Data Experiment Combine

176
Pond Name : Pond 1 Sample Characterizaton Total Solid Container Mass a) 4.765 b) 4.7552 Container + Sampl a) 14.1777 b) 15.4862 Mass Sample a) 9.4127 b) 10.731 1 2 3 Mass After Drying a) 6.8328 6.8329 6.7941 b) 7.1512 7.1483 7.1504 1 2 3 Average Total Solid a) 2.0678 2.0679 2.0291 2.054933 b) 2.396 2.3931 2.3952 2.394767 Average % Solid a) 0.218315 21.83% 22.07% b) 0.223163 22.32% Average pH a) 7.35 7.255 b) 7.16 Average Temp a) 14.7 14 b) 13.3 Density Densitymeter Calibration Volume 100 ml Container Mass 44.8 gr Container Mass + Water 144.05 gr Water Mass 99.25 gr Density 0.9925 gr/ml Density Analysis Volume 100 ml

description

As

Transcript of Data Experiment Combine

Page 1: Data Experiment Combine

Pond Name : Pond 1

Sample Characterizaton

Total SolidContainer Mass a) 4.765

b) 4.7552

Container + Sample a) 14.1777b) 15.4862

Mass Sample a) 9.4127b) 10.731

1 2 3Mass After Drying a) 6.8328 6.8329 6.7941

b) 7.1512 7.1483 7.1504

1 2 3 AverageTotal Solid a) 2.0678 2.0679 2.0291 2.054933

b) 2.396 2.3931 2.3952 2.394767

Average% Solid a) 0.218315 21.83% 22.07%

b) 0.223163 22.32%

AveragepH a) 7.35 7.255

b) 7.16

AverageTemp a) 14.7 14

b) 13.3

DensityDensitymeter Calibration

Volume 100 mlContainer Mass 44.8 gr

Container Mass + Water 144.05 grWater Mass 99.25 gr

Density 0.9925 gr/ml

Density AnalysisVolume 100 ml

Page 2: Data Experiment Combine

Container Mass 44.8 grContainer Mass + Sample a) 160.36

b) 160.47

Sample Mass a) 115.56b) 115.67

Density a) 1.1556b) 1.1567

Average 1.15615

Rheometer Test

Sample PreparationBefore Sentrifuge

Container Mass a) 36.92b) 35.14

Container + Sample a) 537.47b) 514.109

Sample Mass a) 500.55b) 478.969

After SentrifugeSolid Container Mass a) 36.47

b) 36.93

Container + Solid Sample a) 316.28b) 307.73

Solid Mass a) 279.81b) 270.8

Water Container Mass a) 36.47b) 36.93

Container + Water Sample a) 257.26b) 243.31

Water Mass a) 220.79b) 206.38

Total Solid - Solid Sample

Page 3: Data Experiment Combine

Container Mass a) 4.7641b) 4.7694

Mass Container + Sample a) 12.42b) 14.01

Mass Sample a) 7.6559b) 9.2406

1 2 3Mass After Drying a) 7.7667 7.7664 7.7618

b) 8.0066 8.0084 8.0024

1 2 3 AverageTotal Solid a) 3.0026 3.0023 2.9977 3.000867

b) 3.2372 3.239 3.233 3.2364

Average% Solid a) 0.391968 39.20% 37.11%

b) 0.350237 35.02%

DensitySolid Phase

Container Mass 44.8Container Volume 100 ml

Mass Container + Sample a) 152.51b) 153.61

Sample Mass a) 107.71b) 108.81

Density a) 1.0771b) 1.0881

Average 1.0826

Liquid PhaseContainer Mass 14.41

Container Volume 5.486

Mass Container + Liquid a) 19.91b) 19.94

Sample Liquid a) 5.5b) 5.53

Page 4: Data Experiment Combine

Density a) 1.002552b) 1.00802

Average 1.005286

Rheometer CompositionMass Container 35.54

Mass Container + Sample A 185.23Mass Sample A 149.69 0.495925 49.59%

Mass Container + Sample A + B 337.38Mass Sample B 152.15 0.504075 50.41%

Volatile Solids

AContainer Weight 31.1593Container Weight + Sample 54.8445Sample 23.6852

After rehydration oven 36.7006Sample 5.5413

After Muffle Furnace 35.6853Sample 4.526

% Total Solid 23.40%% Fixed Solids 81.68%% Volatile Solids 18.32%

BContainer Weight 60.615Container Weight + Sample 144.7938Sample 84.1788

After rehydration oven 80.9976Sample 20.3826

After Muffle Furnace 77.6213Sample 17.0063

% Total Solid 24.21%% Fixed Solids 83.44%% Volatile Solids 16.56%

Page 5: Data Experiment Combine

Average% Total Solid 23.80%% Fixed Solids 82.56%% Volatile Solids 17.44%

Page 6: Data Experiment Combine

ζ - Target ζ - Actual (Pa)Solid Content mass (gr)

Container Sample

990

990.7

969.53333 0 0

A 4.7408 11.3104 6.5696991.6

926.3 B 4.6597 13.873 9.2133

600

594.4

609.9 10 10

A 4.6771 12.9577 8.2806617

618.3 B 4.7276 13.3713 8.6437

400

445.6

462.93333 7 17

A 4.7598 14.0989 9.3391472.6

470.6 B 4.7147 13.5401 8.8254

100

118.5

122.96667 40 57

A 4.6629 14.28 9.6171112.1

138.3 B 4.7439 12.5351 7.7912

70

71.69

71.02 20 77

A 4.6504 13.261 8.610662.61

78.76 B 4.6714 12.9175 8.2461

40

44.43

44.316667 20 97

A 4.737 17.4141 12.677144.09

44.43 B 4.753 16.3615 11.6085

20

24.23

26.596667 20 117

A 4.7487 15.0872 10.338528.3

27.26 B 4.6513 13.4297 8.7784

10

17.5

17.366667 20 137

A 4.7178 18.7889 14.071117.8

16.8 B 4.7429 17.5126 12.7697

5

5.722

6.339 40 177

A 4.719 20.4469 15.72797.068

6.227 B 4.7393 20.004 15.2647

Tap Water volume (µl)

N x 1000Accumulati

ve (ml) Sample + Container

Page 7: Data Experiment Combine

Solid Content mass (gr)

Final Mass Average Solid Content %TS Average

7.4136 7.4165 7.4178 7.4160 2.6752 40.72% 40.84%

8.4304 8.4357 8.4338 8.4333 3.7736 40.96%

7.8242 7.8294 7.99 7.8812 3.2041 38.69% 37.93%

7.9999 7.9945 7.8254 7.9399 3.2123 37.16%

8.1738 8.178 8.1731 8.1750 3.4152 36.57% 36.73%

7.973 7.9718 7.9687 7.9712 3.2565 36.90%

7.7282 7.7342 7.7276 7.7300 3.0671 31.89% 31.75%

7.2045 7.2074 7.2069 7.2063 2.4624 31.60%

7.2079 7.2099 7.2106 7.2095 2.5591 29.72% 29.62%

7.1039 7.1093 7.1049 7.1060 2.4346 29.52%

8.239 8.2422 8.2402 8.2405 3.5035 27.64% 27.79%

7.9948 7.9992 7.9959 7.9966 3.2436 27.94%

7.3774 7.3774 7.374 7.3763 2.6276 25.42% 24.13%

6.6574 6.6582 6.6568 6.6575 2.0062 22.85%

8.0418 8.0392 8.0368 8.0393 3.3215 23.60% 23.81%

7.8114 7.8072 7.8077 7.8088 3.0659 24.01%

7.8724 7.8742 7.8721 7.8729 3.1539 20.05% 20.21%

7.8382 7.8359 7.8721 7.8487 3.1094 20.37%

15% 20% 25% 30% 35% 40% 45%0

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Page 8: Data Experiment Combine

15% 20% 25% 30% 35% 40% 45%0

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Page 9: Data Experiment Combine

Pond Name : Pond 2

Sample Characterizaton

Total SolidContainer Mass a) 4.6822

b) 4.7

Container + Sample a) 15.9342b) 14.2029

Mass Sample a) 11.252b) 9.5029

1 2 3Mass After Drying a) 5.8293 5.835 5.8321

b) 5.687 5.6903 5.6887

1 2 3 AverageTotal Solid a) 1.1471 1.1528 1.1499 1.149933

b) 0.987 0.9903 0.9887 0.988667

Average% Solid a) 0.102198 10.22% 10.31%

b) 0.104038 10.40%

AveragepH a) 6.98 6.97

b) 6.96

AverageTemp a) 7.8 9.2

b) 10.6

DensityDensitymeter Calibration

Volume 100 mlContainer Mass 44.84 gr

Container Mass + Water 144.09 grWater Mass 99.25 gr

Density 0.9925 gr/ml

Density AnalysisVolume 100 ml

Page 10: Data Experiment Combine

Container Mass 44.84 grContainer Mass + Sample a) 148.5

b) 148.74

Sample Mass a) 103.66b) 103.9

Density a) 1.0366b) 1.039

Average 1.0378

Rheometer Test

Sample PreparationBefore Sentrifuge

Container Mass a)b)

Container + Sample a) 576.37b) 571.41

Sample Mass a)b)

After SentrifugeSolid Container Mass a)

b)

Container + Solid Sample a) 437.22b) 439.76 1

Solid Mass a)b)

Water Container Mass a)b)

Container + Water Sample a) 170.08b) 164.94

Water Mass a)b)

Total Solid - Solid Sample

Page 11: Data Experiment Combine

Container Mass a) 4.75b) 4.78

Mass Container + Sample a) 11.84b) 12

Mass Sample a) 7.09b) 7.22

1 2 3Mass After Drying a) 5.3417 5.3425 5.3409

b) 5.3621 5.3648 5.3638

1 2 3 AverageTotal Solid a) 0.5917 0.5925 0.5909 0.5917

b) 0.5821 0.5848 0.5838 0.583567

Average% Solid a) 0.083456 8.35% 8.21%

b) 0.080826 8.08%

DensitySolid Phase

Container Mass 44.84Container Volume 100 ml

Mass Container + Sample a) 147.09b) 147.02

Sample Mass a) 102.25b) 102.18

Density a) 1.0225b) 1.0218

Average 1.02215

Liquid PhaseContainer Mass 14.4206

Container Volume 5.486

Mass Container + Liquid a) 19.9359b) 19.9474

Sample Liquid a) 5.5153b) 5.5268

Page 12: Data Experiment Combine

Density a) 1.005341b) 1.007437

Average 1.006389

Rheometer CompositionMass Container 36.46559

Mass Container + Sample A 207.1302Mass Sample A 170.6646 0.589567 58.96%

Mass Container + Sample A + B 325.94Mass Sample B 118.8098 0.410433 41.04%

Volatile Solids

AContainer Weight 23.314Container Weight + Sample 46.8784Sample 23.5644

After rehydration oven 25.9101Sample 2.5961

After Muffle Furnace 24.7068Sample 1.3928

% Total Solid 11.02%% Fixed Solids 53.65%% Volatile Solids 46.35%

BContainer Weight 23.504Container Weight + Sample 47.5688Sample 24.0648

After rehydration oven 26.1881Sample 2.6841

After Muffle Furnace 24.9142Sample 1.4102

% Total Solid 11.15%% Fixed Solids 52.54%% Volatile Solids 47.46%

Average

Page 13: Data Experiment Combine

% Total Solid 11.09%% Fixed Solids 53.09%% Volatile Solids 46.91%

Page 14: Data Experiment Combine

Retest4.643

4.8222

13.917215.9606

9.274211.1384

1 2 35.5835 5.5853 5.5836.0162 6.0174 6.0148

1 2 3 Average0.9405 0.9423 0.94 0.940933

1.194 1.1952 1.1926 1.193933

Average0.101457 10.15% 10.43%0.107191 10.72%

Page 15: Data Experiment Combine

ζ - Target ζ - Actual (Pa)Solid Content mass (gr)

Container Sample

250

281.1

257.93333 0 0

A 4.6507 10.584 5.9333240.3

252.4 B 4.7099 14.0945 9.3846

220

226

216.93333 2 2

A 4.65 12.1361 7.4861215.1

209.7 B 4.6213 10.0825 5.4612

190

192.4

193.93333 2 4

A 4.7214 9.3058 4.5844197.2

192.2 B 4.6255 12.2904 7.6649

180

177.4

178.96667 2 6

A 4.7184 11.3203 6.6019180.1

179.4 B 4.7097 11.5828 6.8731

160

164.3

165.6 2 8

A 4.7371 12.3149 7.5778160.2

172.3 B 4.6974 11.4573 6.7599

130

133.3

135.86667 6 14

A 4.7022 9.097 4.3948138

136.3 B 4.6197 9.7112 5.0915

100

103.7

104.66667 8 22

A 4.6948 9.4459 4.7511106

104.3 B 4.7243 9.4436 4.7193

70

75.73

77.526667 14 36

A 4.6285 12.3536 7.725180.78

76.07 B 4.7133 11.5574 6.8441

40

42.75

45.553333 21 57

A 4.7132 13.7535 9.040347.46

46.45 B 4.7215 15.5063 10.7848

10

10.1

10.603333 40 97

A 4.6183 17.7296 13.111310.94

10.77 B 4.6187 13.3564 8.7377

Tap Water volume (µl)

N x 1000Accumulati

ve (ml) Sample + Container

Page 16: Data Experiment Combine

Solid Content mass (gr)

Final Mass Average Solid Content %TS Average

5.2598 5.2601 5.2592 5.2597 0.6090 10.26% 9.98%

5.6196 5.622 5.6181 5.6199 0.9100 9.70%

5.3504 5.3509 5.3509 5.3507 0.7007 9.36% 9.60%

5.1572 5.1596 5.1589 5.1586 0.5373 9.84%

5.157 5.1594 5.1584 5.1583 0.4369 9.53% 9.49%

5.349 5.35 5.3506 5.3499 0.7244 9.45%

5.3336 5.3325 5.3333 5.3331 0.6147 9.31% 9.22%

5.3373 5.3381 5.3376 5.3377 0.6280 9.14%

5.4227 5.4235 5.4257 5.4240 0.6869 9.06% 9.18%

5.3242 5.325 5.3264 5.3252 0.6278 9.29%

5.0876 5.0877 5.0881 5.0878 0.3856 8.77% 8.77%

5.0662 5.0667 5.0661 5.0663 0.4466 8.77%

5.0981 5.0993 5.0999 5.0991 0.4043 8.51% 8.49%

5.1227 5.1243 5.1242 5.1237 0.3994 8.46%

5.2314 5.233 5.2314 5.2319 0.6034 7.81% 7.82%

5.2484 5.2516 5.2484 5.2495 0.5362 7.83%

5.3687 5.3687 5.3688 5.3687 0.6555 7.25% 7.24%

5.5016 5.5016 5.5032 5.5021 0.7806 7.24%

5.2689 5.2689 5.2707 5.2695 0.6512 4.97% 4.98%

5.0548 5.0548 5.0564 5.0553 0.4366 5.00%

4% 5% 6% 7% 8% 9% 10% 11%0

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Page 17: Data Experiment Combine

4% 5% 6% 7% 8% 9% 10% 11%0

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Page 18: Data Experiment Combine

