THROUGH: Dennis Miller, SERAS Program Manager ~ ~ Leader~e ...

DATE:

TO:

THROUGH:

FROM:

SUBJECT:

BACKGROUND

15 April 2011

David Mickunas, U.S. EPA/ERT Work Assignment Manager

Dennis Miller, SERAS Program Manager ~ ~

Danielle McCall, SERAS Task Leader~e(~ ~~/11 Shenandoah Road Site, Hopewell Junction, Town of Fishkill, NY W A # SERAS-042 - Trip Report- March 07 through 11, 20 l 1 Mobilization

The Shenandoah Road Groundwater Contamination Superfund Site (Site) is an area of contaminated groundwater which has impacted private wells that provide drinking water in the Town of East Fishkill, New York (NY), in an area known as Shenandoah. The area impacted by the groundwater contamination is approximately one mile southwest of the intersection of Interstate 84 and the Taconic State Parkway. There are approximately 230 homes in the immediate vicinity of the Site, which is a predominantly residential area. Local residences obtain water from individual wells drawn from the bedrock aquifer contaminated with volatile organic compounds (VOCs).

On 13 April 2000, the New York State Department of Health (NYSDOH) received information from a resident in the Shenandoah area which indicated possible contamination of a private residential well with tetrachloroethene (PCE). Residential well sampling that has been conducted at the Site by the NYSDOH and Environmental Protection Agency (EPA) since April 2000 indicated that a total of 60 residential wells have been contaminated at or above the Federal maximum contaminant level (MCL) of 5 parts per billion (ppb) for PCE and/or trichloroethene (TCE). MCLs are the maximum permissible levels of a contaminant that may be present in water used for drinking purposes. Treatment systems were installed on all of these wells to remove the contaminants of concern (TCE and PCE). The levels of PCE detected in the well water samples ranged as high as 1.6 parts per million (ppm). There are currently 103 point-ofentry treatment (POET) systems installed on all residential wells affected by the YOC contaminants.

lnvestigatory work, conducted in October 2000 by EPA and the New York State Department of Environmental Conservation (NYSDEC) at a former commercial facility at 7 East Hook Cross Road, discovered a I ,200 gallon metal tank containing high concentrations of PCE. Information obtained by the EPA and NYSDEC indicates that the facility was used between the late 1960s and early to mid 1970s for the cleaning of microchip holders or "racks". According to former employees of the facility, waste cleaning solvent (PCE) from this process was discharged into the septic system. As a result of these investigations, the Site was proposed for addition to the National Priorities List (NPL). During excavation of the contaminated soil associated with the former septic tank, two additional PCE disposal areas were discovered. Also in August 2001 , EPA discovered a buried "acid pit" behind the former 7 East Hook Cross Road facility. Based on the high levels of PCE detected in the soil surrounding the acid pit, the pit was probably used for disposal of PCE. The septic system, disposal areas, and the acid pit are believed to be the sources of site groundwater contamination.

SERAS-042-DTR-041511

R2-0008017


During previous contracts, Response, Engineering and Analytical Contract (REAC) 3 and REAC 4,

REAC personnel initiated and performed various tasks needed during the vapor intrusion study. In April

2004, using a Trace Atmospheric Gas Analyzer (TAGA) mass spectrometer/mass spectrometer (MS/MS)

system, REAC personnel performed indoor air monitoring of residences (units) in the vicinity of the

contaminated site in Hopewell Junction, NY. Included during this mobilization was the installation of

permanent sub-slab soil gas probes in each unit’s basement. Sub-slab soil gas samples were collected into

SUMMA® canisters from each unit. All collected samples were analyzed for VOCs in accordance with

modified EPA compendium method Toxic Organic 15 (TO-15), Determination of Volatile Organic

Compounds (VOCs) in Air Collected in Specially-Prepared Canisters and Analyzed by Gas

Chromatography/Mass Spectrometry (GC/MS).

In May 2004, residences with PCE results greater than or equal to the action limit of 11 parts per billion

by volume (ppbv) were re-evaluated in an attempt to locate the source of either PCE or TCE and

determine if they were the result of lifestyle contamination or from intrusion of vapors emanating from

beneath the slab (sub-slab). The evaluation of each unit consisted of the removal of household items from

the units which may have the VOCs of concern, real-time indoor air monitoring using the TAGA MS/MS,

indoor and outdoor ambient air sampling using SUMMA® canisters, and sub-slab soil gas sampling using

SUMMA® canisters. REAC Trip Reports 0076-DTR-083104 and 0076-DTRR1-092104 (revision of

0076-DTR-083104) outline the April and May 2004 mobilizations.

In February 2005, to investigate if seasonal variation affects vapor intrusion, REAC personnel were

mobilized to the Site to conduct sub-slab soil gas sampling during the heating season. Previously

sampled residential locations above the action limit (based on April 2004 data), as well as 15 new

residential locations were sampled. REAC Trip Reports 0076-DTRR2-051905 and 0076-DTRR3-053105

outline the February 2005 mobilization.

Based on data from previous mobilizations, EPA had requested mobilization of REAC personnel to the

Site during the heating seasons of the years 2006 to 2009. REAC personnel have sampled and had

analyzed sub-slab soil gas samples, indoor air, and outdoor ambient air samples from residential locations

with PCE results above 11 ppbv, or as designated by the Environmental Response Team (ERT) Work

Assignment Manager (WAM) or EPA Remedial Project Manager (RPM).

Results obtained during those four years are documented in the following REAC Trip Reports: 0076-

DTRR3-060606 outlines the February 2006 mobilization, 0076-DTR-060707 outlines the March 2007

mobilizations, 0076-DTR-051608 outlines the March 2008 mobilization, and 0076-DTR-051509 and

0076-DTRR1-062909 outline the March 2009 mobilization.

In November of 2009, as a continuation of the study, EPA ERT assigned Work Assignment SERAS-042

to the Scientific, Engineering, Response, and Analytical Services (SERAS) contract. During the heating

season of 2010, personnel from the SERAS contract mobilized to the Site as part of the ongoing vapor

intrusion study. Several locations within 12 residential units were sampled for sub-slab soil gas, indoor

air and outdoor ambient air.

All collected samples were analyzed for VOCs. The results obtained from the January 2010 mobilization

are documented in the following SERAS Trip Reports: SERAS-042-DTR-030910 and SERAS-042-

DTRr1-041210

As part of the ongoing study of sub-slab and indoor air PCE levels, mobilization to the Site by SERAS

personnel took place the week of 07 March 2011.

R2-0008018


OBSERVATIONS AND ACTIVITIES

Permanent Sub-slab Soil Gas Well Installation

A minimum of one permanent sub-slab soil gas probe had been previously installed by REAC personnel

in each of the 13 units to be sampled during the March 2011 mobilization to the Site. The sub-slab soil

gas probes were installed near the center of the basement or at locations chosen by the ERT WAM on site.

Probes were installed flush with the basement slab and capped with a Teflon® plug that was removed

during sampling operations. Probes were installed in accordance with SERAS standard operating

procedure (SOP) #2082, Construction and Installation of Permanent Sub-Slab Soil Gas Wells.

SUMMA® Canister Sub-Slab Soil Gas and Air Sampling: March 2011

On 07 March 2011, SERAS personnel traveled to the Site to conduct sub-slab soil gas, indoor air, and

ambient air sampling at 13 unit locations: 1, 6, 8, 9, 13, 19, 21, 23, 25, 26, 35, 43, and 84. On 08 March

2011, SERAS personnel removed all lifestyle substances (possible chemical sources) from the residences

to be sampled. The residents were then asked to close all windows and doors for 24 hours prior to the

sampling event. Between 09 and 10 March 2011, SERAS personnel collected 13 sub-slab soil gas

samples, 29 indoor air samples, three ambient air samples, and a trip blank for VOC analysis. Refer to

Table 1: Cross References of Unit Numbers and PCE Results, for sample collection information.

With the exception of Unit 84, SERAS personnel collected from each unit, a soil gas sample from each

installed sub-slab probe. A high water table prevented the collection of a soil gas sample from Unit 84.

Indoor air samples were collected from each unit at a location on the first floor and at a location in the

basement. Outdoor ambient samples were collected from locations adjacent to two residential units.

Samples were collected in accordance with SERAS SOP #1704, SUMMA® Canister Sampling, using a

certified clean 6-liter (L) SUMMA® canister and flow controller set to collect a 4 to 5-L time weighted

average (TWA) sample during a 24-hour sampling event. The samples collected in the SUMMA®

canisters were properly documented and delivered to the ERT/SERAS laboratory for analysis. Sub-slab

soil gas and air analyses were performed in accordance with SERAS SOP #1814, GC/MS Analysis of

Sorbent Tubes and Canisters. The target compound list (TCL) included PCE, TCE, vinyl chloride, 1,1-

dichloroethene, trans-1,2-dichloroethene, 1,1-dichloroethane, cis-1,2-dichloroethene, and 1,2-

dichloroethane, as per the ERT WAM’s instruction. A detection limit (DL) of 30 parts per trillion by

volume (pptv) for all sub-slab soil gas samples, indoor air, and ambient air samples was required. Results

are reported in both ppbv and micrograms per cubic meter (µg/m3).

Spatial Data Acquisition/Documentation/Floor Plans

Personnel under the REAC contract had previously logged all locations using Global Positioning System

(GPS) technology and transcribed them to Figure 1: Residential Sample Locations by Unit Number map.

SUMMA® canister number, SUMMA® orifice number, sample date, sample start time, sample end time,

starting orifice flow, sample number, sample locations, and general comments are documented on SERAS

SUMMA® Sampling Worksheets located in Appendix A: SERAS SUMMA® Sampling Worksheets and

Chain of Custody Records.

R2-0008019


RESULTS

SUMMA® Canister Sub-Slab Soil Gas and Air Sampling: March 2011

A study of the indoor air and sub-slab soil gas for 13 previously sampled residential units around the Site

was conducted during the March 2011 mobilization. Homes were re-sampled in an attempt to continue

the documentation of the presence or absence of seasonal and annual fluctuations of PCE in the sub-slab

soil gas and indoor air.

Of the 13 units sampled during this sampling event, March 2011, eight units had sub-slab soil gas

concentrations of PCE above the 11 ppbv (74.6 µg/m3) action limit (Table 1). The sub-slab soil gas PCE

results above the action limit are as follows: Unit 1 SS-1; Sample# 1-042-0061, at 39 ppbv; Unit 8 SS,

Sample# 1-042-0066, at 340 ppbv; Unit 13 SS, Sample# 1-042-0059, at 27 ppbv; Unit 19 SS, Sample# 1-

042-0070, at 82 ppbv; Unit 21 SS, Sample# 1-042-0076, at 46 ppbv; Unit 26 SS, Sample# 1-042-0073, at

170 ppbv; Unit 35 SS, Sample# 1-042-0052, at 29 ppbv; and Unit 43 SS, Sample# 1-042-0046, at 250

ppbv. Due to a high water table, sub-slab soil gas sample collection at Unit 84, Sample# 1-042-0055, was

unsuccessful.

Results from the indoor air samples collected from the basement and the first floor indicate two of the 13

units (Unit 35 and Unit 84) detected PCE above 1.0 ppbv. In the basements; Unit 35 GF, Sample# 1-042-

0053 and Unit 35 GF-Col, Sample# 1-042-0054 had PCE concentrations of 4.6 ppbv and 4.5 ppbv,

respectively; and Unit 84 GF; Sample# 1-042-0056 had a PCE concentration at 1.8 ppbv. The sample

collected on the first floor of Unit 35; Unit 35 FF; Sample# 1-042-0051 had a PCE concentration of 2.1

ppbv.

Discussion of results, reported in both ppbv and µg/m3, for all samples are presented in the April 2011

SERAS Analytical Report (SERAS-042-DAR-040111), found in Appendix B. Tables 2 through 14

present a comparison study of the current and historical PCE data for the units sampled during the March

2011 mobilization.

Meteorological Data

SERAS personnel obtained unedited local climatological data from a certified, permanent station located

at the Dutchess County Airport in Poughkeepsie, NY. Data was provided by the U.S. Department of

Commerce, National Oceanic & Atmospheric Administration’s National Climatic Data Center. One-hour

data averages were collected for the following parameters: wind speed, wind direction, barometric

pressure, temperature, and rainfall. Data were collected to cover periods before and after the March 2011

sampling event and the unedited climatological data are presented in Appendix C: Climatological Data.

Future Activities

No future site mobilizations are scheduled at this time; however, periodic seasonal sampling could be

conducted at the request of the WAM and the RPM.

cc: Central File WA SERAS-042 (with attachment)

Electronic File - I:\Archive\SERAS\042\D\TR\041511

Dennis Miller, REAC Program Manager (cover page only)

R2-0008020


Figure 1 Residential Sample Locations by Unit Number: March 2011 Sampling Event

PA

--0 125 250 500

Legend

~ Unit Locations

U.S. EPA Environmental Response Team Scientific Engineering Response Analytical Service

EP-W-09-031 W.A.# 0-042

750 Feet

1,000

Figure 1 Residential Sample Locations

Shenandoah Road Site East Fishkill, New York

March 2011 Sampling Event

R2-0008021

TABLE 1

Cross Reference Of Unit Numbers and Tetrachloroethene Data Results – March 2011 Event

Shenandoah Road Site

April 2011


Location Sample # Sample Date Result (ppbv) Result (µg/m3)

Unit 1 SS-1 (Stairs) 1-042-0061 3/10/2011 39 270

Unit 1 SS-2 (Furnace) 1-042-0062 3/10/2011 8.5 58

Unit 1 GF 1-042-0063 3/10/2011 0.051 J 0.35 J

Unit 1 FF 1-042-0064 3/10/2011 0.048 0.33

Unit 6 SS 1-042-0079 3/10/2011 9.0 61

Unit 6 GF 1-042-0080 3/10/2011 < 0.030 < 0.20

Unit 6 GF-Col 1-042-0081 3/10/2011 < 0.030 < 0.20

Unit 6 FF 1-042-0082 3/10/2011 < 0.030 < 0.20

Unit 6 AMB 1-042-0083 3/10/2011 < 0.030 < 0.20

Unit 8 SS 1-042-0066 3/10/2011 340 2300

Unit 8 GF 1-042-0067 3/10/2011 0.046 0.31

Unit 8 FF 1-042-0065 3/10/2011 0.16 1.1

Unit 8 AMB 1-042-0068 3/10/2011 < 0.030 < 0.20

Unit 8 AMB-Col 1-042-0069 3/10/2011 < 0.030 < 0.20

Unit 9 SS 1-042-0049 3/10/2011 0.33 2.2

Unit 9 GF 1-042-0048 3/10/2011 < 0.030 < 0.20

Unit 9 FF 1-042-0050 3/10/2011 < 0.030 < 0.20

Unit 13 SS 1-042-0059 3/10/2011 27 190

Unit 13 GF 1-042-0060 3/10/2011 < 0.030 < 0.20

Unit 13 FF 1-042-0058 3/10/2011 < 0.030 < 0.20

Unit 19 SS 1-042-0070 3/10/2011 82 560

Unit 19 GF 1-042-0071 3/10/2011 0.070 0.48

Unit 19 FF 1-042-0072 3/10/2011 0.036 0.24

KEY:

AMB = AMBIENT J = Result is estimated

FF = FIRST FLOOR ppbv = Parts per billion by volume

SS = SUB-SLAB µg/m3 = Microgram per cubic meter

GF = GROUND FLOOR

Col = COLLOCATED

Highlights indicate results at or above the 11 ppbv/74.6 µg/m3 Action Limit.

