The high-precision Penning-trap mass spectrometer ...

The high-precision Penning-trap mass spectrometer PENTATRAP for fundamental studies

Alexander RischkaIMPRS-PTFS Seminar

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OUTLINE

Basics of Penning-Trap Mass Spectrometry

Motivation for precision mass spectrometry

• Contribution to neutrino physics

• Test of special relativity

The PENTATRAP experiment

Basics of Penning-Trap Mass Spectrometry

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Frequency to mass relation

Homogeneous magnetic field B

q/m

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Frequency to mass relation

Homogeneous magnetic field B

q/m

q, B drops at mass difference

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Confinement of the ion of interest

Homogeneous magnetic field B + electrical field E

q/m

U U

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Confinement of the ion of interest

Homogeneous magnetic field B + quadrupolar electrical field E

q/m

U U

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Movement of the confined ion

modified cyclotron motion

magnetron motion

axial motion

Three eigenmotions

B

Brown & Gabrielse, Rev. Mod. Phys. 58, 233 (1986)

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Frequency hirachy

Frequency hirachy: the cyclotron frequency is the most important one

A typical 10-11 measurement needs:

modified cyclotron motion:

magnetron motion:

axial motion:

B drift <

E stability <

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Types of PTMS

PI-ICR, projecting radial motions on a position sensitive detector, destructive

B

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Types of PTMS


FT-ICR, fourier transform the induced image current, non destructive

B

Motivation for precision mass spectrometry

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Field Examples m/m

Nuclear structure

physics

shell closures, shell quenching, regions of

Astrophysicsnuclear models

mass formula

rp-process and r-process path, waiting-point

Weak interaction

studies

CVC hypothesis, CKM matrix unitarity, Ft of

Metrology, fundamental constants

α (h/mCs, mCs /mp, mp/me ), mSi

Neutrino physics

CPT tests QED in HCI

mp and mp me- and me+ mion, electron binding energy

10-6 to 10-7

10-8

10-9 to 10-10

<10-11

<10-11

δVpn, island of stability

deformation, drip lines, halos, seperation energies

nuclei, proton threshold energies, astrophysical

reaction rates, neutron star, x-ray burst

superallowed ß-emitters

~10-10Contribution to neutrino physics research

E (A=100)

Test of E=mc2

<10-11

~10-10

100 keVto

10 keV

1 keV

100 eV – 10 eV

10 eV

< 1 eV

10 eV

< 1 eV

< 1 eV

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Test of E=mc2 with PTMS

1-mc2/E = (-1.4±4.4)10-7

S. Rainville et al., Nature 438, 1096 (2005)

Current value:

1-mc2/E < 10-8

Future measurement:

GAMS 5, measuring the energy of the gamma

PENTATRAP, measuring the Δm(36Cl, 35Cl)

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Contribution to neutrino physics research

mν = Q-Value - Endpoint of spectrum

Looking for missing energy in β-decay,since the dectecion efficiency of ν is too small

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Types of decays: - and EC

KATRIN – Project , MAC-E filter - - Decay of Tritium

ECHo – Project , µCalorimter EC in 163Ho

Requires Q-Value with a relative uncertainty of (δm/m) < 10-11

• Anti electron neutrino, < 2 eV/c2 (90% C.L.)• THe-Trap Experiment for Q-Value

• electron neutrino, 163Ho: mv ≤ 225 eV/c2 (90% C.L.)• PENTATRAP Experiment for Q-Value

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EC in Holmium, ECHo Collaboration

Decay spectrum of 163Ho from µCalorimeter measurement

Q-value to check for systematic uncertainties needed

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Q-value measurement of 163Ho @SHIPTRAP

163HoT1/2: 4570a

EC 100%

163DyT1/2: stable

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Q-value of EC in 163Ho

Status in 2014

µCalorimeter

S. Eliseev, et al. , Phys. Rev. Lett. 115, 062501 (2015)

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163HoT1/2: 4570a

EC 100%

163DyT1/2: stable

-


Status in 2014

Our result

µCalorimeter

Penning-trap@ GSI


Q-Value: ~ 2.8 keV with an 20 eV uncertainty for ECHo Phase 1

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163HoT1/2: 4570a

EC 100%

163DyT1/2: stable

-

Q-Value: ~ 2.8 keV with an 20 eV uncertainty for ECHo Phase 1


Status in 2014

Our result

2 eV uncertainty is needed for ECHo Phase 2

µCalorimeter


Penning-trap@ GSI

The PENTATRAP Experiment

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Features of the PENTATRAP experiment

External ion-source:• Access to higly charge ions

• Simple switching between species

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Features of PENTATRAP Experiment

Five Penning traps:

• Fast switching of ions

• New measurement schemes possible



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Features of PENTATRAP Experiment

Cryogenic trapping region:

• UHV, aiming for < 10-15 mbar

• reducing thermal noise and excitations

Five Penning traps:

• Fast switching of ions

• New measurement schemes possible



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Ion-source and beamline

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Ultra-stable voltage source

Rel. stability: < 10E-8 @ 10 min

Noise (0.1 Hz – 10 Hz): < 1.5 µV

Temp. coeff. < 0.1 ppm/K

Voltage range: 0 V to -100 V

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Ultra-stable voltage source

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Summary & Outlook

• Cryogenic setup in workshop, ready end of 2016

• Measuring 193Pt as alternative candidate to 163Ho

Outlook:

Summary:• Q-value of EC in 163Ho with 20 eV uncertainty

• Beamline commissioned and ready

• StaRep – in commissioning at THe-Trap

Thank you for your attention

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Phase-Sensitive Methods for ω+

Pulse and amplify (PNA)

• Phase evolution with low energy, ion probe less anharmonicitys

• Readout via axial mode, axial resonators have better SNR

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New cryogenic setup

Improvements:• simpler• less vacuum challenges• less assembly time and smaller debug cycle

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Types of PTMS


FT-ICR, fourier transform the induced image current, non destructive

B

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