Wisconsin Department of Natural Resources Laboratory · PDF filea, i,. I e~ Wisconsin...

22
a, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790 Sample: 26Z$35001 P(lge I of 22 £&bor¢Jory.. Wisconsin state Laboratory of Hygiene 2601 Agriculture Dr Madison P/zo7je.. 8004424618 Sample: Fz.e/d #.' MW1010P Collection start: 06lz8/2016 07..50 aim CoJ/ecfec7 6v`.' ZOE MCMANAMA D#., 03180 Cot/#ty.. Rusk VI 53718 Fcac p¢oj?e .. 608-224-6213 I)IVR JD 113133790 Scz7xpJe #.. 262935001 Collection End.. 06/Z8/2016 0]..50 a.in waterbody/Ouif ell Id: ID Point #: Ac.count #.. WAj063 Sc7#ip/€ £ocafz.o7z.. FLAMBEAu hHNE S'c!7xp/e I)escr7Pfro72.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE Siimple soui`ce.. Mon±torin8Wch Sample Depth.. N I)czre jtepor/ed`. 08/08/2016 S'cifxp/e s'/cltrs.. COMPLETE Project No: Sanple Reasorl: Comment: Analyses and Resuits: 4nelysis Method Analysis Dale Lab Coniment EPA 200.7 06/30/2016 C:ode Deschption Re!sult Units LOD Report Limit LOQ 1005 BAREM DISS 0.0444 MGfu 0.00100 0-00300 915 cALcrolvI Dlss 47.0 MGth 0.100 0.300 1030 CHROMIUM I)ISS ND ugth 1.00 3.00 1040 COPPER DISS ND ugth 5.00 15.0 46570 HARDNESS, CA MG CALCULATEI) 171 MGth 0.660 2.00 (MGn As cAco3)

Transcript of Wisconsin Department of Natural Resources Laboratory · PDF filea, i,. I e~ Wisconsin...

Page 1: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

a, i,. I e~

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: 113133790 Sample: 26Z$35001 P(lge I of 22

£&bor¢Jory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadisonP/zo7je.. 8004424618

Sample:

Fz.e/d #.' MW1010PCollection start: 06lz8/2016 07..50 aim

CoJ/ecfec7 6v`.' ZOE MCMANAMAD#., 03180

Cot/#ty.. Rusk

VI 53718Fcac p¢oj?e .. 608-224-6213

I)IVR JD 113133790

Scz7xpJe #.. 262935001

Collection End.. 06/Z8/2016 0]..50 a.inwaterbody/Ouif ell Id:

ID Point #:Ac.count #.. WAj063

Sc7#ip/€ £ocafz.o7z.. FLAMBEAu hHNES'c!7xp/e I)escr7Pfro72.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE

Siimple soui`ce.. Mon±torin8Wch Sample Depth.. NI)czre jtepor/ed`. 08/08/2016 S'cifxp/e s'/cltrs.. COMPLETE

Project No: Sanple Reasorl:Comment:

Analyses and Resuits:

4nelysis Method Analysis Dale Lab Coniment

EPA 200.7 06/30/2016C:ode Deschption Re!sult Units LOD Report Limit LOQ

1005 BAREM DISS 0.0444 MGfu 0.00100 0-00300

915 cALcrolvI Dlss 47.0 MGth 0.100 0.300

1030 CHROMIUM I)ISS ND ugth 1.00 3.00

1040 COPPER DISS ND ugth 5.00 15.0

46570 HARDNESS, CA MG CALCULATEI) 171 MGth 0.660 2.00

(MGn As cAco3)

Page 2: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: 1T3133790 Sample: 26Z935001 Page 2 Of 22

Code Description Resul[ Units LOD Raport Liinit LOQ1046 IRON DISS ND MGEL 0.loo 0.300

925 MAGNEslun¢ Dlss 13.0 MGth 0.loo 0.300

1056 MANGANESE DISS 63.2 ugEL 1.00 3.00

1145 SELENIUM DISS ND ugth 10.0 30.0

1075 SILVER DISS ND ugth 2.00 6.00

logo ZINC DISS 7.29 ugth 5.00 15.0

nalysis Me{liod Aiialysis Date Lab comment

SM2540C 07/05/2016Code Descrip{iorl Result Urlits LOD Report Liriiil LOQ70300 RESIDUE DISS 180C (TOTAL 208 MGth 50,0 50.0

DISSOLVED SOLIDS)

iialysis Method `drlalysis Date L{ib corirment

sM25 1 oBI]PAi 5o. 1 ,sM23 2oB o6rso/2 oi 6Code Description Res{ilt Units LOD Repon Linii[ LOQ410 ALKALINITy TOTAL CAc03 154 MGn, 2.55 2.55

95 CONDUCTIVITY, UMHOS/CM @ 360 uS/cm 10.0 10.025C

403 PHLAB 7.75 SU i.00 I.00

nalysis Method A}ralvsis Date Lab corrrmenl

SM3113B 07/08/2016Code Description Resttlt Units LOD Report Linrit LOQ1025 CADMIUMDISS NI) ugth 0.0500 0,150

rlalysis Method Analysis Dale Lab comment

EPA 245.I 06/29/2016:ode Description Result Units LOD Report Limit LOQ

71890 MERCURY DISS ND ugEL 0.030 0.080

Page 3: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

08/08/2016

Wisconsin Department of Natural ResourcesLaboratory Report

Z4Z...113133790 5'c}mp/e.. 262935002 Pc/g€ 3 a/22

I,flbormfory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadisonP/!o«e.. 8004424618

