WESTINGHOUSE ELECTRIC CORP MEMO RE: GROUNDWATER … · Westinghouse were taken by Westinghouse...

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224266

WestinghouseElectric Corporation

BloomingtonProject

P. 0. Box 997Bloomington, Indiana 47402-0997

February 16,1996 BP96-0033

TO: DISTRIBUTION LIST

Subject: Lemon Lane Groundwater Field Sampling Plan Data Through December 1995

The Lemon Lane Groundwater Field Sampling Plan provides that the parties are to meet at the six monthinterval to discuss the data and recommend any changes in frequency, location, and methodology in thecollection of future data. The six month interval will be the end of February. We have scheduled ameeting for February 29 to conduct this discussion.

This letter forwards for your information the following five (5) enclosures which include the additionaldata collected under the Field Sampling Plan.

ENCLOSURE #1 - DECEMBER RESIDENTIAL WELL RESULTSDecember 4 -7, 1995 the second quarter of samples were taken at the operational residential wells withinone mile of Lemon Lane. This enclosure includes the table of results identifying the sampled well by mapnumber and street address and the field parameters measured, the location map of the residences, thecertificate of analysis from Heritage Labs, and the data validation report on those analyses.

ENCLOSURE #2 - MONITORING WELL RESULTSMonthly sampling of the five monitoring wells began in October 1995. This enclosure includes the tableof results for samples taken in October, November, and December of 1995, the certificate of analysis fromHeritage Labs, the field log sampling sheets, and the data validation report on the analyses.

ENCLOSURE #3 - MONTHLY SPRING SAMPLING RESULTSThe eight consecutive weeks of sampling of the six directly connected springs ended on October 18, 1995.Monthly sampling of those springs began in November. By mutual agreement. Stony West and Snoddysprings were added to this list. Snoddy Spring was not flowing at either the November or Decembersampling events. For convenience in comparing results, this enclosure includes the table of results for theeight consecutive weeks as well as the November and December sampling results. A sample taken ofStony West Spring on October 27, during the fall storm event monitoring, is included in this table. Alsoincluded in this enclosure are the certificate of analysis for the November and December samples of the sixsprings plus Stony West, the certificate of analysis for the October 27 Stony West sample, and the datavalidation report on these analyses.

ENCLOSURE #4 - NINE PERIPHERAL SPRINGS SAMPLING RESULTSThe preliminary results of sampling the nine peripheral springs for water and the five downstream sedimentsamples were transmitted to you on September 28, 1995 along with the certificates of analysis. Thisenclosure includes the table of results for the sediment samples amended with the data validation qualifiersand the data validation report on the previously transmitted analyses.

SUPWFUND.

DISTRIBUTION LIST:

Dan HopkinsUSEPA Region 577 W. Jackson Blvd.Chicago, IL 60604

Resa RamseyIndiana Dept. of Env. Management100 N. Senate Ave.Indianapolis, IN 46206

John LangleyCity of BloomingtonP.O. Box 1216Bloomington, IN 47402

Steve CreechMonroe Co. Health Dept.119 W. 7th St.Bloomington, IN 47404

ENCLOSURE #5 - FALL STORM EVENT SAMPLE RESULTSStorm event sampling was conducted October 27 - 30, 1995 at Illinois Central and Slaughterhouse springs.Pre-storm sediment sampling was conducted at the six spring locations per the Field Sampling Plan. Afterthe storm water sampling was completed on October 30, Westinghouse and EPA representatives inspectedthe springs and concluded no sediment deposition occurred that could be uniquely sampled Therefore nopost-storm sediment samples were taken. This enclosure includes the table of results for water samplingwith flow, conductivity, and temperature, the table of results for the pre-stonn sediment samples, certificateof analysis from Heritage Labs, and the data validation report for these analyses. Also included for yourconvenience in reviewing these data, are the data tables for both springs on diskette with the time-functionsso graphs may be plotted.

The transmiUal of these data packages to the Consent Decree Parties fulfills Westinghouse's commitmentfor data submission in accordance with the Field Sampling Plan. If you have any questions about any ofthese enclosures please contact Mike McCann at the Site Office at (812) 334-0030.

Sincerely,

Dorothy M. AlkeProject Director

ENCLOSURE #1

DECEMBER

RESIDENTIAL WELL

RESULTS

Table 1 - Lemon Lane Residential Wells Sampling Results

Address1608 Lane1613 Lane161 5 Lane1616 Lane1618 Lane3100WoodyardRd.3250Woodyard Rd.3255 Woodyard Rd.3401 Woodyard Rd.3500 Woodyard Rd.3503 Woodyard Rd.3522 Woodyard Rd.3523 Woodyard Rd.3534 Woodyard Rd.3535 Woodyard Rd.3600 Woodyard Rd.3605 Woodyard Rd.3609 Woodyard Rd.3704 Woodyard Rd.3720 Woodyard Rd.3721 Woodyard Rd.3722 Woodyard Rd.3740 Woodyard Rd.3740 Woodyard Rd.3740 Woodyard Rd.3401 Vernal Pike2320 Beaumont1 1 1 N. Kimble220 N. Kimble220 N. Johnson2424 Evergreen

Map*01*02*03*04*05*06*07*08*09*10*11121314*1516171819*2021*22*23A23B23C2425*26*27*28*29

Date12/04/9512/06/9512/04/9512/07/9512/04/9512/06/9512/06/9512/06/9512/05/9512/07/9512/04/95

h1 2/04/9512/04/9512/04/9512/04/9512/04/9512/05/9512/04/9512/04/9512/06/9512/06/9512/05/9512/04/9512/04/9512/04/9512/06/9512/05/9512/05/9512/05/9512/05/9512/05/95

Time17:1517:3510:3017:1511:2511:3015:0513:2510:1018:1509:1510:4010:1017:4515:2011:1511:2512:4515:3009:1015:2513:1008:3015:0008:4513:5013:4008:3017:1014:4516:05

Sample ID #95 12/4/95 LL 1715 SRW0195 12/6/95 LL 1735 SRW0295 12/4/95 LL 1030 SRW039512/7/95LL1715SRW0495 12/4/95 LL 1125 SRW0595 12/6/95 LL 1 130 SRW06951 2/6/95 LL1 505 SRW0795 12/6/95 LL 1325 SRW0895 12/5/95 LL 1010 SRW099512/7/95LL1815SRW1095 12/4/95 LL 0915 SRW1 195 12/4/95 LL 1040 SRW1295 12/4/95 LL 1010 SRW1395 12/4/95 LL 1745 SRW1495 12/4/95 LL 1520 SRW1595 12/4/95 LL 1 1 15 SRW1695 12/5/95 LL 1125 SRW1795 12/4/95 LL 1245 SRW1895 12/4/95 LL 1530 SRW1995 12/6/95 LL 0910 SRW2095 12/6/95 LL 1525 SRW2195 12/5/95 LL 1310 SRW2295 12/4/95 LL 0830 SRW23A95 12/4/95 LL 1500 SRW23B95 12/4/95 LL 0845 SRW23C95 12/6/95 LL 1350 SRW2495 12/5/95 LL 1340 SRW2595 12/5/95 LL 0830 SRW2695 12/5/95 LL 1710 SRW2795 12/5/95 LL 1445 SRW2895 12/5/95 LL 1605 SRW30

Temp(deg C)

12.810013.012.312.511.911.411.213.513.213.013.513.212.813.513.112.713.013.012.313.011.112.414.013.013.412.211.913.08.213.2

Cond(uS/cm)

692542544595700643707659604691660729735692740695717741738846728578948973962679521489490490513

Turb(ntu)0.54.52.64.01.3

0.770.970.580.440.521.12.71.5

0.760.674

0.680.760.781.30.50.282.32.41.1241.3

0.61182.03.1

RGB's(ppb)BDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDLBDL

Also sampled by EPA for other contaminants

Duplicate Samples and Field Blanks

Address3522 Woodyard Rd.3522 Woodyard Rd.3704 Woodyard Rd.3704 Woodyard Rd.2424 Evergreen2424 Evergreen

Map#121219192929

Date1 2/04/9512/04/9512/04/9512/04/9512/05/9512/05/95

Time10:4010:4015:3015:3016:0516:05

Sample ID #95 12/4/95 LL 1040 DRW1295 12/4/95 LL 1040 ERW129512/4/95LL1530DRW1995 12/4/95 LL 1530 ERW1995 12/5/95 LL 1605 DRW3095 12/5/95 LL 1605 ERW30

Temp(deg C)

13.5

13.0

13.2

Cond(uS/cm)

729

738 H

513

Turb(ntu)2.70.350.60.312.70.5

PCB's(ppb)BDLBDLBDLBDLBDLBDL

DuplicateField BlankDuplicateField BlankDuplicateField Blank

02/15/00

W VERNAL PK

It.

W SEV

Figure 1:Residential Water Well Locations in the Lemon Lane Landfill Area

By: brophye

11 Sep 1995

City of Bloomingtcn

Utilities Engineering

1000 1000 2000 3000 Scde: 1" = 1000'

Attachment 1: Data Validation for the Lemon Lane Residential Wells Sampled inDecember, 1995

1. The validation was performed per the requirements for level 4 data in the projectQAPjP. This includes a check for ; Holding Tune, Calibration, Blank Contamination,Precision, Accuracy, and Accuracy of Nominal Reporting Limits against methodrequirements. All analyses met method requirements. The data is accepted with noqualifications.

2. Note: We have reviewed data packages for the following attached samples only. Thistotals 31 wells.

3. The QAPjP requires an assessment of the overall data quality with respect toPrecision, Accuracy, Representativeness, Completeness and Comparability (PARCC).

o Precision and accuracy: Precision and accuracy were accessed by reviewingthe lab performance on lab spiked samples, lab spike duplicates and fieldduplicates. All requirements were met.

o Representativeness: The representativeness requirement involves anassessment of the field sampling and lab analytical techniques. The fieldsampling locations and techniques as well as lab procedures were inaccordance with the approved sampling plan and QAPjP. There were nodeviations and the representativeness requirement was met.

o Completeness: The completeness goal for the project was for all projectdata to be 90% accepted. Completeness is calculated by dividing the totalnumber of acceptable analyses by the total performed. An acceptableanalyses is defined as one that conformed to QC protocols and is notrejected. There were no rejected analyses so the completeness goal was met.

o Comparability: All the samples taken, analyzed and validated byWestinghouse were taken by Westinghouse sampling crews using the sameprocedures and analyzed by the same laboratory. Therefore for the samplestaken by Westinghouse there are no comparability issues.

Overall, the main objective of the sampling event was to determine if PCBs are present ata concentration of .1 ppb or more. The sampling and analysis performed met this goal.

C E R T I F I C A T E O F A N A L Y S I S

Service Location

HERITAGE ENVIRONMENTAL SERVICES, INC.COMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8305

Received

06-DEC-95Complete

18-PEC-95Printed

18-DEC-95

Project Lab 10

A361909PO Number

RN-24352-S 0-00Sampled

04-DEC-95 17:15

Report To

JIM PATRICKBLOOMINGTON PROJECTONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47404-0997

B i l l To

ACCOUNTS PAYABLEWESTINGHOUSE ELECTRIC COMPANYONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47402-0997

Sample DescriptionCLIENT ID: 95 12/4/95 LL 1715 SRW01DESCRIPTION: BLOOMINGTON PROJECTBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SH846-3510BAnalyst: J. GRIFFIN Analysis Date: 07-OEC-95 Test: P230.1.0

ParameterINITIAL WEIGHT OR VOLUMEFINAL VOLUME

Result10005

Det. Limit UnitsmLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: E. 8 IMG HAH Analysis Date: 09-DEC-95 Instrument: GC/ECD Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SU846-35108 P230.1.0

ParameterPCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

ResultBDLBDLBDLBDLBDLBDLBDLBDL

Det. Limit0.000100.000500.000100.00010O.OJ0100.000100.000100.00010

Unitsmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmq/L

TURBIDITYAnalyst: J.

TURBIDITY

(NEPHELOMETRIC) EPA 180.STOAKES Analysis Date

Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result0.50

Det. Limit Unitsntu

Sample CommentsBDL Below Detection Limit

Sample chain of custody number 27760.

This Certificate shall not be reproduced, except in full,without the written approval of the lab.

Additional copies of this report sent to:RUSS CEPKO, UESTINGHOUSE ELECTRIC CORPORATION

Page 1 (continued on next page)

HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361909 95 12/4/95 LL 1715 SRW01Sample Conments

11 STANUIX STREET, PITTSBURG, PA 15222-1384

Approved ___ _ J >y/? - Page 2 (last page)


Service Location


Received

08-DEC-95Complete

15-DEC-95Printed

ll-JAN-96

Project Lab ID

A362140PO Number

RN-24352-S 0-00Stapled

06-DEC-95 17:35

Report To


Bill To


Seqpte DescriptionCLIENT ID: 95 12/6/95 LL 1735 SRW02DESCRIPTION: LEMON LANE RESIDENTIAL WELLSBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDER

PCS SEPARATORS FUNNEL LIQUID-LIQUID EXTRACTION. :. :. Anaiytti %; «$$EU>SMI « i"- • • -• "( . v *•: Anal vsf « Detei iiNwKflS^ • ;' '

ParameterINITIAL WEIGHT OR VOLUME

:: FINAL VOLUME : m^. •:. • •^•••^ ^^ ••• .• ;mm^-

SW846-3510B

Result10005 --v, , : : - - : .

Teatt W30.1.(Oet. LiMit

)-•:• ' '" '

UnitaraLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW845-8080A! ;; :AnalV»ti :. m CtOUS£.:.?; : ; ;• ::; :::;

; : I;).:-; B>'«i»l»»«« tt»t»*:i J1 |S?H?S| .Prep: Pti SEPARATORr FUMtEi. tlOUIO-LIflUIO CXTBACTI01I «»4ft-351l

ParaawterPCB AROCHLOR 1016PLR AKuLnLoR i2?l . . . . . . • . . . : . . . • . . . . . .PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248

, PCB AROCHLOR U54 :PCB AROCHLOR 1260PCB AROCHLOR 1262

Uwtruewt: CC/JsttMJ»Z30.1.0


Testj 0501 ,2,(

Det. Li«it0.0001

DuOa

0.0001Oiijooi0.0001OvOOOl0.00010.0001

\-' -.' •

Unitamg/Lmn/L."*i/.«-mg/Ling/L«ng/LJng/Lmg/Lmq/L

TURBIDITY (NEPHELOMETXIC) EPA 180.1Analy»t: ». PFEFFER Analy*f* Detet 08-DEC-9S 16:30 Test: G602.5.0

ParaMterTURBIDITY

Result4.5

Det. Liait Unitsntu

Saaple CoaventsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A362140 95 12/6/95 LL 1735 SRW02

11 STANHIX STREET, PITTSBURG, PA 15222-1384

Approved : ALfA&VU Page 2 (last page)


Service Location


Receivad

04-DEC-95Cosplete

15-OEC-95Printed

ll-JAN-96

Project Lab ID

A361599PO Husfcer

RN-24352-S 0-00Saapled

04-OEC-95 10:30

Report To


Bid To

ACCOUNTS PAYABLEUESTINGHOUSE ELECTRIC COMPANYONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47402-0997

SMple DescriptionCLIENT ID: 95 12/4/95 LL 1030 SRW03DESCRIPTION: LEMON LANE RESIDENTIAL WELLSBLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDER

PCB SEPARATORY RJNNEL LIQUID-LIQUID EXTRACTION SW846-3510BAnalyst: •». WOOD . :••*. .: Analysis Dstet OWMBfrSS.^;!:;;'" '" ::: • ... -: re»i«'WS»;i;6-'. '':•:".:' '

ParaMterINITIAL WEIGHT OR VOLUMEFINAL VOLUME : : . . . - / - x . ^ . • ' • - • ' - ^ ^--v

Result10005 ' • . • ' • • • • • ; - - •

Det. LiMit UniteraLifctr:-^^->

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAneiy»ti T. PIXCttBT • : Analysis Date: OWtttfK^Prap» K> SEPAMTMY PUHMEL tlOUIO- LIQUID EXTKACTIOK WW4-3SK

ParaawterPCB AROCHLOR 1016PCB AROCHLOR 1221 v-^^mmmPCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248

, PCB AHOCHLOR U5*PCB AROCHLOR 1260PCB AROCHLOR 1262

fft«tnj«wtj CC/ECD • • • - ' •Nt 1*238,1:0

ResultBDL

mo£.--^m^:.i '• , . : : • : • 'BDLBDLBDLBDLBDLBDL

T«*tj OJ01.Z.1

Det. Limit0.000100-00050^0.00010Ovdooia0.00010Ovoooia0.000100;OOdIO

j;.^i^:4'.: ;•; ":•

Units•B/L&9fm:mmg/L«g/Lmg/Lmtte$;t?-mg/Lmq/L1

TURBIDITY (NEPHELOMETRIC) EPA 180.1Analyst: J. STQAKES Analysis Date: OS'OBC*«5 13:00 Test: C602. 5.0

ParaawterTURBIDITY

Result2.6

Det. Kent Unitsntu

Saaple Coaiaants

BDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, UESTIHGHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361599 95 12/4/95 LL 1030 SRH03SMplt COMMOtS


Approved : .u x ^QtiJuc^ Page 2 (last page)


Sarvica Location


Racaivad

08-DEC-95Coaplata

15-DEC-95Printad

ll-JAN-96

Project Lab 10

A362139PO Muafaar

RN-24352-S 0-00Saaplad

07-DEC-95 17:15

Report To


Bill To


Saapla DescriptionCLIENT ID: 95 12/7/95 LL 1715 SRW04DESCRIPTION: LEMON LANE RESIDENTIAL WELLSBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTIONAnalysts 6; HSSEU-SMITtt *naly»t«Dat*: 08-B6C-W

ParaaatarINITIAL WEIGHT OR VOLUMEFINAL VOLUME •••• • :-' •• :••:;::.> x.-:^":- • ' • '-.: t; MxV%:

SW846-3510B. . ' - • • • - " . . " - . "

Rasult1000

:v::.:.5'V: ., /-^x'v -•-,"..• •;.,

"ilwiit-frZHui,!Dat. L1«1t

> - ; -

unit*raL

."•jf" • • • • : - • • . - -

POLYCHLORINATED BIPHEMYLS (PCBS) SH846-8080A:::^.AnatV»t»'e;;aa«r^,:i..: ;•:; ^^••Uni^ttm Jttt»r11Hi«CM i;H:'-;;

Prap: PCB SEP«ATO»T rUNHEL LICUlO-LIflUID EKTXACTIQK MM*»3S1I

ParawtarPCB AROCHLOR 1016PCB AROCHLOR 1221 • i x v^PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248

rPCB AROCM.OR U54PCB AROCHLOR 1260

1 PCB AROCHLOR 1262

i llWtniawrtJ 6C/E£» :

WPZ30.1.0

RaaultBDL

•i.00l::: • • • " : : • / :>• : - :>" . : • ••::•••::.•BDL

: : BDL T f ' "T •• ' • • • • : - - - " ' • . : • • • •BDLBDLBDLBDL

7«*tJ 03DK2^

Dat. Li«it

0.0001

0^00050.0001fcODOI0.00010;oooi0.00010,0001

»V: ;"\-

Unit*

jg/Lwg/Lmg/Ling/Lmg/Lla/L^:^^mg/Lmq/L1

TURBIDITY (HEPHELOMETRIC) EPA 180.1Analytt: S. PFEFFER Anatysfa Data: 08-OECHP5 1«s30 taut: C602.5.0

ParaaatarTURBIDITY

Raault4.0

Dat. Liarit Unitsntu

Saapla CoawntaBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTINCWUSE ELECTRIC CORPORATIOH


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A362139 95 12/7/95 LL 1715 SRW04


Approved : /kuiJi*U yiAtfoUj" 1 Page 2 (last page)


Service Location


Received

04-DEC-95Complete

15-DEC-95Printed

ll-JAN-96

Project Lab IDA361600

PO Number

RN-24352-S 0-00sampled

04-DEC-95 11:25

Report To


Bill To


Saaple DescriptionCLIENT ID: 95 12/4/95 LL 1125 SRW05DESCRIPTION: LEMON LANE RESIDENTIAL WELLSBLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDER

PCB SEPARATOR* FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510B•••••Analyst: t^WfluO^pip'-p^U?;:;::^ : - - . : : : .- - teat; *>Z30,1,0 :

Paraa*terINITIAL WEIGHT OR VOLUMEFINAL VOLUME •:•:•• ••••• •• •• • ••••••• •• ••• • ••••••••••••:•• .- . :• • • : • • • ••••••• ••••• •••••••• - •• :•••••- .-•- :•••••:•••• • ••:•••:

Result1000

••::••$••• -• •,-.•,.:::.•.:;.,,:•,:.::••••••• -.:•,:::-:

Det. Liajit UnitsmL•jjL -..... . .-.. .-.-.. ; . .-..-..

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst! : T, PlUttERT ' f: t:m: ' AnalYirii- Oat«r QS^KH!*i-:; 3% :

Pf«p: PCS SEPARATOtr FUHMEi. UOOIO-tlOjio EXTRACTION: SU844^35l(

P«re*eterPCB AROCHLOR 1016Of-o ADArui AD'":t O^l"- " ' • ' • ' • ' • ' •"• " : ' • • • " • • • • • • • " • • • •••••.••••••• •••:••:•:•:•.•::••:•:•:•:•:•••:•::•.-:•:•"•••:•:•.•:•:•••PCB ARULntOK 1221 - : - • • • . . • . . • • • . • . • . . . • . • • • • . . : • , : : • : • • : : • : • : • : • . • : : • : • : • : • •.-:y;:v:-:-:;x-:PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248

rPCfr AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

ItWtnjBBnt: fiC/ECO»l>Z30.t.O

ResultBDL

-.-.. on t - - • ' • : • ' : • : • ' ' '••'•" . ' ' • • ' • " • • : : • ' • : : •-•:• PUL-. ..• :••••••• . . . •• ,... . . . . • •;•BDLBDLBDLBDLBDLBDL

Testt 03D1XI

Det. LtMit0.000100" rtAftCrt,UUU3U0.00010OidOOIO0.00010Oioooia0.000100^00010

I /••:-•-; • -: ; ." : : . - :

Unitsn»g/L

••••-i- •/»••••••-••••••• ••••••ing/Lmg/Lmg/Lmg/L

::«tg/l'-;:-: Wmg/Lmq/L1

TURBIDITY (NEPHELOMETRIC) EPA 180.1Araiyst: J. STOAKES Analysts Detet OS-DEC-95 lltOO Testi GA02.5.0

PsrMMterTURBIDITY

Result1.3

Det. Li«it Unitsntu

SMple CoMentsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTIHGHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A361600 95 12/4/95 LL 1125 SRH05

11 STANVIX STREET, PITTSBURG, PA 15222-1384

Approved : .du&M tJlR(jtMsr > Page 2 (last page)


Service LocationHERITAGE ENVIRONMENTAL SERVICES, INC.COMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8305

Received08-DEC-95Complete

15-DEC-95Printed

11 -JAN -96

Project Leb IDA362134

PO MotorRN-24352-S 0-00

Soepled06-DEC-95 11:30

Report To


•ill TO


tuple DescriptionCLIENT ID: 95 12/6/95 LL 1130 SRU06DESCRIPTION: LEMON LANE RESIDENTIAL HELLSBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTIONAna ly»t : 0. KISSELC-Wi T» ; : ' Amlysi* '•. Petfet •• Ofc^ 'lll

PerewterINITIAL WEIGHT OR VOLUME

1 FINAL VOLUME •y:-,,.,, :;••-•••,-••; - • • - • - • . , . • - • • • • •.^•^•^^^^•\

?SH846-3510B

Result1000

• -• ,' -•-..:.-• - .....: .••• - - - : • : • !

1:Te«t<::«30it»iDet. Unit

fc-.::1i'/ .'.' '

UnitsmL:.it •-•--- :-•:-• :••:.--.-•-

POLYCHLORINATED BIPHENYLS (PCBS) SH846-8080A;•;•" Ahety»t*-C»::::Cta«l " ;••£••• ••••:<;,;& Amtytf* B«eir,/*1* ?ll:

Prep: MS SEPAMTOKY FUIWEL iJOUIO'LItiUIO EKT«ACTldiliiiiiUiiMl<

PCB AROCHLOR 1016 """" *r

PCB AROCHLOR 1221 \ ;\-PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AROCHLOR 1254 r v;PCB AROCHLOR 1260PCB AROCHLOR 1262

tmmjeent: fiC/«» "•''••. '• -:: ;WPZ30.1.0

ResultBDL

.;::-RDL: "••;-:-:.-.:-.-'::":.-:-.:- ••••::•••-:••• '^BDLBDLBDLBDLBDLBDL

;-t**tj;C8l)t;aL»<

Det. U«it0.0001ft 00050.0001QiOOOl0.0001

:? ^000 J0.0001Oiodoi

r;;-;::.;i:;;:V;;h-':-;-

Unitsmg/Lrtjd/r

• J"S/'*' "••mg/Lmg/Lrag/Lm/i-,-:: -rag/Liiw/L

TURBIDITY (NEPHElOMETaiC) EPA 180.1Anelyst: $. PFEfFER Anetysf* Detet Oa-DK-95 16:SO Test: 0602.5,0

PsreaeterTURBIDITY

Result0.77

Det. Limt Unitsntu

Settle Co nttBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTINCHOUSE ELECTRIC CORPORATIOH


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A362134 95 12/6/95 LL 1130 SRU06


Approved : AfjAAsnJ ' - u i t s A«-J Page 2 (last page)


Sarvica Location

HERITAGE ENVIRONMENTAL SERVICES, INC.COMMERCIAL LABORATORY OPERATIONS7901 U. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8305

Racaivad

08-DEC-95Coaplata

15-DEC-95Printed

ll-JAN-96

Project Lab 10

A362137PO Muter

RN-24352-S 0-00Saapiad

06-DEC-95 15:05

Report To


Bill To


Savpla DMcriptionCLIENT 10: 95 12/6/95 LL 1505 SRW07DESCRIPTION: LEMON LANE RESIDENTIAL WELLSBLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDER

PCS SEPARATOR? FUNNEL LIQUID-LIQUID EXTRACTIONAn«ly»t: 6. KISSEU-WITH ?

