Established pilot scale facility for production of RSW...

• Manufacturingtechnologyforcommercialproductionoffivecomponentborosilicateglassbeadsofvariouscompositions• Newtwintechnologyin40LcapacitypureplatinumcruciblethroughcompleteindigenouseffortformanufacturingofRSWglass

• EstablishedpilotscalefacilityforproductionofRSWglasshavingdensityof5.2g/cc

• Development of an alternate technology formanufacturing of high density larger sizeRSWglass slabs using specialtyrefractorycrucible

Borosilicateglassfrits RSWglasschunkofassortedsize RSWglassof700X700X35mm3

7-componentborosilicateglassbeads Radiationshieldingglassblock5-componentborosilicateglassbeads

• Inthenationalscenario,technologyformanufacturingRSWglassblocksin40LplatinumpothasbeendevelopedforthefirsttimebyCSIR-CGCRI

• Delivered20MTRSWglassblockstoBARC,DAE• Delivered72MTborosilicateglassbeadstoBARC,DAE• CSIR-CGCRIhassuccessfullytransferredthetechnologyofmanufacturingspecialglassbeadstoM/sH&RJOHNSON(INDIA),Mumbai forcommercialproduction tomeet theirannual requirement to the tuneof30-40MT.ThesuccesshasbroughtconsiderablerecognitionforCGCRIandCSIRasawholefor itscontributiontowardsnuclearprogrammeofthecountry

National Awards:• NRDCMeritoriousInnovationAward-2013:Technologyofmanufacturingspecialglassbeadsfornuclearwasteimmobilization• CertificateofMeritUnderCSIRTechnologyAwardforInnovation-2017:Technologyformanufacturingspecialglassbeadsfornuclearwasteimmobilization

• SKOCHORDEROFMERIT-2017:Forqualifyingamongsttop30transformationalinnovationprojectsinIndiaforglassbeadspreparationtechnologyforvitrificationofhighlevelradioactivewaste

• CSIRTechnologyAward-2018:Underthecategory“Innovation”forthenomination“Aninnovativetechnologyformanufacturingofspecialtymaterialforimmobilizationofhighlevelradioactivewaste”

SPeCiAlTy GlASS TeChNoloGy

60Lspecialtyrefractorypotandstirrer 60Lcapacitytiltcastingtechnology

• ManufacturingtechnologyonRadiationShieldingWindow(RSW)glassblock• Technologyforcommercialproductionofborosilicateglassbeadsfornuclearwasteimmobilization

notablE achiEvEmEnts

tEchnologiEs

currEnt r&D activitiEs

ExpErtisE

• Orthopaedic,dentalandmaxillofacialbiomedicalmaterials/implants

• Tissue engineered scaffolds or strutsanddrugdeliverysystems

• Reconstructiveandtraumamaterials• Nano-biomaterialsfordrugdeliveryandscaffoldapplications

• Functional biomaterials, bone and cartilagetissueengineering

• Coatings forbiomedical andhigh-temperatureapplications

• SiAlONanditscompositesformanufacturingofadvancedmachininginserts

High-temperatureprotectivecoatings TribotestingofSiAlONagainstdenseSiliconNitride SiAlONbasedhighspeedcuttingtoolinserts

PlasmasprayedhydroxyapatitecoatingsBioactiveceramicscaffolds

Ceramic-on-PEhipreplacementCaPgranulesOrbitalimplant

BioCeRAMiCS, CoATiNGS ANd CoMPoSiTeS

• Ceramicbasedtotalhipprosthesis(ceramic-on-PE)(TransferredtoM/sIFGLBioceramicsLtd.)• Plasmaspraygradehydroxyapatitegranules(TransferredtoM/sOrthotechLtd.)• Plasmasprayhydroxyapatitecoatingonmetallicbiomedicalimplants(TransferredtoM/sIFGLBioceramicsLtd.)• Manufactureofbioactiveceramicscaffolds/granulesandintegratedorbitalimplant(M/sGESCOLtd.,Chennai)• Injectable,biodegradablebonecementcompositewith/withoutdrugs• High-temperatureprotectivecoatings(TransferredtoM/sSwissGlassCoatsLtd.,M/sVaniFabEngineeringWorks,M/sStandardGlassLiningTechnologyPvt.Ltd.,M/sAdvancedExpertiseTechnologyPvt.Ltd.,M/sAnticorrosiveEquipmentPvt.Ltd.)