Pond Name : Pond 3

Sample Characterizaton

Total SolidContainer Mass a) 4.79

b) 4.85

Container + Sample a) 12.29b) 10.54

Mass Sample a) 7.5b) 5.69

1 2 3Mass After Drying a) 5.1023 5.1032 5.1066

b) 5.0799 5.0805 5.0826

1 2 3 AverageTotal Solid a) 0.3123 0.3132 0.3166 0.314033

b) 0.2299 0.2305 0.2326 0.231

Average% Solid a) 0.041871 4.19% 4.12%

b) 0.040598 4.06%

AveragepH a) 6.72 6.745

b) 6.77

AverageTemp a) 9.4 10.1

b) 10.8

DensityDensitymeter Calibration

Volume 100 mlContainer Mass 44.8 gr

Container Mass + Water 142.7 grWater Mass 97.9 gr

Density 0.979 gr/ml

Density AnalysisVolume 100 ml

Page 19: Data Experiment Combine

Container Mass 44.8 grContainer Mass + Sample a) 146.7

b) 146.43

Sample Mass a) 101.9b) 101.63

Density a) 1.019b) 1.0163

Average 1.01765

Rheometer Test

Sample PreparationBefore Sentrifuge

Container Mass a) 36.32 c) 35.67b) 34.84 d) 34.52

Container + Sample a) 537.58 c) 363.04b) 534.97 d) 350.7

Sample Mass a) 501.26 c) 327.37b) 500.13 d) 316.18

After SentrifugeSolid Container Mass a) 36.32 c) 35.67

b) 34.84 d) 34.52

Container + Solid Sample a) 147.43 c) 114b) 150.84 d) 109.51

Solid Mass a) 111.11 c) 78.33b) 116 d) 74.99

Water Container Mass a) 37.68 c) 35.6b) 37.15 d) 36.11

Container + Water Sample a) 419.54 c) 284.47b) 418.5 d) 277.12

Water Mass a) 381.86 c) 248.87b) 381.35 d) 241.01

Total Solid - Solid Sample

Page 20: Data Experiment Combine

Container Mass a) 4.83b) 4.79

Mass Container + Sample a) 8.59b) 10.18

Mass Sample a) 3.76b) 5.39

1 2 3Mass After Drying a) 5.5251 5.5274 5.531

b) 6.0233 6.0273 6.0301

1 2 3 AverageTotal Solid a) 0.6951 0.6974 0.701 0.697833

b) 1.2333 1.2373 1.2401 1.2369

Average% Solid a) 0.185594 18.56% 20.75%

b) 0.229481 22.95%

DensitySolid Phase

Container Mass 44.8Container Volume 100 ml

Mass Container + Sample a) 151.62b) 149.97

Sample Mass a) 106.82b) 105.17

Density a) 1.0682b) 1.0517

Average 1.05995

Liquid PhaseContainer Mass 14.39

Container Volume 5.486

Mass Container + Liquid a) 19.93b) 19.3

Sample Liquid a) 5.54b) 4.91

Page 21: Data Experiment Combine

Density a) 1.009843b) 0.895005

Average 0.952424

Rheometer CompositionMass Container 34.98

Mass Container + Sample A 139.7Mass Sample A 104.72 0.363119 36.31%

Mass Container + Sample A + B 240.5Mass Sample B 100.8 0.349527 34.95%

Mass Container + Sample C 281.58Mass Sample C 41.08 0.142446 14.24%

Mass Container + Sample D 323.37Mass Sample D 41.79 0.144908 14.49%

Volatile Solids

AContainer Weight 33.5693Container Weight + Sample 62.6762Sample 29.1069

After rehydration oven 34.4828Sample 0.9135

After Muffle Furnace 34.4036Sample 0.8343

% Total Solid 3.14%% Fixed Solids 91.33%% Volatile Solids 8.67%

BContainer Weight 24.9239Container Weight + Sample 43.4183Sample 18.4944

After rehydration oven 25.9285Sample 1.0046

After Muffle Furnace 25.4809Sample 0.557

% Total Solid 5.43%

Page 22: Data Experiment Combine

% Fixed Solids 55.44%% Volatile Solids 44.56%

Average% Total Solid 4.29%% Fixed Solids 73.39%% Volatile Solids 26.61%

Page 23: Data Experiment Combine

ζ - Target ζ - Actual (Pa)Solid Content mass (gr)

Container Sample

550

553.4

560.13333 0 0

A 4.765 11.223 6.458577.3

549.7 B 4.8329 9.9756 5.1427

400

369.6

377.56667 10 10

A 4.6347 10.2532 5.6185408.3

354.8 B 4.794 10.8143 6.0203

300

320.4

317.16667 5 15

A 4.7285 10.5409 5.8124318.1

313 B 4.7013 10.2877 5.5864

200

244.4

254.6 10 25

A 4.8117 9.7636 4.9519257.2

262.2 B 4.8726 10.2797 5.4071

100

124.2

114.09667 40 65

A 4.8715 13.9987 9.1272118.8

99.29 B 4.7189 13.2771 8.5582

80

89.53

78.793333 20 85

A 4.8079 16.7846 11.976767.75

79.1 B 4.7884 15.4801 10.6917

40

42.75

44.77 20 105

A 4.8025 19.7777 14.975242.75

48.81 B 4.7457 17.5144 12.7687

20

28.27

32.2 20 125

A 4.8121 23.33 18.517928.95

39.38 B 4.6909 19.1819 14.491

10

13.13

18.213333 30 155

A 4.7006 22.7994 18.098821.21

20.3 B 4.7993 24.9348 20.1355

5

9.088

9.646 30 185

A 4.8324 19.1598 14.32749.42

10.43 B 4.7378 17.7233 12.9855

Tap Water volume (µl)

N x 1000Accumulati

ve (ml) Sample + Container

Page 24: Data Experiment Combine

Solid Content mass (gr)

Final Mass Average Solid Content %TS Average

6.2486 6.2521 6.2596 6.2534 1.4884 23.05% 23.20%

6.0302 6.0339 6.0385 6.0342 1.2013 23.36%

5.8718 5.875 5.8778 5.8749 1.2402 22.07% 22.25%

6.1418 6.1436 6.1476 6.1443 1.3503 22.43%

6.016 6.0212 6.027 6.0214 1.2929 22.24% 22.32%

5.9487 5.9524 5.9553 5.9521 1.2508 22.39%

5.9006 5.9073 5.9091 5.9057 1.0940 22.09% 22.15%

6.0687 6.0744 6.0781 6.0737 1.2011 22.21%

6.4833 6.4887 6.4927 6.4882 1.6167 17.71% 17.66%

6.2209 6.2257 6.2319 6.2262 1.5073 17.61%

6.7991 6.8038 6.8102 6.8044 1.9965 16.67% 16.81%

6.5979 6.5966 6.6044 6.5996 1.8112 16.94%

7.1099 7.1132 7.1212 7.1148 2.3123 15.44% 15.34%

6.68866 6.6908 6.697 6.6922 1.9465 15.24%

7.5163 7.5217 7.5273 7.5218 2.7097 14.63% 14.23%

6.6904 6.6947 6.6973 6.6941 2.0032 13.82%

7.0788 7.0823 7.0823 7.0811 2.3805 13.15% 13.17%

7.4501 7.4532 7.4623 7.4552 2.6559 13.19%

6.4998 6.498 6.5034 6.5004 1.6680 11.64% 11.59%

6.2328 6.2346 6.2375 6.2350 1.4972 11.53%

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Page 25: Data Experiment Combine

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Page 26: Data Experiment Combine

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

990

990.7

969.5333 0 0

A 4.7408 11.3104 6.5696 7.4136991.6

926.3 B 4.6597 13.873 9.2133 8.4304

600

594.4

609.9 10 10

A 4.6771 12.9577 8.2806 7.8242617

618.3 B 4.7276 13.3713 8.6437 7.9999

400

445.6

462.9333 7 17

A 4.7598 14.0989 9.3391 8.1738472.6

470.6 B 4.7147 13.5401 8.8254 7.973

100

118.5

122.9667 40 57

A 4.6629 14.28 9.6171 7.7282112.1

138.3 B 4.7439 12.5351 7.7912 7.2045

70

71.69

71.02 20 77

A 4.6504 13.261 8.6106 7.207962.61

78.76 B 4.6714 12.9175 8.2461 7.1039

40

44.43

44.31667 20 97

A 4.737 17.4141 12.6771 8.23944.09

44.43 B 4.753 16.3615 11.6085 7.9948

20

24.23

26.59667 20 117

A 4.7487 15.0872 10.3385 7.377428.3

27.26 B 4.6513 13.4297 8.7784 6.6574

10

17.5

17.36667 20 137

A 4.7178 18.7889 14.0711 8.041817.8

16.8 B 4.7429 17.5126 12.7697 7.8114

5

5.722

6.339 40 177

A 4.719 20.4469 15.7279 7.87247.068

6.227 B 4.7393 20.004 15.2647 7.8382

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

250

281.1

257.9333 0 0

A 4.6507 10.584 5.9333 5.2598240.3

252.4 B 4.7099 14.0945 9.3846 5.6196

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Page 27: Data Experiment Combine

250

252.4 257.9333 0 0 B 4.7099 14.0945 9.3846 5.6196

220

226

216.9333 2 2

A 4.65 12.1361 7.4861 5.3504215.1

209.7 B 4.6213 10.0825 5.4612 5.1572

190

192.4

193.9333 2 4

A 4.7214 9.3058 4.5844 5.157197.2

192.2 B 4.6255 12.2904 7.6649 5.349

180

177.4

178.9667 2 6

A 4.7184 11.3203 6.6019 5.3336180.1

179.4 B 4.7097 11.5828 6.8731 5.3373

160

164.3

165.6 2 8

A 4.7371 12.3149 7.5778 5.4227160.2

172.3 B 4.6974 11.4573 6.7599 5.3242

130

133.3

135.8667 6 14

A 4.7022 9.097 4.3948 5.0876138

136.3 B 4.6197 9.7112 5.0915 5.0662

100

103.7

104.6667 8 22

A 4.6948 9.4459 4.7511 5.0981106

104.3 B 4.7243 9.4436 4.7193 5.1227

70

75.73

77.52667 14 36

A 4.6285 12.3536 7.7251 5.231480.78

76.07 B 4.7133 11.5574 6.8441 5.2484

40

42.75

45.55333 21 57

A 4.7132 13.7535 9.0403 5.368747.46

46.45 B 4.7215 15.5063 10.7848 5.5016

10

10.1

10.60333 40 97

A 4.6183 17.7296 13.1113 5.268910.94

10.77 B 4.6187 13.3564 8.7377 5.0548

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

550

553.4

560.1333 0 0

A 4.765 11.223 6.458 6.2486577.3

549.7 B 4.8329 9.9756 5.1427 6.0302

400

369.6

377.5667 10 10

A 4.6347 10.2532 5.6185 5.8718408.3

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Page 28: Data Experiment Combine

400

354.8 377.5667 10 10 B 4.794 10.8143 6.0203 6.1418

300

320.4

317.1667 5 15

A 4.7285 10.5409 5.8124 6.016318.1

313 B 4.7013 10.2877 5.5864 5.9487

200

244.4

254.6 10 25

A 4.8117 9.7636 4.9519 5.9006257.2

262.2 B 4.8726 10.2797 5.4071 6.0687

100

124.2

114.0967 40 65

A 4.8715 13.9987 9.1272 6.4833118.8

99.29 B 4.7189 13.2771 8.5582 6.2209

80

89.53

78.79333 20 85

A 4.8079 16.7846 11.9767 6.799167.75

79.1 B 4.7884 15.4801 10.6917 6.5979

40

42.75

44.77 20 105

A 4.8025 19.7777 14.9752 7.109942.75

48.81 B 4.7457 17.5144 12.7687 6.68866

20

28.27

32.2 20 125

A 4.8121 23.33 18.5179 7.516328.95

39.38 B 4.6909 19.1819 14.491 6.6904

10

13.13

18.21333 30 155

A 4.7006 22.7994 18.0988 7.078821.21

20.3 B 4.7993 24.9348 20.1355 7.4501

5

9.088

9.646 30 185

A 4.8324 19.1598 14.3274 6.49989.42

10.43 B 4.7378 17.7233 12.9855 6.2328

Page 29: Data Experiment Combine

Solid Content mass (gr)

Final Mass Average %TS Average

7.4165 7.4178 7.4160 2.6752 40.72% 40.84%

8.4357 8.4338 8.4333 3.7736 40.96%

7.8294 7.99 7.8812 3.2041 38.69% 37.93%

7.9945 7.8254 7.9399 3.2123 37.16%

8.178 8.1731 8.1750 3.4152 36.57% 36.73%

7.9718 7.9687 7.9712 3.2565 36.90%

7.7342 7.7276 7.7300 3.0671 31.89% 31.75%

7.2074 7.2069 7.2063 2.4624 31.60%

7.2099 7.2106 7.2095 2.5591 29.72% 29.62%

7.1093 7.1049 7.1060 2.4346 29.52%

8.2422 8.2402 8.2405 3.5035 27.64% 27.79%

7.9992 7.9959 7.9966 3.2436 27.94%

7.3774 7.374 7.3763 2.6276 25.42% 24.13%

6.6582 6.6568 6.6575 2.0062 22.85%

8.0392 8.0368 8.0393 3.3215 23.60% 23.81%

7.8072 7.8077 7.8088 3.0659 24.01%

7.8742 7.8721 7.8729 3.1539 20.05% 20.21%

7.8359 7.8721 7.8487 3.1094 20.37%

Solid Content mass (gr)

Final Mass Average %TS Average

5.2601 5.2592 5.2597 0.6090 10.26% 9.98%

5.622 5.6181 5.6199 0.9100 9.70%

Solid Content

Solid Content

0% 5% 10% 15% 20% 25% 30% 35% 40% 45%0

100

200

300

400

500

600

700

800

900

1000

Pond-1Pond-2Pond-3

% Total Solid

Yiel

d St

ress

(Pa)

Page 30: Data Experiment Combine

5.622 5.6181 5.6199 0.9100 9.70%

9.98%

5.3509 5.3509 5.3507 0.7007 9.36% 9.60%

5.1596 5.1589 5.1586 0.5373 9.84%

5.1594 5.1584 5.1583 0.4369 9.53% 9.49%

5.35 5.3506 5.3499 0.7244 9.45%

5.3325 5.3333 5.3331 0.6147 9.31% 9.22%

5.3381 5.3376 5.3377 0.6280 9.14%

5.4235 5.4257 5.4240 0.6869 9.06% 9.18%

5.325 5.3264 5.3252 0.6278 9.29%

5.0877 5.0881 5.0878 0.3856 8.77% 8.77%

Volatile SolidsPond 1

5.0667 5.0661 5.0663 0.4466 8.77%AContainer Weight

5.0993 5.0999 5.0991 0.4043 8.51% 8.49%

Container Weight + SampleSample

5.1243 5.1242 5.1237 0.3994 8.46% After rehydration oven

5.233 5.2314 5.2319 0.6034 7.81% 7.82%

Sample

5.2516 5.2484 5.2495 0.5362 7.83%After Muffle FurnaceSample

5.3687 5.3688 5.3687 0.6555 7.25% 7.24% % Total Solid

5.5016 5.5032 5.5021 0.7806 7.24%% Fixed Solids% Volatile Solids

5.2689 5.2707 5.2695 0.6512 4.97% 4.98% B

5.0548 5.0564 5.0553 0.4366 5.00%Container WeightContainer Weight + SampleSample

Solid Content mass (gr)

Final Mass Average %TS Average After rehydration oven

6.2521 6.2596 6.2534 1.4884 23.05% 23.20%

Sample

6.0339 6.0385 6.0342 1.2013 23.36%After Muffle FurnaceSample

5.875 5.8778 5.8749 1.2402 22.07% 22.25% % Total Solid

Solid Content

0% 5% 10% 15% 20% 25% 30% 35% 40% 45%0

100

200

300

400

500

600

700

800

900

1000

Pond-1Pond-2Pond-3

% Total Solid

Yiel

d St

ress

(Pa)

