TestAmerica Laboratories, Inc. ANALYTICAL REPORT ...

TestAmericaTHE LEADER IN ENVIRONMENTAL TESTING

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Savannah5102 LaRoche AvenueSavannah, GA 31404Tel: (912)354-7858

TestAmerica Job ID: 680-70758-1Client Project/Site: Hercules Hattiesburg APIX 7/26/11

For:Ashland Inc.Ashland Hercules Research Center500 Hercules Rd Bldg 8139Wilmington, Delaware 19808

Attn: Timothy Hassett

Authorized for release by:08/09/2011 05.48:12 PM

Lidya GuliziaProject Manager IIlidya .gulizia©testamericainc.com

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Results relate only to the items tested and the sample(s) as received by the laboratory.

The test results in this report meet all 2003 NELAC requirements for accredited parameters,

exceptions are noted in this report. Pursuant to NELAC, this report may not be reproduced

except in full, and with written approval from the laboratory. For questions please contact

the Project Manager at the e-mail address or telephone number listed on this page

This report has been electronically signed and authorized by the signatory. Electronic signature

is intended to be the legally binding equivalent of a traditionally handwritten signature

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LINKS

cc: Craig Derouen Chris Waters Charlie Jordan

Client: Ashland Inc TestAmerica Job ID: 680-70758-1

Project/Site: Hercules Hattiesburg APIX 7/26/11

Table of ContentsCover Page 1

Table of Contents 2

Case NarrativeSample Summary 5

Method Summary 6

Definitions 7

Detection Summary 8

Client Sample Results 11

Surrogate Summary 55

QC Sample Results 57

QC Association 80

Chronicle 85

Chain of Custody 89

Receipt Checklists 90

Certification Summary 91

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Case NarrativeClient: Ashland Inc. TestAmerica Job ID: 680-70758-1

(5roject/Site: Hercules Hattiesburg APIX 7/26/11

Job ID: 680-70758-1

_______ _______ ____________

Laboratory: TestAmerica Savannah

Narrative

Job Narrative

680-70758-1

Receipt

All samples were received in good condition within temperature requirements.

GCIMS VOA

Method(s) 8260B: A full list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability that

one or more analytes will recover outside acceptance limits The laboratory’s SOP allows for four analytes to recover outside criteria for

this method when a full list spike is utilized. The LCS/LCSD associated with batch 210523 had two analytes outside control limits;

therefore, re-extraction/re-analysis was not performed. These results have been reported and qualified.

Method(s) 82608: A fufl list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability that

one or more analytes will recover outside acceptance limits. The laboratory’s SOP allows for 4 analytes to recover outside criteria for this

method when a full list spike is utilized. The LCS associated with batch 210665 had 3 analytes outside control limits; therefore,

re-extraction/re-analysis was not performed. These results have been reported and qualified.

No other analytical or quality issues were noted.

GC/MS Semi VOA

Method(s) 8270C: The following sample(s) was diluted due to abundance of target analytes ASH-DUP-07261 1 (680-70758-2),

ASH-MW1 7-072611 (680-70758-5), ASH-MW23-07261 1 (680-70758-6), ASH-MWO8-07261 1 (680-70758-1), ASH-MW1 9-072611

(680-70758-7). As such, surrogate recoveries are not reported, and elevated reporting limits (RLs) are provided.

ethod(s) 8270C: The laboratory control sample (LCS) for batch 210278 exceeded control limits for the following analyte(s): famphur.

Famphur has been identified as a poor performing analyte when analyzed using this method; therefore, re-extraction/re-analysis was not

performed.

Method(s) 8270C: A full list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability that

one or more analytes will recover outside acceptance limits. The laboratory’s SOP allows for four analytes to recover outside criteria for

this method when a full list spike is utilized. The LCS associated with batch 210278 had two analytes outside control limits; therefore,

re-extraction/re-analysis was not performed These results have been reported and qualified.

Method(s) 8270C: Internal standard (ISTD) response for the following sample(s) was outside control limits: ASH-MWO8-07261 1

(680-70758-1). The sample(s) was re-analyzed with concurring results. The original set of data has been reported.

Method(s) 8270C: The following analyte(s) recovered outside control limits for the LCS associated with batch 210278: dimethoate. This

analyte was outside the Marginal Exceedance Limits The holding time had expired . therefore, re-extraction and/or re-analysis was not

performed.


GC Semi VOA

Method(s) 8081A_8082. Two surrogates are used for this analysis. The laboratory’s SOP allows one of these surrogates to be outside

acceptance criteria without performing re-extraction/re-analysis The following sample(s) contained an allowable number of surrogate

compounds outside limits: ASH-DUP-07261 1 (680-70758-2), ASH-MWO8-07261 1 (680-70758-1), ASH-MW1 3-072611 (680-70758-4),

ASI-l-MWi 9-072611(680-70758-7), ASH-MW23-07261 1(680-70758-6), GWC-SC-M2-7-1 1 (680-70747-8), GWC-SC-M2.7-I 1

(680-70747-8 MS), GWC-SC-M2-7-1 1(680-70747-8 MSD), ([CS 680-210285/19-A). These results have been reported and qualified.