Sample:

Field #: NIW10L3Collection start.. 06/Z81201610..1S z`m

Co/jcc/ec/ bv..' ZOE MCMANAMAID#.. 03180

Coit#ty.. Rusk

VI 53718Fc£[ P¢oF?e .. 608-224-6213

DNRJD 113133790

Sample #.. 262935002Collec`tion End.. 0612812016 lo..1S am

Waterbody/Outf all Id :ID Point #:Ac.count #.. WA;063

Scr#7p/e focafro7€.. FLAMBEAU NINES'c2mp/e Descr!Z}fro7z.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE

San3ple source: Nloultorin8"ldi Sample Depth:Dczre Repor/ed.. 08/08/2016 5Ycwxp/e 6'z#/z4b'.. COMPLETE

Project No : Sample Reason :Coriiment:

Analyses and Results..nalysis Method Analysis Date Lab comment

EPA 200.7 06/30/2016Cede Description1005 BARIUMDISS

915 CALCIUM DISS

1030 CHROMIUMDISS

1040 COPPERDISS

46570 HARDNESS, CA MG CALCULATED(MGEL AS CAC03)

1046 IRONDISS

925 MAGNESIUM DISS

1145 SELENIUMDISS

1075 sn.vERDlss

1090 ZINCDISS

Resulf Units LOD126 ug/L 1.00

150 MGth 0.100

ND ugth 1.00

21.9 ug/L 5.00

568 MGEL 0.660

1.73 MGth 0.loo

47.2 MGth 0.100

15.1 ug/L 10,0

2.79 ug/L 2.00

ND ugth 5-00

Report Lilnit I-OQ3.00

0-300

3.00

Analysis Method Analysis Date Lab commerit

EPA 245.I 06/29/2016`,ode I)esariptioii Result Units LOD Raport Limit LOQ

71890 MERCURY DISS ND ug/L 0.030 0.080

nalysis Method Alialysis Date Lch corrunen{

EPA 375.2 07/21/2016Code Description Rest{lt Units LOD Report Limit LOQ946 SULFATE DISS 29.4 MGth 4.70 15.0

Page 4: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: 113133790 Sample: 26293S002 P(lge 4 Of 22

Code Descriptioii Resull Units LOD Report Limit LOQ

nalysis Method Analysis Date Lab cornnient

SM3113B 07/08/2016C:ode Description Result Units LOD Report I.imit LOQ1025 CADMIUMDISS ND ug/L 0.0500 0.150

nalvsis Method Aiialysis Dale Lab conimen{

SM2510B,EPA150.1,SM2320B 06/30/2016Code Deseripliori Result Units LOD Report Limi[ LOQ410 ALKALINITY TOTAL CAC03 608 MGth 0.255 0.255

95 CONDUCTIVITY, UMHOS/CM @ 1080 uS/cm i.00 1.0025C

403 PHLAB 6.30 SU 0.100 0.100

iialvsis Method Alralysis Date Lab corrmeri{

SM3113B 06/30/2016Code Desckp{ion Resiilt Uriits LOD Report Limit LOQ1049 LEADDISS ND ug/L 1.00 3.00

Analysis Method Analysi.s Date Lab comment

SM2540C 07/05/2016Code Descripfron Result Units LOD Report Liinit LOQ70300 RESIDUE I)ISS 180C (TOTAL 698 MGth 50.0 50.0

DISSOLVED SOLDS)

4naly,sis Method Analysis Date Lub comment

EPA 200.7 06/30/2016Code De.scription Result Uni,ts LOD Report Linit LOQ1056 MANGANESE DISS 27400 ugth 20.0 60.0

nalysis Method Analysis Date Lab comment

SM3113B 07/01/2016Code Description Result Units LOD Repott Linit LOQ1000 ARSENICDISS ND ug/L 2.00 6.00

Page 5: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: 113133790 Sample: 26Z93sO03 Page 5 Of 22

I,flbor#fop?.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadisonP/Io7!e I. 8004424618

Sample:

F7.a/d #.. MW1013ACollection start: 06lz81201610..2S aim

Co//eczec7 5v... ZOE MCMANAMAJD#.. 03180

Co!f#¢J.. Rusk

VI 53718Fas P¢o7}e .. 608-224-6213

z]rm+z] 113133790

Scz"p/e #.. 262935003Collection End: 06/2812016 10..2S ilm

Wtiterbody/Ouif ;all Id :

ID Point #:Ac.count #: WA063

^Scr#ip/c foca/I.o„.. FLAIVBEAu hflNES'a772p/e Descrzp/z-o7?.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE

San€ple source: Mowitoringwch Sample Depth:Dc!!e j{epor/ed.. 08/08/2016 5'cz7#p/e sY/cj"ts`. COMPLETE

Project No.` Sample Reason:Comment:

Analyses and Results..4nalysis Method Analysis Date Lab comment

SM3113B 07/01/2016i:ediieiiFdriiii-Ji. Result Units LOD Report Limit LOQ1000 ARSENICDISS NI) ugth 2.00 6.00

1nalysis Method Ailalvsis D(ite Lab comment

EPA 245.1 06/29/2016Code Description Res.ilt Units LOD Report Linlit LOQ7i89o MERcuR¥ Dlss r`ro ugth o.o3o o.o8o

nalysis Method Analysis Dale Lab comment

SM2510B,EPA150.1,SM2320B 06/30/2016:ode Description Result Units LOD Report Linit LOQ410 ALKALINITY TOTAL CAC03 351 MGth 2.55 2.55

