IEC 17025 accreditation

issued by /VNSI-ASQ National Accreditation Board/ACLASS. Refer to certificate and scope of accreditation AT-1691.

M D L Method Detection Limit - The minimum concentration of a substance (an analyte) that can be measured and reported with a 99% confidence that the analyte concentration is greater than zero.

M R L Minimum Reporting Limit - Analyte concentration that corresponds to the lowest demonstrated level of acceptable quantitation. The MRL is sample-specific and accounts for preparation weights and volumes, dilutions, and moisture content of soil/sediments.

TIC Tentatively Identified Compound - An analyte identified based on a match wilh the instrument software's mass spectral library. A calibration standard has not been analyzed to confinn the compound's identification or the estimated concentration reported.

of 18 E1303I0TMTLFINAL02 22 13 1349 2/22/13 13:49




P r o j e c t : 13-0162, A b e r d e e n G r o u n d w a t e r

Total Metals

Sample ID: ACGMW26

Station ID: ACGMW26

L a b ID : E l 3 0 3 1 0 - 0 2

Matrix: Groundwater

Date Collected: 1/17/13 16:15

< 4.V'J:'^-:-;„»-;!/.!; • - ^ ^ K ^ - ^ : - - . m. : '•v:.W4A-/f:i ' " ^ A i ' :

-.-•'A.'A%.--,'}.'ie. «i-.Wi/r.v> Qtwl i f ie rs ' . f 4 i % . A - : : U i i i t s . ^ ^ h £ < M R L : - . . •Pivp'arcdii.Analy:ed.".Meihfld'j.- ' l - ' : • f - ' - . -XJC^y" , j ^ ' ^ - ' - ^ - ° ^ S ; . ^ » : . - ^ ^ ^ ^ g ^ > Q " T ^ ^ : . : - K i ^ m A t ' - > - : i - f i r % f - i i ^ - i ! A - - - ^ A . . : s ' i ^ . - A ' ' - - : : A r •

. : « 'm-^û : !,»-

-'Alumihu'ni^S^

Antimony

'"Arsenic

Barium "-?=- X" ' —

'Beryllium ...U3Si.<;i.si

Cadmium

-:7->".raTYyfpyrp;.- .-*'.'.'..' ^ 'K- ' '-*t

'^•"A-A'T^,- . ' - ' ' i ^ ^v .

-=:8W«^rr- • -- . - f . . . , ; - . -

ug/L 1,0 P P P P P P EPA 200 8

--r:r«-"37''rEg'

Ug/L '

13 3fi

" L W B " ' i.''36.-:

1/24/13 Ll 13

:.C^^3;0-U.

: ' ' ^ ^ • : 1-0

ug/L 5.0

'PWZ "" iM3l ."^^Po^".'^îlfe"

2/13/13 • 111.32

1/29/13 ;U2S

EPA 200.8

EPAOOIO

0.50 Ll ug/L 0.50 1/24/13

13 36 :/13/l3 1832 EPA 200 8

•"-x:aiAPÂA-...A'PPP.::rr.. -••• . - ^ S S l:^;,?»îôo•^••;:^• ¥^?vi- : ' .? . - :^S7^' '$^^":250' ** EPA6010:. -.V -i-1/24/l3^y.' "•'M-Vtr^

i^: -=•:• l Magnfesiuffi AApAii^' c : •^:^ |^ ' :* ' '~K!i; 4 j 7()0 'rf \ f i f a « s f j--vK,:, ;iiigA^:j ••;i;s~ Q: sc i :Z ' ' ?Â§^^&Â eoio' Manganese ug/L

ug/L

ug/L

ug/L

II I im^r. ."j j«i*tfjUi., 1 I • .I.,,. .^,n.i.,r.,A

5.0

10

10

ILOOO-

2.0

1/24/13 13 33

^•M/24'/13' • '•13J3^

I 34/13 13 33

2/01/13 c D A A n i o |g -iq hPA60I0

';o'28'' '-l-EPA*Olo

1/24/13?irj,-': 2/01/13

1/24/13 II 2b

2/13/13 18 32

EPA 6010

EPA60iq;-;S

EPA 200 8

"^f^M's;'V--Stj-'^'<:--ni"''-'':i/2^7fFJ^-i7:9/i3'j-Vp-o^^

ug/L 1000

iTl iîrftri.wftrt<

7440-65-5

7440-66-6:.

