TESTAMERICA - ST. LOUIS TestAmericaTestAmerica THE LEADER IN ENVIRONMENTAL TESTING TESTAMERICA - ST....

TestAmericaTHE LEADER IN ENVIRONMENTAL TESTING

TESTAMERICA - ST. LOUIS

TestAmerica Laboratories, Inc.

ANALYTICAL REPORT

REVISED·

PROJECT NO. 1991-135-11/002

Boneywe11 Ponds E

Lot #: F9E010259

sean Chisek

Andrews Engineering, Inc.3300 Ginger Creek Drive~ringfield, IL 6271~

TESTAMERICA LABORATORIES I :INC.

January 7, 2010

LOT#F9E010259_REVISED1~71 ~ RioprTritil North F~rth (itv. MO n~n4r; t91 ~14.,qA.Rt;nti fax ~14.?qR_R757 www.testamericainc.com

1 of 36

F9E010259 (7): E-62F9E010259 (8): E-61F9E010259 (9): E-60F9E010259 (10): E-59F9EO10259 (11): E-58F9E010259 (12): E..57


Case NarrativeLOT NUMBER: F9E010259

Revised

This report contains the analytical results for the 12 samples received under chain of custody by STL81. Louis on May 1,2009. These samples are associated with your HoneyYIell Ponds E project.

The analytical results included in this report meet all applicable quality control procedure requirementsexcept as noted on the following page.

The test results in this report meet all NELAP requirements for parameters in which accreditations areheld by STL St Louis. Any exceptions to NELAP requirements are noted in the case narrative. Thecase narrative is an integral part of this report.

All chemical analysis results are based upon sample as received, wet weight, unless noted otherwise.All radiochemistry results are based upon sample as dried and ground with the exception of tritium,unless requested wet weight by the client.

This report Is revised to report Chemistry data on a wet-weight basis.

ObservationslNonconformances

Reference the chain of custody and condition upon receipt report for any variations on receipt conditionsand temperature of samples on receipt.

Trace ICP Metals

Batch 9125076:The MS (MSD) recovery for uranium is outside the established QC limits. The RPD is within methodacceptance criteria indicating a possible matrix interference. Method performance is demonstrated byacceptable LeS recovery.Affected Samples:F9E010259 (1): E-52F9E010259 (2): E-53F9E010259 (3): E-54F9E010259 (4): E-55F9E010259 (5): E-63F9E010259 (6): E-56

There were no nonconformances or observations noted with any other analysis on this lot.

LOT#F9EOI0259 REVISED 2 of 36


METHODS SUMMARY

F9E010259

.ANALYTICAL_P_ARAME-T-E_R M_ET_H~O_D _

PREPARATIONMETHOD

Method D2216 Percent H20 Dry 105 Degrees C, WeighTrace Inductively Coupled Plasma (Iep) Metals

References:

ASTM Moisture,SW846 GOlOB

ASTM ASTM 2216

ASTM

SW846

Annual Book Of ASTM Standards.

"Test Methods for Evaluating Solid Waste, Physical/ChemicalMethods n , Third Edition, November 1986 and its updates.



SAMPLE SUMMARY·

F9BOI0259

04/29/09 08:2504/29/09 09:0504/29/09 09:4504/29/09 10:3004/29/09 12:3004/29/09 12:~O

04/29/09 13:0004/29/09 14:3004/30/09 08:4504/30/09 10:3004/30/0.9 12:4504/30/09 13:05

wo # SAMPLE# CLIENT SAMPLE ID

LA7EN 001 E-52

LA7EV 002 E-53LA7EW 003 E-54LA7EO 004 E-55LA7E2 005 E-63LA7E3 006 E-56LA7E6 007 E-62LA7E8 008 E-61LA7FA 009 E-60

LA7FC 010 E-59

LA7FE 011 E-58LA7FG 012 E-57

HOTE(S) :

• The analytical results of the samples listed above arc presented on the following pages.

