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    The causes of the high friction angle of Dutch organic soils

    X.H. Cheng a ,, D.J.M. Ngan-Tillard a, E.J. Den Haan b

    a Department of Geotechnology, TU Delft The Netherlandsb GeoDelft Delft The Netherlands

    Received 24 May 2006; received in revised form 28 February 2007; accepted 7 March 2007

    Available online 12 April 2007

    Abstract

    Dutch organic soils have been found in past experiments to possess extremely high effective strength parameters. Since this

    finding is not expected and the phenomenon has yet to be explained, the high yield strength value is not used in practice.

    Understanding the abnormal properties of Dutch organic soils would thus be beneficial from the practical point of view. A

    programme aimed at understanding the unusual properties of Dutch organic soils, non-peat soils in particular, was performed on the

    representative organic soils in Dutch nature reserve park, Oostvaardersplasen (OVP) near Almere. Highly variable fabric of these

    organic soils was characterized by Computed Tomography X-ray scanner and environmental electronic microscope. Recognized

    fabric is in line with the geology of the OVP site. The multi-scale investigation as presented eventually identified the major role

    played by subhorizontal laminae and other non-organic microstructural elements (microfossil skeleton) in the high values of

    OVP organic soils. Deformation mechanisms of the microstructural elements are proposed and these make the unusual

    geotechnical properties explainable. Organics as involved were believed to have a primary contribution in increasing Atterberg

    limits and compressibility, and to allow the generation of high pore water pressures and low effective confining pressures during

    shearing. It has been also observed that high value is always correlated to the low effective confining pressure.

    2007 Elsevier B.V. All rights reserved.

    Keywords: Organic soils; Microfabric; Laminated soils; High friction angle

    1. Introduction

    Past experiments involving a large number ofundrained triaxial tests conducted on Dutch organic

    soils have led to the conclusion that the soils possess

    extremely high effective strength parameters which

    increase while the bulk density of the soil decreases

    (Den Haan, 1995). Since this finding is not in line

    with expectations and the phenomenon has yet to be

    explained, the high yield strength value is not used in

    practice.

    Organic soils cover a large part of the Netherlands.Infrastructure lines are founded on top of organic

    deposits and dikes are made of organic soils. Under-

    standing the abnormal properties of Dutch organic soils

    would thus be beneficial from the practical point of

    view. Depending on the mechanisms responsible for the

    high effective strength of organic soils, less conservative

    values could be used in the design of embankments, and

    more realistic estimations of the strength of dikes could

    be made. One might also think of mimicking nature to

    strengthen soils.

    Engineering Geology 93 (2007) 31 44

    www.elsevier.com/locate/enggeo

    Corresponding author.

    E-mail address:[email protected](X.H. Cheng).

    0013-7952/$ - see front matter 2007 Elsevier B.V. All rights reserved.doi:10.1016/j.enggeo.2007.03.009

    mailto:[email protected]://dx.doi.org/10.1016/j.enggeo.2007.03.009http://dx.doi.org/10.1016/j.enggeo.2007.03.009mailto:[email protected]
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    An international literature review reveals that organic

    soils with a high effective friction angle, are not

    unique to the Netherlands:

    a) An apparent of 34 was considered as particu-

    larly high for a slightly organic clay known as theBothkennar clay in Britain (Hight et al., 1992). The

    dominant angular silt fraction was thought to be

    responsible for the high-, and the 2 to 4% organic

    content was found to increase Atterberg limits.

    During testing, the effective mean stress ranged

    between 25 and 150 kPa.

    b) Relatively highbetween 25 and 40 are reported

    for the reconstituted Osaka bay clay (Tanaka and

    Locat, 1999). A microfossil identified as diatom was

    accounted for both the high- and high Atterberg

    limits. The role of 2 to 4% organic content was notemphasized. An effective friction angle of 44 was

    also found for the diatomaceous fill that has a low dry

    density and high moisture (Day, 1995). The reasons

    for this high effective friction angle were given by

    the interlocking and rough surface features of

    diatoms at low stress level. Effective mean stresses

    between 100 and 300 kPa were recorded during

    testing. This is higher than the stress levels reported

    by others for clays with a higher organic content.

    c) The 10% to 60% organic content of Juturnaiba

    organic clays in Brazil was found to increase the

    of natural samples according to the followingempirical relationship: = 23 + 0.5766 OC with