Yttrium

• Zinc ',rfr:

ug/L 5 0

ug/L 3.0 P P P 'S'^l,-' EPA 6010 3.0

fo

i/:4/i3 13 33

V\?i4i'l3'~, : 13 33..

i/:'3/i3 20::

' T o ' o ' / r r T T ^ ^ ^ ^ ? ^ ! ^ ^ : ^ '

of 18 El30310 TMTL FINAL 02 22 13 1349 2/22/13 13:49





Total Metals

.Sample ID: ACGMW27

Station ID: ACGMW27

L a b I D : E l 3 0 3 1 0 - 0 3

Matrix: Groundwater


of 18 El30310 TMTL FINAL 02 22 13 1349 2/22/13 13:49





Total Metals

Sample ID: ACGMW29

Station ID: ACGMW29

Lab ID: E130310-04

Mat r i x : Groundwater

Dale Collected: 1/16/13 16:40

of 18 E130310 TMTL FINAL 02 22 13 1349 2/22/13 .:49

U N I T E D STATES E N V I R O N M E N T A L P R O T E C T I O N A G E N C Y

Region 4 Science and Ecosystem Support Division

980 Col lege Station Road, Athens , Georgia 30605-2700

D.A.R.T Id: 13-0162


P r o j e c t : 13-0162, A b e r d e e n G r o u n d w a t e r

Total Metals

Sample ID: ACGMW929

Station ID: ACGMW29

L a b ID : E l 3 0 3 1 0 - 0 5

Matrix: Groundwater


Number.- . A'n:i^4iialyle • . ' ^-• : l -#4ir^ •••r-.^ISl^f^;,--* •Re.mt^fiUlifii^rs',>h-f.w, : - P i A ^ W & W ^ i ^ '•. '. '(/hiis^ '•' "

' ' 'Jf t •- - '-•••Ai H -'• '. ,''J:k:i 3;i';-A'':'.--'As'--.-A. :• '.''.P'M.-^A -AlMRI:••fPrepared."'-AnalyreiipMeih'od "- '^Sv^^ '

7429-90;5r;j ja^rtif i ir; I - ^ . ^ 2 ' ' 3 .

7440-36-0

.Aluminum

7782-49-2

7440-22-4

7440-23-5

744lf24-6" ;: Ahz: -..

7440-28-0

744oSl-5

7440-32-6

7440-,62-2

7440-65-5

EPA 6010

Strontium.'^ - .• ,f(pp>;:7'-,:~ "4^^?^^^ •

Thallium

' ZMj^zziZllS^z ' '" '^ Titanium

Vanadium

Yttrium 744p;6'626i:-jV^|Zinc ~. - ' ^ M ^ . - V >*i»':fl!.5.p

of 18 E130310 TMTL FINAL 02 22 13 1349 2/22/13 13:49



Project 13-0162, Aberdeen Groundwater - Reported by Terri White


Total Metals

Sample ID: GEIMW29D

Station ID: GEIMW29D

Lab ID: El30310-06

Matrix: Groundwater


Nu'mHcr- '••''--, '^ -iiiatvte. 'A.-:-.. -•.Sf,?-..^. -r ':.V-;p-?-' -s"" -; -'A' ^Resultsc:QuiilifiikrAi'A-.-: •. •.•tfUifits' ---.'^y'Ai^lRIAS Prepar'ed:.'-W>alx-'icdr'ifethi,d^>AAii':,TfA -*:•;- • - ^ w ; . '-' - . - n i i - . . :---V^Mi::tA •• ••-.• •••iy:t'A, •• ' •• ' •• • "fe-.' • •:->':--:tA^-t.-

7429-90^5'.'fi-'S-4:'.Aluminum'sfl

7440-36-0

7440-38r2?j

7440-39-3

Antimony . . . - . . — j . . p ^ . .