: "• Analysis Data: 08*f #:;;tG

ParaoatarINITIAL WEIGHT OR VOLUME

[•FINAL • VOLUME. : • • ' . • - ' -^- •••" •" '• ' ' •-^^•^\

SW846-3510B

Result

1000, ,5, .. - ..,,- ; ;,,,,.

T««tr PZ38;1»<0«t. Liait

H.:p : • ; ' " " : ; ; . . - :

unitsml;.-- :,--:•-:•:

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAiwlyftts C. CUJUSt • An«ly»i« t>«t«M1-«fC^95 Ii tniMnti 6C/ECO ' ' -• ' T«tj tOOt,2.0Prep: KB SEMMTOItr FUNNEL UOUIO-LiaUlO EXTKACTIMt SM»**r3tt1«U>230.>.fl

ParawtarPCB AROCHLOR 1016DrO ADH^UI AD 1991- ' "•' • • • • " : • ' • • ' • : : • : . • • • • . • " • • ' .•• ."•.:•••.••:•:'•:.••.••::•.•:•:•.•:•.•:•.-.•.•.•.•.••rVD MKULnLUK liil .••:.•-•::••;:•••:•:••:•:•:•: •:•:•:•:•:-:•:-:-:•:•.•:.

PCB AROCHLOR 1232PCB AROCHLOR I24ZPCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Ra*ultBDL

:::.BOL -,;.:- •::•;- - ::;:,, ..' •• :-/-,BDLBDLBDLBDLBDLBDL

Dat. Liarit0.00010;00050.00010.00010.00010,00010.00010.0001

Uhita

mg/L19/C: ^2mg/Lmg/Ln»g/LWLmg/Lmq/L

TURBIDITY (NEPHELOMETRIC) EPA 180.1Analyst: s. PFEFFER Analysis Datt: 08-0^9516:30 Test: G602.5.0

Paraa»tarTURBIDITY

Result0.97

Dat. Liaiit Unitsntu

Saaplt CoaawntsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPK(LHESTINGHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A362137 95 12/6/95 LL 1505 SRH07COAHttfltS


Approved : A/j /f J QlrtAUMf=> Page 2 (last page)


Strvic* Location


R«c«iv*d

08-DEC-95Co*pl*t*

15-DEC-95Printed

11 -JAN -96

Project Ub ID

A362135PO t*-^*~~

RN-24352-S 0-00S«Mpi«d

06-OEC-95 13:25

((•port To


BUI To


DescriptionCLIENT ID: 95 12/6/95 LL 1325 SRW08DESCRIPTION: LEMON LANE RESIDENTIAL HELLSBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDER

PCB SEPARATOR* FUNNEL LIQUID-LIQUID EXTRACTION; : Arwlymtt fi. : KISSEU-SMI TH ; : Amiyvi* D*t«t '&&t $«2

ParMMttrINITIAL WEIGHT OR VOLUME

-FINAL:: VOLUME • • • • : " • " • • . • : • • . : •>-: : '•'• - : "- • - . • . . • • . •• :•• : ^mm^

SH846-3510B

RMUlt

1000-y-S-:-,' •: • • - • . •---,:• ,. ,•:,;:,,

;rt*ttr*z3o,u<0*t. LtMit

Y^n4'.'-^Unit*

ml::,«t:-::::-:':-:::;:.:':v::-:--'-:.

POLYCHLORINATED BIPHENYLS (PCBS) SH846-8080A

Pr M PCS S£PMATO«r FUNNEL LlfiOJO-LlflUIO BXUai&iWJ K

PCB AROCHLOR 1016PCB AROCHLOR 1221 ^^m '. • \ ;: mmPCB AROCHLOR 1232oro ADnrui no 1949 . . . . . .ruo AKULnLUK ••: LtAt. :.. . .:• • . : . . : : : . :PCB AROCHLOR 1248PCB AROCHLOR U54PCB AROCHLOR 1260PCB AROCHLOR 1262

»>zio.i.a • ' • : ; ; :

RMUlt

BDL• .• •. Bftf . . .• .• • v ." '. .'.'.•.•. — . / . • • • ' .'.'. . •. . .•.'• ' " Dl fcv

BDL- • ••pril ' • . . • • • • . • . - . • • . . . • • • . , . . . • • . • • .D U L • • • • • . • • . • • . . - . . • . - . - • • • • . . •

BDLBDLBDLBDL

;;§ |D«t. Li«it

0.0001• OvOOOS-

0.0001Q nnnv:, UUUl

0.0001OvOOOl0.00010.0001

Si;!!?:'-

Unit*

iiig/t • ' ' •'• • 'mg/Lnirr/l:.mg/LW/L

rag/Lina/L

TURBIDITYAnilytt: S.

(NEPHELOMETRIC)PFEFFER A

EPAnttyst

180.1• 0»t»: OS-DEC-95 16:30 Tot

TURBIDITY "r"" *'R«*ult

0.58D*t. Li«

: C602.5.0

it Unit*ntu

BDL Below Detection Unit



Additional copies of this report sent to:RUSS C£PKOt HESTINCHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A362135 95 12/6/95 LL 1325 SRW08CoMMnts


ActsO/LMJApproved : tu2/L<x J^tiAAAt^ Page 2 (last page)


Service Location


Received

06-DEC-95Complete

21-PEC-95Printed

21-DEC-95

Project Lab 10

A361912PC Number


05-DEC-95 10:10

Report To


Bill To



PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510BAnalyst: J. GRIFFIN Analysis Date: 07-DEC-95 Test: P230.1.0

Parameter

INITIAL WEIGHT OR VOLUMEFINAL VOLUME

Result10005

Det. Limit UnitsmlmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: E. B1NGHAM Analysis Date: 09-DEC-95 Instrument: GC/ECD Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SU846-3510B P230.1.0



Det. Limit0.000100.000500.000100.000100.000100.000100.000100.00010

Units

mg/Lmg/Lmg/Lmg/Lmg/L»ng/Lmg/Lmq/L

TURBIDITY (NEPHELOMETRIC) EPA 180.1Analyst: J. STOAKES Analysis Date: 07- DEC -95 10:00 Test: G602.5.0

ParameterTURBIDITY

Result0.44

Det. Limit Unitsntu






HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A361912 95 12/5/95 LL 1010 SRW09Sample Conrnents


Approved : O'U WM l' \( ^ Page 2 (last page)


Service Location


Received

08-DEC-95COBplate

15-DEC-95Printed

ll-JAN-96

Project Lab 10A362141

PO timber

RN-24352-S 0-00Sasplad

07-DEC-95 18:15

••port To


Bill To


SMpU DescriptionCLIENT ID: 95 12/7/95 LL 1815 SRW10DESCRIPTION: LEMON LANE RESIDENTIAL HELLSBLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTIONAnalyst: <5. HSSEU>»!T» Analyml* Data: . 08-ftEC'95 1$

ParameterINITIAL WEIGHT OR VOLUMEFINAL VOLUME •;> "••:"^^4^-,- : ,:- ; ;.

SWa46-3510B

Result1000

:."5'- ' - • - • ' :•

testt »»Z30.1»<Dat. LiMit

>

Unit*raL

• tat

POLYCHLORINATED BIPHEHYLS (PCB5) SH846-8080AAnalysts C. ttOUSE : : Analysis t^artl^W^ Imtruaant: fiC/ICO : ' • T*sti 0301 .i.fl 'Pnspa PCS SEPARATOtr RMKL UOUIO-LIOUIO DCTRACTldKii-JJli iBlMii-MaO.l.O-::

PCB AROCHLOR 1016PCB AROCHLOR 1221 •PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248

r PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

ResultBDL

:-,BOL. . : • • " • . : : ; ;::::.: • • • " . -BDLBDLBDLBDLBDLBDL

Dat. Lia>it

0.0001

0:00050.0001OiOQOl0.00010,00010.00010:0001

Unitsmg/Lrtg/Lmg/Lmg/Lmg/Ling/Lmg/Lmq/L

TURBlDin (NEPHEUOMETR1C) EPA 180.1Analyst: $. PFEFFER Analysis Datai 08-DEC-95 16:30 Tast: C6d2.5.0

ParanatarTURBIDITY

Result0.52

Dat. Liaiit Unitsntu




Additional copies of this report sent to:RUSS CEPKO, HESTINGl'OUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A362141 95 12/7/95 LL 1815 SRW10CoMntt


Approved : /l Ji&vJ fyM J tfa Page 2 (last page)


Service Location


Received

04-DEC-95Complete

15-DEC-95Printed

ll-JAN-96

Project Lab 10

A361603PO tkmtttr


04-DEC-95 09:15

Report To


Bill To


Staple DescriptionCLIENT ID: 95 12/4/95 LL 0915 SRW11BLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDER

PCS SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTIONAnalyst: ». UOCO :.- • • .. -.-•' *n«ly«f« D*ter OHfcC-95

ParameterINITIAL WEIGHT OR VOLUMEFINAL VOLUME ; :

SW846-3510B

Result1000

: -5: ' - " : - : - '

: Teat: >23< f .«

Det. Lla>it

*M::-:-:-

UniteBL

^..-v:,, ,, . .

POLYCHLOR1NATED BIPHENYLS (PCBS) SH846-8080A:;• ;: : Analyst: T, PIHOCEKT : : : : Analysis Octet 05>MC-95 f- . :: :. •• •: '••

Prep: PCS SBPAJUTORV FUMMEL LtOUlO'LlQUIO RTl lrtt ««««XS51I

PereoeterPCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242 :PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Instrument: CC/EOt :WPZ30.UO

ResultBDLB D L • • • • • : • : • ' • ^•^••^••^'- .BDL

' BDL . . • • • • : : : . : : ; • • • : . . . . • • • • . • : . : : - . : .

BDLBDLBDLBDL

Testt OJ01.2J

Oet. Limit0.00010OiOOOSO0.00010OV000100.00010o;oooio0.000100.00010

Jlllr'- :.':': :

Unitsrog/Ling/Lmg/L

S/Ling/L

iq/L

TURBIDITY (NEPHELOMETRIC) EPA 180.1Anelyst: J, STOAJCES Analyst* D«e: 05-OEC-95 13:00 Test: C60Z.5.0

ParaewterTURBIDITY

Result1.1

Det. Li*it Unitsntu

Saaple CoMeentsBDL Below Detection Limit

Saaple chain of custody number 27759.


Additional copies of this report sent to:RUSS CEPKO, UESTIHGHOUSE ELECTRIC CORPORATIOH11 STANHIX STREET, PITTSBURG. PA 15222-1384


HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID: A361603 95 12/4/95 LL 0915 SRU11SMplt CoMNnt*

Approved Page 2 (last page)


Service Location


Received

04-DEC-95Complete

15-DEC-95Printed

11 -JAN -96

Project Lib ID

A361605PO Ik MT

RN-24352-S 0-00Seipted

04-DEC-95 10:40

Report To


Bill To


Swple DescriptionCLIENT ID: 95 12/4/95 LL 1040 SRW12BLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION.:. Analyst; J. GRIFFIN ' . • : ' • . • • ; . : • • Amiysfs DMtr ^C :i%:: '••:.::

PsraMterINITIAL WEIGHT OR VOLUMEFINAL VOLUME • . • : • • • • - . . ' - . • : ; ' ' - : ' -"v^ mz$z:; :~-

SH846-3510&

Result

1000- : - 5 : . ' • : - - : - : : ' - ' - : - - - ' - . : -

Testt KOO.W

Det. Halt

y:-'::;:>::vr, . -.p?: ; ::?: •''•••-: ..: -:: :- - ::•:::•:•• . . .

UnitsnL>il :; . : > , . - : . .

POLYCHLORINATEO BIPHENYLS (PCBS) SW84fi-8080AAne4y»t: E. ilUCHAIt . \.'"."^3 Ar»ly»i« OJrte^ 06^C |:i;:::,::Prep: PCS SEPAJUTOKT FUtUttt LUKllO-UOUlD WTJUkaiOt «U5«A*351<

Psr«wterPCB AROCHLOR 1016PCB AROCHLOR 1221 :PCB AROCHLOR 1232PCB AROCHLOR 1242 ;PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

' : {nstruBinU GC/ttS : : : :" :: "' ' ;

W-W30.1.0- : • • : • - -J ^- - '" • • ' • ' : . -

ResultBDL

BDLBDLBDLBDLBDLBDLBDL

: '1|Det. Liait

0.000100.000500.000100.000100.000100.000100.000100.00010

Illi; :•;••:•;<•;.:'

Unitsmg/L

ml/Lrog/Lmg/L

;fl>g/L

1M/L

TURBIDITY (NEPHELOMETRIC) EPA 180.1Anelysti J. STOAKES Analysts D*tei 05-OEC-95 15:00

PerwMter

TURBIDITY

: .- • 'Reeult

2.7

Test; C60J

Det. limit

,i:::-:::;- :;;.-. I

!«Si6'" '

Unitsntu

Saiple CoMMnts




Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATION11 STANHIX STREET, PITTSBURG, PA 15222-1384


HERITAGE ENVIRONMEHTAL SERVICES, INC. Sample ID: A361605 95 12/4/95 LL 1040 SRH12nt*

Approved : /JU toJ -VmwJ.fK-J Page 2 (last page)


Service Location


Received

04-DEC-95Coaplete

15-DEC-95Printed

11 -JAN -96

Project Lab ID

A361606PO Muaber


04-OEC-95 10:40

Report To


Bill To


Saaple DescriptionCLIENT ID: 95 12/4/95 LL 1040 DRW12BLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDER

PCS SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION. •;;; Analyst: Ogivtnoos "•. "• : :: : :• xfe^^/lmlyrf*^ .-r

ParaMterINITIAL WEIGHT OR VOLUMEFINAL; VOLUME . •. ' ^KiMri

SW846-3510B

Result

10005 ' - • ' - . • ' . ' :

Te»ti rao.t.tDet. Lisiit

If;?-'- '"

UnitsraLrot

POLYCHLOR1NATED B1PHENYLS (PCB51 SU846^8Q80AAnalystvT. PIKOCERT . ' Ar»lysU.IUrtei;p«(||5|:i:;::::':Prep: PCS SEPARATOR* fUMWEl ItQUIO-UQUtO EXtiwCriiiiittiiii Sill

PCB AROCHLOR 1016DrD ADfVUl no 1-991 •'• '''•'•'•:•-•:•:•:•:•:•:•'•:'•:•:•:••:•:•• ••• . • '•.rLB AKULnLUK . lc£.l . . : : . : : . - . . • . . . . . • . . . .PCB AROCHLOR 1232PCB AROCHLOR 1Z42 ?; ?PCB AROCHLOR 1248PCB AROCHLOR 1254 ;-PCB AROCHLOR 1260PCB AROCHLOR 1262

inetruesnt: CC/EC&WPZW.1.0

ResultBDL

. • . nn I ' ' "•' ' '•' ' • • " • - • • '•'• -'• •'•'• •'• • - •' '• '.'-' '•'•'•" "•'•'•'•'•'-• • JJU1_ • •

BDL: BDL • — : > . ; : " • • ; • • • : ^ ->>->;v

BDLBDLBDLBDL

Tests 030t.2.«

Det. Liaiit0.00010O nfifiCK.UUvOU0.00010OiOOOlO0.000100.000100.000100.00010

tf ' •'. . . . . . .

Units

'"•VI /I'" " ••"•"•' "-'•• {||L|/ L •-""•'•"•••'-'"-'

mg/L

^LS/Lmq/L

TURBIDITY (NEPHELOMETRIC) EPA 180. 1Analyst j J. STDAKES Analysts Date: OS^WC-95 13:00 T«sti 6602,5.0

ParaaMtarTURBIDITY

Result2.7

Det. Liaiit Unitsntu

Savpla CoaairntsBDL Below Detection Unit



Additional copies of this report sent to:RUSS CEPKO, UESTINGHOUSE ELECTRIC CORPORATION11 STANHIX STREET, PITTSBURG, PA 15222-1384


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361606 95 12/4/95 LL 1040 ORU1Ztt

Approved/

Page 2 (last page)


Service Location


Received

04-DEC-95Complete

15-DEC-95Printed

11 -JAN -96

Project Lab 10

A361607PO Nuaber

RN-24352-S 0-00Sagpitd

04-DEC-95 10:40

Report To


Bill To


Saaple DescriptionCLIENT 10: 95 12/4/95 LL 1040 ERW12BLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDER

PCB SEPARATOR* FUNNEL LIQUID-LIQUID EXTRACTION• : : Analyst: ». WOOD • • : • - : : : : Anelymi* Detet t6*KC*9*m: .

INITIAL WEIGHT OR VOLUME^FINAL VOLUME " :• •. v .- . '• ••••\^:^^m^^

SW846-3510B

Result1000

. : . 5-:"' ' . • : - . • • . : • • . . - • • . . - • • • . •

Teat: Vztt.fef

Det. Liait

&':"•{• ' • • ' . ' • •Units

nLmt

POLYCHLORIMATED BIPHENYLS (PCBS) SH846-8080A•: ' : "" Analyst:: . T. : flHCICERT : , Analysis Octet ' OS4iB6^J!f . -\'J]

Prep; PCS SEPARATORY FUNMEi LtWJO-LIOUJO EXTIWCTtti i<8t* S51<

ParsawterPCB AROCHLOR 1016PCB AROCHLOR 1221 ;PCB AROCHLOR 1232PCB AROCHLOR 1242 -^•^::-.:?i;"rPCB AROCHLOR 1248PCB AROCHLOR 1254

| PCB AROCHLOR 1260PCB AROCHLOR i 262

inetruasnti CC/SCD*«00,U05:':: - • • • - - • •

ResultBDLBDLBDLBOLBDLBDLBDLBDL

Test: 0501.2,1'"•. :': .:•..:;:-:'.

Det. Listit0.000100;000500.00010o^oooio;0.00010OiOOOIO0.00010o;oooio

£JV|:-.. '•'.'

Unitsmg/L*g/L•B/Ling/Lrag/L:lg/L

wg/Lroq/L


TURBIDITY

(HEPHELOMETRIC) EPA 180.1STOAttS Analysts Date: 05-OEC-95 13:00 tests 66(8,5*0

Paraaieter Result0.35

Oet. Lisiit Unitsntu

Saaple itsBDL Below Detection Unit



Additional copies of this report sent to:RUSS CEPKO, HESJINGHOUSE ELECTRIC CORPORATIONII STAHHIX STREET. °ITTSBURG. PA 15222-1384


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361607 95 12/4/95 LL 1040 ERH12



Service Location


Received

04-DEC-95Ccepltte

15-DEC-95Printed

ll-JAN-96

Project Lab ID

A361604PO Ifeaber

RN-24352-S 0-00Seapled

04-DEC-95 10:10

Report To


•ill To


Seaple DescriptionCLIENT ID: 95 12/4/95 LL 1010 SRW13BLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION:; ; •;&•{ ynti :: »; WXD , : : ; ;• : : :•; : ;: . : ; : ; . . : -; Anetys f e Deter • OS-DBC<«SS-:: :-": ; -


: FINAL-. VOLUME. • .,•: ::>>: " •. • •;•••• - : ; i mx^ •••••••

5*846-35108

Result1000

: • 5 - - . . : . • • • • . .

:;-::X:::."l;!Mv:$Terts P2M,t,(

Det. Lt«it

>.&;:j:; ;•:-.'•• ••; :-.Units

mL••Sit"" • ' " : : :" ' :

1

POLYCHLORINATED WPHEHYLS (PCBS) SH846-B080A i |Anaiystt T. fimXEKT • ...: Analysts B«t«i."«pt |>f :.;:.;-:.. Instrument: CC/ECP • ' Test: <S0^2iO .Prep: ':p»:«IWTaw^WMia/ilWIO-UOUJO.:^ ' ' ' ' : - : - • ' • • " ' : ; o -??-^f-^--FN^ : ' ' ' •

Psraawter

PCB AROCHLOR 1016PCB AROCHlfiR 1221PCB AROCHLOR 1232PCB AROCHlOfr 1Z42PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

ResultBDL

::BDL ..;..i::::; ^f-O.-^;

BDL

BDLBDLBDLBDL

Det. Liait0.00010diboosb0.00010oioooio:0.00010O^OOOIO0.00010o; oooio

Unitsjg/L

«g/Lng/LJ9/L

mq/L

TURBIDITY (HEPHELOMETRIC) EPA 180.1Analysts J. STOAICES Analy«{« Date? 05-OEC-W 13:00 Test! G60Z,5.0

ParaMeter

TURBIDITYResult

1.5

Det. Linit Unitsntu

Saeple Co itsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATION11 STAWIX STREET' PITTSBURG, PA 15222-1384


HERITAGE ENVIRONMENTAL SERVICES, INC. Sanple ID: A361604 95 12/4/95 LL 1010 SRW13

tB

Approved : dUMfrJ MJlAULf<^ Page 2 (last page)


Service Location

HERITAGE ENVIRONMENTAL SERVICES,COMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8305

INC.Received

06-DEC-95Complete

21-DEC-95Printed

21-DEC-95

Project Lab ID

A361910PO Number


04-DEC-95 17:45

Report To


Bill To



PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SH846-3510BAnalyst: J. GRIFFIM Analysis Date: 07-DEC-95 Test: P230.1.0

Parameter


Result10005

Det. Limit Units

mLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: E. BINGHAN Analysis Date: 09-OEC-95 instrument: GC/ECD Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SU&D-3510B P230.1.0

Parameter

PCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Result

BDLBDLBDLBDLBDLBDLBDLBDL

Det. Limit0.000100.000500.000100.000100.000100.000100.000100.00010

Units

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmq/L

TURBIDITY (NEPHELOMEFRIC) EPA 180.1Analyst: J. STOAKES Analysis Date: 07-DEC-9S 10:00 Test: G602.S.O

Parameter

TURBIDITYResult

0.76Det. Limit Units

ntu




Additional copies of this report sent to:RUSS CEPKO, HESTIhSHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A361910 95 12/4/95 LL 1745 SRHHSample Comments


0, >1 A&Approved : / , >1 & / r\,+-^^ Page 2 (last page)


Service Location


Received

06-DEC-95Complete

18-DEC-95Printed

18-DEC-95

Project Lab ID

A361908PO Number


04-DEC-95 15:20

Report To


•Bill To




Parameter


Result10005

Oet. Limit Units

mLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: E. BINGHAM Analysis Date: 09-DEC-95 Instrument: GC/ECD Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510B PZ30.1.0

Parameter



Det. Limit

0.000100.000500.000100.000100.000100.000100.000100.00010



TURBIDITY


Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result0.60

Det. Limit Units

ntu






HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361908 95 12/4/95 LL 1520 SRW15Sample Comments


Approved : ' V/U^YNQJ. /y-"QV ^\ 1 - Page 2 (last page)


Smrvics Location


Rscaivsd

04-OEC-95COSplSt*

15-DEC-95Printed

11 -JAN -96

Project Lab ID

A361608PO Huster

RN-24352-S 0-00Sasplsd

04-DEC-95 11:15

Report To


Bill To


Saapl* DescriptionCLIENT ID: 95 12/4/95 LL 1115 SRW16BLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION: :: • Xri«lY»t J ;: m\ VJOW m : ; -: : .; :: :. : :: < J :. :"- *n*lyiM « Mitt r W'SK tip f .

ParssMterINITIAL HEIGHT OR VOLUME

1 FINAL VOLUME ' ' '" ' : - ' : : ^m^^mm-r \

SW846-3510B

Result

1000• " 5 - • • . : : . - : " . " • • ' -

.:.T«*t*:'«BO.W

D«t. LiMit

&$''.

Unit*mLroL

1

KOLTCHLUR1KATHJ BIPHENYL5 {fCBS) 5*W46-8Q80AAft»ly»ti T^ PKCKEBT .' .. - .:;•:... Arwty»i«:Ort«i:'05^»iC| S;:f ;;;•::;;;Prtpt PCS SCPMUTORT FUNNEL UOUIO-tlOUlft WTWCTlOlK s iii-JSlK

PirMMttrPCB AROCHLOR 1016PCB AROCHU1R 1221 ;PCB AROCHLOR 1232PCB AROCHLOR 1242 ' ' " : " v : V 7-^y^"PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Irtitruwntt «VECD . , - ' - :

WWM.t.O

RMUlt

BDL.. BDL, . • • • • ' . ' • : : • • • • • • • • : • ; • : • , • : • • • • • , . ' . : - : :;:

BDL.-'BOL'" "•'•'•' . . : : : . . : . - - - - . . ' " . . ' : ' : : ' : .:•::

BDLBDLBDLBDL

Twt: <BOI.2.«

D*t. LtBit0.00010OiOOOSO0.00010OiOOOlO0.00010OiOOOIO0.000100.00010

^ '..' ;'..