- All calculations are performed. before rounding to avoid round-off errors in calculated results.

- Results noted as liND" were not detected at or above the stated limit.

- This report must not be reproduced. except in full~ without the wriuen approval oCthe laboratory.

- Results for Ute following parameters are Dever reported on a dry weight basis: color. corrosivity, density, flashpoint, ignitability~ layers, odor,

paint filter test, pH, porosity pressure, reactivity, redox potential, specific gravity, spot tests, solids. solubility. temperarore, viscosity ~ and weight.

SAMPLEDDATE

SAMPTIME



Andrews Engineering. Inc.

Client Samp1e ID: E-52

TOTAL Meta1s

Lot-Sample # •.. : F9E010259-001Date Sampled... : 04/29/09 08:25 Date Received.• : 05/01/09% MOisture...•. : 47

Matrix..... ~.: SOLID

REPORTING PREPARATION- WORK_PARAM:__E_T_E_R RE_S_UL_T LIMIT _UN_I_T_S ,;.",;,ME.;...T""-H_O_D__----- ANALYSIS DATE ORDER #

Dilution Factor: 1

Prep BatCh ft .•• : 9125076Uraniwn 96 • 4

LOT#F9EOI0259 REVISED

50.0 mg/kg SW846 6010B'Analysis Time .. : 23:17

05/05/09 LA7ENlAD

5 of 36

Lot-Sample I ... : F9EOI0259-001Date ~led.•. : 04/29/09 '08:25% Moisture•.... : 47

Andrews Engineering./ Inc_

Client Sample ID: E-52

Genera1 Chemistry

Work Order # ... : LA7EN

Date Received.• : 05/01/09


Matrix..•. _..•. : SOLID

PARAMETER

Percent MoistureRESULT47.1

LOT#F9E010259 REVISED 6 of 36


Andrews EngineeringJ Inc.


TOTAL Metals

Lot-Samp1e I : F9E010259-002Date Sampled : 04/29/09 09:05 Date Received.. : 05/01/09'Moisture : 44

Matrix : SOLID

WORKORDER #RESULTPARAMETER

REPORTING PREPARATION-LIMIT UNITS METHOD ANALYSIS DATE---------- ~~~-~~ ----- ---------

Dilution Factor: 1

Pr~ BatCh I ••• : 9125076Uranium 215 50.0 mg/kg SW846 6010B

Analysis Time .. : 23:55

05/05/09 LA7EVlAD


Andrews Engineering, Inc_

Client S~le 10: E-53

General Chemistry


Lot-Sample I : F9E010259-002Date Sampled : 04/29/09 09:05% Moisture : 44

PARAMETERPercent MOisture

Work Order :It ••• : LA7EV

Date Received•• : 05/01/09Matrix•......•. : SOLID

Dilution Pactor: 1



Andrews Engineering, Inc.

Client Sample ID: B-54

TOTAL Metals

Lot-Sample I : F9EOI0259-003Date Sampled : 04/29/09 09:45 Date Received.. : 05/01/09% MOisture•••.. : 46

Matrix._._._.: SOLID

RESULTPARAMETERREPORTING PREPARATION- WORKLIMIT UNITS METHOD ANALYSIS DATE ORDER #------- ----~~ ~--~----------

Dilution Factor: 1

Prep Batch I ... : 9125076Uranium 125 50.0 mg/kg SW846 6010B


05/05-05/06/09 LA7EW1AD



Client S~le ID: E-54

General Chemistry


Lot-Sample I ... : F9E010259-0Q3Date ~led••• : 04/29/09 09:45., Moisture..•.. : 46