    OC, the organic content expressed in percentage

    (Coutinho and Lacerda, 1989). Angles were found to

    increase up to 57 with effective mean stress

    pressures decreasing from 300 to 50 kPa.

    d) A very high ranging between 60 and 90 was

    found for Swedish clayey gyttja with 10% organiccontent (Larsson, 1990). It was related to the

    abundance of micro-fibers discovered by electron

    scanning microscopy. However, whether the micro-

    fibers are organics or was not established. Effective

    mean stresses up to 100 kPa and as low as 15 kPa

    were recorded during testing.

    e) Organic clay from Cubzac-les-Ponts in France with

    organic contents up to 25% and bulk densities in the

    range 12 to 16 kN/m3, did not reveal particularly

    high angles (Shahanguian, 1981). From the

    reported CIU tests on normally consolidated clayunder effective mean stresses between 30 and 70 kPa,

    back calculation reveals only 2834 or less.

    f) Krieg (2000) studied the geotechnical properties of

    various organic clays from Schwerin, Berlin and

    Rotterdam, and found values ofranging from 44

    to 74. Bulk density varied from 1.2 to 1.5 t/m3 with

    organic contents up to 30%. Diatoms and remains of

    plant fibers were thought to be the cause of the high

    strength values. During testing, recorded minimum

    effective mean stresses were above 50 kPa.

    The multi-scale fabric of organic soils is highlyvariable and the fundamentals of their behaviour are not

    Table 1

    Geotechnical classification and index properties of OVP organic soils

    Depth

    (G.L., m)

    Geotechnical classification

    and identification.

    N(%) sa D50

    (m)

    Samples for triaxial compression

    No. Depth (m) Wn (%) n (g/cm3) a/r

    1.162.06 (a) Very organic brown silty clay,

    with very closely spaced thin laminae

    of fine grained silt (Almere deposits)

    1020 2.2552.455 5 CIU10A 1.181.35 144 1.332 1.0

    CIU10B 1.351.53 167 1.295 1.5

    2.062.78 (b) Very organic clayey dark brown silt,with very closely spaced thin laminae of

    medium-grained silt (Almere deposits)

    30 2.085 12 CAU11B 2.062.26 203 1.226 CAU11D 2.262.44 212 1.210

    CIU11C 2.642.84 257 1.145 1.7

    2.562.93 (c) Dark brownblack peat, with

    significant amounts of fine wood fibers.

    Spongy structure

    2.933.40 (d) Very organic light gray clayey silt,

    with very closely spaced thin laminae

    of mediumgrained silt and with

    vertical rootlets

    33 2.039 8 CIU12C 3.043.24 303 1.149 2.0

    CIU12A 3.243.42 148 1.264 1.0

    3.404.58 Mixed layers of very organic soils: (c) peat soil+ 70 1.602 CIU14A 3.413.51 355 1.074 2.0

    CIU14B 3.513.61 360 1.074 1.5

    (d) Very organic clayey SILT CAU13 4.024.22 323 1.198

    a

    Calculated by the relation 1/s=N/1.365+(1

    N)/2.695. This relation was obtained for Dutch organic soils according to the method used bySkempton and Petley (1970)for organic soils. The temperature used in loss-on-ignition test (N) was 550 C.

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    well understood. A programme aimed at understanding

    the unusual properties of Dutch organic soils, non-peat

    soils in particular, was launched in the 1990's. The

    Dutch nature reserve park in Oostvaardersplasen (OVP)

    near Almere, the Netherlands, was chosen as sampling

    site. The OVP Holocene soil deposits are believed to berepresentative of Dutch organic soils, which consist of

    layers of organic clay and silt and peat.

    The geology of the OVP site can be schematised

    usingVan Loon and Wiggers (1975). After the sea level

    rose at the end of the last ice age (Weichselien up to

    8000 BC), a peat layer was formed above Pleistocene

    sands. Sea transgressions and regressions succeeded

    each other. During transgressions large areas of peat

    were eroded and clay was formed. During regression,

    peat was formed. At the end of the subboreal (3000 to

    900 BC) several sea transgressions led to the formation

    of the Flevo lake. Peat was eroded by wave action and

    the lake expanded. A detritus-gyttja layer started to format about 1250 BC from the eroded peat in the fresh water

    environment of the lake. Around 0 BC, the connection

    of the Flevo lake to the Wadden Sea to the North became

    wider. In the fresh to slightly brackish waters of the

    newly formed Zuiderzee lagoon, the silts and clays of

    the Almere deposits were formed. They contain an

    upwards diminishing amount of organic matter derived

    Fig. 1. Stress paths and radial strain changes (a) silts b and d (b) clay a and peat c.