Page 31: Data Experiment Combine

6.1436 6.1476 6.1443 1.3503 22.43%

22.25%% Fixed Solids% Volatile Solids

6.0212 6.027 6.0214 1.2929 22.24% 22.32%

5.9524 5.9553 5.9521 1.2508 22.39%Average% Total Solid

5.9073 5.9091 5.9057 1.0940 22.09% 22.15%

% Fixed Solids% Volatile Solids

6.0744 6.0781 6.0737 1.2011 22.21%

6.4887 6.4927 6.4882 1.6167 17.71% 17.66%

6.2257 6.2319 6.2262 1.5073 17.61%

6.8038 6.8102 6.8044 1.9965 16.67% 16.81%

6.5966 6.6044 6.5996 1.8112 16.94%

7.1132 7.1212 7.1148 2.3123 15.44% 15.34%

6.6908 6.697 6.6922 1.9465 15.24%

7.5217 7.5273 7.5218 2.7097 14.63% 14.23%

6.6947 6.6973 6.6941 2.0032 13.82%

7.0823 7.0823 7.0811 2.3805 13.15% 13.17%

7.4532 7.4623 7.4552 2.6559 13.19%

6.498 6.5034 6.5004 1.6680 11.64% 11.59%

6.2346 6.2375 6.2350 1.4972 11.53%

Page 32: Data Experiment Combine

0% 5% 10% 15% 20% 25% 30% 35% 40% 45%0

100

200

300

400

500

600

700

800

900

1000

Pond-1Pond-2Pond-3

% Total Solid

Yiel

d St

ress

(Pa)

Page 33: Data Experiment Combine

Volatile Solids Volatile Solids Volatile SolidsPond 2 Pond 3A A

Container Weight 31.1593 Container Weight 23.314 Container WeightContainer Weight + Sample 54.8445 Container Weight + Sample 46.8784 Container Weight + Sample

23.6852 Sample 23.5644 Sample

After rehydration oven 36.7006 After rehydration oven 25.9101 After rehydration oven5.5413 Sample 2.5961 Sample

After Muffle Furnace 35.6853 After Muffle Furnace 24.7068 After Muffle Furnace4.526 Sample 1.3928 Sample

% Total Solid 23.40% % Total Solid 11.02% % Total Solid% Fixed Solids 81.68% % Fixed Solids 53.65% % Fixed Solids% Volatile Solids 18.32% % Volatile Solids 46.35% % Volatile Solids

B BContainer Weight 60.615 Container Weight 23.504 Container WeightContainer Weight + Sample 144.7938 Container Weight + Sample 47.5688 Container Weight + Sample

84.1788 Sample 24.0648 Sample

After rehydration oven 80.9976 After rehydration oven 26.1881 After rehydration oven20.3826 Sample 2.6841 Sample

After Muffle Furnace 77.6213 After Muffle Furnace 24.9142 After Muffle Furnace17.0063 Sample 1.4102 Sample

% Total Solid 24.21% % Total Solid 11.15% % Total Solid

0% 5% 10% 15% 20% 25% 30% 35% 40% 45%0

100

200

300

400

500

600

700

800

900

1000

Pond-1Pond-2Pond-3

% Total Solid

Yiel

d St

ress

(Pa)

Page 34: Data Experiment Combine

% Fixed Solids 83.44% % Fixed Solids 52.54% % Fixed Solids% Volatile Solids 16.56% % Volatile Solids 47.46% % Volatile Solids

Average Average% Total Solid 23.80% % Total Solid 11.09% % Total Solid% Fixed Solids 82.56% % Fixed Solids 53.09% % Fixed Solids% Volatile Solids 17.44% % Volatile Solids 46.91% % Volatile Solids

Page 35: Data Experiment Combine

0% 5% 10% 15% 20% 25% 30% 35% 40% 45%0

100

200

300

400

500

600

700

800

900

1000

Pond-1Pond-2Pond-3

% Total Solid

Yiel

d St

ress

(Pa)

Page 36: Data Experiment Combine

Volatile Solids

Container Weight 33.5693Container Weight + Sample 62.6762

29.1069

After rehydration oven 34.48280.9135

After Muffle Furnace 34.40360.8343

% Total Solid 3.14%% Fixed Solids 91.33%% Volatile Solids 8.67%

Container Weight 24.9239Container Weight + Sample 43.4183

18.4944

After rehydration oven 25.92851.0046

After Muffle Furnace 25.48090.557

% Total Solid 5.43%

0% 5% 10% 15% 20% 25% 30% 35% 40% 45%0

100

200

300

400

500

600

700

800

900

1000

Pond-1Pond-2Pond-3

% Total Solid

Yiel

d St

ress

(Pa)

Page 37: Data Experiment Combine

% Fixed Solids 55.44%% Volatile Solids 44.56%

% Total Solid 4.29%% Fixed Solids 73.39%% Volatile Solids 26.61%

Page 38: Data Experiment Combine

Pond Name : Pond 1 New

Sample Characterizaton

Total SolidContainer Mass a) 4.7731

b) 4.7914

Container + Sample a) 28.0453b) 30.1805

Mass Sample a) 23.2722b) 25.3891

1 2 3Mass After Drying a) 5.2584 5.2547 5.2584

b) 5.3054 5.3061 5.3054

1 2 3 AverageTotal Solid a) 0.4853 0.4816 0.4853 0.484067

b) 0.514 0.5147 0.514 0.514233

Average% Solid a) 0.0208 2.08% 2.05%

b) 0.020254 2.03%

AveragepH a) 6.76 6.88

b) 7

AverageTemp a) 14.2 13.8

b) 13.4

DensityDensitymeter Calibration

Volume 100 mlContainer Mass 44.89 gr

Container Mass + Water 144.05 grWater Mass 99.16 gr

Density 0.9916 gr/ml

Density AnalysisVolume 100 ml

Page 39: Data Experiment Combine

Container Mass 44.89 grContainer Mass + Sample a) 144.88

b) 144.85

Sample Mass a) 99.99b) 99.96

Density a) 0.9999b) 0.9996

Average 0.99975

Rheometer Test

Sample PreparationBefore Sentrifuge

Container Mass a) 37.71 37.44b) 37.46 37

Container + Sample a) 555.25 534.77b) 544.19 545.46

Sample Mass a) 517.54 497.33b) 506.73 508.46

After SentrifugeSolid Container Mass a)

b)

Container + Solid Sample a) 128.11b) 117.97

Solid Mass a) 128.11b) 117.97

Water Container Mass a) 35.38b) 36.95

Container + Water Sample a) 438.18b) 437.24

Water Mass a) 402.8b) 400.29

Total Solid - Solid Sample

Page 40: Data Experiment Combine

Container Mass a) 4.79b) 4.8

Mass Container + Sample a) 13.12b) 10.53

Mass Sample a) 8.33b) 5.73

1 2 3Mass After Drying a) 5.6283 5.6349 5.6313

b) 5.3032 5.3543 5.3522

1 2 3 AverageTotal Solid a) 0.8383 0.8449 0.8413 0.8415

b) 0.5032 0.5543 0.5522 0.536567

Average% Solid a) 0.10102 10.10% 9.73%

b) 0.093642 9.36%

DensitySolid Phase

Container Mass 44.92Container Volume 100 ml

Mass Container + Sample a) 146.4b) 145.83

Sample Mass a) 101.48b) 100.91

Density a) 1.0148b) 1.0091

Average 1.01195

Liquid PhaseContainer Mass 14.43

Container Volume 5.486 cm3

Mass Container + Liquid a) 19.9b) 19.89

Sample Liquid a) 5.47b) 5.46

Page 41: Data Experiment Combine

Density a) 0.997083b) 0.995261

Average 0.996172

Volatile Solids

A

Container Weight 33.2324Container Weight + Sample 57.3359Sample 24.1035

After rehydration oven 33.64Sample 0.4076

After Muffle Furnace 33.4085Sample 0.1761

% Total Solid 1.69%% Fixed Solids 43.20%% Volatile Solids 56.80%

BContainer Weight 26.9075Container Weight + Sample 39.1131Sample 12.2056

After rehydration oven 27.1201Sample 0.2126

After Muffle Furnace 26.9424Sample 0.0349

% Total Solid 1.74%% Fixed Solids 16.42%% Volatile Solids 83.58%

Average% Total Solid 1.72%% Fixed Solids 29.81%% Volatile Solids 70.19%

Page 42: Data Experiment Combine

ζ - Target ζ - Actual (Pa)Solid Content mass (gr)

Container Sample

300

296.2

257.73333 0 0

A 4.8787 17.9012 13.0225227.9

249.1 B 4.9497 18.2758 13.3261

200

190.8

179.13333 10 10

A 4.9792 13.6884 8.7092159.5

187.1 B 4.8118 13.5392 8.7274

160

152.5

145.76667 5 15

A 4.6408 12.1739 7.5331147.8

137 B 4.5935 12.2631 7.6696

130

132.3

125.56667 5 20

A 4.609 11.0054 6.3964129.6

114.8 B 4.6456 10.7015 6.0559

100

108.7

96.933333 10 30

A 4.7226 9.8928 5.170289.2

92.9 B 4.6339 9.3408 4.7069

60

58.9

58.79 20 50

A 4.6257 10.9627 6.33757.22

60.25 B 4.6023 10.5867 5.9844

40

50.15

44.99 20 70

A 4.5855 11.0952 6.509739.72

45.1 B 4.6266 12.1244 7.4978

20

23.9

23.786667 25 95

A 4.6167 11.1674 6.550723.9

23.56 B 4.5835 13.1569 8.5734

10

15.48

27.39 20 115

A 4.6785 16.8571 12.178646.83

19.86 B 4.5988 16.0969 11.4981

1

0.6732

0.7852667 40 155

A 4.7169 27.0967 22.37980.3366

1.346 B 4.6415 22.1018 17.4603

0 (Start)

0

0 0 155

A 4.7731 28.0453 23.27220

0 B 4.7914 30.1805 25.3891

Tap Water volume (µl)

N x 1000Accumulati

ve (ml) Sample + Container

Page 43: Data Experiment Combine

Solid Content mass (gr)

Final Mass Average Solid Content %TS Average

6.2216 6.2233 6.2194 6.2214 1.3427 10.31% 10.18%

6.2883 6.2909 6.2861 6.2884 1.3387 10.05%

5.8314 5.8322 5.8293 5.8310 0.8518 9.78% 9.91%

5.6849 5.6891 5.6875 5.6872 0.8754 10.03%

5.3709 6.2896 5.371 5.6772 1.0364 13.76% 11.71%

5.3349 5.337 5.3336 5.3352 0.7417 9.67%

5.2217 5.2226 5.2185 5.2209 0.6119 9.57% 9.55%

5.222 5.2243 5.2224 5.2229 0.5773 9.53%

5.2043 5.202 5.2033 5.2032 0.4806 9.30% 9.28%

5.0704 5.0699 5.0691 5.0698 0.4359 9.26%

5.142 5.1412 5.1394 5.1409 0.5152 8.13% 8.07%

5.082 5.0834 5.0805 5.0820 0.4797 8.02%

5.0729 5.0743 5.0724 5.0732 0.4877 7.49% 7.43%

5.1784 5.1808 5.1782 5.1791 0.5525 7.37%

5.032 5.032 5.031 5.0317 0.4150 6.33% 6.47%

5.149 5.1502 5.1482 5.1491 0.5656 6.60%

5.4654 5.4681 5.4643 5.4659 0.7874 6.47% 6.24%

5.2901 5.2935 5.2898 5.2911 0.6923 6.02%

5.5897 5.5947 5.5903 5.5916 0.8747 3.91% 3.91%

5.3216 5.3249 5.3224 5.3230 0.6815 3.90%

5.2584 5.6349 5.6313 5.5082 0.7351 3.16% 2.65%

5.3054 5.3543 5.3522 5.3373 0.5459 2.15%

2% 4% 6% 8% 10% 12% 14%0

50

100

150

200

250

300

Pond-1 New

% Total Solid

Yiel

d St

ress

(Pa)

Page 44: Data Experiment Combine

2% 4% 6% 8% 10% 12% 14%0

50

100

150

200

250

300

Pond-1 New

% Total Solid

Yiel

d St

ress

(Pa)

Page 45: Data Experiment Combine

Pond Name : Pond 2

Sample Characterizaton

Total SolidContainer Mass a) 4.68

b) 4.79

Container + Sample a) 31.43b) 33.63

Mass Sample a) 26.75b) 28.84

1 2 3Mass After Drying a) 5.5963 5.5998 5.5935

b) 5.7893 5.7963 5.7922

1 2 3 AverageTotal Solid a) 0.9163 0.9198 0.9135 0.916533

b) 0.9993 1.0063 1.0022 1.0026

Average% Solid a) 0.034263 3.43% 3.45%

b) 0.034764 3.48%

AveragepH a) 7.06 7.035

b) 7.01

AverageTemp a) 20.3 19.85

b) 19.4

DensityDensitymeter Calibration

Volume 100 mlContainer Mass 44.84 gr

Container Mass + Water 144.09 grWater Mass 99.25 gr

Density 0.9925 gr/ml

Density AnalysisVolume 100 ml

Page 46: Data Experiment Combine

Container Mass grContainer Mass + Sample a) 21.88

b) 21.87

Sample Mass a) 121.84b) 122.56

Density a) 1.2184b) 1.2256

Average 1.222

Rheometer Test

Sample PreparationBefore Sentrifuge

Container Mass a) 35.5 c) 36.59b) 36.38 d) 35.59

Container + Sample a) 556.72 c) 552.23b) 557.24 d) 569.74

Sample Mass a) 521.22 c) 515.64b) 520.86 d) 534.15

After SentrifugeSolid Container Mass a) 35.5 c) 36.59

b) 36.38 d) 35.59

Container + Solid Sample a) 186.119 c) 174.43b) 188.7 d) 204.23

Solid Mass a) 150.619 c) 137.84b) 152.32 d) 168.64

Water Container Mass a) 37.32b) 36.34

Container + Water Sample a) 369.44b) 379.24

Water Mass a) 332.12b) 342.9

Total Solid - Solid Sample

Page 47: Data Experiment Combine

Container Mass a) 4.64b) 4.62

Mass Container + Sample a) 24.15b) 20.31

Mass Sample a) 19.51b) 15.69

1 2 3Mass After Drying a) 5.9165 5.4207 5.9159

b) 5.7492 5.7552 5.7516

1 2 3 AverageTotal Solid a) 1.2765 0.7807 1.2759 1.111033

b) 1.1292 1.1352 1.1316 1.132

Average% Solid a) 0.056947 5.69% 6.45%

b) 0.072148 7.21%

DensitySolid Phase

Container Mass 21.69Container Volume 100 ml

Mass Container + Sample a) 116.92b) 112.69

Sample Mass a) 95.23b) 91

Density a) 0.9523b) 0.91

Average 0.93115

Liquid PhaseContainer Mass 9.37

Container Volume 5.486 cm3

Mass Container + Liquid a) 14.52b) 14.79

Sample Liquid a) 5.15b) 5.42

Page 48: Data Experiment Combine

Density a) 0.938753b) 0.987969

Average 0.963361

Volatile Solids

A

Container Weight 27.4124Container Weight + Sample 41.215Sample 13.8026

After rehydration oven 27.9429Sample 0.5305

After Muffle Furnace 27.6112Sample 0.1988

% Total Solid 3.84%% Fixed Solids 37.47%% Volatile Solids 62.53%

BContainer Weight 26.8891Container Weight + Sample 48.2387Sample 21.3496

After rehydration oven 27.6684Sample 0.7793

After Muffle Furnace 27.2112Sample 0.3221

% Total Solid 3.65%% Fixed Solids 41.33%% Volatile Solids 58.67%

Average% Total Solid 3.75%% Fixed Solids 39.40%% Volatile Solids 60.60%

Page 49: Data Experiment Combine

ζ - Target ζ - Actual (Pa)Solid Content mass (gr)

