U.S. POLYMERIC
Transcript of U.S. POLYMERIC
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U.S. POLYMERIC
HITCO MATERIALS DIVISION
([_ASA-CL_-179_I17) FXliC-EEi_'5.Xl_'J. 'XES_ CATA[_,_,(Jb'l.: }H 5E3q LC2 tiC,. 2 ([]5CC) 1_3 F
CSC L 1 IB
G3/27
_189- 13_. 0,_
FM 5834 LOT #2
D-09275
FINGERPRINT TEST DATA REPORT
NAS8-36298 COPY # 9
Page 1 of 2
FILLER TESTING
NAS8-36298
U.S. POLYMERIC O.E. 71108
F iller _05 for NASA _ot#
I. Carbon Content, Z
QAI-5560_AMP_E
*2A-i *2*-2 .2A-399.31 99.18 99.40
NASA LOT# 2 AVERAGE 99.30
2. Ash Content, XPTM-71B
0.0 0.0 0.0
0.0 o.e 0.0AVG. 0. • 0. • 0. •
NASA LOT# 2 AVERAGE 0.0
3. Atomic Absorption, ppm
CTM-53B
(Values are average of2 determinations)
#2A-I #2A-2 #2A-3 LOT#2
__ AVG.Na 7.0 7.5 9.0 7.8
K 1.5 1.0 2.5 1.7
Ca 2.5 1.5 2.0 2.0
MO 0.0 0.0 0.0 0.0Li 0.0 0.0 0.0 0.0
TOTAL 11. • 10. • 13.5 11.5
3a. Moisture Content, XCTM-53B
.041 .034 .039
AVG. .036 .027 .042
NASA LOT# 2 AVERAGE .035
3b. Ash Content, X
CTM-53B
0.005 0.000 0.015
0.000 0.025 0.000AVG. 0.003 0.013 0.008
NASA LOT# 2 AVERAGE 0.008
4. pH, Units
ASTM D1512
4.60 4.40 4.50
AVG. 4.60 4.50 4.60
NASA LOT# 2 AVERAGE 4.57
5. Particle Size, microns
S.E.M. procedure
(Average values areof 20 determinations)
AVG. .56 .57 .52
Maximum .90 1.25 1.17
Minimum .23 .20 .25
Std. Dev .22 .28 .24
NASA LOT# 2 AVERAGE SIZE .55
6a. TGA, *C at 50% Loss
CTM-51
842 850 857
NASA LOT# 2 AVERAGE 850
HITCO MATERIALS DIVISION
700 E. DYER ROAD, SANTA ANA, CALIFORNIA92707 * (714) 549-1101 * TWX (910) 505-1130 * FAX # (714) 549-2858-5-2437
Page 2 of 2
Filler Lot _or NASA Lot# 2
6b. TGA
CTM-51
See Charts 6A-6C
7. Particle Size Distribution
CTM-72See Charts 7A-7C
7a. Partlcle Size, micronsCTM-72
2A£_ _ #2A-3.86 .97 .95
.e5 _ .92AVG. .86 1.02 .94
NASA LOT# 2 AVERAGE .94
U.S. Polymeric
Hmmld M. Qurmlshl, Mmnager
Ouallty Assurance Department
J CHART 5A
ORIGINAL PAGE I$
OF POOR QUALITY
!
r!i
/
ORIGINAE P A"G-_.
OF POOR QUA.L,I'I-_,
CHART 6B
J
OP_C..NAL PAGE ._
Oi\ POOR (_UALI'I'Z,
CHART 6C
I
T
OB .POOR QuALi,r,r
"- _ _ _ _ _ ,..; _ ...;
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CHART 7A
V *
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Z
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r.._ _,0_ _ _ "-
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41,
ORIGINAL PAGE 1_
OE POOR QUALITY
ORIGINAL PAGE IS
OF POOl{ QUALITY.
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CHART 7C
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6
2.
3.
4.
5.
6.
7.
8.
9.
10.
II.
12.
13.
14.
15.
TABLE OF CONTENTS
RESIN TESTING
NAS8-36298
U.S. Polymeric O.E. 71108
91LD Resin Lot for NASA Lot# 2
PAGE
Resin Solids ...................................... I
Specific Gravity .................................. 1
Brook_ield Viscosity .............................. I
Gel Time .......................................... 1
Atomic Absorption ................................. 1
Gas Chromatography ................................ I
TGA ............................................... 1
DSC ............................................... 1
HPLC .............................................. 1
GPC ............................................... I
pH ................................................ 2
Phenol Content .................................... 2
Chang's Index ..................................... 2
RDS ............................................... 2
NMR ............................................... 2
CHARTS
Gas Chromatography .................................. 6A - 6C
TGA ................................................. 7A - 7C
DSC ................................................. 8A - 8C
HPLC ................................................ 9A - 9C
GPC ................................................. 10A - 10C
RDS ................................................. 14A - 14C
NMR ................................................. 15A - 15C
RESIN TESTING
NAS8-36298
Page 1 of 2
U.S. Polymeric O.E. 71108
I. Resin Solids, X
PTM-7C
91LD Resin Lot for NASA Lo_# 2
AVG.
#2-1 #2-___22 #2-370.8 70.4 71.7
70.8 70.2 71.2
7 1 ._..._9 72 ._.___00 7 • ._.__.5571.2 70.9 71.1
Lot# 2 AVERAGE 71.1
2. Specific Grsvlty @ 25-C
PTM-29C
1.141 1.140 1.139
Lot# 2 AVERAGE 1.140
3. Viscosity, Brookfleld, cps. @ 22.8°CPTM-14C
1250 1250 1500
Lot# 2 AVERAGE 1333
4. Gel Time, mln:sec
PTM-47B
3:30 3:38 3:34
Lot# 2 AVERAGE 3:34
5. Atomic Absorption, ppmCTM-53B
Ca
Mg
LIAVG.
Ns 4
K •
3
I
08
#2-2 #2-3 LOT1 AVG
4 8 5.3
• • 0.02 2 2.3
1 1 1.0
_ 0.__338 11 9.0
6. Volmtlles, Gas ChromatogrsphyCTM-55
See Charts 6A-6C
7. TGA, X Weight Loss st 500"CCTM-51 (AIR)
#2-1 #2-2 #2-3
39.5 40.1 39.4
Lot# 2 AVERAGE 39.7
See Chart 7A-7C
8. DSC, temperature "C
CTM-50A
183 191 183
Lot# 2 AVERAGE 186
See Chart 8A-8C
9. HPLC
CTM-49A
See Chart 9A-9C
10. GPC, Average molecular wt.CTM-49A
1718 1801 1598
Lot# 2 AVERAGE 1706
See Chart 10A-10C
(_ HITCO MATERIALS DIVISION700 E DYER ROAD, SANTA ANA. CALIFORNIA92707 • (714) 54_1101 = TW_ (910) 59_1130 . FAX # (714) 54_285_2437
Page 2 o£ 2
91LD Resln Lot £or NASA _otl 2
11. pH, units
CTM-1B#2-1 #2-2 #2-38.5 8.3 8.4
Lot# 2 AVERAGE 8.4
12. Phenol Content,
CTM-55 Appendix I
AVG.
1o. o4 11.09 _1.74Ao. so ll. e8
9.94 10.94 11.81
Lot# 2 AVERAGE 10.90
13. Chang's Index, ml.
CTM-5B
24.2 24.8 25.2
Lot# 2 AVERAGE 24.7
14. RDS, Minimum Viscosity, cps.CTM-57A
Mln, Visc. "C#2-1 278 107
#2-2 249 111
#2-3 239 113AVG. 255 110
See ChRrts 14A-14C
15. NMR
Vendor procedure
See Charts 15A-15C
U. S. Polymeric
Hmmid M. Quraishl, Manager
Quality Assurance Department
ORIGINAL PAGE 1_
OF POOP, QU,kLITY
TYPICAL GAS CHROMATOGRAPH SET-UP
ColumnLength 6"_,
Dia._Liquid _ase_It. S _._
|upport_
Carrier Gas -IJ-,tP_
htemeter
Inlet Prss___llPSi |Irate /Din
CflARTSPE_D....s_za[_Siz,_
hieDetector "FT_
Vo I taleSensi t. ,,
Flow Itateso.,pl/mi n_tlydro|en _ Ai r_$cavln|!