Unitsng/Lm/&--K:mg/Lm/l ••:,:.,

mg/L:ing/Lmg/Lmq/L


TURBIDITY

(NEPHELOMETRIC) EPA 180.1JTOAKES An»ty»t« 0««s 05^0£C-95 13:00 T«*ti 6602,5

Pars*wter Rtsult74

D«t. Li«it

,:o:V

Unitsntu

1:5 DILUTION

Sasplt ConasntsBDL Below Detection Limit



Additional copies of this report sent to:


HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID: A361608 95 12/4/95 LL 1115 SRH16Saaplt CoMnts

RUSS CEPKO, VESTINGHOUSE ELECTRIC CORPORATION11 STAMIIX STREET, PITTSBURG, PA 15222-1384

Approved : /ujJOAU ^JLtfAiAJs/ Page 2 (last page)


Service Location


Received

06-DEC-95Complete

18-DRC-95Printed

18-DEC-95

Project Lab ID

A361913PO Nifnber


05-DEC-95 11:25

Report To


Bill To



PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SH846-3510BAnalyst: J. DANIELSON Analysis Date: 07- DEC -95 Test: P230.1.0


Result10005


POLYCHLORINATED BIPHENYLS (PCBS) SU846-8080AAnalyst: B. UOOO Analysis Date: 11-DEC-95 Instrument: GC/ECD Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510B P230.1.0

Parameter



Det. Limit0.000100.000500.000100.000100.000100.000100.000100.00010



TURBIDITY


Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result0.68

Det. Limit Unitsntu






HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361913 95 12/5/95 LL 1125 SRW17Sample Comments !


Approved : / (^ rt/Yx^Y^ yV L*- . Page 2 (last page)


Service Location


Received

04-DEC-95Complete

15-DEC-95Printed

11 -JAN -96

Project Leb 10

A361609PO Htflber

RN-24352-S 0-00Soiled

04-OEC-95 12:45

Report To


•ill To


Seaple Description

CLIENT ID: 95 12/4/95 LL 1245 SRW18BLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTIONi Analyst: »; : WOOD x : • • • . • ; • : .. . • • ' • • ; ;- ? Analysts Datei ; OS*B6Cr9S ; i . •;

ParejaeterINITIAL WEIGHT OR VOLUMEFINAL VOLUME • . . - - • ••:: • - • . - - •"..: - • : • • . : . • ' •^^•••••. :•::::•:--,- • ;

SM846-3510B

Result1000

o, 5''- • • • • • • . : : • . : • - • • • • • • - . • • • ' •

Tests P2M.1.<

Det. Lfsrit

&U :?:/•'.:•:< ;.'::!'

UnitsmL,'fllt:: :•.•..-•:.--•-:-: :•• .

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnely»trT. PHtOCHlT ; . : »M \ntUMt-9t ^y::i.:Prep: PC8 SCPAJUTORY WWttt LtOOtO'LlOJlO EXTJWCTtl* **W-351I

Parss»terPCB AROCHLOR 1016

•'•:PrR::'fiRflTHi-hD/::li?71:'' ' '- •• ' : " •' • '- •••>.>>'•>.-::•':'•:.•:.•:•.•:•:•••••:•.••:•:•ri/o /\Kwi>riuuK mi . . . . . . ...... ...... .PCB AROCHLOR 1232PCB AROCHLOR 1Z4Z !PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

:,: Inetrusentt : OC/iCD* Y- ' ; : : < - ;•: '• . . .JiPZM.UO

ResultBDLpniDUl. • . - • • . • - . - . . • . - . . . - •

BDLBDLBDLBDLBDLBDL

Teett <OO$Jul

Oet. Licit0.00010O flAft«5ii

0.00010OiOOQIO0.000100.000100.000100.00010

tipt:lH-:;:|i;:;:-i:--

Unita»g/Lna/t.«W. «--:.-:•:'•..•'•.:•-.-.-:"9/Ling/tmg/Lmg/Ln»9/LHH/L

TURBIDITY (NEPHELOHETRIC) EPA 180. 1Analyst! J. STOMCES Analysis Date: OS-OEC-95 13:00 Testj C602.5.0

PareaatsrTURBIDITY

Result0.76

Oet. Lisiit Unitsntu

Ssaple Consents




Additional copies of this report sent to:RUSS CEPKO, HESTIHGHOUSE ELECTRIC CORPORATION11 STANUIX STREET, "ITTSBURG, PA 15222-1384


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361609 95 12/4/95 LL 1245 SRH18

Approved Jtu&rJ fefc? _ Page 2 (last page)


Service Location


Received

06-DEC-95Complete

18-DEC-95Printed

18-DEC-95

Project Lab ID

A361904PO Number


04-DEC-95 15:30

Report To


Bill To





Result

10005

Det. Limit Units

mLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: E. 8INGHAM Analysis Date: 09-DEC-95 Instrument: GC/ECD Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SU846-3510B P230.1.0


Result


Det. Limit

0.000100.000500.000100.000100.000100.000100.000100.00010

Units



TURBIDITY


Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result0.78

Det. Limit Units

ntu






HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A361904 95 12/4/95 LL 1530 SRW19Comments


Approved : Page 2 (last page)


Service Location


Received

06-DEC-95Complete

18-DEC-95Printed

18-DEC-95

Project Lab ID

A361905PO Number


04-DEC-95 15:30

Report To


Bill To


Sample DescriptionCLIENT ID: 95 12/4/95 LL 1530 DRW19DESCRIPTION: BLOOMINGTON PROJECTBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDER


Parameter


Result

10005

Oct. Limit Units

mLml

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: E. BINGHAM Analysis Date: 09-DEC-95 Instrument: GC/ECD Test: 0301.2.0

Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510B P230.1.0

Parameter


Result


Det. Limit

0.000100.000500.000100.000100.000100.000100.000100.00010

Units



TURBIDITY

(NEPHELOMETKIC) EPA 180.STOAKES Analysis Date

Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result

0.60

Det. Limit Units

ntu




Additional copies of this report sent to:RUSS CEPKO. HESTINCMUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361905 95 12/4/95 LL 1530 DRW19Sanple Conments




Service Location


Received

06-DEC-95Complete

18-DEC-95Printed

18-DEC-95

Project Lab ID

A361906PO Number


04-DEC-95 15:30

Report To


Bill To


Sample DescriptionCLIENT ID: 95 12/4/95 LL 1530 ERW19DESCRIPTION: BLOOMINGTON PROJECTBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510BAnalyst: J. GRIFFIN Analysis Date: 07- DEC -95 Test: P230.1.0

Parameter


Result10005


POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: E. BINGHAH Analysis Date: 09-DEC-9S Instrument: GC/ECD Test: 0301.2.0Prep: PCB SEPARATOR? FUNNEL LIQUID-LIQUID EXTRACTION SU846-3510B P230.1.0

Parameter



Det. Limit0.000100.000500.000100.000100.000100.000100.000100.00010



TURBIDITY


Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result


ntu






HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361906 95 12/4/95 LL 1530 ERW19Sample Comments




Service Location


Received

08-DEC-95Coiplete

15-OEC-95Printed

ll-JAN-96

Project Lab ID

A362133PO Nuaber

RN-24352-S 0-00Saaplad

06-DEC-95 09:10

Report To


BUI To


(••pi* DescriptionCLIENT ID: 95 12/6/95 LL 0910 SRW20DESCRIPTION: LEMON LANE RESIDENTIAL WELLSBLANKET ORDER RELEASE »: NOT RECEIVED WITH ORDER

PCB SEPARATORY RJNNEL LIQUID-LIQUID EXTRACTION: :: Analyst:1 C. HSSELt- Wl T8 ". • : • .: ' : - : Analyst I Datet : »>6eC-V5 i; : V:

Parameter

INITIAL WEIGHT OR VOLUME-FINAL "VOLUME"- --.•:•..:•.:• . . . , • • : : . - • : . • . • : • : - • • • , . . - .. :y:.^.^. ;:.;.•;>. v..- .

SH846-3510B

Result

1000- -5- - " ..•••..•-.-•-, -- ' •:-.

Te*t« «30,U

Det. Liarit

> • ; : • ; • • . ' • ; : : .'Units

raL.mt •:•,:::•-:-,::-•:-:-•

POLVCHLORINATED BIPHEHYLS (PCBS) SH846?B08PJ ¥l '1f'.:

PrepV Ftt SEPAft r RJM^ : :: :" •'':-V:;-v:^ Hj.-;.. ,:.

Psraaeter

PCB AROCHLOR 1016PCB AROCHLOR 1221 < <m^mtmPCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248

1 PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Result

BDL

BDLBDLBDLBDLBDLBDL

Det. L1a)it0.0001

OiOOOS0.00010,00010.00010;000l0.00010:0001

Units

Ig/Lmg/Lmg/Lmg/L<ng/Lmg/Lmq/L1

TURBIDITY (NEPHELOMETRIC) EPA 180.1Analyst: $. PFEFFER Analysts Date: 0»*DEC-«5 1AsSO Test: 0602.5.0

Paranater

TURBIDITYResult

1.3Det. Limit Units

ntu

CoaaantsBDL Below Detection Limit

Simple chain of custody number 27762.




HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A362133 95 12/6/9S LL 0910 SRM20

11 STAWIX STREET, PITTSBURG, PA 15222-1384

Approved : 4uMl*J WLfffuutt Page 2 (last page)



Received

08-DEC-95Complete

15-DEC-95Printed

11 -JAN -96

Project Lab ID

A362138PO Huatjer

RN-24352-S 0-00Sealed

06-DEC-95 15:25

Report To


BUI To


Staple DescriptionCLIENT ID: 95 12/6/95 LL 1525 SRW21DESCRIPTION: LEMON LANE RESIDENTIAL WELLSBLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION' Analyst; fi.KISSEU-WITB Analysis Date: OB-OK-^S-S*::'

ParaMterINITIAL WEIGHT OR VOLUMEFINAL VOLUME • :^. ^ ^m-- •• : • • ;>-^:: • ^ - ••, :••

SH846-3510B

Result1000

,.5-,. . • • : . : • , , • ..„ ,

Teat; W30.U

Det. Limit

):'':-::'"

unitsmlf l i t . . -

POLYCHLORINATED BIPHEHYLS (PCBS) SW846-8080AAnalyst* C. : ttOUSC : . :;, • . : : ; ; : -ip :; Analysis Date: H 'WC'W "V"Prep: KB SEPAftATOty nMMEL LJflUID-LIflUIO DOSACTICal SU844-351I

Paraavter

PCB AROCHLOR 1016P C S AROCHLOR 1221 : : : : : : : : :PCB AROCHLOR 1232PCB AROCHLOR 1Z4ZPCB AROCHLOR 1248PCB AROCHLOR 1Z54PCB AROCHLOR 1260PCB AROCHLOR 1262

instruaant: 6C/EC&»pao.i.o

Result

BDL-,,:.PUl.-- .- •• : ,• : . ••: •. ., . •: ,:. •"

BDLBDLBDLBDLBDLBDL

Test! 0301 .Z,(

Det. Ltait0.0001

.UUU90.0001Q^OOOI0.00010,00010.00010;d001

):'":::-':

Units«g/Lrog/Lmg/Ling/Lmg/Lmg/Lmg/Lnw/L

TURBIDITY (HEPHELOMETRIC) EPA 180.1Analyst: S. PFEFfE* Analysts Date: OS«0€C-*S 16:30 Test i fi602. 5.0

Parameter

TURBIDITYResult

0.50Det. Liaiit Units

ntu

Swplt CementsBDL Below Detection Limit





HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A362138 95 12/6/95 LL 1525 SRH21Conninti


Approved : /J/jjtAAtJ / i fJjt Cj ^ Page 2 (last page)


Service Location


Received

06-DEC-95Complete

18-DEC-95Printed

18-DEC-95

Project Lab ID

A361914PO Number


05-DEC-95 13:10

Report To


B i l l To



PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SH846-3510BAnalyst: J. DANIELSOM Analysis Date: 07-DEC-95 Test: P230.1.0

Parameter


Result

10005

Det. Limit Units

mLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: B. UOOO Analysis Date: 11 -DEC -95 Instrument: GC/ECD Test: 0301.2.0

Prep: PCB SEPARATOR FUNNEL LIQUID -LIQUID EXTRACTION SW846-3510B P230.1.0

Parameter


Result


Det. Limit

0.000100.000500.000100.000100.000100.000100.000100.00010

Units



TURBIDITY

(NEPHELOMETKIC) EPA 180.STOAKES Analysis Date

Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result


ntu




Additional copies of this report sent to:RUSS CEPKO, UESTINCMUSE ELECTRIC CORPORATION




f]

Approved : I _VU .•V\jrX 2 L y] ^^^ Page 2 (last page)


S*rvic« Location


Received

04-DEC-95Coeplete

15-DEC-95Primtd

11 -JAN -96

Project Leh ID

A361601PO IkNber

RN-24352-S 0-00Sealed

04-DEC-95 08:30

Report To


CLIENT ID: 95 12/4/95 LL 0830 SRW23A*BLANKET ORDER RELEASE *: NOT RECEIVED

Bill To


Description

WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510B•:.:'Ar»iV»iu. "•.'. M0» ?;.:;: •'' ^v;^-^;::'^:/to»ly»f<i Mit»V «*&tC*i«3v • ; • • : • ' • : v:: • ' •' ' T«»t: P23Q.1.0: ' -

PerwwterINITIAL WEIGHT OR VOLUMEFINAL VOLUME •••': ^-- .-• • • . : -: : • . ' ' '"' :mm^U •

Result1000

: • • • • • 5 : ; • - • • • • • • • ' • • • • : '

Oct. Liait UnitsnLffit

1

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080A: :: Ann4y»ts : T. n«CKE«T : . . •:.• : . • ;.;:;•; Amlysis Dat*: ' (HWbic^W ": ' - -.:; • . iMtruMnU fiC/ECD • • • ' . • T»*t J CflOt.2.& • : ' :; .• " • ' .

pp»p: P« WWUT08Y HWMEl LIQUID -LIQUID EXTIUCTtii»liy«i6 R51« WM.t.O :!

PSTMNt«r

PCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 124ZPCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

••suitBDL

:;-;::,BDL ,., ..,.,,,.:.,:,..;.:,:

BDLBDLBDLBDLBDLBDL

D*t, U»it0.000100^000500.00010o;oooio0.000100;000100.000100.00010

unit*mg/L::mm::mmg/Ljpg/Lmg/Lmti I.mg/LmoA

TURBIDITY (NEPHELOMETRIC) EPA 180.1Anslyst: 4. STOAJCES Analysts 0«t«: Q5-*CC-95 IJiOO T«t: WOZ.5,0

ParMMtcrTURBIDITY

Result2.3

D«t. Liait Unitsntu

SABplt COMMntSBDL Below Detection Unit



Additional copies of this report sent to:RUSS CEPKO, WESTINGHOUSE ELECTRIC CORPORATION11 STANVIX STREET. PITTSBURG. PA 15222-1384


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361601 95 12/4/95 LL 0830 SRU23ASaapl* CoMMnts



Service Location


Received

06-DEC-95Complete

18-OEC-95Printed

18-DEC-95

Project Lab ID

I A361907PO Number


04-DEC-95 15:00

Report To


Bill To


Sample DescriptionCLIENT ID: 95 12/4/95 LL 1500 SRW23BDESCRIPTION: BLOOMINGTON PROJECTBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDER



Result10005


POLYCHLORINATED BIPHENYLS (PCBS) SU846-8080AAnalyst: E. B1NGHAH Analysis Date: 09-DEC-95 Instrument: GC/ECO Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SUS46-35108 P230.1.0



Det. Limit0.000100.000500.000100.000100.000100.000100.000100.00010



TURBIDITY

(NEPHELOMETiUC) EPA 180.STOAKES Analysis Date

Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result2.4

Det. Limit Uni tsntu




Additional copies of this report sent to:RUSS CEPKO, VESTINCHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361907 95 12/4/95 LL 1500 SRW23BSample Comments

11 STAMIX STREET, PITTSBURG, PA 15222-1384



Service Location


Received

04-DEC-95Complete

15-OEC-95Prin.ad

11- JAN -96

Project Lab 10

A361602PO Maber


04-DEC-95 08:45

Report To


Bill To


Seaple DescriptionCLIENT ID: 95 12/4/95 LL 0845 SRW23CBLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDER

PCB SEPARATOR* FUNNEL LIQUID-LIQUID EXTRACTION*n«ty»ti ». WOOO - ;: ::: •••• . - . ' • • An«ty»l» D*t«: 0!P-OK'«5

ParameterINITIAL WEIGHT OR VOLUMEFINAL VOLUME • : . . • • • ... " :•••• : •. : .-w .- tmmmm?- \

SH846-3510B

Result1000

: - . s - • - . . - : • • • • • • • . - • : • . • .

Tests PZHU.i

Det. Li«it

H-::. > • " • : • •Units

nL••tet::-:- •' ::"

1

POLYCHLORINATEO BIPHENYU (PCBS) SH84$saD8pAt jAne4y»t; T. PINCKERT . .- . ; ,Ah»ty»i« BsteX'OSiiificlJ*! ^^ . ' . /• • '.Prepi>C« SEPARATOW FUNMEl LtWIO-LlOUll) PCTWM lti W«4-351« P2M.1.0 :' ' " • • = ' ""-".•• :: ; - - ' : - - \ ^ ' '_ '.\:".^^'^'-] '."' -: •

PareMSterPCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

ResultBDLBDLBDLBOLBDLBDLBDLBDL

Det. Lfsrit0.000100.000500.000100.000100.000100;000100.00010o; oooio

Unitsrag/tiWLn»g/Ling/Ln>g/Ling/Lmg/LinQ/L

TURBIDITY (HEPHELOMETRIC) EPA 180.1Analysts J. STOWCCT Analysis Dates 0*MD£C*95 15:00 Testr C602.5.0

PersewterTURBIDITY

Result

1.1Det. Li«ft Units

ntu

Saaple CoMwntsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATION11 STAMtlX STREET, PITTSBURG, PA 15222-1384


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361602 95 12/4/95 LL 0845 SRW23CSMplt




Received08-DEC-95Complete

15-DEC-95Printed

ll-JAN-96

Project Lab ID

A362136PO Muter


06-DEC-95 13:50

Report To


Bill To


Saaple DescriptionCLIENT ID: 95 12/6/95 LL 1350 SRW24DESCRIPTION: LEMON LANE RESIDENTIAL WELLSBLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTIONAnalyst: 6. KISSELL-9UTK Analysts Dete: M-fieC-95

PerMMter


SW846-3510B

Result1000

, 5 - • • • : • • • -

Testt W30*i;«Det. Li*«t

r;":'\: .-.:'. '•'Units

raLIHt : • : , - . - :V

POLYCHLORINATED BIPHENYLS (PCBS) SH846-8080AAnalyst! C/'ttCWr^-n?--.- •" :-, ; : :- Analysts Date: 1HN&**C'-;-'- Instruaant: fiC/ECO .. : - '•• tmttt V3M&ttr,'\^. -':Pr*p: PCS SEPJWATWT WWIEL LiflUIO -LIQUID EXTRACTidli:*yiUt3SiOB P230.1.0

PerMwttrPCB AROCHLOR 1016B/*D AnA/^UI AO tl1*! . • • • . • • . • . • . . . .••.•...-.•.•.-.•..•.•.•.•.•.•.•.•.•.•.•.•.-.•.•..•.•.•.•.•.•.•PC B AROCH LOR 1 2 Z IPCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248

rPCB AROCHLOR U54i PCB AROCHLOR 1260

PCB AROCHLOR 1262

ResultBDL

^.•BDL ••^•W'BDLBOLBDLBDLBDLBDL

Det. Liait

0.0001

0^00050.0001d.oooi0.00010;00010.00010:0001

Unitsrog/Lm/img/L

mg/Ln»g/L*g/Lmg/Linq/L

TURBIDITY (NEPHELOMETRIC) EPA 180.1Analyst: S. PFEFFER Analysts Datet 08-D6C-95 16:30 Test: CM2.5.0

Paraaeter

TURBIDITYResult

24Det. Linit Units

ntu

Saaple Coevents




Additional copies of this report sent to:RUSS CEPKO, WESTINGHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A362136 95 12/6/95 LL 1350 SRM24SMplt COMMHtt


Approved : /bjJJ)*J niHALAJjsx- Page 2 (last page)


Service Location


Received

06-DEC-95Complete

18-DEC-95Printed

18-DEC-95

Project Lab ID

A361915PO Number

RN-24352-S 0-00Samp tea

05-DEC-95 13:40

Report To


Bill To


Sample DescriptionCLIENT ID: 95 12/5/95 LL 1340 SRU25DESCRIPTION: BLOOMINGTON PROJECTBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510BAnalyst: J. OANIELSON Analysis Date: 07-OEC-95 Test: P230.1.0

Parameter


Result

10005

Det. Limit Units

mLmL

POLYCHLORINATED BIPHENYLS (PCBS) SH846-8080AAnalyst: B. WOOD Analysis Date: 11 -DEC- 95 Instrument: GC/ECO Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SU846-35108 P230.1.0

Parameter


Result


Det. Limit

0.000100.000500.000100.000100.000100.000100.000100.00010

Units



TURBIDITY


Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result

1.3Det. Limit Units

ntu







11 STANUIX STREET, PITT5BURG, PA 15222-1384



Service Location


Received

06-DEC-95Complete

21-DEC-95Printed

21-DEC-95

Project Lab ID

A361911PO Hunter


05-DEC-95 08:30

Report To


Bill To



PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510BAnalyst: J. GRIFFIN Analysis Date: 07-pEC-95 Test: P230.1.0

Parameter


Result1000

5

Det. Limit UnitsmLml

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: E. BINGHAH Analysis Date: 09-OEC-95 Instrument: GC/ECO Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTJCMf SW8W-35108 PZ30.1.0

Parameter



Det. Limit0.000100.000500.000100.000100.000100.000100.000100.00010


TURBIDITY (NEPHELOMEVRIC) EPA 180.1Analyst: J. STOAKES Analysis Date: 07-DEC-95 10:00 Test: G602.S.O

Parameter

TURBIDITYResult


ntu

Sample GarmentsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTIN1HOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361911 95 12/5/95 LL 0830 SRVIZfSample Comments


Approved : M < /UV ' l tL ' J Y[/^~— Page 2 (last page)


Service Location


Received

06-DEC-95Complete

21-DEC-95Printed

21-DEC-95

Project Lab ID

A361920PO Number


05-DEC-95 17:10

Report To


Bill To



PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510BAnalyst: J. DAMIELSON Analysis Date: 07-DEC-95 Test: P230.1.0

Parameter


Result

1000

5


POLYCHLORINATED BtPHENYLS (PCBS) SH846-8080AAnalyst: B. WOOD Analysis Date: 11-DEC-95 Instrument: 6C/ECD Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510B P230.1.0

Parameter


Result

BDL

BDLBDLBDLBDLBDLBDLBDL

Det. Limit0.000100.000500.000100.000100.000100.000100.000100.00010



TURBIDITY


Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result

18Det. Limit Units

ntu






HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361920 95 12/5/95 LL 1710 SRH27Sample Comments

11 STANWIX STREET, PITTSBURG, PA 15222-1384

Approved : (-J ^ / u ^ M I jAl^^ Page 2 (last page)


Service Location


Received

06-DEC-95Complete

18-DEC-95Printed

18-DEC-95

Project Lab 10 j

A361916PO Number


05-DEC-95 14:45

Report To


Bill To



PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SH846-3510BAnalyst: J. DANIELSON Analysis Date: 07-DEC-95 Test: P230.1.0


Result

10005


POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: B. WOOD Analysis Date: 11 -DEC- 95 Instrument: GC/ECD Test: 0301.2.0

Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SU846-3510B P230.1.0

Parameter


Result


Det. Limit

0.00010

0.000500.000100.000100.000100.000100.000100.00010

Units


TURBIDITY (NEPHELOMETRIC) EPA 180.1Analyst: J. STOAKES Analysis Date: 07-DEC-9S 10:00 Test: G602.5.0

ParameterTURBIDITY

Result2.0

Det. Limit Units

ntu




Additional copies of this report sent to:RUSS CEPKO, UESTINCWUSE ELECTRIC CORPORATION




Approved : / /L//A//Z 6 ^/ Ls ~ Page 2 (last page)


Service Location


Received

06-DEC-95Complete

18-DEC-95Printed

18-DEC-95

Project Lab ID

A361917PO Number


05-DEC-95 16:05

Report To


Bill To



PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510BAnalyst: J. OANIELSON Analysis Date: 07-DEC-95 Test: P230.1.0

Parameter


Result10005

Det. Limit Units

mLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: B. WOOD Analysis Date: 11-DEC-95 Instrument: GC/ECD Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SWS46-3510B P230.1.0

Parameter


Result


Det. Limit

0.000100.000500.000100.000100.000100.000100.000100.00010

Units

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L


TURBIDITY


Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result

3.1Det. Limit Units

ntu







Service Location


Received

06-DEC-95Complete

18-DEC-95Printed

18-DEC-95

Project Lab 10

A361918PO Number


05-DEC-95 16:05

Report To


B i l l To


Sample DescriptionCLIENT ID: 95 12/5/95 LL 1605 DRW30DESCRIPTION: BLOOMINGTON PROJECTBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510BAnalyst: J. DAMIELSON Analysis Date: 07-OEC-95 Test: P230.1.0

Parameter


Result10005

Det. Limit Units

mLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: B. WOOD Analysis Date: 11-DEC-95 Instrument: GC/ECO Test: 0301.2.0Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510B P230.1.0

Parameter


Result


Det. Limit

0.00010

0.000500.000100.000100.000100.000100.000100.00010

Units



TURBIDITY


Parameter

1: 07-DEC-9S 10:00 Test: G602.5.0

Result

2.7Det. Limit Units

ntu




Additional copies of this report sent to:RUSSCEPKO, HESTING.IOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A361918 95 12/5/95 LL 1605 DRW30Sample Comments




Service Location


Received

06-DEC-95Complete

18-DEC-95Printed

18-DEC-95

Project Lab ID

A361919PC Number


05-DEC-95 16:05

Report To


Bill To


Sample DescriptionCLIENT ID: 95 12/5/95 LL 1605 ERU30DESCRIPTION: BLOOMINGTON PROJECTBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDER

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510BAnalyst: J. DAN1ELSON Analysis Date: 07-DEC-95 Test: P 230. 1.0

Parameter


Result

10005

Det. Limit Units

mLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080AAnalyst: B. UOOO Analysis Date: 11-DEC-95 Instrument: GC/ECD Test: 0301.2.0

Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SU846-3510B P230.1.0

Parameter


Result


Det. Limit

0.00010

0.000500.000100.000100.000100.000100.000100.00010

Units



TURBIDITY


Parameter

1: 07-DEC-95 10:00 Test: G602.5.0

Result

0.50

Det. Limit Units

ntu

Sample Comments






HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID: A361919 95 12/5/95 LL 1605 ERW30Sample Comments


Page 2 (last page)

ENCLOSURE #2

MONITORING WELL

RESULTS

Monitoring Well SamplingLemon Lane Landfill

WELLNUMBERJW4D4W4D4W4D

4W4II/IW4IMW4I

I/IW6UIW6i/IW6

MW7MW7Ml 7

k/IWBDMW8DMW8D

DUPLDUPLDUPL

BLANKBLANKBLANK

MEASURINGPOINT

ELEVATION(FT. ABOVE MSL)

887.15887.25887.25

886.29886.41886.41

865.73865.73865.73

863.12863.12863.12

855.76855.76855.76

863.12863.12863.12

UtKIHTO

WATER(FT.)