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    from peat and gyttja and several laminations of various

    thickness and gradation. The laminations are believed to

    be the result of wave and storm actions (Van Loon andWiggers, 1976). At about 1600 AD, the connection to

    the Wadden Sea rapidly widened even further. The water

    became brackish to salty and the marine deposits of the

    Zuiderzee were formed. The Zuiderzee was closed by a

    dike in 1932. Lake Ijssel was created and then reclaimed

    to form the Zuiderzee polder in 1968. Human activities

    resulted in the formation of a thin and reworked cover of

    fresh water soils: the Ijsselmeer deposits. The OVP are a

    nature reserve in this polder where little reworking has

    taken place. The upper layer has gone through several

    stages of weathering in recent decades.

    From the results of a preliminary laboratory testingprogramme which focussed on the soft organic clays of

    the Almere deposits, the samples were found to fail in

    undrained triaxial compression with values of 50 to

    60. The values were calculated assuming zero

    cohesion and the mobilized effective angle of internal

    friction was at maximum. The high values were

    found to remain irrespective of the sampler, sample size

    and consolidation history (Den Haan, 2003). The latter

    results eventually stimulated the multi-scale investiga-

    tion of the OVP organic soils, excluding peat, by using

    advanced microscopy technologies. The results arepresented hereafter. In the study, one attempts to relate

    the presence of microfossils, observed by means of

    electronic microscope, and the presence of silty lamina-

    tions, recognized by Computed Tomography X-ray

    scanner and electronic microscope to the high resistanceof the OVP soils. The use of these technologies is shown

    to be decisive for the comprehension of the behaviour

    of heterogeneous soils like OVP organic soils, even if

    it is not new. X-ray CT scanner allowed a major

    breakthrough in the understanding of shear strain

    localisation in sand specimens subjected to triaxial

    testing (Desrues et al., 1996). It also appeared suitable

    for the study of strain localisation in clayey materials

    in few occasions, when compacted shear bands form

    under large confining pressures (Tillard, 1992) or

    existing fissures affect macro-cracking (Sun et al.,

    2004). To discover the real-time fabric change ofclayey soils at different loading states, environmental

    scanning microscopy (ESEM) is useful, particularly

    when equipped in the ESEM chamber with a micro-

    loading module (Cheng et al., 2004 and Cheng,

    2004).

    2. Triaxial compression of OVP organics soils:

    Macro-level observations

    2.1. Profile description

    Samples down to 5 m below the ground level were

    recovered using the Delft Continuous Begemann

    Table 2

    Triaxial compression properties of OVP organic soils

    Soil type Test No. End of consolidation Failure, i.e. maximum shear stress state

    a() v () r() 3 (kPa) s (kPa) a() r() t(kPa) s (kPa) 3,f(kPa) () assuming c = 0

    Organic silt CIU11C 0.15 0.33 0.09 83 83 0.29 0.02 40 57 17 45

    CIU12A 0.05 0.17 0.06 39 39 0.17 0 17 25 8 43CIU12C 0.19 0.38 0.09 121 121 0.30 0.04 49 81 32 38

    CAU11B 0.20 0.16 0.02 30 45 0.26 0.05 27 34 7 52

    CAU11D 0.16 0.18 0.01 19 32 0.22 0.02 23 28 5 56

    CAU13 0.11 0.09 0.01 25 38 0.13 0.02 19 23 4 56

    Organic clay CIU10A 0.05 0.15 0.05 41 41 0.13 0.01 22 31 9 46

    CIU10B 0.12 0.27 0.08 83 83 0.35 0.03 35 57 22 38

    Peat CIU14A 0.08 0.17 0.04 40 40 0.17 0 22 25 3 63

    CIU14B 0.15 0.33 0.10 79 79 0.31 0.01 41 49 5 65

    Table 3

    Variation in and c with organic soil type and effective confining stress

    OVP a very organic silty clay 2 tests:

    CIU10A and CIU10B

    OVP b, d very organic clayey silt OVP c peat 2 tests:

    CIU14a and CIU14b3 CIU tests CIU11C,

    CIU12C and CIU12A

    3 CAU tests CAU11B,

    CAU11D and CAU13

    () 29.7 35.8 (R2= 0.974) 44.0 (R2= 0.990) 64.3

    c(kPa) 7.7 4.5 (R2= 0.974) 4.6 (R

    2= 0.990) 0

    n

    (g/cm3) 1.314 1.186 1.211 1.074

    3,f(kPa) 8.6; 22 8.1; 16.7; 31.6 4.0; 4.6; 7.1 3.0; 5.3

    34 X.H. Cheng et al. / Engineering Geology 93 (2007) 3144

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    sampler. FromDen Haan (2003), it can be expected that

    they are high quality samples which behave as Laval

    samples during consolidated triaxial testing. Visual

    inspection of the OVP cores and index properties

    (bulk density, specific density, natural water content,

    loss-on-ignition and particle size distribution) weredetermined. The results from the analysis are summa-

    rized inTable 1. Sand layers and the top deposits are not

    considered.

    The bulk density of OVP soils was found to decrease

    and fluctuate with depth. As expected, geotechnical

    indices of OVP organic soils were found to be highly

    variable at the centimeter scale of resolution of routine

    test measurements. For example, the water content of

    two neighboring samples CIU12A and CIU12C was

    found to deviate by 155%. Using XRD analysis, size

    distribution analysis and petrographic analysis on 30 mthick thin sections and natural samples, it was shown

    that OVP organic soils are mixtures of clay, silt and fine

    sand-size fractions. The clay-size fraction consists of

    illite, quartz, calcium carbonate and organics. The

    medium silt-size fraction dominates in the mixture and

    is made of quartz, calcium carbonate and organics. The

    fine sand-size fraction consists of quartz, pyrite, shells

    and organics. Organics present in the OVP soils are

    derived from eroded peat and gyttja formed in an earlier

    period. Wood fragments, stems and rootlets co-exist in

    the OVP soils with micro-organisms such as algae and

    plankton, amorphous organics and silicate and calcium

    carbonate microfossils. Some thin laminations of

    medium to coarse silts could be observed with the

    naked eye. In the dry state, the OVP soils do not

    disintegrate under light to moderate finger pressure due

    to the binding effect provided by their amorphous

    organic and clay fractions.Denomination of the OVP organic soils has not been

    possible due to the diversity of classifications proposed

    in the literature to distinguish true peats from organic

    soils. Progressive transition from one soil type to

    another renders the segmentation of the organic soils

    profile even more difficult. However, disregarding the

    top and bottom sandy layers, the soil profile was

    schematised as shown in Table 1 and four types of

    organic soils (a to d) have been identified accordingly.

    2.2. Description of testing programme

    After classification, 10 samples were selected. Samples

    66 mm in diameter and 150 mm in height (whenever

    sufficient material was available) were subjected to

    undrained triaxial tests after isotropic and anisotropic

    consolidation, abbreviated CIU and CAU respectively.

    Application of a back pressure of 200 kPa ensured

    saturation to a satisfactory level withB-values greater than

    0.94. The pore pressure was monitored in the traditional

    way at the sample ends and further by using a needle probe

    in the middle of sample. The ratio of the axial to the radial

    strain was calculated at the end of the isotropic

    Fig. 2. CT-numberdepth profile.

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    consolidation. The radial strain was derived frommeasurements of axial strain and volumetric strain made

    from the start to the end of the isotropic consolidation

    phase. Special attention was paid to the effects of shear

    rate and remoulding process on shear strength. Two

    undrained creep tests on anisotropically consolidated

    specimens were carried out under constant deviatoric

    stress to examine the possible reduction of strength due to

    an extremely low shear rate. One sample was brought to

    failure by undrained shear and subsequently subjected to a

    few cycles of unloadingreloading. The purpose of the so-

    called remoulding process in place was to examine the

    degradation of strength due to de-structuring.

    Fig.1 illustrates the stress pathsfollowed during testingin the deviatoric stress (t=1/2(13))effective mean

    stress (s =1/2(1+3)) plane as well as the change in

    radial strain as function of the effective mean stress.

    The observed strength results are summarized in

    Table 2per soil type and consolidation path. Initial soil

    bulk density and effective confining stress at failure

    (3,f) are also indicated.

    2.3. Results and discussions

    As can be seen inTable 1, the very organic clayey

    silts (soils b and d) form the important constituent of the

    Fig. 3. Laminations in sample 10B (a) CT-number profile (b) sample reconstitution after test (c) nebulous material in bright lamina, 5.0 cm from

    bottom. d) shell-like structures in zone in between bright laminae, 7.0 cm from bottom.