Container Sample

300

313.4

266.6 0 0

A 5.16 10.088 4.928243.4

243 B 4.92 10.0942 5.1742

200

207.7

180.2 10 10

A 4.8 9.8714 5.0714188.2

144.7 B 4.65 10.7632 6.1132

160

178.4

173.66667 5 15

A 4.83 10.5257 5.6957169.6

173 B 4.93 9.3324 4.4024

130

131.3

133.96667 10 25

A 4.83 11.2595 6.4295135.3

135.3 B 4.71 11.0782 6.3682

60

56.04

64.68 30 55

A 4.87 14.3141 9.444168.33

69.67 B 4.79 10.9539 6.1639

50

45.44

48.02 20 75

A 4.92 12.5404 7.620448.47

50.15 B 4.76 10.2355 5.4755

40

39.72

40.95 10 85

A 4.94 12.4842 7.544242.07

41.06 B 4.88 14.0271 9.1471

20

26.93

26.593333 20 105

A 4.85 13.7472 8.897224.91

27.94 B 4.87 15.2008 10.3308

10

11.78

14.81 25 130

A 4.92 16.2122 11.292216.49

16.16 B 4.75 14.9031 10.1531

5

6.059

6.6196667 40 170

A 4.9 12.8326 7.93266.732

7.068 B 4.56 14.6663 10.1063

0

1.683

1.683 0 170

A 4.68 31.43 26.752.02

1.346 B 4.79 33.63 28.84

Tap Water volume (µl)

N x 1000Accumulati

ve (ml) Sample + Container

Page 50: Data Experiment Combine

Solid Content mass (gr)

Final Mass Average Solid Content %TS Average

5.8651 5.868 5.8587 5.8639 0.7039 14.28% 14.52%

5.6844 5.6872 5.6788 5.6835 0.7635 14.76%

5.4861 5.4865 5.4826 5.4851 0.6851 13.51% 13.41%

5.4622 5.4669 5.4606 5.4632 0.8132 13.30%

5.5665 5.5697 5.5612 5.5658 0.7358 12.92% 13.15%

5.5201 5.5203 5.5168 5.5191 0.5891 13.38%

5.5775 5.5782 5.5724 5.5760 0.7460 11.60% 11.80%

5.4748 5.4787 5.4702 5.4746 0.7646 12.01%

5.8146 5.8164 5.8086 5.8132 0.9432 9.99% 9.57%

5.3583 5.3549 5.3485 5.3539 0.5639 9.15%

5.5799 5.5793 5.5736 5.5776 0.6576 8.63% 8.59%

5.2295 5.2312 5.2254 5.2287 0.4687 8.56%

5.5922 5.5931 5.5867 5.5907 0.6507 8.62% 8.53%

5.6529 5.6554 5.6461 5.6515 0.7715 8.43%

5.5965 5.5983 5.5916 5.5955 0.7455 8.38% 8.32%

5.7264 5.7255 5.7172 5.7230 0.8530 8.26%

5.6497 5.6447 5.6423 5.6456 0.7256 6.43% 7.06%

5.5325 5.5342 5.5274 5.5314 0.7814 7.70%

5.4064 5.407 5.4015 5.4050 0.5050 6.37% 6.40%

5.2107 5.211 5.2062 5.2093 0.6493 6.42%

5.5963 5.5998 5.5935 5.5965 0.9165 3.43% 3.45%

5.7893 5.7963 5.7922 5.7926 1.0026 3.48%

2% 4% 6% 8% 10% 12% 14% 16%0

50

100

150

200

250

300

Pond-2 New

% Total Solid

Yiel

d St

ress

(Pa)

Page 51: Data Experiment Combine

2% 4% 6% 8% 10% 12% 14% 16%0

50

100

150

200

250

300

Pond-2 New

% Total Solid

Yiel

d St

ress

(Pa)

Page 52: Data Experiment Combine

Pond Name : Pond 3

Sample Characterizaton

Total SolidContainer Mass a) 4.75

b) 4.7

Container + Sample a) 26.3b) 28.19

Mass Sample a) 21.55b) 23.49

1 2 3Mass After Drying a) 5.5836 5.5948 5.5849

b) 5.544 5.5827 5.5724

1 2 3 AverageTotal Solid a) 0.8336 0.8448 0.8349 0.837767

b) 0.844 0.8827 0.8724 0.866367

Average% Solid a) 0.038875 3.89% 3.79%

b) 0.036882 3.69%

AveragepH a) 6.91 6.9

b) 6.89

AverageTemp a) 14.6 14.6

b) 14.6

DensityDensitymeter Calibration

Volume 100 mlContainer Mass 44.8 gr

Container Mass + Water 142.7 grWater Mass 97.9 gr

Density 0.979 gr/ml

Density AnalysisVolume 100 ml

Page 53: Data Experiment Combine

Container Mass 44.8 grContainer Mass + Sample a) 146.15

b) 146.1

Sample Mass a) 101.35b) 101.3

Density a) 1.0135b) 1.013

Average 1.01325

Rheometer Test

Sample PreparationBefore Sentrifuge

Container Mass a) 47.16 c) 36.82b) 48.96 d) 35.72

Container + Sample a) 482.21 c) 494.16b) 524.8 d) 489.44

Sample Mass a) 435.05 c) 457.34b) 475.84 d) 453.72

After SentrifugeSolid Container Mass a) 47.16 c) 36.82

b) 48.96 d) 35.72

Container + Solid Sample a) 122.99 c) 125.24b) 133.71 d) 135.5

Solid Mass a) 75.83 c) 88.42b) 84.75 d) 99.78

Water Container Mass a) 37.22 c) 36.29b) 36.34 d) 36.56

Container + Water Sample a) 395.29 c) 404.97b) 418.7 d) 388.69

Water Mass a) 358.07 c) 368.68b) 382.36 d) 352.13

Total Solid - Solid Sample

Page 54: Data Experiment Combine

Container Mass a) 4.63b) 4.65

Mass Container + Sample a) 17.959b) 16.799

Mass Sample a) 13.329b) 12.149

1 2 3Mass After Drying a) 6.9905 6.9964 6.9906

b) 7.1744 7.1829 7.1638

1 2 3 AverageTotal Solid a) 2.3605 2.3664 2.3606 2.3625

b) 2.5244 2.5329 2.5138 2.5237

Average% Solid a) 0.177245 17.72% 19.25%

b) 0.207729 20.77%

DensitySolid Phase

Container Mass 44.8Container Volume 100 ml

Mass Container + Sample a) 129.189b) 133.37

Sample Mass a) 84.389b) 88.57

Density a) 0.84389b) 0.8857

Average 0.864795

Liquid PhaseContainer Mass 9.37

Container Volume 5.486

Mass Container + Liquid a) 14.91b) 14.67

Sample Liquid a) 5.54b) 5.3

Page 55: Data Experiment Combine

Density a) 1.009843b) 0.966096

Average 0.987969

Volatile Solids

A

Container Weight 26.3899Container Weight + Sample 49.0279Sample 22.638

After rehydration oven 27.3231Sample 0.9332

After Muffle Furnace 26.9156Sample 0.5257

% Total Solid 4.12%% Fixed Solids 56.33%% Volatile Solids 43.67%

BContainer Weight 23.7445Container Weight + Sample 45.0337Sample 21.2892

After rehydration oven 24.6215Sample 0.877

After Muffle Furnace 24.2417Sample 0.4972

% Total Solid 4.12%% Fixed Solids 56.69%% Volatile Solids 43.31%

Average% Total Solid 4.12%% Fixed Solids 56.51%% Volatile Solids 43.49%

Page 56: Data Experiment Combine

ζ - Target ζ - Actual (Pa)Solid Content mass (gr)

Container Sample

500

573.9

646.26667 0 0

A 4.59 9.7558 5.1658744.2

620.7 B 4.98 10.5743 5.5943

300

351.4

324.7 10 10

A 4.76 7.8879 3.1279302.3

320.4 B 5.02 9.2464 4.2264

250

262.2

259.96667 10 20

A 4.96 8.4536 3.4936245.1

272.6 B 4.9 8.087 3.187

200

215.9

191.9 10 30

A 4.61 9.2211 4.6111180.1

179.7 B 4.61 7.974 3.364

160

154.5

142.83333 15 45

A 4.73 10.0448 5.3148145.1

128.9 B 4.62 9.8033 5.1833

100

84.15

96.936667 20 65

A 5 10.7515 5.7515110.4

96.26 B 4.95 10.2018 5.2518

40

44.09

46.223333 30 95

A 4.64 11.5035 6.863547.12

47.46 B 4.61 10.098 5.488

20

35.34

20.643333 40 135

A 4.61 10.1769 5.566912.79

13.8 B 4.98 9.965 4.985

10

8.475

11.015 40 175

A 4.73 13.6636 8.933611.44

13.13 B 4.7 17.6295 12.9295

5

6.732

6.0586667 60 235

A 5.01 14.624 9.6145.385

6.059 B 4.71 16.8617 12.1517

0

3.366

2.3573333 0 235

A 4.75 26.3 21.551.35

2.356 B 4.7 28.19 23.49

Tap Water volume (µl)

N x 1000Accumulati

ve (ml) Sample + Container

Page 57: Data Experiment Combine

Solid Content mass (gr)

Final Mass Average Solid Content %TS Average

5.9484 5.9477 5.93217 5.9428 1.3528 26.19% 26.17%

6.4507 6.4461 6.4313 6.4427 1.4627 26.15%

5.575 5.6074 5.603 5.5951 0.8351 26.70% 25.62%

6.0635 6.0603 6.0487 6.0575 1.0375 24.55%

5.8917 5.8841 5.8785 5.8848 0.9248 26.47% 26.19%

5.7255 5.7255 5.7255 5.7255 0.8255 25.90%

5.7216 5.7182 5.7077 5.7158 1.1058 23.98% 24.57%

5.4561 5.4587 5.4543 5.4564 0.8464 25.16%

5.4051 5.8999 5.8887 5.7312 1.0012 18.84% 20.11%

5.7339 5.7307 5.7209 5.7285 1.1085 21.39%

6.1098 6.2661 6.2599 6.2119 1.2119 21.07% 18.47%

5.9617 5.7005 5.6887 5.7836 0.8336 15.87%

5.8524 6.6246 6.608 6.3617 1.7217 25.08% 21.74%

5.6211 5.6218 5.6153 5.6194 1.0094 18.39%

5.4216 5.4216 5.4216 5.4216 0.8116 14.58% 13.47%

5.6858 5.6859 5.4179 5.5965 0.6165 12.37%

5.7306 5.7347 5.7294 5.7316 1.0016 11.21% 11.46%

6.2197 6.2125 6.2062 6.2128 1.5128 11.70%

6.0141 6.0136 6.0062 6.0113 1.0013 10.42% 10.26%

5.9472 5.9382 5.9288 5.9381 1.2281 10.11%

5.5836 5.5836 0.8336 3.87% 3.73%

5.544 5.5440 0.8440 3.59%

Page 58: Data Experiment Combine

0% 5% 10% 15% 20% 25% 30%0

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400

500

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Pond-3 New

% Total Solid

Yiel

d St

ress

(Pa)

Page 59: Data Experiment Combine

0% 5% 10% 15% 20% 25% 30%0

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400

500

600

700

Pond-3 New

% Total Solid

Yiel

d St

ress

(Pa)

Page 60: Data Experiment Combine

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

300

296.2

257.7333 0 0

A 4.8787 17.9012 13.0225 6.2216227.9

249.1 B 4.9497 18.2758 13.3261 6.2883

200

190.8

179.1333 10 10

A 4.9792 13.6884 8.7092 5.8314159.5

187.1 B 4.8118 13.5392 8.7274 5.6849

160

152.5

145.7667 5 15

A 4.6408 12.1739 7.5331 5.3709147.8

137 B 4.5935 12.2631 7.6696 5.3349

130

132.3

125.5667 5 20

A 4.609 11.0054 6.3964 5.2217129.6

114.8 B 4.6456 10.7015 6.0559 5.222

100

108.7

96.93333 10 30

A 4.7226 9.8928 5.1702 5.204389.2

92.9 B 4.6339 9.3408 4.7069 5.0704

60

58.9

58.79 20 50

A 4.6257 10.9627 6.337 5.14257.22

60.25 B 4.6023 10.5867 5.9844 5.082

40

50.15

44.99 20 70

A 4.5855 11.0952 6.5097 5.072939.72

45.1 B 4.6266 12.1244 7.4978 5.1784

20

23.9

23.78667 25 95

A 4.6167 11.1674 6.5507 5.03223.9

23.56 B 4.5835 13.1569 8.5734 5.149

10

15.48

27.39 20 115

A 4.6785 16.8571 12.1786 5.465446.83

19.86 B 4.5988 16.0969 11.4981 5.2901

1

0.6732

0.785267 40 155

A 4.7169 27.0967 22.3798 5.58970.3366

1.346 B 4.6415 22.1018 17.4603 5.3216

0 (Start)

0

0 0 155

A 4.7731 28.0453 23.2722 5.25840

0 B 4.7914 30.1805 25.3891 5.3054

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Page 61: Data Experiment Combine

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

300

313.4

266.6 0 0

A 5.16 10.088 4.928 5.8651243.4

243 B 4.92 10.0942 5.1742 5.6844

200

207.7

180.2 10 10

A 4.8 9.8714 5.0714 5.4861188.2

144.7 B 4.65 10.7632 6.1132 5.4622

160

178.4

173.6667 5 15

A 4.83 10.5257 5.6957 5.5665169.6

173 B 4.93 9.3324 4.4024 5.5201

130

131.3

133.9667 10 25

A 4.83 11.2595 6.4295 5.5775135.3

135.3 B 4.71 11.0782 6.3682 5.4748

60

56.04

64.68 30 55

A 4.87 14.3141 9.4441 5.814668.33

69.67 B 4.79 10.9539 6.1639 5.3583

50

45.44

48.02 20 75

A 4.92 12.5404 7.6204 5.579948.47

50.15 B 4.76 10.2355 5.4755 5.2295

40

39.72

40.95 10 85

A 4.94 12.4842 7.5442 5.592242.07

41.06 B 4.88 14.0271 9.1471 5.6529

20

26.93

26.59333 20 105

A 4.85 13.7472 8.8972 5.596524.91

27.94 B 4.87 15.2008 10.3308 5.7264

10

11.78

14.81 25 130

A 4.92 16.2122 11.2922 5.649716.49

16.16 B 4.75 14.9031 10.1531 5.5325

5

6.059

6.619667 40 170

A 4.9 12.8326 7.9326 5.40646.732

7.068 B 4.56 14.6663 10.1063 5.2107

0

1.683

1.683 0 170

A 4.68 31.43 26.75 5.59632.02

1.346 B 4.79 33.63 28.84 5.7893

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Page 62: Data Experiment Combine

0

1.346 1.683 0 170 B 4.79 33.63 28.84 5.7893

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

500

573.9

646.2667 0 0

A 4.59 9.7558 5.1658 5.9484744.2

620.7 B 4.98 10.5743 5.5943 6.4507

300

351.4

324.7 10 10

A 4.76 7.8879 3.1279 5.575302.3

320.4 B 5.02 9.2464 4.2264 6.0635

250

262.2

259.9667 10 20

A 4.96 8.4536 3.4936 5.8917245.1

272.6 B 4.9 8.087 3.187 5.7255

200

215.9

191.9 10 30

A 4.61 9.2211 4.6111 5.7216180.1

179.7 B 4.61 7.974 3.364 5.4561

160

154.5

142.8333 15 45

A 4.73 10.0448 5.3148 5.4051145.1

128.9 B 4.62 9.8033 5.1833 5.7339

100

84.15

96.93667 20 65

A 5 10.7515 5.7515 6.1098110.4

96.26 B 4.95 10.2018 5.2518 5.9617

40

44.09

46.22333 30 95

A 4.64 11.5035 6.8635 5.852447.12

47.46 B 4.61 10.098 5.488 5.6211

20

35.34

20.64333 40 135

A 4.61 10.1769 5.5669 5.421612.79

13.8 B 4.98 9.965 4.985 5.6858

10

8.475

11.015 40 175

A 4.73 13.6636 8.9336 5.730611.44

13.13 B 4.7 17.6295 12.9295 6.2197

5

6.732

6.058667 60 235

A 5.01 14.624 9.614 6.01415.385

6.059 B 4.71 16.8617 12.1517 5.9472

0

3.366

2.357333 0 235

A 4.75 26.3 21.55 5.58361.35

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Page 63: Data Experiment Combine