PARAMETERPercent Moisture

Work Order # •.• : LA7EWDate Received.• : 05/01/09

Matrix•..•..•.. : SOLID

Dilution Factor: 1





TOTAL Metals

Lot-Sample I : F9EO~0259-004

Date Sampled : 04/29/09 10:30 Date Received.. : 05/01/09, MOisture••••• : 44

Matrix.•..... : SOLID

RESULTPARAMETERREPORTING PREPARATION- WORKLIMIT UNITS METHOD ANALYSIS DATE ORDER #------- ------ ----- ---------

Dilution Factor: 1

Prep Batch I ... : 9125076uranium 184 50.0 mg/kg 811846 6010B

Analysis Time.~: 00:08

05/05-05/06/09 ·LA7BO~



Andrews Engineering, Inc_


General Chemistry

Lot-sample I ... : F9E010259-004Date sampled•.• : 04/29/09 ~O:30

t Moisture••.•• : 44

Work Order I ... : LA7EODate Received.. : 05/01/09

Matrix•.••....• : SOLID

Dilution Factor: 1

PREPARATION- PREP_PARAMET_E_R_- - _RE_S_UL_T__ RL _UN_I_T_S ME__TH_O_D ANALYSIS DATE BATCH #Percent Moisture 44.3 0.10 t ASTM MOisture. % 05/09-05/11/09 9131060




Andrews Engineering, Inc ..


TOTAL Metals

Lot-sample i ... : F9E010259-005Date Sampled..• : 04/29/09 12:30 Date Received•• : 05/01/09'Moisture..... : 47

Matrix••..... : SOLID

REPORTING_P_ARMJIE__T_E_R_~~ _RE_S_UL_T~~__ LIMIT UNITS METHOD

WORKORDER #

Prep BatCh I ... : 9125076Uranium . 142 50 .. 0 mg/kg 8W846 6010B 05/05-05/06/09 LA7E2~

LOT#F9E010259 REVISED

Dilution Factor: 1 Analysis Time .. : 00:15

13 of 36

Andrews Engineering I Inc.

Client sample 10: E-63

Genera1 Chemistry


Lot-Sample I ... : F9E010259-005Date ~led••• : 04/29/09 12:30% MOisture.. __ .: 47

PA.RAr-mTERPercent Moisture

work Order :It ••• : LA7E2Date Received•• : 05/01/09

Matrix.......•. : SOLID

Dilution Factor: 1




C1ient Sample ID: E-56

TOTAL Metals

Lot-Sample 1_ •• : F9E010259-006Date Sampled : 04/29/09 12:10 Date Received.• : 05/01/09'Moisture : 50

Matrix : SOLID

PARAMETERREPORTING PREPARATION-LIMIT UNITS METHOD ANALYSIS DATE------ ---------

WORKORDER #

Prep Batch 1_ •• : 9125076Uranimn 120

LOT#F9EOI0259_REVISED

50.0 mg/kgDilution Factor: 1

SN846 6010B 05/05-05/06/09 LA7E3~


15 of 36


Client sample ID: E-56

General Chemistry

Lot-sample i ... : F9E010259-006 Work Order I ... : LA7E3Date ~1ed.•. : 04/29/09 12:10 Date Received•• : 05/01/09% Moisture•.•.• : 50




Matrix...•••••. : SOLID

16 of 36


Andrews Engineering. Inc_


TOTAL Metals

Lot-Sample 1 : F9E010259-007

Date Sampled•.. : 04/29/09 13:00 Date Received•. : 05/01/09\ Moisture••••. : 46

Matrix_. __ ._.: SOLID

RESULTPARAMETERREPORTING PREPARATION- WORKLIMIT UNITS METHOD ANALYSIS DATE ORDER #------- ------ ----- ---------

Dilution Factor: 1

Prep BatCh I ... : 9125076Uranium 261 50.0 mg/kg SW846 6010B


05/05-05/06/09 LA7E61AD

LOT#F9E010259_REVISED 17 of 36



Client Sample ID: E-62·

General Chemistry

Lot-Sample # ... : F9E010259-007Date sampled•.. : 04/29/09 13:00% Moisture.•... : 46

Work Order # ••• : LA7E6Date Received•• : 05/01/09

Matrix....•••.. : SOLID

Dilution Factor: 1



PREPARATION- PREPRL _UN__I_T_S ME_T_H_O_D - ANALYSIS DATE BATCH #0.10' ASTM MOisture, % 05/09-05/11/09 9131060


18 of 36


Andrews Engin~ering, Inc.