R2-0008022

TABLE 1 (continued)

Cross Reference Of Unit Numbers and Tetrachloroethene Data Results – March 2011 Event


April 2011


Location Sample # Sample Date Result (ppbv) Result (µg/m3)

Unit 21 SS 1-042-0076 3/10/2011 46 310

Unit 21 GF 1-042-0077 3/10/2011 0.097 0.65

Unit 21 FF 1-042-0078 3/10/2011 0.069 0.47

Unit 23 SS 1-042-0088 3/10/2011 2.8 J 19 J

Unit 23 GF 1-042-0089 3/10/2011 0.58 4.0

Unit 23 FF 1-042-0090 3/10/2011 0.44 3.0

Unit 25 SS 1-042-0084 3/10/2011 9.8 67

Unit 25 GF 1-042-0085 3/10/2011 < 0.030 < 0.20

Unit 25 GF-Col 1-042-0086 3/10/2011 0.060 0.40

Unit 25 FF 1-042-0087 3/10/2011 < 0.030 < 0.20

Unit 26 SS 1-042-0073 3/10/2011 170 1100

Unit 26 GF 1-042-0074 3/10/2011 0.038 0.26

Unit 26 FF 1-042-0075 3/10/2011 0.031 0.21

Unit 35 SS 1-042-0052 3/10/2011 29 190

Unit 35 GF 1-042-0053 3/10/2011 4.6 31

Unit 35 GF-Col 1-042-0054 3/10/2011 4.5 30

Unit 35 FF 1-042-0051 3/10/2011 2.1 14

Unit 43 SS 1-042-0046 3/10/2011 250 1700

Unit 43 GF 1-042-0047 3/10/2011 0.34 2.3

Unit 43 FF 1-042-0045 3/10/2011 0.042 0.29

Unit 84 SS 1-042-0055 3/10/2011 NS NS

Unit 84 GF 1-042-0056 3/10/2011 1.8 12

Unit 84 FF 1-042-0057 3/10/2011 0.64 4.3

KEY:

AMB = AMBIENT J = Result is estimated

FF = FIRST FLOOR ppbv = Parts per billion by volume

SS = SUB-SLAB µg/m3 = Microgram per cubic meter

GF = GROUND FLOOR

Col = COLLOCATED

NS = NO SAMPLE

Highlights indicate results at or above the 11 ppbv/74.6 µg/m3 Action Limit.

Highlights indicate results at or above 1 ppbv/6.78 µg/m3 in the Indoor Air.

R2-0008023

TABLE 2

Comparison of Current and Historical Tetrachloroethene Data-Unit 1


April 2011


Sample Event: Apr-04 May-04

Sample Date: 4/26/2004 5/19/2004

Sample # Results (ppbv) Results (µg/m3) Sample # Results (ppbv) Results (µg/m

3)

17771 / SS-Stairs 60 406 17818 / SS-Stairs 42 285

17772 / SS-Furnace 14 95 17821 / SS-Furnace 10 68

17819/ GF ND ND

17820 / FF ND ND

Sample Event: Feb-05 Mar-07

Sample Date: 2/25/2005 3/27/2007


3)

17971 / SS-Stairs 73 500 41807 / SS-Stairs 52 350

17972 / SS-Furnace 13 91 41808 / SS-Furnace 9.6 65

17970 / GF 0.10 0.71 41809 / GF 0.050 0.34

17968 / FF 0.067 0.46 41810 / FF 0.037 0.25

17969 / FF DUP 0.062 0.42

Sample Event: Mar-08 Mar-09

Sample Date: 3/5/2008 3/26/2009


3)

40725 / SS-Stairs 49 330 076-0030 / SS-Stairs 50 340

40726 / SS-Furnace 9.8 66 076-0031 / SS-Furnace 8.8 60

40727 / GF 0.094 0.64 076-0032 / GF 0.079 0.54

40728 / FF 0.057 0.39 076-0033 / FF 0.068 0.46

ND = Not Detected SS = Sub-slab

ppbv = parts per billion by volume GF = Ground floor

µg/m3 = micrograms per cubic meter FF = First floor

DUP = Duplicate

R2-0008024

TABLE 2 (continued)



April 2011


Sample Event: Jan-10

Mar-11

Sample Date: 1/14/2010

3/10/2011

Sample # Results (ppbv) Results (µg/m3)

Sample #

Results

(ppbv) Results (µg/m3)

1-042-0024 / SS-Stairs 43 290

1-042-0061 / SS-1 (Stairs) 39 270

1-042-0025 / SS-Furnace 7.8 53

1-042-0062 / SS-2 (Furnace) 8.5 58

1-024-0023 / GF 0.057 0.38

1-024-0063 / GF 0.051 J 0.35 J

1-042-0022 / FF 0.043 0.29

1-042-0064 / FF 0.048 0.33

ppbv = parts per billion by volume SS = Sub-slab

µg/m3 = micrograms per cubic meter GF = Ground floor

FF = First floor

J = Result is estimated. The area of the internal standard, chlorobenzene-d5, was above QC limits for

initial and confirmation analyses

R2-0008025

TABLE 3



April 2011



Sample Date: 4/26/2004 5/19/2004


3)

17789 / SS 300 2030 17808 / SS 200 1360

17809 / GF 0.57 3.9

17810 / FF 0.25 1.7


Sample Date: 2/25/2005 3/27/2007


3)

17964 / SS 380 2500 41785 / SS 280 1900

17963 / GF 0.37 2.5 41786 / GF 0.26 1.8

17962 / FF 0.16 1.1 41787 / FF 0.10 0.68

41788 / FF-CO 0.10 0.68

Sample Event: Mar-09 Jan-10

Sample Date: 3/26/2009 1/14/2010


3)

076-0034 / SS 21 140 1-042-0039 / SS 13 85

076-0035 / GF 0.089 0.60 1-042-0040 / GF 0.028 0.19

076-0036 / FF 0.054 0.37 1-042-0041 / GF-CO 0.026 0.18

076-0037 / AMB 0.069 0.47 1-042-0042 / FF 0.024 0.16

076-0038 / AMB-CO 0.063 0.43 1-042-0043 / AMB 0.031 0.21



CO = Collocated FF = First floor

AMB = Ambient

R2-0008026

TABLE 3 (continued)



April 2011


Sample Event: Mar-11



1-042-0079 / SS 9.0 61

1-042-0080 / GF ND ND

1-042-0081 / GF-Col ND ND

1-042-0082 / FF ND ND

1-042-0083 / AMB ND ND




Col = Collocated AMB = Ambient

R2-0008027

TABLE 4



April 2011



Sample Date: 4/26/2004 5/19/2004


3)

17763 / SS 440 2980 17828 / SS 350 2370

17829 / GF 12 81

17830 / FF 4.5 31


Sample Date: 2/25/2005 3/27/2007


3)

17929 / SS 600 4100 41792 / SS 500 3400

17928 / GF 0.39 2.6 41793 / GF 2.0 14

17927 / FF 0.88 6.0 41794 / FF 1.4 9.4


Sample Date: 3/26/2009 1/14/2010


3)

076-0002 / SS 330 2200 1-042-0018 / SS 370 2500

076-0003 / GF 0.20 1.3 1-042-0017 / GF 0.081 0.55

076-0004 / FF 0.14 0.95 1-042-0016 / FF 0.32 2.2

076-0002 / AMB 0.041 0.28 1-042-0014 / AMB 0.020 0.14

076-0006 / AMB-CO 0.056 0.38 1-042-0015 / AMB-CO 0.018 0.12



CO = Collocated FF = First floor

AMB = Ambient

R2-0008028

TABLE 4 (continued)



April 2011





1-042-0066 / SS 340 2300

1-042-0067 / GF 0.046 0.31

1-042-0065 / FF 0.16 1.1

1-042-0068 / AMB ND ND

1-042-0069 / AMB-Col ND ND




Col = Collocated AMB = Ambient

R2-0008029

TABLE 5



April 2011



Sample Date: 4/26/2004 5/19/2004


3)

17753 / SS 17 115 17801 / SS 14 94.9

17802 / GF 0.15 1.0

17803 / FF ND ND


Sample Date: 2/25/2005 3/27/2007


3)

17931 / SS 16 110 41800 / SS 12 82

17932 / GF 0.046 0.31 41801 / GF ND ND

17930 / FF 0.036 0.24 41802 / FF ND ND


Sample Date: 3/5/2008 3/26/2009


3)

40711 / SS 15 100 076-0023 / SS 13 87

40709 / GF 0.072 0.49 076-0024 / GF 0.076 0.52

40710 / FF 0.070 0.47 076-0025 / FF 0.082 0.56




R2-0008030

TABLE 5 (continued)



April 2011



Mar-11


3/10/2011



1-042-0021 / SS 10 69

1-042-0049 / SS 0.33 2.2

1-042-0020 / GF 0.019 0.13

1-042-0048 / GF ND ND

1-042-0019 / FF 0.023 0.16

1-042-0050 / FF ND ND




R2-0008031

TABLE 6



April 2011



Sample Date: 4/26/2004 5/20/2004


3)

17758 / SS 31 210 17825 / SS 31 210

17826 / GF ND ND

17827 / FF 0.41 2.8


Sample Date: 2/25/2005 3/27/2007


3)

17977 / SS 3.2 22 41803 / SS 18 120

17976 / GF - NS NS NS 41804 / GF 0.053 0.36

17974 / FF 0.27 1.8 41805 / FF 0.22 1.5

17975 / AMB ND ND 41806 / AMB ND ND


Sample Date: 3/5/2008 3/26/2009


3)

40719 / SS 19 130 076-0026 / SS 33 220

40720 / GF 0.048 0.32 076-0027 / GF 0.091 0.62

40721 / FF 0.043 0.29 076-0028 / GF-CO 0.087 0.59

076-0029 / FF 0.084 0.57




NS = No sample AMB = Ambient

R2-0008032

TABLE 6 (continued)



April 2011



Mar-11


3/10/2011



1-042-0003 / SS 32 210

1-042-0059 / SS 27 190

1-042-0002 / GF 0.050 0.34

1-042-0060 / GF ND ND

1-042-0001 / FF 0.039 0.26

1-042-0058 / FF ND ND




R2-0008033

TABLE 7



April 2011



Sample Date: 4/26/2004 5/19/2004


3)

17760 / SS 59 400 17814 / SS 59 400

17815 / GF 0.27 1.8

17817 / FF 1.9 12.9

17816 / AMB ND ND


Sample Date: 2/24/2005 3/27/2007


3)

17923 / SS 82 550 41772 / SS 82 560

17921 / GF 0.082 0.55 41773 / GF 0.052 0.36

17922 / FF 0.32 2.2 41773 / FF 0.071 0.48


Sample Date: 3/5/2008 3/26/2009


3)

40716 / SS 83 560 076-0020 / SS 87 590

40717 / GF 0.084 0.57 076-0021 / GF 0.14 0.97

40715 / FF 0.060 0.41 076-0022 / FF 0.24 1.6



ppbv = parts per billion by volume FF = First floor

AMB = Ambient

R2-0008034

TABLE 7 (continued)



April 2011



Mar-11


3/10/2011



1-042-0026 / SS 100 680

1-042-0070 / SS 82 560

1-042-0027 / GF 0.058 0.39

1-042-0071 / GF 0.070 0.48

1-042-0028 / FF 0.049 0.33

1-042-0072 / FF 0.036 0.24



FF = First floor

R2-0008035

TABLE 8



April 2011



Sample Date: 4/26/2004 5/19/2004


3)

17759 / SS 95 644 17811 / SS 4.6 31.2

17812 / GF 0.85 5.8

17813 / FF 0.30 2.0


Sample Date: 2/25/2005 3/27/2007


3)

17938 / SS 83 560 41760 / SS 52* 360*

17937 / GF 0.29 2.0 41761 / GF 0.40 2.7

17936 / FF 0.20 1.4 Unit 21 / GF Collocated 0.40 2.7

41763 / FF 0.21 1.4

41764 / AMB 1 ND ND

41765 / AMB 2 ND ND


Sample Date: 3/5/2008 3/26/2009


3)

40714 / SS 52* 350* 076-0008 / SS 52 350

40712 / GF 0.13 0.86 076-0007 / GF 0.19 1.3

40713 / FF 0.11 0.73 076-0009 / FF 0.14 0.96




* = ppbv to µg/m3 are transferred directly from validated laboratory data. Laboratory results may vary based on rounding methods and

conversion factors.

R2-0008036

TABLE 8 (continued)



April 2011



Mar-11


3/10/2011


Sample #

Results

(ppbv) Results (µg/m3)

1-042-0029 / SS 42 290

1-042-0076 / SS 46 310

1-042-0030 / GF 0.048 0.33

1-042-0077 / GF 0.097 0.65

1-042-0031 / FF 0.075 0.51

1-042-0078 / FF 0.069 0.47



FF = First floor

R2-0008037

TABLE 9



April 2011



Sample Date: 4/26/2004 5/20/2004


3)

17765 / SS 860 5830 17841 / SS 320 2170

17842 /GF 0.71 4.8

17843 / FF 0.56 3.8

17844 / AMB ND ND


Sample Date: 2/24/2005 3/27/2007


3)

17926 / SS 1400 9300 41789 / SS 1200 8000

17924 / GF 0.93 6.3 41790 / GF 0.70 4.8

17925 / FF 0.89 6.0 41791 / FF 0.075 0.51


Sample Date: 3/26/2009 1/14/2010


3)

076-0043 / SS 180 1200 1-0420036 / SS 68 460

076-0044 /GF 0.44 3.0 1-042-0037 / GF* 0.56 3.8

076-0045 / FF 0.46 3.1 1-042-0038 / FF 0.53 3.6




* = Due to possible carryover from previous result, should be used with caution.