95 CONDUCTIVITY, UMHOS/CM @ 967 uS/cm 10.0 10.025C

403 PHLAB 6.88 SU 1.00 1.00

nalvsis Method Analysi.s Date Lab comment

EPA 375.2 07/21/2016I,,,`. ,,`..``.,.ipt- rl.-\!,.', I `,I,,` I.,-)1' R(p",., L,,,,,, I-1)(I)

946 SULFATEDISS 187 MGth 47.0 150

ralysis Method Analysis Dale Lab comment

EPA 200.7 06/30/2016

Page 6: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lch: 113133790 Sample: 26Z93S003 Page 6 Of 22

Description1005 BARIUMDISS

915 CALCIUM DISS

io3o clmoMluMDlss1040 COPPERDISS

46570 HARDNESS, CA MG CALCULATED(MGth AS CAC03)

1046 IRONDISS

925 MAGNE SIUM DISS

1056 MANGANESE DISS

1145 SELENIUMDISS

1075 SH.VERDISS

1090 ZINCDISS

Resull Units LOD77.4 ugth I.00

151 MGn, o.loo

ND ugth I.00

ND ugth 5-00

599 MGfr 0.660

0.285 MGth 0.loo

53.6 MGth 0.loo

4390 ug/L 1.00

NI) ugth 10.0

3.21 ug/L 2.00

ND ugth 5.00

rialysis Methc]d Analysis Dale Lab comment

SM3113B 07/08/2016i:iEET5e-:-Eii;ption Result Units LOD Report Limit LOQ

1025 CADMIUMI)ISS ND ug/L 0.0500 0.150

1nalvsis Metliod Amalvsis Date Lab co7mnent

•SM3113B 06/30/2 016

I-,;`i: ,\.,``.,.,.p,,"i, R`..`,,i,I !,,,` I,)I, il`:.."-, I,,:i,,I()(-,

1049 LEADDISS NI) ugH 1.00 3.00

nalysis Methoc] Analysis Date Lab corriment

SM2540C 07/05/2016:ode Description Result Units LOD Report Limit LOQ70300 RESIDUE DISS 180C (TOTAL 648 MGth 50.0 50.0

DISSOLVED SOLIDS)

Page 7: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab..1+3133790 Sample: 26&93sO04 Page 7 Of 22

I,&borflJory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadison VI 53 718P/jo7je.. 8004424618 Fan. P4oj7e.` 608-224-6213

Sample,

Fz.e/d #.. MW1013BCollection start.. 06/281201610..30 &m

Co//€cJec7 bv.. ZOE MCMANAMAJD#.. 03180

Co?/#fy.. Rusk

DNR ID 113133190

Sample #: 26293SO®4

Collection End.. 0612812016 10..30 zlm

wate].body/Outf all ld :ID Point #:Account #.. WAj063

Sc}#]p/e foca/I-o7!.. FLAMBEAU AflNES'c}#!pfe Descrzpfz.o7?.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE

Sample source: Surf ]8Icewaller Sample Depth:Dc7fe Reporfed.. 08/08/2016 5Ycz;#p/e s'fo/!t6'.. COMPLETE

Proj ect No : Sample Reason :Comment:

Analyses ai.d Results..

r!alysis Method Analysis Date Lab commerit

EPA 200.7 06/30/2016Code Description Result Units LOD Report Limit LOQ

1056 MANGANESE DISS 32200 ug/L 20.0 60.0

}ialysis Method Analysis Date Lab comment

SM2540C 07/05/2016-`,-ode Description Re:suit Units LOD Report Limit LOQ

70300 RESIDUE DISS 180C (TOTAL 3100 MGA, 50.0 50.0DISSOLVED SOLIDS)

nalysis.Method Analysis Date Lab c,omment

SM3113B 07/01/2016I:&55fro&§EFi§T{6ir---- Re:sult Units LOD Report Limit LOQ

1000 ARSENIC DISS ND ug/L 2.00 6.00

Page 8: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

08/08/2016

Wisconsin Department of Natural ResourcesLaboratory Report

Zc}b..113133790 6'o7#p/e.. 262935004 Pcrge 8 a/22

iialvsis Method A}ralvsis Date Lab corlunenl

EPA 200.7 06/30/2016Code Descriptionloos BARIUMDISS

915 CALCIUM DISS

1030 CHROMIUMDISS

1040 COPPERDISS

46570 IIARDNESS, CA MG CALCULATED(MGth AS CAC03)

1046 IRONDISS

925 MAGNESIUM DISS

1145 SELENIUMDISS

1075 SELVERDISS

1090 ZINCDISS

Res.ilt Units

10.5 ugth

609 MGth

1.13 ugEL

573 ugth

2130 MGth

LOD Reporl Limil LOQ1.00 3.00

0.loo 0.300

1.00 3.00

5.00 15.0

0.660 2.00

NI) MGEL 0.100

149 MGth 0.100

ND ugAJ 10-0

4.46 ug/L 2.00

130 ugth 5.00

nalvsis Method A]ralvsis Date Lab com}nenl

SM2510B,E PA150.1,SM23 20B 06/30/2016Code Desariptiori Result Units LOD Report Liniif LOQ410 ALKALINITY TOTAL CAC03 570 MGth 0.255 0,2.55