111.94112.46112.43

70.1270.1568.01

49.2549.1248.47

40.3140.2

40.15

86.5386.7386.45

40.3140.2

40.15

GROUND WATERELEVATION

(FT. ABOVE MSL)775.21774.79774.82

816.17816.26818.4

816.48816.61817.26

822.81822.92822.97

769.23769.03769.31

822.81822.92822.97

SAMPLENUMBER

95 10/24/95 LL 1550 SMW4D95 11/17/95 LL 1045 SMW4D95 12/18/95 LL 1050 SMW4D

95 10/24/95 LL 1500 SMW4I95 11/17/95 LL 1000 SMW4I95 12718/95 LL 1205 SMW4I

95 10/25/95 LL 1 1 15 SMW695 1 1/17/95 LL 0900 SMW695 12/18/95 LL 1600 SMW6

95 10/25/95 LL 0950 SMW795 1 1/17/95 LL 1500 SMW795 12/18/95 LL 1445 SMW7

95 10/26/95 LL 1015 SMW8D95 11/17/95 LL 1100 SMW8D95 12/18/95 LL 0950 SMW8D

95 10/25/95 LL 0950 DMW795 1 1/17/95 LL 1 500 DMW795 12/18/95 LL 1445 DMW7

95 10/25/95 LL 1300 EMW8D95 1 1/17/95 LL 1 100 EMW8D95 12/18/95 LL 1600 EMW6

SAMPLINGAPPARATUS

bladder pumpbladder pumpbladder pump






TEMPdeg.C

13.613.512.4

14.013.913.5

13.512.812.4

17.316.414.5

10.611.811.9

17.316.414.5

PH6.816.29

6.616.34

6.776.03

6.796.78

6.526.19

6.796.78

SPECIFICCONDUCTANCE

^uMHOS)98310631288

664653740

494479532

384350148

227019701427

3843bO148

SUM UhAROCHLORS

CONC.(PPB)BDLBDLBDL

1.11.1

0.54

0.680.620.30

0.360.170.29

BDLBDLBDL

0.360.160.28

BDLBDLBDL

02/02/96

1

3

3aa

H

H

WESTINGHOOSE ELECTRIC CORPORATIONGROUND WATER SAMPLING FIELD LOG

BLOOMINGTON, INDIANA

Site UCru>Kt Uvle tfell No.Sampling PurposeDate/Time: M*M.J3y In WT^ OutSampling Personnel fal y_VHNu Background Well »*A Weather______l__

I. Well Information

Reference Pt. (casing & height above grade) foC - 6if>>-f ?tACCWell Diameter "*" Well Depth from RP_J_______.Water Depth from RP \ll

II. Well Volume Information

Length of Water Column iMtOfa Volume of Water Column,

III. Evacuation Information

Evacuation MethodRedline «^ Calibration Stds: <—-' 7 . ' 10Purge Volume (Gals) T pH SpC Time

7.Z.-5. »"V-7 i »>

i-*.. C. <J «3c>

V V C ^-«V

^B IV. Sample Data

Container(s) Preservation Time Collected Sample ID No. Analysis

n V. Field Measurements

Temp._J___i_____ pH__J«iJLI SpC &1» Film.

VI. Remarks/Miscellaneous Observations (

. Sample DestinationuEMS Laboratory Via By

m.e.Field Services Coordinator

3

3

SiteSampling Purpose l t-tDate/Time:

WESTINGHOUSE ELECTRIC CORPORATIONGROUND WATER SAMPLING FIELD LOG


Well No.

Sampling PersonnelHNu Background

In OutHtO

Well »»»*» Weather P rujuJ f

I. Well Information

Reference Pt. (casing & height above grade)Well Diameter _ ^ _ Well Depth from RPWater Depth from RP M"Z.*-tl


Length of Water Column Volume of Water Column

.Calibration Stds:T pH

10SpCto 3 s

Time


Evacuation MethodRedlinePurge Volume (Gals)

•y J"\--?

i-y-r

IV. Sample Data


aV. Field Measurements

. U.:TTemp. PH SpC Film

VI. Remarks /Miscellaneous Observations

VII. Sample Destination

EMS Laboratory Via By

Field Services Coordinator

"W

•m

_jll•«•

-1

—:

-•

33

WESTINGHODSE ELECTRIC CORPORATIONGROUND WATER SAMPLING FIELD LOG


Site rto + __ Well No._|lESampling Purpose r»/x)Date/Time: >t-\Vg>^? In tozo Out.Sampling Personnel vt-tHNu Background Well MA Weather.

I. Well Information

Reference Pt. (casing & height above grade).Well Diameter "2 " Well Depth from RP_Water Depth from RP in


Length of Water Column tV'*'7 Volume of Water Column a • (*7


Evacuation Method Q ec?

Redline \s~ Calibration Stds: ^ 7 '—- 10Purge Volume (Gals) T pH SpC Time

25- »?.-k i

IV. Sample Data


V. Field Measurements

Temo. »^.H PH _ SpC Film

VI. Remarks/Miscellaneous Observations


EMS Laboratory Via _ By


a

3

VESTINGHOUSE ELECTRIC CORPORATIONGROUND WATER SAMPLING FIELD LOG


Well No.Sampling Purpose naiqruiMDate/Time: tofxnps- In 13'S's- outSampling Personnel.HNu Background Well VJA Weather CIOAJPW

I. Well Information

Reference Pt. (casing & height above grade)Well Diameter • "*•*" Well Depth from RP.Water Depth from RP

87•no.i


Length of Water Column \ Volume of Water Column 8 • y*—

III . Evacuation Information

Evacuation Method O€o»tATec?I Redline \^1 Purge Volume (Gals)

as-1 e.i>1 «.T

Calibration Stds:T pH

iS.o £.4*7N.I (.<.,'M,o £.4,,

u^^ 7 i*SpC737-

4.67

£<W

^ 10TimeIMM&( ^ X o

\~\S~1~-

IV. Sample Data



Temp. iM.£3 pH 6.(o SpC_ Film




Field Services oordinator

333

SiteSampling Purpose .Date/Time: (<( [Sampling Personnel F"1"!HNu Background

WESTINGHOOSE ELECTRIC CORPORATIONGROUND VATER SAMPLING FIELD LOG

BLOOMINGTON. INDIANA

Well

In <£>i>xoH*O

out

Veil MA Weather 3S°P

I. Well Information

Pt. (casing & height above grade)ter 1*2." Well D

*fReferenceWell Diameter.Water Depth from RP_

6E\/€\___

Well Depth from RP___£LZ_


Length of Water Column '* • Volume of Water Column




i\.°> C.n

10SpC Time

IV. Sample Data


J


Temp. \ >- * pH • "H SpC.5'>

VI. Remarks /Miscellaneous Observations d(_C. \T2___

Film

IIVII. Sample Destination


3 Field Services Coordinator

3333333

33

SiteSampling Purpose.Date/Time: 'z|lf



Well No.

in outSampling Personnel.HNu Background Well Weather M0"F

I. Well Information

Reference Ft. (casing & height above grade)Well Diameter " t, M" Well Depth from RP.Water Depth from RP &%-o\

87


Length of Water Column ) Volume of Water Column


Evacuation Method_Redline ^Purge Volume (Gals)

9-1 *

.Calibration Stds:" T pH

10SpC Time

IV. Sample Data



Tenm. ("?• •* pH SpC_ Film


a




a


BLOOtUXGTQS, INDIANA

Site_Sampling PurposDate/Time:

Well No.

Sampling Personnel.HNu Background_^_

Ho«JLIn Out_H2£_

Well__£4A Weather Co'r

I. Well Information

Reference Pt. (casing & height above grade) T*>P <rf UMifgWell Diameter ~2*n Well Depth from RPWater Depth from RP


Length of Water Column -I Volume of Water Column ' '


Evacuation Method Qt5PRedl ine LPurge Volume (Gals)

•3.7*

M

Calibration Stds:" T pH SpC

IV. Sample Data

Container(s) Preservation Time Collected Sample ID No.

.10Time

Analysis


Temp. 1"3.ST pH_ 6 ."?! SpC Film



EMS Laboratory Via_ By


33

3d1. /

H



Site _ grnysj Ae Well No.Sampling PurposeDate/Time : u l - i X " In t>&> OutSampling Personnel*HNu Background Well *** Weather

I. Well Information

Reference Pt. (casing & height above grade) UukrtrWell Diameter _ "2'' _ Well Depth from RPWater Depth from RP_


Length of Water Column <.^-^S Volume of Water Column,


Evacuation Method.Redline • 'Purge Volume (Gals)

3 .-7VM.ooM.i-y


IZ.* <J. in,123 f -.12.6 6".o3

, - 7SpC

4 So>i T«**-HH9

- 10Time08 SoOOSi

»O5^

IV. Sample Data


q {C(Sr 0*10 5>si«ln|9iu_o*»S'>iu4, rc6£


Temp. ^-3 pH___4L£l SpC__ 32 Film.

CLe/w-t__VI. Remarks/Miscellaneous Observations

JII. Sample Destination



331

-1

1

3

-



Site Utr-ioM LA«sltSampling Purpose »i<s»4Date/Time: V*-|lB P?Sampling Personnel H-\ W 9fX~HNu Background Well

I. Well Information

Reference Pt. (casing & heightWell Diameter -2U"Water Depth from RP M<

Well No. &

In /sT^O Out /(

\r/Ul \4V C**.AAA. Weather /J'O*/* U3

above grade) E>eVfe<^- FVC dAeWell Depth from RP T3L.3-

?. W7

<•**)

L -*V»f

/

f


Length of Water Column 3'%58> Volume of Water Column 3.B"£. ^ —



A


10SpC?.*-

Time

$5*.

IV. Sample Data



Temp. 11-M pH SpC Film





t1I

9a



Site lc/vv|Sampling Purpose_Date/Time: |_£l

Well No. _ ~]_

Sampling PersonnelHNu Background

In OutHf\

Well N!*V Weather (t>t>° f-

I. Well Information

Reference Pt. (casing & height above grade)Well Diameter _ "S." _ Well Depth from RPWater Depth from RP

U>UTV CAP *r"TfrT?"


Length of Water Column Volume of Water Column -f &T4* * ~'


Evacuation MethodRedl ine *- ^Purge Volume (Gals)

its-

.Calibration Stds: _T pH

!(.•) 6.83SpC

10Time

IV. Sample Data



Temp.__Ui!__ pH__ SpC Film

VI. Remarks /Miscellaneous Observations

1VII. Sample Destination



I•f

3aaa

3i3i

•v

i

i

i

WESTINGHOtJSE ELECTRIC CORPORATIONGROUND WATER SAMPLING FIELD LOG

BLOOHINGTON, INDIANA

Site Well No.7Sampling PurposeDate/Time:Sampling PersonnelHNu Background

In Out /

Well M.A Weather

I. Well Information

Reference Pt. (casing & height above grade) LuUvTC CtfWell Diameter 3*2." Well Depth from RP.Water Depth from RP

<b~*-




Evacuation MethodRedl ine '-Purge Volume (Gals)

l\


10SpC Time

IV. Sample Data



Tenm. V<» - oH SpC_ Film




Fis.ld Services Coordinator

3

3331

33

3

WESTINGHODSE ELECTRIC CORPORATIONGROUND WATER SAMPLING FIELD LOG


Site ugrr«™ u**siC Well No 7S amp lingPurpose_^^Date/Time :_i2difc/±21 ^ In M**** Out_Sampling Personnel.HNu Background Well Mfl Weather 4t7'f-

I. Uell Information

Reference Pt. (casing & height above grade)Well Diameter "****' Well Depth from RP_Water Depth from RP Me . i -g


Length of Water Column ^'- 8^ Volume of Water Column \\_


Evacuation MethodRedline v^ Calibration Stds: ^^Purge Volume (Gals) T pH SpC Time

U N-.r- lll.s W-* I

IV. Sample Data

Container(s) Preservation Time Collected Sample ID No. AnalysisZ V<u^

>


Temp. N.S pH SpC /M g? Film.

VI. Remarks/Miscellaneous Observations Poar> o 1*00 fc'so -anu - (l«j

3VII. Sample Destination


Field Service^ Coordinator

33

03

SiteSampling PurposeDate/Time: (



Well No..

Sampling PersonneHNu Background

In out

Well

I. Well Information

Reference Pt. (casing & height above grade).Well Diameter ^Water Depth from RP_

Well Depth from RP


Length of Water Column « Volume of Water Column


Evacuation Method QtO

. .1» 1

RedlinePurge Volume (Gals)

i£w*O

L^ Calibration Stds: t ^T pH

/<•<• trz.7

SpC

1 170

' — ' 10Time

/o: 13

IV. Sample Data

Container(s)2


Tenm. [g-^ pH_

Preservation Time Collected Sample ID No.

SpC_ Film

VI. Remarks/Miscellaneous Observations ^ f2<zvur?t^

34z

JVII. Sample Destination


ul/.PField Services Co

31IB



Site LA.VJC Well No.Sampling PurposeDate/Time: lt|H.[;S - inSampling Personnel.HNu Background.

Out

Well Weather -VS-JP

I. Well Information

Reference Pt. (casing & height above grade) f^CWell Diameter x2-" Well Depth from RP_Water Depth from RP g6.~l3» -


Length of Water Column Q> -11 Volume of Water Column



Calibration Stds:

J * PH

7SpC

(970

10Time(too

IV. Sample Data



Temp. ''« P pH SpC_ Film





33aa

a



SiteSampling Purpose,Date/Time: »•*•[ l*»

Well

in OutSampling Personnel *-m Niv/HNu Background Well MA. Weather -«-ic*r

I. Well Information

Reference Pt. (casing & height above grade).Well Diameter 3-"Water Depth from RP

Well Depth from RPg> (vrn




Evacuation Method,RedlinePurge Volume (Gals)

(-If

.Calibration Stds:T pH SpC

ISO. ~7

10Time

333

IV. Sample Data


\


Temp. l'-? PH SpC

VI. Remarks /Miscellaneous Observations pu\flot(3»

c^-^r i vcr 4 ff • "Jt't- *^A Ul _, c» i PN.T <r*c r

Film

Q

1




Attachment 1: Data Validation for the Lemon Lane Landfill Monitoring Wells forOctober/November/December, 1995

1. The validation was performed per the requirements for level 4 data in the projectQAPjP. This includes a check for ; Holding Tune, Calibration, Blank Contamination,Precision, Accuracy, and Accuracy of Nominal Reporting Limits against methodrequirements. All analyses met method requirements. The data is accepted with noqualifications.

2. A total of 21 analyses were reviewed. This includes 5 wells sampled three times and 6blanks/dupes.


o Precision and accuracy: Precision and accuracy were accessed by reviewingthe lab performance on lab spiked samples, lab spike duplicates and fieldduplicates. All requirements were met.

o Representativeness: The representativeness requirement involves anassessment of the field sampling and lab analytical techniques. The fieldsampling locations and techniques as well as lab procedures were inaccordance with the approved sampling plan and QAPjP. There were nodeviations and the representativeness requirement was met.

o Completeness: The completeness goal for the project was for all projectdata to be 90% accepted. Completeness is calculated by dividing the totalnumber of acceptable analyses by the total performed. An acceptableanalyses is defined as one that conformed to QC protocols and is notrejected. There were no rejected analyses so the completeness goal was met.

o Comparability: All the samples taken, analyzed and validated byWestinghouse were taken by Westinghouse sampling crews using the sameprocedures and analyzed by the same laboratory. Therefore for the samplestaken by Westinghouse there are no comparibility issues.

Overall, the main objective of the sampling event was to determine if PCBs are present ata concentration of .1 ppb or more. The sampling and analysis performed met this goal.


Service Location


Received

25-OCT-95Complete

15-NOV-95Printed

07-DEC-95

Project Lab ID

A35817PO Number

RN-24352-S 0-00SMpted

24-OCT-95 15:50

Report To


Bill To


SMple DescriptionCLIENT ID: 9510/24/95LL1550SMW4DSAMPLE ID: 9510/24/95LL1550SMU4DBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION

PCB SEPARATORY FUNNEL LIQUID-LIQUID ; EXTRACTION SM846-3510B ,:,:.;;,:' • ' - :


; FINAL VOLUME ' - . '!•

Result9805

Det Lf*itml

Units

' POLYCHLORINATED BIPHENYLS (PCBS)t $M846-«080A'

'P230.1 .0 ;: ' l'".

PCB AROCHLOR 1016Paraneter

PCB AROCHLOR 1232PCB AROCHIOR 1242PCB AROCHLOR 1248

PCB AROCHLOR 1260AROCHUJR 1262

ResultBDL

BDLBDL.BDLBDLBDLBDL

Det. Limit0.00010

i PvOooso;0.00010

loVbooibb.oooib0.00010

Units

mg/Lg/L

..•B/L

rog/L

.TURBIDim<NEPHELOMETRIC) ••• EPA

TURBIDITYParameter Result

52Det. Limit Units

ntu

SMple Content*Amended report: Corrected client's sample ID per DCE. arm 12/7/95




Page 1 (continued on next p?ge

HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A358179 9510/24/95LL1550SHVKSMple CoMents


Approved : M VI JLnVgJyW J \ J VI A-^ Page 2 (last page)


Service Location


v"

, A/ i

Received

25-OCT-95Complete

15-NOV-95Printed

07-DEC-95

Project Lab IDA35817E

PO Nuaber

RN-24352-S 0-00SaMpled

24-OCT-95 15:00

Report To

JIM PATRICKBLOOMINGTON PROJECTONE CITY CENTRE - SUITE 210 v fSP.O. BOX 997 VBLOOMINGTON, IN 47404-0997 >

Bill To

ACCOUNTS PAYABLEHESTINGHOUSE ELECTRIC COMPANYONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47402-0997

Saaple DescriptionCLIENT ID: 9510/24/95LL1SI5Q5MW4ISAMPLE ID: 9510/24/95LL1500SMW4IBLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDERDESCRIPTION

PCB SEPARATORY! Analyst: t. RIDGE

INITIAL WEIGHTFINAL VOLUME

FUNKEL LIQUID-LIQUID'•"•'M !: ';;'.';:• ;::;::/:':*nalyiit. Oat*:;?:

ParaMterOR VOLUME

EXTRACTION SW846-3510B^XT*»5.;' :.-:,: '. ; i. :;: &'. : . . .'•:' • '•-• : - :'- . ' ;:;--:^ :•;:-: ?V t*«tf • P250.UO ' ' • -

9805

Result Det. Linit UnitsmlmL

POLYCHLORINATED BIPHENYLS (PCBS) SW84e^080A ; j ; i ;• 'Xnriytts''»i::'Vibw£:::! Datet 27*OCT-9S; .-'.- ;' ; Iwtrwent: GC/ECD '.-. i' fiJI Mt:-' 050 1.2.0: . . . : , - - : ; - ^; .' Prep: PC8 SCPARATORT IfUWEL LfOUID- LIQUID extR idii-;:MB4i-3510B P230.1 .0 ' •^•if^\ ""••'} \:'^W^M-' -:.";' - • "• : '-. ' • :-,;: ." ' '.

PsraaeterPCB AROCHLOR 1016

• n/^ t>'- A fi A/*iJ i An i -o *» i • • " • ' • • " • ' 'PCB AROCHLOR 12Z1PCB AROCHLOR 1232PCB AROCHLOR 1242 :PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262 -

ResultBDLBDL : :: ' ' - : • :••. .- : .~WBDL0.001 IBDLBDL: : ' • . • • • • ' . ^BDLBDL

Det. Linit0.00010moooso0.00010;o. oooio0.000100:000100.000100.00010

Units•^/j-mg/Lmg/Lmg/L ymg/Lmg/L -; ;mg/Lmq/L

1242 is degraded.

TURBIDITYAnalyst; S;

TURBIDITY

(NEPHELOMETRIC) EPA 180.PFEffER Analysis Date

Parameter

I •%•:.• . -:-\ . ' • • . ^ • .•• : ; •• , - - ^ ' . . • • • - : - •r ZS-OCT-95 17:00 : ?; ; ; Test: B602.5.0

Result77

Det. LtMit Unitsntu

Sample Ccmnents

Amended report: Corrected client's sample ID per DCE.



arm 12/7/95


HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A358178 9510/24/9SLL1S50SHWSMplt COMMHtB


Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATIOH11 STANHIX STREET, PITTSBURG, PA 15222-1384

Approved : U. JAJIA\O(/* J JI *V-W.g>l Page 2 (last page


Service Location

HERITAGE ENVIRONMENTALCOMMERCIAL LABORATORY (7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8305

SERVICES, INC.JPERATIONS

Received

25-OCT-95Complete

15-NOV-95Printed

15-NOV-95

Project Lab ID

A358182PO Nunber


25-OCT-95 11:15

Report To


Bill To


Sample Description

CLIENT ID: 9510/25/95LL1115SMW6SAMPLE ID: 9510/25/95LL1115SMW6BLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION

PCBtSEPARATORY FUNNEL LIQaiO*LI(ltttfffE)CTRACt70Ni s^ r ^m^^^^^^^Miti i l ii ll K

ParameterINITIAL WEIGHT OR VOLUME::FiNAL;voluME::yv-::PtiLYCHLORINATED BIPHENYLS (PCBS) SW84^8080A)i>« ^Bi:i «lilfiip'iilj ^

ParameterPCB AROCHLOR 1016PCB AROCHLOR 1221 : •••' .mmmmmmmmmmPCB AROCHLOR 1232PCBsAWCHLbR 1242 /^..vV-^: :, --: ^mmwm ,PCB AROCHLOR 1248mxiwsxxvtm i

PCB AROCHLOR 1260mmmc ^1242 is degraded.

• SW845-3510B. m

Result990

:v'5;:^v.:v.::^:-^:yx;;:^

&-M-&^^^:^^^^^m\ ; imtfument: ;• ;iiC/ECO-: ;. : jjjitIB P230.1.0 ''•i;'::-:: v'':|l!:f:^^ ;;:lii

ResultBDLBDL x-:..;;^ :;:•:; :::/ ;-;S :>.::;:

BDL0.00068 ^;gBDL

•:ym.7^^m: :-"^ymBDL

::v:BDL.- -.•::,::;;:;: 'V. -•.••:•:-;:••;::.,;:;::-:;:.:,

fSPilsWsliS-iiiltis'tv-liid i:

Det. Limit

KilSlDet. Limit

0.00010:0;000500.00010

Im oooio0.00010

s yOiOOOlO0.00010^booio

)ir^--^--'-Units

mLmL

>:; 1; ' ' -V- : . . - - :•:::-

Unitsm9/j-mg/L ;mg/L:mg/Lmg/L:mg/Lmg/Lmq/L

TURBIDITY:; : inatVtts? ;:;

TURBIDITY

^NEPHELOMETRIC):£PA,18p««^^^^^^:p*EfFM:-:s:;:f:;:;S::-:s!':-?:.i-:.-::* . S-; : - : . ; - . '^ . - :^- •:• ':-:: - • : - : •^•••^« iH^^Mtii 6602.5-0- -v- •,

Parameter Result

0.51

Det. Limit Units

ntu

Sanple Comments





HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A358182 9510/25/95LL1115S1Sample Comments

Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATION11 STANUIX STREET, PITTSBURG, PA 15222-1384

Approved : / ^y( A r\jT*Lri J] Y\A - Page 2 (last page


Service Location


Received

25-OCT-95Complete

15-NOV-95Printed

07-DEC-95

Project Lab ID

A358180PO Nueber


25-OCT-95 09:50

Report To


Bill To


Staple DescriptionCLIENT ID: 9510/25/95LL0950SMW7SAMPLE ID: 9510/25/95LL0950SMU7BLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDERDESCRIPTION

PCB SEPARATOR?