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    OVP organic soils. Despite some deviation in water

    contents, all b and d specimens present more or less the

    same loss-on-ignition. For the sake of simplicity, soils b

    and d will not be distinguished later on, as far as strength

    parameters are concerned. The presence of vertical

    rootlets in soil d caused several aborts during the triaxial

    tests and explains the divergence observed between the

    deformation behaviour of soils b and d.

    Values of N or s, Wn, n and a/r are listed in

    Table 1. They are the loss-on-ignition, the specific

    density, the natural water content, the bulk density and

    the ratio of axial strain to radial strain at the end of

    isotropic consolidation. They indicate respectively that

    all organic OVP soils are very organic, very light and

    slightly anisotropic. Despite having such properties, the

    position of their failure envelopes in the t-s' plane

    Fig. 4. Failure mode of Sample CAU11D: CT images are enhanced pictures with the threshold range of CT-number values in [400,680].

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    (Fig. 1) are extremely high and the following observa-

    tions can be made on their strength and their

    deformation characteristics, i.e., ratio of axial strain toradial strain at the end of isotropic consolidation and

    rebound of radial strain at the near failure state.

    The amount of binding (cohesion) is scattered and

    remains limited to a few kPa.

    If cohesion is ignored, values of' increase of 5 to

    15 and range between 38 and 56 for non-peaty soils

    and 65 for peaty soils (see Tables 2 and 3).

    The remarkably high values of were found to

    increase in the order of very organic clay, silt and

    then peat soils.

    The high of non-peat soils was found to beslightly related to the anisotropy of the samples in

    terms of the ratio of axial to radial strain measured at

    the end of isotropic consolidation (seeTable 1) and

    independent of the loading rate and remoulding

    process (CIU12A and CAU11A inFig. 1).

    As far as the peat soil samples (CIU 14A and 14B)

    are concerned, the failurewas reached without any

    subsequent decrease in shear stress, which eventually

    led to a constant Maximum at the post-failure

    state. This post-failurebehaviour can be explained

    by considering the sample geomet ry and theboundary conditions at the moment of failure: the

    samples became very flat after around 30% vertical

    compression, and possible activation of permanent

    shear bands was limited by the end restraints on flat

    samples. This stress feature is sufficient to distin-

    guish peat soil from other organic soils, in addition to

    the abundance of plant remains.

    All samples were found to fail with high at a

    considerably low effective confining stress (b35 kPa).

    This observation is in agreement with the trend

    observed byKenney et al. (1967), for clayey soils up

    to a normal stress of 100 kPa. But, values of the

    OVP soils were found to be significantly higher than

    those reported by Kenney et al. and close to those

    observed by Coutinho and Lacerda (1989) and Larsson

    (1990) for organic soils. Microscopic observations

    presented in next section will clarify this point.

    The influence of consolidation history on strength forvery organic clayey silt is noticeable. The triplet of

    CAU tests on OVP soils b and d led to a lower

    effective confining stress and a 8 higher than the

    triplet of CIU tests as indicated inTable 3.

    All samples were strongly compressed during shear,

    and failed near the point where the sample diameter

    was restored to its initial size by the lateral extension

    during shear, i.e. at around r=0% in the graphs of

    Fig. 1a and b, seeTable 2. Sample CIU12C (shown in

    Fig. 1a) was an extreme exception, probably due to

    the inclusion of several vertical rootlets. Thisdeformation feature indicates that all organic soil

    samples at their initial state had little possibility of

    lateral extension except to collapse. Nevertheless,

    both vertical and lateral compressions were allowed

    with slight anisotropy as mentioned earlier. Micro-

    scopic observations presented in the next section will

    elucidate this point.

    3. Unusual minifabric of OVP organic soils at

    submillimeter scale

    The observation of high variability of the OVPindices and the inverse correlation between their high-

    values and bulk density have given reason to study the

    density distribution at submillimeter scale (0.10.5 mm).

    A medical Computed Tomography X-ray scanner

    (Cheng and Ngan-Tillard, 2006) was used to inspect

    undisturbed sample cores in depth (see Fig. 2) with a

    resolution of 0.290.291 mm3. The attenuation of

    the X-rays is called the CT-number and is measured in

    Hounsfield units (HU) which are defined as HU=1000

    (water) /water where and water are the linear

    attenuation coefficients of the material and water,respectively. Variations in CT-numbers are known to

    correlate to either changes in bulk density or chemistry

    or both. Six samples as listed in Table 1 were also

    scanned after the triaxial tests in order to visualize the

    failure mode.

