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Title PIQ8

Sllneia a.-leal Oolp. Site r.c:..u, •

u.s. IPA, a.gian I ~&IniON Dlviaion

llater Section

~~ U.S. IPA, Rlgion 1 11118ta llai'JIQIL ITt Diviaion cr a.perf\RS a.ctJ.on .Joellalat

Office OCQuality ~·

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1. Project Name: Silreala Cheaical Corp. Site. Lovell. MA

2. Project lequeated By: Heather Pord/Joel Bal .. t

3. Date of lequeat:

4. Date of Project Initiation: June 4. 1987

' 5. Project Officer: Joel Bal .. t

6. Project Deacription

A. Object he and Scope State•nt: To collect aotl a...,lea for diox:iftl and furaa~. 'l'be acope of tba 11lftltilation will be preliainary in nature to deteraiae if dioxiftl ud farlftl are preaent at tbe Site. Soil aaplea for PCB aDd Mtal acnniq will alao be taken. Put data for otber bOVD contudaanta and their loeatioa~. aa wll aa but eqiaeerlq judleMnt • will be uaed to deteraiae the aapliftl locatloa~ on alte.

B. Data Uaye: Data will be uaed to datendne lf tba coatainaota of COQcem are pre .. nt • aboft detecttcm Uaita at tba aapliftl loeatioa~. aad rilk uaua•ot for 1011 upoeun.

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c. Monitoring Network Deaign and Rationale: A total of a leaat eight a .. plea vill be collected vith at leaat oae duplicate and one perforunce evaluation aaaple. lo-15 aaaplea vill be taken for PCB and Mtal acreening at lSD. The objective• of the aaapling are: 1) to -.alidate queationable dioun data froa preri.oua aoil ••pling, and 2) to determne if diod.n/ furan containation euata outatde of the cruabed atoae area in the aoutbeut comer of the Site. S) To eYaluate Mtala

' and PCB aoil containation in aelect locationa. Dioxin aa.plea vill be collected at locationa indicated on the attached up, exact loeationa vill be detemaed on-aite. Metala/PCB ••pling location• vill be determned on-aite baaed on flald judpMnta.

D. Monitoring ParaMtere and their rrequencJ of Collecttonz

Diouna and lurana Metala and PCB Screeniq

I. ParaMter Table

._bar of Par-ter laiiPlea la!2le Matrix

dioxina • 8+4 QA/QC aoil furaDI

•tala lo-U+2 aoil field dup.

PCB 1o-U+2 aotl field dup •

ADalztical Met bOd l!!ele

.. lernc:e Pnaenatioa

CLP •dtfted tea Metbod 8280

See table 1 tea

lee table 1 tc

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aouw tiM

21 dAJI

6 •ntu

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ParaMter

Arocolor - 1016 Aroc:olor - 1221 Arocolor - 1232 Aroc:olor - 1242 Arocolor - 1248 Aroc:olor - 1254 Arocolor - 1260 Arocolor - 1262 Arocolor - 1268

Cr .. ... C4 Pb

Table 1

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Analztical Method

8080 8080 8080 8080 8080 8080 8080 8080 8080

7090 7060 7471 7130 7420

Det. Lildt

.02 ( .. /ka)

.03

.02

.02

.02

.01

.01

.01

.01

10 (UI/1) 1

.2 .10 10

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7. Schedule of Taeka and Product•

Data Activity

April 6 l!litiate Project/Dawelop Vork/QA Plan

June 4 Conduct Sapllq and Dallwery of Sapl• to Lab

June 4-2S Lab Analy1i1 of Saplee

June 25-July 2 Data Validated

July 3 Validated Data Preeented to Joel lalut

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8. Project Or1an1aation and leaponaibility

The,folloVinl ia a liat of k., project peraonnel and their correapondins r .. ponaibilitiea:

Sa8plina Operation• - Cary Lipaon

SaiiPliDI QC - Cary Lipaon

Laboratory AllalJ11a - CLP • lSD (acreenins)

Laboratory QC - CLP 6 lSD (acreeniq)

Data Proc .. ains Activitiea - lSD

Overall lielcl QA - Gary Lipaon

Oftrall Project Coordination - Joel lalut

(lote: AD orsaniaational chart abould be aupplied with tbia plan.)