• SiAlONbasedhighspeedcuttinginserts(M/sDoubleDeeTechnology,Mumbai)• HighheatresistantenamelfritforapplicationinMIGseriesaero-engineparts(CG-B-55AandCB-ABK-13)(M/sHAL,Koraput)

ExpErtisE

tEchnologiEs


• Patientspecificimplantsusingadditivemanufacturing

• Surface engineering (plasma spray coating, anodization,etc.)ofmaterialsforloadbearingimplants

• Biostable, bioactive and osteoconductive/inductive polymer composites for spinalreconstructionandbonereplacements

• Biomaterialsfromseaoriginandbiogenicsource

• Wound dressing system for diabetic andnon-diabeticpatients

• Inorganic/ceramic based antacid for instant reliefandsustainedbufferingaction

• Metallization of ceramics, ceramic to ceramic/metal joining, microwave processing of materialsandthermalbarriercoatings

• Multi-ion doped CaP based powders/scaffolds/coatingsforboneregeneration

• SiAlONbasedhighspeedcuttingtoolinsertsformachiningofferrous,non-ferrousalloysandwoodcutting

• Rock drilling bits/cutting inserts based on SiAlON-WCcomposites

Bioactiveglassnanofibersforwoundhealing

ElectrospunnanofibersDopedHApcoatedintramedullarypins

HApcoatingonPEEK

Patientspecifichipstems Fishscalederivedhydroxyapatite

Ceramicbasedantacid

Sugar-glassNPs

TechnologyAwardfordevelopingmanufacturingtechnologyofbioceramicimplantsfromCSIR,India(2010)

Technologytransferof“Manufactureofplasmaspraygradehydroxyapatitegranules”toM/sOrthotech,GujaratinFebruary2018

BestTechnologyAwardforthedevelopmentoforbitalimplantprosthesisfromNationalResearchDevelopmentCorporation,Govt.ofIndia(2005)

Technologytransferof“Manufactureofbioactiveceramicscaffolds/granulesandintegratedorbitalimplant”toM/sGESCO,ChennaiinMay2015

Gamma sterilization

BioCeRAMiCS, CoATiNGS ANd CoMPoSiTeS

FacilitiEs


• MF,UF,hollowfibre,capillary,hydrophobicandgasseparationceramicmembranes• WatertreatmenttechnologiesforArsenic,Iron&Fluorideremoval,industrialanddomesticwastewater• Gasseparationmaterials/filmsforflue/syngasenrichment,hydrogen,CO2sequestration• Membranecontactor/photobioreactorforCO2sequestrationandwastewaterremediation• Edibleoilandsugarcanejuiceclarification

• CeramicmembranebasedtechnologyforAs&Feremovalfromgroundwater• High-capacityceramicmembranemodulesforremovalof(i)Fe&Ascontamination(ii)riverwaterturbidityandsuspendedparticulates

• Aluminahollowfibremembranefabricationtechnology

DemonstrationofAs&Feremovalplant Prototypefortextileeffluenttreatment(A)Contaminatedgroundwater(B)ceramicmembranetreatedwater

Ceramicmembraneofdifferentdimensions(A)capillary(B)hollowfiber(C)singlechannelsupport

(D)multichannel

Ceramichydrophobicmembrane(A)outersurface,(B)innersurface

Gasseparationmembrane

Ceramicmembranebasedclarificationofricebranoilatindustrypremises

MembranebasedlaboratorysetupforgasseparationPalladiumcoatedmembraneoverceramicsupport

Ceramicmembranebasedclarificationofsugarcanejuiceatindustrypremises(A-Initialfeed,B&C-Membranefiltrate)

EnrichmentoffluegasatVSP,VisakhapatnamLabscalemembranephotobioreactorforalgalbiomassproduction

• M/sEntechMetalsPvt.Ltd.,Kolkata• M/sVictorEngineeringCo.,Assam• M/sZeolite(India)Pvt.Ltd.,Kolkata

• M/sPorelDassWater&EffluentControlPvt.Ltd.,Howrah• M/sRollabssHiTechIndustries,Kolkata• M/sServoTechnologyLtd.,UttarPradesh

CeRAMiC MeMBRANe ANd WATeR TeChNoloGy

Technologies transferred to:

ExpErtisE

tEchnologiEs

CeRAMiC MeMBRANe ANd WATeR TeChNoloGy

• CeramicmembraneforgasseparationinS-I&Cu-Clcycleforcleanenergy• Ceramicmembranebasedprocessesforremediationofpharmaceuticalsandpersonalcareproducts• Ceramicmembraneprototypefortreatmentandrecyclingoftextileeffluents• CeramicmembranebasedMBRprocessfortannerywastewatertreatment• Palladium,Zeoliteandcompositemembraneforselectiveseparationofhydrogenfromgasmixture• Defluoridationandarsenicseparationfordrinkingwater• Ceramic–polymercompositemembranesforenvironmentalapplications• ProductionfacilityofInternationalstandardmultichannelporousceramictubularsupport

notablE achiEvEmEnts• 170ceramicmembranebasedwatertreatmentplantsinstalledforFeandAsremoval• IndustrialtrialforgasseparationwasconductedatM/sVisakhapatnamSteelPlant• IndustrialtrialforclarificationofricebranoilatM/sNavyugAgroIndustriesPvt.Ltd.,Burdwan• IndustrialtrialforclarificationofsugarcanejuiceatM/sSriSantTukaramSahakariSakharKarkhanaLtd.,Pune• RBGVSwaikaMemorialAward(Teamawardforappliedresearch)underOilTechnologists’AssociationofIndia(OTAI)MeritAward–2015fortheworkon‘Technologydevelopmentforrefiningofricebranoilmiscellausingceramicmicrofiltrationmembrane’

As&Feremovalplant(5000L/day)atDakshinJagaddal,South24Parganas,WB

Highcapacity(8m3/day)ceramicmembranebasedriverwaterpurificationplantinstalledatTaki,North24Parganas,WB

Ceramichollowfibremembraneextruder


Anode-supported planar SOFC single cell• Simpleandup-scalablefabricationprocesspatented• Standardsize:10cmx10cmx1.5(±0.05)mm;customsizesandshapesavailable

• Operatingtemperaturebetween750°Cand800°C

Thermally cyclable glass-based sealants for SOFC application• PatentedcompositionanddevelopedincollaborationwithGlassDivision

• Able tomake hermetic seal betweenmetal-metalandmetal-ceramicinterfaces

• Capable of withstanding large number of thermalcyclesbetweenroomtemperatureand800°C

Paper-based ceramic separator for Li-ion battery application• Simpleandup-scalablefabricationprocesspatented• Paperseparatorcanbemadeofanyshapeandisareplacementofcommercialpolymerseparator• Provideexcellentessentialseparatorpropertiessuchashighporosity,lowthermalshrinkage,highmechanicalstrength,lowinternalresistanceandexcellentwettabilitytoelectrolyte

• Electrochemicalperformancecomparabletothatofcommercialpolymerseparator

tEchnologiEs


• SolidOxideFuelCell(SOFC)• Li-ionbattery• DenseceramicmembraneforH2andO2separation• SolidOxideElectrolyserCell(SOEC)• Photocatalytic H2 generation and CO2capturingthroughhierarchicalporousnanostructures

Fuel Cell ANd BATTeRy

Low Temperature Solid Oxide Fuel Cell (LT-SOFC)• Developedlowtemperaturesolidoxidefuelcell(LT-SOFC)electrolytecomposition:10and20mol.%Gd-andSm-dopedCeria(CeO2)(GDCandSDC)

• SinteringtemperatureofnewlydevelopedGDCisaslowas1200°C• DevelopedtechniquetoproduceGDCorSDCinlargevolume(kg-level)• DevelopmentofnovelcathodeandanodecompositionsforLT-SOFCisinprogress

SOFCsinglecellsofdifferentdimensionsandmicrostructureofaSOFCsinglecell

CGCRIdeveloped20-cell1kWSOFCstackandtheperformanceoftheindividualcells

IllustrationofSOFCpowerthroughaCGCRIdeveloped500Wstack

Development and demonstration of kW level SOFC stack• Developed and successfully demonstratedseveral 1 kW working SOFC stacks using H2 andoxygen/air first time in the country and holding keypatentsinthisarea

• Current research is targeting to develop 2-3 kW ratingSOFC stacks to make prototype device, jointly withindustrialpartners

ExpErtisE

Up-scalability and further modification of paper-based ceramic separator• Asemi-automatedapparatushasbeendesignedanddevelopedtofabricatepaper-basedceramicseparatorinlargevolume(e.g.18650typeorpouchcell)intheformofrollsof50-100meterslengthofvariedwidthforLi-ionbatteries

Solid oxide electrolyser cell• InitiatedactivityonhydrogenproductionfromhightemperaturesteamusingSolidOxideElectrolyserCell(SOEC)withconventionaldoped lanthanummanganite-basedperovskite,newlydevelopedBa-Sr-Co-Fe-basedperovskiteandSr-Fe-Mn-baseddoubleperovskitesbasedairelectrodes