Arsenic, '-^st:' Barium

7440-4l--7jWjy-BVryllm f 'J " •^^WlyZ'^' Cadmium 7440-43-9

7440-70-2''tii-^Calcium Liji2« U,.2^?iA<w . •,., :'.-.,s • J i L -

ug/L

ui/L?'

ug/L

1.0

"Z 5.0

1/24/13 13 36

~i/Un-i ,.13-36

1/24/13 13 33

2/01/13 -

I.JS.'SAB 2/13/13

11 01

; EP.A 6 0 1 0

ug/L >mAkZ^zoZ"^^p

0.50 1/24/13 13 36

2/13/13 t l 09 j^

I/2W13 21 00

'.rjriTw/iT

2/13/13 II O'l

9313 i^.=. ft,VfV,V

EPA 2 0 0 8

E P A 2 6 0 . ' 8 '

EPA 6 0 1 0

•eepmp EPA 200 8

' '^$iS^-^''^~iip/i~'AAS^^^Pn^^'2*'>i^'A'.~^SS\'i]^^ i g ! f e :3^ in : t b "%v^- ; j . - ; ; jB^y^ ' y^ l3 33----'':.'';.-:20 00 ,= ' ;^^^

7440-47-3

S40-48-4, l^^^^.h ;,.;..^'j;d

7440-50-8

7439,-89-6^

7439-92-1 7439:954^.'

7439-96-5

Chromium EPA 5010

of 18 EI3O310 TMTL FINAL 02 22 13 1349 2/22/13 13:49



Project 13-0162, Aberdeen Groundwater - Reported by Terri White


Total Metals

Sample ID: GEIMW29L

Station ID: GEIMW29L

Lab ID: El30310-07

Matrix: Groundwater


of 18 EI30310TMTLFrNAL02 22 13 1349 2/22/13 13:49




Total Metals (TMTL) - Quality Control

US-EPA, Region 4, SESD

EPA 6010

Silver

Barium

Beryllium

Cobalt

Chromium

Copper

Molybdenum

Nickel

Tin

Strontium

Titanium

Vanadium

^'ttrium

Zinc

u

u

u

u

u

u

u

u

LI

U

Ll

U

U

U

5.0

5.0

3.0

5,0

5,0

10

10

10

15

5,0

5,0

5.0

3,0

10

ug

Analyte Result

Reporting

Limit Units

Spike Soiu-ce %REC

Level Result %REC Limits RPD

RPD

Limit Notes

Batch 1301092 - M 200.2 Metals Water

Rlank(130l092-BLKI) Prepared: 01/24/13 Analyzed: 01/29/13

Blank (I30I092-BLK2) Prepared: 01/24/13 Analyzed: 02/01/13

EPABOIO

Aluininuin

Manganese

Calcium

Magnesium

Iron

Sodium

Potassium

u

u

u

u

u

u

u

too

5,0

250

250

100

1000

1000

" t

LCS(I30I092-BSI) Prepared: 01/24/13 Analyzed: 01/29/13

EPA 6010

Silver

Barium

Beryllium

Cobalt

Chromium

Copper

Molybdenum

Nickel

Tin

Strontium

Titanium

99,897

195,07

49,550

99,151

199,75

102.74

100 35

199.80

103,18

98,877

101,93

5.0

5,0

3,0

5,0

5,0

10

10

10

15

5,0

5,0

"t 7L 100,00

200.00

50 000

100,00

200,00

100,00

100,00

200,00

100,00

100,00

100,00

99.9

97.5

991

9 9 2

9 9 9

103

IOO

99,9

103

98,9

102

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

Page II of 18 E130310 TMTL FINAL 02 22 13 1349 2/22/13 13:49

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Divis ion

980 College Station Road, Athens, Georgia 30605-2700

D.A.R.T Id: 13-0162




Analyte Result

Reporting

Limit Units

Spike Source ?-iREC

Level Result %REC Li)nits RPD

RPD

Limit Notes


LCS(130I092-BSI) Prepared; 01/24/13 Analyzed: 01/29/13 Vanadium

\'ttriuin

Zinc,

100.54

101.33

200.69

5,0

3,0

10

ug/L 100,00

100.00

200,00

101

101

100

85-115

85-115

85-115

LCS (1301092-BS2) Prepared: 01/24/13 Analyzed; 02/01/13

EPA 6010 Aluminum

Manganese

Calcium

.Magnesium

Iron

Sodium

Potassium

5028,3

513,59

5267.4

5105.5

6059,1

10068

9o93,7

IOO

5,0

250

250

IOO

1000

1000

"t / L 5000.0

500.00

5000.0

5000,0

5000,0

IOOOO

IOOOO

lOI

103

105

102

121

101

96,9

85-115

85-115

85-115

85-115

85-115

85-115

85-115

OL-2

Matrix Splke(130l092-MSI) Source: El30307-02 Prepared: 01/24/13 Analyzed: 01/29/13