Split
Tmper_u rej, el;
Det. _ I_Column InitialFinal ,.2/Q I,.te_ I
Solvent ,'/__J_'... , _ J
conch..(z.,.J__.._._./_
GAS CHROMATOGRAPHY STANDARD SOLVENT
TEST METHOD CTM-55
STANDARD SOLVENT/MONOMER RETENTION TIME (MINS.)
MEOH .6
ETHANOL i,18
MECL2 1.28
ACETONE i.45
IPA 1,83
THF 3.O8
ACETONITRILE 3.2
CRESOL 4.O3
MEK 4,O8
FURFURAL 15,03
TOLUENE 17.98
CHLOROBENZENE 19,6
PHENOL 22,08
NOTE: THF WAS USED TO DILUTE THE RESIN SAMPLES.
ORI'G.rN'AL F'AGE KS
OF POOR QUALITM
•-%:_ REAL TIME CHROMRTOGRH_I :I.i.%
F--
f
f ---_
L
L ", \L
._..IN_L FULL SCALE MV =1008.08
SAMPLE' _I LD 2-1diS:C: C=011017E, 1Gt_._/ML
TIME II :49")RTE 12"I E_,E:6]F'ERATOR : .JGZ
RUN TIME:)ELAY TIME'":H At..I: 0
38.00 MINUTES13.00
_'I:: RET PEAK AREA E: _EAK'10. TIME AREA _. L HT.
2 ._5 17_95 1.70 204140 9
SIC5 2010908 B47 _ _= 1_37
39 22 05 162080 6
T OTFIL FIREB= 2:3E:26_ 1"tHRESHOLD= 1MI_q F't:: WIDTH= 15_I;'EA REJECT= 10E,0
075 2' 2355_ 2 11953397 3 84306,065 4 127093 2 96802 1 a700
UEFFTICRL SCALE
CHART 6A
F_CTOF'- 1Y
5_
6_
• I
19_
p
c-
SAMPLE: 91 LD 2-I
M Isc. : c=o. Ie_7_;1et$/l_.
TIME: 11:49DATE: 12/10/88OPERATOR: JGZ
_LIN TIME: 30.00DELAY TIME' 0.00CHAN: 0
MIHUTES
FK RET PERK RRER BNO. TIME AREA _ L
PEFII..HT.
5 1.70 204140 e.seE;6 3.05 2010908 04.594
39 22.05 162080 6.s18
TOTAL AREA= 2377120THRESHOLD= 1MIH PI::.WIDTH= 15RRER REJECT= 2300
2 I195S3 843061 $700
;)RIGiNAL FACE -c
OF. POOR QUM.ITY
Fr
PEFiL
I
r
I-
L__,
LL
L \L\
FINAL FULL
T I ME CH_TAMATO_.3RF.tM ,f::_;f:
SCALE M',.'.=IO0O O_
""_E,RMF'LE:
MISC:_1 LD 2 _-
"q JC=O. 101 _,-_IIg/ML
TIME I,::1.DATE 1.':--'.."10./8 t-OPERFIT "IR : .IG."
_.:I.tt4TIFIE: 30.00DELAY TIME: 0.00C.HRt4: 0
M I t,tLtT ES
PK PET PEAK AREA BNO T IME AF:ER % L
PEAKHT.
24 15 16 27 38 59 6
10 61E: 112.5 le_34 71.7,5 22
.6E: 1634
.43 185470 135890
.93 119280095 41333_,.., _E:..2_7 942558 939875 1060145 119498 10446015 197270
095108
7 93969 685
2 415342551549619070
6 1_7II 525
TOTAL R_:ER= 171171_TH_'ESHOLD= IHIN P_. NIDTM= 15_RE_ REJECT= I_00
3 14_o 2072 101813 72100
,_4 .E ....4 3544 2494 189I 5472 39_ 100153 9916
CHART 6B
VERTICAL SCALE
6_7 "--
10_
18_
25_
FFICTOR : I"g,
I
L
(
SAMPLE : -_J LD ."-',.MISC. • C:O. 101.',-_/HL
TIME: 16: I.-DATE" 1"=',."IA.."E;_._OF'EPRTOR : JGZ
RUH TIME: 30.00DELAY TIME: O.OOC:HAN: 0
M INUTE$
Pt( RET F'EAK AREA E:NO TIME AREA % L
PEAKHT.
=,., 1 . 7EI 135890 8 . 1,-?_5-', l'_"°c'c_ 71 350
7 3.95 41333 _ 47234 21.98 104460 _.,249
-_ 97 .35 2z.15 I 270 11 80_
IOTPL AREA= I¢71753THRESHOLD= IMIN.PK.WIDTH= 15AREA REJECT= 11000
'2 161E:13 721004 5852 10015
Q_I6
_.I_l: REAL TIME CHPOMATO_PAfq
ORIGINAL PAGE
OF POOR. QUALITy
VEFIT ICAL
CHART 6C
SCALE FHCTOR: 1X
wm •
L ,
FINAL FULL SCALE M)..) =1000.0(_
_,_h,-."._ " _1 LD 2'-_,r,11S F. C= 0. 1012 _, _;4_;/Ml.
TIME 16:5-_DATE 12.'10.-86,7PEg'ATO_: : .IGZ
_:UH TIME: 30.00DELAY TIME? O.O0f'.HAN : 0
M INUTES
F'}.i RET PEAK AREA E:N.A TI ME AREA :. L
PERKHT.
2'4 15 1
7 38 59 6
lC: 1 !_S "22
40 22
_ 420445 1258_ 81270 283 196320 528 2E;99700 8460 2293O_ 146483 614003 54263 115 165300 4
TOTALTHF'E$MI_R F_PEA
AREA= 3412211H i"lL D= 1t::. 1,_]DTH= lgRE JEC:T= 1000
12'3 3 435037 2 I"_.382 2 I14_5753 2 11447980 3 85372067 4 251043 4 69180 3 248590 2 9873844 3 9807
gAMFLE: 91 LD 2-3MISC. C=0.10126_M_/NL
TIME: 1_:58DATE: :2.."10.-.'8_OF'EF:RTOP: JGZ
RUN TIME: 30.00DELAY TIME: 0.O0CHAH- 0
MINUTES
PK RET PEAl:: AREA E:NO. TIME RPER % L
5 1._8 _1270 2.393 2g 1.83 196320 5.779 27 3.28 2899700 B5.364
39 22.03 54263 1.597 240 22.15 165300 4.86_ 3
TOTAL AREA= 3396853THPESHOLD= IMIN.PI_ WI[,TH= 15AREA REJECT= 6200
PEAt:.HT.
