Thermo Scientific Dionex ICS-900 Product Specifications › portal › es › open ›...
Transcript of Thermo Scientific Dionex ICS-900 Product Specifications › portal › es › open ›...
C H R O M A T O G R A P H YP
rod
uct S
pe
cificatio
ns
The Thermo Scientific™ Dionex™ ICS-900 is an integrated, dual piston, isocratic ion chromatography system that performs “no compromise” IC separations. The system is designed for ease of use, providing fast startup times and reliable, stable performance for your demanding applications. Built with the aim of maintaining low operating costs, the Dionex ICS-900 uses proven and reliable technologies to deliver results you can count on.
Thermo Scientific Dionex ICS-900Ion Chromatography System
Low-Cost Reliability• Sensitive, stable, heated conductivity
detection for precise results
• Thermo Scientific™ Dionex™ MMS™ 300 MicroMembrane™ Suppressor suppression with displacement chemical regeneration (DCR) technology for drift free baseline and ease-of-use
• Flexible pump flow range to support 2, 3, and 4 mm isocratic anion and cation columns
• Dual-piston, serial pumping system with PEEK™ flowpath for low maintenance costs and maximum up-time
• All-polymeric flow pathway to eliminate contamination and corrosion
• Thermo Scientific™ Dionex™ Chromeleon™ Chromatography Data System Software for full control, quality integration, and versatile reports to exceed all your data processing needs
• USB connectivity for fast, troublefree instrument connection and configuration
• Integrated IQ/OQ/PQ to routinely assure the quality of your results
• Compatible with all Dionex IC autosamplers. The Thermo Scientific Dionex AS-DV autosampler is recom-mended for economical unattended operation, including sample filtration
• Compatibility with a broad range of Dionex polymeric separation columns for unparalleled application flexibility and reliability.
2
Peak areas and retention times are highly reproducible and baselines are stable and noise-free, as demonstrated in these overlays of anion determinations (n=20).
1
2
3
4 5
6
7
0 5 10 15
µS
Minutes
25004
Column: Thermo Scientific™ Dionex™ IonPac™ AS24, 2 mm
Eluent: 0.8 mM carbonate/0.1 mM bicarbonate
Flow Rate: 0.3 mL/minInj. Vo lume: 2.5 µLTemp: AmbientDetection: Suppressed conductivity
Thermo Scientific™
Dionex™ AMMS™ 300, 2 mmSample: Seven anion standard
Peaks: 1. Fluoride 4 mg/L
2. Chloride 20
3. Nitrite 20
4. Bromide 20
5. Nitrate 20
6. Phosphate 40
7. Sulfate 20
Column: Dionex IonPac CS12A, 3 mmEluent: 20 mM MSAFlow Rate: 0.5 mL/minInj. Volume: 10 µLTemperature: AmbientDetection: Suppressed conductivity, Thermo Scientific™ Dionex™ CMMS™ 300, 4 mm, 100 mM TBAOH regenerantSample: Six cation standard, 1/50 dilution
Peaks: 1. Lithium 1 mg/L 2. Sodium 4 3. Ammonium 5 4. Potassium 10 5. Magnesium 5 6. Calcium 10
0 6 12
µS
Minutes
12
3
4
5 6
Overlay of cation separations performed on the Dionex ICS-900 using a 3 mm Dionex IonPac CS12A cation-exchange column. Results show high reproducibility.
µS
Minutes
1
2
3
4 5 6 7
25007
Column: Dionex IonPac AS14, 2 mmEluent: 0.8 mM carbonate/ 0.1 mM bicarbonateFlow Rate: 0.3 mL/minInj. Volume: 2.5 µLTemperature: AmbientDetection: Suppressed conductivity, Dionex AMMS 300, 2 mmSample: Seven anion standard
Peaks: 1. Fluoride 4 mg/L
2. Chloride 20
3. Nitrite 20
4. Bromide 20
5. Nitrate 20
6. Phosphate 40
7. Sulfate 20
0 5 10 15
10
0
Dionex IonPac AS14 2 mm column for reduced reagent usage with high performance and fast separation.