Indigenouslybuiltpaper-basedceramicseparatorequipmentandproducts

State-of-the-artSOFCstackteststationofratingupto1kW

Impedanceanalyzer

DesktopSEM

Tapecastingfacility

Automatedspraycoatingequipment

Screenprintingfacility


FacilitiEs

Fuel Cell ANd BATTeRy

tEchnologiEs/proDucts

• Specialtyopticalfiber• Fiberlaser• Fiberamplifier• FiberBragggrating• Photoniccrystalfiber

Parameters CATV WDMWavelength 1540-1560nm C–bandNo.ofchannels 1 16/32InputPower -3to+3dBm -20to-3dBmOutputPower 20to23dBm 18to20dBmNoisefigure <6dB <5dBGainflatness - <1dB

Optical amplifier for CATV and WDM applications Industrialpartner:SFOTechnologies,Cochin

Embeddablestrainsensorforconcretestructures

Weldablestrainsensor Embeddablestrainsensorwithtemperaturecompensation

Accelerometerandvibrationsensor

CW/QCW Thulium fiber laser prototype for lithotripsy, soft tissue vaporization and material processing

Operatingwavelength: 1.94µm

Max.outputpower: 30W

Powerstability: 1–2%

Modulation: 10Hz–1kHz

Coolingmode: Aircooling

All-fiber supercontinuum light source for confocal microscopy and optical coherence tomographyIndustrialpartner: VinvishTechnologiesPvt.Ltd., Thiruvananthapuram

Max.powerlevel: 2W

Wavelengthrange: 500–2200nm

Operatingtemperature: 15–45°C

Fiber Bragg grating (FBG) and Long Period Fiber Grating (LPFG) based sensing technology(a)AvailableFBGsensors:Strain,temperature,vibration,acceleration,pressure,acousticsignalanddisplacementsensorsfor

structuralhealthmonitoringandprocesscontrol

(b)AvailableLPFGsensors:HighlysensitiveLPFGrefractiveindexsensorsfordetectioninchemicalandbiologicalapplications

CW Ytterbium fiber laser prototype for stent cutting, welding and additive manufacturing

Pulsed Ytterbium fiber laser prototype for marking on metal surfaces, deep engraving, solar cell scribing and material processing

Operatingwavelength: 1.064/1.074µm

Max.outputpower: 100W

Beamquality(M2): <1.2

Coolingmode: Aircooling

Optical amplifier prototype for FTTH and free space communicationIndustrialpartner: VinvishTechnologiesPvt.Ltd., Thiruvananthapuram

Outputsignalpower: 40dBm

Inputsignallevel: 0to+10dBm

Noisefigure(at0dBminputsignal): ~6dB

Operatingwavelength: 1540–1565nm

FiBeR oPTiCS ANd PhoToNiCS

Operatingwavelength:1.064µm

Max.avg.outputpower:20W

Pulsewidth:80–200ns

Coolingmode:AircoolingPulserep.rate: 20–200kHz 40–150kHzMax.pulseenergy: 1.0mJ 0.5mJ

M2: <1.8 <1.3

ExpErtisE

FacilitiEs

• Fiber laser for medical applications: CW/modulatedThuliumfiberlaser(at1.94µm)isbeingdevelopedtoreplacecurrentHo:YAGtechnologyforlithotripsy

• Fiber lasers for industrial applications: (a)HighpowerCWYtterbium laser for stent cuttingandadditive manufacturing (b) High energy pulsedYtterbium laser for marking and engraving onmetalsurfaces

• FBG sensing system:(a)strainandforcesensorsforonlinehealthmonitoringofpantograph(b)real-timevibrationmonitoringofgeneratorsinpowerplants(c)temperaturemonitoringinthermalpowerplants(d)weightinmotionofrollingstocks

• FBGbasednarrowlinewidthlaserforHydrophone

• LPFG sensors:forselectiveanalytedetectioninchemicalandbiologicalapplications

• Photonic crystal fibers: (a) supercontinuum(SC)generationinvisibleandmid-IRregions(b)highpowerbeamdeliverybyhollowcorePCFsforbiophotonicandindustrialapplications

Kidneystone Fragmentedstone Softtissueablation

SmartpantographwithFBGsensors

VisiblepartofSClightdispersedbyanopticalwedge

HollowcorePCFforbeamdelivery

Carbonizationmarkingonstainlesssteel

Fineengravingonpolishedaluminium

FBGsensorsforvibrationmonitoringof

generators

FBGsensorsforweightinmotionofrollingstocks

Preformanalyzer FBGwritingfacility

Fiberanalyzer Lasingperformancetestset-up

PreformfabricationinhightemperatureMCVDsystem

Specialtyfibersplicingsystem

Attenuationmeasurementset-up

Fiberfabricationinthedrawingtower

• CSIR Technology Award –2012for‘Developmentofcompletelypackagedcommercial-gradeC-bandErbium-DopedFiberAmplifiers(EDFA)forCATVandtelecomnetworks’