AMB = Ambient

R2-0008038

TABLE 9 (continued)



April 2011





1-042-0088 / SS 2.8 J 19 J

1-042-0089 / GF 0.58 4.0

1-042-0090 / FF 0.44 3.0



FF = First floor

J = Result is estimated. The area of the internal standards, bromochloromethane and chlorobenzene-d5, were above QC limits for initial and

replicate analyses

R2-0008039

TABLE 10



April 2011



Sample Date: 4/26/2004 5/20/2004


3)

17780 / SS 21 142 17838 / SS 19 129

17781 Ambient ND ND 17839 / GF 0.24 1.6

17840 / FF ND ND


Sample Date: 2/24/2005 3/27/2007


3)

17910 / SS 15 100 41778 / SS 15 100

17907 / GF ND ND 41779 / GF ND ND

17908 / GF DUP ND ND 41780 / FF ND ND

17909 / FF ND ND


Sample Date: 3/5/2008 3/26/2009


3)

40730 / SS 15 100 076-0039 / SS 14 93

40732 / GF 0.031 0.21 076-0040 / GF 0.071 0.48

40731 / FF 0.036 0.25 076-0041 / GF-CO 0.065 0.44

076-0042 / FF 0.056 0.38




CO = Collocated DUP = Duplicate

R2-0008040

TABLE 10 (continued)



April 2011



Mar-11


3/10/2011



1-042-0032 / SS 10 70

1-042-0084 / SS 9.8 67

1-042-0033 / GF 0.032 0.22

1-042-0085 / GF ND ND

1-042-0034 / GF-CO 0.033 0.22

1-042-0086 / GF-Col 0.060 0.40

1-042-0035 / FF 0.035 0.24

1-042-0087 / FF ND ND




CO or Col = Collocated

R2-0008041

TABLE 11



April 2011


Sample Event: Apr-04

May-04


5/20/2004



17756 / SS 220 1500

17835 / SS 55 370

17836 / GF 0.26 J 1.8 J

17837 / FF ND ND

Sample Event: Feb-05

Mar-11


3/10/2011



17906 / SS 72 490

1-042-0073 / SS 170 1100

17905 / AMB ND ND

1-042-0074 / GF 0.038 0.26

GF / FF No sampling allowed

1-042-0075 / FF 0.031 0.21




AMB = Ambient

J = Result is below the method detection limit and is estimated.

R2-0008042

TABLE 12



April 2011



Sample Date: 2/24/2005 3/21/2006


3)

17917 87 590 44453 / SS 72 490

44452 / GF * *

44451 / FF 4.7 32

44454 / AMB 0.029 U 0.20 U


Sample Date: 3/21/2006 3/9/2007

REAC Collocated SUMMAs


3)

44452R / GF 8.8 59 41795 / SS 73 490

44451R / FF 2.5 17 41796 / GF 1 7.7 52

41797 / GF 2 9.4 64

41798 / FF 3.5 24

41799 / AMB ND ND


Sample Date: 3/26/2009 1/14/2010


3)

076-0010 / SS 29 200 1-042-0007 / SS 50 340

076-0011 / GF 3.2 22 1-042-0005 / GF 6.4 43

076-0012 / GF-CO 3.2 21 1-042-0006 / GF-CO 6.4 43

076-0013 / FF 2.2 15 1-042-0004 / FF 2.8 19




CO = Collocated AMB = Ambient

* = Not analyzed. Sample drew in ambient air during shipping.

R2-0008043




April 2011





1-042-0052 / SS 29 190

1-042-0053 / GF 4.6 31

1-042-0054 / GF-Col 4.5 30

1-042-0051 / FF 2.1 14



Col = Collocated FF = First floor

R2-0008044

TABLE 13



April 2011



Sample Date: 2/25/2005 3/21/2006


3)

17953 430 2900 44458 / SS 380 2600

44456 / GF 0.76 5.1

44455 / FF 0.42 2.8

44457 / AMB ND ND


Sample Date: 3/21/2006 3/27/2007



3)

44456R / GF 0.55 3.7 41769 / SS 370 2500

44455R / FF 0.34 2.3 41770 / GF 0.94 6.4

41771 / FF 0.48 3.2


Sample Date: 3/26/2009 1/14/2010


3)

076-0014 / SS 210 1400 1-042-0010 / SS 260 1700

076-0015 / GF 0.37 2.5 1-042-0009 / GF 0.44 3.0

076-0016 / FF 0.060 0.41 1-042-0008 / FF 0.055 0.37




AMB = Ambient

R2-0008045




April 2011





1-042-0046 / SS 250 1700

1-042-0047 / GF 0.34 2.3

1-042-0045 / FF 0.042 0.29



FF = First floor

R2-0008046

TABLE 14



April 2011


Sample Event: Feb-06

Mar-06


3/21/2006



44448 79 520

44462 / SS 52 360

44463 / GF 0.44 3.0

44464 / FF 0.18 1.2


Mar-07


3/9/2007




41757 / SS 20 130

44463R / GF 0.34 2.3

41753 / GF 1 0.033 0.22

44464R / FF 0.15 1.0

41754 / GF 2 0.034 0.23

41756 / FF ND ND

41755 AMB 1 ND ND

41758 AMB 2 ND ND


Mar-09


3/26/2009



40724 / SS 84 570

40724 / SS 42 280

40723 / GF 1.2 8.3

40723 / GF 0.15 1.0

40722 / FF 0.44 3.0

40722 / FF 0.068 0.46




AMB = Ambient

R2-0008047




April 2011



Mar-11


3/10/2011



1-042-0013 / SS 31 210

1-042-0055 / SS NS NS

1-042-0012 / GF 1.1 7.7

1-042-0056 / GF 1.8 12

1-042-0011 / FF 0.20 1.3

1-042-0057 / FF 0.64 4.3



NS = No sample collected FF = First floor

R2-0008048


APPENDIX A

SUMMA® Sampling Worksheets and Chain of Custody Records


April 2011

R2-0008049


R2-0008050


`

R2-0008051


R2-0008052


R2-0008053


R2-0008054


R2-0008055


R2-0008056


R2-0008057


R2-0008058


R2-0008059


R2-0008060


R2-0008061


R2-0008062


R2-0008063


R2-0008064


R2-0008065


R2-0008066


R2-0008067


R2-0008068


R2-0008069


R2-0008070


R2-0008071


R2-0008072


R2-0008073


R2-0008074


R2-0008075


R2-0008076


R2-0008077


R2-0008078


APPENDIX B

Final Analytical Report


April 2011

R2-0008079

Program Manager

SERAS-042-DAR-040111

ANALYTICAL REPORT

Prepared by LOCKHEED MARTIN

Shenandoah Road Site East Fishkill, NY

April20ll

EPA Work Assignment No. SERAS-042 LOCKHEED MARTIN Work Order SER00042

EPA Contract No. EP-W-09-031

Submitted to D. Mickunas EPA- ERT

109 T.W. Alexander Drive Research Triangle Park, NC 27711

Date

REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full

without the written consent of ERT/SERAS.

Analysis by: ERT/SERAS

Prepared by: Y. Mehra

Validated by: R. V arsolona

R2-0008080

Environmental Response Team/Scientific Engineering, Response and Analytical Services 2890 Woodbridge Avenue, Building 209 Annex Woodbridge NJ 08837

Testing Laboratories Information Detailed Sample Information Introduction Case Narrative Summary of Abbreviations

Section I

Table of Contents

Results of the Analysis for VOC (ppbv) in Air Results of the Analysis for VOC (J.lg/m3

) in Air

Section II

Results of the LCS Analysis for VOC in Air Results of the Duplicate Analysis for VOC in Air

Section Ill

Chains of Custody

Appendices

Appendix A Data for VOC in Air

Appendix A will be furnished on request.




Table l.la Table l.lb

Table 2.1 Table 2.2

W058

R2-0008081


TESTING LA BORA TORIES INFORMATION

Analysis of Volatile Organic Compounds in Air (SERAS SOP# 1814, EPA Method T0-15)

ERT/SERAS Laboratory 2890 Woodbridge Avenue Edison, NJ 08837

fiR. ~

All analyses were performed according to our NELAP-approved quality assurance program. The test results meet the requirements of the current NELAP standards, where applicable, except as noted in the laboratory case narrative provided. Results are intended to be considered in their entirety and apply only to those analyzed and reported herein.

ERT/SERAS Laboratory is certified by the New Jersey Department of Environmental Protection, NELAP Laboratory Certification lD # 12023 for VOC analysis in air by T0-15.


REPORT OF LA BORA TORY ANALYSIS This report shall not be reproduced, except in full


R2-0008082


SERAS Sample#

Rl03003-01 R103003-02 Rl03003-03 R103003-04 R103003-05 R103003-06 Rl03003-07 Rl03003-08 Rl03003-09 Rl03003-l0 Rl03003-11 Rl03003-12 RI03003-l3 Rl03003-14 Rl03003-15 R103003-l6 Rl03003-17 R103003-18 Rl03003-19 R103003-20 Rl03003-21 Rl03003-22 R103003-23 R103003-24 Rl03003-25 Rl03003-26 R103003-27 Rl03003-28 R103003-29 RI03003-30 R103003-31 Rl03003-32 R103003-33 RI03003-34 Rl03003-35 RI03003-36 Rl03003-37 R103003-38 Rl 03003-39 Rl03003-40 Rl03003-4l Rl03003-42 R103003-43 RI03003-44 RI03003-45 Rl03003-46

Detailed Sample Information

Field Sample #

1-042-0045 1-042-0046 1-042-0047 1-042-0048 1-042-0049 1-042-0050 1-042-0051 1-042-0052 1-042-0053 1-042-0054 1-042-0056 1-042-0057 1-042-0058 1-042-0059 l-042-0060 1-042-0061 1-042-0062 1-042-0063 1-042-0064 1-042-0065 1-042-0066 1-042-0067 l-042-0068 l-042-0069 1-042-0070 1-042-0071 l-042-0072 1-042-0073 1-042-0074 1-042-0075 1-042-0076 1-042-0077 1-042-0078 1-042-0079 1-042-0080 1-042-0081 1-042-0082 1-042-0083 1-042-0084 1-042-0085 1-042-0086 1-042-0087 l-042-0088 1-042-0089 1-042-0090 1-042-0091


without the written consent of ERT/SERAS. SERAS-042-DAR-040111

R2-0008083


REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full without the written consent of ERT/SERAS.

Introduction

SERAS personnel, in response to WA# SERAS-042, provided analytical support for environmental samples collected from the Shenandoah Road Site in East Fishkill, New York as described in the following table. The support also included QA/QC, data review and preparation of an analytical report containing analytical and QA/QC results. The samples analyzed at SERAS were treated with procedures consistent with those specified in SERAS SOP #1008, Operation of Sample Refrigeration Units and Sample Receiving, Handling and Storage.

Chain of Custody # Number of

Sample

Sampling Date

Date Received

Date Analyzed

Matrix Analysis/ Method

Laboratory Data Package

SERAS-042-03/10/11-0012 2 03/10/11 03/11/11 03/15/11 through 03/17/11

Air/ Soil Gas

VOC/SERAS SOP #1814

(EPA Method TO-15)

ERT/SERAS W 058 SERAS-042-03/10/11-0013 2 SERAS-042-03/10/11-0014 2 SERAS-042-03/10/11-0015 2 SERAS-042-03/10/11-0016 2 SERAS-042-03/10/11-0017 2* SERAS-042-03/10/11-0018 2 SERAS-042-03/10/11-0019 2 SERAS-042-03/10/11-0020 2 SERAS-042-03/10/11-0021 2 SERAS-042-03/10/11-0022 2 SERAS-042-03/10/11-0023 2 SERAS-042-03/10/11-0024 2 SERAS-042-03/10/11-0025 2 SERAS-042-03/10/11-0026 2 SERAS-042-03/10/11-0027 2 SERAS-042-03/10/11-0028 2 SERAS-042-03/10/11-0029 2 SERAS-042-03/10/11-0030 2 SERAS-042-03/10/11-0031 2 SERAS-042-03/10/11-0032 2 SERAS-042-03/10/11-0033 2 SERAS-042-03/10/11-0034 2 SERAS-042-03/10/11-0035 1 Blank

*At the request of the Task Leader, sample 1-042-0055 was not analyzed.

SERAS-042-DAR-040111 1

R2-0008084




Case Narrative

Sampling was conducted as per the site-specific Quality Assurance Project Plan (QAPP) and analyzed by the analytical methods stated in the QAPP. The laboratory reported the data to three significant figures. Any other representation of the data is the responsibility of the user. All data validation flags have been inserted into the results tables. At the request of the Work Assignment Manager, the laboratory reported results for eight chlorinated compounds. VOCs in Air Package W 058 The area of the internal standard chlorobenzene-d5 was above QC limits on the initial and confirmation analyses for sample 1-042-0063. The tetrachloroethene result for this sample is qualified estimated (J). The area of the internal standards bromochloromethane and chlorobenzene-d5 were above QC limits for sample 1-042-0088 and its replicate. The tetrachloroethene result for this sample is qualified estimated (J). The results presented in this report only relate to the samples analyzed. All results are intended to be considered in their entirety. The Environmental Response Team/Scientific, Engineering, Response and Analytical Services laboratory is not responsible for utilization of less than the complete report.