EPA 6010 Silver

Barium

Beryllium

Cobalt

Chromium

Copper

Molybdenum

Nickel

Tin

Strontium

Titanium

Vanadium

^'ttrium

Zinc

98,522

209.72

49.479

99385

198.10

103.35

99.617

196.61

102.82

106.36

103.52

100.44

101.45

199.61

5 0

5.0

3.0

5.0

5.0

10

10

10

15

5.0

5.0

5.0

3.0

10

"t 7L 100.00

200.00

50.000

100.00

200.00

100.00

100.00

200.00

100.00

100.00

100.00

100.00

100.00

200.00

u 13.465

u 0.61717

u u u u u

6.3462

U

U

0.83376

3.5654

98.5

98.1

99.0

98.8

99.1

103

99.6

98.3

103

IOO

104

IOO

101

98.0

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

of 18 E130310 TMTL FINAL 02 22 13 1349 2/22/13 13:49

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY



D.A.R.T Id: 13-0162 Project: 13-0162, Aberdeen Groundwater - Reported by Terri White



Analyte

Reporting

Result Limit Units

Spike Source "'oREC

Level Result %REC Limits RPD

RPD

Limit Notes


M a t r i x S p i k e ( I 3 0 I 0 9 2 - M S 2 ) S o u r c e : E l 3 0 3 1 0 - 0 2 Prepared: 01 /24/13 Analyzed: 01 /29/13

EPA 6010 Silver

Barium

Ber\'llium

Cobalt

Chromium

Copper

Molybdenum

Nickel

Tin

Strontium

Titanium

Vanadium

N'ttrium

Zinc

97.595

282.81

49759

101.19

222.09

105.51

103.27

204.59

79.514

152.41

109.03

II0.5I

108.89

222.72

5.0

5.0

3.0

5.0

5.0

10

10

10

15

5.0

5.0

5.0

3.0

10

ug/L

" " -" " " "

"

" "

100.00

200.00

50.000

100.00

200.00

100.00

100.00

200.00

100.00

100.00

100.00

100.00

100.00

200.00

, U

88,812

0,59388

2,0584

27.507

5.6140

9.7858

13.983

U

53.637

38.694

11.020.

8.6528

27.335

97.6

97.0

98.3

99.1

97.3

9 9 9

93.5

95.3

79.5

98.8

70.3

99.5

IOO

9 7 7

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

Matrix Spike (1301092-MS3) Source: E130307-02 Prepared: 01/24/13 Analyzed: 02/01/13 EPABOIO Aluminum

Manganese

Calcium

Magnesium

Iron

Sodium

Potassium

5037.9

531.53

5663.9

5574.6

5789.1

12551

11078

100

5.0

250

250

IOO

1000

1000

nil. 5 0 0 0 . 0

5 0 0 . 0 0

5 0 0 0 . 0

5 0 0 0 . 0

5 0 0 0 . 0

IOOOO

IOOOO

U

18.521

1295.1

4 7 2 . 3 1

4 2 6 . 2 1

2646 .1

I 4 I 3 . 6

101

103

107

104

107

9 9 . 0

9 6 . 6

7.5-125

7 5 - 1 2 5

7 5 - 1 2 5

7 5 - 1 2 5

7.5-125

7 5 - 1 2 5

7 5 - 1 2 5

M a t r i x S p i k e ( 1 3 0 l 0 9 2 - M S 4 ) S o u r c e : E l 3 0 3 1 0 - 0 2 Prepared; 01 /24 /13 Analyzed; 02 /01/13