I14_5114478537298739807
)
_,._ CHART 7B
ORIGINAL I'I_GE IS
OF POOR QUALIT_ . . t::)
QC _l.LIj ',,e" ¢0ZCf) COLI.I,-',I"- '_LD r'l ,,_ COW QIN
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.... C:) C:)
CHART 7C
.... OR/_I'NAL +PTTGE 1FSCHART 8B
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CHART 9A
_" A FILE A:PHENO39. HDR TAKEN 09-05-1986 16:56:50
--******** AREA PERCENT REF'ORT
_, ****************************************************************************
Sample Name: 91LD,2-1,C=6.85 Operator Initials: OGZ *
hate: 09-05-1986 16:56:50 Method:F'HENOLIC DATA FILE: A:PHENO39. PTS *
nterface: 4 Cycle#: 39 Channel#: 0 Vial#: N.A. *
• _tarting Peak Width: 10 Threshold: .01 ********************************************************************************
Instrument Type: BECKMAN HF'LC Column Type: MICROBONDAF'AK C-IB *
Solvent Description: THF/WATER, 2:1 BY WEIGHT *
Operating Conditions: R.T., FLOWRATE=I.5 ML/MIN *• Detector O: 220NM/.5AU Detector 1: *
Misc. Information: LENGTH=25 *
*******************************************************************************
Starting Delay: 0.00 Ending Retention Time: 10.00
:'_ Ret Peak Area B Peak Normal iz ed Area/
Wo. Ti me Area % L Ht. % Hei ght
1.78 120482 75.1672 2 5050 100.000 2_c.9
4 2.05 39804 24.8328 2 4045 33.037 9.8
Tc al Area: 160286 Area Reject: 10C)0 One sample per 1.000 sec.
t_
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FILE A:F'HENO38.HDR TAKEN 09-05-1986 16:40:05
CHART 9B
******** AREA PERCENT REPORT ********
Starting Delay:
P; Ret
No. T i me
_ ****************************************************************************
_ample Name: 91LD,2-2,C=6.77 Operator Initials: JGZ *Date: 09-05-198616:40:05 Method:PHENOLIC DATA FILE: A:PHENO38.FTS *
nterface: 4 Cycle#: 38 Channel#: 0 Vial#: N.A. *
tarting F'eak Width: 10 Threshold: .01 *
Instrument Type: BECKMAN HF'LC Column Type: MICROBONDAFAK C-18 *
Solvent Description: THF/WATER, 2:1 BY WEIGHT *
Operating Conditions: R.T., FLOWRATE=I.5 ML/MIN *
Detector O: 220NM/.5AU Detector 1: *
Misc. Information: LENGTH=25 *
*****************************************************************************
0.00 Ending Retention Time: 10.00
Peak Area B Peak Normalized Area/
Area % L Ht. % Height
1.7B 121012 74.99642 5109 10D.000 2,.73
4 2.05 40345 25.00362 4092 33.340 9.9
___.al Area: 161357 Area RejeEt: 1000 One sample per 1.0()0 sec.
X
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Z
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Q_
ORIGIN'AL PAGE IS
OF POOR QUALITY
CHART 9C
-r r 67 opening raw data file A:LASTRUN.PTS53 creating file A:PHENO40.F'TS at line 4620
.,_ FILE A:PHENO37.HDR TAKEN 09-05-1986 16: 04:07
•_ ******* AREA F'ERCENT REF'DRT ********
_mple Name: 91LD,2-3,C=6.79 Operator Initials: 3GZ *I _te: 09-05-1986 16:04:07 Method:PHENOLIC DATA FILE: A:PHENO37.PTS *
Interface: 4 Cycle#: 37 Channel#: 0 Vial#: N.A. *
Ftarting Pea_:: Width: 10 Threshold: .01 *.. ****************************************************************************
_nstrument Type: BECKMAN HPLC Column Type: MICROBONDAFAK C-1B *
Solvent Description: THF/WATER, 2:1 BY WEIGHT *
Operating Conditions: R.T., FLDWRATE=I.5 ML/MIN *
Detector 0: 220NM/.5AU Detector 1: *
Misc. Information: LENGTH=25 *
. ****************************************************************************
;t _ting Delay: 0.00 Ending Retention Time: 10.00
:'k Ret Peak Area B Peak Normal ized Area/
_o Time Area % L Hr. % Height
1.78 121706 75.2396 2 5098 IC)0.0[)0 23.9
2.05 40052 24.7604 2 4076 32.909 9.8
F_tal Area: 161758 Area Reject: 1000 One sample per 1.C)00 sec.
t,.
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oRIGD{_J_ P.AGg lg
OF EOOR Q_:AI,ITY
I
GPC CALIBRATION PLOT
*** Calibration Data ***
Calibration Name:
Mist Information:
Fit Type: 3
Lo9 Mo] Wt = A + B× + Cx^2 + D×'_3
Az 2.538977 B= 2.115815 C= -.5646824
Coefficient of Determination: 0.9902
Ret Time Molecular Weight
o
D= 3.606432E-02
Log Mol Wt
3.50 35000
4.33 15000
4.B3 3600
5.09 2350
6. O0 570
7. 17 92
7.50 72
Log Mol Wt GPCC_I,IBR_TIONPLOT
185
418
318
218
m
4.544
4.176
3.556
3.371
2.756
1.964
I.$57
m
m
I
D
m
I I I I I1
18 2.8 3.8 4.! 5.8 6.9Jleiention Time or Vol-,e
?.8
m
m
m
m
ORIGINAL PAGE IS
OF POOR QUALITY CHART 10A
" A FILE B:GF'C28 .HDR TAKEN ()8-C)5-1986 17:13:56
* Sample Name: 91LD 2-1 =2.68 Operator Initials: GBF *
* 9ate: 08-05-1986 14:C)5:42 Method: DATA FILE: B:GPC28 .F'_S *
* interface: 5 Cycle#: 28 Channel#: 0 Vial#: N.A. *
* _tarting Peak Width: 60 Threshold: 0 *********************************************************************************
* Instrument Type: HF'LCIBECKMAN Column Type: UL_RASTYF:AGEL 500A
* Solvent Description: THF *
* Operating Conditions: T=35C FLOWRATE=2.0ML/MIN *
* Detector O: 254NM/.1AU Detector 1: *
* Misc. Information: CALIBRATION/GPC *
*******************************************************************************
S+ artir,g Delay: O.C)OC tibration file: GPCPHEN
Mulecular Weight Distribution Averages
Baseline TIMES: 3.85 to 10.00 MW:
P _cess .TIMES: 3.85 to 10.00 MW:
T tal Area: 196902
Mw= 1718
M- = 370
M /Mn= 4. 6439
Mz= 4134
1501
Ending Retention Time: I0.()0
22295 to 2
22295 to 2
Mol Wt 5 418 IB
3 2IB 18
OR. _ _,.ml'A_ v, _._,-
OE FOOR QUA/.Zl_. CHART lOB
4 _ FILE B:GF'C22 .HDR TAKEN 08-05-19B6 17:18:27
oample Name: 91LD 2-2 C=2.b8 Operator Initials: GBF *
Date: 0S-05-1986 11:5B:33 Method: DATA FILE: B:GPC22 .PTS
nterface: 5 Cycle#: 22 Channel#: 0 Vial#: N.A. *
tartir, g Peak Width: &O Threshold: 0 *
Instrument Type: HPLC/BECKMAN Column Type: ULTRASTYRASEL 500A *
Solvent Description: THF *
Operating Conditions: T=35C FLOWRATE=2.0ML/MIN *Detector O: 254NM/.1AU Detector 1: *
÷ Misc. Information: CALIBRATION/GPC *
_. ****************************************************************************
Starting Delay: 0.00 Ending Retention Time: 10.0£)
Se ibration file: GPCPHEN
Qc ecular Weight Distribution Averages
Baseline TIMES: 3.85 to
or_cess TIMES: 3. B5 to
Tc al Ar_: 240471
lw_ 1801
_n= 36B
M_ Mn= 4.8q45
M_ 4352
_ 1573
10. O0 MW: 22295 to 2
_oo_ t 0 210. C)O MW : _-_..-,
Mol Wt 518
418
Lo_ Mol Wt v:. l_eaz-6umx
3 2 118 18 18
CUB %
188
?5
56
Z5
69
18
CHART IOC
* 3ample Name: 91LD _ _ C=2.68 Operator Initials: GBF *
* Date: OB-O5-19B6 11:28:37 Method:GPC DATA FILE: A:GPC20.PTS *
* Interface: 5 Cycle#: 20 Channel#: 0 Vial#: N.A. *
* Btarting Peak Width: 60 Threshold: .01 **********************************************************************************
Starting De2 ay: 0.00Calibration file: GF'CPHEN
Instrumer,t Type: HF'LC/BECKMAN Column Type: ULTRASTYRAGEL 500A *
Solvent Description: THF *
Operating Conditions: T=35C FLOWRATE=2.0ML/MIN *
Detector O: 254NM/.1AU Detector 1: *
Misc. Information: CALIBRATION/GF'C *
*****************************************************************************
Ending Retention Time: I0.00
Averages
10.00 MW: 22295 to 2
10.00 MW: 22295 to 2
M tecular Weight Distribution
B_aeline TIMES: 3.85 to
Process TIMES: 3.85 to
T Lal Area: 271362°.