FUNNEL LIQUID-LIQUID EXTRACtlOK SW846-3510B \'ll^^M-\^^^.:^:^^VWI.:4:--:;.;:i.':M'-AnetY»ts. Dateriai T^x :;;'/? / :: : •• - ' : - •: ':••'.. •'::'.:•••- ':> •'-:':'- •;.-.-i:::ta«tr P230.1.0 :':^':> ••'

ParaMterOR VOLUME 880

5

Result Det. Liarit UnitsmLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-80SOA!: -• Analysts-::** goOO-:-:?lllf -'l i t.lMm-i aci'n^ : .

• •• Crap; P« SWAWtfdRr ^

PsrtsttterPCB AROCHLOR 1016

,;i PCB AROCHLOR 1221 m :/: : ' •" ' ±V-" : •-: - mmMm .PCB AROCHLOR 1232PCB AROCHLOR 1242 rPCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262 •,^-'.^^/::1242 is degraded.

Inatruaent: GC/ECO ' f%'IB P230.1.0'.'. ;'..::;':':: .

:..:'::;;"::';'.' ' . ( •

ResultBDL

•';BDL ^;::-;^v.'^;:-:^.;:BDL0.00036BDLBDLBDLBDL

Test: 050T.2.I

Oct. Liuit0.000100.000500.000106.000100.00010

; /o: oooio0.000100.00010

J'..'| ;". -

Unittn»g/Ljng/Lmg/Lmg/Lmg/Lmg/L :;mg/Lmq/L

TURBIDITY (NEPHELOHETRIC) EPA 180. K;::: Arial :;* PflFiFl« :W!:::V^^ :'• ' ' '.'" ' testj G60Z.5.0

ParaneterTURBIDITY

Result23

Det. Unit Unitsntu

Saaple CommentsAmended report: Corrected client's sample ID per DCE.



arm 12/7/95


HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A358180 9510/25/95LL0950SHVSanpl* Cements


Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATION11 STAWIX STREET, PITTSBURG, PA 15222-1384

Approved : H "jA SU \/r<XjZ~)J \ JA/LJ2--V Page 2 (last page)


Service Location


Received

25-OCT-95Complete

15-NOV-95Printed

15-NOV-95

Project Lab ID

A3581S1PO Number


25-OCT-95 09:50

Report To


Bill To


Sample DescriptionCLIENT ID: 9510/25/95LL0950DMW7SAMPLE ID: 9510/25/95LL0950DMW7BLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDERDESCRIPTION

PCB 5EPARATORYAnalyitt Mi SIMS ' :


FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510B ;-V:fi::;:-;:-';t::i;:^^^^^^ •. i. :"' . - , • : p "< •'- '' - '- ' ' '- •; ;-. : - .. 1" . Test f P230.1.0

Parameter

OR VOLUME 9805

Result Det. Limit UnitsmlmL

POLYCHLORINATED BIPHENYLS (PCBS) SH846*8Q80A*;: Analyit:. BiVWOOO'-: i^i V:U:-;. H^:V»'V»*«:D*U?':;1?^P6i .- Instrument: iJC/ECO •.;;;-•• --^pTett: 0501.2.0 . . . .;;

:| frrepr PCB SEPARATOR? FUNNEL LIQUID-LIQUID EXTRACTION S\itti-iil510a P230.1.0 /: ' . ; • ' ' : A ;

Parameter

PCB AROCHLOR 1016PCB AROCHLOR 1221 ;PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Result

BDLBDLBDLb;ooo36; ;BDLBDL :': x: :'----:mBDLBDL :.-V.-,:A:.v>>-^,f:v,^^

Det. Limit

0.00010

0.000500.000100.000100.000100.000100.000100.00010

Units

mg/Ling/Lmg/Lmg/Lmg/Lmg/Lmg/Lmq/L

1242 is degraded.

TURBIDITY (NEPHELOMETRIC) EPA 180.1•?; Analysti $i PFEFFER Analysis Date: &<XT-'K 17:00 : ; Tests C602.5.0

Parameter

TURBIDITYResult

19Det. Limit Units

ntu




Page 1 (continued on next p'ige)

HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A358181 9510/25/95LL09SQDHWSanple Comments

Additional copies of this report sent to:RUSS CEPKO, VESTINGHOUSE ELECTRIC CORPORATION11 STANUIX STREET, PITTSBURG, PA 15222-1384



Service Location

HERITAGE ENVIRONMENTALCOMMERCIAL LABORATORY7901 H. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8305

SERVICES, INC.OPERATIONS

Received

Ol-NOV-95Collet*

07-DEC-95Printed

07-DEC-95

Project

PO Nu

RN-24352-S

Leb 10

A35894;•ber

-0-Stapled

26-OCT-95 10:15

Report To


Bill To


CLIENT ID: 95 10/26/95 LLBLANKET O^DER RELEASE I: NOT R

Description

WITH ORDER

PtiiSEWW^I::!**ip**i*iHr;:« ^


''FlMAt'-'WLUME^^

Result880

Oet. Limit UnitsmL

ifmT •.•:••:':>::•,:•:••••'::••

POLYCHLORIMATED BIPHENYLS (PCBS) SW846IW80A:;;:: 'Kmtf*^^ «:: Date:;?: W 6* llt;::;;:;; IJImtrumenit : • • CC/ECD ; pi lill ;&**•& <801 .2';0 ::;: ;1|* i; ' ;: -": . • . • .|-.|Nii i! i0 ^BjlitHiit iJ«ui6: mi t|i>;iip( tofl::pz30.i ;0 • - ;&£1-^^^ .11 ;•: E::m> M :::;:: ' ' .

ParameterPCB AROCHLOR 1016

<WB$U»CHLOR£im;»PCB AROCHLOR 1232mmtitmjmmm^ '': :^.^w

PCB AROCHLOR 1248PCB ARDCHLOR 3M4TM^ • : : ' < •:' J il'iiiS ;;-PCB AROCHLOR 1260

:''PCBi;:-AROCHLOR:x1262 • -AV"' . ^-, ' ••• ;v:i ; ^^v;

ResultBDLPnt •' '.;•• '• '•"••'• '•• '.':.•':'..•':'..•'..•.:•.::•:• .••.:•:•.:.•.••DUL . • •. v.v.. •.-• . . • • . • . • • . • . • • . • . - . • . • . • . • . • • . • . • . • • . • . • • . • . • . . • •

BDLy-m. m :m;mm

BDL.•; BDL .•';•-•'• .••''•^m.^E.

BDLv-vBDL ' : - ' - - - • • v > : > ' - f : •""•' :::.: '^:-^ • -

Det. Limit0.00010.00050.00010.00010.00010.00010.00010:0001

Units

mg/L;::mg/t:f;!;::J9A;mg/L -mg/L:fflq/Lmg/Lmq/L

J:5 DILUTIONMIXTURE DEGRADED 1242 AND 1248

TOTAL SUSPENDED SOLIDS EPA*-;ii i *.:;jci;:mi}«^^^

< fn ' •*'• . ••': : -: :::-.;--:: •:••.••'•.'•<::••.+.•:'.•.•.•'.••;•'•••; .- :x':: ::-: x': : . • • • ' :: . .:. '•' •• :• ' . •. • .'•. • •• ' - . - . . ' . . ' ••.•: : ': ' .:. . :• ' •'.'••: . . . ,' .• '• •:•' .• • '•: :' ': •'•"•::-:- •1 OU . Z <mmmimm-m: * ia •• - •:•:; :• = <» : : :: x- • •• :: :: ' ' .' •: ; ' • • : ' :- :- : • ' :: :* :: ;•• - : ; ':, ;•«• ; ' . -: :: " : : - <•? i : x?- •::*:- : •ly•i«^Datat:• 'jWifr1ii5:;:ib7:45:: '"• :•• '."•'. • ' " • • ' • • • ' '. ' • • . •.,". .-:^' ''-h, . :':.-:::::.;i ' Test j G403. 7.0 '..-.. "••

Parameter

SUSPENDED SOLIDSResult

10Det. Limit

1Units

mq/L

Staple CementsBDL Below Detection Limit




HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A358942 95 10/26/95 LL 1015S HH£SMple Conments

Additional copies of this report sent to:RUSS CEPKO, HESTIHGHOUSE ELECTRIC CORPORATIOH11 STAWIX STREET, PITTSBURG, PA 15222-1384

Approved : (/ / V// J/ 01 Page 2 (last page)


Service Location


Received

25-OCT-95COSplete

15-NOV-95Printed

07-OEC-95


PO NuaberRN-24352-S 0-00

Saspled

25-OCT-95 13:00

Report To


Bill To


Sample DescriptionCLIENT ID: 9510/25/95LL1300EMW8DSAMPLE ID: 9510/25/95LL1300EMW8DBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION

PCS SEPARATOR*;!• Analystt H^lllW

INITIAL WEIGHTFINAL VOLUME I

FUJWEL LIQUID-LIQUID

ParameterOR VOLUME

gUg lON-. SW846-3510B ; =j m l :-. '^ . • - ^^^ •-.,.

9705

Result Det. Llatit UnitsmlmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846^8080Aj ty»tr*;::;wD»£lll»^:: Prep? PCS' StPAMTOtT FWia UCWtO-UQUID EXTRACTIW 0^

ParameterPCB AROCHLOR 1016PCB AWOLOR 1221 r? :" >? ^ :-^"^ rm$$m:\ •••PCB AROCHLOR 1232PCB ARLCHLOR 12*2 -V'MP- ;• ; ••; . •.- ••• , .;, • ::, '• "vs •:Bm ..--PCB AROCHLOR 1248

::PCB.:::AROCHLOR;xie54;---v-.---:':':.'.- ••••:• •'• - .,:."v :^^x^\ ,:PCB AROCHLOR 1260

:;::pcB-ARocHLOR:-;i262: - - ^ ' ••• ••••. • •••• •• ••• - , •• - . ' m^ '• ; •

TURBIDITY (NEPHELOHETRIC) EPA 180. 1-.. /Wrtyrt^t^: W|i :. ;r f : ' Analysis Date: :jaj*«rr ?5; '17:00

ParsswterTURBIDITY

"'•Jmtruwnt: GC/ECD ^.i':.';.-'»P230,1.0- ' :"'. '. ' :" •1";r-'"".-:':

ResultBDL

- BDL : • : • • : ; : . .v^.-: ,:--BDLBDLBDLBDLBDLBDL

. ••: , - •- • :- , . . - .

Result0.32

te»ti;:fi501.2.(

Det. Llaiit0.000100.000500.000100.000100.00010

y 0.000100.000100.00010

! Test; G602

Det. Liatit

* ::'^':-'-:^:. '

Unitsmg/Lmg/Lmg/Lmg/L ;,.•a/Lmg/L Hmg/Lmq/L

.5.0 '-;• •

Unitsntu

Saaple CosnentsAmended report: Corrected sample description per DCE. arm 12/7/95





HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A358183 9510/25/95LL1300EMWSanpl* Comments


Approved : ^' v mJ?7V\y>/XlV/ \^A JU^ Page 2 (last page;


Service Location


Received

17-NOV-95Complete

04-OEC-95I Printed

04 -DEC -95

Projtct Lab 10A360483

PO Nuaber


17-NOV-95 10:45

Report To


•III To


Staple Description

CLIENT ID: 95 11/17/95 LL 1045 SMW4DBLANKET ORDER RELEASE i: NOT RECEIVED WITH ORDERDESCRIPTION: GRAB

PCBSEPARATORY F1JHNEL LIQUID-LIQUID EXTMCTIOW SH846-3510B $$?%!?- ; e i l ^ v

INITIAL WEIGHT OR VOLlSlF 1000Result Oat. Li«it Units

ml

FirmmterPCB AROCHLOR 1016PCB AROCHtOR|J2ZJPCB AROCHLOR 1232PCB AROCHLOfcli4PCB AROCHLOR 1248PCB WHKHLQRm&PCB AROCHLOR 1260PCB AROCHLOR


Oat. Llnit0.00010mooosoo.oooio0.00010000100.00010

mg/Lmg/Lmm«ng/L

COMMTltft



This Certificate shall not be reproduced, except in ft/77,without the written approval of the lab.




S«rv1ct Location

HERITAGE ENVIRONMENTAL SERVICES, INC.COMMERCIAL LABORATORY OPERATIONS7901 H. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8305

R*c*iv*d

17-NOV-95CoapUtt

04-DEC-95Printed

04-DEC-95

Project Lab ID

A36048PO Nurt»r

RN-24352-S 0-00SMpled

17-NOV-95 10:00

Report To


•111 To


Staple DescriptionCLIENT ID: 95 11/17/95 LL 1000 SMW4IBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: GRAB

PCB SEPARATORY FUNHEL LIQUID-LIQUID EXTRACTION SW46-3510B,>,,,,,,,, ,,,,, ,,.,,,. --'"•• •• •••••• •• ' ^ ^ ^ ^

PereneterINITIAL WEIGHT OR VOLUMEiNAP LUM& iiifMlii

Result1000

Det. Liait UnitsmL

POLYCHLORINATED BIfpfp||irti

>i:::pd;:;:iEP«At0ir

PCB AROCHLOR 1016KB; AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AHOCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Parameter ResultBDLBDLBDLBDL_0.0011BDLBDLBDL

Det. LiBit

0.00010#,00050o.oooio•fctiooio0.00010OiOOOlO0.00010

IftlitS

•ng/Lmq/L

Sasple CoMMntsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTIHGHOUSE ELECTRIC CORPORATION11 STAWIX STREET, PITTSBURG, PA 15222-1384

Approved : Page 1 (last page]


Service LocationHERITAGE ENVIRONMENTAL SERVICES, INC.COMMERCIAL LABORATORY OPERATIONS7901 U. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8305

Received

17-NOV-95Collet*

Ol-DEC-95Printed

Ol-DEC-95


PO Nuaber

RN-24352-S 0-00Seapled

17-NOV-95 09:00

Report To

OIM PATRICKBLOOMINGTON PROJECTONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47404-0997

BUI To


Staple DescriptionCLIENT ID: 95 11/17/95 LL 0900 SMW6BLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: GRAB

ParameterINITIAL WEIGHT OR VOLUME 1000

Result Oct. Limit unitsmLmL

TOLYCHLORIMATED BIPHEHYLS (PCBS)?i ltmma»W£ •?'' •".

PCB AROCHLOR 1016PCB ARDCHtOR 1221PCB AROCHLOR 1232PliB AROCHLOR 1242PCB AROCHLOR 1248PCS ARQCHLOR US*PCB AROCHLOR 1260PCff AROCHLOR 1262

Paraaeter Remit0.00062BDL .m--BDLBDLBDLBDLBDLBDL

Det. Li wit

0.00010

ro;00050o.oooioM 000100.00010

Units

0.00010

ng/LIg/L

mg/L1016 Is degraded.

Sanple CommentsBDL Below Detection Limit


This Certificate shall not be reproducedt except in fu77,without the written approval of the lab.

Additional copies of this report sent to:RUSS CEPKO, HESTIHGHOUSE ELECTRIC CORPORATION11 STANHIX STREET, PITTSBURG, PA 15222-1384

Approved Page 1 (last page;



Received17-NOV-95Complete

04-DEC-95Printed

04-DEC-95


PO MuterRN-24352-S 0-00

(••plod16-NOV-95 15:00

Report To


Bill To


Saaple DescriptionCLIENT ID: 95 11/17/95 LL 1500 SMW7BLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: GRAB


PCB AROCHLOR 1016PCBPMCHIOR imPCB AROCHLOR 1232PCB ARDCHLOR 1242PCB AROCHLOR 1248PCB AWHLOR 1*54PCB AROCHLOR 1260PCS AROCHLX)R 1262

Parameter ResultBDLmimBDL

^DL.,:--::::,;:0.00017

Det. Limit0.00010

M00050o.oooio

maamft0.00010

BDLBDL

o.oooiommom

Units

ing/L

Saapla CowcntsBDL Below Detection Limit



Additional copies of this report sent to:RU5S CEPKO, HESTINGHOUSE ELECTRIC CORPORATION11 STAWIX STREET, PITTSBURG, PA 15222-1384



Service Location



04-DEC-95Printed

04-DEC-95

Project Lab ID

A360486PO Niflfcer


16-NOV-95 15:00

Report To


Bill To


Saaple DescriptionCLIENT ID: 95 11/17/95 LL 1500 DMW7BLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: GRAB

W^ SEPAIWTORY rlJKNEL LI ID-LIQUID EXTTIACTIW SW^Igpitvstfvei:::

INITIAL HEIGHTFINAL; VOLUME i

ParaMSterOR VOLUME

Result1000

w ,mmmm

:W^^& fS j : ^&^&%$&%!&Sif8£$ijlx%iSHiiSssjiiifBSiKsiiiaeeii

Oet.

:

Liait UnitsmLiii pp/ >

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080A

PCB AROCHLOR 1016PCB AROCHtOR H21PCB AROCHLOR 1232PCBt AROCHLOR1242PCB AROCHLOR 1248PCBiAROCHLOR ia54PCB AROCHLOR 1260PCB AROCHLOR 1262

ParameterBDL

Result

;;BDL::II:BDLBDL0.00016BDLBDLBDL

Det. Liait0.00010OT0050o.oooioioioooio;0.00010fcoooio0.000100.00010

Units

mg/L

mg/L*Kj/Ln>gAmg/L

SMple ConnentsBDL Below Detection Limit







Received

17-NOV-95Collet*

04-DEC-95Printed

04-DEC-95

Project Leb ID

A36048<PO Nuiber

RN-24352-S 0-00SMpltd

17-NOV-95 11:00

Report To


•III To


•••pie DeecriptfonCLIENT ID: 95 11/17/95 LL 1100 SMW8DBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: GRAB

PCB SEPARATORY FUNNEL-•'•'•••••' ' ft | r;! i-( t,; l

PereaeterINITIAL WEIGHT OR VOLUME

Reeult1000

Oet. limit UhftsraL

BIPHENYLS (PCBS)

PCB AROCHLOR 1016PCS AROCHLOR imPCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Pereaeter ReeultBDL8DLBDLBDLBDLBDLBDLBDL

Oet.

0.00010

o.oooio^QQDIO;0.00010

o.oooioo.oooio

Units

.03/1.

Senple Comment*BDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTIHGHOUSE ELECTRIC CORPORATIOH11 STANHIX STREET, PITTSBURG, PA 15222-1384



Service Location


Received17-NOV-95Coaplete

04-DEC-95Printed

04-DEC-95

Project Lab ID

A360485PO Muter


17-NOV-95 11:00

Report To

JIN PATRICKBLOOMINGTON PROJECTONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47404-0997

•III To


Staple DescriptionCLIENT ID: 95 11/17/95 LL 1100 EMW80BLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: GRAB

ParemterINITIAL WEIGHT OR VOLUME 1000

Result Det. LiMit UnitsmL

POLYCHLORINATED BI

PCB AROCHLOR 1016mmmwwmwPCB AROCHLOR 1232

Parameter

PCB AROCHLOR 1248

PCB AROCHLOR 1260PCBAKOCHLOR 1262


Result Det. Li«it0.00010

1&000500.00010

0.00010

o.oooiofcdooio

Unitsmg/L

•ng/L

•ng/L

taspl* CosaintsBDL Below Detection Limit






Service Location


Received

20-DEC-95Complete

04 -JAN -96Printed

04-JAN-96


PO NuBber


18-DEC-95 10:50

Report To


Bill To


Staple DescriptionCLIENT ID: 95 12/18/95LL1050SMU4DDESCRIPTION: WATERBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDERDESCRIPTION

PCB SEPARATORS FUNNEL LIQUID-LIQUID EXTRACTIONAnalyst: J, DMIELSW Analysis D»tes 21 -DEC-95


•:SH846-35lptt?H;-;|;:l:r;|-;:V:;v;:

Result1000

. . 5 ' • . • • . : , . - • . - - - - - : - • • - • • • • - ; : • - -•••: •

'•:T«tV-«at£if3Det. Liaiit

M«p&-:.,"- :

units

mL:ffit;:::-:^ '

PCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AROeHLDR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Parameter Result

.BDLBDLBDLBDLBDLBDLBDL

Det. Li«it

o.oooiOvOOOS0.0001

Units

mg/L

0>0001o.oooioioooiQ.pool

Sample Comments




Additional copies of this report sent to:RUSS CEPKO, WESTIHGHOUSE ELECTRIC CORPORATIOH11 STAWIX STREET, PITTSBURG, PA 15222-1384



Service Location


Received

20-DEC-95Conplete

04-JAN-96Printed

04 -JAN -96

Project Lab ID

A363167PO Nuaber


18-DEC-95 12:05

Report To


Bill To


Saaple DescriptionCLIENT ID: 95 12/18/95LL1205SMW4IDESCRIPTION: WATERBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION: ' AMtiwt*" J» DAMIELSW • : ';-" !::\ '• ' Analysis 0»t»:! i|||«pS: .: •.

ParameterINITIAL WEIGHT OR VOLUMEFINAL VOLUME ; i;

SW846-35100 (;

Result10005

;'-'ii»ts .P2W.13Det. Unit

Rilf •Units

mlmL

POLYCHLORINATED BIPHENYLS (PCBS) SWB4€-8080A.• Analyst; t. UIUIMK -;; • • ; , • : • : -*mty»fs:Dater:-: ft|c |!>i::|L :

ParameterPCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 12621016 IS DEGRADED

irwtfui»»»ts :6$teti> ' -?:; .-';: :/;!;.)B P230.1.0' " -l'\!;:"- •. • '.'. '..'. . '.

Result0.00054

' BDL' :;:'••: v::-::::-:,,-.:::. • : : , : . • . , • • • •BDLBDLBDLBDLBDLBDL

"!;•• Test:. '0501.2.1

Det. Li*it0.0001

oioooi0.00010.00010,00010.00010.0001

:-il:li;lv--:t'tMt\ .

Units

rag/LJig/Ling/L

iwi/L

Sanpl* ComnentsBDL Below Detection Limit






Strvlce Location


Rectivcd20-OEC-95Complete

04-JAN-96Printed

04-JAN-96

Project Lab 10A363171

PO NuaberRN-24352-S 0-00

Saaplrt18-DEC-95 16:00

Report To


Bill To


Saaple DescriptionCLIENT ID: 95 12/18/95LL1600SMW6DESCRIPTION: WATERBLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDERDESCRIPTION

PCS SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510B ^ > ; ; ? ; ; ; > ^• ' Analyst: /. bwnEtSOB • . -. ^Analysts Date: a ii ||||| ^UlMl' <••••• <' -'. ':/:'" ' "' ' .• • *:>;C r«rtiTiP^«i,0f v ' -: .

Parameter


Result

1000

5" " "•' • " " ' :"

Det. Lieilt Units

mLM

POLYCHLORINATED BIPHENYLS (PCBS) •'' r'' ;• **w* D»t« &*£Hfr '

ticjuio-Liouio

PCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AKOCHLOR 1262

ParMieter Result

0.00030Wl -;':••••:::•

BDL

BDLBDL

BDLBDL

Det. Liaiit

0.0001

0.00010:00610.0001

0.00010:0061

Unitsg/L

mg/L

mg/L

1016 IS DEGRADED

Sanple CommentsBDL Below Detection Limit






Service Location


Received

20-DEC-95Couplet*

04-JAN-96Printed

04-JAN-96

Project Lab ID

A363170PO Ntafeer

RN-24352-S 0-00U«pled

18-DEC-95 16:00

Report To


Bill To


Sasple DescriptionCLIENT ID: 95 12/18/95LL1600EMW6DESCRIPTION: MATERBLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDERDESCRIPTION

^Datef ' :

ParaaeterINITIAL WEIGHT OR VOLUMEFINAL VOLUME

Result10005 • •

Det. Lieiit Unitsmlit

.i .0

PCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248

Pera«eter

PCB AROCHLOR 1260PCB AROCHLOR 1262

ResultBDL

BDLBDLBDLBDLBDL

Det. Lisiit0.0001OvOOOSo.oooiP;0001O.OOOI

0.0001djoooi

Units

nig/Lmg/L

mq/L

SMpte Comnents



This Certificate shaU not be reproduced, except in full,without the written approval of the lab.