• CSIR Technology Award for Innovation–2015for‘Developmentofcompletelypackagedall-fibersupercontinuumlightsource’• CW/QCWThuliumfiberlaserandPulsedYtterbiumfiberlasertechnologiestransferredtoM/sBharatElectronicsLtd.,Bangalore

• Multicomponent glass based fibers: (a)Rareearth doped glass-ceramic based fibers forbroadband lightsourcesforOCTapplication(b)photosensitivefiberforregeneratedFBGsensorsusableathightemperature


FiBeR oPTiCS ANd PhoToNiCS


tEchnologiEs


• Specialty glass/glass-ceramics for engineering,medical,spaceandstrategicapplications

• Moderate to pilot scale production of glasses onnationaldemand

• Energyefficientglassmeltingtechnology(microwave)

• Technologicalsolutionstoindustrythroughlaboratoryscaletrials

• Testing&calibrationofglazingproducts

Nd3+ doped phosphate laser glass for high energy and high power laser applications

Edge cladding glass for Nd-glass disc drives in high power laser systems

As–Se based chalcogenide glass production and window fabrication for thermal imaging

Laser quality Nd3+ doped phosphate glass (5 L scale production)

Thermally cyclable sealant glass for solid oxide fuel cell (SOFC)

Hermeticsealforbothmetal-metalandmetal-ceramicinterfacesThermalStability :Upto1000hCyclability(25°C-800°C-25°C) :20cycles

Bottompouringflowcastingfacility Nd3+dopedphosphateglass

Sealantsafter15cycles(>27days)

PerformanceofSOFCstack+glasssealant@15cycles

FinishedNd-glassrodsanddiscs

Highabsorbingedgecladdingglasses

• ProductionofNd3+dopedphosphateglassblocksindifferentdimensions (5Lcapacity) to fabricatelaserrodsanddiscs

• Setting up a national facility and technologydevelopmentfortheproductionoflargesizeddiscs(15Lcapacity)

TechnologydevelopmentofedgecladdingglassforlargesizeNd:glassdiscstoreduceparasiticoscillations:• Absorptioncoefficient~7.5cm-1

• Linearrefractiveindex,coefficientoflinearthermalexpansionandhardnessmatchingwithNd-laserglass

ProcessedAs2Se3glasswithtransmissionupto12µm

Density,ρ :2.78g.cm-3

RefractiveIndex,ne :1.53EmissionWavelength:1.053µmFluorescenceLifetime:>280µs

GlASS SCieNCe ANd TeChNoloGy

ExpErtisE

Density,ρ :4.61g.cm-3 RefractiveIndex,n1500 :2.83TransmissionWindow:0.8µm–12.5µm Transmission(8–12μm) :60%

Microwavemeltingofglass:Aprospectivegreenprocessingtechnology

ChalcogenideglassforIRoptics/thermalimagingapplications

Architectural Glass Research and Testing (AGRT) facility

• Significantenergyandtimesavingsinglassmelting• StabilisationofhigherFe[II]inglassandtherebypreparationofIRabsorbingglassinair• Lowvolatilisationlossofmaterialandlesscontaminationfromcruciblewall• LowOH-contentinglass

• Extended transmission in theMWIR (3 – 5 µm) andFWIR(8–12µm)bands

• Lowertemperaturecoefficientofrefractiveindex(dn/dt),wider transmissionwindow, higher usage temperaturethanGesinglecrystal

• Cost-effectiveandeasierfabricationforlensproduction• Suitable for fabrication of uncooled thermal imagingdevices

ThisisajointinitiativeofCSIR-CGCRIandGlazingSocietyofIndiafortestingofenergyperformance,materialcharacteristics,safetyaswellasstructuralperformanceofarchitecturalglass,glazingsystemandassociatedmaterials

Varioustypesofglassespreparedadoptingmicrowaveheating

IRtransmittingchalcogenideglassespreparedatCSIR-CGCRI

Imageformationusingdevelopedchalcogenideglass

Rockingfurnace(10000C,rock450inbothways,autoquenchingfacility)

5LInductionheatingglassmeltingfurnaceswithbottompouringfacility

6kW,2.45GHz,multimodemicrowaveheatingglassmeltingfurnace(16000C)

ZygoInterferometer,bulkhomogeneityupto10-6

UV-Vis-NIRspectrofluorimeter,λEMrange200-5000nm

EnergyperformancetestingofglazingsystemusingFTIRspectrometerandUV-Vis-NIRspectrophotometer