EPA 6010 Aluminum

Manganese

Calcium

Magnesium

Iron

Sodium

Potassium

12212

764.45

10379

7006.0

13085

3934S

10940

100

5.0

250

250

IOO

1000

1000

"t 7L

'

5000.0

500.00

5000.0

5000.0

5000.0

IOOOO

IOOOO

6958.6

235.71

5041.1

1725.9

7523.5

29469

936.69

105

106

107

106

III

98.8

IOO

75-125

75-125

75-125

75-125

75-125

75-125

75-125

of 18 EI30310 TMTL FINAL 02 22 13 1349 2/22/13 13:49






EPA 6010 Silver

Barium

Beryllium

Cobalt

Chromium

Copper

Molybdenum

Nickel

Tin

Strontium

Titanium

Vanadium

Yttrium

Zinc

98.214

210.36

49.815

99.019

200.06

100.71

99353

198.28

101.63

106.71

100.61

99.551

101.68

200.71

5.0

5.0

3.0

5.0

5.0

10

10

10

15

5.0

5.0

5.0

3.0

10

"t yL 100.00

200.00

50.000

100.00

200.00

100.00

100.00

200.00

100.00

100.00

100.00

100.00

100.00

200.00

U

13.455

u 0.61717

U

U

, u u u

5,3462

u U

0,83376

3,5654

98.2

98.4

99,5

98,4

100

101

99,4

99.1

102

100

101

99.5

101

98.5

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

0.313

0.302

0.677

0.369

0.984

2.59

0.265

0,844

1,16

0,328

2,95

0,889

0,231

0.552

20

20

20

20

20

20

20

20

20

20

20

20

20

20

Analyte

Reporting

Result Limit Units

Spike Source '!i,REC

Level Result ^oREC Limits RPD

RPD

Limit Notes


M a t r i x S p i k e O u p ( 1 3 0 1 0 9 2 - M S D I ) Source: EI30307-02 Prepared; 01/24/13 Analyzed: 01/29/13

Matrix Spike Dup (I30I09Z-MSD2) Source: El30310-02 Prepared: 01/24/13 Analyzed; 01/29/13

EPABOIO Silver

Barium

Ber>'llium

Cobalt

Chromium

Copper

Molybdenum

Nickel

Tin

Strontium

Titanium

Vanadium

Yttrium

Zinc

97,559

284,34

49,354

99,356

220,87

108.52

101,80

206.03

82,412

152.05

113.12

109.54

108,54

219.12

5,0

5,0

3,0

5,0

5,0

10

10

10

15

5.0

5,0

5,0

3,0

10

"t yL 100.00

200.00

50.000

100,00 .

200.00

100.00

100.00

200.00

100.00

100.00

100.00

100.00

100.00

200.00

u 88.812

0.59388

2.0584

27.507

5.6140

9.7858

13.983

U

53.637

38.694

11.020

8.6528

27.335

97.7

97.8

97.5

97.3

96.7

103

92.0

96.0

82.4

98.4

74.4

98.5

99.9

95.9

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

0.0651

0.540

0.797

1.82

0.554

2.81

1.44

0.701

3.58

0.242

3.68

0.793

0.321

1.63

20

20

20

20

20

20

20

20

20

20

20

20

20

20

QM-1

of 18 El30310 TMTL FINAL 02 22 13 1349 2/22/13 13:49




D.A.R.T Id: 13-0162




EPA 6010

Aluminum

•Manganese

Calcium

Magnesium

Iron

Sodium

Potassium

5058.4

540.09

6823.5

5728.4

5892.3

12662

II 160

100

5.0

250

250

IOO

1000

1000

ug/L

" -" " " -

5000.0

500.00

5000.0

5000.0

5000.0

IOOOO

IOOOO

U

18.521

1295.1

472.31

426.21

2646.1

I4I3.6 /

101

104

III

105

109

100

97.5

75-125

75-125

75-125

75-125

75-125

75-125

75-125

0.407

1.58

2.37

0.942

1.77

0.881

0.745

20

20

20

20

20

20

20

Analyte

Reporting

Result Limit Units

Spike Source '/oREC

Level Result ".iREC Limits RPD

RPD

Limit Notes


M a t r i x Spike D u p ( l 3 O I 0 9 2 - M S D 3 ) Source: EI30307-02 Prepared: 01/24/13 Analyzed; 02/01/13