Additional copies of this report sent to:RUSS CEPKO, UESTINGHOUSE ELECTRIC CORPORATION11 STANHIX STREET, PITTSBURG, PA 15222-1384



Service Location


Received

20-DEC-95Couplet*

04-JAN-96Printed

04-JAN-96

Project Lab ID

A363169PO Nuaber


18-DEC-95 14:45

Report To


Bill To


SMple DescriptionCLIENT ID: 95 12/18/95LL1445SMW7DESCRIPTION: WATERBLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDERDESCRIPTION

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION: : tests ' P330.1.& j'.


units


PCB AROCHLOR 1232PCB /\RQCHLOR 1242PCB AROCHLOR 1248PCB AROCHIJ)R 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Result

0.00029

BDLBDLBDLBDLBDLBDL

Det. limit0-0001OiOOOS0.00010.0001o.oooiOiOOOl0.00010;0001

unitsmg/L

mg/Lroci/L

1016 IS DEGRADED

ale C itsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTIHGHOUSE ELECTRIC CORPORATION11 STANVIX STREET, PITTSBURG, PA 15222-1384



Service Location


Received

20-DEC-95Complete

04-JAN-96Printed

04-JAN-96

Project Lab ID

A363168PO Umber


18-DEC-95 14:45

Report To


Bill To


Sample DescriptionCLIENT ID: 95 12/18/95LL1445DMW7DESCRIPTION: WATERBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION

PCB SEPARATORY rTJWEL LIQUID-LIQUID EXTRACTION•:" Ahaty»ti J. WUtlElSON " • ' Analysis D«te: !«iii»Pl;::-:.:

ParameterINITIAL WEIGHT OR VOLUMEFINAL VOLUME ! •

SH846-35IOB

Result10005 , ... ;.- .. . ,

-TestvPZMtfLi

Oet. Limit

illii'i''-'Units

mlmL

L.PC« UQUIO-LIOUIO

PCB AROCHLOR 1016PCS AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLORll262i

Parameter Result0.00028BDLBDLBDLBDL

BDLBDL

Det. Limito.oooio;ooo5o.oooi0:0001,00010001

Units

flig/Lmg/L

000 00010.0001

mg/L

1016 IS DEGRADED

SMple CommentsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, NESTIMGHOUSE ELECTRIC CORPORATION11 STANHIX STREET, PITTSBURG, PA 15222-1384




Received20-DEC-95Couplet*

04-JAN-96Printed

04-JAN-96

Project Leb 10

A363165TO Muter

RN-24352-S 0-00Svpled

18-DEC-95 09:50

Report To


Bill To


Ssspte DeteriptfonCLIENT ID: 95 12/18/95LL0950SMW8DDESCRIPTION: WATERBLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDERDESCRIPTION

PCB LIQUID-LIQUID

PsrsaeterINITIAL HEIGHT OR VOLUMEFINAL VOLUME i •.-,;•,.:;. -

Result930

Oet. Unit UnitsHlL

i> ij!3i!iiT«P: PCB sEP«At«r fuHNEt tiouip-uouiD EXTRACTi«( SH846-aft5ibft «30vi;i»^S!?^ :.:;':i' -':;:-tpl'-:lll'!::i:li|

PCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR IZ42PCB AROCHLOR 1248PCB mROCHLIJR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

PerimeterBDLBDLBDLBDLBDLBDLBDLBDL

Result Det. Limito.oooi0.0001Q*POQI0.0001ioiodoiQ.00010.0001

Units

Sample Comnents




Additional copies of this report sent to:RUSS CEPKO, HESJINGHOUSE ELECTRIC CORPORATION11 STANVIX STREET, PITTSBURG, PA 15222-1384


,D

ENCLOSURE #3

MONTHLY

SPRING SAMPLING

RESULTS

Lemon Lane - 6 Connected Springs + Sloney West & SnoddyGrab water sampling

SiteSlaughterhouse Sp.

PH Culvert

PHRoad

ICG-1

Quany Spring

Illinois Central Sp.

StoneyWest

Data08/3O/9509/08/9500/1310609/20/9509/27/9510/04/9510/11/9510/18/9511/15/9512/13/95

08/30/9509/06/9509/13/9509/20/9509/27/9510/04/9510/11/9510/18/9511/15/9512/13/95

08/30/9509/06/9509/13/9509/20/9509/27/9510/04/9510/11/9510/18/9511/15/9512/13/95

08/30/9509/08/9509/13/9509/20/9509/27/9510/04/9510/11/9610/18/9511/15/9512/13/95

08/30/9509/06/9509/13/9509/20/9609/27/9510/04/9510/11/9510/18/9511/15/9612/13/96

08/30/9509/08/9509/13/9509/13/9509/13/9609/20/9509/20/9509/20/9509/27/9509/27/9509/27/9610/04/9510/04/9510/04/9510/11/9510/11/9610/11/9510/18/9510/18/9510/18/9511/15/9611/15/9511/15/9512/13/9512/13/9512/13/96

10/27/9511/15/9512/13/95

Time13:15093009:0009:1009:0509:3009:1509:30092513:10

13:4510:0009:1509:3509:2509:4509:4510:0010:1013:25

14:0510:2009:2509:5009:4009:5510:1010:15102013:40

142511:3009:45102010:0010:1510:4010:4012:1014:30

14:4511. -0510:0010:4510:10103011:0011:0013:0014:40

152012:00103010:30103011:1511:1511:1510301030103011:0011:0011:0011:4511:4511:4511301130113013:4013:4013:4015:0015:0015:00

09:1011:1514:05

Sample*95 8/30/95 SL 1315 SSW95 9/B/95 SL 0930 SSW95 9/1 3/95 SL 0900 SSW95 9/20/95 SL 0910 SSW95 9/27/95 SL 0905 SSW95 10/4/95 SL 0930 SSW95 1 0/1 1 /OS SL 091 5 SSW95 10/18/95 SL 0930 SSW95 11/15/95 SL 0925 SSW95 12/13/95 SL 1310 SSW

95 0/30/95 PC 1345 SSW95 9/8/95 PC 1000 SSW95 9/13/95 PC 0915 SSW95 9/20/95 PC 0935 SSW95 9/27/95 PC 0925 SSW95 10/4/95 PC 0945 SSW95 10/1 1/95 PC 0945 SSW95 10/18/95 PC 1000 SSW95 11/15/95 PC 1010 SSW95 12/13/95 PC 1325 SSW

95 8/30/95 PR 1405 SSW95 9/8/95 PR 1020 SSW95 9/13/95 PR 0925 SSW95 9/20/95 PR 0950 SSW95 9/27/95 PR 0940 SSW95 10/4/95 PR 0866 SSW96 10/11/95 PR 1010 SSW95 10/18/95 PR 1015 SSW95 1 1/1 5/95 PR 1020 SSW95 13/13/95 PR 1340 SSW

958/30/9511 1425 SSW959/B/95I1 1130 SSW95 9/13/95 11 0945 SSW95 9/20/95 11 1020 SSW959/27/9511 1000 SSW9510/4/9511 1015 SSW9510/11/9511 1040 SSW9510/18/9511 1040 SSW9511/15/9611 1210 SSW9512/13/9511 1430 SSW

95 8/30/95 QU 1445 SSW95 9/8/95 QU 1 105 SSW95 9/13/95 QU 1000 SSW95 9/2O/95 QU 1045 SSW95 9/27/95 QU 1010 SSW95 10M/95 QU 1030 SSW95 10/11/95 QU 1100 SSW95 10/18/95 QU 1100 SSW95 11/15/95 QU 1300 SSW96 12/13/95 QU 1440 SSW

95 8/30/95 IL 1520 SSW95 9/8/95 1C 1200 SSW96 B713/95 IL 1030 SSW95 9/13/95 IL 1030 DSW95 9/13/95 IL 1030 ESW95 9/20/95 IL 1 1 1 5 SSW95 9/20/95 IL 1 1 1 5 DSW95 9/20/95 IL 1 1 1 5 ESW95 9/27/95 IL 1030 SSW95 9/27/95 IL 1030 DSW95 9/27/95 IL 1030 ESW95 10/4/95 IL 1 100 SSW95 10/4/95 IL 1 100 DSW95 10/4/95 IL 1100 ESW95 10/1 1/95 IL 1 145 SSW95 1 0/1 1 /96 IL 1 1 45 DSW95 10/11/95 IL 1145 ESW95 10/18/95 IL 1130 SSW95 10/18/95 IL 1130 DSW95 10/18/95 IL 1130 ESW95 11/15/95 IL 1340 SSW95 11/15/95 IL 1340 DSW95 11/15/95 IL 1340 ESW95 12/13/95 IL 1500 SSW95 12/13/95 IL 1500 DSW95 12/13/95 IL 1500 ESW

95 10/27/95 SW 0910 SSW95 1 1/1 5/95 SW 1 1 1 5 SSW95 12/13/95 SW 1405 SSW

PCB

BULBDLBDLBDLBDLBDL

BDL(UJ)BDLBDLBDL

BDLBDLBDLBDLBDLBDLBDLBDLBDLBDL



ID8.68(J)8.4(J)5.93.64.84.05.133

1514

31 (J)28 (J)BDL

20 WulftBDL1718

BDL1214

BDL1817

BDL1212

BDL1212

BDL1416

BDL

BDLBDLBDL

• MoWure condensation on the turbktty sample via

emparatui(degC)

1S.J17.217.017.814.915.914.514.11127.8

16.116.116215.913.013.413.713311.07.4

16.716.716.816.818216216.216.014.213.1

26.525224.122.416.919.919.017.79.73.3

16.916316215.814.515.014.914.511.67.7

14.013.9142

14.1

13.7

13.7

13.7

13.6

13.7

12.8

11.77.7

pravsntBi

onducttvtt(uS/cm)

778760767797850832850697847882

840825868830801824920862865843

810795808800860859908834883906

258222239235218268230223257897

656835852677700709892704708727

619599620

682

692

717

675

687

700

703

541743

Turbidity(ntu)

6.9172913.0014.1021.4011.3015206.5111.60

22*2.041.801.623.577.821.725.193.137.13

6.6*8.099.3512306.339.637.539.673235.97

0.98*1.141.141.551.181.651.020.781.09330

6.7*6.993.973.616.717.926.665254.2117 JO

0.61 *2.160.98

0.47

0.54

0.88

0.54

0.41

1.60

0.85

7.70528

Flow(Opm)

25202519161418261510

1-31-30.50.5<1<1<1<1<11

3-53-522

1-2111

2-41

5-103-55555545

30-40

3310510102-44625

373130

37

24

27

24

13

13

10

25

field measurement. These am

Convnonts

DuplicateField blank

DuplicateFieM blank

DuplicateFWdUank




DuplicateRen blank

DuplicateFtou blank

TSS« 26. stoim samplestart « 0.1 25 ft.

Heritage lab results.

02/09/96

Attachment 1: Data Validation for the Lemon Lane DirectlyConnected Springs for November/December, 1995

1. The validation was performed per the requirements for level4 data in the project QAPjP. This includes a check for:Holding Time, Calibration, Blank Contamination, Precision,Accuracy, and Accuracy of Nominal Reporting Limits againstmethod requirements. All analyses met method requirements.The data is accepted with no qualifications.

2. Note: We have reviewed data packages for the followingattached samples only. This totals 7 springs sampled twicefor a total of 18 analyses (including 4 blanks and dupes) .

3. The QAPjP requires an assessment of the overall data qualitywith respect to Precision, Accuracy, Representativeness,Completeness and Comparability (PARCC) .

o Precision and accuracy: Precision and accuracy were accessedby reviewing the lab performance on lab spiked samples, labspike duplicates and filed duplicates. All requirementswere met.

o Representativeness: The representativeness requirementinvolves an assessment of the field sampling and labanalytical techniques. The field sampling locations andtechniques as well as lab procedures were in accordance withthe approved sampling plan and QAPjP. There were nodeviations and the representativeness requirement was met.

o Completeness: The completeness goal for the project was forall project data to be 90% accepted. Completeness iscalculated by dividing the total number of acceptableanalyses by the total performed. An acceptable analyses isdefined as one that conformed to QC protocols and is notrejected. There were no rejected analyses so thecompleteness goal was met.

o Comparability: All the samples taken, analyzed andvalidated by Westinghouse were taken by Westinghousesampling crews using the same procedures and analyzed by thesame laboratory. Therefore within the samples taken byWestinghouse there are no comparability issues.

Overall, the main objective of the sampling event was todetermine if PCBs are present at a concentration of .1 ppb ormore. The sampling and analysis performed by Westinghouse wasconsistent with this goal and the data is of sufficient qualityto satisfy this goal.



Received18-OCT-95

Complete

25-OCT-95Printed

26-OCT-95


TO Nuofcer


18-OCT-95 09:30

Report To


Bill To


Sample DescriptionSAMPLE ID: 95 10/18/95 SL 0930 SSWBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: BLOOMINGTON PROJECT

PCB SEPARATORYAnalyst: R. RIDGE


FUNNEL LIQUID-LIQUID EXTRACTION SH846-3510A;: ;; ; ' iAnatysfs Bater l^-OCT-95 test j P230. 1.0

ParameterOR VOLUME 985

$ >>:

Result Oet. Limit UnitsmLmL

POLYCHLORINATED BIPHENYLS <PCBS) SH846-8080Analyst: L. WILLIAMS Analysis Date: 19-OCT-95 Instrument: GC/ECD Test: 0301.2.0Prep: PCS SEPARATORV •:- tKt:-l:iO Itt>Lt'aiUiD''.Ekl1UCTION SU846-3510A P230.1.0


Parameter Result


Oet. Limit Units0.0001 mg/L0.0005 mg/L0.0001 mg/L0.0001 mg/L0.0001 mg/l0.0001 mg/L0.0001 mg/L0.0001 mq/L







Service Location


Received

18-OCT-95Complete

25-OCT-95Printed

26-OCT-95


PO Nuaber


18-OCT-95 10:00

Report To


Bill To


Sample DescriptionSAMPLE ID: 95 10/18/95 PC 1000 SSWBLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDERDESCRIPTION: BLOOMINGTON PROJECT

PCB SEPARATORYAhalyst: R. RIOGE


FUNNEfc LIQUID-LIQUID EXTRACTION SH846-3510A-^^^ jtofcl ljirittttr'l iW1 : ' . • . ' • . • • • .h" - - . - . . . •:-:::-;-- ' - ' '" / • • ' " " • • ' • • • " . T«*ti P230.1.0


5

Result Det. Limit UnitsmLmL

POLYCHLORINATED BIPHENYLS (PCBS) SH846-8080Analyst: L. WIU.IAMS : :>haiysfs Oatet 20'OCT-9S Jhstrument: GC/ECO Test; 0301.2.0

: Prep: PCB SEPARATORY FUNNEL LIQUlD-llQUlD EXTRACTION SU846-3510A P230.1 .0

ParameterPCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232

CB AROCHLOR 1242rPCB AROCHLOR 1248

PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262


Det. Limit0.00010,00050.0001O.OOQ10.00010.00010.0001d.oooi

Unitsmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

Sample Comments



This Certificate shall not be reproduced, except in fulltwithout the written approval of the lab.





Received

18-OCT-95Complete

25-OCT-95Printed

26-OCT-95

Project Lib ID

A357431PO Hunber


18-OCT-95 10:15

Report To


Bill To


Sample DescriptionSAMPLE ID: 95 10/18/95 PR 1015 SSWBLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDERDESCRIPTION: BLOOMINGTON PROJECT

PCB SEPARATORYAnalyst: R. RIDGE


FUNNEL LIQUID-LIQUI• l-f VV:::: Si&I JjrtiityM t t>»te:

Parameter

OR VOLUME

D EXTRACTION SW846-35IOA f ; '^19-OCT-95 '•:•;.••;:•;. . • • - • • : : • : • . • • • : " • / . ; • • • . ' ' • • : ' - " - : : : T*slts:PZ56.1-0 .

Result10005

Det. Unit UnitsmLmL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080Analyst: ;| ?;wiM4 :r-jWf : ^«-i>»»«*?::'*-OCf-95- Instrunentt GC/KD ; " testt 0301.2.0Prep: PCS SCTARATQRr^

ParameterPCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOfr 1242 ; >PCB AROCHLOR 1248PCB AROCH10R 1 54PCB AROCHLOR 1260PCB AROCHtOR 1262


Det. Li»it

0.0001

0,00050.00010:60010.00010.00010.00010.0001

Unitsmg/Lmg/Lmg/Lmg/Lmemg/tmg/Lmq/L

Sanple ComentsBDL Below Detection Limit




Approved : _ Page 1 (last page)


Service Location


Received

18-OCT-95Complete

25-OCT-95Printed

26-OCT-95

Project Lab ID

A357432PO Nuber


18-OCT-95 10:40

Report To


Bill To


Saapte DescriptionSAMPLE ID: 95 10/18/95 II 1040 SSWBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDERDESCRIPTION: BLOOMINGTON PROJECT

PCB SEPARATORYAnalyst: G. CUOUSE


FUNNEi UQUIfr-fclQUID EXTRACTION SH846-3510A ^^^mmmm''\ '••••- •<';\'"'!;<ffaLlfri*-tlit*t-:\9*0&^ '•••-• :"-:' •' • "• "•'' ' • ' • • • ' . ': - \;-:ofii»tj:'p230,.t,0


5

Result Oet. Linit UnitsmLmL

POLYCHLORINATED BIPHENYLS (PCBS) SH846-8080S Analysts U tt.U^;;!S |l ^^«^0•t« .aBpOfet-«5:. Iftatrwent: GC/ECD ,. .. te»tt 0301.2.0

*^ .. • : ...:; V;.:" •?.';:" : ':

ParaawterPCB AROCHLOR 1016PCB AROCHLOR im°CB AROCHLOR 1232

_CB AROCHLOR I24ZPCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262


Det. Linit0.00010.00050.0001o.dooi0.00010.00010.00010.0001

Unitsmg/L

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmq/L

Sanple CoamentsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, NESTIHGHOUSE ELECTRIC CORPORATION11 STANUIX STREET, PITTSBURG, PA 15222-1384




Received

18-OCT-95Complete

25-OCT-95Printed

26-OCT-95

Project Lab ID

A357433PO Nunber

RN-24352-S 0-000Sanpted

18-OCT-95 11:00

Report To


Bill To


Saople DescriptionSAMPLE ID: 95 10/18/95 QU 1100 SSWBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDERDESCRIPTION: BLOOMINGTON PROJECT

PCB SEPARATORYAnalyst: G. CLOUSE


FUNNEL LIQUID-

ParameterOR VOLUME

LIQUID•Date: 19

EXTRACT ION SW846-3510A"OCt-95 Test: P230. 1.0

9605


POLYCHLORINATED BIPHENYLS (PCBS) SH846-8080Analyst; L. WILLIAMS:'' ':'::;::

::.}:;;|i!:lyv::;.bjite:-:'2D*6(:T-95 Instrument: GC/EO)

Prep: PCS SCPARATQRY FUNMEL LIQUIDtlOUlD EXTRACTION SU846-3510A P230.1.0T**tT 03(11.2.0.


ResultBDLBDLBDL0.0040BDLBDLBDLBDL

Det. Limit0.00010.00050.00010.00010.00010,00010.00010.0001

Unitsmg/LfligAmg/Lmg/LIDC

mg/xmg/Lmq/L

Sanple CementsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATION11 STANVIX STREET, PITTSBURG, PA 15222-1384



Service Location

HERITAGE ENVIRONMENTAL SERVICES, INC.COMMERCIAL LABORATORY OPERATIONS7901 M. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8305

Received18-OCT-95

Complete

25-OCT-95Printed

26-OCT-95


PO NumberRN-24352-S 0-000

Smpled18-OCT-95 11:30

Report To


Bill To


Sample DescriptionSAMPLE ID: 95 10/18/95 IL 1130 SSWBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: BLOOMINGTON PROJECT

PCB SEPARATORYAnalyst: G. CLOUSE


FUNNElf LIQUID-LIQUID EXTRACTION SW846-3510A;vv:';:;-y::-:i- :Ahatv*<»-0*te:-;r9-OCT-y5 .• •• :;;: . • . :- :t»ft? P230.1.0


5


POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080Analyst: L. WILLIAMS :.j K -^V >; fttiatyif * "Date: :»*a^^95:y . (Mtrtnent GC/ECD,. :.;;-;::. Test: 0301,2.0Prep: PCB SEPARATOR^ FUMEL LIQUID-LIQUID EXTRACTION SU846-3510A PZ30. 1.0

PCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232"'*B AROCHLOR 1242>^B AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

Parameter Result6DLBDLBDL0.012BDLBDLBDLBDL

Det. Limit

0.00050.00250.00050.00050.00050.00050.00050.0005


1:5 dilution

Sample CowmentsBDL Belw Detection Limit




Approved : Ax"ZT

Page 1 (last page)


Service Location


Received

18-OCT-95Complete

25-OCT-95Printed

26-OCT-95

Project Lab 10

A357435PO Nunber

RN-24352-S 0-000Sanpled

18-OCT-95 11:30

Report To


Bill To


Sanple Description

SAMPLE ID: 95 10/18/95 IL 1130 DSW-DUPLICATEBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: BLOOMINGTON PROJECT

PCB SEPARATORYAnalyst! G.CLOUSE


FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510A: : ; • : • . : ; Analysts Date: 19-OCT-95 Test: PSO. 1.0


5

Result Det. Listit UnitsmlmL

POLYCHLORINATED 6IPHENYLS fl>CBS) SH846-8080 ; ? ;: Ahalyiti U : iLiiAW:>'-;-?lt:|fe Initrunent: 6C/ECD ' ' • .'; :

: !: - • ; • ; ; : ; • : •;:T*«t;: .0501*2.0 :

Pfep: PCS SEPARATORr FUNNEL £fQulbVlIOUlD EXTRACTION SU846-3510A P230.1.0 ;; :


ResultBDLBDLBDL0.012BDLBDLBDLBDL

Det. Limit0.00050.00250.00050.00050.00050.00050.00050.0005

unitsmg/Lmg/Lmg/Lmg/Lmemg/umg/Lmq/L

1:5 dilution

Saiple Comsents







Service Location


Received

18-OCT-95Complete

25-OCT-95Printed

26-OCT-95

Project Lab ID

A357436PO Nunber


18-OCT-95 11:30

Report To


Bill To


Sanple DescriptionSAMPLE ID: 95 10/18/95 IL 1130 ESW-FIELD BLANKBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: BLOOMINGTON PROJECT

PCB SEPARATORYAnalyst: fi.CLOUSE


FUNNEL LIQUID-LI.:•''"? •' --.V::;;iilfiaiV»<i:'::Oi(

ParameterOR VOLUME

QUID EXTRACTION SW846-3510Arte: 19-OCT-95 Itesit: P230.1.0

9305

Result Det. Limit unitsmLmL

POLYCHLORINATED BIPHEMYLS (PCBS) SW846-8080Analyst: t; ViLUJ i: ^^^^ ! ^** '-; -!*!*^ ':" Inttrunent: GC/ECD ' • ; ' . - ' • • ; • ' . : • . • Test: 0501.2.0Prep: PCB SEPARATOR FUNNEL LIOOID- LIOUID EXTRACTION SW846-3510A P250.1 .0

ParaneterPCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232

:B AROCHLOR 1242^CB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262


Det. Limit0.00010.00050.00010.00010.00010.00010.00010.0001

Unitsmg/Lrog/Lmg/Lmg/Lmg/Lmg/Lmg/Lmq/L

Saiple ComentsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, UESTINGHOUSE ELECTRIC CORPORATIOH11 STANUIX STREET, PITTSBURG, PA 15222-1384



Service Location

HERITAGE ENVIRONMENTALCOMMERCIAL LABORATORY (7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8305

SERVICES, INC.)PERATIONS

Received

Ol-HOV-95Complete

07-DEC-95Printed

07-DEC-95

Project lab ID

A35894PO Nuaber

RN-24352-S -0-Savpled

27-OCT-95 14:15

Report To


Bill To


Seaple DescriptionCLIENT ID: 95 10/27/95 SW 0910 SSWBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION


7905

Result Det. LiMit Unitsmlrot

POLYCHLORINATED BlPHEHYlS (PCBS) SH84

PCB AROCHLOR 1016

PCBlARSLjp£

PCB AROCHLOR 1248

PCB AROCHLOR 1260

ParaawterBDL

Result

BDL

BDL

BDLiDl

Oet. LiBit0.0001

0.0001

0.0001Wimmp.pool

mmm

units

1:5 DILUTIONMIXTURE DEGRADED 1242 AND 1248

SUSPENDED SOLIDSter

26Result Det. Liaiit Units

nw/L

CcMncntsBDL Belw Detection Limit




HERITAGE ENVIRONMENTAL SERVICES. INC. Sample ID; A358941 95 10/27/95 SH 0910 SSIComfits

Additional copies of this report sent to:RUS5 CEPKO, UESTIHGHOUSE ELECTRIC CORPORATION11 STANHIX STREET, PITTSBURG, PA 15222-1384

Approved : (TTU f W U Page 2 (last page)



Received

15-NOV-95Complete

Ol-DEC-95Printed

Ol-DEC-95

Project Lab ID

A360175PO Nunber

RN-24352-S 0-00Swpled

15-NOV-95 09:25

Report To


•ill To


Staple DescriptionCLIENT ID: 95 11/15/95 SL 0925 SSWSAMPLE ID: 95 11/15/95 SL 0925 SSWBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDERDESCRIPTION: GRABPROJECT NAME: LEMON LANE

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SH846-35IO& ; - ; ' ^^ ^- , > 1Aftttytt* n MWCMf* .- -^ - '*nrty*i» t«t*?'1$-»WSH«E*v "* *<• , - ?'«" -" **> '"" - ' , ttM&ftSMj* "- "'-'- ^

PereneterINITIAL WEIGHT OR VOLUMEFINAL VOLUME

Result10005

Det. Limit Units

mLmL

POLYCHLORIHATED BIPHENYLS (PCBS) S«

PCB SEPAHATOBY

PCB AROCHLOR 1016PCB AROCHLOR 1221PCB AROCHLOR 1232PCB AROCHLOR 1242PCB AROCHLOR 1248PCS AROCHLOR 1254PCB AROCHLOR 1260

ParMnterBDLBDLBDLBDLBDLBDLBDL

Result Det. LiMit0.00010,00050.0001$,00010.00010.00010.00010.0001

Units

mg/Lm/i

•g/Lnw/L

Seeple ComentsBDL Below Detection Limit


This Certificate shall not be reproduced, except in fi/77,without the written approval of the lab.

Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATION11 STANHIX STREET, PJTTSflURG, PA 15222-1384



Service Location



Ol-DEC-95Printed

Ol-DEC-95

Project Leb ID

A360176PO Mater

RN-24352-S 0-00tapled

15-NOV-95 10:10

Report To


Bill To


Savple DescriptionCLIENT ID: 95 11/15/95 PC 1010 SSUSAMPLE ID: 95 11/15/95 PC 1010 SSWBLANKET ORDER RELEASE 1 : NOT RECEIVED WITH ORDERDESCRIPTION: GRAB

r PROJECT NAME: LEMON LANE

PCB SEPARATORY FUNNEL tlQUXD LlEI)UItli|atfiy!l5|;plit |:;|j5:;:M«afllirr •, , ,, iJfMta&'JMtfiHIti ttt

PareMterINITIAL WEIGHT OR VOLUMEFINAL VOLUME

itlllt JHB4f«35IWv; ; ; !»V^^£<T ^ ~i - ^ * - ,., «& .. H v, ;, T^**fatoto$&& , *

Result Det. Unit Units1000 ml5 ml

POLYCHLORIHATED BIPHENYLS (PCBS) SW46-8W•.*h»ly*tt;4,.miWX ,% .. •• ' { ;Jta*ly»«>»*titV^> iPrepl PCS tEHUttTQRY FUMfEl LIQBlIHLlttllD Bmucrf0| i


: ;'Result Det. Lisitt Units

BDL 0.0001 rog/L^W&ÂJffiCflL^R;: ^ :x-xBDE-^^^-^^ -XYX^x-xQi-OOOS^ xiM/fc^^^^^

CB AROCHLOR 1232

PCB AROCHLOR 1248

PCB AROCHLOR 1260

BDL 0.0001 mg/L^•>x— ••:xl:-:->^Rrt(-x-;-:-^^^^•^•Xv:-x-v> ;:v:vPWfcxvX-xx-x:x^--x-:vX-::x-::xx-x-x-x-x::-x-Xv:-x- ;xvXvX-xV;*-UWVl.:.v xflig/::fc-x-:vX-:-x-x-x-x:x

BDL 0.0001 ng/LvXvX-x-:-^ :X'::BDtvx:x::v::x-v::x-x-::x:::x^x::-XvXv:-x-x-XvX- •x-x-xÔ.iQO.Ol-x- ving/xtvx^xx-x-vx-x-:

BDL 0.0001 mg/L:v-™>£-stv:-x-^•;;.:•;:;.:•::;. :"v/DUtv//////^v/AV"//A\v//:///:Âv:^.\v/.-.v.v.v.v •.•.•.•.•.•.•.v.v.V-VWWJ.'-v •.•.HH|/.-.l;v.v.v.v.v.v.v.v.v.



This Certificate shall not be reproduced, except In full,without the written approval of the lab.





Received

15-NOV-95Complete

Ol-DEC-95Printed

Ol-DEC-95


PO Nuaber


15-NOV-95 10:20

Report To


Bill To


Staple DescriptionCLIENT ID: 95 11/15/95 PR 1020 SSWSAMPLE ID: 95 11/15/95 PR 1020 SSWBLANKET ORDER RELEASE 1: NOT RECEIVED WITH ORDERDESCRIPTION: GRABPROJECT NAME: LEMON LANE ^

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510B ; ^c^^ tf/^:^M^ \


POLYCHLORINATED fl|PHEmS (PCBS) SW846-808(Wt

Prep* WttWMWWf POMEL Liab»>£ia8D tXflACTIO* CU646-3SKParameter

PCB AROCHLOR 1016

PCB AROCHLOR 1232

PCB AROCHLOR 1248

PCB AROCHLOR 1260' vEA ffWJ... ..- ]

Result Det. Liaiit Units1000 mL

"5 " :'IL"

IBS^;:': f 'Result Det. Linit Units

BDL 0.0001 mg/L:v:;:-:BDl :;: x : ^

BDL 0.0001 mg/L

BDL'""""" ••••'•'•••••••-•••••••'•'••••••'•••••••'•••• 0*0001 mg/L:::-x-:BQ£:-:-::>x::-::::::^ v.:::v:::-:v:0:;:00QJx;:-:TO

BDL 0.0001 mg/L— 1 H 1 — _LMJ 1

SMpIt CoBHMntsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATION11 STAHHIX STREET, PITTSBURG, PA 15222-1384



Service Location


Received

15-NOV-95Complete

Ol-DEC-95Printed

Ol-DEC-95

Project lib ID

A360179PO Nu*er


15-NOV-95 12:10

Report To


Bill To


L

Staple DescriptionCLIENT ID: 95 11/15/95 II 1210 SSWSAMPLE ID: 95 11/15/95 II 1210 SSWBLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDERDESCRIPTION: GRABPROJECT NAME: LEMON LANE

PCB SEPARATORS FUNNEL LI QUID-LI QUID EXTRACTION SH846-35IOR


10005'

Result Det. Unitmlml

Units

POLYCHLORINATED BIPHENYLS (PCBS)An.ly«tJ J. mm* ******* 0*tl»Preps PCB SEPARATOKT FUNNEL LfttinKLtOUIft

PCB AROCHLOR 1016

CB AROCHLOR 1232

PsrsMter

BDLResult Det. If aft

0.0001xlxtOPDDS!

0.0001

units

PCB AROCHLOR 1248PGBli CtiKfflliZSlPCB AROCHLOR 1260

BDL

BDL

BDL

.0.0001.

oioooi

Sasple Coasents








Received

15-NOV-95Coaplete

Ol-DEC-95Printed

Ol-DEC-95

Project Lab ID

A360180PO Nuaber


15-NOV-95 13:00

Report To


SaapleCLIENT ID: 95 11/15/95 QU 1300 SSWSAMPLE ID: 95 11/15/95 QU 1300 SSWBLANKET ORDER RELEASE #: NOT RECEIVEDDESCRIPTION: GRABPROJECT NAME: LEMON LANE

Bill To


Description

WITH ORDER

PCB SEPARATORY FWWEL LIQUID-LIQUID EXTRACTION SW846-3510B ^ > ; *f>^<^;waiyM-J 'T-* rllwKWf * •••. *• "->\ ^ :- WHy>tJt Ottt43 iV'-HOV™-?"-*"1..


sw M is? - •• ^ *- ' ' - ' tmll ?MWvl*W- ' ' •.

Result Det. Lialt UnitslOPP mL5 «fJHL.

POLYCHLORINATEO BIPHENYLS (PCBS) SW84€-8080A


• PCS '•'• AROGtiLOR • • J '22i'' '• '•^"''"''•''-•--••'•''-•'-•'--•'--'-•'•^•^•^'--•'-^•'^"•"^^PCB AROCHLOR 1232

PCB AROCHLOR 1248

.?w rwm '.iw

•55. . ; ' '< ^ "" "" ' •••• --xj "~*\ 2^-^ iJaJ. "•

SB*® !?? 'Result Det. Lisiit Units

0.0051 0.0002 mg/LS IMSiOiODls

BDL 0.0002 rog/Ls w^$i$QQ& mfi£t*mt

BDL 0.0002 mg/L:v >::>:BM:>SH::>>::>:::: ^ O^QOM ::: /;I S:;i::vS

BDL 0.0002 mg/L; mmm oom m&mmm

AROCHLOR 1016 IS DEGRADED1:2 DILUTIOH

Saaple CoaaentsBDL Below Detection Limit





HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A360180 95 11/15/95 QU 1300 SSMtS

11 STAHU1X STREET, PITTSBURG, PA 15222-1384



Service Location


Received

15-NOV-95Ceeplete

Ol-DEC-95Printed

Ol-DEC-95

Project Lab ID

A360181PO Niafeer

RN-24352-S 0-00Ssepled

15-NOV-95 13:40

Report To


Bill To


Seeple Description

CLIENT ID: 95 11/15/95 IL 1340 SSUSAMPLE ID: 95 11/15/95 IL 1340 SSUBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION: GRABPROJECT NAME: LEMON LANE

PCB SEPARATORY FUNHEL LIQUID-LIQUID EXTRACTION SH84€-3510B .. :: : . , . . : ; ,: , . ,•,:,:ftM*It^«. T" *" ftttM'ifcll'li'l v * . < v t^.tt4*}u tkfa»A. 4 Au-IWtuAlt*' "^ •.A>.•:•. •: ~-f •. *~LJ.*. . M.*em-A "--a w. '-V*HtmiTfifff T* rlHWUSH*" j • • > ^ ? #h»iy»f * S*Wi iQ-KW'W-.-^ xa^t

PersaeterINITIAL WEIGHT OR VOLUMEFINAL VOLUME

fswv-w ,-- - -- J««v« r*j*i» i *w ^ \ •

Result10005

Det. Lisiit Unitsmlml

POLYCHLORINATED BIPHENYLS (PCBS) SW8W-8080AAn.ly.tt A* Wm* - \; A - " - *t»t*«l$ **»Pfepif PCS SO»AMTt»1F raNMBL tMOJO-ilOKD EXTRACTION

PereaeterPPBI AROCHLOR 1016

PCB AROCHLOR 1232

Result0.012

Det. LiMit0.0005

Units

BDL

BDL

BDL

xM0025>0.0005

.PCB.jlpraU!RJl248..

PCB AROCHLOR 1260

0.0005wmm0.0005 mg/L

' ' ' " '

1016 IS DEGRADED1:5 DILUTION

Senple CoMwntsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO. WESTINGHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A360181 95 11/15/95 IL 1340 SSUSaapU CoMtnts




Service Location


Received

15-NOV-95Complete

Ol-DEC-95Printed

Ol-DEC-95

Project Lab ID

A360182PO Nuiber


15-NOV-95 13:40

Report To


Bill To


Sample DescriptionCLIENT ID: 95 11/15/95 IL 1340 DSWSAMPLE ID: 95 11/15/95 IL 1340 DSWBLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDERDESCRIPTION: GRABPROJECT NAME: LEMON LANE —

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXHWCTtf5: 5W»6*35IO» 4 ; ; '' :;V4<! ,

INITIAL WEIGHT OR VOLUM?FiNAtTOLUME

Result Det. Li*it Units1000 raL5 ml

POLYCHLORIHATED EIPHENYLS (PCBS) SW846-801Analyttt 4* "(MWFWh -:,;• ,f y- taalifclfStttK INWMfcPrej»< P4S SERMUTOtY fttWEt LIQUlDHLlOUID EXTRXCTIOJi SUft

PCB AROCHLOR 1016 "" ^

PCB AROCHLOR 1232

PCB AROCHLOR 1248

PCB AROCHLOR 1260

lillS^:f iS^ 'Result Det. Linit Units

0.012 0.0005 mg/L

BDL 0.0005 mg/L

BDL 0.0005 mg/L

BDL 0.0005 mg/L

AROCHLOR 1016 IS DEGRADED1:5 DILUTION




Additional copies of this report sent to:RUSS CEPKO, HEST1NGHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A360182 95 11/15/95 IL 1340 DSWSaopl* Conents




Service Location


Received

15-NOV-95Complete

Ol-DEC-95Printed

Ol-DEC-95

Project Lab ID

A360183PO Muter

RN- 24352 -S 0-00Sealed

15-NOV-95 13:40

Report To


SanpleCLIENT ID: 95 11/15/95 IL 1340 ESWSAMPLE ID: 95 11/15/95 IL 1340 ESWBLANKET ORDER RELEASE f : NOT RECEIVEDDESCRIPTION: GRABPROJECT NAME: LEMON LANE

Bill To


Description

WITH ORDER

., ,

PCB SEPAIWTORY FUNNEL LIQUID-LI(W EXTRACTION SW846-3510B , * ': -'•,•-:. , ,: /w^5 ,• ™?WV*»<I.V**\**.'''"^WPJSSB!S¥HS;jAWiS¥- WfctyMW Wit*'? 1p-WW ff' \

ParameterINITIAL WEIGHT OR VOLUMEFINAL VOLUME '•' '''

,'•. , ,- •. • -. nm

Result Det. L1000

"5

POLYCHLOHNATED B1PHENYLS JFCBS) SWB46-808<^^V^Vl '"'*" "* -; t ; V "* '

prept pta:i«tpXiwTflJnr roMct irao bMitpiD EXTRACTION st04e^3Sitti P2Stt«4»9 "- ::' ' ' ' '"•• 'Parameter

PCB AROCHLOR 1016

PCB AROCHLOR 1232'P(^v'AROQ}WHft''"i5r4^"-"v-'-^^^^^^PCB AROCHLOR 1248

PCB AROCHLOR 1260>: PflpftlHWHJW^..r.\&:-twsi\tf\ku&-:;*GiV&::""-":";"^^

Result Det. LBDL 0,

BDL 0.,,,:•: ,= ,,,,-,,,,,,-,,,,,-, -..„

x Xv/xBI^^x\v:v//x-x\vX\vXvXvXXvXvXvX-XvX<vX\^^ x-x-x-x-x-xQ-^

BDL 0.

F*W* **«r <i*it Units

..Ik.

ff -. *•• f-. f.v A > w ^ <. . .

*" s ^ JvS" C^ & "• ••

{•it units0001 mg/LOOD5 «g/L0001 rog/L«001 »g/l0001 mg/LOQQ1 mg/L0001 mg/L'Aft A I Jnft/tUUUl v/HJ U

Saaple CoaawitsBDL Below Detection Limit






Service Location


Received

15-NOV-95Complete

01 -DEC -95Printed

Ol-DEC-95

Project Lab ID

A360178PO Huaber


15-NOV-95 11:15

Report To


Bill To


Saaple DescriptionCLIENT ID: 95 11/15/95 SW 1115 SSWSAMPLE ID: 95 11/15/95 SW 1115 SSWBLANKET ORDER RELEASE *: NOT RECEIVED WITH ORDERDESCRIPTION: GRAB

I PROJECT NAME: LEMON LANE

Paraa»terINITIAL WEIGHT OR VOLUME

r:FiNAmVOtUMElP^

Result Det. Llarit Units1000 mL

POLYOiLORIK^TED BIPHENYLS f PCBSV SWB46*&01

'•'•:•'.•'•' f S^^P*> "• SWWt- ;- **••• ffW™ * ^* * •: • : P* ^ C*r •:•. *i> * ?^f- • •• x »Si?ff»* " >:-ft™ * "Hi* * •* S^S :-TTW^P


'-vnf*n*\vjinn*>M if 'Anv.vr •*%*•/% '••' •*• .v.v.v.v.v.v.v.v.v.v.v.v.v.vv.v.v.v. vv:::PGB,xAMQGHlORx-J22:l ^

'B AROCHLOR 1232H*"-"-'-'J( »VA[f*M*'-"*»UfiV.v«.jV -»'J«.v.v.v.v.v. .%V.V:. V.V//AV///////////////////.-.-.V.'.'.-.-/.V.-.V.V.V.I.V.V.V.V.V

l iMm^XM^PCB AROCHLOR 12483cMim$a ^PCB AROCHLOR 1260

>>PfH flOfi(M!f>A1J^^

l ^^^^^^^^^^^^^^^^^^^^^^^^^^^^^ ffi

Result Det. Ltait UnitsBDL 0.0001 mg/L

ox^x-XvX v:-x:BDL:;::x:-xx;:-:x;x-xx-x-:;: o:;.x-x--:.x-x-:-v :vx:-±;--<Ji:OOD5-x JJJg/fes^o ;--BDL 0.0001 mg/L

.v.v.'.v.v.v.v v.1.v.-»s«.l-.-.-.-.- •.•.V.\V.-.-.V.\\V.-.-.V:.>.-.V.\V.-.V.V.-.-.-/.V:A-.-.-.I.-.\V.V ':.:::-;;:.:"jK-'--'*m*tr*"-' .•;I ,:. .' K.V/.I.V.V.-.V.-.V.-.V.V:jxvxvx-xvx ^mmmm^mmm^M^ mzm*w^ mm^m .BDL 0.0001 mg/L

mm wMmmmmmmmmm mmfimtom, fimmmBDL 0.0001 mg/L

v:v:v>>x-:v/:|:v:;

Saaple CosMsntsflDL Below Detection Limit







Received

14-DEC-95Complete

28-DEC-95Printed

28-DEC-95

Project Leb ID

A362669TO Muter


13-DEC-95 13:10

Report To


SenileCLIENT ID: 95 12/13/95 SL1310SSWDESCRIPTION: WATERBLANKET ORDER RELEASE #: NOT RECEIVEDDESCRIPTION

Bill To


Description

WITH ORDER

PC*: smRATORl^Mitt^^itf^^

ParameterINITIAL WEIGHT OR VOLUMEFiNAEsvoiuME:;

Result1000

Det. LiMit UnitsmL

PCB AROCHLOR 1016

JTCBJ ^

PCB AROCHLOR 1248PCS O tOR l£54?PCB ARQCHLPR 1260

PCB AROCHLOR 1268

ParameterBDLBDLBDLBDLBDLBDLBDLBDtBDL

Result Det. L1*it0.00010

0.0001010*00010;0.00010

o.oooio0.00010

Units

fflg/Lmg/L

mg/L

CannttntsBDL Below Detection Limit



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Bill To


SMple DescriptionCLIENT ID: 95 12/13/95 PC1325SSWDESCRIPTION: WATERBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDERDESCRIPTION

*£». 0Parameter

INITIAL WEIGHT OR VOLUMEFINAL; VOLUME; ; : IWx.: m

Result10005 .--

Det. Liait Unitsmlml

PCB AROCHLOR 1016Parameter

PCB AROCHLOR 1232•peisMQGHMPtzp:PCB AROCHLOR 1248

PCBAROCHLOR 1260

PCB AROCHLbR 1268

ResultBDLBDLBDLBDLBDLiBDLBDL

BDL

Det. Liarit0.00010

vmooosop.pooioo!oooioM000100.00010

impbom0.00010

Unitsmg/Lmg/Lmg/L«9/L

mg/Lm/lmg/L

Saapla ComentsBDL Below Detection Limit



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28-DEC-95

Project Lab 10

A362671PO Nuaber

RN-24352-S 0-00Sanpled

13-DEC-95 13:40

Report To


Bill To


Sanple DescriptionCLIENT ID: 95 12/13/95 PR1340SSWDESCRIPTION: WATERBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION

PC* SEPARATOR* *WNEi ilQUlO-tlQUID EXTRACTIM $»340*3$I3& —Analyst s j. ftANIEtSOi ; Xnvtyvf* Dates 1S-OE<M» " , T«*ts MSO.t.a


Result10005

Det. LiMit unitsroLmi

POi1fCHlORI»ATE0An»4y»t: S. «SS6tt-6«tR» toety«f« *et»t t*'BEC'9S .. ImtruMnt: VK/tm

, »np$ Ml SEPARATORlf FUWKi LJOUHW.IOU1D EXTRACTIOtt 6U8W-351CUJ P230.1.&

PCB ARPCHLOR 1016

PCB AROCHLOR 1232

Parameter

PCB AROCHLOR 1248

PCB AROCHLOR 1260AROCHLOR

ResultBDL

BDL

BDL

BDL

Det. Liaiit0.00010

Units

0.00010

0.00010

PrPPplp

o!oooibmg/Lig/txmq/LPCB AROCHLOR 1268 BDL

Sample ConnentsBDL Below Detection Limit






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A362673PO Nuataer

RN-24352-S 0-00Saspled

13-DEC-95 14:30

Report To


Bill To


Sample DescriptionCLIENT ID: 95 12/13/95 I11430SSWDESCRIPTION: WATERBLANKET ORDER RELEASE If: NOT RECEIVED WITH ORDERDESCRIPTION

mmanmumParameter


Result Det. Lt«it Units950 ml5 «L

POLYCHLORINATE0 BIPHENYLS (PCBS) SW84e-$01Analysts tt. IftssELL-anTU ;-imtyif»J>»t»t>1^6| ^Pripj PCt *B**RMQtt fUMWt U<K»tM.1aUtD iXtWUftt&«B

Paraawter

PCB ...AROCHLOR 1016

PCB AROCHLOR 1232' '""DPff'-'-'ftDA^WI-'-rtD^-VO-i.lTtD//.MIWJtTOtUlv//it^*tv/:^v.v/.v///^^^^^

PCB AROCHLOR 1248£»8»B$«3^^J$!UP£H^QRJ26Q

•••j^jjj'-^QCH^

» 0 * - * , ' ! 'f' "- instrument: GC/K& Tests 0501.2.0 -W*351t» «SK>.1,0

Result Det. Limit UnitsBDL 0.00010 mg/L

V.V. ."•.•.•;•: .v.-.vRn' fcv.v.v.-.V.-. .•.•...•.•.-.-.•.•..•..•.•.•.•.. •.-.v.-.v.'.-.-.-.. •.-.•.-.•.•.•.. -.V.', •.•.•.•.•.•.•.•.•'A-.V.iQ0Q50. iWI/L ' " ""'

BDL .v^^.^_v^^jyW)010.v ,mg/L,,..,.,,,, .,

BDL d!b0010 mg/L

.... Z ZBpLlIZ~ZZZ.vZZ ZJJIPQIQ." "W/L . . "... , . '."..BDL b!obdib WL

Staple ConsentsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, NESTINGHOUSE ELECTRIC CORPORATION11 STANHIX STREET, PITTSBURG, PA 15222-1384



Service Location


Received

14-DEC-95Complete

28-DEC-95Printed

28-OEC-95

Project Lab ID

A362674PO Number

RN-24352-S 0-00Saspled

13-DEC-95 14:40

Report To


Bill To


Sasple DescriptionCLIENT ID: 95 12/13/95 QU1440SSWDESCRIPTION: WATERBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDERDESCRIPTION

K» SEPARATOR* FUHMEl UHWID-UQUJD EXTRACTION $H$46-3$JO&Aneiy»*t £» lINGHNt - Analysts dates W-DECHW Tests *>230.t.O <


Result9405


POWtHLORIHATEDAnalysts «. KlSSELi-ftHlti ^ t^tyrt* D»t*M*HBB<M» * <• twtt-unrrtrr &/&*Prep: PCI SEPAWTdfilf FUWiCl. UOUJD-LIOU1D EXTRACTIOi SUSAo-35106

,Teat* ftSftl.2.0 * ,

PCB AROCHLOR 1016Paraewter Result

BDL

PCB AROCHLOR 1232*ei:ffliSM;?i24zi.PCB AROCHLOR 1248PCB AROCHLOR:1254PCB AROCHLOR 1260PGB ARQCHIOR 1262PCB AROCHLOR 1268

BDL

0.0033

BDL•Dftl.DUL" •

BDL

Det. Llsrft0.00010

""6'oooio"

Units

o.oooioo^oodio;o.oooio

mg/L

Oioooiao.oooio mq/L

1248 is degraded.

Coononts




Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATION11 STANHIX STREET, PITTSBURG. PA 15222-1384


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A362674 95 12/13/95 QU1440SSWStaple Cements

Approved : Y JU/W/y/tZU: > \U - Page 2 (last page)



Received

14-DEC-95Complete

28-DEC-95Printed

28-DEC-95

Project Lab 10

A362675PO Number


13-DEC-95 15:00

Report To


Bill To


Sanple DescriptionCLIENT ID: 95 12/13/95 IC1500SSWDESCRIPTION: WATERBLANKET ORDER RELEASE f: NOT RECEIVED WITH ORDERDESCRIPTION

: SEPARATORParameter

INITIAL WEIGHT OR VOLUMEFINAL; .'VOLUME mmm^-

Result950

Oet. LtaitmL

Units

PCB AROCHLOR 1016MAMGHLOR 1221PCB .AROCHLOR 1232MP^^tQRI242VPCB AROCHLOR 1248

Paraneter

PCB AROCHLOR 1260PCpAROCHtOR 1262PCB AROCHLOR 1268

ResultBDLBDLBDL

Det. Liaiit0.00050OV00250;0.00050

BDL0.014

;BDLBDLBDLBDL

0.00050M000500.00050

0.00050

Units

mg/Lm/img/L

mg/L1:5 dilution.1248 is degraded.

