An Introduction to Infrared
29
An Introduction to An Introduction to Infrared Infrared By: By: Lalita Chopra Lalita Chopra Assistant Professor Assistant Professor Chemistry Chemistry
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An Introduction to Infrared
Transcript of An Introduction to Infrared
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An Introduction to InfraredBy:Lalita ChopraAssistant ProfessorChemistry
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THE ELECTROMAGNETIC SPECTRUM
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WHAT IS SPECTROSCOPY?Atoms and molecules interact with electromagnetic radiation (EMR) in a wide variety of ways.Atoms and molecules may absorb and/or emit EMR.Absorption of EMR stimulates different types of motion in atoms and/or molecules.The patterns of absorption (wavelengths absorbed and to what extent) and/or emission (wavelengths emitted and their respective intensities) are called spectra.The field of spectroscopy is concerned with the interpretation of spectra in terms of atomic and molecular structure (and environment).
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INFRARED SPECTROSCOPYInfrared radiation stimulates molecular vibrations.Infrared spectra are traditionally displayed as %T (percent transmittance) versus wave number (4000-400 cm-1).Useful in identifying presence or absence of functional groups.
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INFRARED SPECTROSCOPYWavenumber = 1/ wavelength
Chart1
93.65889
95.36569
97.10359
97.98438
98.87316
98.87316
98.87316
92.81699
91.1558
95.36569
97.98438
91.98264
91.98264
92.81699
90.3364
91.98264
97.10359
96.23072
84.80311
81.79476
90.3364
99.77
99.77
98.87316
93.65889
92.81699
91.98264
82.53669
82.53669
95.36569
99.77
91.1558
76.78467
75.41042
86.34852
88.7196
91.1558
95.36569
76.78467
68.89944
78.18396
95.36569
90.3364
83.28535
73.39503
72.08145
81.0595
95.36569
95.36569
78.89314
73.39503
81.79476
94.50844
91.1558
90.3364
87.13176
85.57233
85.57233
84.0408
59.63079
46.72919
48.01234
62.38475
71.4335
81.79476
86.34852
80.33085
78.18396
84.0408
90.3364
88.7196
79.60875
70.15503
72.08145
81.0595
77.48116
78.18396
84.80311
90.3364
90.3364
88.7196
82.53669
68.89944
66.45527
76.78467
90.3364
91.98264
84.80311
77.48116
78.18396
84.0408
81.0595
76.78467
65.26589
35.31991
21.30157
27.92922
48.8873
45.48032
37.62449
48.8873
74.06077
81.79476
75.41042
72.73528
69.5244
66.45527
56.48604
46.30913
36.28978
26.45632
28.43819
45.07149
67.05806
75.41042
78.89314
78.89314
68.89944
54.48223
48.44785
58.56356
74.73255
77.48116
70.15503
58.56356
55.97829
59.09476
61.82396
55.47509
37.96576
27.92922
36.61895
60.71748
70.79138
75.41042
87.13176
89.52435
88.7196
88.7196
89.52435
90.3364
90.3364
89.52435
87.9221
83.28535
80.33085
81.79476
87.9221
64.0978
51.14508
60.17168
89.52435
84.80311
82.53669
81.0595
79.60875
76.09444
65.85789
45.89285
27.42936
19.99681
24.83582
43.4726
66.45527
75.41042
76.78467
76.09444
52.5495
33.45724
31.98029
46.30913
61.82396
78.18396
86.34852
86.34852
86.34852
88.7196
91.1558
90.3364
89.52435
88.7196
89.52435
90.3364
91.98264
92.81699
91.98264
91.98264
92.81699
93.65889
93.65889
93.65889
93.65889
93.65889
93.65889
93.65889
93.65889
92.81699
93.65889
94.50844
94.50844
93.65889
93.65889
94.50844
93.65889
92.81699
92.81699
92.81699
92.81699
92.81699
93.65889
93.65889
93.65889
93.65889
93.65889
93.65889
94.50844
94.50844
94.50844
93.65889
93.65889
93.65889
94.50844
93.65889
93.65889
93.65889
92.81699
92.81699
92.81699
92.81699
92.81699
92.81699
92.81699
92.81699
91.98264
91.98264
91.98264
91.1558
91.1558
91.1558
90.3364
90.3364
90.3364
90.3364
89.52435
89.52435
88.7196
88.7196
87.9221
87.9221
87.13176
86.34852
85.57233
85.57233
85.57233
84.80311
84.80311
84.0408
84.0408
83.28535
83.28535
81.79476
81.0595
80.33085
79.60875