0

2.356 2.357333 0 235 B 4.7 28.19 23.49 5.544

Page 64: Data Experiment Combine

Solid Content mass (gr)

Final Mass Average %TS Average

6.2233 6.2194 6.2214 1.3427 10.31% 10.18%

6.2909 6.2861 6.2884 1.3387 10.05%

5.8322 5.8293 5.8310 0.8518 9.78% 9.91%

5.6891 5.6875 5.6872 0.8754 10.03%

6.2896 5.371 5.6772 1.0364 13.76% 11.71%

5.337 5.3336 5.3352 0.7417 9.67%

5.2226 5.2185 5.2209 0.6119 9.57% 9.55%

5.2243 5.2224 5.2229 0.5773 9.53%

5.202 5.2033 5.2032 0.4806 9.30% 9.28%

5.0699 5.0691 5.0698 0.4359 9.26%

5.1412 5.1394 5.1409 0.5152 8.13% 8.07%

5.0834 5.0805 5.0820 0.4797 8.02%

5.0743 5.0724 5.0732 0.4877 7.49% 7.43%

5.1808 5.1782 5.1791 0.5525 7.37%

5.032 5.031 5.0317 0.4150 6.33% 6.47%

5.1502 5.1482 5.1491 0.5656 6.60%

5.4681 5.4643 5.4659 0.7874 6.47% 6.24%

5.2935 5.2898 5.2911 0.6923 6.02%

5.5947 5.5903 5.5916 0.8747 3.91% 3.91%

5.3249 5.3224 5.3230 0.6815 3.90%

5.6349 5.6313 5.5082 0.7351 3.16% 2.65%

5.3543 5.3522 5.3373 0.5459 2.15%

Solid Content

0% 5% 10% 15% 20% 25% 30%0

100

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300

400

500

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800

900

1000

Pond-1 NewPond-2 NewPond-3 New

% Total Solid

Yiel

d St

ress

(Pa)

Page 65: Data Experiment Combine

Solid Content mass (gr)

Final Mass Average %TS Average

5.868 5.8587 5.8639 0.7039 14.28% 14.52%

5.6872 5.6788 5.6835 0.7635 14.76%

5.4865 5.4826 5.4851 0.6851 13.51% 13.41%

5.4669 5.4606 5.4632 0.8132 13.30%

5.5697 5.5612 5.5658 0.7358 12.92% 13.15%

5.5203 5.5168 5.5191 0.5891 13.38%

5.5782 5.5724 5.5760 0.7460 11.60% 11.80%

Volatile SolidsPond 1 New

5.4787 5.4702 5.4746 0.7646 12.01%A

5.8164 5.8086 5.8132 0.9432 9.99% 9.57%

Container WeightContainer Weight + Sample

5.3549 5.3485 5.3539 0.5639 9.15%Sample

5.5793 5.5736 5.5776 0.6576 8.63% 8.59%

After rehydration ovenSample

5.2312 5.2254 5.2287 0.4687 8.56% After Muffle Furnace

5.5931 5.5867 5.5907 0.6507 8.62% 8.53%

Sample

5.6554 5.6461 5.6515 0.7715 8.43%% Total Solid% Fixed Solids

5.5983 5.5916 5.5955 0.7455 8.38% 8.32%

% Volatile Solids

5.7255 5.7172 5.7230 0.8530 8.26%BContainer Weight

5.6447 5.6423 5.6456 0.7256 6.43% 7.06%

Container Weight + SampleSample

5.5342 5.5274 5.5314 0.7814 7.70% After rehydration oven

5.407 5.4015 5.4050 0.5050 6.37% 6.40%

Sample

5.211 5.2062 5.2093 0.6493 6.42%After Muffle FurnaceSample

5.5998 5.5935 5.5965 0.9165 3.43% 3.45% % Total Solid

5.7963 5.7922 5.7926 1.0026 3.48%% Fixed Solids

Solid Content 0% 5% 10% 15% 20% 25% 30%

0

100

200

300

400

500

600

700

800

900

1000

Pond-1 NewPond-2 NewPond-3 New

% Total Solid

Yiel

d St

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(Pa)

Page 66: Data Experiment Combine

5.7963 5.7922 5.7926 1.0026 3.48%

3.45%

% Volatile Solids

Solid Content mass (gr)

Final Mass Average %TS Average Average

5.9477 5.93217 5.9428 1.3528 26.19% 26.17%

% Total Solid% Fixed Solids

6.4461 6.4313 6.4427 1.4627 26.15%% Volatile Solids

5.6074 5.603 5.5951 0.8351 26.70% 25.62%

6.0603 6.0487 6.0575 1.0375 24.55%

5.8841 5.8785 5.8848 0.9248 26.47% 26.19%

5.7255 5.7255 5.7255 0.8255 25.90%

5.7182 5.7077 5.7158 1.1058 23.98% 24.57%

5.4587 5.4543 5.4564 0.8464 25.16%

5.8999 5.8887 5.7312 1.0012 18.84% 20.11%

5.7307 5.7209 5.7285 1.1085 21.39%

6.2661 6.2599 6.2119 1.2119 21.07% 18.47%

5.7005 5.6887 5.7836 0.8336 15.87%

6.6246 6.608 6.3617 1.7217 25.08% 21.74%

5.6218 5.6153 5.6194 1.0094 18.39%

5.4216 5.4216 5.4216 0.8116 14.58% 13.47%

5.6859 5.4179 5.5965 0.6165 12.37%

5.7347 5.7294 5.7316 1.0016 11.21% 11.46%

6.2125 6.2062 6.2128 1.5128 11.70%

6.0136 6.0062 6.0113 1.0013 10.42% 10.26%

5.9382 5.9288 5.9381 1.2281 10.11%

5.5836 0.8336 3.87% 3.73%

Solid Content

Page 67: Data Experiment Combine

5.5440 0.8440 3.59%

3.73%

Page 68: Data Experiment Combine

0% 5% 10% 15% 20% 25% 30%0

100

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300

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800

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Pond-1 NewPond-2 NewPond-3 New

% Total Solid

Yiel

d St

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(Pa)

Page 69: Data Experiment Combine

Volatile Solids Volatile Solids Volatile SolidsPond 1 New Pond 2 New Pond 3 New

A A

Container Weight 33.2324 Container Weight 27.4124 Container WeightContainer Weight + Sample 57.3359 Container Weight + Sample 41.215 Container Weight + Sample

24.1035 Sample 13.8026 Sample

After rehydration oven 33.64 After rehydration oven 27.9429 After rehydration oven0.4076 Sample 0.5305 Sample

After Muffle Furnace 33.4085 After Muffle Furnace 27.6112 After Muffle Furnace0.1761 Sample 0.1988 Sample

% Total Solid 1.69% % Total Solid 3.84% % Total Solid% Fixed Solids 43.20% % Fixed Solids 37.47% % Fixed Solids% Volatile Solids 56.80% % Volatile Solids 62.53% % Volatile Solids

B BContainer Weight 26.9075 Container Weight 26.8891 Container WeightContainer Weight + Sample 39.1131 Container Weight + Sample 48.2387 Container Weight + Sample

12.2056 Sample 21.3496 Sample

After rehydration oven 27.1201 After rehydration oven 27.6684 After rehydration oven0.2126 Sample 0.7793 Sample

After Muffle Furnace 26.9424 After Muffle Furnace 27.2112 After Muffle Furnace0.0349 Sample 0.3221 Sample

% Total Solid 1.74% % Total Solid 3.65% % Total Solid% Fixed Solids 16.42% % Fixed Solids 41.33% % Fixed Solids

0% 5% 10% 15% 20% 25% 30%0

100

200

300

400

500

600

700

800

900

1000

Pond-1 NewPond-2 NewPond-3 New

% Total Solid

Yiel

d St

ress

(Pa)

Page 70: Data Experiment Combine

% Volatile Solids 83.58% % Volatile Solids 58.67% % Volatile Solids

Average Average% Total Solid 1.72% % Total Solid 3.75% % Total Solid% Fixed Solids 29.81% % Fixed Solids 39.40% % Fixed Solids% Volatile Solids 70.19% % Volatile Solids 60.60% % Volatile Solids

Page 71: Data Experiment Combine

0% 5% 10% 15% 20% 25% 30%0

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500

600

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800

900

1000

Pond-1 NewPond-2 NewPond-3 New

% Total Solid

Yiel

d St

ress

(Pa)

Page 72: Data Experiment Combine

Volatile SolidsPond 3 New

Container Weight 26.3899Container Weight + Sample 49.0279

22.638

After rehydration oven 27.32310.9332

After Muffle Furnace 26.91560.5257

% Total Solid 4.12%% Fixed Solids 56.33%% Volatile Solids 43.67%

Container Weight 23.7445Container Weight + Sample 45.0337

21.2892

After rehydration oven 24.62150.877

After Muffle Furnace 24.24170.4972

% Total Solid 4.12%% Fixed Solids 56.69%

0% 5% 10% 15% 20% 25% 30%0

100

200

300

400

500

600

700

800

900

1000

Pond-1 NewPond-2 NewPond-3 New

% Total Solid

Yiel

d St

ress

(Pa)

Page 73: Data Experiment Combine

% Volatile Solids 43.31%

% Total Solid 4.12%% Fixed Solids 56.51%% Volatile Solids 43.49%

Page 74: Data Experiment Combine

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

990

990.7

969.5333 0 0

A 4.7408 11.3104 6.5696 7.4136991.6

926.3 B 4.6597 13.873 9.2133 8.4304

600

594.4

609.9 10 10

A 4.6771 12.9577 8.2806 7.8242617

618.3 B 4.7276 13.3713 8.6437 7.9999

400

445.6

462.9333 7 17

A 4.7598 14.0989 9.3391 8.1738472.6

470.6 B 4.7147 13.5401 8.8254 7.973

100

118.5

122.9667 40 57

A 4.6629 14.28 9.6171 7.7282112.1

138.3 B 4.7439 12.5351 7.7912 7.2045

70

71.69

71.02 20 77

A 4.6504 13.261 8.6106 7.207962.61

78.76 B 4.6714 12.9175 8.2461 7.1039

40

44.43

44.31667 20 97

A 4.737 17.4141 12.6771 8.23944.09

44.43 B 4.753 16.3615 11.6085 7.9948

20

24.23

26.59667 20 117

A 4.7487 15.0872 10.3385 7.377428.3

27.26 B 4.6513 13.4297 8.7784 6.6574

10

17.5

17.36667 20 137

A 4.7178 18.7889 14.0711 8.041817.8

16.8 B 4.7429 17.5126 12.7697 7.8114

5

5.722

6.339 40 177

A 4.719 20.4469 15.7279 7.87247.068

6.227 B 4.7393 20.004 15.2647 7.8382

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

250

281.1

257.9333 0 0

A 4.6507 10.584 5.9333 5.2598240.3

252.4 B 4.7099 14.0945 9.3846 5.6196

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Page 75: Data Experiment Combine

250

252.4 257.9333 0 0 B 4.7099 14.0945 9.3846 5.6196

220

226

216.9333 2 2

A 4.65 12.1361 7.4861 5.3504215.1

209.7 B 4.6213 10.0825 5.4612 5.1572

190

192.4

193.9333 2 4

A 4.7214 9.3058 4.5844 5.157197.2

192.2 B 4.6255 12.2904 7.6649 5.349

180

177.4

178.9667 2 6

A 4.7184 11.3203 6.6019 5.3336180.1

179.4 B 4.7097 11.5828 6.8731 5.3373

160

164.3

165.6 2 8

A 4.7371 12.3149 7.5778 5.4227160.2

172.3 B 4.6974 11.4573 6.7599 5.3242

130

133.3

135.8667 6 14

A 4.7022 9.097 4.3948 5.0876138

136.3 B 4.6197 9.7112 5.0915 5.0662

100

103.7

104.6667 8 22

A 4.6948 9.4459 4.7511 5.0981106

104.3 B 4.7243 9.4436 4.7193 5.1227

70

75.73

77.52667 14 36

A 4.6285 12.3536 7.7251 5.231480.78

76.07 B 4.7133 11.5574 6.8441 5.2484

40

42.75

45.55333 21 57

A 4.7132 13.7535 9.0403 5.368747.46

46.45 B 4.7215 15.5063 10.7848 5.5016

10

10.1

10.60333 40 97

A 4.6183 17.7296 13.1113 5.268910.94

10.77 B 4.6187 13.3564 8.7377 5.0548

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

550

553.4

560.1333 0 0

A 4.765 11.223 6.458 6.2486577.3

549.7 B 4.8329 9.9756 5.1427 6.0302

400

369.6

377.5667 10 10

A 4.6347 10.2532 5.6185 5.8718408.3

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Page 76: Data Experiment Combine

400

354.8 377.5667 10 10 B 4.794 10.8143 6.0203 6.1418

300

320.4

317.1667 5 15

A 4.7285 10.5409 5.8124 6.016318.1

313 B 4.7013 10.2877 5.5864 5.9487

200

244.4

254.6 10 25

A 4.8117 9.7636 4.9519 5.9006257.2

262.2 B 4.8726 10.2797 5.4071 6.0687

100

124.2

114.0967 40 65

A 4.8715 13.9987 9.1272 6.4833118.8

99.29 B 4.7189 13.2771 8.5582 6.2209

80

89.53

78.79333 20 85

A 4.8079 16.7846 11.9767 6.799167.75

79.1 B 4.7884 15.4801 10.6917 6.5979

40

42.75

44.77 20 105

A 4.8025 19.7777 14.9752 7.109942.75

48.81 B 4.7457 17.5144 12.7687 6.68866

20

28.27

32.2 20 125

A 4.8121 23.33 18.5179 7.516328.95

39.38 B 4.6909 19.1819 14.491 6.6904

10

13.13

18.21333 30 155

A 4.7006 22.7994 18.0988 7.078821.21

20.3 B 4.7993 24.9348 20.1355 7.4501

5

9.088

9.646 30 185

A 4.8324 19.1598 14.3274 6.49989.42

10.43 B 4.7378 17.7233 12.9855 6.2328

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

300

296.2

257.7333 0 0

A 4.8787 17.9012 13.0225 6.2216227.9

249.1 B 4.9497 18.2758 13.3261 6.2883

200

190.8

179.1333 10 10

A 4.9792 13.6884 8.7092 5.8314159.5

187.1 B 4.8118 13.5392 8.7274 5.6849

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Page 77: Data Experiment Combine