    Scans of 1 mm thick 66 mm diameter soil slices were

    made at 1, 4 or 100 mm intervals. In Fig. 2, each solid

    point corresponds to the average CT-number of four 1 mm

    thick slices and the arrows indicate the positions of two

    samples CIU10B and CAU11D subjected to detailed

    scanning after shearing. The images of the specimens after

    the test are displayed inFigs. 3 and 4respectively. The

    Table 4

    Correlation of CT-numbers, bulk densities and of all scanned

    samples

    Scanned

    sample

    ()

    n

    (g/cm3)

    Mean of

    CT-number

    values PHU

    Standard

    deviation of

    CT-number

    values

    CAU11A

    (undrained creep)

    1.307 498 91

    CIU10B 29.7 1.405 619 133

    CAU13 44 1.22 440 236

    CAU11D 44 1.25 432 87

    CIU11C 35.8 1.219 370 128

    CIU12C 35.8 1.204 208 211

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    CT-number profile of sample CIU10B is shown in Fig. 3a.

    Changes of CT-number profiles of sample CAU11D

    caused by triaxial testing are shown inFig. 5.

    From the CT analysis, the following observations can

    be made on the material variability:

    The CT-numbers of the OVP soils oscillate but

    gradually decrease with depth

    Several magnitudes and lengths of oscillations are

    observed both in overall CT-number profile (Fig. 2)and

    at the meso-scale within the samples (Figs. 3 and 5).

    Peaks in CT-number profiles correspond to the

    presence of light subhorizontal laminae in the CT

    images.

    A light subhorizontal laminae appears about every

    3 cm in sample CIU10B. Its cross-section is

    characterized by the presence of a nebula of moreattenuating material (seeFig. 3c). Visual inspection

    of sample CIU10B after failure allowed to correlate

    the light subhorizontal laminae of the CT images to

    23 mm thick silty layers. Other slightly darker

    laminae are visible on the CT images of sample

    Fig. 5. Statistical analyses of CT-numbers over sample CAU11D.

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    CIU10B and CAU11D but cannot be detected with

    the naked eye on the failed samples. Lenses of attenuating material can be found in cross-

    sections recorded outside the light and slightly darker

    laminae. This is the case for the slice recorded at a

    distance of 5.0 cm from the bottom of sample

    CIU10B and shown in Fig. 3d. Lenses can be

    oriented vertically rather than horizontally.

    The CT analysis also allowed to visualize the 3D

    geometry of the failed samples.

    The failure mode of sample CAU11D combined an

    inclined shear plane in the upper part with a major

    vertical crack at the bottom (Fig. 4). The shear plane

    formed across several dense laminae while the

    vertical cracking detached the weak part at the

    bottom. In the cross-section at 8 cm from the bottom

    where the shear band is present (Fig. 4d), lenticular

    elements are noticeable, even at a micro-CT levelshown in Fig. 4(e). One cross-section of sample

    CAU11D changed due to triaxial shear as visualized

    in Fig. 4(b) and (c). It can be seen that around this

    section more vertical cracks (the dark zones in the

    image) were developing when the sample failed. So,

    the splitting failure mechanism cannot be excluded in

    the inter-laminate zones especially when the effective

    lateral stress is low. The role played by weak zones

    present in the sample before testing (Fig. 4b) will

    have to be clarified.

    Fig. 6. Microstructure of marked denser lamina of sample 10B (after

    triaxial test).

    Fig. 7. Microstructure of marked denser lamina of sample CAU11D(after triaxial test).

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    Sample CIU10 B turned out to be exceptional. A

    continuous increase of shear stress during triaxial

    testing was observed as shown in Fig. 1 with a

    bending point marked with a star in theFig. 1b. Thissample would have reached a much higherthan if

    the maximum shear stress had been reached. Its

    mobilized is 29.7 at bending point against 60 at

    the end of the test. Bright subhorizontal laminae were

    found in abundance in the CT images and no

    permanent shear band could be identified across the

    sample in the CT images. The exceptional stress

    behaviour might be correlated to the CT observations.

    A statistical analysis of CT-numbers for all the

    scanned samples has made possible the correlation of

    the mean and deviation values of CT-numbers per

    sample together with the bulk densities (after triaxial

    compression) and -values measured in the laboratory.