TOTAL Metals

Lot-Sample I : F9EOI0259-008Date Sampled : 04/29/09 14:30 Date Received•• : 05/01/09t MOisture : 49

Matrix : SOLID

PARAMETERREPORTING PREPARATION-LIMIT UNITS METHOD ANALYSIS DATE----- .;...~......;...------

WORKORDER #

Dilution Factor: 1

Prep Batch I ... : 9125076Uranium 137


50.0 mg/kg SW846 6010BAnalysis Time .. ~ 00:34

05/05-05/06/09 LA7B81AD

19 of 36

Andrews Engineering. Inc.

Client S~le ID: E-61

General Chemistry


Lot-sample I ... : F9E010259-008Date Samp1ed••. : 04/29/09 14:30% MOisture ..... : 49

PARAlVIETER

Percent Moisture

Work Order :ft. ••• : LA7E8Date Received•• : 05/01/09

Matrix...•..... : SOLID

Dilution Factor: 1

LOT#F9EOI0259_REVISED 20 of 36



Client sample ID: E-60

TOTAL Metals

Lot-S~le #_._: F9E010259-009Date S~led••• : 04/30/09 08:45 Date Received.. : 05/01/09% MOisture..... : 48

Matrix.•..... : SOLID

PARAMETER RESULT

Dilution Factor; 1

Prep Batch I ... : 9125076Uranium 410


50.0 mg/kg SW846 6010BAnalysis Time .. : 00:40

05/05-05/06/09 LA7FA1AD

21 of 36



General Chemistry


Lot-Sample I : F9EOI0259-009Date Sampled : 04/30/09 08:45% MOisture•.•.. : 48


Work Order 1: .... : LA7FADate Received•. : 05/01/09


Dilution Factor: 1





TOTAL Metals

Lot-Sample I : F9E010259-010Date Samp1ed : 04/30/09 10:30 Date Received.• : 05/01/09t Moisture : 46

Matrix•...... : SOLID

RESULTPARAMETERREPORTING PREPARATION- WORKLIMIT UNITS METHOD ANALYSIS DATE ORDER #

------~ ------ ----- ----~~---

Dilution Factor: 1

Prep BatCh I ... : 9125076Uranium 297 50.0 mg/kg SW846 6010B


05/05-05/06/09 LA7FC~





General Chemistry

Lot-Sample # ••• : F9E010259-010·Date S~led..• : 04/30/09 10:30'MOisture..... : 46

Work Order #•.• : LA7FCDate Received•• : 05/01/09


Dilution Factor: 1


LOT#F9E010259_REVISED

PREPARATION- PREPRL UNITS METHOD ANALYSIS DATE BATCH #----- ---------0.10' ASTM Moisture, % 05/09-05/11/09 9131060


24 of 36



Client sample ID: B-58

TOTAL Meta1s

Lot-Sample 1 __ .: F9E010259-011Date S~led_ .. : 04/30/09 12:45 Date Received.. : 05/01/09'MOisture•.•.. : 49

Matr~ : SOLID

WORKORDER #RESULTPARAMETER

REPORTING PREPARATION-LIMIT UNITS METHOD ANALYSIS DATE

--~~--- -~~~-~ ~---- ---------

Dilution Factor~ 1

Prep BatCh I ... : 9125076Uranium 122 50 ... 0 mg/kg SW846 6010B


05/05-05/06/09 LA7FBLAD




·Client Sample In: 8-58

General Chemistry

Lot-Sample I ... : F9E010259-011Date Samp1ed•.. : 04/30/09 12:45'Moisture..... : 49