SERAS-042-DAR-040111 2

R2-0008085




Summary of Abbreviations BFB Bromofluorobenzene C Centigrade CLP Contract Laboratory Program COC Chain of Custody conc concentration cont continued CRDL Contract Required Detection Limit CRQL Contract Required Quantitation Limit D (Surrogate Table) value is from a diluted sample and was not calculated Dioxin Polychlorinated dibenzo-p-dioxins (PCDD) and Polychlorinated dibenzofurans (PCDF) DFTPP Decafluorotriphenylphosphine EMPC Estimated maximum possible concentration GC/MS Gas Chromatography/ Mass Spectrometry IS Internal Standard LCS Laboratory Control Sample LCSD Laboratory Control Sample Duplicate MDA Minimum Detectable Activity MS (BS) Matrix Spike (Blank Spike) MSD (BSD) Matrix Spike Duplicate (Blank Spike Duplicate) MW Molecular Weight NA Not Applicable or Not Available NAD Normalized Absolute Difference NC Not Calculated NR Not Requested/Not Reported NS Not Spiked % D Percent Difference % REC Percent Recovery SOP Standard Operating Procedure ppbv parts per billion by volume ppm parts per million pptv parts per trillion by volume PQL Practical Quantitation Limit PAL Performance Acceptance Limit QA/QC Quality Assurance/Quality Control QL Quantitation Limit RL Reporting Limit RPD Relative Percent Difference RSD Relative Standard Deviation SERAS Scientific, Engineering, Response and Analytical Services SIM Selected Ion Monitoring Sur Surrogate TIC Tentatively Identified Compound TCLP Toxicity Characteristic Leaching Procedure VOC Volatile Organic Compound * Value exceeds the acceptable QC limits m3 cubic meter g gram kg kilogram L liter µg microgram µL microliter mg milligram mL milliliter ng nanogram pg picogram pCi picocurie s sigma

Data Validation Flags

J Value is estimated R Value is unusable J+ Value is estimated high (metals only) U Not detected J- Value is estimated low (metals only) UJ Not detected and RL is estimated N Presumptively present (Aroclors only) Rev. 1/14/09

SERAS-042-DAR-040111 3

R2-0008086

Environmental Response Team/Scientific Engineering, Response and Analytical Services2890 Woodbridge Avenue, Building 209 AnnexWoodbridge NJ 08837

Method SERAS SOP# 1814

SERAS Sample No.Sample NumberSample Location:

Results RL Results RL Results RL Results RL Results RLAnalyte ppbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv

Vinyl Chloride U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300trans-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300cis-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,2-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.0300 0.0362 0.0300Trichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300Tetrachloroethene U 0.0300 U 0.0300 0.0422 0.0300 0.344 0.0300 U 0.0300

Method: SERAS SOP#1814



Vinyl Chloride U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300trans-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300cis-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 0.159 0.03001,2-Dichloroethane U 0.0300 0.224 0.0300 0.448 0.0300 0.436 0.0300 U 0.0300Trichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 0.0894 0.0300Tetrachloroethene U 0.0300 2.12 0.0300 4.59 0.0300 4.46 0.0300 1.78 0.0300

Page 1 of 4

Unit 84 GF

WA# SERAS-042 Shenandoah Road Site

1-042-0050 1-042-0051 1-042-0053 1-042-0054 1-042-0056R103003-06 R103003-07 R103003-09 R103003-10 R103003-11

Table 1.1a Results of the Analysis for VOC (ppbv) in AirWA# SERAS-042 Shenandoah Road Site

Table 1.1a (cont) Results of the Analysis for VOC (ppbv) in Air

Method Blank1-042-0091 1-042-0045 1-042-0047 1-042-00483/15/2011Trip Blank Unit 43 FF Unit 43 GF Unit 9 GF

R103003-46 R103003-01 R103003-03 R103003-04

Unit 9 FF Unit 35 FF Unit 35 GF Unit 35 GF-COL




Vinyl Chloride U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300trans-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300cis-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,2-Dichloroethane 0.140 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300Trichloroethene 0.0546 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300Tetrachloroethene 0.640 0.0300 U 0.0300 U 0.0300 0.0514 J 0.0300 0.0484 0.0300

Unit 84 FF Unit 13 FF Unit 13 GF Unit 1 GF Unit 1 FF


1-042-0057 1-042-0058 1-042-0060 1-042-0063 1-042-0064R103003-12 R103003-13 R103003-15 R103003-18 R103003-19


REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full

without the written consent of ERT/SERAS.SERAS-042-DAR-040111 4

R2-0008087





Vinyl Chloride U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300trans-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300cis-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,2-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300Trichloroethene 0.0493 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300Tetrachloroethene 0.155 0.0300 0.0457 0.0300 U 0.0300 U 0.0300 0.0701 0.0300




Vinyl Chloride U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300trans-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300cis-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,2-Dichloroethane 0.0359 0.0300 U 0.0300 0.0525 0.0300 0.212 0.0300 0.0365 0.0300Trichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300Tetrachloroethene 0.0355 0.0300 U 0.0300 0.0378 0.0300 0.0311 0.0300 0.0965 0.0300

Unit 19 FF3/16/2011

Unit 26 GF Unit 26 FF Unit 21 GF


1-042-0072Method Blank

1-042-0074 1-042-0075 1-042-0077R103003-27 R103003-29 R103003-30 R103003-32

Unit 8 FF Unit 8 GF Unit 8 AMB Unit 8 AMB-COL Unit 19 GF



1-042-0065 1-042-0067 1-042-0068 1-042-0069 1-042-0071R103003-20 R103003-22 R103003-23 R103003-24 R103003-26

Page 2 of 4





Vinyl Chloride U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300trans-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300cis-1,2-Dichloroethene U 0.0300 0.0661 0.0300 U 0.0300 U 0.0300 U 0.03001,2-Dichloroethane 0.104 0.0300 0.0363 0.0300 0.0349 0.0300 0.0301 0.0300 U 0.0300Trichloroethene U 0.0300 0.0631 0.0300 U 0.0300 U 0.0300 U 0.0300Tetrachloroethene 0.0688 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300

Unit 21 FF Unit 6 GF Unit 6 GF-COL Unit 6 FF Unit 6 AMB


1-042-0078 1-042-0080 1-042-0081 1-042-0082 1-042-0083R103003-33 R103003-35 R103003-36 R103003-37 R103003-38




R2-0008088





Vinyl Chloride U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300trans-1,2-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.0300 U 0.0300cis-1,2-Dichloroethene U 0.0300 0.857 0.0300 U 0.0300 0.129 0.0300 0.0537 0.03001,2-Dichloroethane 0.108 0.0300 0.0947 0.0300 0.282 0.0300 U 0.0300 0.0313 0.0300Trichloroethene U 0.0300 0.0663 0.0300 U 0.0300 0.0726 0.0300 U 0.0300Tetrachloroethene U 0.0300 0.0596 0.0300 U 0.0300 0.583 0.0300 0.440 0.0300




Vinyl Chloride U 1.50 U 1.50 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethene U 1.50 U 1.50 U 0.0300 U 0.0300 U 0.0300trans-1,2-Dichloroethene U 1.50 U 1.50 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethane U 1.50 U 1.50 U 0.0300 U 0.0300 U 0.0300cis-1,2-Dichloroethene U 1.50 U 1.50 U 0.0300 U 0.0300 U 0.03001,2-Dichloroethane U 1.50 U 1.50 U 0.0300 U 0.0300 U 0.0300Trichloroethene U 1.50 U 1.50 U 0.0300 U 0.0300 U 0.0300Tetrachloroethene 245 1.50 340 1.50 U 0.0300 0.329 0.0300 28.7 1.50

Unit 43 SS Unit 8 SS 3/17/2011 Unit 9 SS Unit 35 SS


1-042-0046 1-042-0066 Method Blank 1-042-0049 1-042-0052R103003-02 R103003-21 R103003-05 R103003-08

Unit 25 GF Unit 25 GF-COL Unit 25 FF Unit 23 GF Unit 23 FF



1-042-0085 1-042-0086 1-042-0087 1-042-0089 1-042-0090R103003-40 R103003-41 R103003-42 R103003-44 R103003-45

Page 3 of 4





Vinyl Chloride U 0.0300 U 0.0300 U 0.0300 U 0.150 0.0329 0.03001,1-Dichloroethene U 0.0300 U 0.0300 U 0.0300 U 0.150 U 0.0300trans-1,2-Dichloroethene 0.0303 0.0300 U 0.0300 U 0.0300 U 0.150 0.219 0.03001,1-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.150 U 0.0300cis-1,2-Dichloroethene 0.0844 0.0300 U 0.0300 U 0.0300 U 0.150 0.320 0.03001,2-Dichloroethane U 0.0300 U 0.0300 U 0.0300 U 0.150 U 0.0300Trichloroethene 0.163 0.0300 U 0.0300 U 0.0300 U 0.150 0.367 0.0300Tetrachloroethene 27.4 1.50 39.2 1.50 8.54 0.0300 82.3 0.150 167 1.50

Unit 13 SS Unit 1 SS-1 Unit 1 SS-2 Unit 19 SS Unit 26 SS


1-042-0059 1-042-0061 1-042-0062 1-042-0070 1-042-0073R103003-14 R103003-16 R103003-17 R103003-25 R103003-28




R2-0008089




Results RL Results RL Results RL Results RLAnalyte ppbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv

Vinyl Chloride U 0.0750 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethene U 0.0750 U 0.0300 U 0.0300 U 0.0300trans-1,2-Dichloroethene U 0.0750 U 0.0300 U 0.0300 U 0.03001,1-Dichloroethane U 0.0750 U 0.0300 0.0363 0.0300 U 0.0300cis-1,2-Dichloroethene U 0.0750 U 0.0300 U 0.0300 U 0.03001,2-Dichloroethane U 0.0750 U 0.0300 U 0.0300 U 0.0300Trichloroethene 0.107 0.0750 U 0.0300 U 0.0300 U 0.0300Tetrachloroethene 45.5 0.0750 9.00 0.0300 9.82 0.0300 2.79 J 0.0300

1-042-0076 1-042-0079 1-042-0084 1-042-0088Unit 21 SS Unit 6 SS Unit 25 SS Unit 23 SS

R103003-31 R103003-34 R103003-39 R103003-43

WA# SERAS-042 Shenandoah Road SiteTable 1.1a (cont) Results of the Analysis for VOC (ppbv) in Air

Page 4 of 4



R2-0008090


Method SERAS SOP#1814


Results RL Results RL Results RL Results RL Results RLAnalyte µg/m3 µg/m3 µg/m3 µg/m3 µg/m3 µg/m3 µg/m3 µg/m3 µg/m3 µg/m3

Vinyl Chloride U 0.0767 U 0.0767 U 0.0767 U 0.0767 U 0.07671,1-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.119trans-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,1-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.121 U 0.121cis-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,2-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.121 0.146 0.121Trichloroethene U 0.161 U 0.161 U 0.161 U 0.161 U 0.161Tetrachloroethene U 0.203 U 0.203 0.286 0.203 2.33 0.203 U 0.203




Vinyl Chloride U 0.0767 U 0.0767 U 0.0767 U 0.0767 U 0.07671,1-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.119trans-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,1-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.121 U 0.121cis-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 0.630 0.1191,2-Dichloroethane U 0.121 0.908 0.121 1.81 0.121 1.77 0.121 U 0.121Trichloroethene U 0.161 U 0.161 U 0.161 U 0.161 0.480 0.161Tetrachloroethene U 0.203 14.4 0.203 31.1 0.203 30.2 0.203 12.1 0.203

R103003-06 R103003-07 R103003-09 R103003-10 R103003-11

Unit 9 FF Unit 35 FF Unit 35 GF Unit 35 GF-COL Unit 84 GF1-042-0050 1-042-0051 1-042-0053 1-042-0054 1-042-0056

Table 1.1b Results of the Analysis for VOC (µg/m3) in AirWA# SERAS-042 Shenandoah Road Site

Table 1.1b (cont) Results of the Analysis for VOC (µg/m3) in AirWA# SERAS-042 Shenandoah Road Site

Method Blank1-042-0091 1-042-0045 1-042-0047 1-042-00483/15/2011Trip Blank Unit 43 FF Unit 43 GF Unit 9 GF

R103003-46 R103003-01 R103003-03 R103003-04

Page 1 of 4




Vinyl Chloride U 0.0767 U 0.0767 U 0.0767 U 0.0767 U 0.07671,1-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.119trans-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,1-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.121 U 0.121cis-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,2-Dichloroethane 0.568 0.121 U 0.121 U 0.121 U 0.121 U 0.121Trichloroethene 0.293 0.161 U 0.161 U 0.161 U 0.161 U 0.161Tetrachloroethene 4.34 0.203 U 0.203 U 0.203 0.348 J 0.203 0.328 0.203

R103003-12 R103003-13 R103003-15 R103003-18 R103003-19

Table 1.1b (cont) Results of the Analysis for VOC (µg/m3) in Air

Unit 1 GF Unit 1 FF


1-042-0057 1-042-0058 1-042-0060 1-042-0063 1-042-0064Unit 84 FF Unit 13 FF Unit 13 GF



R2-0008091





Vinyl Chloride U 0.0767 U 0.0767 U 0.0767 U 0.0767 U 0.07671,1-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.119trans-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,1-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.121 U 0.121cis-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,2-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.121 U 0.121Trichloroethene 0.265 0.161 U 0.161 U 0.161 U 0.161 U 0.161Tetrachloroethene 1.05 0.203 0.310 0.203 U 0.203 U 0.203 0.475 0.203




Vinyl Chloride U 0.0767 U 0.0767 U 0.0767 U 0.0767 U 0.07671,1-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.119trans-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,1-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.121 U 0.121cis-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,2-Dichloroethane 0.145 0.121 U 0.121 0.213 0.121 0.859 0.121 0.148 0.121Trichloroethene U 0.161 U 0.161 U 0.161 U 0.161 U 0.161Tetrachloroethene 0.241 0.203 U 0.203 0.256 0.203 0.211 0.203 0.654 0.203

Unit 19 FF3/16/2011

Unit 26 GF Unit 26 FF Unit 21 GF


1-042-0072Method Blank

1-042-0074 1-042-0075 1-042-0077R103003-27 R103003-29 R103003-30 R103003-32

Unit 8 FF Unit 8 GF Unit 8 AMB Unit 8 AMB-COL Unit 19 GF



1-042-0065 1-042-0067 1-042-0068 1-042-0069 1-042-0071R103003-20 R103003-22 R103003-23 R103003-24 R103003-26

Page 2 of 4





Vinyl Chloride U 0.0767 U 0.0767 U 0.0767 U 0.0767 U 0.07671,1-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.119trans-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,1-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.121 U 0.121cis-1,2-Dichloroethene U 0.119 0.262 0.119 U 0.119 U 0.119 U 0.1191,2-Dichloroethane 0.419 0.121 0.147 0.121 0.141 0.121 0.122 0.121 U 0.121Trichloroethene U 0.161 0.339 0.161 U 0.161 U 0.161 U 0.161Tetrachloroethene 0.466 0.203 U 0.203 U 0.203 U 0.203 U 0.203