Matrix Spike Dup (130I092-MSD4) Source: El30310-02 Prepared; 01/24/13 Analyzed; 02/01/13

EPA 6010

Aluminum

Manganese

Calcium

Magnesium

Iron

Sodium

Potassium

I 2 I 3 2

7 4 0 . 7 0

10088

6 7 7 5 . 0

12798

3 8 3 2 9

10582

IOO

5.0

250

250

IOO

1000

1000

u g / L

"

5 0 0 0 . 0

5 0 0 . 0 0

5 0 0 0 . 0

5 0 0 0 . 0

5 0 0 0 . 0

IOOOO

IOOOO

5968.5

235.71

5041.1

1726.9

. 7523.5

29469

936.69

103

101

lOI

101

105

88.6

96.5

75-125

75-125

75-125

75-125

75-125

75-125

75-125

0.655

3.15

2.85

3.35

2.21 •

2.62

3.33

20

20

20

20

20

20

20

MRL Verification (li01092-PSl) Prepared: 01/24/13 Analyzed: 01/2^/13

EPA 6010

Silver

Barium

Ber\llium

Cobalt

Chromium

Copper

Molybdenum

Nickel

Tin

Strontium

Titanium

Vanadium

Yttrium

Zinc

5.3386

5.3336

3.0781

5.0200

5.7409

9.9564

10.997

10.675

15.891

4.9962

5.4825

4.6900

2.9708

11.662

5.0

5.0

3.0

5.0

.5.0

10

10

10

15

5.0

5.0

5.0

3.0

10

ug/L

" "

--" "

" "

"

-

5.0000

5.0000

3.0000

5.0000

5.0000

10.000

10.000

10.000

15.000

5.0000

5.0000

5.0000

3.0000

10.000

107

107

103

IOO

115

99,6

no 107

106

99.9

no 93.8

99.0

117

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

MRL-2

MRL-2

MRL-2

MRL-2

MRL-2

MRL-2.

U

MRL-2

MRL-2

MRL-2

MRL-2.

U

MRL-2

MRL-2.

U

MRL-2.

u

MRL-2

of 18 El30310 TMTL FINAL 02 22 13 1349 2/22/13 13:49






.Analyte Result

Reporting

Limit Units

Spike Source ^oREC

Level Result '^iREC Limits RPD

RPD

Limit Notes

Batch 1301092 - iM 200.2 Metals Water

MRL Verincation (I30I092-PS2) Prepared: 01 /24/13 Analyzed; 02 /01/13

EPA 6010

Aluminum

Manganese

Calcium

Magnesium

Iron

Sodium

Potassium

110.70

5.4963

271.42

250.64

109.00

1174.5

1001.9

IOO

5.0

250

250

IOO

1000

1000

" l yL 100.00

5.0000

250.00

250.00

100.00

1000.0

1000.0

in

no

109

100

109

117

100

70-130

70-130

70-130

70-130

70-130

70-130

70-130

MRL-2

MRL-2

MRL-2

MRL-2

MRL-2

MRL-2

MRL-2


Blank (1301093-BLKl) Prepared: 01/24/13 Analyzed: 02/13/13

EPA 200.8

Arsenic

Selenium

Cadmium

Antimony

Thallium

Lead

u u u u u u

1-0

2.0

0.50

1.0

1.0

I.O

ug/

' ' ' •

'

LCS(130I093-BSI) Prepared: 01/24/13 Analyzed; 02/13/13

EPA 200.8

Arsenic

Selenium

Cadmium

Antimony

Thallium

Lead

221.10

224.70

55.218

196.83

212.79

220.08

5.0

10

2.5

5.0

5.0

5.0

ug/L 200.00

200.00

50.000

200.00

200.00

200.00

111

112

110

98:4

106

no

85-115

85-115

85-115

85-115

85-115

85-115

Matrix Spike (I30I093-MSI) Source: El30307-02 Prepared: 01/24/13 Analyzed: 02/13/13