160

152.5

145.7667 5 15

A 4.6408 12.1739 7.5331 5.3709147.8

137 B 4.5935 12.2631 7.6696 5.3349

130

132.3

125.5667 5 20

A 4.609 11.0054 6.3964 5.2217129.6

114.8 B 4.6456 10.7015 6.0559 5.222

100

108.7

96.93333 10 30

A 4.7226 9.8928 5.1702 5.204389.2

92.9 B 4.6339 9.3408 4.7069 5.0704

60

58.9

58.79 20 50

A 4.6257 10.9627 6.337 5.14257.22

60.25 B 4.6023 10.5867 5.9844 5.082

40

50.15

44.99 20 70

A 4.5855 11.0952 6.5097 5.072939.72

45.1 B 4.6266 12.1244 7.4978 5.1784

20

23.9

23.78667 25 95

A 4.6167 11.1674 6.5507 5.03223.9

23.56 B 4.5835 13.1569 8.5734 5.149

10

15.48

27.39 20 115

A 4.6785 16.8571 12.1786 5.465446.83

19.86 B 4.5988 16.0969 11.4981 5.2901

1

0.6732

0.785267 40 155

A 4.7169 27.0967 22.3798 5.58970.3366

1.346 B 4.6415 22.1018 17.4603 5.3216

0 (Start)

0

0 0 155

A 4.7731 28.0453 23.2722 5.25840

0 B 4.7914 30.1805 25.3891 5.3054

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

300

313.4

266.6 0 0

A 5.16 10.088 4.928 5.8651243.4

243 B 4.92 10.0942 5.1742 5.6844

200

207.7

180.2 10 10

A 4.8 9.8714 5.0714 5.4861188.2

144.7 B 4.65 10.7632 6.1132 5.4622

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Page 78: Data Experiment Combine

200

144.7 180.2 10 10 B 4.65 10.7632 6.1132 5.4622

160

178.4

173.6667 5 15

A 4.83 10.5257 5.6957 5.5665169.6

173 B 4.93 9.3324 4.4024 5.5201

130

131.3

133.9667 10 25

A 4.83 11.2595 6.4295 5.5775135.3

135.3 B 4.71 11.0782 6.3682 5.4748

60

56.04

64.68 30 55

A 4.87 14.3141 9.4441 5.814668.33

69.67 B 4.79 10.9539 6.1639 5.3583

50

45.44

48.02 20 75

A 4.92 12.5404 7.6204 5.579948.47

50.15 B 4.76 10.2355 5.4755 5.2295

40

39.72

40.95 10 85

A 4.94 12.4842 7.5442 5.592242.07

41.06 B 4.88 14.0271 9.1471 5.6529

20

26.93

26.59333 20 105

A 4.85 13.7472 8.8972 5.596524.91

27.94 B 4.87 15.2008 10.3308 5.7264

10

11.78

14.81 25 130

A 4.92 16.2122 11.2922 5.649716.49

16.16 B 4.75 14.9031 10.1531 5.5325

5

6.059

6.619667 40 170

A 4.9 12.8326 7.9326 5.40646.732

7.068 B 4.56 14.6663 10.1063 5.2107

0

1.683

1.683 0 170

A 4.68 31.43 26.75 5.59632.02

1.346 B 4.79 33.63 28.84 5.7893

ζ - Target ζ - Actual (Pa)

Solid Content mass (gr)

Container Sample Final Mass

500

573.9

646.2667 0 0

A 4.59 9.7558 5.1658 5.9484744.2

620.7 B 4.98 10.5743 5.5943 6.4507

300

351.4

324.7 10 10

A 4.76 7.8879 3.1279 5.575302.3

Tap Water

volume (µl) N x

1000

Accumulative (ml) Sample +

Container

Page 79: Data Experiment Combine

300

320.4 324.7 10 10 B 5.02 9.2464 4.2264 6.0635

250

262.2

259.9667 10 20

A 4.96 8.4536 3.4936 5.8917245.1

272.6 B 4.9 8.087 3.187 5.7255

200

215.9

191.9 10 30

A 4.61 9.2211 4.6111 5.7216180.1

179.7 B 4.61 7.974 3.364 5.4561

160

154.5

142.8333 15 45

A 4.73 10.0448 5.3148 5.4051145.1

128.9 B 4.62 9.8033 5.1833 5.7339

100

84.15

96.93667 20 65

A 5 10.7515 5.7515 6.1098110.4

96.26 B 4.95 10.2018 5.2518 5.9617

40

44.09

46.22333 30 95

A 4.64 11.5035 6.8635 5.852447.12

47.46 B 4.61 10.098 5.488 5.6211

20

35.34

20.64333 40 135

A 4.61 10.1769 5.5669 5.421612.79

13.8 B 4.98 9.965 4.985 5.6858

10

8.475

11.015 40 175

A 4.73 13.6636 8.9336 5.730611.44

13.13 B 4.7 17.6295 12.9295 6.2197

5

6.732

6.058667 60 235

A 5.01 14.624 9.614 6.01415.385

6.059 B 4.71 16.8617 12.1517 5.9472

0

3.366

2.357333 0 235

A 4.75 26.3 21.55 5.58361.35

2.356 B 4.7 28.19 23.49 5.544

Page 80: Data Experiment Combine

Solid Content mass (gr)

Final Mass Average %TS Average

7.4165 7.4178 7.4160 2.6752 40.72% 40.84%

8.4357 8.4338 8.4333 3.7736 40.96%

7.8294 7.99 7.8812 3.2041 38.69% 37.93%

7.9945 7.8254 7.9399 3.2123 37.16%

8.178 8.1731 8.1750 3.4152 36.57% 36.73%

7.9718 7.9687 7.9712 3.2565 36.90%

7.7342 7.7276 7.7300 3.0671 31.89% 31.75%

7.2074 7.2069 7.2063 2.4624 31.60%

7.2099 7.2106 7.2095 2.5591 29.72% 29.62%

7.1093 7.1049 7.1060 2.4346 29.52%

8.2422 8.2402 8.2405 3.5035 27.64% 27.79%

7.9992 7.9959 7.9966 3.2436 27.94%

7.3774 7.374 7.3763 2.6276 25.42% 24.13%

6.6582 6.6568 6.6575 2.0062 22.85%

8.0392 8.0368 8.0393 3.3215 23.60% 23.81%

7.8072 7.8077 7.8088 3.0659 24.01%

7.8742 7.8721 7.8729 3.1539 20.05% 20.21%

7.8359 7.8721 7.8487 3.1094 20.37%Volatile SolidsPond 1A

Solid Content mass (gr) Container Weight

Final Mass Average %TS Average Container Weight + Sample

5.2601 5.2592 5.2597 0.6090 10.26% 9.98%

Sample

5.622 5.6181 5.6199 0.9100 9.70%After rehydration oven

Solid Content

Solid Content

0% 5% 10% 15% 20% 25% 30% 35% 40%0

100

200

300

400

500

600

700

800

900

1000

Pond-1 NewPond-2 NewPond-3 NewPond-1Pond-2Pond-3

% Total Solid

Yiel

d St

ress

(Pa)

Page 81: Data Experiment Combine

5.622 5.6181 5.6199 0.9100 9.70%

9.98%

Sample

5.3509 5.3509 5.3507 0.7007 9.36% 9.60% After Muffle Furnace

5.1596 5.1589 5.1586 0.5373 9.84%Sample

5.1594 5.1584 5.1583 0.4369 9.53% 9.49%

% Total Solid% Fixed Solids

5.35 5.3506 5.3499 0.7244 9.45%% Volatile Solids

5.3325 5.3333 5.3331 0.6147 9.31% 9.22%

BContainer Weight

5.3381 5.3376 5.3377 0.6280 9.14%Container Weight + SampleSample

5.4235 5.4257 5.4240 0.6869 9.06% 9.18% After rehydration oven

5.325 5.3264 5.3252 0.6278 9.29%Sample

5.0877 5.0881 5.0878 0.3856 8.77% 8.77%

After Muffle FurnaceSample

5.0667 5.0661 5.0663 0.4466 8.77% % Total Solid

5.0993 5.0999 5.0991 0.4043 8.51% 8.49%

% Fixed Solids% Volatile Solids

5.1243 5.1242 5.1237 0.3994 8.46%

5.233 5.2314 5.2319 0.6034 7.81% 7.82%

Average% Total Solid

5.2516 5.2484 5.2495 0.5362 7.83%% Fixed Solids% Volatile Solids

5.3687 5.3688 5.3687 0.6555 7.25% 7.24%

5.5016 5.5032 5.5021 0.7806 7.24%Volatile Solids

5.2689 5.2707 5.2695 0.6512 4.97% 4.98%

A

5.0548 5.0564 5.0553 0.4366 5.00%Container WeightContainer Weight + SampleSample

Solid Content mass (gr)

Final Mass Average %TS Average After rehydration oven

6.2521 6.2596 6.2534 1.4884 23.05% 23.20%

Sample

6.0339 6.0385 6.0342 1.2013 23.36%After Muffle FurnaceSample

5.875 5.8778 5.8749 1.2402 22.07% 22.25% % Total Solid

Solid Content

Page 82: Data Experiment Combine

6.1436 6.1476 6.1443 1.3503 22.43%

22.25%% Fixed Solids% Volatile Solids

6.0212 6.027 6.0214 1.2929 22.24% 22.32% B

5.9524 5.9553 5.9521 1.2508 22.39%Container WeightContainer Weight + Sample

5.9073 5.9091 5.9057 1.0940 22.09% 22.15%

Sample

6.0744 6.0781 6.0737 1.2011 22.21%After rehydration ovenSample

6.4887 6.4927 6.4882 1.6167 17.71% 17.66% After Muffle Furnace

6.2257 6.2319 6.2262 1.5073 17.61%Sample

6.8038 6.8102 6.8044 1.9965 16.67% 16.81%

% Total Solid% Fixed Solids

6.5966 6.6044 6.5996 1.8112 16.94%% Volatile Solids

7.1132 7.1212 7.1148 2.3123 15.44% 15.34% Average

6.6908 6.697 6.6922 1.9465 15.24%% Total Solid% Fixed Solids

7.5217 7.5273 7.5218 2.7097 14.63% 14.23%

% Volatile Solids

6.6947 6.6973 6.6941 2.0032 13.82%

7.0823 7.0823 7.0811 2.3805 13.15% 13.17%

7.4532 7.4623 7.4552 2.6559 13.19%

6.498 6.5034 6.5004 1.6680 11.64% 11.59%

6.2346 6.2375 6.2350 1.4972 11.53%

Solid Content mass (gr)

Final Mass Average %TS Average

6.2233 6.2194 6.2214 1.3427 10.31% 10.18%

6.2909 6.2861 6.2884 1.3387 10.05%

5.8322 5.8293 5.8310 0.8518 9.78% 9.91%

5.6891 5.6875 5.6872 0.8754 10.03%

Solid Content

Page 83: Data Experiment Combine

6.2896 5.371 5.6772 1.0364 13.76% 11.71%

5.337 5.3336 5.3352 0.7417 9.67%

5.2226 5.2185 5.2209 0.6119 9.57% 9.55%

5.2243 5.2224 5.2229 0.5773 9.53%

5.202 5.2033 5.2032 0.4806 9.30% 9.28%

5.0699 5.0691 5.0698 0.4359 9.26%

5.1412 5.1394 5.1409 0.5152 8.13% 8.07%

5.0834 5.0805 5.0820 0.4797 8.02%

5.0743 5.0724 5.0732 0.4877 7.49% 7.43%

5.1808 5.1782 5.1791 0.5525 7.37%

5.032 5.031 5.0317 0.4150 6.33% 6.47%

5.1502 5.1482 5.1491 0.5656 6.60%

5.4681 5.4643 5.4659 0.7874 6.47% 6.24%

5.2935 5.2898 5.2911 0.6923 6.02%

5.5947 5.5903 5.5916 0.8747 3.91% 3.91%

5.3249 5.3224 5.3230 0.6815 3.90%

5.6349 5.6313 5.5082 0.7351 3.16% 2.65%

5.3543 5.3522 5.3373 0.5459 2.15%

Solid Content mass (gr)

Final Mass Average %TS Average

5.868 5.8587 5.8639 0.7039 14.28% 14.52%

5.6872 5.6788 5.6835 0.7635 14.76%

5.4865 5.4826 5.4851 0.6851 13.51% 13.41%

5.4669 5.4606 5.4632 0.8132 13.30%

Solid Content

Page 84: Data Experiment Combine

5.4669 5.4606 5.4632 0.8132 13.30%

13.41%

5.5697 5.5612 5.5658 0.7358 12.92% 13.15%

5.5203 5.5168 5.5191 0.5891 13.38%

5.5782 5.5724 5.5760 0.7460 11.60% 11.80%

5.4787 5.4702 5.4746 0.7646 12.01%

5.8164 5.8086 5.8132 0.9432 9.99% 9.57%

5.3549 5.3485 5.3539 0.5639 9.15%

5.5793 5.5736 5.5776 0.6576 8.63% 8.59%

5.2312 5.2254 5.2287 0.4687 8.56%

5.5931 5.5867 5.5907 0.6507 8.62% 8.53%

5.6554 5.6461 5.6515 0.7715 8.43%

5.5983 5.5916 5.5955 0.7455 8.38% 8.32%

5.7255 5.7172 5.7230 0.8530 8.26%

5.6447 5.6423 5.6456 0.7256 6.43% 7.06%

5.5342 5.5274 5.5314 0.7814 7.70%

5.407 5.4015 5.4050 0.5050 6.37% 6.40%

5.211 5.2062 5.2093 0.6493 6.42%

5.5998 5.5935 5.5965 0.9165 3.43% 3.45%

5.7963 5.7922 5.7926 1.0026 3.48%

Solid Content mass (gr)

Final Mass Average %TS Average

5.9477 5.93217 5.9428 1.3528 26.19% 26.17%

6.4461 6.4313 6.4427 1.4627 26.15%

5.6074 5.603 5.5951 0.8351 26.70% 25.62%

Solid Content

Page 85: Data Experiment Combine

6.0603 6.0487 6.0575 1.0375 24.55%

25.62%

5.8841 5.8785 5.8848 0.9248 26.47% 26.19%

5.7255 5.7255 5.7255 0.8255 25.90%

5.7182 5.7077 5.7158 1.1058 23.98% 24.57%

5.4587 5.4543 5.4564 0.8464 25.16%

5.8999 5.8887 5.7312 1.0012 18.84% 20.11%

5.7307 5.7209 5.7285 1.1085 21.39%

6.2661 6.2599 6.2119 1.2119 21.07% 18.47%

5.7005 5.6887 5.7836 0.8336 15.87%

6.6246 6.608 6.3617 1.7217 25.08% 21.74%

5.6218 5.6153 5.6194 1.0094 18.39%

5.4216 5.4216 5.4216 0.8116 14.58% 13.47%

5.6859 5.4179 5.5965 0.6165 12.37%

5.7347 5.7294 5.7316 1.0016 11.21% 11.46%

6.2125 6.2062 6.2128 1.5128 11.70%

6.0136 6.0062 6.0113 1.0013 10.42% 10.26%

5.9382 5.9288 5.9381 1.2281 10.11%

5.5836 0.8336 3.87% 3.73%

5.5440 0.8440 3.59%

Page 86: Data Experiment Combine

Volatile Solids Volatile SolidsPond 2A

Container Weight 31.1593 Container Weight 23.314

Container Weight + Sample 54.8445 Container Weight + Sample 46.878423.6852 Sample 23.5644

After rehydration oven 36.7006 After rehydration oven 25.9101

0% 5% 10% 15% 20% 25% 30% 35% 40%0

100

200

300

400

500

600

700

800

900

1000

Pond-1 NewPond-2 NewPond-3 NewPond-1Pond-2Pond-3

% Total Solid

Yiel

d St

ress

(Pa)

Page 87: Data Experiment Combine

5.5413 Sample 2.5961

After Muffle Furnace 35.6853 After Muffle Furnace 24.70684.526 Sample 1.3928

% Total Solid 23.40% % Total Solid 11.02%% Fixed Solids 81.68% % Fixed Solids 53.65%% Volatile Solids 18.32% % Volatile Solids 46.35%

BContainer Weight 60.615 Container Weight 23.504Container Weight + Sample 144.7938 Container Weight + Sample 47.5688