Work Order I ... : LA7FEDate Received.. : 05/01/09

Matrix....•.... : SOLID

Dilution Factor: 1

PA.R.AI"!ETER

Percent Moisture


PREPARATION- PREPRL _UN_I_T_S ~ME_T_H~O_D ANALYSIS DATE BATCH #0.10 \ ASTM MOisture. t 05/09-05/11/09 9131060


26 of 36



C1ient ~le ID: E-57

TOTAL Metals

Lot-Sample I ... : F9EOI0259-012Date S~led._.: 04/30/09 13:05 Date Received•• : 05/01/09~ Moisture .•••• : 46

Matrix•...... : SOLID

PARAMETERREPORTING PREPARATION-LIMIT UNITS METHOD ANALYSIS DATE----- --------~---

WORKORDER #

Dilution Factor: 1

Prep BatCh •••• : 9125076uranimn 693


50.'0 mg/kg 8W846 6010BAnalysis Time~.: 01:13

05/05-05/06/09 LA7FG1AD

27 of 36



Client Samp1e ID: E-57

Genera1 Chemistry

Lot-Sample # : F9EOI0259-012Date Sampled : 04/30/09 13:05% MOisture ••••• : 46

Work Order 1: .... : LA7FGDate Received.. : 05/01/09

Matrix•..•.•..• : SOLID

Dilution Factor: 1



PREPARATION- PREP

RL UNITS METHOD ANALYSIS DATE BATCH #----- ---------0.10 \ ASTM MOisture. t 05/09-05/11/09 9131060

Analysis Time .. = 00:00

28 of 36


METHOD BLANK REPORT

TOTAL Meta1s

Client Lot B... : F9E010259 Matrix : SOLID

PARAMETERREPORTING PREPARATION-LIMIT UNITS METHOD ANALYSIS DATE----- ---------

WORKORDER #

MB Lot-Sample I: F9E050000-076 Prep BatCh I ... : 9125076Uranium ND 50.0 mg/kg SW846 GOlOB

Dilution Factor: 1


HOTE(S) :

Calculations are performed before rounding to avoid round-off errors in ~Iculated resulrs.


05/05/09 LCA6K1AA

29 of 36


LABORATORY CONTROL SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot I ... : F9E010259 Matrix : SOLID

METHODPARAMETERPERCENTRECOVERY

RECOVERY

LIMITSPREPAR.A.TION-ANALYSIS DATE WORK·ORDER #---------

LCS Lot-S~le#: F9EOSOOOO-D76 Pr~ Batch # ... : 9125076Uranium 110 {SO - 120} SW846 60l0B 05/05/09 LCA6KIAC

Dilution Factor: 1

HOTElS) :Calculations are performed before rounding to avoid round-off errors in calculated results.


Analysis Time AA: 23:10

30 of 36

MATRIX SPIKE SAMPLE BVALtIATIOll REPORT

TOTAL Metals

Client Lot ft ••• : F9E010259Date S~led._.: 04/29/09 08:25 Date Received•• : 05/01/09


Matrix : SOLID

PARAMETERPERCENTRECOVERY

RECOVERY

LIMITS RPD

RPD

LIMITS METHODWORKORDER #

MS Lot-samp1e #: F9E010259-001 Prep Batch 1_ •• : 9125076

Uranium 147 N210 N

(75 - 125)(75 - 125) 23

SW846 60l0B(O-30) SW846 60l0B

t MOisture..... : 4705/05/09 LA7EN1AE05/05/09 LA7ENIAF

NOTE(S) :

Dilution Factor: 1


Calculations are performed before rounding to avoid round-off errors in calculated results.

N Spiked analyte recovery is outside stated control limits.