GlASS SCieNCe ANd TeChNoloGy


FacilitiEs

NANoSTRuCTuRed MATeRiAlS

• Nanocomposite, mesoporous and hydrophobic coatings on glass,polymersandmetals

• Antireflective(AR)coatingsonglassandplastics• Singlelayergraphenefilmsonglass/Sisubstrates

tEchnologiEs


Anti-scratch hybrid composite coatings on plastic ophthalmic lenses and sheets• Sol-derivedhybridprecursorswithroomtemperatureshelf-lifeof2-6months• Abilitytodeposithard-coatingsondifferentopticalqualityplastics• Surfacehardnessbetween5and6H(ASTMD3363)

Inorganic-organic hybrid antireflective (AR) coatings on plastic substrates

Tailorable refractive index coatings on plastic for scratch healing• Controllablethickness(1-4µm)andrefractiveindex(1.48-1.65)• WidesubstrateoptionincludingCR-39®,PC,acrylic,PPandrelatedplastics• High transparency, excellent abrasion resistivity, good hardness, and adhesion alongwiththermalandchemicalresistance

Antireflective (AR) cum hydrophobic coatings using ordered mesoporous silica on textured solar cover glass for enhanced conversion efficiency and easy maintenance• Thecoatingsareaimedtoaddressbio-fouling,dustandreflectionloss

• Performance evaluation of small-scale solar modules, withdevelopedAR-cum-hydrophobiccoverglass,isunderprogress

• Largeareacoatingprocessisbeingdeveloped• Thermalandchemicalresistance

Transparent, conducting coating of single layer graphene on glass substrates for application as bottom electrode

(a)Hard-coatedplasticophthalmiclensesand(b)polycarbonate(PC)sheet(600x600mm2)

Figure(A)and(B)showhowmatchingRIcoatingscanhealthescratchesaswellasgetting

advantageofmuchbettersurfacehardness

Solarcoverglass(600x600mm2)withARcumhydrophobic(SWCA=123±3o)coatingfittedon36nos.solarcells(single

cell)showinghydrophobiceffect

Superhydrophobic coating on glass substrate

Photographofwaterdropsonsuperhydrophobicfilmsdepositedfloatglass

ARcoatedCR-39®lensesshowingthereflectioncolourovertheentirevisiblerange

• ARcoatingswithtunablereflectionminimaortransmissionmaxima• Minimalreflectionof~1%atspecificwavelengths• Hydrophobicinnaturewith~5Hhardness(ASTMD3363)foreasycleaning

• Technology transferred to two Indian companies on anti-scratch coatings on plastic ophthalmic lensesandsheets


(a) (b)

ExpErtisE

ReFRACToRieS ANd TRAdiTioNAl CeRAMiCS

tEchnologiEs• Syntheticaggregatelikemullite,zirco-mullite,ullite-corundum,spinel• Lowandultralowcementcastables(45-90%Al2O3)• Ricehuskashnodulesforheatinsulation• Hydrationresistantsinteredlimeandlimerefractory• Magnesiaspinelrefractoryforcementrotarykiln

• Syntheticrefractoryaggregates• Carbon based refractories forsteelmakingand functionalapplications

• Cementandchemicallybondedmonolithicrefractories• Utilizationofsolidindustrialwaste(iron&steel,mining,powerplantetc.)

• ValueadditiontoIndianrefractoryrawmaterials• Testingofclay,refractoryrawmaterialsandproducts


• Basicrammingmassenablingsteelrefining in induction furnace ascurrentsilicarammingmassisnotsuitable

• High alumina aggregates frombauxite of Indian origin: IndianBauxite is not suitable for hightemperature application as itcontains detrimental impuritiesCaO, Fe2O3, SiO2andTiO2. Withstructural modification by CSIR-CGCRI, significant enhancementof high temperature propertiesachievedandvalidatedthrough30tonplanttrial

• Training on refractory processingand characterization, terracottaprocessing

• TechnicalsupporttoMSMEsectors

FacilitiEs

HightemperatureMOR Compressivecreepfacility Inductionmeltingfurnace Highcapacitypress

ExpErtisE

• Sol-gelthinfilms

• Mesoscalepatterningofthinfilms

• Functionalnanomaterials

• Zeolites,oxidepowdersandfibres

tEchnologiEs

• Anti-glarecoatingonophthalmiclensesandglasssheets• Antireflective coatings on ophthalmic and other circular glasslenses

• Highlypuresilicaglassdiscs,platesandrodsbysol-gelprocessing• Microwaveassistedlowemissivityindiumtinoxidesol-gelcoatingonsoda-lime-silicaglass