Unit 21 FF Unit 6 GF Unit 6 GF-COL Unit 6 FF Unit 6 AMB


1-042-0078 1-042-0080 1-042-0081 1-042-0082 1-042-0083R103003-33 R103003-35 R103003-36 R103003-37 R103003-38




R2-0008092





Vinyl Chloride U 0.0767 U 0.0767 U 0.0767 U 0.0767 U 0.07671,1-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.119trans-1,2-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.119 U 0.1191,1-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.121 U 0.121cis-1,2-Dichloroethene U 0.119 3.40 0.119 U 0.119 0.512 0.119 0.213 0.1191,2-Dichloroethane 0.439 0.121 0.383 0.121 1.14 0.121 U 0.121 0.127 0.121Trichloroethene U 0.161 0.356 0.161 U 0.161 0.390 0.161 U 0.161Tetrachloroethene U 0.203 0.404 0.203 U 0.203 3.96 0.203 2.98 0.203




Vinyl Chloride U 3.83 U 3.83 U 0.0767 U 0.0767 U 0.07671,1-Dichloroethene U 5.95 U 5.95 U 0.119 U 0.119 U 0.119trans-1,2-Dichloroethene U 5.95 U 5.95 U 0.119 U 0.119 U 0.1191,1-Dichloroethane U 6.07 U 6.07 U 0.121 U 0.121 U 0.121cis-1,2-Dichloroethene U 5.95 U 5.95 U 0.119 U 0.119 U 0.1191,2-Dichloroethane U 6.07 U 6.07 U 0.121 U 0.121 U 0.121Trichloroethene U 8.06 U 8.06 U 0.161 U 0.161 U 0.161Tetrachloroethene 1660 10.2 2310 10.2 U 0.203 2.23 0.203 194 10.2

Unit 43 SS Unit 8 SS 3/17/2011 Unit 9 SS Unit 35 SS


1-042-0046 1-042-0066 Method Blank 1-042-0049 1-042-0052R103003-02 R103003-21 R103003-05 R103003-08

Unit 25 GF Unit 25 GF-COL Unit 25 FF Unit 23 GF Unit 23 FF



1-042-0085 1-042-0086 1-042-0087 1-042-0089 1-042-0090R103003-40 R103003-41 R103003-42 R103003-44 R103003-45

Page 3 of 4





Vinyl Chloride U 0.0767 U 0.0767 U 0.0767 U 0.383 0.0840 0.07671,1-Dichloroethene U 0.119 U 0.119 U 0.119 U 0.595 U 0.119trans-1,2-Dichloroethene 0.120 0.119 U 0.119 U 0.119 U 0.595 0.869 0.1191,1-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.607 U 0.121cis-1,2-Dichloroethene 0.334 0.119 U 0.119 U 0.119 U 0.595 1.27 0.1191,2-Dichloroethane U 0.121 U 0.121 U 0.121 U 0.607 U 0.121Trichloroethene 0.874 0.161 U 0.161 U 0.161 U 0.806 1.97 0.161Tetrachloroethene 186 10.2 266 10.2 57.9 0.203 558 1.02 1130 10.2

Unit 13 SS Unit 1 SS-1 Unit 1 SS-2 Unit 19 SS Unit 26 SS


1-042-0059 1-042-0061 1-042-0062 1-042-0070 1-042-0073R103003-14 R103003-16 R103003-17 R103003-25 R103003-28




R2-0008093




Results RL Results RL Results RL Results RLAnalyte µg/m3 µg/m3 µg/m3 µg/m3 µg/m3 µg/m3 µg/m3 µg/m3

Vinyl Chloride U 0.192 U 0.0767 U 0.0767 U 0.07671,1-Dichloroethene U 0.297 U 0.119 U 0.119 U 0.119trans-1,2-Dichloroethene U 0.297 U 0.119 U 0.119 U 0.1191,1-Dichloroethane U 0.304 U 0.121 0.147 0.121 U 0.121cis-1,2-Dichloroethene U 0.297 U 0.119 U 0.119 U 0.1191,2-Dichloroethane U 0.304 U 0.121 U 0.121 U 0.121Trichloroethene 0.576 0.403 U 0.161 U 0.161 U 0.161Tetrachloroethene 309 0.509 61.0 0.203 66.6 0.203 18.9 J 0.203

1-042-0076 1-042-0079 1-042-0084 1-042-0088Unit 21 SS Unit 6 SS Unit 25 SS Unit 23 SS

R103003-31 R103003-34 R103003-39 R103003-43

WA# SERAS-042 Shenandoah Road SiteTable 1.1b (cont) Results of the Analysis for VOC (µg/m3) in Air

Page 4 of 4



R2-0008094


Page 1 of 1LCS:03/15/11

LCS LCSSpike Amount Recovered

Analyte ppbv ppbv % Recovery

Vinyl Chloride 1.03 0.985 95 57 - 1171,1-Dichloroethene 1.05 0.940 90 54 - 120trans-1,2-Dichloroethene 1.05 0.920 87 60 - 1201,1-Dichloroethane 1.05 1.01 95 68 - 125cis-1,2-Dichloroethene 1.05 0.962 92 62 - 1231,2-Dichloroethane 1.05 1.00 94 58 - 131Trichloroethene 1.04 0.981 94 73 - 130Tetrachloroethene 1.04 0.970 92 68 - 128

LCS:03/16/11



Vinyl Chloride 1.03 1.08 105 57 - 1171,1-Dichloroethene 1.05 1.06 101 54 - 120trans-1,2-Dichloroethene 1.05 1.03 98 60 - 1201,1-Dichloroethane 1.05 1.08 103 68 - 125cis-1,2-Dichloroethene 1.05 1.05 100 62 - 123

Table 2.1 Results of the LCS Analysis for VOC in AirWA# SERAS-042 Shenandoah Road Site

QC Limits % Recovery

QC Limits % Recovery

1,2-Dichloroethane 1.05 1.07 102 58 - 131Trichloroethene 1.04 1.04 100 73 - 130Tetrachloroethene 1.04 1.03 99 68 - 128

LCS:03/17/11



Vinyl Chloride 1.03 1.05 102 57 - 1171,1-Dichloroethene 1.05 0.986 94 54 - 120trans-1,2-Dichloroethene 1.05 0.969 92 60 - 1201,1-Dichloroethane 1.05 1.08 103 68 - 125cis-1,2-Dichloroethene 1.05 1.03 98 62 - 1231,2-Dichloroethane 1.05 1.06 101 58 - 131Trichloroethene 1.04 1.05 101 73 - 130Tetrachloroethene 1.04 1.03 99 68 - 128

% RecoveryQC Limits



R2-0008095


Page 1 of 2Sample Number 1-042-0045

Initial Analysis Duplicate AnalysisResults Results QC Limit

Analyte ppbv ppbv RPD RPD≤*

Vinyl Chloride U U NC 251,1-Dichloroethene U U NC 25trans-1,2-Dichloroethene U U NC 251,1-Dichloroethane U U NC 25cis-1,2-Dichloroethene U U NC 251,2-Dichloroethane U U NC 25Trichloroethene U U NC 25Tetrachloroethene 0.0422 0.0419 1 25

Sample Number 1-042-0072



Vinyl Chloride U U NC 251,1-Dichloroethene U U NC 25trans-1,2-Dichloroethene U U NC 251 1-Dichloroethane U U NC 25

Table 2.2 Results of the Duplicate Analysis for VOC in AirWA# SERAS-042 Shenandoah Road Site

1,1-Dichloroethane U U NC 25cis-1,2-Dichloroethene U U NC 251,2-Dichloroethane 0.0359 0.0331 8 25Trichloroethene U U NC 25Tetrachloroethene 0.0355 0.0336 5 25




Vinyl Chloride U U NC 251,1-Dichloroethene U U NC 25trans-1,2-Dichloroethene U U NC 251,1-Dichloroethane U U NC 25cis-1,2-Dichloroethene U U NC 251,2-Dichloroethane 0.0525 0.0566 8 25Trichloroethene U U NC 25Tetrachloroethene 0.0378 0.0481 24 25



R2-0008096


Page 2 of 2




Vinyl Chloride U U NC 251,1-Dichloroethene U U NC 25trans-1,2-Dichloroethene U U NC 251,1-Dichloroethane U U NC 25cis-1,2-Dichloroethene 0.0537 0.0577 7 251,2-Dichloroethane 0.0313 0.0359 14 25Trichloroethene U U NC 25Tetrachloroethene 0.440 0.460 4 25




Vinyl Chloride U U NC 251,1-Dichloroethene U U NC 25trans-1,2-Dichloroethene U U NC 251 1-Dichloroethane U U NC 25

WA# SERAS-042 Shenandoah Road SiteTable 2.2 (cont) Results of the Duplicate Analysis for VOC in Air

1,1-Dichloroethane U U NC 25cis-1,2-Dichloroethene U U NC 251,2-Dichloroethane U U NC 25Trichloroethene U U NC 25Tetrachloroethene 245 261 6 25




Vinyl Chloride U U NC 251,1-Dichloroethene U U NC 25trans-1,2-Dichloroethene U U NC 251,1-Dichloroethane U U NC 25cis-1,2-Dichloroethene U U NC 251,2-Dichloroethane U U NC 25Trichloroethene U U NC 25Tetrachloroethene 2.79 2.53 10 25



R2-0008097

~

(f) ERT m ~ SERAS, Edison, NJ

(f) EPA Contract Number: EP-W-09-031 I

0

~(11fRt o3oos )> Lab i# Sample i# ;p 0

""" 0 ~

~

1-042-0045

1-042-0046

Location

Unit43 FF

Unit43 SS

Analyses Matrix

T0-15 (VOAs) Air

T0-15 (VOAs) Soil Gas ---

CHAIN OF CUSTODY RECORD

S1te i#: SERAS-042

Contact Name: D McCall

Contact Phone: 609-865-6414

No: SERAS-042-03/10/11-0012

Collected Numb Cont

3110/2011 1 __ .,. ___ 3110/2011 1

-y --

Lab: SERAS Lab

Lab Phone: (732) 321-4252

Container Pntservative SUMMA i# OrlficeiD Stop Volume Vol

Summa Canister~ None

Summa Canister-None

000219 - 013929

1000064 013799

Pntssure Units

-5 4.8 Liters -- --5 5.22 Liters

--- -- ... --~---- ---------

~---~

- ·-------------- ---~-

-- -+---..... ----------

Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP #1814. Detection limit of 0.030 ppbv.

SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY i#

Items/Reason ·nquished by Date

JJi )HA Received by Date Time Items/Reason Relinquished By Date Received by Date

IS : c<dlllLA,.,/'ts.\~~Sit~/11 ~ ?f.~J,; Time

(~

--- ---- -.,.--....-- ----- ------ -·- ------------ -----

------------

R2-0008098

(j) m ~ (j)

I 0 ~ tV

6 )> :::0 6 ~ 0 ..... ...... ......

Page1~ ERT

SERAS, Edison, NJ

EPA Contract Number: EP-W-09-031


Site #: SERAS-042



No: SERAS-042-03/1 0/11-0013

Lab: SERAS Lab

Lab Phone: (732) 321-4252

Wo1f R I o 3__oo 3 Lab # Sample I# Location Analyses Matrix Collected Numb Container

Cont - Preservative ' SUMMA I# OrlflceiD - Stop Volume Vol l

Q_ 3 1-042-0047 • Unit 43 GF

0:1 1-042-0048 Unit 9 GF

T0-15 (VOAs) Air ~ __,_

T0-15 (VOAs) Air

3/10/2011

3/10/201 1

1 Summa Canister

1Summa Canister


Items/Reason Date Received by Date~ime Items/Reason

None

None

Pressure Units -----000201~13910 - - --

-5 4.78 Liters -~000265--o13918 -- -6.5 4M Liters

_ __._-


CHAIN OF CUSTODY I

~

-l

Relinquished By Date~ b"'-y-..--Date Time

~ltf/1~ !f'f{tc '~ ----~1

R2-0008099

(/) m ~ (/)

6 ~ N

6 )> ::u 6 ~ 0 ..... .....

Page 1

ERT

SERAS, Ed1son, NJ


wa#f_[o3C03 Lab ## Sample ## ~Location

1-042-0049 ~Unit 9 SS

1-042-0050 Unit 9 FF

-~------~-

----~---~

Analyses Matrix

T0-15 (VOAs) Soil Gas

T0-15 (VOAs) Air


Site ##: SERAS-042



Collectad

3110/2011

3110/2011

Numb Container Cont

- 1- Summa Canister

Summa Canister ---

Pre .. rvative SUMMA##

None 000233

None 000271

No: SERAS-042~3/1 0/11-0014

Lab. SERAS Lab

Lab Phone. (732) 321-4252

OrlflceiD Stop Volume Vol Pressure Unlta

t

j 013958 0 4.85 Liters

013782 -6.5 4 .83 Liters

- --- .,..

r

._ .... L ~~-: rJ e _7- -- -----------=-.--}-~ ~------------ _ _.___ ------

Spec1allnstructions: T0-15 for requested 8 compounds as per SERAS SOP ##1814. Detection limit of 0.030 ppbv


CHAIN OF CUSTODY II

Date Received by Date Time Items/Reason Relinquished By Date Date T1me

~~ ------ --

3/11//1 ~!~ll}lftuJy~s -¥~7 .5/l'fJII ..,-

----~·

R2-0008100

(J) m ~ (J)

6 ~ 1\)

6 )> :;u 6 ~ 0 ...... ...... ......

