123447504 Chemistry Investigatory Project

15
SUBMITTED BY: ALOK KUMAR XII ‘A’ K.V. NO.1,Gandhinagar CHEMISTRY INVESTIGATORY PROJECT AISSCE CHEMISTRY INVESTIGATORY PROJECT

description

qfwwtewyreutiyrlut;kyrjhegsfawdfeghr5juei6ku5y4tf

Transcript of 123447504 Chemistry Investigatory Project

Page 1: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

SUBMITTED BY:

ALOK KUMARXII ‘A’K.V. NO.1,Gandhinagar

CHEMISTRY

INVESTIGATORY

PROJECT

AISSCE

Page 2: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

2

Laboratory certificate

This is to certify that ALOK KUMAR of class XII (Science) Roll No has success fully completed his investigatory project in chemistry prescribed by the Central Board of Secondary Education (CBSE) in chemistry laboratory of Kendriya Vidyalaya No 1, Sector 30, Gandhinagar during the year 2012-13.External Examiner Subject Teacher

…………………………. ..………………………

Page 3: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

3

LABORATORY CERTIFICATE

Page 4: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

4

ACKNOWLEDGEMENT

This project is prepared by ALOK KUMAR of class XII in Kendriya Vidyalaya No 1, Sector 30, Gandhinagar under the guidance of our chemistry teachers,

Mr. AK JHA Mrs. ANITA NAIR

Page 5: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

5

AIMTO PREPARE

Urea FORMALDEHYDE RESIN (BAKELITE)

Page 6: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

6

• Formation and structure• Urea-formaldehyde resins, as

a group, are formed by a step-growth polymerization reaction that can be either acid- or base-catalyzed.

• Urea is reactive towards formaldehyde at the ortho and para sites (sites 2, 4 and 6) allowing up to 3 units of formaldehyde to attach to the ring. The initial reaction is formation of a hydroxymethyl Urea:

• HOC6H5 + CH2O → HOC6H4CH2OH

PREFACE

Page 7: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

7

• The hydroxymethyl group is capable of reacting with either another free ortho or para site, or with another hydroxymethyl group. The first reaction gives a methylene bridge, and the second forms an ether bridge:

• HOC6H4CH2OH + HOC6H5 → (HOC6H4)2CH2 + H2O

• The diUrea (HOC6H4)2CH2  is called bisUrea F. BisUrea-F can further link generating tri- and tetra-and higher Urea oligomers.

• 2 HOC6H4CH2OH → (HOC6H4CH2)2O

+ H2O

Page 8: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

8

DIAGRAM

Page 9: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

9

Urea FORMALDEHYDE RESIN (BAKELITE)

Page 10: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

10

REQUIREMENTS

• Beaker • Urea• Conc. HCl • Dropper• Water • Rod• Filter paper• Formaldehyd

e

Page 11: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

11

THEORY• Urea resins are

condensation polymerization products of Ureaic derivatives with aldehyde such as formaldehyde.

• Most important member of this class is Bakelite, Urea formaldehyde resin.

• Its prepared by condensing Urea with formaldehyde in the presence of acidic or basic catalyst.

Page 12: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

12

PROCEDURE

• Take 5 ml of glacial acetic acid and 2.5 ml of 40% formaldehyde in a beaker.

• Add 2.5g of Urea into it.• Cover the beaker with

watch glass or filter paper.• Add few drops of HCl to it

and place it on hot plate.• Pink mass will be formed

in the beaker.• Wash, dry and weigh the

product formed.

Page 13: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

13

RESULT

• Pink mass i.e. Urea formaldehyde (Bakelite) is yielded.

Page 14: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

14

PRECAUTIONS

• The reaction is sometimes vigorous and it is better to be little away from the beaker while adding conc. HCl.

• Urea should be stirred in the formaldehyde solution for at least 10 mints to make it a saturated solution.

• Conc. hydrochloric acid should be added drop wise carefully.

Page 15: 123447504 Chemistry Investigatory Project

CHEMISTRY INVESTIGATORY PROJECT

15

THE END