µS1
0 50
Dionex IonPac AS14 2 mm column for reduced reagent usage with high Dionex IonPac AS14 2 mm column for reduced reagent usage with high performance and fast separation.performance and fast separation.
Application and column fl exibility: 2, 3, and 4 mm isocratic columns
Outstanding access to chromatography components
Ultra reliable, low carryover, electricRheodyne injection valve
Dual piston, serial pumping system with stability from0.01 to 5.00 mL/min at pressures to 5000 psi
Heated conductivity cell and Dionex MMS™ 300 MicroMembraneSuppressor for stable, noise-free results
2
1
3
4
52
3
3
5
4
1
3Dionex iCS-900 iC SyStem SpeCifiCationS
analytical pump and Hydraulics
Type Serial dual-reciprocating pistons, microprocessor-controlled constant stroke, variable speed
Construction Chemically inert, metal-free PEEK pump heads and flow paths compatible with aqueous eluents of pH 0–14 and reversed-phase solvents
Pump Operating Pressure 0–35 MPa (0–5000 psi)
Flow Rate Range 0.00–5.00 mL/min without changing pump heads
Flow Precision <0.1%
Flow Accuracy <0.1%
Pressure Ripple <1%
Eluent Bottle Pressure No gas required
Vacuum Degasser Optional with external vacuum degasser
Gradient Capabilities Optional with Thermo Scientific Dionex RFC-30
Eluent Generation Optional with Dionex RFC-30
injection Valve
6-port, 2 position Rheodyne valve, electically actuated
Column Heater/thermostat
Optional External Heater, CTS-10, 25 to 85 °C, minimum 5 °C above ambient
Suppressor Compatibility
Chemical Suppression 6- or 10- port, 2-position high-pressure Rheodyne valves, fully inert PEEK construction, electrically activated
Displacement Chemical Regeneration Yes, anion and cation, 2 and 4 mm
Electrolytic Suppression, Self-Regenerating Optional with Dionex RFC-10
Electrolytic Suppression, Self-Regenerating, Optional with Dionex RFC-10 External Water
Suppression Capacity Anions: Thermo Scientific™ Dionex™ ASRS™ Anion Self-Regenerating Suppressor 300 (4 mm): 200 μeq/min Dionex ASRS 300 (2 mm): 50 μeq/min Dionex AMMS 300 Suppressor (4 mm): 150 μeq/min Dionex AMMS 300 (2 mm): 37.5 μeq/min Thermo Scientific™ Dionex™ Anion Atlas™ Electrolytic Suppressor: 25 μeq/min
Cations: Thermo Scientific™ Dionex™ CSRS™ 300 Cation Self-Regenerating Suppressor (4 mm): 110 μeq/min Dionex CSRS 300 (2 mm): 37.5 μeq/min Dionex CMMS 300 Cation MicroMembrane Suppressor (4 mm): 150 μeq/min Dionex CMMS 300™ (2 mm): 37.5 μeq/min Thermo Scientific™ Dionex™ Cation Atlas™ Electrolytic Suppressor: 25 μeq/min
Void Volume Thermo Scientific™ Dionex™ SRS™ Self-Regenerating Suppressor 300 (4 mm): <50 μL Dionex SRS 300 (2 mm): <15 μL Dionex MMS 300 (4 mm): <50 μL Dionex MMS 300 (2 mm): <15 μL Dionex AMMS-ICE 300 (4 mm): <50 μL Dionex AMMS-ICE 300 (2 mm): <15 μL Dionex AAES: <35 μL Dionex CAES: <35 μL
Sequential Suppression for Anions Yes, Dionex MMS 300 + Thermo Scientific Dionex CRD 300 Carbonate Removal Device
Suppressor Wear Parts None; peristaltic pump and inline filters not required
4Dionex iCS-900 iC SyStem SpeCifiCationS (ContinueD)
Conductivity Detector
Type Bipolar heated conductivity cell, microprocessor-controlled digital signal processing over the range 0–10,000 μS/cm
Detector Linearity 1%
Maximum Cell Pressure 10 MPa (1500 psi)
Resolution 0.0047 nS/cm
Cell Calibration Factory calibrated as a new system and calibrated in the field individually with memory retention and transfer