0 ..... Q)

Page 1

ERT

SERAS, Edison, NJ

EPA Contract Number: EP-W-OS-031


Site#: SERAS-042



wo1FR 103co3 Lab # Sample # Location Analyaea Matrix Collected Numb Container

Cont

1-042-0051 Unit 35 FF T0-15 (VOAs) Air -t-

3/10/2011 1 Summa Canister

1-042-0052 Unit35SS-T0~5(V0As) SoiiGas 3/10/2011 1 Summa Canister

-~ ----------


R linquished by Date Received by -----~-- ------~---------_, __ _

CJt ~~·I··~ Date Time Items/Reason

$/II/I/ IS;CXJ 111!_/HMiy s I j

---- ------ - -- - - .... --~- -- --

No: SERAS-042-03/1 0/11-0015

Preservative SUMMA # Orlfic.eiD

None 000239 ~3924 None +000082 013788

lab: SERAS lab

lab Phone: (732) 321-4252

Stop Volume Vol Preaaure Unita

-4 4.42 Liters 0 4.98 - Liters

----


CHAIN OF CUSTODY#

Relinquished By Date

~ Date Time -

~- _'5/lf(//1 -r.t·~f,. (~ /

-- - -

R2-0008101

ERT

SERAS, EdiSOn, NJ


wo#(i(I0~3 Lab II Sample II Location

1-042-0053 - Unit 35 GF

1-042-0054 Unit 35 GF· Col

Analyses Matrix

T0-15 (VOAs) Air

T0-15 (VOAs) Air


Site II: SERAS-042



Collected Numb Container Cont

3/10/2011 1 Summa Canister + --

3/1012011 Summa Canister

---

... -

Preservative SUMMA #I

None 000236

None 000179

~ ---

No: SERAS-042-03/10/11-0016

OrlflceiD

013765

013908

Lab SERAS Lab

lab Phone· (732) 321-4252

Stop Volume Vol Pressure Units

-6 4.83 Liters

-6.5 4.54 Liters

-.------+------

- --+



CHAIN OF CUSTODY I

Date Received by Date Time Items/Reason Relinquished By ----

3/lt 1ft

R2-0008102

ERT

SERAS, Edison, NJ


wc%R I 03_oo3


Site #: SERAS-042

Contact Name: 0 McCall

Contact Phone: 609-865-641 4

No: SERAS-042-03/10/11-0017

Lab: SERAS Lab

Lab Phone: (732) 321-4252

- - r Lab # Sample # l ocation Analyses Matrix Collected Numb Container Pre .. rvatlve SUMMA# OrlflceiD Stop Volume y()'l" ~

Cont Preuure Units ~- ~ 'f. --.2:_042-0055_ Unit 84 SS

1-042-0056 Unit 84 GF

T0-15 (VOAs) ~Soil Gas 3/10/2011 1 Summa CanisterNone T0-15 (VOAs) Air --3110/2011~-.,...-1 -=s,-umma CanisterNone

__ oooo~ 013907

000170 1013952

~ - -29.5 ...., --

-6

--------- ---------------------------------------.-----r---, -----

-- ----- --.--------

- --t--

-----------SAMPLES TRANSFERRED FROM

Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP #1814. Detection limit of 0.030 ppbv. CHAIN OF CUSTODY#

'*- ~ M± ~~a.- 0~~ ~~~ 1-_f>~ - ooss-. SwmMtt tn.\IIM ~a.\lt -~~r__.i ..... ~~w~st,_,&..__ __ -~ -=-~ - -

r:---4.7 Liters

4.86 Liters

----.

----------,--- -----

R2-0008103

ERT

SERAS, Ed1son, NJ


Wo:tt=-_K I o 300 3 Lab #I Sample #I ' Location

1-042-0057 Unit 84 FF __.___ 1-042-0058 Unit 13 FF

AnalyHs Matrix

T0-15 (VOAs) Air

T0-15 0/0As) Air

---------+--------~-----

------------


Site #1: SERAS-042



No: SERAS-042-03/1 0/11-0018

Collected

3/10/2011

3/1012011

Numb Contelner Coot

1 Summa Canister

Preservative SUMMA #I T OrlflceiD

None----000017

Summa Can1ster None 000194

013954

013964

~--- .-- - -- ------------------ ---

------ --------

Lab SERAS Lab

Lab Phone: (732) 321-4252


0 4.69 L1ters

-6 5.02 Lrters ~~~

-------~----- - - -- r

- .. - -- - -+-

- -~

Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP 11814. Detection limit of 0 030 ppbv.


CHAIN OF CUSTODY II

Date Received by Date Items/Reason Relinquished By ------- --------~ Time Date

S/11/lt 15": 00

Time

(rbO

R2-0008104

0 N N

Page 1

ERT

SERAS, Ed1son, NJ


Wo#=RlD.~3 Lab II Sample II Location

1-042-0059 Unit 13 SS

1-042-0060 Unit 13 GF

Analyse• Matrix


T0-15 (VOAs) Air


S1te #: SERAS-042



Collected

3/10/2011

3110/2011

Numb Container Cont

1 Summa Canister

Summa Can1ster

No: SERAS-042-03/1 0/11-0019

Lab SERAS Lab

Lab Phone· (732) 321-4252

Preservative SUMMA II OrlflceiD Stop Volume Vol

None

None

000261

000087

013777

013800

Pressure Units

-6

-7

..

5.32 Liters

4.75 Liters

-----~

- ,----

Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP 111814. Detection limit of 0 030 ppbv.

Items/Reason Date Received by Date Time Items/Reason -----

.3/ "I I I ts:oo

,-----

-r -1_


CHAIN OF CUSTODY II

Relinquished By Date~ Date

·3/1'1/ 1 ( ·~r-==- ~ ~{ r({/l( Time

R2-0008105

en m ~ en ~ 1\.)

6 )> :::u 6 .,. 0 ...... ...... ......

0 N w

Page 1

ERT CHAIN OF CUSTODY RECORD

Site #: SERAS-042



No: SERAS-042-03/1 0/11-0020 SERAS, Edison, NJ


wo1FRfo3CXJ3 Lab t# Sample # Location Analyses Matrix Collected

iJo 1-042-0061 Unit 1 SS-1 __ T0-15 (VOAsJ__Soil ~ 3/10/2011 __

12 . 1-042-00S~it 1 SS-2 _ T0-15(VOAs)~iiGa~/10/20_11 _ _,_

------

----'--- --- - - I

Numb Container Preservative SUMMA t# OrlflceiD Cont

1 Summa Canister--None 000216 013923

Summa Canister r None 000193 013936

-- -- ------,--

~--- -----

Lab: SERAS Lab

Lab Phone: (732) 321-4252


-6 4.96 Liters

-6 4.67 Liters

---~



CHAIN OF CUSTODY t#

Items/Reason Date - R eceived by-- Date-- Time Items/Reason Relinquished By Date

WJ__)~~ ·~ :S/11/11 15: ~o _ffii/fiM!y.5/L~) f<l I

-- -- - - - --- -- -·~ ----- -------------- --- ----

------------------------ -----

Date Time

3/,'f {J{ ~1100 -- -1!-1/J . -

R2-0008106

en m ~ en ' 0 ~ N I

0 )> ::u ' 0 ~ 0 ...... ~

~

Page 1

ERT

SERAS, Ed1son, NJ


~{03C03 Lab. Sample• Location Analyses Matrix

1-042-0063 Unit1 GF T0-15 (VOAs) Air

1-042-0064 Unit 1 FF T0-15 (VOAs) Air


S1te _,: SERAS-042



Collected

3/1012011

3110/2011 t-

Numb Container Cont

1 Summa Canister

1 Summa Canister

No: SERAS-042-03/1 0/11-0021

Preservative SUMMA • OrlflceiD

None

None

000141

001138

013957

013769

Lab SERAS Lab

Lab Phone· (732) 321-4252

Stop Pressure

-5.5

-9

Volume Vol Units

4.81 Liters

4.24 L1ters

-----------~-- --- -

-----...,---

Spec1allnstructions: T0-15 for requested 8 compounds as per SERAS SOP •1814. Detection limit of 0.030 ppbv

Date Received by Date Time Items/Reason ----

~~D~~ 5/lt/11

+

-+--


CHAIN OF CUSTODY _,

Relinquished By Date

.. .....

R2-0008107

(/) m ~ (/)

6 ~

"' 6 )> :::0 I

0

~ ...... ....... ......

0 N CJI

Page 1

ERT

SERAS Ed1son, NJ


vvo#Rra~3 Lab il Sample il ~Location

:2 C) 1-042-0065 Unit 8 FF

~ \ 1-042-0066- Unit 8 SS

Analyaea Matrix

T0-15 (VOAs) Air



S1te il: SERAS-042



Collected

3/10/2011

311012011

Numb Container Cont

'--1 Summa Canister ---1 Summa Can1ster

"t -----

No: SERAS-042~3/1 0/11-0022

Preservative SUMMA il OrlflceiD

None

None

000144

000186

013779

013949 ~

Lab SERAS Lab

Lab Phone: (732) 321-4252

Stop Volume Vol Preuure Units

-4.5 4 75 L1ters

-7 4.75 Liters

------- ~~-,..

... -

Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP i#1814. Detection limrt of 0.030 ppbv.

Items/Reason Re nquished by Date Received by Date Time Items/Reason -----

At OAT --<C--,,~t.W9. ,!,\1·1~ S/lljj(

+ -


CHAIN OF CUSTODY i1

RelirlQUlshed By

R2-0008108

(/) m ~ (/)

6 ~ N

6 )> ::0 6 ~ 0 _.

r Page1 ~

ERT

SERAS, Edison, NJ


wcr#= R 1 o 3CD 3 Lab # Sample #

1-042-0067

1-042-0068

Location

Unit 8 GF

Unit 8AMB

AnalyHs Matrix

T0-15 (VOAs) Air

T0-15 (VOAs) Air


Site#: SERAS-042


Contact Phone· 609-865-6414

Collect.d Numb Container Cont

3/10/2011 1 Summa Canister +

3/10/2011 Summa Canister --+

___ ...

Special instructions: T0-15 for requested 8 compounds as per srfAA.s SOP #1814. Detection limit of 0.030 ppbv.

Items/Reason Date Received by Date Time Items/Reason

~~I h -¥'J1111jf>y 3/IJ I II

No: SERAS-042-03/1 0/11-0023

Lab: SERAS Lab

Lab Phone: (732) 321-4252

PreHrvative SUMMA I OrlflceiD Stop Volume Vol Pressure Units

None 001128 ----:

None 000010

013797

013931

~ ---~

-7.5

-6


CHAIN OF CUSTODY #

4.6 L1ters

R2-0008109

ERT

SERAS, Edison, NJ


Lab * Sample * Location

1-042-0069 Untt 8 AMBCol

1-042-0070 Unit 19 SS

AnalyHa Matrix

T0-15 (VOAs) Air



Site II: SERAS-042


Contact Phone· 609-865-6414

Collactad

3/10/2011

3/10/2011

Numb Container Cont

1 Summa Canister

Summa Canister

No: SERAS-042-03/1 0/11-0024

Lab: SERAS Lab

Lab Phone: (732) 321-4252

PraHrvativa SUMMA I OrlfieeiD Stop Volume Vol Pressure Unita

None 000068 013785 4.71 Ltters

None 000118 _,_013801 - -2.5 4.85 Liters- ·

--------------------,--

r •

i-

SAMPLES TRANSFERRED FROM -----Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP #1814. Detection limit of 0.030 ppbv. CHAIN OF CUSTODY I

Items/Reason Date Time

_2(r ~Jt( /~

R2-0008110

0 1\) co

Page 1

ERT

SERAS, Edison, NJ


wc/=II=K to 3:XJ 3 Lab # Sample # Location

1-042-0071

1-042-0072

Unit 19 GF

Unit 19 FF

T0-15 (VOAs) Air

T0-15 (VOAs) Air


Site #: SERAS-042



No: SERAS-042-03/1 0/11-0025

Lab: SERAS Lab

Lab Phone: (732) 321-4252

Collect.d Numb Cont

Cont.iner Preservative SUMMA # OrtflceiD Stop Volume Vol

3110/2011

3110/2011

1

1

Summa Canister None

Summa Canister None

Pressure Units

0011~13956 -11 .5 4.71 liters --000253 -ti13774~- -7.5 4.7- liters

- --- ------------.,----------r-------~---~ --------~--------------------------------------------

------ --- - -

------~

=r ---+-- ___ __._ - -t- -

I



CHAIN OF CUSTODY #

-·

Received by Date Time --Items/Reason Date Time -~-~------ --~- --------------------- --~----~--------~~~q~~-~---