• Sol-gelbased indiumtinoxide foamwithmicrowaveabsorbingproperty

AntiglareCoater,Kanpur

Ghantiwala,Gujrat

AdvancedSurfaceTechnology,Gurgaon

LuciferEnterprise,Delhi

BharatElectronicsLimited,Taloja

Akemi-al,Kolkata


Technologies transferred to:

• Polyurethane based low density anticorrosive mouldablenanocompositeformakingshoeoutsolesusableinmarineenvironment

• Superhydrophobic biocompatible coating on cotton fabricwith antibacterial property for application in biomedicaldevices/garments

SodiumtitanatenanotubeforadsorptionofSr2+,theradioactiveion

Polyurethanenanocompositesheet Fabricwithsuperhydrophobiccoating

Sol-Gel SCieNCe ANd TeChNoloGy

• Highfidelity1D/2Dsurfacepatterned(periodicity:microtonanosizerange)metaloxideopticalthinfilmsforgratingcouplerplanarwaveguidesensor/improvingsolarlightharvestingefficiency

• Developmentofporousmaterialsfordecontaminationofwater

• Ricehuskbasedzeolitesfordefluoridationofwater

• Poroussodiumtitanatebasedmaterialsfortheremovalofradioactivewastes(Cs(I)&Sr(II)fromwaste)

ExpErtisE

tEchnologiEs


• Advanced functionalmaterials, nanomaterialsanddevices forenergy,environmentalandhealthcareapplications

• Ceramic based sensors for combustible andpollutantgases,relativehumidityandppmlevelmoisturedetection,diseasediagnostics

• Fabricationofpiezoceramicbasedactuatorsandnanogeneratorsforstrategicapplications

• Functionalmaterialsforsolarcellapplications

TracemoistureanalyzerHightemperaturehumiditysensor

LPG Pocketmodule

Powerconsumption 1Watt

MinimumdetectionlimitLEL-3500ppm

500ppm

Sensitivity[(Ra–Rg)/Ra] >85%

Sensor resistance (in air at 350oC)

15–50k.ohm

Responsetime 10sec

Operatingtemperature 350oC

• Dielectricconstant(ε)=2500at10kHz• Piezoelectriccoefficient(d33)=230pC/N• Electromechanical coupling factor (Kp)=0.49

• Saturationpolarization(Ps)=80µC/cm2

@200V• Blockingforce=800N• Displacement=1.9µm@40layers

SENSORS

ThinfilmcapacitivebasedlowppmmoisturesensorNano-Biosensorsforacetonedetectioninbreath(biomakerfordiabetes)

SensorsforpesticidedetectioninfruitsandvegetablesDevelopmentofceramicbasedsensorsforcombustibleandpollutantgases

SelfpoweredgassensorforLPGgasdetection

Renewable EnergyProcessTechnologyandNewmaterialsDyesensitizedsolarcellsNanogenerators

Support to Strategic SectorDevelopment of piezoelectric materialsfor sonar applications for DRDO,H2 sensor for BRNS, ISRO moisturesensorforIndianNavy

Advanced Functional Materials/Coatings for Sensors, Actuators,

energy and environmental Applications

ACTUATORS

PZTbasedwafersandmultilayersDevelopmentofPiezoelectricpolymerandpolymerceramiccomposites

Leadfreepiezoceramicwafersforstrainandpressuresensors

CSIR 800Water quality testing and monitoring invillagesofWestBengal

FocusedBasicResearchOxideionconductingmaterialsElectrodematerialsMultiferroicmaterialsPerovskitebasedphotovoltaicmaterialsNew materials for ppb level moisturedetection

Moisture sensors:• Low-to-highppm(1to1000ppm)moistureandhighrelativehumiditysensorsforstrategicandindustrialapplications

Tea aroma sensors: • Morethan30differenttypesofMOSSensorswithoptimizedsensingpropertiesfordetectingVOCsinteaaroma Gas sensors:

• Solar powered LPG leak alarmand sensors for volatile organicsandairpollutinggases

Piezoceramic wafers and multilayer actuators

SeNSoR ANd ACTuAToR

ExpErtisE

training & DEmonstration on tErracotta WarEs

proDuct DEvElopmEnt

The centre provides R & D towards standardization,evaluation and optimized utilization of ceramic rawmaterials for ceramic wares. Expertise in the areas ofenergyconservation,pollutioncontrol,wasteminimization,whiteware, cluster development, quality improvement,productivity/processimprovementandcostreductionfor

localindustries

HighaluminaheatsinkforLEDbulbs

Oilandgasfiredchamberkilnforruralindustry

CeramicproductsdevelopedusingflyashfromNTPC Glazedartware Tilesandbricksfromgranitedust