Method(s) 8081A_8082: Internal standard (ISTD) response for the following sample(s) exceeded the control limit on Column two

ASH-DUP-07261 1(680-70758-2), ASH-MWO8-07261 1(680-70758-1), ASH-MW13-07261 1(680-70758-4). ASH-MW23-07261 1

(680-70758-6). As such, the sample results associated with this ISTD were reported from the other column, which met ISTD acceptance

—-Ncriteria. Sample matrix co-eluted with the ISTD on column two resulting in the high biased recovery.

Method(s) 8081A_8082: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 210285 were outside control limits. The

TestAmerica Savannah

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Job ID: 680-70758-1 (Continued)

______________ _____

Laboratory: TestAmerica Savannah (Continued)

associated laboratory control sample (LCS) recovery met acceptance criteria.

Method(s) 8081A_8082: A full list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability

that one or more analytes will recover outside acceptance limits. The laboratory’s SOP allows for one analytes to recover outside criteria

for this method when a full list spike is utilized. The LCS associated with batch 210285 had one analyte outside control limits; therefore,

re-extraction/re-analysis was not performed. These results have been reported and qualified.

Method(s) 8081A_8082: The pesticide LCS exceeded control limits for the surrogate DCB. The remaining batch QC met acceptance

criteria for DCB. The pesticide LCS met acceptance criteria established within the SOP for all spiked target analytes; therefor the data have

been flagged and reported. Re-extraction of the samples would have been outside of holding times.

Method(s) 8081A_8082: The following sample(s) was diluted due to the nature of the sample matrix: ASH-MW17-07261 1 (680-70758-5).

Elevated reporting limits (RLs) are provided. Due to the level of dilution required for the following sample(s), surrogate recoveries are not

reported.

Method(s) 81 51A: Surrogate recovery for the following sample(s) was outside control limits: ASH-MW17-07261 1 (680-70758-5),

ASH-MtN23-07261 1 (680-70758-6). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not

performed.

Method(s) 81 51A: This method incorporates the use of second column confirmation. Corrective action for unacceptable percent recovery

is not taken for surrogate compounds unless the results from both columns are outside criteria. Any results which fall outside criteria are

qualified and reported.


MetalsNo analytical or quality issues were noted.

General Chemistry

Method(s) 335.4, 9012A: The matrix spike/ matrix spike duplicate (MS/MSD) recoveries for batch 210679 were outside control limits. The

associated laboratory control sample (LCS) recovery met acceptance criteria.


Comments

No additional comments.

0TestAmerica Savannah

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Sample SummaryClient: Ashland Inc. TestAmerica Job ID: 680-70758-15roJect/Site. Hercules Hattiesburg APIX 7/26/11

Lab Sample ID Client Sample ID Matrix Collected Received660-70758-1 — ASH-MWOS-072611 Water 07(26111 09:25 07127/1109:20

680-70758-2 ASH-DUP-072611 Water 07/26/11 00:00 07(27/11 09:20

680-70758-3 ASH-RSI-07261 1 Water 07/26/11 08:57 07127111 09:20

680-70758-4 ASH-MW1 3-072611 Water 07/26/11 09:20 07/27/11 09:20

680-70758-5 ASH-MW1 7-072611 Water 07/26/11 11:45 07/27/11 09:20

680-70758-6 ASH-MW23-07261 1 Water 07/26/1112:51 07/27/11 09:20

680-70758-7 ASH-MW1 9-072611 Water 07/26/11 14:20 07/27/11 09:20

680-70758-9 Trip Blank Water 07/26/11 00:00 07/27/11 09:20


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Method SummaryClient: Ashland Inc. TestAmerica Job ID: 680-70758-1


____-_

__

______

Method Method Description Protocol Laboratory

8260B Volatile Organic Compounds (GC/MS) SW846 TAL SAV

8270C Semivolatile Organic Compounds (GCIMS) SW846 TAL SAV

8081A_8082 Organochiorine Pesticides & PCBs (GC) SW846 TAL SAV

8151A Herbicides (GC) SW846 TAL SAV

8290 Dioxins/Furans, HRGC/HRMS (8290) SW846 TAL WSC

6020 Metals (ICPIMS) SW846 TAL SAV

7470A Mercury (CVAA) SW846 TAL SAV

9012A Cyanide, Total and/or Amenable SW846 TAL SAV

9034 Sulfide, Acid Soluble and Insoluble (Titrimetric) SW846 TAL SAV

Protocol References:

SW846 = “Test Methods For Evaluating Solid Waste, Physical/Chemical Methods”, Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7868

TAL WSC = TestAmeiica West Sacramento, 880 Riverside Parkway, West Sacramento, CA 95605, TEL (916)373-5600

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DefinitionslGlossaryClient Ashland Inc. TestAmerica Job ID: 680-70758.1

3roectISite: Hercules Hattiesburg APIX 7/26/11

Qualifiers

GC1MS VOA

Qualifier Qualifier Description

* LCS or LCSD exceeds the control limits

GC/MS Semi VOA

Qualifier Qualifier Description* LCS or LCSD exceeds the control limits

D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a

dilution may be flagged with a D.E Result exceeded calibration range.