78.18396
76.78467
75.41042
74.06077
72.73528
71.4335
69.5244
68.28009
68.89944
70.15503
70.15503
68.28009
65.85789
66.45527
69.5244
70.79138
70.79138
70.15503
69.5244
68.28009
67.05806
65.85789
65.26589
65.26589
65.85789
65.85789
64.67921
64.0978
66.45527
69.5244
71.4335
71.4335
72.08145
71.4335
70.79138
70.15503
70.15503
68.89944
67.66632
65.26589
62.95062
60.17168
57.51542
54.48223
48.44785
36.9511
23.95478
18.94224
20.92033
25.51779
28.69614
29.21909
25.28841
21.11009
16.84422
12.16955
9.976999
11.73784
16.69281
19.46238
19.11406
22.08503
31.40792
43.08183
51.14508
54.48223
56.48604
58.03712
59.63079
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61.26822
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97.98438
97.98438
97.98438
97.98438
98.87316
98.87316
98.87316
98.87316
98.87316
98.87316
98.87316
97.98438
97.10359
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98.87316
98.87316
98.87316
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
99.77
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99.77
98.87316
98.87316
98.87316
98.87316
98.87316
98.87316
98.87316
98.87316
98.87316
98.87316
98.87316
98.87316
98.87316
wavenumber/ cm-1
%T
Aspirin (acetylsalicylic acid)
N-methylaniline
4.55E+029.37E+01
4.63E+029.54E+01
4.71E+029.71E+01
4.78E+029.80E+01
4.86E+029.89E+01
4.94E+029.89E+01
5.01E+029.89E+01
5.09E+029.28E+01
5.17E+029.12E+01
5.25E+029.54E+01
5.32E+029.80E+01
5.40E+029.20E+01
5.48E+029.20E+01
5.55E+029.28E+01
5.63E+029.03E+01
5.71E+029.20E+01
5.79E+029.71E+01
5.86E+029.62E+01
5.94E+028.48E+01
6.02E+028.18E+01
6.09E+029.03E+01
6.17E+029.98E+01
6.25E+029.98E+01
6.33E+029.89E+01
6.40E+029.37E+01
6.48E+029.28E+01
6.56E+029.20E+01
6.63E+028.25E+01
6.71E+028.25E+01
6.79E+029.54E+01
6.87E+029.98E+01
6.94E+029.12E+01
7.02E+027.68E+01
7.10E+027.54E+01
7.17E+028.63E+01
7.25E+028.87E+01
7.33E+029.12E+01
7.41E+029.54E+01
7.48E+027.68E+01
7.56E+026.89E+01
7.64E+027.82E+01
7.71E+029.54E+01
7.79E+029.03E+01
7.87E+028.33E+01
7.95E+027.34E+01
8.02E+027.21E+01
8.10E+028.11E+01
8.18E+029.54E+01
8.25E+029.54E+01
8.33E+027.89E+01
8.41E+027.34E+01
8.49E+028.18E+01
8.56E+029.45E+01
8.64E+029.12E+01
8.72E+029.03E+01
8.79E+028.71E+01
8.87E+028.56E+01
8.95E+028.56E+01
9.03E+028.40E+01
9.10E+025.96E+01
9.18E+024.67E+01
9.26E+024.80E+01
9.33E+026.24E+01
9.41E+027.14E+01
9.49E+028.18E+01
9.57E+028.63E+01
9.64E+028.03E+01
9.72E+027.82E+01
9.80E+028.40E+01
9.87E+029.03E+01
9.95E+028.87E+01
1.00E+037.96E+01
1.01E+037.02E+01
1.02E+037.21E+01
1.03E+038.11E+01
1.03E+037.75E+01
1.04E+037.82E+01
1.05E+038.48E+01
1.06E+039.03E+01
1.06E+039.03E+01
1.07E+038.87E+01
1.08E+038.25E+01
1.09E+036.89E+01
1.10E+036.65E+01
1.10E+037.68E+01
1.11E+039.03E+01
1.12E+039.20E+01
1.13E+038.48E+01
1.13E+037.75E+01
1.14E+037.82E+01
1.15E+038.40E+01
1.16E+038.11E+01
1.16E+037.68E+01
1.17E+036.53E+01
1.18E+033.53E+01
1.19E+032.13E+01
1.20E+032.79E+01
1.20E+034.89E+01
1.21E+034.55E+01
1.22E+033.76E+01
1.23E+034.89E+01
1.23E+037.41E+01
1.24E+038.18E+01
1.25E+037.54E+01
1.26E+037.27E+01
1.27E+036.95E+01
1.27E+036.65E+01
1.28E+035.65E+01
1.29E+034.63E+01
1.30E+033.63E+01
1.30E+032.65E+01
1.31E+032.84E+01
1.32E+034.51E+01
1.33E+036.71E+01
1.33E+037.54E+01
1.34E+037.89E+01
1.35E+037.89E+01
1.36E+036.89E+01
1.37E+035.45E+01
1.37E+034.84E+01
1.38E+035.86E+01
1.39E+037.47E+01
1.40E+037.75E+01
1.40E+037.02E+01
1.41E+035.86E+01
1.42E+035.60E+01
1.43E+035.91E+01
1.43E+036.18E+01
1.44E+035.55E+01
1.45E+033.80E+01
1.46E+032.79E+01
1.47E+033.66E+01
1.47E+036.07E+01
1.48E+037.08E+01
1.49E+037.54E+01
1.50E+038.71E+01
1.50E+038.95E+01
1.51E+038.87E+01
1.52E+038.87E+01
1.53E+038.95E+01
1.54E+039.03E+01
1.54E+039.03E+01
1.55E+038.95E+01
1.56E+038.79E+01
1.57E+038.33E+01
1.57E+038.03E+01
1.58E+038.18E+01
1.59E+038.79E+01
1.60E+036.41E+01
1.60E+035.11E+01
1.61E+036.02E+01
1.62E+038.95E+01
1.63E+038.48E+01