Flow Cell Chemical Compatibility (Standard) Fully compatible with all typical ion chromatography eluents, including MSA
autosampler
Automation Using Autosampler Yes, Dionex AS-DV, AS-AP, AS-HV Autosamplers or third party
Sequential/Simultaneous Injection Yes, depending on autosampler capabilities
Automated Dilution Yes, available with Dionex AS-AP Autosampler
Dilution Factor, Dionex AS-AP Autosampler 1:1 to 1:1000
Dilution Time, Dionex AS-AP Autosampler 15 s with sample overlap
Inline Sample Degassing Optional with Thermo Scientific Dionex CRD 200/CRD 300
Inline Filtration Optional with Dionex AS-DV Autosampler or inline filter
Automation Flexibility High, conditionals using Chromeleon software and post run features
Semiautomated System Qualification Yes, IQ/OQ/PQSequential Suppression for Anions
System Software Chromeleon Chromatography Data System requires Windows 7, XP, or Vista
• Automated ProcedureWizards
• System Wellness and Predictive Performance
• Virtual Column Simulator (evaluation mode standard, isocratic and gradient optional)
• Application Templates
• Multivendor Automation Support of 3rd Party (fully controls over 200 instruments from more than 25 manufacturers, including GC, HPLC, and MS)
• Customizable System Control Panels
• System Status Virtual Channels
• Power Failure Protection
• Sequential Injection
• System Trigger Commands and Conditionals
• Automated ProcedureWizards
• System Wellness and Predictive Performance
• Virtual Column
• Daily Audit Trail
• Sample Audit Trail
• Multiple Network Control and Network Failure Protection
• System Calibration Storage (factory, present, and previous; completely user selectable)
• Customized Reporting
physical Specifications
Physical Specifications Dimensions (h × w × d): 33 cm × 24 cm × 40 cm 13 in × 9.5 in × 15.7 in
Weight 10 kg (22 lb)
Power Requirements 100 to 240 V ac, 50 to 60 Hz, autoranging
System Flow Path All polymeric (PEEK), anion or cation configurations
Thermo Fisher Scientific, Sunnyvale, CA USA is ISO 9001:2008 Certified.
Pro
du
ct Sp
ecifica
tion
s
PS70300_E 02/13S
www.thermoscientific.com/dionex©2013 Thermo Fisher Scientific Inc. All rights reserved. ISO is a trademark of the International Standards Organization. All other trademarks are the property of Thermo Fisher Scientific Inc. and its subsidiaries. Specifications, terms and pricing are subject to change. Not all products are available in all countries. Please consult your local sales representative for details.
Australia +61 3 9757 4486Austria +43 1 333 50 34 0Belgium +32 53 73 42 41Brazil +55 11 3731 5140China +852 2428 3282
Denmark +45 70 23 62 60France +33 1 60 92 48 00Germany +49 6126 991 0India +91 22 2764 2735Italy +39 02 51 62 1267
Japan +81 6 6885 1213Korea +82 2 3420 8600Netherlands +31 76 579 55 55Singapore +65 6289 1190 Sweden +46 8 473 3380
Switzerland +41 62 205 9966Taiwan +886 2 8751 6655UK/Ireland +44 1442 233555USA and Canada +847 295 7500
ordering informationIn the U.S., call (800) 346-6390 or contact the Thermo Fisher Scientific Regional Office nearest you. Outside the U.S., order through your local Thermo Fisher Scientific office or distributor. Refer to the following part numbers.
Dionex iCS-900 ion Chromatography System part number
Dionex ICS-900 Ion Chromatography System, with Chromeleon SE and PC 067552
Dionex ICS-900 Ion Chromatography System with Chromeleon SE, without PC 067551
Dionex ICS-900 Ion Chromatography System expansion unit 067550