95 CONDUCTIVITY, UMHOS/CM @ 3070 uS/cm I.00 1.0025C

403 PHLAB 6.42 SU 0.100 0.100

iialvsis Method Aiialvsis Date Lab coriimen{

EPA 375.2 07/21/2016Code Description Result {jni{.s LOD Report Lini{ LOQ946 SULFATE Dlss isio MGn. 235 750

nalysis Method Analysis Date Lab comment

SM3113B 07/08/2016Code Description Result Units LOD Report Limit LOQ

1025 CADMIUMDISS 0.685 ugth 0.0500 0.150

Page 9: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

08,/08/2016

Wisconsin Department of Natural ResourcesLaboratory Report

Zcrb..113133790 S'a7xp/e.. 262935005 Pcrge 9 a/22

I,¢bor¢fory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadisonP/!07je.. 800J424618

Sample,

Field #.. NIW1013CCo//ec/3.o7j s/¢rf.. 06/28/201610:10 am

Co//€c!ec/ dy... ZOE MCMANAMAJD#., 03180

Co!f#¢J.. Rusk

VI 53718FrtL-P¢o7!e .. 608-224-6213

DjvR /I) 113133790

Sample #: 26293S00SCollection End: 06/2812016 10..1® aim

Walerbody/Outf all Id :ID Point #:Account #.. WA:063

^S¢#!p/e foca/z.07!.. FLAIvmEAu hHhEAS'""p/e De,s'cj.I.p/z.a/2.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE

Saniple source: Morirtorin8Wch Sample Depth.`Dc!re jzeporfed,. 08/08/2016 S'cz7xp/e s'rcj/zis`. COMPLETE

Proj ect No : Sanple Rea,son :Comment:

Analyses and Results:

rialysis Method Analysis Dare Lab comment

EPA 245.1 06/29/2016Code Description Result Units LOD Repo1.i Limit I.OQ71890 MERCURY DISS NI) ug/L 0.030 0.080

nulysis Method Analysis Date Lab comment

EPA 200.7 06/30/2016T6dFi- Description Re!sul{ Units LOD Report I.imit LOQ

1056 MANGANESEDISS 10700 ug/L 10.0 30.0

Analysis Method Analysi.s Date Lab comment

SM2510B ,EPA 150.1,SM232 0B 06/30/2 016f6dEiniiEFiFir6ir------- Result units LOD Report Lini{ LOQ410 ALKALINITYTOTAL CAC03 543 MGth 0.255 0.255

95 CONDUCTIVITY, UMHOS/CM @ 3050 uS/cm I.00 I.00

Page 10: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: 1+3133190 Sample: 26Z93S005 Page lo of 22

fTJJ{froE§dr;F{{J;I---- Result units LOD Report Liinit LOQ25C

403 PHLAB 6.68 SU 0.loo 0.100

nalvsis Metliod Aiialysis Date Lab corlimenl

SM2540C 07/05/2 016i:[5J-fit;i;i;iJfr--- Res.lit units LOD Report Linii{ LOQ70300 RESIDUE DISS 180C (TOTAL 2940 MGth 50.0 50.0

DISSOLVED SOLIDS)

nalysis Method A]la[ysis Date Lab commerll

SM3113B 07/01/2016i=5iEIfE:Eifii6i-- Res.Ilt units LOD Report Linii[ LOQ

1000 ARSENICI}ISS 21.3 ug/L 2.00 6.00

4nalysis Method Analysis Dale Lab comment

EPA 200.7 06/30/2016Code Descriptionloos BARIUM DISS

915 CALCIUM DISS

1030 clmoMluMDlss1040 COPPERDISS

46570 HARDNESS, CA MG CALCULATED(MGEL AS CAC03)

1046 IRONDISS

925 MAGNESIUM DISS

1145 SELENIUM DISS

1075 SH.VERDISS

1090 ZINCDISS

Result Units LOD Report Limit LOQ15.5 ug/L 1.00 3.00

579 MGEL 0.100 0.300

ND ug/L i.00 3.00

ND ug/L 5.00 15.0

2050 MGEL 0.660 2.00

13.3 MGth

146 MGth

NI) ugfu

4.64 ugth

354 ugth

4ncllysis Method Analysis Date Lab comment

SM3113B 07/08/2016.`:-,h`.`. ,)"-`=;i,-,", ----- ` -__-` ` R`..`,,,, ,-,,,,` I-,)1\ R..r"i., I :,,,i, ((.)`']'

1025 CADMIUMDISS ND ug/L 0.0500 0.150

Page 11: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

08/08/2016

Wisconsin Department of Natural ResourcesLaboratory Report

Lab: 113133]90 Sample: 262935006 Page I l of 22

I,&bor¢tory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrM adison lh71 53 718P/jo7je.. 8004424618 Fcrt p¢oj!e.. 608-224-6213

Sample,

F7.e/d #.. MW1014CCo//€c/z-o7! S/¢rJ.. 06/28/2016 08:30 am

Co/Jcc/ed Sv..' ZOE MCMANAMAJD#., 03180

Co?/7?fy.. Rusk

DIVRJD 113133790

Sample #.. 26293S006Collection End.. 06/28/2016 08..30 ilm

Waterbody/Outf all Id :ID Point #..Ac.count #: WA;063

^Sd#jp/e foccr/z.07i.. FLAIvmEAU NINES'c!xp/e Descrzpfz.07z.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE

Sample source: NloHi:tor.\ngwch Sample Depthi`Dcf}e Rej7or/ed.. 08/08/2016 5'c"7jp/e s'J#/Its.. COMPLETE

Projec:i No : Sample Reason..