1.64E+038.25E+01
1.64E+038.11E+01
1.65E+037.96E+01
1.66E+037.61E+01
1.67E+036.59E+01
1.67E+034.59E+01
1.68E+032.74E+01
1.69E+032.00E+01
1.70E+032.48E+01
1.70E+034.35E+01
1.71E+036.65E+01
1.72E+037.54E+01
1.73E+037.68E+01
1.74E+037.61E+01
1.74E+035.25E+01
1.75E+033.35E+01
1.76E+033.20E+01
1.77E+034.63E+01
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1.78E+037.82E+01
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1.98E+039.45E+01
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2.00E+039.37E+01
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2.06E+039.28E+01
2.07E+039.37E+01
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2.10E+039.37E+01
2.11E+039.37E+01
2.11E+039.45E+01
2.12E+039.45E+01
2.13E+039.45E+01
2.14E+039.37E+01
2.14E+039.37E+01
2.15E+039.37E+01
2.16E+039.45E+01
2.17E+039.37E+01
2.18E+039.37E+01
2.18E+039.37E+01
2.19E+039.28E+01
2.20E+039.28E+01
2.21E+039.28E+01
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2.22E+039.28E+01
2.23E+039.28E+01
2.24E+039.28E+01
2.24E+039.28E+01
2.25E+039.20E+01
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2.27E+039.20E+01
2.28E+039.12E+01
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2.92E+039.98E+00
2.93E+031.17E+01
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3.00E+035.65E+01
3.01E+035.80E+01
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3.44E+039.89E+01
3.45E+039.89E+01
3.46E+039.89E+01
3.46E+039.89E+01
3.47E+039.89E+01
3.48E+039.80E+01
3.49E+039.71E+01
3.49E+039.80E+01
3.50E+039.89E+01
3.51E+039.89E+01
3.52E+039.89E+01
3.53E+039.98E+01
3.53E+039.98E+01
3.54E+039.98E+01
3.55E+039.98E+01
3.56E+039.98E+01
3.56E+039.98E+01
3.57E+039.98E+01
3.58E+039.98E+01
3.59E+039.98E+01
3.59E+039.98E+01
3.60E+039.98E+01
3.61E+039.98E+01
3.62E+039.98E+01
3.63E+039.98E+01
3.63E+039.98E+01
3.64E+039.98E+01
3.65E+039.98E+01
3.66E+039.98E+01
3.66E+039.98E+01
3.67E+039.98E+01
3.68E+039.98E+01
3.69E+039.98E+01
3.70E+039.98E+01
3.70E+039.98E+01
3.71E+039.98E+01
3.72E+039.98E+01
3.73E+039.98E+01
3.73E+039.98E+01
3.74E+039.98E+01
3.75E+039.98E+01
3.76E+039.98E+01
3.76E+039.98E+01
3.77E+039.98E+01
3.78E+039.98E+01
3.79E+039.98E+01
3.80E+039.98E+01
3.80E+039.98E+01
3.81E+039.98E+01
3.82E+039.98E+01
3.83E+039.98E+01
3.83E+039.98E+01
3.84E+039.98E+01
3.85E+039.98E+01
3.86E+039.98E+01
3.86E+039.98E+01
3.87E+039.98E+01
3.88E+039.98E+01
3.89E+039.98E+01
3.90E+039.98E+01
3.90E+039.89E+01
3.91E+039.89E+01
3.92E+039.89E+01
3.93E+039.89E+01
3.93E+039.89E+01
3.94E+039.89E+01
3.95E+039.89E+01
3.96E+039.89E+01
3.96E+039.89E+01
3.97E+039.89E+01
3.98E+039.89E+01
3.99E+039.89E+01
4.00E+039.89E+01
N-methylaniline
wavenumber/ cm-1
%T
Aspirin (acetylsalicylic acid)
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INFRARED SPECTROSCOPYIn the IR region of the electromagnetic spectrum, the absorption of radiation by a sample is due to changes in the vibrational energy states of a molecule.
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INFRARED SPECTROSCOPYMethane
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INFRARED SPECTROSCOPYOnly vibrations that cause a change in polarity give rise to bands in IR spectra which of the vibrations for CO2 are infrared active?Symmetric stretch
Asymmetric stretch
Bending (doubly degenerate)
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INFRARED SPECTROSCOPYWhat is a vibration in a molecule?Any change in shape of the molecule- stretching of bonds, bending of bonds, or internal rotation around single bonds
What vibrations change the dipole moment of a molecule?Asymmetrical stretching/bending and internal rotation change the dipole moment of a molecule. Asymmetrical stretching/bending are IR active.
Symmetrical stretching/bending does not. Not IR active
-
INFRARED SPECTROSCOPYHuman Breath
Chart2
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