    Results are gathered in Table 4. Assuming a homoge-

    neous chemistry for all samples, the following relation-

    ship has been derived by fitting all the data in the table,

    which enabled the transformation of average CT-numbers (PHU) to the bulk density (

    n) for any volume

    (minimum volume: 0.30.31 mm).

    gn 0:0006P

    HU1 3:1

    The relationship has an R-square of 0.84 and is valid

    for OVP soils with a bulk density ranging from 1.05 to

    1.35 g/cm3. Similar correlations are available in the

    literature (Cortellazzo et al., 1995) but could not be used

    for the OVP soils as they were established for materials

    of different nature and structure and using different CTparameters.

    The six samples scanned after testing were grouped in

    pairs according to the soil type and the bulk density level

    in Table 4. It may be seen that a clear correlation of

    density to does not exist. Neither do more

    homogenous samples, i.e. the ones with less deviations

    of CT-numbers necessarily correlate with higher

    values. But more detailed analysis of CT-numbers over

    sample CAU11D enables a better understanding of local

    deformation. The increased CT-number values shown in

    Fig. 5a after the test are obviously the consequence of the

    consolidation that made the sample denser. By analyzingthe length changes of three parts (bottom, middle and

    top, each of them 5 cm long) the axial strains at the end of

    test are calculated to be approximately 20% for both

    bottom and middle part and 40% for the top part

    respectively. The mean of these three local deformations,

    i.e. 27%, well agrees with the axial strain value measured

    by means of LVDT during the test. The CT-number per

    voxel over different parts of this sample as shown in

    Fig. 5b does not follow a normal distribution since the

    histogram envelopes are skewed and present several

    peaks especially for the middle part of the samplebecause of the presence of laminae. The volume of three

    different parts after test are determined by fitting the

    maximum square inside each CT image of the core. They

    are 121.5, 132.8 and 112.3 cm3 for the low, the middle

    and the top parts respectively. With respect to the initial

    volume of 160.8cm3 ( =6.4 cm,H=5 cm) of each part,

    the relative volume changes are 24%, 17% and 30% for

    the three parts. As the average of these ratios of 24% does

    not agree with average volume change of 18.6%

    measured at the end of triaxial test, the corrected relative

    volume change with respect to the measured average

    volume change are used to represent the local volume

    Fig. 8. (a) Representative microfabric of OVP non-peat organic soils:

    deflocculated matrix of fine flat/porous silts (before consolidation test,

    broken diatoms as indicated). (b) Organics: plant remains in the debris

    aggregate, possibly wood cellular walls indicated by arrows (after

    consolidation test).

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    strain of different parts of sample CAU11D, i.e. 18% forthe bottom, and 13% for the middle and 23% for the top.

    Local radial strain of the bottom, middle and top parts

    then follow equal to 1%, 3.5% and 8.5%, all in extension.

    These values of local deformations confirm that denser

    laminae as more presented in bottom and middle parts

    than in the top part could more restrict axial compressive

    and radial extensional deformation.

    In conclusion, the unusual minifabric of the OVP non-peat soils has been studied by means of the CT-scanner.

    Two types of ministructures are thought to affect the shear

    strength and deformation of OVP samples: subhorizontal

    light and slightly darker laminae and, outside laminae

    light lenses. Zones containing more laminae were found

    to deform less both axially and radially. In the weakest

    part of the samples, the splitting failure mechanism cannot

    Fig. 10. Schematic diagram of micro-deformation mechanisms of observed different layers (inside and outside denser laminae.

    Fig. 9. Intact diatom embedded in amorphous organics (Existence of much carbon in EDAX results indicates the presence of organics and calciferous

    matter together with Ca as indicated. The sulphate may be also present as a relatively high amount of S indicates).

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    be excluded when confining stress is low. The micro-

    structure of the laminae and lenses is analyzed in the

    following section to better understand their contribution

    to the strength of the OVP soils.

    4. Microfabrics of OVP soils (up to a few tens ofmicrometers across)

    Optical and electron microscopy equipped with EDAX

    (energy diffraction analysis of X-rays for chemical

    element identification) were used for the close-up

    observation of the areas marked in Fig. 3(b) (sample

    CIU10B) andFig. 4(a) (sample CAU11D). The denser

    lamina of sample 10B was dominated by angular, platy

    and elongated siliceous silts, while organic micro-fibers

    were also identified with EDAX (Fig. 6). More or less the

    same microstructures were found for the bright laminabesides the shear band zone in sample CAU11D, shown in

    Fig. 7, with the impression that more elongated and

    lenticular siliceous silts (broken diatoms) were present.