Items/Reason

~~~"'-< ~+~_,___~D~ ~ ~Jo/ll JS:I'Jo fl11/~_!p~ ~~~~'!!I!J.L~~--~ - --41"-ft Ltri15

R2-0008111

(/) m ~ (/) I

0 ~ N

6 )> ::0 6 ~ 0 ~ ...... ~

Page 1

ERT

SERAS, Edison, NJ


wo=tt:rK 1 o 3CJ:J 3 Lab # Sample # Location

;) '&' ~2-00~ Unit 26 SS

d. "J 1-042-007 4 Unit 26 GF ~- ___,_

----------

Analyses Matrix


T0-15 (VOAs) - Air


Site#: SERAS-042



No: SERAS-042..03/1 0/11..0026

Collected

3/10/2011

3/1012011

Numb Container Preservative SUMMA #I OriflceiD Cont

1 Summa Canister~ None 000~ 013768

Summa Canister None ---000200 013790

---------------~

~-- -- ---+

Lab: SERAS Lab

Lab Phone: (732) 321-4252

Stop Volume Vol Preuure Units

-5 4. 7 Liters ~ ---7.5 --4.68 - Liters

----~-i

SAMPLES TRANSFERRED FROM ------------------

Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP #1814. Detection limit of 0.030 ppbv. CHAIN OF CUSTODY#

Items/Reason ---o8te Received by Date Time Items/Reason Relinquished By- Date Date Time --- . ~®_ ~~,£--t--•~........,._,'--"-~J!tlll ~3/11/Lt ts:oo ll/ll/11qly5/ $ ~~J/I!fL/~£1~~-'::""..::-~i(( I~

--- -- ------

r-- •

R2-0008112

U> m ~ U> 6 ~ N

6 )>

~ ~ 0 ..... ..... .....

0 (,.) 0

Page 1

ERT

SERAS, Edison, NJ

EPA Contract Number: EP-W-09..031

wottfi03Co3 Lab # Sample # Location Analyses Matrix

1-042-0075 ~Unit26FF T0-15(VOAs) Air

1-042..0076 Unit 21 ss- T0-15 (VOAs)- Soil Gas


Site #: SERAS-042



Collected

311012011

311012011

Numb Coot

1 +--

1 ----

Container

Summa Canister

Summa Canister ---

Preservative SUMMA#

None 000003

None 000001

No: SERAS-042-03/1 0/11-0027

OrlflceiD

013789

013932

Lab: SERAS Lab

Lab Phone: (732) 321-4252

Stop Volume Vol Preaaure Units

-7 4.68 Liters -3 5.54 ~Liters

------

---r


ltemsfReason ltemsiReason Date Received by Date Time _...:....__---:- ___;;..._ __ _ ~~~"-A-1~~# -¥~

-.--


CHAIN OF CUSTODY #

- - ... ......

------;

-----;- - -

Relinquish_ed_e_:.y_3/J_~~-·:-u ~- 3~:{u:

R2-0008113

Special Instructions: TO-15for requested 8 compounds as per SERAS SOP #1814. Detection limit of 0.030 ppbv.

TO-15 (VOAs) Air

TO-15 (VOAs) Air

I

!

~

Lab: SERAS Lab

Lab Phone: (732) 321-4252

No: SERAS-042-03/10/11-0028


CHAIN OF CUSTODY #

~


Site #: SERAS-042



Collectad I Numb Container I Preservative i SUMMA~ OrificelD I Stop Volume' VolI Cont I . Pressure Units3/10/2011! 1, Summa Canister I None : 000192 1013793 -7.5 4.69 Liters

3/10/2011! 1 Summa Canister ! None i 001131 1013767 -7.5 4.25 Liters, I

MatrixAnalyses

1-042-0077 I Unit 21 GF1-042-0078 I Unit 21 FF

~I -

_~C2# fR[0300 3Lab # Sample # I Location

Page 1~

ERT

SERAS, Edison, NJEPA Contract Number: EP-W-09-031

(f)m

~(f)Ia~N6»;UIa~a....•.....•.....•.

oCN....a.

~ Rali".,','a' by ! Date , Ra",,,,' by . D.te' Tima I: Item"R •• ,," : Rali""o'ed BY. i Date. ~fY , Date : Time

(~Qk( 7~3MII 15:&"'1 '1I11/f/"c.l'I5'>~/:S//'{L/1 ~ 3~( (~II

!I

i!

R2-0008114

(/) m

~ (/)

I

0 ~ 1\,)

~ :::0 6 ~ 0 ...... ...... ......

Page 1

ERT

SERAS, Edison, NJ

EPA Contract Number: EP-W-o9-031

wo#((1o3C03 Lab # Sample # Location

1-042-oO~Unit 6 SS

1-042-oD80 Unit 6 GF

Analyses Matrix


T0-15 (VOAs) Air


S1te #: SERAS-042

Contact Name D McCall


No: SERAS-042-03/1 0/11-0029

Lab SERAS Lab

Lab Phone: (732) 321-4252


Preservative SUMMA # OrlficeiD Stop Volume Vol

3110/2011

3110/2011 +

------~

Summa Canister

Summa Canister

None 000264 None----ooo273

~----

- ..l.-_---

Pressure Units

013948

013941

-7.5

-5.5

--~- ---

4.59 Liters

5.16

------~-

1 '

Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP #1814. Detection limit of 0 030 ppbv.


CHAIN OF CUSTODY I#

Date Received by Date Time Items/Reason Relinquished By Date Time -----

~10~ SLII/11

R2-0008115

(/) m ~ (/)

I

0 ~ 1\.)

6 )> :::u 6 ~ 0 ...... ...... ......

0 w w

Page 1

ERT

SERAS, Ed1son, NJ


Wo#' ~fQ3C03 Lab I# Sample I# Location

1-042-0081 Unit 6 GFCol

---1-042-0082 Unit 6 FF

--==r - --... ---

-- -~------

Analyses Matrix

T0-15 (VOAs) Air

T0-15 (VOAs) Air


Site 1#: SERAS-042



No: SERAS~42~3/10/11~030

Lab· SERAS Lab

Lab Phone: (732) 321-4252

Collectad Numb Container Cont

Preservative SUMMA I# OrlflceiD Stop Volume Vol Pressure Units

3/10/2011 1 Summa Canister None 000263 013937 -8 4.58 Liters

3/10/2011 Summa Can1ster None 000209 013945 -7.5 4 72 L1ters ---

---- ...

·~----------------------- _,

r

~---- --__ .._

--t-Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP 1#1814. Detection limit of 0 030 ppbv.


CHAIN OF CUSTODY #I

Items/Reason Date Received by Date Time ltems/Reas:...:.o_n __ Re.:_li_nq~u-=is:..:_hed:..: By Date ~ Dfe Time

.3Ht ~,$/11/11 IS~JJ!!/Aooly5·l ~::Jli't/IJ-~ 'l>{'"-~14. L~

R2-0008116

(J) m ~ (J)

I 0 ~ 1\)

6 )> :::u I

0 ~ 0 ~

~

~

Page 1

ERT

SERAS, Edison, NJ

EPA Contract Number EP-W-09-031

wef/FRlo3C03 Lab tl Sample tl LocatJon

1-042-0083 Un1t 6 AMB

1-042-0084 Unit 25 SS

--- --

Matrix


S1te tl SERAS-042

Contact Name. D McCall

Contact Phone 609-865-6414


T0-15(V0As) Air 3110/2011 1 Summa Can1ster

T0-15 (VOAs) Soil Gas 311 0/2011 ~

Summa Camster

Pntservative SUMMA #I

None 000259 - None --000079

No: SERAS-042-03/10/11-0031

OrtflceiD

013762

013795

Lab SERAS Lab

Lab Phone (732) 321-4252

Stop Volume Vol Pntuunt Unlta

-7.5 4 15 Lrters

-7.5 4.43 Liters

- ---

+ --,

-r

---+

-- -------

-_-T-


Special Instructions T0-15 for requested 8 compounds as per SERAS SOP #1814. Detect1on lim1t of 0.030 ppbv. CHAIN OF CUSTODY I

+ -----

- -- - ~ ~--;

R2-0008117

U> m ~ U>

I

0 ~ N

6 )> :;o 6 ~ 0 ~

...... ......

0 w CJ1

Page 1~ ERT

SERAS, Edison, NJ


'Vl!O#U(JQ3003 _ Lab # Sample # Location Analyses Matrix

1:1 0 1-042-0085 -Ly-=-, - 1--,·042-0086

Unit 25 GF

Unit 25 GFCol

T0-15 (VOAs) Air

T0-15 (VOAs) Air

-------.....--- -- -- ------------


Site #: SERAS-042



Collected~Numb Container Coot

No: SERAS-042-03/1 0/11-0032

Lab: SERAS Lab

Lab Phone: (732) 321-4252

Preservative SUMMA # OriflceiD f Stop Volume~ Pressure Units

3/10/2011

3/10/2011 L 1 Summa Canister 1 None 000169 013778 -r - -6.5 4.85 Liters

I -I

I

1Summa Canister 1 None ____ 0002~013927 --- -7 --4.71 Liters--

SAMPLES TRANSFERRED FROM --------

Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP #1814. Detection limit of 0.030 ppbv. CHAIN OF CUSTODY I

Items/Reason Date Time Items/Reason Relinquished By

-------------------------------------

- ------ ---- -------------

R2-0008118

(/) m ~ (/)

I

0 ~ 1\)

I

0 )> :::0 I

0 ~ 0 ~

~

~

Page 1

ERT

SERAS, Ed1son, NJ

EPA Contract Number. EP-W-09-031

vv CJ#= ij( LCJ 5CV 3 Labtf Sampletf I l ocation

___,_ l.f~ 1-042-0087 Unit25 FF

1.{_3 1-042-0088 Unit23 SS

Analyaes Matrix

T0-15 (VOAs) Air



S1te tf: SERAS-042



No: SERAS-042-03/10/11-0033

Lab SERAS Lab

Lab Phone: (732) 321-4252

Collected ..--Numb Container Preservative SUMMA tf OrlflceiD ~ - Stop Volume Vol

3/10/2011

3110/2011

Cont

1 Summa Canister None 000007

1 Summa Canister None 000034 ~----- -------

013943

013911

Pressure Units

-6.5 4.71 Liters

4.76 Liters

------- ------------- - --

---~-------~--- -----,----

-------------------~

-- --+

- _ ____,

- ------.. ---- ---- --------------------~ -- .

-------1 I SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY tf Spec1allnstructions: T0-15 for requested 8 compounds as per SERAS SOP tf1814. Detection limit of 0.030 ppbv

Date Received by

j~o~~ Date Time-

, .. m,.,•••son •• u""""""' ~·" ~ ..... · __ b_y ---'~"'-l-r I, T/i: _ ,.

_,J""'"'s:'-""o-"'-o~lr!~ifhtly~,)._ ~l'f//L -rr- ~ f•,p vuu

----~- - --- ~

J/11/ll

T

R2-0008119

0 w ~

Page 1

ERT

SERAS, Ed1son, NJ


Lab # Sample # Location

1-042-00-ag--Unit 23 GF

1-042-0090 Unit 23 FF

--+-

Analyses Matrix

T0-15 (VOAs) Air

T0-15 (VOAs} Air


S1te #: SERAS-042




3110/2011 1 Summa Canister 3110/2011 ~--1-Summa Canister

No: SERAS-042~3/10/11~034

Lab· SERAS Lab

Lab Phone: (732) 321-4252

Preservative ~ SUMMA # OriflceiD Stop Volume Vol Pressure Units

None -- ~000184 1 013760 -4.5 5.05 Liters

4.61 Liters ~~-

None 000171 013784 -7.5

t----1---~----l --+ ~--~----..,--------_1

..,..___ ------___ ,__ ______ .,._ __ --~---- -- ___________ __,

+

1 SAMPLES TRANSFERRED FROM

- --Special Instructions: T0-15 for requested 8 compounds as per SERAS SOP #181 4. Detection limit of 0.030 ppbv. CHAIN OF CUSTODY #

Items/Reason Date Date - T~ Items/Reason Relinquished By Date

R2-0008120

0 w 00

Page1 C

ERT

SERAS, Ed1son, NJ


w~t<tOJXJ3 Lab t# Sample t# Location

1-042-0091 Trip Blank

Analyses Matrix

T0-15 (VOAs) Blank


Site#· SERAS-042



No: SERAS-042-03/1 0/11-0035

Lab SERAS Lab

Lab Phone: (732) 321-4252

Collected Numb Container Preservative ~ SUMMA t# OrlflceiD Stop Volume Vol Cont Pressure Units

3110/2011 1 Summa Canister None ~ 000165 -29.5

----------

·- ---·--- ----,

--1

.,. - _ _,

Special instructions: T0-15 for requested 8 compounds as per SERAS SOP #1814. Detection limit of 0.030 ppbv.


CHAIN OF CUSTODY #I

Items/Reason Date Received by Date Time Items/Reason -

.Jfo/~ 3}11 /It .....c.:ls:..cc..::~-=-~ftii/Afk:rlyst'5 ?/'

t - - -

R2-0008121


APPENDIX C

Climatological Data


April 2011

R2-0008122


Local Climatological Data from Dutchess County Airport

Poughkeepsie, NY Elevation: 156 feet above sea level

Latitude: 41.627 Longitude: -73.884

March 2011


Date

Time

(LST)

Dry Bulb

Temperature

(F)

Dew point

Temperature

(F)

Relative

Humidity

%

Wind

Speed

(MPH)

Wind

Direction

Station

Pressure

(in. hg)

Precipitation

Total

(inches)

5 53 36 29 76 0 0 30.35

5 153 36 30 79 0 0 30.33

5 253 34 31 89 0 0 30.3 T

5 351 36 32 85 3 140 30.28

5 353 36 32 85 3 140 30.28 T

5 453 37 33 86 0 0 30.25

5 531 37 34 89 3 150 30.25

5 553 35 33 92 3 250 30.24

5 642 36 34 92 3 250 30.23

5 653 36 33 89 0 0 30.23

5 719 37 34 89 0 0 30.22

5 753 42 38 86 6 170 30.22

5 802 43 37 79 9 150 30.22

5 853 43 39 86 8 170 30.22

5 953 45 40 83 8 180 30.19 T

5 1051 46 41 83 9 170 30.19

5 1053 47 41 80 8 170 30.19

5 1121 48 41 77 8 230 30.16

5 1146 52 43 72 6 VR 30.14

5 1153 52 42 69 7 220 30.14

5 1253 54 43 67 6 170 30.11

5 1353 58 42 55 8 170 30.06

5 1453 58 43 58 13 150 30.04

5 1553 57 42 57 15 160 30.03

5 1653 55 43 64 14 170 30.03

5 1753 54 43 67 8 170 30.03

5 1853 53 44 72 7 170 30.01

5 1953 54 45 72 8 170 30.03

5 2053 53 46 77 10 180 30.01

5 2153 53 47 80 7 VR 30.01

5 2253 53 47 80 9 170 30

5 2313 52 46 80 11 160 29.98

5 2348 52 46 80 7 160 29.96

5 2353 52 46 80 9 160 29.96