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9. Data Quality RequireMnta and Aleeee•nta

CLP Lab will follow contract require .. nte.

BSD - In-Bouse QC will be followed.

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Data Coi!J)arability: Data au•t be c011parable for all •oil uaple location•. All aaaplea will be analysed by the •aae •thod with the ••.e detection liait. Data Co!fletene••= 80 percent coapletene••• al•o the Perfor.ance !valuation •a.ple and the duplicate a .. ple cannot be loat.

10. Sa!plins Procedure•: Saapling Guidance Manual for Rational Dioxin Study (July. 1984). For .. tal •creeniDI and PCB• - aee attached procedure••

11. Ba!ple Cuatody Procedure•: IPA, ... ion I, lSD Vater Section'• Chain of Cuatody Procedure• will be followed.

12. Calibration Procedure• and Preventive Maintenance: lo field eqUlpaent requirins calibration will be uaed.

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13. Doc:uMntation, Data Reduction, and Reportiag

A. DoCUMntation: All Sita aaapllag actbitiea, ineludiq aupliag loeationa, will be doc:u•nted bJ Vater Section pereonnel.

1. Data Reduction and leportins: law data will be ~riaed and incorporated into report for. bJ Vater Section peraonnel. 'l'be final report will include at a aini- a a..-ry of the Site aaapllnc activitiea and the final QC'D anal11i• reaulta. A draft report of the Site aaapliag activitiea will be forwarded to Joel lalut at the coapletion of tbe field work.

14. Data Validation& Data validation for the diozin/furan analyaia vill be conducted by llio Goffi, lSD.

!be lSD Laboratory Cbaaieal Section will validate the PCI and •tal data.

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15. Corrective Action: 'l'be CLP baa eorreetive aetion built into it to prevent an out of control aituation onee tbe a.-plea are into tbe Laboratory Analytical Proee11. 'l'bia will be followed linea all aaple1 are to be analysed by CLP.

lSD: Data will be qualified to reflect any abnoraal quality control reaultl.

Ooee data 11 received by project officer it will be bi1 deci1ioo if corrective action 11 to include reaaaplins.

16. Iaporta: 'l'be final report 11 to pruented to:

Joel lalaat, bMdial Project Manqer CT Superfund Section (RIC) Vaate Hanqe•nt Dlrilion

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Sa.pling Procedure• for Soil Collection IPA Region I

Surveilllnce and ADaly1i1 Divieion - Water Section

Netall: A ainiaaa of 100 au per eaaple ehall be collected for the ecreening of •tale. Thi1 will be collected in an acid vuhecl glue container ( 1. W&lhed in laboratoi'J ,racle

'deteraent: 2. rinaed with 1:2 BCl: 3. rinaed with tap water: 4. rinaed with 1:2 IIN03: 5. riDiecl with tap water: 6. riDied with dietillecl water). !be container will be capped with teflon. Baapliq tooll ahall 1ae aev voocl or plaetic apatul .. or apooDI. If thaae will not penetrate the JI'OUDd aurface, then acid vaabecl ataialeae ateel aball 1ae uaed.

PCBa: A ainiaaa of 100 1• per aa.ple a hall be collected for the cleteraination of polychlorinated bipbenyll (PCia). Thi1 will be collected in a aobent rinaecl 1laaa container (1. aoak in cb ... olv for 10 ainutee: 2. rt01e three tiMe with tap water: 3. rinae three ti•• with acetone: 4. rtnae three tiMe with hexane: 5. air di'J: 6. cap with teflon which ... cleaned with acetone, hexane and baked at no• for 2 boura). Baapling to6la ahall be eolvent r1Diecl atainleaa ateel apoona or apatulaa.

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barcode: *569047*barcodetext: SDMS Doc ID 569047