CrockerymadefromwastecalciumhydroxideLowcostruralsanitaryware

Major Activities• Development of importsubstitute products andencourage ‘Make in India’program

• Utilization of wastes likeGranitedust,Flyash,Calciumhydroxide & Marble dust inceramicproducts

• Development of newprocesses like Pad Printingetc. to improve design ofpotteryproducts

• MonitoringthedeteriorationofairqualityinKhurjaindustrialsector towards pollutioncontrol

• Improvingenergyefficiencyoftunnel&shuttlekilnsthroughcannibalisation

• Establishingcommon facilitycentre in Khurja potterycluster, Bareilly terracottacluster & Rohtash potterycluster

• Checking efficiency of thekilns in newly established‘Energy ManagementCell’

• Skills developments in thefield of Pottery and Glassbeadsforruralmass

Padprintingandartisticstonewareporcelainplatters

ouTReACh CeNTRe AT khuRJA uTTAR PRAdeSh

ISO 9001:2015 certified R&D center thatundertake R&D projects to solvetechnicalproblemsof local industriesandprovide testing & certification services toindustries. Actively conduct technicaltrainingandskilldevelopmentprograms.

Low-temperaturematuredbonechina(Patented)

Lowenergyintensivekilnfurniture EcofriendlyterracottabottlesandjewelleryReplacementofUkraineclayinvitrifiedceramictilebody

MORapparatus

Surfaceabrasion Autoclave Colourmeasurement

Deepabrasion TG/DTA ParticlesizeanalyzerImpacttester

Slipperinessmeter Moistureexpansiontester Dilatometer

ICPforchemicalanalysis

Major Activities• Quality testing and certification oftraditional ceramic products andalliedmaterials

• ReplacementofUkraineclayinbodycomposition for polished vitrifiedceramictileproduction

• Integrated pottery developmentproject (IPDP) forsocio-economicupliftmentofruralpotters

• Technology for manufacture ofceramic insulator body and glaze,utilizinglocallyavailablerawmaterial

• Bone china tableware: utilizationof di calcium phosphate (DCP) inbone china tableware application,standardizationofbonechinabodyinmanufacturing

• Lowtemperaturematuredstonewarecrockery

• Refractories: china clay derivedmullitegrog,lowenergyintensivekilnfurniture,manufacturingtechnologyforcordieritemullitebats

• Wasteutilization:ceramictilesfromvitrifiedtilepolishingsludge,recyclingof crockery and sanitaryware firedscrap

• Surface active nano coatings fortraditionalceramicproducts

• Skill development trainingon different aspects ofmanufacturingoftraditionalceramicproductsandalliedrawmaterials

training program For rural artisans

tEsting & cErtiFication oF cEramic proDucts anD alliED matErials

proDuct DEvElopmEnt

ouTReACh CeNTRe AT NARodA GuJARAT


FacilitiEs

• Major support towards structural andmicrostructural characterization ofmaterialsfortheInstitute

• Macro, Micro and Nano-mechanicalcharacterization

• Magnetic characterization ofmultiferroicmaterials

• Dynamic fracturemechanics and highstrainratebehaviorofmaterials

• Evaluation of nano mechanical properties of bulk and coatingmaterials

• Developmentandunderstandingofmultiferroicmaterialsandtheirpropertiesinbulk,thinfilm,nanoscalesystemsfornewgenerationspintronicdeviceapplications

• Highstrainratedeformationbehaviorofceramicsandcomposites(polymerandmetalmatrix)

• Development of laboratory based Pair DistributionFunction (PDF) analysis technique in a conventionalXRD using Ag radiation for study of short rangestructureindisordered/nanomaterials.

• Developmentofnovelmaterials forapplications in conservationandrestorationofheritagebuildings

UniversalTestingMachine(UTM)

X-rayfluorescence(XRF)analyzer 300kVHigh-ResolutionTransmissionElectronMicroscope(HRTEM)

X-RayPhoto-electronSpectroscope(XPS) InductivelyCoupledPlasmaMassSpectrometer(ICP-MS)

HighresolutionXRD SplitHopkinsonpressurebarapparatus Magneticforcemicroscope

Vickershardnesstester Scratchtester Hysitronnanoindenter

FieldEmissionScanningElectronMicroscope(FESEM)

Thephase-contrastimagesofmagneticdomainsunder±20kOemagneticfieldinaclusterofnanoparticlesofBiFeO3

AdVANCed MeChANiCAl ANd MATeRiAlS ChARACTeRizATioN

ExpErtisE

Established pilot scale facility for production of RSW...

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