    Outside the laminae, a looser microfabric was

    identified in which much finer silts and clay dominated

    the soil matrix with a much higher content of organics.

    Fig. 8a illustrates such a microfabric of the organic silts of

    soil type d. This chosen microfabric is believed to be

    representative. The silts generally included quartz frac-

    tions, broken diatoms, shell and faeces fractions while

    organics were present in variable size and form (seeFigs.

    8b and 9). This kind of deflocculated matrix is capable ofholding much water and contributes greatly to the high

    compressibility of the soil. Lenses found on the CT

    images outside the laminae can be microfossils (diatom or

    shell or unknown microfossils) or other silicates etc.

    The close observation of the material inside and

    outside the dense laminae allows to postulate the fol-

    lowing micro-mechanisms as sketched inFig. 10, which

    are considered to be responsible for the high friction angle

    of OVP organic soils. The medium-coarse siliceous silts

    inside denser laminae and the fine siliceous/carbonate silts

    outside interlock during deformation due to their shapes,either angular or elongated or even lenticular. The inter-

    locking mechanism prevails inside denser laminae

    because of the higher contact opportunity of silts. But it

    can also take place in the looser material when samples

    have gone through a consolidation process. Main siliceous

    silts involved in OVP organic soils were broken diatoms

    with lighter specific density (1.92.2 g/cm3) than quartz

    (2.65 g/cm3). Broken diatom-related silts have very rough

    surfaces because of their nano-pores. Broken diatoms led

    to many elongated or lenticular silt-size fractions in OVP

    organic soils. Although the micro-mechanical properties

    of lenticular elements deserve further study, one can

    imagine that they can sustain considerable amount of

    tensile stress rather than compressive stress.

    5. Concluding discussions

    1) From geotechnical classification point of view, naturalOVP organic soils contain three types of soft soils, e.g.

    very organic clay, very organic silt and peat soil. Despite

    a large spread in index properties, all OVP organic soils

    exhibit extremely high values of during consolidated

    undrained triaxial compressions. The macro-mechani-

    cal properties of OVP organic soils depend on details of

    multi-level fabric to varying degrees. The multi-scale

    investigation as presented bridged the gap between

    laboratory observations and microstructure, which

    eventually identified non-organic microstructural ele-

    ments serving as internal confinement in OVP organicssoils. Deformation mechanisms of the microstructural

    elements are proposed and these make the unusual

    geotechnical properties explainable.

    2) On one hand, the presence of dense subhorizontal

    laminae is revealed. The laminae are shown to be rich

    in angular and platy particles of medium silt size which

    are believed to interlock during deformation and

    contribute to the high strength of the OVP soils. We

    have defined a programme focused on the influence of

    laminae on the strength and deformation of OVP soils

    by testing samples with and without laminae in simple

    shear and Ko oedometer. On the other hand, lense-likestructures are observed at several scales outside dense

    laminae and are believed to have a role of self-

    confinement in much the same way as horizontally

    orientated plant fibers in peat. We propose to elucidate

    their role in the high strength of the OVP soils in a

    Distinct Element Modelling environment.

    3) In the OVP tested soils organic materials were

    believed to have a primary contribution in increasing

    Atterberg limits and compressibility. But their role in

    increasing strength was not evident except in peat

    soil. Coexistence of organics and microfossils madeidentification of organics difficult. On the other hand,

    unlike in fibrous peat the fibrous microstructural

    elements were difficult to detect in a back-swap light

    microscopy equipped in several geotechnical labo-

    ratories, simply because of their non-organic nature.

    4) Organics and microfossils are associated to high

    water content and allow the generation of high pore

    water pressures and low effective confining pressures

    during shearing. It has been observed that high

    value is always correlated to low effective confining

    pressure. Moreover samples show little possibility of

    lateral extension other than collapse.

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    5) Further investigation of the mechanics of microfab-

    rics will enhance the understanding of the fundamen-

    tal behaviour of soft organic soils. It may also enable

    the creation of innovative ground improvement

    techniques based on smart geomaterials.

    Acknowledgements

    This research was supported by Delft Earth Research

    Centre. Part of the experimental work was performed

    with the CT scanner purchased by TUDelft within the

    framework of the STW project entitled Control of flow

    in porous media using gels.

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    44 X.H. Cheng et al. / Engineering Geology 93 (2007) 3144