Comment:

Analyses antl Results:

4nalysis Method Arialysis Date Lab comnient

SM3113B 07/01/2016Code Desaription Result Units LOD Repoi.i I.i}nit LOQ1000 ARSENIC DISS 27.2 ug/L 2.00 6.00

lralvsis Method Aiialvsis D(ite Lcib comment

SM2510B,EPA150.1,SM2320B 06/30/2016Code Desorip{ion Resillt Uiiits LOD Report Liniil LOQ410 ALKALINITY TOTAL CAC03 269 MGth 2.55 2.55

95 CONDUCTIVITY, UMHOS/CM @ 1000 uS/cm 10.0 10.025C

403 PHLAB 6.90 SU 1.00 I.00

rulysi.s Method Analysis Date Lab coriiment

EPA 200.7 06/30/2016Code Descriptiori Res.ilt Units LOD Report Linit{ LOQ

1005 BARIUM DISS 32.5 ug/L 1.00 3.00

915 CALCIUM DISS 150 MGth 0.loo 0.300

1030 cmoMluM Dlss NI) ug/L 1.oo 3.oo

Page 12: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08,/08/2016 Lab: 1+3T33790 Sample: 26Z93S006 Page 1 2 Of 22

`:ode Description ResulJ Units LOD Repol.i himit LOQ

1040 COPPER DISS ND ugth 5.00 15.0

46570 HARDNESS, CA MG CALCULATED 523 MGEL 0.660 2.00

(MGEL AS CAC03)1046 IRON DISS 4.69 MGth 0.loo 0.300

925 MAGNEslln4 Dlss 36.4 MGth 0-loo 0.300

1056 MANGANESE DISS 1710 ugiv 1.00 3.00

1145 SELENIUM DISS ND ugth 10.0 30.0

1075 SH.VER DISS NI ugth 2.00 6.00

1090 ZINC DISS 266 ugth 5.00 15.0

mlysis Method Analysis Date Lab comment

EPA 245.1 06/29/2016i:5EEinEiE;S[{5ir---- Result units I.oD Report Limit I.OQ71890 MERCURY DISS ND ugth 0.030 0.080

nalvsis Method A]ralysis Date Lab comment

SM3113B 07/08/2016i:5diin[§CFSi{6ir---- Res.Ilt uiiits LOD Report Limit LOQ

1025 CADMIUMDISS ND ugfu 0.0500 0.150

4rialysis.Method Analysis Date Lab comment

EPA 375.2 07/21/2016T6ETir5EiiiFiT5T--- Result Units LOD Report Limit LOQ946 SULFATEDISS 211 MGth 47.0 150

iralvsis Method Anelvsis Date Lab c,oriiment

SM3113B 06/30/2016f55irifJEi;i;ipiion Resi{lt Units LOD Report Liniil LOQ1049 LEAD DISS ND ug/L 1.00 3.00

Page 13: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: 1L3133790 Sample: Z62935008 Page I 3 Of 22

I,&bor¢fo]}j.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadison lvI 53 718P;jo7€e.. 8004424618 Fff¥ P*o7?e.. 608-224-6213

Sample:

Field #:

Collection Start:

Collected bv:

JD #..Con,nty,

Sci"ple Location:

MW1014B06/28/2016 08:43 amZOE MCMANAMA03180RuskFLAIVBEAu nnNE

DNR ID 113133790

Sample #.. 262935008Collection End.. 06/2812016 08=43 gim

wate].body/Outf all Id :ID Point #:

Account #: WA063

^S'c}7#pze Descr!P/z.ojz.. GROUNDWATER MONITORING WELL -SPLIT SAMPLESample source: Morf uor.\ng"idi Sample Depth: INDc7fe Repor/ed.. 08/08/2016 S'c!7#p/e stcztets.. COMPLETE

Project No: Sample Reason :Comment:

Analyses and Results:

nalvsis Method A}ialysis Date Lab corirmen[

EPA 245.I 06/29/2016Code Description Res.Ilt Units LOD Report Limit LOQ71890 MERCURY DISS ND ug/L 0.030 0.080

Analysis Method Amalysi.s Date I.ab comment

EPA 200.7 06/30/2016Code Deseription Result Urii{s LOD Report Limit LOQ

1005 BARIUM DISS 21.7 ug/L 1.00 3.00

915 cALcluM Dlss 5ii MGfr 0.loo 0.300

1030 CHROMIUM I)ISS ND ug/L 1.00 3.00

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Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: 1T3133790 Sample: 26Z93S008 Page 14 Of 22

Code Descriptioii Result Units LOD Repoi.t Linit LOQ1040 COPPER DISS 455 ugth 5.00 15.0

46570 HARDNESS, CA MG CALCULATED 1770 MGth 0.660 2.00

(MGEL AS CAC03)1046 IRON DISS ND MGth 0.100 0.300

925 MAGNEslun4 Dlss 120 MGA 0.100 0.300

1145 SELENIUM DISS ND ugEL 10.0 30.0

1075 SILVER DISS 3.20 ugth 2.00 6.00

1090 ZINC DISS 1040 ugA- 5.00 15.0

4rlalysis Method Antilysis Dale Lab comnient

SM2540C 07/05/2016Code Desc'riptioil Result Units LOD Repol.i Limit LOQ70300 RESIDUE DISs l80C (TOTAL 2450 MGth 50.0 50.0

DISSOLVED SOLIDS)