MATRIX SPIKE SAMPLE DATA REPORT

TOTAL Metals

Client Lot B••• : F9E010259Date S~1ed.•• : 04/29/09 08:25 Date Received.. : 05/01/09

Matrix.••..•••. : SOLID

SAMPLE SPIKE MEASRD PERCNT PREPARATION-PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE---- ~----- -------

MS Lot-~le #: F9EOI0259-001 Prep Batch I ... : 9125076t MOisture .•.•. : 47

Uranium

WORKORDER #

96.4 100 244 N mg/kg 147 SW846 GOlOB96.4 100 307 N mg/kg 210 23 SW846 6010B

Dilution Factor: 1

Analysis Time •. : 23:42

05/05/0905/05/09

LA7EN1AELA7ENIAF

NOTE(S) :

Calculations are perfonned before rounding to avoid round-off errors in calculated results..

N Spiked analyte recovery is outside Stated control limits.

LO.T#F9E 010259_REVI SED 32 of 36


SAMPLE DUPLICATE EVALUATION REPORT

General Chemistry

Dilution Factor: 1

Matrix.••.••. : SOLID

RPD PREPARATION- PREPLIMIT METHOD ANALYSIS DATE BATCH #

SD Lot-Sample #: F9E010259-012(0-0.0) ASTM Moisture/ % 05/09-05/11/09 9131060

Analysis Time .. : 00:000.13

RPD

Work order I ... : LA7FG-SMPLA7FG-DUP

Date Received•• : 05/01/09

%46.3

tmITS-----PARAM RESULTPercent Moisture

46.2

Client Lot # ... : F9E010259

Date ~1ed••• : 04/30/09 13:05% Moisture.•... : 46

DUPLICATERESULT


J. THE LEADER IN ENVIRONMENTAL TESTING

.TestAmericaDrinking Water? Yes 0 No Qt

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Temperature on Receipt---

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.Project?get'Ch .~s·eJ1 oa~/ / /0'1 Chain oI1C:~7299eCf",

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Sample Temperature (8):**

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Date: 6-/-oj~ Information

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DHLUPSFedEx

THE L.EADER IN ENVtRONMENTAL T£STJNG

CONDmON UhON RECEIPT FORMClient: And!~

Quote No: 11 ~qlJ

COCIRFA No: I g.,3C?() .. J21:;Jq'l

_ _ ~ Jlnitiated By: ~

TestAmerica

Shipper:

Shippipg # (8):*

1. -_-...---------2. -------------3. ------------4. ------------5. ------------

*Numbered shippi.ng lines correspond to Numbered Sample Temp lines ••Sample must be received at40C :I::ZOC"lfn~ note contents below. Temperaturevariance does NOT affect the fol1owing: Metals-Liquid or Rad tests· Uquid or Solids

1~..y

1.

2.

3..

4.

5.

6.

. 7.

Was sample received broken?

Is sample volume sufficient foranal sis?

8.

9.

10.

11.

12."

13. y

Are there custody seals present on bottles?

Do custody seals ort bottles appear to betam red with?Was sample received with proper pH'? (If not,make note below)

Sample received in proper containers?

Headspace in VOA or TOX liquid samples?(If Yes. note sample 10's below)

Was Internal COC/Workshare received?

Was pH taken by original TestAmerica lab?

1 For DOE..AL (pantex, LANL. Sandia) sitcs~ pH of ALL containers received must be verified, EXCEPTVO~ TOX and soils.

Notes:

Informed by: _Corrective Action:D Client Contact Name:o Sample(s) processed ~'as is~

o Sa~l~~onh~duntit ffrcl~~~n6ti~: ~~~~~~~~~~~~~~~~_

Project Management Review: Date: S(!l.l...09~------------THIS FORM MUST BE COMPLETED AT E TIME THE ITEMS ARE BEING CHECKED IN. IF ANY ITEM IS COMPLETED BY SOMEONE OTHER THANTHE lNITIATOR, THEN THAT PERSON IS UtRED TO APPLY THE1R INITIAL AND THE DATE NEXT TO THAi ITEM.

LOT# F 9E 0 1 0 2 5 9 REVI SED ADMIN-0004, REVISED 10121108 \\SlsvrO I\QA\FORMS\ST-LOUlS\ADMJN\AdminOO4 rev1Ldoc36 of 36

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