EPA 200.8

•Arsenic

Selenium

Cadmium

Antimony

Thallium

Lead

220.31

232.63

54.710

199.60

218.31

223.25

5.0

10

2.5

5.0

5.0

5.0

ug/L

" -" " "

200.00

200.00

50.000

200.00

200.00

200.00

U

U

U

0.016066

u

0.24975

no

116

109

99.8

109

III

70-130

70-130

70-130

70-130

70-130

• 70-130

of 18 E130310 TMTL FINAL 02 22 13 1349 2/22/13 13:49



980 College Station Road. Athens, Georgia 30605-2700

D.A.R.T Id: 13-0162




EPA 200.8

Arsenic

Selenium

Cadinium

.Antimony

Thalliuin

Lead

218.23

225.49

55.819

100.58

215.76

236.04

5.0

10

2 5

5 0

5.0

5.0

ug/L

"

"

"

"

200.00

200.00

50.000

200.00

200.00

200.00

1.9337

1.5894

0.058284

0.10713

U

11.526

108

112

112

50.2

108

112

70-130

70-130

70-130

70-130

70-130

70-130

.Analyte

Reporting

Result Limit Units

Spike Source %REC

Level Reside ».'oREC Limits RPD

RPD

Limit Notes

B a t c h 1301093 - M 200.2 M e t a l s W a t e r

M a t r i x Sp ike (130 l093-MS2) Source: El30310-02 Prepared: 01/24/13 Analyzed: 02/13/13

QM-I

Matrix Spike Dup (1301093-MSDI) Source: El30307-02 Prepared: 01/24/13 Analyzed; 02/13/13

EPA 200.8

Arsenic

Selenium

Cadmium

Antimony

Thallium

Lead

220.85

215.89

54.928

195.91

211.79

223.38

5.0

10

2.5

5.0

5.0

5.0

ug/L

"

-

"

"

"

200.00

200.00

50.000

200.00

200.00

200.00

U

U

U

0.016055

U

0.24975

no

108

no

98.4

106

112

70-

70-

70-

70-

70-

70-

30

30

130

30

30

30

0.244

7.00

0.398

1.36

3.03

0.0569

20

20

20

20

20

20

Matrix Spike Dup (1301093-MSD2) Source: El30310-02 Prepared: 01/24/13 Atialyzed: 02/13/13

EPA 200.8

Arsenic

Selenium

Cadinium

Antimony

Thallium

Lead

217.35

216.57

54.999

101.80

221.47

239.92

SO

10

2.5

5.0

5-P

5.0

ug/L

"

"

"

"

"

200.00

200.00

50.000

200.00

200.00

200.00

1.9337

1.5894

0.058284

0.I07I3

U

11.526

108

107

no

50.8

111

114

70-130

70-130

70-130

70-130

70-130

70-130

0.402

4.04

148

1.20

2.61

1.53

20

20

20

20

20

20

QM-1

MRL Verification (I30I093-PSI) Prepared: 01/24/13 Analyzed: 02/13/13

EPA 200.8

Arsenic

Selenium

Cadmium

Antimony

Thallium

1.1288

2.2018

0.55980

0.52760

0.64800

1.1454

I.O

2.0

0.50

1.0

I.O

LO

ug/L

"

"

LOOOO

2.0000

0.50000

0.50000

0.50000

I OOOO

113

no

114

106

130

115

65-135

65-135

65-135

65-135

55-135

65-135

MRL-2

MRL-2

MRL-2

MRL-2.

U

MRL-2.

U

MRL-2

of 18 El30310 TMTL FINAL 02 22 13 1349 2/22/13 13:49



Project 13-0162, Abertdeen Groundwater - Reported by Terri White

Notes and Definitions for Q C Samples

u MRL-2

QC-6

QL-2

( M-1

The analyte was not detected at or above the reporting limit.

MRL verillcation for Non-Potable Water matrix

Calibration check standard greater than mediod control limits.

Laboratory Control Spike Recovery greater than method control limits

Matrix Spike Recovery less than method control limits

of 18 El30310 TMTL FINAL 02 22 13 1349 2/22/13 13:49

MEMORANDUM FROM TERRI WHITE, USEPA TO JON … · Project: 13-0162, Aberdeen Groundwater - Reported...

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