6 44 52 45 77 8 160 29.95

LST = Local standard time % = percent

MPH = Miles per hour F = Fahrenheit

in. hg. = Inches of mercury VR = Variable

T = Trace

R2-0008123





March 2011


Date

Time

(LST)

Dry Bulb

Temperature

(F)

Dew point

Temperature

(F)

Relative

Humidity

%

Wind

Speed

(MPH)

Wind

Direction

Station

Pressure

(in. hg)

Precipitation

Total

(inches)

6 53 52 46 80 14 160 29.95

6 130 52 46 80 10 180 29.93

6 153 52 46 80 8 200 29.93

6 253 52 47 83 7 180 29.9

6 353 53 47 80 7 160 29.88

6 453 53 47 80 7 180 29.85

6 553 53 48 83 7 VR 29.84

6 653 53 48 83 7 170 29.83 0.01

6 751 54 48 80 7 170 29.83

6 753 53 49 86 10 160 29.83 T

6 829 54 48 80 10 180 29.83

6 853 53 49 86 8 170 29.82 0.03

6 926 54 50 86 7 170 29.81

6 953 53 50 90 6 VR 29.8 0.02

6 1043 54 50 86 7 200 29.77

6 1053 54 49 83 6 VR 29.77 0.02

6 1130 54 50 86 5 190 29.76

6 1150 54 50 86 6 VR 29.76

6 1151 54 50 86 5 190 29.76

6 1153 54 50 86 6 VR 29.76 0.06

6 1212 54 50 86 5 VR 29.77

6 1233 54 50 86 5 VR 29.75

6 1253 54 51 90 0 0 29.75 0.04

6 1306 54 52 93 5 160 29.73

6 1332 54 52 93 3 VR 29.72

6 1353 55 51 86 7 160 29.71 0.01

6 1416 55 52 90 5 140 29.7

6 1453 55 52 90 6 140 29.67 T

6 1553 54 51 90 10 130 29.66 0.04

6 1653 53 51 93 5 140 29.65 0.08

6 1740 52 50 93 6 350 29.65

6 1746 52 50 93 7 350 29.65

6 1753 50 48 93 14 340 29.65 0.09

6 1823 37 36 96 18 20 29.65

6 1828 37 36 96 20 20 29.65




T = Trace

R2-0008124





March 2011


Date

Time

(LST)

Dry Bulb

Temperature

(F)

Dew point

Temperature

(F)

Relative

Humidity

%

Wind

Speed

(MPH)

Wind

Direction

Station

Pressure

(in. hg)

Precipitation

Total

(inches)

6 1843 37 36 96 17 360 29.66

6 1853 36 34 92 15 20 29.66 0.29

6 1951 36 34 92 16 360 29.63

6 1953 35 33 92 15 10 29.62 0.36

6 2053 34 32 92 15 10 29.62 0.39

6 2102 34 32 92 14 10 29.61

6 2115 34 32 92 14 10 29.61

6 2137 34 30 85 13 20 29.6

6 2141 34 32 92 14 20 29.59

6 2144 34 30 85 18 20 29.57

6 2153 34 31 89 11 10 29.58 0.28

6 2253 34 32 92 9 10 29.55 0.16

6 2325 34 30 85 18 10 29.53

6 2335 34 30 85 11 20 29.52

6 2347 34 30 85 11 10 29.51

6 2353 33 31 92 10 20 29.51 0.23

7 49 34 30 85 14 10 29.47

7 53 34 31 89 13 10 29.47 0.07

7 100 34 30 85 15 10 29.46

7 125 34 30 85 13 20 29.44

7 134 34 30 85 16 10 29.43

7 146 34 30 85 17 20 29.42

7 151 34 30 85 14 20 29.42

7 153 33 31 92 13 20 29.42 0.02

7 214 34 30 85 14 20 29.4

7 226 34 30 85 17 20 29.39

7 230 34 30 85 16 20 29.39

7 251 34 30 85 15 20 29.38

7 253 33 30 89 15 20 29.38 0.07

7 312 34 30 85 13 10 29.39

7 326 34 30 85 16 10 29.39

7 345 34 30 85 8 330 29.4

7 353 33 30 89 11 340 29.4 0.09

7 432 34 30 85 10 360 29.42

7 451 32 30 92 11 360 29.41



in. hg. = Inches of mercury

R2-0008125





March 2011


Date

Time

(LST)

Dry Bulb

Temperature

(F)

Dew point

Temperature

(F)

Relative

Humidity

%

Wind

Speed

(MPH)

Wind

Direction

Station

Pressure

(in. hg)

Precipitation

Total

(inches)

7 453 32 30 92 13 360 29.42 0.01

7 458 32 30 92 11 360 29.42

7 548 34 28 79 15 360 29.46

7 553 33 29 85 17 350 29.46 0.03

7 608 34 28 79 18 360 29.46

7 619 34 28 79 11 350 29.47

7 640 34 28 79 10 350 29.48

7 653 33 28 82 10 350 29.49 T

7 714 34 28 79 11 350 29.5

7 737 34 28 79 15 350 29.53

7 753 33 28 82 10 350 29.54 T

7 806 34 28 79 7 340 29.55

7 824 32 28 85 6 340 29.58

7 850 34 30 85 0 0 29.6

7 853 33 30 89 3 310 29.6 T

7 900 34 30 85 5 310 29.6

7 953 35 26 70 13 300 29.65

7 1053 35 24 64 17 280 29.71

7 1153 37 25 62 11 310 29.76

7 1253 38 23 55 16 330 29.8

7 1353 40 24 53 13 320 29.83

7 1453 42 24 49 16 340 29.84

7 1553 41 27 58 10 10 29.87

7 1653 40 26 57 7 20 29.93

7 1753 38 20 48 9 340 29.96

7 1853 33 24 70 8 20 30.01

7 1953 32 22 67 3 360 30.06

7 2053 30 22 72 0 0 30.08

7 2153 29 22 75 0 0 30.11

7 2253 28 21 75 0 0 30.14

7 2353 27 18 69 5 10 30.16

8 53 27 18 69 6 10 30.17

8 153 26 17 69 5 30 30.2

8 253 25 17 72 6 30 30.2

8 353 25 18 75 0 0 30.23



in. hg. = Inches of mercury T = Trace

R2-0008126





March 2011


Date

Time

(LST)

Dry Bulb

Temperature

(F)

Dew point

Temperature

(F)

Relative

Humidity

%

Wind

Speed

(MPH)

Wind

Direction

Station

Pressure

(in. hg)

Precipitation

Total

(inches)

8 453 24 16 71 0 0 30.27

8 553 23 16 74 0 0 30.31

8 653 24 17 75 0 0 30.33

8 753 26 17 69 8 10 30.37

8 853 29 16 58 10 10 30.38

8 953 32 15 49 9 20 30.37

8 1053 35 16 46 14 360 30.37

8 1153 37 15 41 10 10 30.37

8 1253 39 14 36 13 10 30.37

8 1353 41 14 33 10 30 30.36

8 1453 40 12 32 5 VR 30.36

8 1553 41 15 35 5 340 30.36

8 1653 40 15 36 6 360 30.37

8 1753 36 13 39 7 20 30.39

8 1853 34 18 52 7 20 30.39

8 1953 33 25 72 6 10 30.39

8 2053 31 25 78 0 0 30.4

8 2153 30 24 78 3 30 30.42

8 2253 30 24 78 0 0 30.43

8 2353 28 25 89 0 0 30.43

9 53 28 25 89 0 0 30.42

9 153 27 24 88 0 0 30.42

9 253 26 23 88 0 0 30.41

9 353 26 22 85 0 0 30.43

9 453 25 22 88 0 0 30.43

9 553 24 22 92 0 0 30.44

9 653 25 21 85 0 0 30.45

9 753 27 22 81 3 20 30.47

9 853 30 24 78 3 310 30.47

9 953 34 24 67 0 0 30.46

9 1053 39 22 51 6 130 30.45

9 1105 39 21 48 6 140 30.44

9 1153 41 23 49 13 100 30.41

9 1253 42 22 45 10 130 30.37

9 1353 43 21 42 7 140 30.36




R2-0008127





March 2011


Date

Time

(LST)

Dry Bulb

Temperature

(F)

Dew point

Temperature

(F)

Relative

Humidity

%

Wind

Speed

(MPH)

Wind

Direction

Station

Pressure

(in. hg)

Precipitation

Total

(inches)

9 1453 42 22 45 13 130 30.36

9 1553 41 21 45 11 140 30.35

9 1653 40 24 53 9 140 30.33

9 1753 39 24 55 11 150 30.33

9 1853 38 26 62 5 160 30.36

9 1953 37 27 67 5 VR 30.33

9 2020 37 27 67 9 140 30.35

9 2053 37 27 67 13 130 30.35

9 2153 36 28 73 7 VR 30.32

9 2253 36 28 73 10 110 30.28

9 2313 36 28 73 17 110 30.28

9 2351 36 28 73 7 140 30.27

9 2353 36 28 73 5 VR 30.27

10 53 36 29 76 7 130 30.23

10 153 36 29 76 6 150 30.2

10 253 37 30 76 8 140 30.17

10 353 37 31 79 10 120 30.16 0.01s

10 453 37 32 82 9 130 30.16 T

10 508 37 32 82 10 130 30.16

10 553 38 33 82 6 VR 30.14

10 653 38 34 86 6 130 30.14 T

10 753 39 35 86 0 0 30.12 0.02

10 853 41 36 82 8 110 30.09

10 953 42 37 83 8 130 30.06 T

10 1053 42 38 86 11 130 30.06 T

10 1151 45 39 80 14 120 30.03

10 1153 44 39 83 16 120 30.03 T

10 1253 45 40 83 13 120 30 T

10 1337 45 41 86 9 120 29.98

10 1345 45 41 86 13 110 29.96

10 1353 45 41 86 14 120 29.96

10 1400 45 41 86 13 120 29.96

10 1443 45 41 86 15 120 29.93

10 1453 45 41 86 16 110 29.93 0.01

10 1530 46 43 89 14 110 29.91




T = Trace

R2-0008128





March 2011


Date

Time

(LST)

Dry Bulb

Temperature

(F)

Dew point

Temperature

(F)

Relative

Humidity

%

Wind

Speed

(MPH)

Wind

Direction

Station

Pressure

(in. hg)

Precipitation

Total

(inches)

10 1553 46 42 86 14 120 29.91 T

10 1607 46 43 89 11 110 29.9

10 1626 46 43 89 13 110 29.89

10 1653 46 42 86 13 110 29.89 0.01

10 1753 46 42 86 15 110 29.87 0.01

10 1800 46 43 89 17 110 29.85

10 1853 46 42 86 16 110 29.85 0.01

10 1953 46 43 89 15 120 29.83 0.08

10 2053 47 43 86 15 120 29.79 0.15

10 2153 48 44 86 11 110 29.76 0.16

10 2253 48 45 89 15 110 29.7 0.15

10 2353 49 46 89 8 100 29.66 0.14

11 53 50 46 86 16 110 29.62 0.22

11 153 50 47 90 13 110 29.58 0.21

11 253 52 49 90 11 150 29.57 0.19

11 301 52 48 86 9 210 29.57

11 308 52 48 86 8 190 29.58

11 322 52 48 86 7 170 29.57

11 336 52 48 86 7 160 29.58

11 344 52 48 86 3 150 29.57

11 351 52 48 86 7 130 29.57

11 353 51 48 90 7 140 29.57 0.2

11 409 50 48 93 5 270 29.58

11 425 50 48 93 0 0 29.58

11 433 50 48 93 0 0 29.57

11 453 50 48 93 0 0 29.57 0.11

11 553 50 48 93 14 70 29.51 0.1

11 653 51 47 86 0 0 29.54 T

11 753 51 46 83 0 0 29.55

11 846 50 46 86 5 170 29.56

11 853 50 47 90 5 180 29.56

11 953 50 48 93 3 170 29.57

11 1015 50 48 93 7 170 29.57

11 1030 50 48 93 7 170 29.57

11 1051 52 48 86 7 180 29.56



in. hg. = Inches of mercury T = Trace

R2-0008129





March 2011


Date

Time

(LST)

Dry Bulb

Temperature

(F)

Dew point

Temperature

(F)

Relative

Humidity

%

Wind

Speed

(MPH)

Wind

Direction

Station

Pressure

(in. hg)

Precipitation

Total

(inches)

11 1053 52 48 86 7 180 29.56

11 1151 52 46 80 7 240 29.57

11 1153 51 47 86 7 230 29.57

11 1228 52 45 77 7 220 29.56

11 1253 52 43 72 7 230 29.55

11 1312 52 43 72 9 220 29.55

11 1321 52 43 72 7 240 29.55

11 1353 52 41 66 11 260 29.55 0.01

11 1453 52 39 61 9 230 29.55

11 1553 53 37 55 9 230 29.54

11 1653 52 35 53 14 240 29.57

11 1753 49 32 52 10 240 29.59

11 1853 45 31 58 8 260 29.63

11 1953 44 28 53 13 260 29.64

11 2053 43 28 56 7 240 29.65

11 2153 43 27 53 5 220 29.63

11 2253 42 28 58 10 230 29.62

11 2353 39 27 62 17 240 29.63

12 53 38 27 65 7 240 29.63

12 153 37 27 67 6 220 29.63

12 253 36 27 70 6 VR 29.62

12 353 35 27 73 5 230 29.63

12 453 35 28 76 6 230 29.64

12 553 36 29 76 6 210 29.65

12 653 37 30 76 8 220 29.66

12 753 38 30 73 9 220 29.67

12 853 40 31 70 10 230 29.66

12 953 42 31 65 9 230 29.66

12 1053 45 32 60 16 250 29.65

12 1153 46 32 58 14 240 29.64

12 1253 50 32 50 15 250 29.61

12 1353 52 28 40 9 200 29.59

12 1453 54 26 34 10 230 29.56

12 1553 52 26 37 11 240 29.58

12 1653 52 26 37 13 220 29.57




R2-0008130





March 2011


Date

Time

(LST)

Dry Bulb

Temperature

(F)

Dew point

Temperature

(F)

Relative

Humidity

%

Wind

Speed

(MPH)

Wind

Direction

Station

Pressure

(in. hg)

Precipitation

Total

(inches)

12 1753 51 28 41 5 210 29.59

12 1853 45 30 56 3 120 29.62

12 1953 45 32 60 0 0 29.63

12 2053 43 36 76 0 0 29.64

12 2153 44 36 74 0 0 29.64

12 2253 43 35 73 0 0 29.63

12 2353 42 36 79 0 0 29.61

13 53 41 35 79 0 0 29.62

13 153 37 34 89 0 0 29.62

13 253 36 33 89 0 0 29.64

13 353 34 32 92 0 0 29.64

13 453 36 33 89 0 0 29.67

13 553 44 33 65 8 280 29.69

13 653 44 29 56 8 260 29.72

13 753 44 27 51 10 270 29.75

13 853 45 28 51 13 290 29.78

13 953 46 25 44 17 300 29.79

13 1053 45 25 46 15 310 29.82

13 1153 44 26 49 16 280 29.84

13 1253 45 26 47 11 300 29.85

13 1353 46 26 46 13 270 29.84

13 1453 47 27 46 5 VR 29.85

13 1553 45 28 51 11 270 29.89

13 1653 44 28 53 11 270 29.91

13 1753 43 29 58 11 290 29.95

13 1853 42 28 58 11 290 29.98

13 1953 42 29 60 10 280 29.98

13 2053 41 29 62 7 280 30.01

13 2153 40 28 62 7 260 30.01

13 2253 38 28 67 3 260 30.01

13 2353 35 29 79 3 50 30.01




R2-0008131

THROUGH: Dennis Miller, SERAS Program Manager ~ ~ Leader~e ...

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