M = 1598
Mn= 260
M,-,/Mn= 6.1449
M = 3922
My= 1389
25
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!13. ETA* ETA ........ E_r_ ........ TORQUE ..... .... TIME ....... TEMP .....F'OISE POISE POISE - _BRAMS-CM - MIN .... DEG. :£---
1 .I.35 le+002 .1.256e+0C)2 4. 992e+001 1. 696e+001 _.-O00e-O01 3. 200e+OOi:_ z
._ 1. _44e+002 I. 266e+002 4.52.1 e+O0:1 _I;686e+001 1..f_'_Oe+O00 3. _e,Oe*O01 _-
--_ .3 1.268e+002 I. 19_e÷002.. 4.D1_e+O01 1.591e+OOi_2..DE_Oe÷O00 _'3._K)e_-O01--__4 1. 152e+002 1. 081e÷002 _.._9B2e+O01 i. 446e+001 3. OODe+O00 ".,.400e+O01 ;_
5 I. 022e+002 9.49C_e+001 3. 799e+001 I :2B2e+OCll #. O00e+O00 "..._600e+O01
6 I_.971e+001 Bi175e+O01 "3.igBe+OOX--1.'125e+OO1---51.'OOOe-+-O00 ---'..8r_Oe_-_}K__-.P
7 "7.W26e÷OCil 7. OE_7e+(iO J 3. 550e+001 9. 945e+000 6. O00e+OOCi 4. O00e+OOi
E_ &. O97e+O01 ,6.O03e+O01 3. 397e+001 _ B. 65Cie÷OOCi _7_O00e+O00 4. I00e+001
_. _157e+001 --.5.200e+001_ --3.296e+00i _ _7o 728e÷OOO---E_JODOe+OOO-2 _o300e+DDJ___
1_:_ 5. 522e+(_01 " ;4.55qe÷OC)l - 31128e-_d;(_i- 6. 926e÷ObC_--_-_'-(_be+6(]O--- _4_-500e+-_EOi--7
I i 4.913e+001 3. 904e+001 2. _E}2e+OC)l 6.1&4e÷O00 a.DOOe+OOJ 4.70Oe+O01
12 4. 464e÷001 3* 4-_-_e÷£tOL-_?._. Ofi7e+OCil=-5._fiO2e+090____. IOOe+_O01--= _4+ 900e-,-DOl
13 4. 033e+OAI 2. 964e+OOi _2.735e+OD1 ....5. O57e+OO0 .i_.DCK_e+O01 5. I00e÷001
14 3. 706e+001 2. 634e÷001 2. 606e+001 4. &52e+O00 I. 30Cie*CiOl 5. 300e+O01
-- :I5 2. 322e+001 --2. 355e÷Or11 -L-2. _,4_--e÷001-2- 4. i65e_-000 -"I. 40_+001 - 5. 500e÷C.TOi-L:
6 2.9&SemCiOl 2. _52e+0C)I 2.060e+00_I _" 3.718e+000 -41. 500e+OOf 5. 700e+001
17 _ _'2-4e._'?.K*_--4-,-_Z&e+OO _ _.-,_;:l-7_.eli,T, lr._-_-_._27e+O_l13_-T---._A_OEbe_.-ZL1 .._.9.CIDe+C}_ _j --
18 2. 603e÷OCil :I . 94_e÷0(:11 I. 726e÷0CII -3. 268e+000 ....I ..70_-i-001 6. 100e+OOi
19 ,._, 466e+001 - 1,901e÷001 - -1 , 570e+0C)1-----3.094e+000_ -1 .BOOe÷OOl _ 300e+001 _.
20 _ 363e÷001 1 883e÷OOJ 1. 428e÷001 2. 965e+0CI0 I. 900e+001 6. 400e+0C)1
- 21 2. 217e+001 _I.S29e+001 -_ i. 254e+001 2.TBOe÷O00 2:00Cie*O01 6. _500e÷O0! -
22 2. 071e+001 1.77Be+001 I .061 e+O01 - 2. 598e÷_;0_3 _#10_le÷OCil- o. 800e-_Ki:1
":._'3 i. E_E_le÷('l(')-_ - _-_656e+C_,_ B. _i7;+OC)C) _o_5_e-+oclo _-._-CTOe÷OC)_--=7.OOOe+O01_. • . . .....
24 I. 760e_-,:',0! I. 597e_-001 ":7..-'x83e4.000-"-2.208e÷000 - _'_._e_-o01 --7. 200e+O0 I
25 !.574e+001 I. 449e+00] 6.153e-I-000 1.976e+DO0°'2. #OOe+O01 -7. 400e+001
2_ :I.46be÷001 . .1_3_7e+001 -5.297e-I-000 I ._40e+O00 2,_00e÷001 --'7.60(_e+O01
27 I. 299e_-001 I. 226e÷00:I 4. 304e+000 -_ ._31e+CiO0 2. _t'K._e+O01 7. BO{_e+O01
28 I. 160e÷O01 I. lOSe+O01 :_3._42e+000 I',456e+000 _2_._'00e+001 8.0C,(,6+00_I
29 I. 064e+001 I. Ol Ie_-OOi -:_ 3_305e+000 1. 335e+000- --2.800e+bC)l B. 2CiOe+OC)!
30 9.2_9e+000 _#.egoe+O0_ 2._95e+OOO---=;_i_5e',OON 2.gOOe+O0i- e._Or.,e+O0__3 _ 7. O52e+OOr._ =-2"7.710e_O00 --I. _;48e_-OCiO 9. _BCCe-O01- =3. O00e_-OO] - B.-6OOe+O0_1
--- "_o _"9°.3t_3e._OO0E_.9_7-e+O00 - -"_.._e._-OOO:-'_.-iT"_ge_-13t3_Z_-_._t_Oe+-O01 ÷ -E_. BOOem.r',O. 3
• . ;- ," • , " • . ::_ _--___',,",_ • -'-r -__ -- _ _-_..". _-_
_36 5. B27e+O00 --3._77e+000- 6. 155e-001 --4.BO6e-O01 -__oSOOe+OOi 9.500e+001
=:;_'_ ,6. O06e'_-{K)O -- 5. 839e+OOO-'_.i._D9e+OOD-- 7.-.535e--00i ,;3. 600e÷O01 :_.700e+O01
-- T_ --5.95_÷O00-"_:'_'98e_-OIYO--e'l. ---2_6e'_)CR:)-=-_'_".-_e=Z_-OOi-"_'_rjOe'+--O01 .:.._I.O.I Oe+O02
40 5. 391e+000-; _5.287e+000 I. 057e+000 6.'766e-00.| __3._-.90.0e+0_01 I ,O30e+rK_2
: I _. 839e÷000 3.6BBe__CK_--.__ ,ObBe+O00 -_BiTe--OOi L_OOOe+O01 --_,-050e+002
:.:43 _-3.582e+O_K_ ....G. _519e-_O0 __, 770e-_001 - :_ _.gae_-4_,_'__=!-'_i_--_P-_e+O02 7-
--_# - 2.4_7_+000 --2. 379e÷000 --_.,5._BOe-._D_i_3oi%Sb_,,O0.1 ...._300__-_-_L_;_I 1£_ -_
=........._-_. _a_+ooo___. _e_6oO-_-_ oe-ooz---_._=_--_5-i-7_7-_c_, _;-a _ _oe*oo_,6 2.529e+00(_ __2.4_e÷DDD ;__-_3.?,e-001---3. l-7_-e-_O1---4_-50(_e'_O0! ---I._5_Oe+__O[Q2_LL-c.