84.1788 Sample 24.0648

After rehydration oven 80.9976 After rehydration oven 26.188120.3826 Sample 2.6841

After Muffle Furnace 77.6213 After Muffle Furnace 24.914217.0063 Sample 1.4102

% Total Solid 24.21% % Total Solid 11.15%% Fixed Solids 83.44% % Fixed Solids 52.54%% Volatile Solids 16.56% % Volatile Solids 47.46%

Average% Total Solid 23.80% % Total Solid 11.09%% Fixed Solids 82.56% % Fixed Solids 53.09%% Volatile Solids 17.44% % Volatile Solids 46.91%

Volatile Solids Volatile Solids

A

Container Weight 33.2324 Container Weight 27.4124Container Weight + Sample 57.3359 Container Weight + Sample 41.215

24.1035 Sample 13.8026

After rehydration oven 33.64 After rehydration oven 27.94290.4076 Sample 0.5305

After Muffle Furnace 33.4085 After Muffle Furnace 27.61120.1761 Sample 0.1988

% Total Solid 1.69% % Total Solid 3.84%

Page 88: Data Experiment Combine

% Fixed Solids 43.20% % Fixed Solids 37.47%% Volatile Solids 56.80% % Volatile Solids 62.53%

BContainer Weight 26.9075 Container Weight 26.8891Container Weight + Sample 39.1131 Container Weight + Sample 48.2387

12.2056 Sample 21.3496

After rehydration oven 27.1201 After rehydration oven 27.66840.2126 Sample 0.7793

After Muffle Furnace 26.9424 After Muffle Furnace 27.21120.0349 Sample 0.3221

% Total Solid 1.74% % Total Solid 3.65%% Fixed Solids 16.42% % Fixed Solids 41.33%% Volatile Solids 83.58% % Volatile Solids 58.67%

Average% Total Solid 1.72% % Total Solid 3.75%% Fixed Solids 29.81% % Fixed Solids 39.40%% Volatile Solids 70.19% % Volatile Solids 60.60%

% Total Solid % Volatile Solids % Total Sol% Volatile Solids23.80% 17.44% 0.017 0.70211.09% 46.91% 0.037 0.606

4.29% 26.61% 0.041 0.4351.72% 70.19% 0.043 0.2663.75% 60.60% 0.111 0.4694.12% 43.49% 0.238 0.174

2.400548

-1.906967E-114.00874E-07

-8.345652E-050.0058389733

-0.4371170843

0.017 0.037 0.041 0.043 0.111 0.2380.000

0.100

0.200

0.300

0.400

0.500

0.600

0.700

0.800

f(x) = − 0.00342673848 x⁶ + 0.05920873993 x⁵ − 0.39622987573 x⁴ + 1.3260105847 x³ − 2.38524031421 x² + 2.10157797371 xR² = 1

Relation TS and VS

Column AAPolynomial (Column AA)Polynomial (Column AA)

Total Solid

Vola

tile

Solid

Page 89: Data Experiment Combine

2.46732.0359388332

Page 90: Data Experiment Combine

Volatile SolidsPond 3AContainer Weight 33.5693

Container Weight + Sample 62.6762Sample 29.1069

After rehydration oven 34.4828

0% 5% 10% 15% 20% 25% 30% 35% 40%0

100

200

300

400

500

600

700

800

900

1000

Pond-1 NewPond-2 NewPond-3 NewPond-1Pond-2Pond-3

% Total Solid

Yiel

d St

ress

(Pa)

Page 91: Data Experiment Combine

Sample 0.9135

After Muffle Furnace 34.4036Sample 0.8343

% Total Solid 3.14%% Fixed Solids 91.33%% Volatile Solids 8.67%

BContainer Weight 24.9239Container Weight + Sample 43.4183Sample 18.4944

After rehydration oven 25.9285Sample 1.0046

After Muffle Furnace 25.4809Sample 0.557

% Total Solid 5.43%% Fixed Solids 55.44%% Volatile Solids 44.56%

Average% Total Solid 4.29%% Fixed Solids 73.39%% Volatile Solids 26.61%

Volatile Solids

A

Container Weight 26.3899Container Weight + Sample 49.0279Sample 22.638

After rehydration oven 27.3231Sample 0.9332

After Muffle Furnace 26.9156Sample 0.5257

% Total Solid 4.12%

0% 5% 10% 15% 20% 25%0.00%

10.00%

20.00%

30.00%

40.00%

50.00%

60.00%

70.00%

80.00%

f(x) = − 1.67660168394255 x + 0.578308721335036R² = 0.491329367604623

Column WLinear (Column W)

Total Solid

Vola

tile

Solid

Page 92: Data Experiment Combine

% Fixed Solids 56.33%% Volatile Solids 43.67%

BContainer Weight 23.7445Container Weight + Sample 45.0337Sample 21.2892

After rehydration oven 24.6215Sample 0.877

After Muffle Furnace 24.2417Sample 0.4972

% Total Solid 4.12%% Fixed Solids 56.69%% Volatile Solids 43.31%

Average% Total Solid 4.12%% Fixed Solids 56.51%% Volatile Solids 43.49%

0% 5% 10% 15% 20% 25%0.00%

10.00%

20.00%

30.00%

40.00%

50.00%

60.00%

70.00%

80.00%

f(x) = − 1.67660168394255 x + 0.578308721335036R² = 0.491329367604623

Column WLinear (Column W)

Total Solid

Vola

tile

Solid

0.017 0.037 0.041 0.043 0.111 0.2380.000

0.100

0.200

0.300

0.400

0.500

0.600

0.700

0.800

f(x) = − 0.00342673848 x⁶ + 0.05920873993 x⁵ − 0.39622987573 x⁴ + 1.3260105847 x³ − 2.38524031421 x² + 2.10157797371 xR² = 1

Relation TS and VS

Column AAPolynomial (Column AA)Polynomial (Column AA)

Total Solid

Vola

tile

Solid

Page 93: Data Experiment Combine

0% 5% 10% 15% 20% 25%0.00%

10.00%

20.00%

30.00%

40.00%

50.00%

60.00%

70.00%

80.00%

f(x) = − 1.67660168394255 x + 0.578308721335036R² = 0.491329367604623

Column WLinear (Column W)

Total Solid

Vola

tile

Solid

Page 94: Data Experiment Combine

0% 5% 10% 15% 20% 25%0.00%

10.00%

20.00%

30.00%

40.00%

50.00%

60.00%

70.00%

80.00%

f(x) = − 1.67660168394255 x + 0.578308721335036R² = 0.491329367604623

Column WLinear (Column W)

Total Solid

Vola

tile

Solid

Page 95: Data Experiment Combine

Total Solid Target Sample Sample MassDry Mass

% Solid Actual1 2 3 Average

10%A 4.8621 27.3275 22.4654 7.08179 7.0798 7.0826 7.081397 9.88%B 4.8565 27.9278 23.0713 7.14459 7.1456 7.14469 7.14496 9.92%

6%A 4.9164 34.6028 29.6864 6.8421 6.8346 6.8434 6.840033 6.48%B 4.9196 30.0862 25.1666 6.531 6.5333 6.5335 6.5326 6.41%

1%A 4.94 28.13 23.19 5.154 5.156 5.1586 5.1562 0.93%B 4.81 25.47 20.66 4.9466 4.938 4.9452 4.943267 0.65%

MF002

Solidifier Mass SampleMass Sample Percentage Solidifier

10%A

B

6%A

B

1%A

B

MF006

Solidifier Mass SampleMass Sample Percentage Solidifier

10%A

B

Container Mass

Container + Sample

Mass Container

Mass Container + Sample

Mass Solidifier

Mass Container

Mass Container + Sample

Mass Solidifier

Page 96: Data Experiment Combine

6%A

B

1%A

B

Page 97: Data Experiment Combine

Rheometer Test

Solidifier Type MF006

Total Solid

Solidifier Concentration

0 Minute

1% Average 3% Average 0.5% Average 1.5% Average

10% 5.8125 7.10225 6.732 6.3955 7.74 6.225 4.376 3.1988.392 6.059 4.71 2.02

6% 1.01 0.8416 1.683 1.8515 0.6732 0.6732 1.01 1.1780.6732 2.02 0.6732 1.346

1% 0 0 0 0 0.3366 0.3366 0.3366 0.67330 0 0.3366 1.01

Total Solid

Solidifier Concentration

2 Minute

1% Average 3% Average 0.5% Average 1.5% Average

10% 107 134.05 722.3 720.95 48.1 52.83 521 577.55161.1 719.6 57.56 634.1

6% 309.3 318.4 704.1 614.1 30.63 37.025 497.8 487.9327.5 524.1 43.42 478

1% 299.6 301.25 507.3 526.2 6.059 6.5635 334.6 311.55302.9 545.1 7.068 288.5

Total Solid

Solidifier Concentration

5 Minute

Page 98: Data Experiment Combine

Total Solid 1% Average 3% Average 0.5% Average 1.5% Average

5 Minute

10% 195.6 184.65 405.9 488.45 50.15 51.665 368 359.05173.7 571 53.18 350.1

6% 284.4 272.65 428.5 410.5 29.28 28.44 230.2 222.15260.9 392.5 27.6 214.1

1% 183.8 173.6 286.1 277.85 14.81 15.315 154.3 144.95163.4 269.6 15.82 135.6

Page 99: Data Experiment Combine

Total Solid

Solidifier Concentration

7 Minute

1% Average 3% Average 0.5% Average 1.5% Average

10% 183.8 176.9 412.1 399.75 29.73 33.715 330 336.65170 387.4 37.7 343.3

6% 189.5 184.95 319.8 332.9 27.26 26.59 179.9 177.15180.4 346 25.92 174.4

1% 120.8 113.75 212.4 202.9 13.8 12.115 97.27 96.765106.7 193.4 10.43 96.26

Total Solid

Solidifier Concentration

10 Minute

1% Average 3% Average 0.5% Average 1.5% Average

10% 118.8 102.83 307.1 315.6 33.32 32.31 242 232.486.86 324.1 31.3 222.8

6% 160.2 155.15 235.6 227.2 22.89 23.225 145.1 146.1150.1 218.8 23.56 147.1

1% 88.86 86.335 118.75 124.325 13.8 12.455 76.74 73.54583.81 129.9 11.11 70.35

Rheometer Test

Solidifier Type MF002

Total Solid

Solidifier Concentration

0 Minute

Page 100: Data Experiment Combine

Total Solid 1% Average 3% Average 0.5% Average 1.5% Average

0 Minute

10% 4.712 5.0485 3.702 4.039 3.2 2.9465 4.039 3.87055.385 4.376 2.693 3.702

6% 0.8366 1.0913 1.01 0.8417 1.346 1.0096 1.01 1.011.346 0.6734 0.6732 1.01

1% 0.3366 0.3366 0 0 0.6732 0.6732 1.683 1.34650.3366 0 0.6732 1.01

Total Solid

Solidifier Concentration

2 Minute

1% Average 3% Average 0.5% Average 1.5% Average

10% 74.39 75.14 696 924.5 50.49 50.995 125 169.275.89 1153 51.5 213.4

6% 55.5 84.45 1099 1090.5 3.702 4.8805 249.7 284.75113.4 1082 6.059 319.8

1% 13.46 15.315 862 833.4 0.6732 0.5196 162.9 189.6517.17 804.8 0.366 216.4

Total Solid

Solidifier Concentration

5 Minute

1% Average 3% Average 0.5% Average 1.5% Average

10% 79.44 94.27 987.4 911.9 17.17 15.99 283.7 303.4109.1 836.4 14.81 323.1

6% 57.56 55.2 807.8 719.1 6.227 6.143 278 265.05

Page 101: Data Experiment Combine

6%52.84

55.2630.4

719.16.059

6.143252.1

265.05

5 Minute

1% 21.21 20.535 588.4 572.2 0 0 234.6 232.619.86 556 0 230.6

Total Solid

Solidifier Concentration

7 Minute

1% Average 3% Average 0.5% Average 1.5% Average

10% 105.4 104.2 571.2 591.9 13.8 13.125 261.9 270.45103 612.6 12.45 279

6% 47.46 45.44 494.1 507.4 5.722 6.0585 187.3 186.5543.42 520.7 6.395 185.8

1% 17.5 15.95 385.7 380.15 0 0 189.8 182.114.4 374.6 0 174.4

Total Solid

Solidifier Concentration

10 Minute

1% Average 3% Average 0.5% Average 1.5% Average

10% 92.56 101.835 473.9 476.45 10.1 10.3 207 200.95111.11 479 10.5 194.9

6% 40.73 39.38 283.4 274.5 5.049 4.8805 120.8 118.9538.03 265.6 4.712 117.1

1% 13.46 12.62 211.7 210.35 0.3366 0.5049 163.6 156.3511.78 209 0.6732 149.1

Page 102: Data Experiment Combine

TS 10% TS 1%

Time Solid Time Solid

0.5% 1% 1.5% 3% 0.5% 1% 1.5% 3%

0 6.225 7.10225 3.198 6.3955 0 0.3366 0 0.6733 0

2 52.83 134.05 577.55 720.95 2 6.5635 301.25 311.55 526.2

5 51.665 184.65 359.05 488.45 5 15.315 173.6 144.95 277.85

7 33.715 176.9 336.65 399.75 7 12.115 113.75 96.765 202.9

10 32.31 102.83 232.4 315.6 10 12.455 86.335 73.545 124.325

TS 6%

Time Solid

0.5% 1% 1.5% 3%

0 0.6732 0.8416 1.178 1.8515

2 37.025 318.4 487.9 614.1

5 28.44 272.65 222.15 410.5

7 26.59 184.95 177.15 332.9

10 23.225 155.15 146.1 227.2

Page 103: Data Experiment Combine

TS 10% TS 1%

Time Solid Time Solid

0.5% 1% 1.5% 3% 0.5% 1% 1.5% 3%

0 2.9465 5.0485 3.8705 4.039 0 0.6732 0.3366 1.3465 0

2 50.995 75.14 169.2 924.5 2 0.5196 15.315 189.65 833.4

5 15.99 94.27 303.4 911.9 5 0 20.535 232.6 572.2

7 13.125 104.2 270.45 591.9 7 0 15.95 182.1 380.15

10 10.3 101.835 200.95 476.45 10 0.5049 12.62 156.35 210.35

TS 6%

Time Solid

0.5% 1% 1.5% 3%

0 1.0096 1.0913 1.01 0.8417

2 4.8805 84.45 284.75 1090.5

5 6.143 55.2 265.05 719.1

7 6.0585 45.44 186.55 507.4

10 4.8805 101.835 118.95 274.5

0 2 5 7 100

100

200

300

400

500

600

700

800

900

1000

1100

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

Page 104: Data Experiment Combine

0 2 5 7 100

100

200

300

400

500

600

700

800

900

1000

1100

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

Page 105: Data Experiment Combine

0 2 5 7 100

100

200

300

400

500

600

700

800

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

Page 106: Data Experiment Combine

0 2 5 7 100

100

200

300

400

500

600

700

800

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

Page 107: Data Experiment Combine

0 2 5 7 100

100

200

300

400

500

600

700

800

900

1000

1100

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

Page 108: Data Experiment Combine

0 2 5 7 100

100

200

300

400

500

600

700

800

900

1000

1100

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

Page 109: Data Experiment Combine

0 2 5 7 100

100

200

300

400

500

600

700

800

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

Page 110: Data Experiment Combine

0 2 5 7 100

100

200

300

400

500

600

700

800

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

Page 111: Data Experiment Combine

0 2 5 7 100

100

200

300

400

500

600

700

800

900

1000

1100

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

Page 112: Data Experiment Combine

0 2 5 7 100

100

200

300

400

500

600

700

800

900

1000

1100

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

Page 113: Data Experiment Combine

MF002

Target SolidsMass Container Mass Sample

10%35.76 300.23 264.47 1.32235

10%35.7 282.77 247.07 2.4707

10%35.39 295.09 259.7 3.8955

10% 35.98 290.42 254.44 7.6332MF006

Target SolidsMass Container Mass Sample

10%36.95 272.49 235.54 1.1777

10%35.79 288.46 252.67 2.5267

10%35.39 285.12 249.73 3.74595

10% 36.22 293.02 256.8 7.704

MF002

Target SolidsMass Container Mass Sample

7%35.68 282.37 246.69 1.23345

7%35.64 287.35 251.71 2.5171

7%37.58 262.84 225.26 3.3789

7%35.7 273.71 238.01 7.1403

MF006

Target SolidsMass Container Mass Sample

7%35.27 281.93 246.66 1.2333

7%36.35 278.18 241.83 2.4183

7%35.4 275.93 240.53 3.60795

7%35.33 258.67 223.34 6.7002

Mass Container + Sample

Mass Solidifier (theoretical)