4nalysis Method Analysis Date Lab comment

EPA 375.2 07/21/2016Code Descriptioii Result Uniis LOD Report I.imit LOQ946 SULFATE DISS 1210 MGEL 235 750

llalysis Method Aiialysis D(lie Lab comment

SM3113B 07/01/2016Code Description Resillt Ullits LOD Report Limit LOQ

1000 ARSENICDISS ND ugth 2`00 6.00

nalysis Method Analysis Date Lab comment

SM3113B 06/30/2016`.ode Desci-iption Resul[ Units LOD Report Limit LOQ

1049 LEADDISS ND ug/L 1.00 3.00

Analysis.Method Analysis Date Lab comment

EPA 200.7 06/30/2016Code Description Result Uiiits LOD Report Linit LOQ1056 MANGANESE DISS 10800 ugth 10.0 30.0

Page 15: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: 1T3T3379® Sanple: 26E93S009 Page I 5 Of 22

£¢bormtory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadison VI 53 718P/jo7je.. 8004424618 Ffrt. P¢077e.. 608-224-6213

Sample,

F7.e/d #.. MW1014ACollection start.. 0612612016 08..S0 z\m

Co//ecJec7 bv.' ZOE MCMANAMAJD#.. 03180

Co!f#ty.. Rusk

DNRJD 113133790

Sc}7#p/e #.. 262935009

Collec`tion End: 06/26/2016 08..S0 iimWaterbody/Ouif all ld :

ID Point #:Ac.count #: WA\063

^Scr#Ip/e foca/z.o73.. FLAMBEAU NINESYaxp!e Dt?sc/.zP/i.07z.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE

Sample source`. Surt3ueewatf3r Sample Dapth:Da/e Raporjed.. 08/08/2016 S'¢7xp/e 6?c!/!tb'.. COMPIJETE

Project No : Sample Reason :Comment:

Analyses and Resuits..n{ilysis Method Analysis Date Lab comment

SM3113B 07/01/2016fina6- Description Result Units LOD Report Liinit LOQ

1000 ARSENIC DISS ND ug/L 2.00 6.00

iialysis Method Analysis Date Lab comment

EPA 200.7 06/30/2016Code Description1005 BARIUMDISS

915 CALCIUM DISS

1030 CHROMIUMDISS

1040 COPPERDISS

46570 HARDNESS, CA MG CALCULATED(MGn As cAco3)

1046 IRONDISS

925 MAGNESIUM DISS

1056 MANGANESE DISS

1145 SELENIUMDISS

1075 SHjvERDISS

1090 ZINCDISS

Res{Ilt Units LOD

13.6 ugth I.00

335 MGth 0.100

ND u8rfu 1.00

ND ugth 5.00

1330 MGEL 0.660

ND MGEL 0.100

120 MGth 0.100

98.2 ug/L 1.00

ND ugth 10.0

ND ugth 2.00

8.40 ug/L 5.00

1nalvsis Method Analysis Date Lab corirmenr

SM3113B 07/08/2016

Page 16: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: 1+3T33790 Sample: 2629350Ow Page l 6 Of 22

Code Descriptioii Result Units LOD Repol.i Li]nit LOQ1025 CADMIUMDISS ND ug/L 0.0500 0.150

nalysis Method Aiialysis Date Lab coryrmeii[

EPA 245.1 06/29/2016-Code Description Result Units LOD Report Limit I,OQ

71890 MERCURY DISS NI) ug/L 0.030 0.080

n{ilysis Method Analysis Date I~ab comment

EPA 375.2 07/21/2016T6d{iniiFFii{{5Tr----- Result units LOD Re|ioi.t Linit LOQ946 SULFATEDISS 855 MGEL 235 750

nalysis Me{hcid Analysis Date Lab coriimerit

SM2510BF PA150.1,SM232 0B 06/30/2 016Code i5Z;I;STidfr-- Result units LOD Report Liniil LOQ410 ALKALINITY TOTAL CAC03 486 MGth 0.255 0.255

95 CONDUCTIVITY, UMHOS/CM @ 2090 uS/cm I.00 1.0025C

403 PHLAB 6.75 SU 0.100 0.100

nalysis Method Aunlysis Dale Lab comment

SM2540C 07/01 /2 016-i:ode Description Result Units LOD Report Linijl LOQ

70300 RESIDUE DISS 180C (TOTAL 1850 MGth 50.0 50.0DISSOLVED SOLIDS)

nalysis Method Analysis Date Lab corlrment

SM3113B 07/05/2016i:JdT--5e:s-chp{ion Result Units LOD Rapor{ Lirliit LOQ

1049 LEADI)ISS ND ug/L I.00 3.00

Page 17: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: 113T33]9® Sample: 26293S010 Page 1 7 Of 22

£&bor¢fory.. Wisconsin state Laboratory of Hygiene2601 Agricu]tuFe DrMadison lh71 53 718P/jo7!e.. 8004424618 Fcur p¢oj7e.. 608-224-6213

Sam.plc:

Field#: 4®14

Collection start.. 06lz812016 09..00 i."Co//€cfec7 bv.. ZOE MCMANAMA

JD#.. 03180Cot/#O;.. Rusk

DjvR/D 113133790

Sci7#j7/e #.. 262935010

Collection End.. 06/2812016 09..00 aim

Waterbody/Ouifall Id:ID Point #:Account #.. V`lA;063

^Scr777p/e focafz.o7!.. FLAMBEAu nflNEAS'c}fflpze I)escr7Pfz-o7?.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE

Sample source: Mohitorin8Vwdi Sample Depth: RII)aire I?ej7or/ed`. 08/08/2016 6Yc#7qp/e s'£"/w,}`.. COMPLETE

Project No: Sanple Reason :Comment:

Analyses and Results:.