--"-#7"-5;-2 &_=DOO -:-G._+_O-Ci_T6____. 67e-._O_-:_,T_e-_:KI1 ="------_---'_A0e+002___ : .
- .s-..z.i_z:s,,+c,c<,=-_,es__-,-(<,o=,7i.__Be-C;_--____:];S.e:_CT-._._--_..OC_Z,__-;;_.-IBoW÷oo2-:.T9 5.591e+000 5. 426e+000 .I._49e+000 _-7. 010e-_001 --_.-_OOeeC_l 1.20(1_e'*'C_C)2 -
50 2.915e+000 --2.87Ge+O00 - _. 928e-001 ....._. _'Te"O-O I ---4.900e+O01 I .220e+002
._ ..-_-= _..----__-_=_::_. :._.... ..__.-_=_=-.-_.-....._.:.= ........... = -.....
............... !_;__. ....: ....._ . ---_- :- --:_. .=-,_.... " -
'_ .-:" ----.-.- .'_L --'-'-'-- -'_'" "-- ..... '- -;'"':"-- ---: ......
..................... ......
• --.__ . __ - ....... .
:A FINGERF'R!NT VISCOSITY PROFILE 91LI} RESIN-NASA-LOT'2--_ .................. -'_L....
.: -_-.-- -- ....... __
h _. ETA* ETA ...... ETA" TORQUE TIME
POISE POISE POISE GRAMS-CM - " MIN.-
=.I 4.18Ge+O00 4. C)73e+000 9. 518e-001 5. 246e-001 -5:_000e+001
2 "5. 029e+000 4.881 e+Cx'_O I. 2 _ I e+0C_0 6. 309e-001 5. lOOe+O01
3 _. 973e+00C_ 6. 753_-+000 1. 739e+CK-) 8. 739e--001 "5._-200e÷OO 1
5z_ I. 8&6e+O01 1. 754e+001 6. 376e+000 2. _4C_e+OC_O '5. _OOe+O01
Op._.,INAIC PAGE
Of POOR QUALrl_
...... -TE'_6.... DEG. -:!2 .
1.240e÷002. _
1. 260e+002
.2BOe+O02 -
.300e÷002
. --_.---._-_. =: - :- . _- -
. o
- _ --'-- .... _-_-2.'_- _.L"- i _ _T- --T_--._-'-_ .... -3.--_'- " "
.... 3_=_ £ ...................... [ ..................... __..L...........
• : :- :" :_.'_:._ Z_ ..... _ .-
...... __...... .:-.--__ _.;-_7-.. -- - -_--- _ ". --. 7: T " "- -'. "E"._-'-- ---G_,-.-: ";---'-,_._.-- -'-
_---.... ;-__: :--- -: . - =.._........ -.- _ -
". _. _. ________..___= ......... - ....... _......... :............. _ -.-- __. .=_....=-=-__ ...... =. _.-= ............... .-;.:__.__-.-=:____:_.__-- _ . .
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SOLVENT ONLYSCAN
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CHART 15B
I-
I-
[
I
I-
....... + ....
i .
TEST
la.
lb.
2a.
2b.
2c.
3.
4.
5.
6.
7a.
7b,
7c,
8a.
8b.
9a.
9b,
10a.
10b.
10c.
TABLE OF CONTENTS
FABRIC TESTING
NAS8-36298
Polymerlc O.E, 71108
Fabric for NASA Lot# 2
PAGE
CHARTS
Visual Inspection ................................... 3A - 3M
TGA ................................................. 6A - 6M
Breaking Strength, WARP ........................... I
Breaking Strength, FILL ........................... I
Carbon Assay ...................................... I
Hydrogen Assay .................................... 2
Nitrogen Assay .................................... 2
Visual Inspection ................................. 2
Specific Gravity .................................. 2
pH ................................................ 3
TGA ............................................... 3
Atomic Absorption ................................. 3
MQisture Content .................................. 4
Ash Content ....................................... 4
Filament dlameterp WARP ........................... 4
Filament diameter, FILL ........................... 4
Thread Count, WARP ................................ 5
Thread Count, FILL ................................ 5
Areal weight ...................................... 5
Vclatlles ......................................... 6
Weight Change on Acetone Wash ..................... 6
FABRIC TESTING
NAS8-3629B
Page 1 of 6
U.S. POLYMERIC 0.£. 71108
SWB-8 Fabric for NASA Lot# 2
la. Breaking Strength, £bs/in, WARP #2-___I #2-2
ASTM D1682 PICK 61 42CENTER 55 44
PLAIN 75 60AVG. 63.7 48.7
#2-3
92
98
2772.3
#2-4 #2-...._5 #2-6 #2-7 #2-8 #2-9PICK 16 27 63 48 25 12
CENTER 69 84 65 87 14 41
PLA IN 7__6 7___7 66 8__8 4__8 7_3_3AVG. 53.7 62.7 64.7 74.3 29.0 42
#2-10 #2-1! #2-12 #2-13 LOT2PICK 24 59 71 38 44.5
CENTER 71 92 103 64 68.2
PLAIN 23 4__3 8_._.2.2 28 58.9AVG. 39.3 64.7 85.3 43.3 57.2
lb. Breaking Strength, Ibs/inoh, FILL #2-1 #2-2ASTM D1682 PICK 72 59
CENTER 83 66
PLAIN 67' 6"3AVG. 74.0 63.3
AVG
#2-377
63
7"371.0
2a. Carbon
MDQAI
#2-4 #2-5 #2-__6 #2-__._Z #2-8 #2-..__99PICK 92 28 71 102 25 53
CENTER 71 77 39 48 22 46
P L A I N 6__I 47" 7__00 27 19 5__55
AVG. 74.7 50.7 60.0 59.0 22.0 51.3
#2-10 #2-11 #_ #2-1.__3 _OT2
PICK 73 83 30 55 63.1
CENTER 20 83 58 51 55.9
PLAIN 58 8.._55 88 4..55AVG. 50.3 83.7 58.7 50.3 59.2
AVG
Assay, X #2-I #2-2 #2-____3
5560 PICK 99.2 99.6 99.8CENTER 99.6 99.8 99.6
PLAIN 99.0 98-9 99.___99
AVG. 99.27 99.43 99.77
#2-.._4 #2-.__._55 #2-...._6 #2-7 #2-8 #2-_._.._9PICK 99.1 99.2 99.9 99.7 99.7 99.7
CENTER 99.8 99.7 99.6 99.8 99.7 99.8
PLAIN 99.9 99.____!0 99.9 99.4 99.9 99..____99AVG. 99.60 99.30 99.80 99.63 99.77 99.80
HITCO MATERIALS DIVISION
700 E DYER ROAD, SANTA ANA, CALIFORNIA 92707 , (714) 549-1101 • TVV3((910) 595-1130 • FAX # (714) 549-2858-5-2437
Page 2 o_ 6
_WB-8 Fabric _or NASA Lot# 2
2m. Carbon ksssy_
MDQAI 5560
PICK
CENTER
PLAIN
AVG.