Mass Container + Sample

Mass Solidifier (theoretical)

Mass Container + Sample

Mass Solidifier (theoretical)

Mass Container + Sample

Mass Solidifier (theoretical)

Page 114: Data Experiment Combine

MF002

Target SolidsMass Container Mass Sample

1%35.44 262.74 227.3 1.1365

1%35.96 280.31 244.35 2.4435

1%36.18 283.4 247.22 3.7083

1%35.84 278.21 242.37 7.2711

MF006

Target SolidsMass Container Mass Sample

1%35.46 283.85 248.39 1.24195

1%37.33 279.14 241.81 2.4181

1%35.59 278.87 243.28 3.6492

1%35.76 282.19 246.43 7.3929

Mass Container + Sample

Mass Solidifier (theoretical)

Mass Container + Sample

Mass Solidifier (theoretical)

Page 115: Data Experiment Combine

Mass Solidifier (actual)Solidifier used Target Solids

1.3 0.5

MF002

10%

2.48 110%

3.88 1.510%

7.64 3 10%

MF006

10%Mass Solidifier (actual)

1.15 0.510%

2.5158 110%

3.76 1.5 10%

7.7102 3

MF002

7%

7%

Mass Solidifier (actual) 7%

1.2398 0.5 7%

2.5017 1

MF006

7%

3.3716 1.5 7%

7.1367 3 7%

7%Mass Solidifier (actual)

1.269 0.5

MF002

1%

2.3996 11%

3.5623 1.51%

6.6994 31%

Percentage Solidifier (%)

Percentage Solidifier (%)

Percentage Solidifier (%)

Percentage Solidifier (%)

Page 116: Data Experiment Combine

MF006

1%

Mass Solidifier (actual) 1%

1.13 0.5 1%

2.4462 1 1%

3.708 1.5

7.2789 3

Mass Solidifier (actual)

1.2662 0.5

2.4171 1

3.6007 1.5

7.4042 3

Percentage Solidifier (%)

Percentage Solidifier (%)

Page 117: Data Experiment Combine

Mass Container Mass Sample

35.76 300.23 264.47 1.32235 1.3 0.5

35.7 282.77 247.07 2.4707 2.48 1

35.39 295.09 259.7 3.8955 3.88 1.5

35.98 290.42 254.44 7.6332 7.64 3

36.95 272.49 235.54 1.1777 1.15 0.5

35.79 288.46 252.67 2.5267 2.5158 1

35.39 285.12 249.73 3.74595 3.76 1.5

36.22 293.02 256.8 7.704 7.7102 3

35.68 282.37 246.69 1.23345 1.2398 0.5

35.64 287.35 251.71 2.5171 2.5017 1

37.58 262.84 225.26 3.3789 3.3716 1.5

35.7 273.71 238.01 7.1403 7.1367 3

35.27 281.93 246.66 1.2333 1.269 0.5

36.35 278.18 241.83 2.4183 2.3996 1

35.4 275.93 240.53 3.60795 3.5623 1.5

35.33 258.67 223.34 6.7002 6.6994 3

35.44 262.74 227.3 1.1365 1.13 0.5

35.96 280.31 244.35 2.4435 2.4462 1

36.18 283.4 247.22 3.7083 3.708 1.5

35.84 278.21 242.37 7.2711 7.2789 3

Mass Container + Sample

Mass Solidifier (theoretical)

Mass Solidifier (actual)

Percentage Solidifier (%)

Page 118: Data Experiment Combine

35.46 283.85 248.39 1.24195 1.2662 0.5

37.33 279.14 241.81 2.4181 2.4171 1

35.59 278.87 243.28 3.6492 3.6007 1.5

35.76 282.19 246.43 7.3929 7.4042 3

Page 119: Data Experiment Combine

MF006

No %TS %Solidifier TimeMass Solidifier Sludge

Container Target Actual Container

1 7% 1% 0 / 2 Min 4.6649 2 1.96 35.672 7% 1% 5 Min 4.6325 2 2 35.973 7% 1% 7 Min 4.8395 2 2.06 35.944 7% 1.5% 0 / 2 Min 4.9241 3 3 36.745 7% 1.5% 5 Min 4.8107 3 3.07 35.956 7% 1.5% 7 Min 4.7867 3 3 36.527 7% 3% 0 / 2 Min 4.8094 6 6.07 36.338 7% 3% 5 Min 4.939 6 6.13 37.499 7% 3% 7 Min 4.611 6 6.19 35.67

10 2% 1% 0 / 2 Min 4.6649 2 2.04 35.6711 2% 1% 5 Min 4.6325 2 2.01 35.9712 2% 1% 7 Min 4.8395 2 2.08 35.9413 2% 1.5% 0 / 2 Min 4.9241 3 3.01 36.7414 2% 1.5% 5 Min 4.8107 3 3.04 35.9515 2% 1.5% 7 Min 4.7867 3 2.95 36.5216 2% 3% 0 / 2 Min 4.8094 6 5.97 36.3317 2% 3% 5 Min 4.939 6 5.96 37.4918 2% 3% 7 Min 4.611 6 5.98 35.6719 1% 1% 0 / 2 Min 4.6649 2 2.14 35.6720 1% 1% 5 Min 4.6325 2 2.18 35.9721 1% 1% 7 Min 4.8395 2 2.05 35.9422 1% 1.5% 0 / 2 Min 4.9241 3 3.04 36.7423 1% 1.5% 5 Min 4.8107 3 3.07 35.9524 1% 1.5% 7 Min 4.7867 3 3.17 36.5225 1% 3% 0 / 2 Min 4.8094 6 6 36.3326 1% 3% 5 Min 4.939 6 6.12 37.4927 1% 3% 7 Min 4.611 6 6.08 35.67

Page 120: Data Experiment Combine

MF002Sludge % Solidifier

No %TS %SolidifierContainer + Sample Sample

Actual253.72 218.05 0.9% 1 7% 1%235.45 199.48 1.0% 2 7% 1%235.77 199.83 1.0% 3 7% 1%236.84 200.1 1.5% 4 7% 1.5%235.73 199.78 1.5% 5 7% 1.5%236.91 200.39 1.5% 6 7% 1.5%236.33 200 3.0% 7 7% 3%

237.3 199.81 3.1% 8 7% 3%235.87 200.2 3.1% 9 7% 3%227.27 191.6 1.1% 10 2% 1%254.92 218.95 0.9% 11 2% 1%238.64 202.7 1.0% 12 2% 1%241.43 204.69 1.5% 13 2% 1.5%236.54 200.59 1.5% 14 2% 1.5%240.04 203.52 1.4% 15 2% 1.5%222.25 185.92 3.2% 16 2% 3%238.25 200.76 3.0% 17 2% 3%248.78 213.11 2.8% 18 2% 3%230.83 195.16 1.1% 19 1% 1%235.99 200.02 1.1% 20 1% 1%235.14 199.2 1.0% 21 1% 1%

234 197.26 1.5% 22 1% 1.5%231.54 195.59 1.6% 23 1% 1.5%

238.9 202.38 1.6% 24 1% 1.5%231.09 194.76 3.1% 25 1% 3%238.14 200.65 3.1% 26 1% 3%257.45 221.78 2.7% 27 1% 3%

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TimeMass Solidifier Sludge % Solidifier

Container Target Actual Container Container + Sample SampleActual

0 / 2 Min 4.6649 2 2.0546 35.67 228.48 192.81 1.1%5 Min 4.6325 2 2.0282 35.97 241.85 205.88 1.0%7 Min 4.8395 2 2.0381 35.94 236.19 200.25 1.0%0 / 2 Min 4.9241 3 3.031 36.74 237.59 200.85 1.5%5 Min 4.8107 3 3.0123 35.95 240.48 204.53 1.5%7 Min 4.7867 3 2.9732 36.52 235.61 199.09 1.5%0 / 2 Min 4.8094 6 5.9943 36.33 241.53 205.2 2.9%5 Min 4.939 6 6.0038 37.49 252.05 214.56 2.8%7 Min 4.611 6 5.9475 35.67 252.83 217.16 2.7%0 / 2 Min 4.6649 2 2.01 35.67 247.59 211.92 0.9%5 Min 4.6325 2 2.05 35.97 249.35 213.38 1.0%7 Min 4.8395 2 2.0572 35.94 248.57 212.63 1.0%0 / 2 Min 4.9241 3 3.02 36.74 241.61 204.87 1.5%5 Min 4.8107 3 3.13 35.95 246.5 210.55 1.5%7 Min 4.7867 3 3.23 36.52 254.47 217.95 1.5%0 / 2 Min 4.8094 6 6.09 36.33 251.52 215.19 2.8%5 Min 4.939 6 6.25 37.49 249.99 212.5 2.9%7 Min 4.611 6 6.05 35.67 239.02 203.35 3.0%0 / 2 Min 4.6649 2 2.01 35.67 233.9 198.23 1.0%5 Min 4.6325 2 2.03 35.97 239.44 203.47 1.0%7 Min 4.8395 2 1.99 35.94 238.08 202.14 1.0%0 / 2 Min 4.9241 3 2.98 36.74 236.64 199.9 1.5%5 Min 4.8107 3 2.98 35.95 238.56 202.61 1.5%7 Min 4.7867 3 3 36.52 243.01 206.49 1.5%0 / 2 Min 4.8094 6 6.01 36.33 234.69 198.36 3.0%5 Min 4.939 6 5.96 37.49 238.6 201.11 3.0%7 Min 4.611 6 5.96 35.67 238.21 202.54 2.9%

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Total Solid Target Sample Sample MassDry Mass

% Solid Actual1 2 3 Average

10%A 4.8621 27.3275 22.4654 7.08179 7.0798 7.0826 7.081397 9.88%B 4.8565 27.9278 23.0713 7.14459 7.1456 7.14469 7.14496 9.92%

6%A 4.9164 34.6028 29.6864 6.8421 6.8346 6.8434 6.840033 6.48%B 4.9196 30.0862 25.1666 6.531 6.5333 6.5335 6.5326 6.41%

1%A 4.94 28.13 23.19 5.154 5.156 5.1586 5.1562 0.93%B 4.81 25.47 20.66 4.9466 4.938 4.9452 4.943267 0.65%

Container Mass

Container + Sample

Page 123: Data Experiment Combine

Rheometer Test

Solidifier Type MF006

Total Solid

Solidifier Concentration

0 Minute

0% 1% 1.5% 3.0%

3%0.3366 1.01 19.35 370.2

2%0.3366 37.82 48.47 640.5

1%0 3.029 16.66 390.1

Total Solid

Solidifier Concentration

2 Minute

0% 1% 1.5% 3.0%

10%0.3366 55.54 420.9 117.1

6%0.6732 331.7 502.9 1114

1%0 177.4 323.5 620

Total Solid

Solidifier Concentration

5 Minute

Page 124: Data Experiment Combine

Total Solid 0% 1% 1.5% 3.0%

5 Minute

10%0.3366 192.5 606.4 960.3

6%1.01 171.7 625.4 893.3

1%0 145.7 393.8 630.1

Page 125: Data Experiment Combine

Total Solid

Solidifier Concentration

7 Minute

0% 1% 1.5% 3.0%

10%0.3366 198.6 503 1127

6%1.01 337.3 619.7 844.2

1%0 172.3 359.5 664.4

Rheometer Test

Solidifier Type MF002

Total Solid

Solidifier Concentration

0 Minute

0% 1% 1.5% 3.0%

10%0 63.28 90.21 182.9

6%0.3366 6.395 25.92 105.7

1%0 0.6732 6.75 100.6

Page 126: Data Experiment Combine

Total Solid

Solidifier Concentration

2 Minute

0% 1% 1.5% 3.0%

10%0 111.4 210.7 725.4

6%0.3366 68.66 210.4 867.4

1%0.6732 42.75 109.4 862

Total Solid

Solidifier Concentration

5 Minute

0% 1% 1.5% 3.0%

10%4.712 129.6 159.2 937.1

6%0 74.72 224.8 1112

1%0.6732 35.01 235.9 854.4

Total Solid

Solidifier Concentration

7 Minute

0% 1% 1.5% 3.0%

10%5.049 135 192.5 499.2

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6%0 107 198.3 1167

7 Minute

1%1.01 63.62 271 989.6

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TS 3% TS 1%

Time Solid Time Solid

0% 1% 1.5% 3.0% 0% 1% 1.5% 3.0%

0 0.3366 1.01 19.35 370.2 0 0 3.029 16.66 390.1

2 0.3366 55.54 420.9 117.1 2 0 177.4 323.5 620

5 0.3366 192.5 606.4 960.3 5 0 145.7 393.8 630.1

7 0.3366 198.6 503 1127 7 0 172.3 359.5 664.4

TS 2%

Time Solid

0% 1% 1.5% 3.0%

0 0.3366 37.82 48.47 640.5

2 0.3366 331.7 502.9 1114

5 0.3366 171.7 625.4 893.3

7 0.3366 337.3 619.7 844.2

Page 129: Data Experiment Combine

TS 3% TS 1%

Time Solid Time Solid

0% 1% 1.5% 3.0% 0% 1% 1.5% 3.0%

0 0 63.28 90.21 182.9 0 0 0.6732 6.75 100.6

0 2 5 70

100

200

300

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500

600

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800

900

1000

1100

TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

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2 0 111.4 210.7 725.4 2 0.6732 42.75 109.4 862

5 4.712 129.6 159.2 937.1 5 0.6732 35.01 235.9 854.4

7 5.049 135 192.5 499.2 7 1.01 63.62 271 989.6

TS 2%

Time Solid

0% 1% 1.5% 3.0%

0 0.3366 6.395 25.92 105.7

2 0.3366 68.66 210.4 867.4

5 0 74.72 224.8 1112

7 0 107 198.3 1167

0 2 5 70

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TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

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TS 3%, S 1%TS 3%, S 1.5%TS 3%, S 3%TS 2%, S 1%TS 2%, S 1.5%TS 2%, S 3%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

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TS 3%, S 1%TS 3%, S 1.5%TS 3%, S 3%TS 2%, S 1%TS 2%, S 1.5%TS 2%, S 3%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

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TS 3%, S 1%TS 3%, S 1.5%TS 3%, S 3%TS 2%, S 1%TS 2%, S 1.5%TS 2%, S 3%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

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TS 3%, S 1%TS 3%, S 1.5%TS 3%, S 3%TS 2%, S 1%TS 2%, S 1.5%TS 2%, S 3%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%

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TS 10%, S 0.5%TS 10%, S 1%TS 10%, S 1.5%TS 10%, S 3%TS 6%, S 0.5%TS 6%, S 1%TS 6%, S 1.5%TS 6%, S 3%TS 1%, S 0.5%TS 1%, S 1%TS 1%, S 1.5%TS 1%, S 3%