Sample Cements




Additional copies of this report sent to:RUSS CEPKO, NESTINGHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A362675 95 12/13/95 IC1500SSMContents


Approved : M ^/(J/rirV^ X/l/ >\/f ./ Page 2 (last page)


Servict Location


Received

14-DEC-95Complete

28-DEC-95Printed

28-DEC-95

Project L»b ID

A362676PO Nunber


13-DEC-95 15:00

Report To


Bill To


Staple DescriptionCLIENT ID: 95 12/13/95 IC1500DSWDESCRIPTION: WATERBLANKET ORDER RELEASE I: NOT RECEIVED WITH ORDERDESCRIPTION

& :'&Tiii ^Parameter

INITIAL WEIGHT OR VOLUMEResult

980Oet. Linit Units

mLmL

PCB AROCHLOR 1016rM ftlUJeHLOR^MZlPCB AROCHLOR 1232

Parameter

1242PCB AROCHLOR 1248MlROCHLOR 1254PCB AROCHLOR 1260

BDLBDLBDLBDL

Result Det. Linit0.0010

i (LQQ50:o.ooio'

Units

n»9/L

mg/L

PCB AROCHLOR 1268

0.016•BDLBDLBDLBDL

0.0010OiOOlO0.0010D.poio:o.obib m q L

1:10 dilution.1248 Is degraded.

CouMntsBDL Below Detection Limit



Additional copies of this report sent to:PUSS CEPKO. HESTINGHOUSE ELECTRIC CORPORATION


HERITAGE ENVIRONMENTAL SERVICES, INC. Sample ID: A362676 95 12/13/95 IC1500DSUCements


Approved : 7 ./( UJIIA yEUM /W ^ \ _ Page 2 (last page)


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14-DEC-95Complete

28-DEC-95Printed

28-DEC-95

Projtct Lab IDA362677

PO Nunber


13-DEC-95 15:00

Report To


Bill To


Sawple DescriptionCLIENT ID: 95 12/13/95 IC1500ESWDESCRIPTION: WATERBLANKET ORDER RELEASE #: NOT RECEIVED WITH ORDERDESCRIPTION

Parameter

INITIAL WEIGHT OR VOLUME'Result

870Det. Limit Units

mLiiiL;

PCB AROCHLOR 1016J*eB>lROCHLOR 12:21PCB AROCHLOR 1232IpCftxARpeHLOR 1242PCB AROCHLOR 1248PMJ1ROCMLOR 1254PCB AROCHLOR 1260PGBSAROCHLOR 1262PCB AROCHLOR 1268

BDLBDLBDLBDLBDLBDLBDLBDLBDL

o.oooio0.000100.00010

0.00010 mq/L

Saaple CaanentsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, HESTINGHOUSE ELECTRIC CORPORATIONII STANHIX STREET, PITTSBURG, PA 15222-1384



Service Location


Received

14-DEC-95Ccoplete

28-OEC-95Printed

28-DEC-95

Project Lab ID

A362672PO Nuaber


13-DEC-95 14:05

Report To


Bill To


Saaple DescriptionCLIENT ID: 95 12/13/95 SW1405SSWDESCRIPTION: WATERBLANKET ORDER RELEASE f : NOT RECEIVED WITH ORDERDESCRIPTION

ParameterINITIAL WEIGHT OR VOLUMEFINALS

1000Result Det. Llarit

mLUnits

PCB AROCHLOR 1016PCB AJmeHLORxtMlPCB AROCHLOR 1232

ParameterBDLmmBDLBtil

Result Det. Li*it0.00010

Units

PCB AROCHLOR 1248PCExftROel(tOl;ixl2S4PCB AROCHLOR 1260PCBSAraCrlLORil262PCB AROCHLOR 1268

BDLBDtBDLBDLBDL

0.00010xSOOMo.oooioX&QOQIQ;0.00010poooio0.00010

mg/Lm/mmq/L

Saapte ConsentsBDL Below Detection Limit



Additional copies of this report sent to:RUSS CEPKO, UESTIHGHOUSE ELECTRIC CORPORATION11 STANHIX STREET, PITTSBURG, PA 15222-1384

Approved : Page 1 (last page)<^

ENCLOSURE #4

NINE PERIPHERAL SPRINGS

SAMPLING RESULTS

Table 2 - Lemon Lane PeripheraJ Spring Sediment Sample Results

SpringStoney West

Stoney East

WN-1

WS-2

ICG-6

Snoddy

Bypass 37

Urban

Crestmont

Station12345

12345

12345

12345

12345

12345

12345

12345

12345

Sample #95 8/31/95 SW1 0905 SSD95 8/31/95 SW2 0900 SSD95 8/31/95 SW3 0845 SSD95 8/31/95 SW4 0830 SSD95 8/31/95 SW5 0825 SSD

95 8/31/95 SE1 1005 SSD95 8/31/95 SE2 0955 SSD95 8/31/95 SE3 0950 SSD95 8/31/95 SE4 0940 SSD95 8/31/95 SE5 0930 SSD

95 8/31/95 WN1 1135 SSD95 8/31/95 WN2 1130 SSD95 8/31/95 WN3 1 125 SSD95 8/31/95 WN4 1120 SSD95 8/31/95 WN5 11 15 SSD

95 8/31/95 WS1 1205 SSD95 8/31 /95WS2 1200 SSD95 8/31/95 WS3 1157 SSD95 8/31/95 WS4 1155 SSD958/31/95WS51150SSD

95 8/31/95 IG1 1335 SSD95 8/31/95 IG2 1330 SSD95 8/31/95 IG3 1325 SSD958/31/95IG41320SSD95 8/31/95 IG5 131 5 SSD

95 8/31/95 SN1 1420 SSD95 8/31/95 SN2 141 5 SSD95 8/31/95 SN3 1410 SSD95 8/31/95 SN4 1405 SSD95 8/31/95 SN5 1400 SSD

95 8/31/95 BY1 1510 SSD958/31/95BY21505SSD95 8/31/95 BY3 1500 SSD95 8/31 /95BY4 1455 SSD958/31/95BY51450SSD

95 8/31/95 UR1 1555 SSD95 8/31/95 UR2 1550 SSD958/31/95UR31545SSD95 8/31/95 UR4 1540 SSD95 8/31 /95UR5 1535 SSD

95 8/31/95 CR1 1630 SSD95 8/31/95 CR2 1625 SSD95 8/31/95 CR3 1620 SSD95 8/31/95 CR4 1615 SSD95 8/31/95 CR5 1610 SSD

Date08/31/9508/31/9508/31/9508/31/9508/31/95

08/31/9508/31/9508/31/9508/31/9508/31/95

08/31/9508/31/9508/31/9508/31/9508/31/95

08/31/9508/31/9508/31/9508/31/9508/31/95

08/31/9508/31/9508/31/9508/31/9508/31/95

08/31/9508/31/9508/31/9508/31/9508/31/95

08/31/9508/31/9508/31/9508/31/9508/31/95

08/31/9508/31/9508/31/9508/3t/9508/31/95

08/31/9508/31/9508/31/9508/31/9508/31/95

Time09:0509:0008:4508:3008:25

10:0509:5509:5009:4009:30

11:3511:3011:2511:2011:15

12:0512:0011:5711:5511:50

13:3513.3013:2513:2013:15

14:2014:1514:1014:0514:00

15:1015:0515:0014:5514:50

15:5515:5015:4515:4015:35

16:3016:2516:2016:1516:10

PCB(ppm)

BDL(UJ)BDL(UJ)

BDLBDL(UJ)

0.67(R), BDL(UJ)*

BDLBDL(UJ)BDL(UJ)BDL(UJ)

BDL

BDLBDLBDLBDLBDL

BDLBDLBDLBDLBDL

BDL(UJ)BDL(UJ)BDL(UJ)BDL(UJ)BDL(UJ)

BDLBDLBDLBDL

BDL(UJ)

BDL(UJ)BDL(UJ)BDL(UJ)BDL(UJ)BDL(UJ)

BDLBDLBDLBDLBDL

BDLBDLBDLBDLBDL

BDL - Below Detection Limit of 0.1 ppmLab mislabeled samples from ICG-6 spring, e.g. sample labeled "95 8/31/95 I62 1330 SSD"

in field log is labeled "95 8/31/95 IG2 1330 SSD" on the Certificate of Analysis.* Duplicate sample

02/08/96

Attachment 1: Validation of Sporadic Springs Data

1. The validation was performed per the requirements for level 4 data in the projectQAPjP. This includes a check for ; Holding Time, Calibration, Blank Contamination,Precision, Accuracy, and Accuracy of Nominal Reporting Limits against methodrequirements. All samples met method requirements with the following exceptions:

o The following samples should be flagged "UJ" as estimatesbecause of low surrogate recovery (note UJ is for the BDLsamples, if the result is above detection, then flag with a "J"):

8/31/95 BY4 14558/31/95 BY3 15008/31/95 BY2 15058/31/95 BY1 15108/31/95 IG1 13358/31/95 IG2 13308/31/95 IG3 13258/31/95 IG4 13208/31/95 SN5 14008/31/95 SW4 08258/31/95 SW2 09008/31/95 SW1 09058/31/95 SE4 09408/31/95 SE3 09508/31/95 SE2 0955

o The following samples should be flagged with a "UJ" becauseof low recovery of a matrix spike compound:

8/31/95 BY5 14158/31/95 IG5 1315

o The following samples should be flagged "R" as unusablebecause of baseline irregularities:

8/31/95 SW5 0825 (original prep and analysis) this samplewas reanalyzed and reported as BDL, the reanalysis did notmeet hold times and should be flagged as a "UJ")


o Precision and accuracy: The precision requirements as measured byduplicate spiked samples have been met. The accuracy requirements forsome of these samples is called into question because of low surrogaterecovery. The lab routinely only spikes one surrogate into sedimentsiunples. In some of the samples, the recovery of the surrogate (TCMX)was below QC limits. This indicates some matrix suppression of thesurrogate. For most sample batches the recovery of the matrix spikecompound (Aroclor 1260) was adequate except for 2 batches where it wasjust slightly low. The lab should begin using 2 surrogates for solid matrices.Data with low surrogate recovery has been flagged as estimates and is not

rejected since the matrix spike compound was usually within recoverylimits.

o Representativeness: The representativeness requirement involves anassessment of the field sampling and lab analytical techniques. The fieldsampling locations and all lab techniques were in accordance with theapproved sampling plan and are considered adequate.

o Completeness: The completeness goal for the project was for all projectdata to be 90% accepted. Completeness is calculated by dividing the totalnumber of acceptable analyses by the total performed. An acceptableanalyses is defined as one that conformed to QC protocols and is notrejected.

The project completeness is most correctly applied to all project data andcan only be calculated at the completion of the total project. Looking at thecompleteness of this event only, there was only one analysis with rejecteddata. Therefore the completeness goal was satisfied even if viewed on anevent basis.

o Comparability: The comparability of this data is not evaluated since alldata was taken by the same techniques and analyzed by the same lab.

The main objective of the sampling event was to determine the presence of PCBs in thespring sediments. While there was some surrogate matrix suppression, the matrix spikecompound has the more closely matched sorption characteristics to the real contaminants.Since the recovery of the matrix spike compound was for the most part adequate, the

data quality is sufficient to meet project goals. It is recommended that the lab begin usingtwo surrogates for solid matrix extractions.

ENCLOSURE #5

FALL STORM EVENT

SAMPLE RESULTS

October 1995 Storm EventSediment Sampling at 6 Connected Springs

SpringSlaughterhouse Sp.Packinghouse CulvertPackinghouse RoadICG-1Quarry Sp.Illinois Central Sp.

Date10/23/9510/23/9510/23/9510/23/9510/23/9510/23/95

Time17:3017:5017:5518:0518:1518:30

Sample #95 1 0/23/95 SL 1730SSD95 10/23/95 PC 1750SSD95 10/23/95 PR 1 755 SSD9510/23/9511 1805 SSD95 1 0/23/95 QU 181 5 SSD95 10/23/95 1C 1830 SSD

PCB(ppm)*1.66(J)BDL(J)0.28(J)

1.562500

*PCB results are dry weight corrected.

02/16/96

Illinois Central Spring - October 1995 Storm Event - Composite Samples

Hrs aftertimeO

0123456789

1011121314151617181920

Date10/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/95

Time00:0001:0002:0003:0004:0005:0006:0007:0008:0009:0010:0011:0012.0013:0014:0015:0016:0017:00

L 18:0019:0020:00

TotalFlow(gpm)

25252525274986 11171341229977645851463340373232

Comp.PCB(Ppb)

1818182018161718181514141214141214

Dupl.PCB(PPb)

16

13

BlankPCB(PPb)

BDL

TSS(mg/L)

5BDLBDLBDLBDL

2BDL

3BDL2

BDLBDLBDL

2BDL

2BDL

DuplicateTSS

(mg/L)

BDL

BDL

Field blankTSS

(mg/L)

2

Cond(uS/cm)688.7688.8688.5688.4688.0685.9684.5686.6696.5687.6686.8686.8680.7675.3673.2674.4676.8679.1680.9681.5680.9

Temp(deg C)13.4013.3913.3913.3813.3813.3713.4013.3713.3413.3313.3313.3413.3513.3613.3713.3813.3713.3713.3713.3713.37

SL CumRain aftertime zero

00.010.030.220.470.520.520.520.520.520.520.520.520.530.530.530.530.530.530.530.53

End of composite sampling. After this time all samples were grab.

02716/96

Illinois Central Spring - Oct. 1995 Storm Event - Grab Samples

HoursAfter

TimeO0

0.250.5

0.751

1.251.5

1.752

2.252.5

2.7534567

7.258

8.59

9.259.5

9.7510

10.2510.5

10.75111213141516171819202122232425262728293031323334353637383940

Date10/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/951 0/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/95

Time00:0000:1500:3000:4501:0001:1501:3001:4502:0002:1502:3002:4503:0004:0005:0006:0007:0007:1008:0008:3509:0009:1509:3009:4510:0010:1510:3010:4511:0012:0013:0014:0015:0016:0017:0018:0019:0020:0021:0022:0023:0000:0001:0002:0003:0004:0005:0006:0007:0008:0009:0010:0011:0012:0013:0014:0015:0016:00

TotalFlow

(gpm)25

25

25

25274986117

134

122

99

776458514633403732323029272523242323212120211920212424242424

PCB(ppb)

16

19141214152217181312141121241819

21.616181512

16131715181718141512151516162525

27(J)

Dupl.PCB(ppb)

12

12

14

BlankPCB(ppb)

BDL

TSS(mg/L)

2

2BDLBDLBDLBDL

2BDLBDLBDLBDLBDL

2BDL

22

BDLBDLBDLBDLBDL

2

BDL

BDLBDLBDL

3BDLBDL

3BDLBDLBDLBDL

2BDLBDL

Dupl.TSS

(mg/L)

BDL

2

BDL

BlankTSS

(mg/L)

BDL

Cond.(uS/cm)688.7

688.8

688.5

688.4688.0685.9684.5686.6

696.5

687.6

686.8

686.8680.7675.3673.2674.4676.8679.1680.9681.5680.9679.2677.2674.8672.1668.4662.2653.0642.6631.1618.4607.3597.2589.0580.1569.5552.6532.8513.3495.9482.4

Temp(deg C)13.40

13.39

13.39

13.3813.3813.3713.4013.37

13.3«r

13.33

13.33

13.3413.3513.3613.3713.3813.3713.""13.13.3713.3713.3713.3713.3713.3713.3713.3813.3813.3813.3813.3813.3813.3813.3913.3913.3913.4013.4013.4013.4113.41

Pagel 02/16/96

Illinois Central Spring - Oct. 1995 Storm Event - Grab Samples

HoursAfter

TimeO4142434445464748495051525354555657585960616263646566676869707172737475

K 7677787980818283848586878889909192

Date1 0/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/95

L1 0/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/29/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/9510/30/95

Time17:0018:0019:0020:0021:0022:0023:0000:0001:0002:0003:0004:0005:0006:0007:0008:0009:0010:0011:0012:0013:0014:0015:0016:0017:0018:0019:0020:0021:0022:0023:0000:0001:0002:0003:0004:0005:0006:0007:0008:0009:0010:0011:0012:0013:0014:0015:0016:0017:0018:0019:0020:00

TotalFlow

(gpm)24242323212019201817181715151313141313151515151415151412131313131313131313141215101010121211121111121211

PCB(ppb)14(J)2424252115181714171719

19

16

12

14

17

16

Dupl.PCB(ppb)24(J)

0.37*

BlankPCB(ppb)BDL

14*

TSS(mg/L)BDL

3BDLBDLBDLBDLBDLBDLBDLBDLBDL jBDL

Dupl.TSS

(mg/L)BDL

BDL

BlankTSS

(mg/L)BDL

Cond.(uS/cm)469.2456.8449.1443.8441.5442.7446.4454.0463.3472.2481.4489.8499.0508.0516.9525.3533.4540.8548.7556.5563.8570.9576.9582.8588.8594.0598.7603.4607.7611.4615.5619.3622.3626.0628.7631.8634.6637.3639.8642.2644.5647.0649.3651.2652.8654.6656.1657.1657.5657.5656.3654.4

Temp(deg C)13.4113.4213.4213.4313.4313.4413.4413.4513.4513.4613.4613.4613.4713.4713.4713.4713.4713.4713.4813.5113.5213.5113.5113.4913.4813.4813.4813.4813.4813.4813.4713.4713.4713.4713.4713.4713.4713.4713.4713.4613.4613.4713.4713.4613.4613.4613.4613.4613.4613.4613.4513.45

Lab error resulted in PCB results for duplicate and blank samples being switched.

October storm event samples were taken at the emergence. May storm event samples were taken at the mouth of the culvert.Two sets of samples were taken at the culvert to test comparability of Oct. storm event results with May storm event results.

38.5

10/27/9510/27/95

03:0008:30

1211

1813 BDL

3BDL

2BDL

Page 2 02/16/96

Slaughterhouse Spring, October 1995 Storm EventHoursAfter

TimeO01A

2.25

2.52.75

24

4.254.5

4.75

55.25

5.55.75

6789

101112131415161718192021222324252627282930313233343536

Date1 9/2 //9b

10/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/27/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/9510/28/95

Time00:0001:0002:0002:1502:3002:4503:0004:0004:1504:3004:4505:0005:1505:3005:4506:0007:0008:0009:0010:0011:0012:0013:0014:0015:0016:0017:0018:0019:0020:0021:0022:0023:0000:0001:0002:0003:0004:0005:0006:0007:0008:0009:0010.0011:0012:00

Cum rainafter timezero (in)

u0.01

0.03

0.220.47

0.52

0.52

0.52

0.520.520.520.52

0.520.530.53

0.53

0.530.53

0.53

0.53

0.53

0.530.530.53

0.53

0.530.53

0.53

0.53

0.53

0.530.54

0.56

0.560.570.57

0.6

TotalFlow(gpm)

IB

18

16

1846

76

62483935323432302822252523222220201919171716161716151515141515

Comp.PCB(ppb)

1.34

0.53

0.3KJ)0.33(J)0.16(JJ_0.2(J)0.250.25

0.21(40.2(J)0.17(J)0.22(J)0.15(J)

BDL0.23

BDL

GrabPCB(ppb)

BOL(UJ)0.31

BDL(UJ)BDL(UJ)BDL(UJ)BDL(UJ)BOL(UJ)BDL(UJ)

BDL(UJ)BDL1UJ)BDL(UJ)

0.12BDL(UJ)BDL(UJ)BOL(UJ)BOL(UJ)BDL(UJ)BDL(UJ)BDL(UJ)BDL(UJ)BDL(UJ)BDL(UJ)

BDL(UJ)

BDL(UJ)

Dup. GraPCB(ppb)

BDL(UJ)

BDL(UJ)

BlankPCB(ppb)

BOL

BDL

BDL

Comp.TSS

(mg/L)

240

89594032293031362230311202323

GrabTSS

(mg/L)

201701309676716155

4337464537246133492425212425

20

19

Dupl.TSS

(mg/L)

42

23

BlankTSS

(mg/L)

BDL

Cond.(uS/cm)

755.7758.7759.5766.1764.0759.0762.8771.3779.9785.3780.6724.3776.6763.1756.0769.1775.1790.4787.1786.6784.8784.0784.7784.8782.6787.0764.9754.0759.9758.8754.3748.4742.3754.9741.6735.1733.6737.2739.9740.8733.9744.5741 3739.0743.7735.6

Temp(degC)13.b313.6913.7613.7813.8414.1814.2214.3414.4814.4814.3014.2814.5314.9015.2115.2315.1214.9:14.65^14.4614.3514.2914.2114.1314.0613.9413.8813.9013.8113.7713.6913.5613.5413.6013.6113.5813.6913.8913.8313.7P13.5113.4213.2813.1513.0913.04

02/16/96

Attachment 1: Validation of Fall Storm Event Data

1. The validation was performed per the requirements for level 4 data in the projectQAPjP. This includes a check for ; Holding Time, Calibration, Blank Contamination,Precision, Accuracy, and Accuracy of Nominal Reporting Limits against methodrequirements. All samples met method requirements with the following exceptions:

o Illinois Central grab samples taken on 10/28/95 at 1600 and1700 did not have surrogates added to them. They have beenflagged "j" as estimates.

o Some of the sample extract for the duplicate grab sampletaken from Illinois Central at 10/28/95 1700 was lost duringconcentration. This may make the reported value low and itis flagged "j" as an estimate.

o The Illinois Central grab sample for 10/27/95 taken at 1600mistakingly had a spiking solution of Aroclor 1260 added to it.The lab has acknowledged this error in the case narrative.

Therefore the reported values for Aroclor 1260 and 1262 areflagged "R" as unusable. The summary table shows only thetotal PCBs based on the other Aroclors present in the sample.The certificate of analysis still shows the Aroclor 1260 and1262 values.

o The following composite samples taken from SlaughterhouseSpring were near the limit of detection and althoughquantitated, the extract concentration was below the provenlinear range of the instrument. These are flagged "j" asestimates.

10/27/95 SL 060010/27/95 SL 070010/27/95 SL 080010/27/95 SL 090010/27/95 SL 120010/27/95 SL 130010/27/95 SL 140010/27/95 SL 150010/27/95 SL 1600

o Most of the Slaughterhouse Spring grab samples were foundto be below the limit of detection. The detection limit studywas based on a 1 liter extraction from water. The grabsamples from Slaughterhouse spring were taken in a 1 literbottle. The lab separated 200 ml out for TSS analysis. Thus,a typical extraction volume was 700 ml. This will change theactual detection limits. Due to variances in actual extractionvolumes and slight variations in instrument sensitivities, allthe Slaughterhouse grab samples that were below detectionare flagged "UJ" as estimates.

o The following sediment samples had low surrogate recoveryand are flagged "J" as estimates:

10/23/95 SL 173010/23/95 PC 175010/23/95 PR 1755


o Precision and accuracy: The precision and accuracy requirements asmeasured by lab spiked samples have been met. The precision between fieldduplicates was adequate.

o Representativeness: The representativeness requirement involves anassessment of the field sampling and lab analytical techniques. The Heldsampling locations and techniques were in accordance with the approvedsampling plan. The sampling location at Illinois Central Spring waschanged to be closer to the emergence relative to the spring storm event.This was done to eliminate the possibility of surface influx at the samplelocation. Some duplicate samples were taken at the previous sampling point(the culvert entrance) at Illinois Central during the event so thatcomparisons may be made between results from the past and presentlocations. The agreement between locations was excellent. This was to beexpected since this storm did not generate any surface inflow.

During storm sampling events, two types of samples are taken. The hourlycomposite sample was taken with a continuous sampling pump by filling agallon jug over the span of an entire hour. The grab sample was taken witha sampling pump into a 1 liter bottle over the span of about 15- 30 seconds.

At Illinois Central Spring, a comparison of the TSS and PCB results for thegrab versus composites taken in the same time frames shows no significantdifference between the samples. This is contrary to the trend observed atthis spring during previous storm sampling where the grab samples hadconsistently higher PCB levels. In the past the higher grab samples wereattributed to higher sampling flows that more closely represented in streamwater velocities. This caused more suspended material to be in the grabsamples and resulted in higher PCB levels.

During this event the stream flows did not reach levels where sedimentswere suspended. In this case, the majority of the PCBs are likely dissolvedand not impacted by sampling device flow rates.

At Slaughterhouse Spring, there is a difference in that most of the grabsamples were reported as BDL while the composites taken during the sametime period were generally just above the detection limit. An inspection ofthe raw data package was conducted to determine the cause of thisdifferential. The conclusions from this review are that the grab samples hadless volume extracted and were processed on a GC instrument that wasslightly less sensitive than the instrument used on the composite samples.While normally such minor variations will not effect results, with samplesvery near the detection limit, these variations can make the difference.

o Completeness: The completeness goal for the project was for all projectdata to be 90% accepted. Completeness is calculated by dividing the totalnumber of acceptable analyses by the total performed. An acceptableanalyses is defined as one that conformed to QC protocols and is notrejected.

The project completeness is most correctly applied to all project data andcan only be calculated at the completion of the total project. Looking at thecompleteness of this event only, there was only one analysis with rejecteddata. Therefore the completeness goal was satisfied even if viewed on anevent basis.

o Comparability: The comparability of this data is not evaluated since alldata was taken by the same techniques and analyzed by the same lab.

The main objective of the sampling event was to determine the PCB concentration withrespect to flows during a fall storm response. Even though some of the data is qualifiedas estimates, the data is still useful towards this end. The sampling period for bothsprings was of sufficient length to cover the entire storm response and overall the data isjudged to be of sufficient quality to meet the project goal.

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