4nalysis Method Arialysis Date Lab comment

SM3113B 07/01/2016

Code Descriptioi. Result Units LOD Report himit LOQ1000 ARSENICDISS ND ug/L 2.00 6.00

rralvsis Method Alialvsis Date L{ib commeiit

SM3113B 07/05/2016Code Description Resiilt Units LOD Report Linit LOQ1049 LEAD Dlss run u8th i.00 3.00

Analysis Method Analysi.s Dtffe Lub cominen[

EPA 245.1 06/29/2016Code Deseription Result Units LOD Report Limit LOQ71890 MERCURY DISS ND ug/L 0.030 0.080

nalysis Method Analysis Dale Lab comment

SM3113B 07/08/2016

Page 18: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

08/08/2016

Wisconsin Department of Natural ResourcesLaboratory Report

Lab: 113133790 Sample: 26293S010 Page 1 8 Of 22

Code Descriptioii Result Units LOD Report Limit LOQ1025 CADMIUMDISS 0.0778 ugth 0.0500 0.150

halvsis Method Analvsis Dcite Ijab commeni

SM2540C 07/05/2016Code Deseription Result Units LOD Report Linrif LOQ70300 RESIDUE DISs l80C (TOTAL 488 MGth 50.0 50.0

DISSOLVED SOLIDS)

1iralvsis Method A}.alvsis Date Lab conirmen[

EPA 375.2 07/21/2016Code Description Resillt Uiiits LOD Eel)or[ Lirrli{ LOQ

946 SULFATE DISS 116 MGth 23.5 75.0

nalysis Method Arlalysi.s Dc}{e Lab comment

EPA 200.7 06/30/2016Code Description1005 BARIUMDISS

915 CALCIUM DISS

1030 clmoMluMDlss1040 COPPERDISS

46570 HARDNESS, CA MG CALCULATED(MGEL AS CAC03)

1046 IRONDISS

925 MAGNESIUM DISS

1056 MANGANESE DISS

1145 SELENIUMDISS

io75 sn.vERDlss

1090 ZINCDISS

Result Units LOD Report Limit LOQ36.4 ug/L I-00

81.3 MGth 0.loo

ND ugth I.00

ND u8fr 5.00

316 MGft 0.660

ND MGth 0.loo

27.4 MGth

2030 ugth

ND ugfu

rlD ugth

6.04 ugAJ

Page 19: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

08,/08/2016

Wisconsin Department of Natural ResourcesLaboratory Report

fcrb..113133790 6'c#7?p/e.. 262935011 Page J9 o/22

£q!borotory.. Wisconsin state Labol.atory of Hygiene2601 Agriculture DrMadison lh71 53 718P/!07je.. 8004424618 Fcur p#o7?e.. 608-224-6213

Sample,

F''€'d #.. MW|000PRCollection start.. 06lz812016 0]..3S am

Co/Jccfet7 bv.. ZOE MCMANAMAJD#.. 03180

Co{f#¢J.. Rusk

DNR ID 113133790

S:cz7xp/e #.. 262935011

Collec.{ion End:. 06lz812016 07..35 gim

Waterbody/Outf all Id :ID Point #:Account #: "A,063

Sc}#jp/€ £oca/z.o7z.. FLAMBEAu hflNES'cj/72p/e Deb`crrp#-07z.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE

Sample source: Nhorirtoringwch Sample Depth.`Dcrfe Repor/ed.. 08/08/2016 STcgmp/e 6'zc2/zfb'`. COMPLETE

Project No: Sample Reason:coTiiTnent:

Analyses and Resuits..rialysis Method Analysis Date Lab comment

SM2 540C 07/05/2 016Code Description Result Units LOD Report Limit LOQ70300 RESIDUE DISS 180C (TOTAL 544 MGAij 50.0 50.0

DISSOLVED SOLIDS)

nalysis Method Arlalysis Date Lab comment

SM3113B 07/05/2016Code Desci.ipliori Result Unils LOD Report Limit LOQ1000 ARSENIC DISS 8.55 ugth 2.00 6.00

lialvsis Method A}.alvsis Date Lcib corlimeiil

EPA 200.7 06rso;2016Code Deseription1005 BARIUMDISS

915 CALCIUM DISS

1030 CHROMIUMDISS

1040 COPPERDISS

46570 HARDNESS, CA MG CALCULATED(MGEL AS CAC03)

1046 IRONDISS

925 MAGNESIUM DISS

1056 MANGANESE DISS

ii45 sELENruMDlss

Res{Ilt Units LOD Report hiriiit34.3 ugth 1.00

Ill MGEL 0.100

NI) ugth I.00

NI) ugth 5.00

394 MGth 0.660

0.507 MGn. 0.loo

28.6 MGft 0.100

2070 ug/L I.00

ND u8fr io.0

Page 20: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08,/08/2016 Lab: 1L3T33790 Sample: 26293S011 Page 20 Of 22

`,ode Description Result Units LOD Repoi.t Limit LOQ

1075 SHjvERDISS ND ug/L 2.00 6.00

1090 ZINCDISS 302 ug/L 5.00 15.0

nalvsis Method Airalvsis Date Lab coriiinenf

SM3113B 07/05/2016Code Descrip{iori Result Units LOD R.epori Limit LOQ

1049 LEAD DISS NI) ugth 1.00 3.00

nalysis Method Analysis Date Lab comnient

EPA 245.I 06/29/2016:ode Description Result Units LOD Report Limit LOQ

71890 MERCURY DISS ND ug/L 0.030 0.080

nalysis Method Analysis Date Lab com]nenl

EPA 375.2 07/21/2016Code Description Result Units LOD Report Limit LOQ946 SULFATE DISS 196 MGth 47.0 150

Comj#e7jJ.. MATRIX SPIKE QC EXCEEI)£D.