% (CONTINUED)
#2-10 #2-11 #2-12 #2-13 LOT2 AVG99.9 99.9 99.4 99.9 99.6299.6 99.5 99.8 99.9 99.71
99.2 99.4 99.6 99.9 99.5399.57 99.60 99.60 99.90 99.62
% #2-1 #2-22b, Hydrogen Assay,MDQAI 5560
#2-3
PICK .03 .02 .01
CENTER .03 .01 .01
PLAIN .02 .02 ,01AVG. .027 .017 .010
#2-___!4 #2-5 #2-s #2-7PICK ,02 .01 .02 <.01
CENTER .01 <.01 .02 <.01
PLAIN .01 <.0___._1 .01 <.0..__/1AVG. .013 EST .004 .017 EST .001
#2-8
<. 01
<.01
<.01
EST. 001
#2-9
<.01
<.01
<.01
EST .001
#2-1____9_ePICK <.01 .01
CENTER <.01 <.01
PLAIN .01AVG. EST .004 EST .004
#_-12 #2-13 LOT2 AVG<.01 <.01 .010
.01 <.01 .007
.01 <.01 .007
EST .007 EST .001 .008
2_. Nitrogen Assay,MDQAI 5560
% #2-1 #2-2 #2-3PICK .22 .19 .11
CENTER .21 .23 .09
PLAIN .09 .09 .16AVG. .17 .17 .12
#2-4 #2-5 #2-6 #2-7 #2-8 #2-9PICK .1 .1 .1 .1 .2 .3
CENTER .1 .02 .1 .1 .2 .2
PLAIN ,1 .1 .1 .04 .1 .1AVG. .1 .073 .1 .08 .167 .2
#2-10 #2-11 #2-1_ #2-13 60T2PICK .1 .1 .1 .; .14
CENTER .2 .1 .2 .1 .14
PLAIN .2 .1 .1 .02 .10AVG. ,167 ,1 .133 .073 .127
A.VG
3. Visual Inmpectlon
OCi-102
See Charts 3A-3M
4. Specific Gravity,PTM-84
Units #2-1 #2-2 #2-3PICK 1.7376 2.0163 2.0137
CENTER 1.7742 2.0569 2.0601
PLAIN 1.9094 _ 0466 2.0501AVG. 1.807 2.040 2.041
4.
.
.
7S.
_WB-8
Gravity, Units
Fabric for NASA Lot# 2
(CONTINUED)
Page 3 of 6
#2-4 #2-5 #2-__6 #2-7 #2-8 #2-9PICK 2.1453 2.1458 2.2223 2.0307 2.1896 1.7857
CENTER 2.1874 2.7238 2.1354 2.0625 2.1918 1.8273
PLAIN _.1789 _.2718 2.1337 _.1014 2._909 1.7342
AVG. 2.171 2.380 2.164 2.065 2.191 1.782
#2-10 #2-11 #2-12 #2-13 LOT2 AVG
PICK 1.6823 1.7784 1.5362 1.6062 1.9146
CENTER 1.8032 1.7732 1.6435 1.7198 1.9969
PLAIN _.7129 _.7895 _.7164 _.7572 1.9689AVG. 1.733 1.780 1.632 1.694 1.960
pH, Units
CTM-24B
AVG.
#2-I #2-___22 #2-___336.6 4.2 6.1
6.3 4.___2 6._._22AVG. 6.45 4.2 6.15
#2-4 #2-5 #2-__6 #2-7 #2-8 #2-96.0 6.2 6.4 6.0 6.4 6.9
6..___z 6._..3_2 6.4 6. e 6...__4 7._.._6.15 6.2 6.4 6.0 6.4 6.95
#2-10
6.2
6.2
AVG. 6.2
TGA, "C at 50X Weight LossCTM-51 (AIR)
Atomic Absorption, ppm
CTM-53B
#2-11 #2-12 # 2-I_________3 LOT2 AVG6.6 6.0 6.6 6.18
6.5 6.___0 6..__e9 6.206.55 6. • 6.85 6.19
SET UP# 1
#2-2 939#2-4 926
#2-5 934
#2-7 913#2-9 879
#2-11 876
#2-13 905AVG. 910
See Chart 6A-6M
.21Na 3
K 1Ca 31
Mg •
Li ...0_0AVG. 35
#2-5 #2-6 #2-7
5 6 4
2 1 1
16 13 15
I 1 0
_@0 __0 __o24 21 20
#2-4
Na 3
K 2
Ca 25
Mg •
AVG. 30
SET UP# 2
#2-1 867
#2-3 881#2-6 834
#2-8 825
#2-10 833#2-12 782
AVG. 837
42-2 #2-34 6
1 1
32 16
• 1
__0 o37 24
#2-8 #2-99 11
1 1
77 101
I 1
88 114
Page 4 o£ 6
SWB-8 Fabric for NASA Lot# 2
7a. Atomic Absorption, ppm (CONTINUED)
CTM-53B
#2-10 #2-11 #2-12 #2-13
Na 7 6 4 4
K I I 1 1
Ca 62 54 29 30
Mg • • • 1
AVG. 70 61 34 36
LOT2 AVG
5.5
1.2
38.5
0.5
0.0
45.7
7b. Moisture Content, X
CTM-53B
#2-1 .020
#2-2 .025#2-3 .020
#2-4 .015
#2-5 .005
#2-6 .015
#2-7 .o05
Lot#
#2-8 .000
#2-9 .010
#2-10 .015
#2-11 .010
#2-12 .005
#2-13 .005
2 AVERAGE .011
7(3. Ash Content,
CTM-53B
#2-1 .020
#2-2 .035#2-3 .020
#2-4 .020
#2-5 .010
#2-6 .035
_2-7 .030Lot#
#2-8 .080
#2-9 .059
#2-10 .070
#2-11 .055
#2-12 .005
#2-13 .029
2 AVERAGE .036
88. Filament diameter,
S.E.M. procedure
(diameters are an
10 measurements)
microns, WARP
average o£
AVERAGE 9.12
Minimum 8.25
Maximum 9.75
Std. Dev 0.52
#2-2 #2-39.60 9.64
8.00 8.9510.90 10.30
0.94 0.43
#2-___44AVERAGE 9.58
Minimum 7.95
Maximum 11.25
Std. Dev 1.15
#2-5 #2-_ #2-7 #2-8 #2-910.03 9.36 9.65 9.28 9.74
8.75 8.00 8.05 8.00 8.3512.45 10.60 11.50 11.00 10.45
1.21 0.89 0.97 0.90 0.56
AVERAGE 9.85
Minimum 7.75
Maximum 12.00
Std. Dev 1.28
#2-12 #2-13 _OT2 AVG
e. 55 9.18 10.11 9.59
8.55 8.10 8.25 7.75
10.55 10.05 12.05 12.45
0.66 0.64 1.25 0.92
8b. Filament diameter,
S.E.M. procedure(diameters are an
10 measurements)
microns, FILL
average of
#2-1
AVERAGE 10.00
Minimum 9.00
Maximum 13.50
Std. Dev 1.34
98.
9b.
10a.
Thread Count,
PTM-5A
AVG.
AVG.
Thread Count,PTM-5A
AVG.
AVG.
Areal Weight
PTM-3A
SWB-8 Fabric for NASA Lot# 2
per inch, WARP #2-I
AVG.
4141
4041
4_!140.8
Pmge
#2-2
4443
4544
4444
5o_ 6
#2-3
40
4040
41
4__o40.2
#2-4 #2-5 #2-6 #2-7 #2-8 #2-944 43 40 39 36 4044 43 40 38 36 40
43 42 40 39 36 41
43 43 40 39 36 41
4_.4 4_22 4__0 3_.8 35 4_!I43.6 42.6 40 38.6 35.8 40.6
LOT2 AVG
39.9
39.6
39.8
39.8
39.5
39.7
#2-10 _ #2-12 #2-13
35 40 42 35
35 39 42 34
36 39 41 35
35 39 41 34
3_.55 40 40 3.435.2 39.4 41.2 34.4
per inch, FILL #2-I38
38
38
38
38AVG. 38. •
#2 -2
38
38
38
38
3838. •
#2-3
35
36
35
36
3635.6
#2-4 #2-_____55 #2-6 #2-7 #2-8 #2-_.___99
38 39 38 39 37 37
38 38 38 39 39 37
39 38 37 39 39 38
39 38 37 39 38 37
39 38 37 3-0 40 3-038.6 38.2 37.4 38. s 38.6 37.4
_OT2 AVG38.2
38.3
38.3
38.3
38.438.3
#2-2
3. 516
3. 510
3. 722
3. 583
#2-10 _ _ #2-15
39 41 39 39
38 41 39 39
39 41 39 38
38 42 39 39
3-0 41 39 3938.4 41.2 39.0 38.8
gm/4x4LEFT
CENTER
RIGHT
AVG.
as received, #2-1
3. 416
3. 234
3. 327
3. 326
#2-_____33. 214
3. 196
3. 375
3. 262
Page 6 of 6
SWB-8 Fabric _or NASA Lot# 2
10a. Areal WeightPTH-3A
LEFT
CENTERRIGHT
AVG.
as received, gm/4x4
#2-8
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CENTER -.13 -,18 -,25 -,26 -,16
RIGHT .oe _ _ -.e7AVG. -,09 -,15 -.21 -.21 -.12
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Hamld M. Quralshl, Manager
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TABLE OF CONTENTS
PREPREG TESTING
NAS8-36298
U.S. Polymeric O.E. 71108
FM 5834 NASA LOT# 2 U.S.P. LOT# D09275
PAGE
Resln Content, Soxhlet ............................ 1
Filler Content, Soxhlet ........................... I
Cloth Content, Scxhlet ............................ I
Volatile Content .................................. 1
Flow .............................................. 1
Resin Content, Dry Basis .......................... 2
Tack .............................................. 2
Gel Tlme .......................................... 2
Atomic Absorption ................................. 2
Mclsture Content .................................. 2
Ash Content ....................................... 3
TGA ............................................... 3
DSC ............................................... 3
Infrared (IRZB} Baseline .......................... 3
Environmental History ............................. 3
Specific Gravity .................................. 3
Tensile Strength .................................. 4
Tensile Modulus ................................... 4
Tensile Elongation ................................ 4
Flexural Strength ................................. 4
Flexural Modulus .................................. 5
Compressive Strength .............................. 5
Compressive Modulus ............................... 5
Double Shear Strength ............................. 5
Barccl Hardness ................................... 5
Residual Volatlles ................................ 6
Resin Content, Pyrolysis .......................... 6
Acetone Extraction ................................ 6
CTE, with ply ..................................... 6
CTE, crossply ..................................... 6
CHARTS
8A - 8G
9A - 9G
10A - 10G
21A - 21G
Uo So
PREPREG TESTING
NAS8-36298
POLYMERIC O.E. 71108
11.
FM 5834 NASA LOT#
Resin Content, Soxhlet, X
CTM-6D
U.S.P. LOT# D09275
AVG.
ROLL#1 ROLL#2 ROLL#3 ROLL#4 ROLL#5
START START _TART START START37.5 36.0 35.1 36.3 37.9
39.6 36.3 35.4 35.8 37.3
37.1 35.2 35.2 35.6 39.338.1 35.8 35.2 35.9 38.2
NASA LOT# 2
lb. Filler Content, Soxhlet, X
CTM-6D
AVG.
15.6 15.0 14.6 15.1 15.8
16.5 15.1 14.7 14.9 15.5
15.8 14.9 14.7 14.9 15.9
NASA LOT# 2
Ic. Cloth Content, Soxhlet, X
CTM-6D
AVG.
46.9 49.0 50.3 48.6 46.3
43.9 48.6 49.9 49.3 47.2
47.5 50.3 50.1 49.6 44.346.1 49.3 50.1 49.2 45.9
NASA LOT# 2
2. Volatile Content, X
PTM-17B
AVG.
4.5 5.4 5.4 5.5 5.1
4.3 5.7 5.5 5. a 5.44.___33 5.___4 5.2 _ 5.__._s4.4 5.5 5.4 5.4 5.4
NASA LOT# 2
3. Flow, X
PTM-19G
AVG.
Page 1 of 6
ROLL#6 ROLL#7
_TART START38.0 37.237.4 37.7
38.2 37.837.9 37.6
AVERAGE 36.9
15.8 15.5
15.6 15.7
15.8 15.6
AVERAGE 15.4
46.2 47.3
47.0 46.6
45.9 46.5
46.4 46.8
AVERAGE 47.7
5.6 6.1
5.5 5.5
5. s5.5 5.8
AVERAGE 5.3
11.0 18.8 13.5 18.4 19.1 17.2 19.0
11.7 20.3 17.6 19.5 20.0 17.9 20.2
11.9 19.6 16.0 19.4 19.0 18.0 19.7
NASA LOT# 2 AVERAGE 17.7
HITCO MATERIALS DIVISION
700 E DYER ROAD, SANTA ANA. CALIFORNIA 92707 • (714) 549-1101 • "rwx (910) 595-1130 • FAX # {714) 549-2858-5-2437
Page 2 of 6
FM 5834 NASA LOT# 2 U.S.P. LOT# D09275
4. Resin Content, Dry Basis,
PTM-16F, Type II
ROLL#1 ROLL#2 ROLL#3
START START START
38.3 38.7 41.5
38.8 41.0 41.6
38.9 36.6 39.4AVG. 38.7 38.8 40.8
ROLL#4 ROLL#5 ROLL#6 ROLL#7
START START START START
37.7 42.4 38.0 43.3
40.1 41.6 38.4 42.7
34.5 41.3 39.4 dl.837.4 41.8 38.6 42.6
NASA LOT# 2 AVERAGE 39.8
5. Tack, Ibs
PTM-80
60 44 36 40 48 35 42
NASA LOT#2 AVERAGE 44
6. Gel Time, Seconds
PTM-20E
87 68 70
7a. Atomic Absorption,CTM-53B
ppm
62 73 65 63
NASA LOT# 2 AVERAGE 70
ROLL#1 ROLL#2 ROLL#3 ROLL#4
START START START START
Na 8 7 13 6
K 2 2 I 1
Ca 18 17 16 15
Mg 2 2 I I
TOTAL 30 28 31 23
ROLL#5 ROLL#6 ROLL#7
START START STARTNa 6 10 5
K 2 1 1Ca 16 35 58
Mg 1 1 2
TOTAL 25 47 66
LOT#2
AVG.
8I
25
1
36
7b. Moisture Content,
CTM-53B
ROLL#1 ROLL#2 ROLL#3 ROLL#4 ROLL#5
START START START START START
3.11 2.85 3.44 2.97 3.13
NASA LOT#
ROLL#6 ROLL#7
START START
3.77 2.83
2 AVERAGE 3.16
Page 3 of 6
FM 5834 NASA LOT# _ U.S.P. LOT# D09275
7c. Ash Content, %
CTM-53B
ROLL#1 ROLL#2 ROLL#3
START START START.04 .04 .03
ROLL#4 ROLL#5 ROLL#6 ROLL#7START FTART START FTART
.04 .04 .o2 .04NASA LOT# 2 AVERAGE .03
8. TGA, % Weight Loss at 500"C
CTM-5i (Nitrogen)
7.1 4.9 7.6 6.4 6.9 7.9 6.5
NASA LOT# 2 AVERAGE 6.8
See Chart 8A-SG
9. DSC, "CCTM-50A ROLL#I-S
ROLL#2-S
ROLL#3-SROLL#4-S
ROLL#5-SROLL#6-S
_OLL#7-S
NASA LOT# 2
FIRST TEMPERATURE
182
182
182182
181
183
180AVERAGE 182
SECOND TEMPERATURE
240
243
241243
241
239243
241
See Chart 9A-gG
10. Infrared (IRZB) Basellne
CTM-21C
ROLL#1 ROLL#2 ROLL#3 ROLL#4 ROLL#5
START START _TART START1.08 1.09 1.09 1.07 1.07
NASA LOT# 2
ROLL#6 ROLL#7
FTART START1.05 1.08AVERAGE 1.08
See Chart 10A-lOG
11. Envlronmentml History Date manufactured: 28 Nay 1986
Packaged in: Polyethylene bagsupported in
cardboard carton
Date shipped: a July _986 in40"F truck
12. Specific Grmvltyt Cured, Units
ASTM D 792
i 1,516 1,513 1.500
1.513 1.527 1.501
1.511 _ 1,499AVG. 1.513 1.522 1.500
I._I_ 1.50s 1.496 l,Sil1,523 1.509 1.485 1,5_2
1.50__.___4_ i.si_____31.520 1.507 1.491 1.512
NASA LOT# 2 AVERAGE 1.509
13a,
13b.