Analysis Method Analysis Date Lub comment

SM2510B,EPA150.1,SM2320B 06/30/2016Code Description Result Uwifs LOD Report Lini{ LOQ410 ALKALINITY TOTAL CAC03 211 MGth 2.55 2.55

95 CONDUCTIVITY, UMHOS/CM @ 779 uS/cm 10.0 10.025C

403 PHLAB 6.78 SU 1.00 I.00

inalysis Method Analysis Date Lab comment

SM3113B 07/08/2016Code Description Result Uni}s LOD Report Linit LOQ)

1025 CADMIUMDISS 0.107 ugivL 0.0500 0.150

Page 21: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

Wisconsin Department of Natural ResourcesLaboratory Report

08/08/2016 Lab: T13133]90 Sample: 26Z93SOL2 Page 2 I of 22

I,&4ordrfory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadison Wrl 53 7 1 8P/!o7je.. 8004424618 Fur p#oj7e.. 608-224-6213

Sample,

F7.e/d #.I MW1000RCollection start: 06/2812016 01..20 am

Co/JecJec7 6v... ZOE MCMANAMAJD#., 03180

Co!f#ty.. Rusk

DNJZJD 113133790

Sample #.. 26Z93S012Collection End: ®6/28/2016 07..20 aim

wate].body/Outf all Id:ID Point #:Account #: WAL063

Scr#}p/€ £occ}/z.of!.. FLAMBEAU NINES'amp/e Descrrpfz.o77.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE

Sample source: Pillonftorin8Wch Sample Depth:Dczfe Jtepor/ed.. 08/08/2016 5'c[7xp/e s/czr€is.. COMPLETE

Project No: Sanple Retlsan :Commerlt:

Ai.alyses and Resuits:nalysis Method Analysis Date I.ab comment

EPA 245.1 06/29/2016ffJile Description Resuli Units LOD Report I.ilnit I.OQ71890 MERCURY DISS ND ug/L 0.030 0.080

llalysis Method Aiialysis Date Lab comment

EPA 200.7 06/30/2016-Code Description Res{Ilt Units LOD Report Limit LOQ

1056 MANGANESE DISS 10200 ug/L 10.0 30.0

4rialysis Method Analysis Date Lab comment

SM3113B 07/05/2016:ode Desci.iption Resuh Units LOB Report Linit LOQ1000 ARSENIC DISS NI) ug/L 2.00 6.00

4ralysis Method Analvsis Date Lab Comment

EPA 200.7 06/30/2016

Code Description Result Units LOD Rapori Limit LOQ

1005 BARIUIVI DISS 28.3 ugth 1.00 3.00

915 CALCIUM DISS 69.0 MGfr 0.loo 0.300

1030 CHROMIUM DISS NI) ugth 1.00 3.00

1040 COPPER DISS 65.4 ugth 5.00 15.0

46570 IIARDNESS, CA MG CALCULATED 259 MGth 0.660 2.00

(MGEL AS CAC03)

Page 22: Wisconsin Department of Natural Resources Laboratory  · PDF filea, i,. I e~ Wisconsin Department of Natural Resources Laboratory Report 08/08/2016 Lab: 113133790

08/08/2016

Wisconsin Department of Natural ResourcesLaboratory Report

Lab: 113133790 Sample: 262935012 Page 22 Of 22

Code Descriptioi. Result Units LOB Report Li]nit LOQ1046 IRON DISS ND MGEL 0.100 0.300

925 MAGNEslun¢ Dlss 21.0 MGEL 0.100 0.300

1145 SELENIUM DISS ND ugEL 10.0 30.0

1075 SILVER DISS ND ugEL 2.00 6.00

1090 ZINC DISS ND ugEL 5.00 15.0

iialvsis Method Analvsis Date Lab comment

SM2510BJIPA150.1,SM2320B 06/30/2016Code Descripliori Res{Ilt Units LOD Report Linli[ LOQ410 ALKALINITY TOTAL CAC03 145 MGth 2.55 2.55

95 CONDUCTIVITY, UMHOS/CM @ 559 uS/cm 10.0 10,025C

403 PHLAB 6.53 SU I.00 I.00

nalysis Method f roalysis Date Lab comment

SM3113B 07/08/2016Code Description Restilt Units LOD Report Lirliil LOQ1025 CADMIUMDISS 0.0711 ugth 0.0500 0.150

4nalysis Method Analysis Date Lab comment

SM3113B 07/05/2016:ode Description Resull Units LOD Report Liinit LOQ1049 LEADDISS ND ug/L 1.00 3.00

nalysis Method Analysis Date Lab coriiment

SM2540C 07/05/2016Code Description Resiilt Units LOD Report Liniit LOQ70300 RESIDUE DISs l80C (TOTAL 380 MGth 50.0 50.0

DISSOLVED SOLDS)

Analysis Method Analysis Date Lab comment

EPA 375.2 07/21/2016Code Description Result Units LOD Report Linlil LOQ946 SULFATE DISS 107 MGth 23.5 75.0

Co7#/tge7!f.. MATRIX SPIKE QC EXCEEDED.