13C.
14a.
FM 5834 NAS_ LOT#
Tensile Strength, ksl, WARP
FTMS 406-1011
AVG.
U.S.P. LOT# D09275
ROLL#1 ROLL#2 ROLL#3 ROLL#4 ROLL#5
START START START START START22.87 24.71 29.95 27.64 22,81
25.17 21.18 30.48 26.27 22.37
24.65 25.99 25.90 25.48 20.25
24.40 22.83 27.55 22.55 22.68
23.67 _3.47 27.46 26.0__4 21.0_.__._8824.15 23.64 28.27 25.60 21.84
NASA LOT#
Tensile Modulus, msi, WARP
FTMS 406-1011
4.59 4.88 4.57 5.34
5.66 5.38 5.18 6.17
4.74 4.84 4.99 5.454.93 5,06 4.92 5.36
5.02 4.80 5.34 4.914.99 4.99 5.00 5.45AVG.
Tensile Elongation, %, WARPFTMS 406-1011
.50 .62 .68 .60
-- .53 .65 .53
.60 .65 .58 .54
.54 .55 .64 .51
.54 .58 _ .ss
.55 .se .63 .55AVG.
Flexursl Strength, ksl, WARP
FTMS 406-1031
33.89 37.80 47.66 37.41
36.63 38.59 43.56 37.08
41.72 36.87 45.82 40.61
38.59 32.49 45.90 39.15
40.45 31.68. 44.35 34.6038.26 35.49 45.46 37.77AVG.
2
Page 4 o_ 6
ROLL#6 ROLL#7
START START
29.86 28.65
29.89 27.54
28.63 24.87
31.79 27.13
29.72 25.1329.98 26.70
AVERAGE 25.74
38.21 43.37 39.23
33.17 42.09 41.7337.20 44.55 41.86
32.90 44.63 42.03
43.66 41.5935.88 43.66 41.29
NASA LOT@ 2 AVERAGE 39.69
.68 .55 .64
.64 .60 .63
.53 -- .57
.64 .53 .60
.62 .57 .55
.62 .56 .60
NASA LOT# 2 AVERAGE .59
3.95 5.79 5.61
4.20 5.48 5.26
4.43 -- 5.40
4.36 6.15 5.80
4.16 6.02 5.38
4.22 5.86 5.49
NASA LOT# 2 AVERAGE 5.14
14b.
15B.
15b.
16.
17.
F M 5834 NASA LOT#
Flexural Modulus, msi, WARPFTMS 406-1031
AVG.
2 U.S.P. LOT# D09275
ROLL#1 ROLL#2 ROLL#3 ROLL#4 ROLL#5
START START START START START
4.32 4,28 6.06 4.46 4.32
4.16 4,80 5.58 4.44 3.70
4.08 4.72 5.68 4.50 4.06
4.38 3.82 6.04 4.40 3.96
4.38 4.32 4.88 4.42 4.24
4.26 4.39 5.65 4.44 4.06
NASA LOT# 2
Compressive Strength, ksi, WARPFTMS 406-1021
Page 5 o£ 6
AVG.
ROLL#6 ROLL#7
STAR.___./_T START4.94 4.76
4.82 4.66
5.22 4.32
5.28 4.88
5.02 4.68
5.06 4.66
AVERAGE 4.65
26.50 24.88 27.59 25.71 26.56 29.07 28.84
22.75 24.65 26.86 26.83 23. S5 27.76 26.08
24.73 24.14 27.22 25.94 26.89 27.90 27.80
25.37 23.31 26.15 26.68 24.98 28.33 30.12
_5.15 _3.19 27.42 25.47 27.17 28.7_ 28.5124.90 24.03 27.05 26.12 25.91 28.36 28.27
NASA LOT# 2 AVERAGE 26.38
Compressive Modulus, msl, WARP
FTMS 406-1021
5. 12 4.96 5.07 5.25 4.86
4.44 4.59 4.56 5.26 4.54
5.04 4.22 5.02 4.97 5.02
5.09 4.50 4.67 5.32 4.794.4._.._.66 _ 4. e9 4.6.__.._9
4, 97 4.55 4.82 5.14 4.78NASA LOT# 2
AVG.
Double Shear Strength, ksl
FTMS 406-1041A
AVG.
3.55 2.98 3.21 3.66 3.33
3.42 3.33 3.60 3.62 3.39
3.26 3.09 3.85 3.48 3.35
3.42 3.21 3.35 3.49 3.373.36 3.62 3.54 3.93
3.4e 3.25 3.51 3.64 3.3sNASA LOT# 2
Barcol Hardness,
ASTM D-2583
(Average of 10
Units
determinations)
69.5 68.8 70.5 70.4 69.7
NASA LOT# 2
5.23 4.83
4.50 4.52
4.62 4.69
4.75 4.92
4.884.80 4.77
AVERAGE 4.83
3.08 3.62
3.48 3.21
3.31 3.43
3.57 3.94
3.32 3.54AVERAGE 3.44
70.8 72.4
AVERAGE 70.3
18.
19.
20.
21S.
21b
FM 5834 NASA LOT# 2
Residual Volstlles,
PTM-98
ROLL#1 ROLL#2 ROLL#3
_TART START _TART2.32 2.34 2.62
2.35 2.28 2.63
2.36 2.37 2.60
AVG. 2.34 2.33 2.62
Resin Content,CTM-14B
Pyrolysis, %
39.44 35.74 35.92
37.60 35.74 34.23
_9.39 36.82 36.5__4AVG. 38.61 36.10 35.56
Acetone Extraction, %CTM-18A
AVG.
-.15 .81 °59
1.19 -.46 .16
.72 .54 .40
.58 .30 .38
CTE, In/in "F,
PTM-61B
-.27
1.07
AVG. .40
wlth PLY
• 75
.46
• 62
-. 26
-.51
-. 39
CTE, in/inPTM-61B
13.44
9.80
AVG. 11.62
°F, Crosl
11.31
11.19
PLY
11.20
11.20
Page 6 o£ 6
U.S.P. LOT# D09275
ROLL#4 ROLL#5 ROLL#6 ROLL#7
START START START START
2.35 2.49 2.39 2.49
2.28 2.77 2.41 2.37
2.34 2.73 2.46 2.45
2.33 2.66 2.42 2.44
NASA LOT# 2 AVERAGE 2.45
36.23 38.50 40.14 36.08
37.24 37.34 38.56 34.60
37.69 34.35 39.48 34.36
37.05 36.73 39.40 35.01
NASA LOT# 2 AVERAGE 36.95
.69 1.98 .00 -.55
1.38 -.16 -.62 .38
.86 .16 3.66 -.22
.98 .66 1.01 -.13
NASA LOT# 2 AVERAGE .54
.58 1.09 .10 -6.92
.61 .86 .77 .78
.60 .98 .44 -3.07
NASA LOT# 2 AVERAGE -.06
13.79
12.96
13.38
13.12 15.62 14.38
_5.75 14.09
12.94 15.69 14.24
NASA LOT# 2 AVERAGE 12.89
See Chart 21A-21G
U.S. Polymeric
Hamld M. Quralshl, Manager
Quality Assurance Department
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