GC Semi VOA

Qualifier Qualifier Description* LCS or LCSD exceeds the control limits

o Surrogate or matrix spike recovenes were not obtained because the extract was diluted for analysis; also compounds analyzed at a

dilution may be flagged with a D.E Result exceeded calibration range.

p The %RPD between the primary arid confirmation columnldetector is >40%. The lower value has been reported.

X Surrogate is outside control limits

Metals

Qualifier Qualifier Description

F MS or MSD exceeds the control limits

Glossary

,7bbviation These commonly used abbreviations may or may not be present in this report.

________—

Listed under the “D” column to designate that the result is reported on a dry weight basis.

EPA United States Environmental Protection Agency

ND Not Detected above the reporting level.

MDL Method Detection Limit

RL Reporting Limit

RE, RE1 (etc.) Indicates a Re-extraction or Reanalysis of the sample.

%R Percent Recovery

RPD Relative Percent Difference, a measure of the relative difference between two points.


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Detection SummaryClient: Ashland Inc. TestAmerica Job ID: 680-70758-1


Client Sample ID: ASH-MW08-072611 Lab Sample ID: 680-70758-1

Analyte Result Qualifier ML EDL TEF TEQ tinlt Oil Fac D Method Prep Type

Total TCDF 60 14 14 pg/L 1.05 8290 Total

Analyte -

________

Result Qualifier RL MDL UnIt Oil Fac D Method — Prep Type

Benzene 4600 50 ug/L 50 82600 Total/NA

Carbon tetrachlonde 2600 50 ug/L 50 826DB Total/NA

Chlorobenzerte 220 50 ug/L 50 8260B Total/NA

Chloroform 640 50 ug/L 50 8260B Total/NA

Ethylberizene 55 50 ug/L 50 82600 Total/NA

Methylene Chloride 340 250 ug/L 50 826DB Total/NA

1,4-Dioxane 13000 1000 ug/L 100 8270C Total/NA

o,o,o”-Triethylphosphorothioale 3400 1000 ug/L 100 8270C Total/NA

alpha-BHC 0,61 0.051 ug/L 1 8081A_6082 Total/NA

gamma-BHC (Lindane) 0.30 0051 ug/L 1 8081A_8082 Total/NA

Arsenic 42 2.5 ug/L 1 6020 Total/NA

Barium 260 5.0 ugiL 1 6020 Total/NA

Analyte Result Qualifier RL RL Unit Dil Fac D Method Prep Type

Sulfide 5.0 1.0 mgIL 1 9034 Total/NA

Client Sample ID: ASH-DUP-07261 I Lab Sample ID: 680-70758-2

Analyte Result Qualifier ML EDL TEF TEQ Unit DII Fac D Method Prep Type

Total TCDF 66 10 6,0 pg/L 1.01 8290 Total

Analyte Result Qualifier RL MDL Unit Dil Fac 0 Method Prep Type

Benzene 5100 50 ugIL 50 826DB Total/NA

Carbon tetrachloride 2700 * 50 ugIL 50 826DB Total/NA

Chlorobenzene 240 50 ug/L 50 826DB Total/NA

Chloroform 640 50 ugiL 50 826DB Total/NA

Ethylbenzene 61 50 ug/L 50 826DB Total/NA

Methylene Chloride 350 250 ug)L 50 826DB Total/NA


o,o,o”-Triethylphosphorothioate 3300 510 ug/L 50 8270C Total/NA

alpha-BHC 0.75 0049 ug/L 1 8081A_8D82 Total/NA

gamma-BHC (Lindane) 0.45 0 049 ug/L 1 8D81A_8D82 Total/NA

Arsenic 44 2 5 ugIL 1 6020 Total/NA

Barium 260 5 0 ug/L 1 6020 Total/NA

Analyte Result Qualifier RL RL Unit Dii Fac D Method Prep Type

Sulfide 17 1 0 mg/L 1 9D34 Total/NA

Client Sample ID: ASH-RSI-072611 Lab Sample ID: 680-70758-3

Analyte Result Qualifier RL MDL Unit Oil Fac 0 Method Prep Type

Barium 12 5 0 ugiL 1 602D Total/NA

Analyte Result Qualifier RL RL Unit Dii Fac D Method Prep Type

Sulfide 2 3 1 0 mg/L 1 9034 Total/NA

Client Sample ID: ASH-MWI3-07261 I Lab Sample ID: 680-70758-4

Analyte Result Qualifier ML EDL TEF TEQ Unit Dil Fac D Method Prep Type

Total TCDF 17 10 3.3 pg/L 1 8290 Total

Analyte — Result Qualifier RL MDL Unit Oil Fac D Method Prep Type

Benzene 390 10 U9IL 10 826DB Total/NA

Carbon tetrachloride 620 10 ug/L 10 82600 Total/NA

Chlorobenzene 24 10 ug/L 10 826DB Total/NA


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Detection SummaryClient: Ashland Inc TestAmerica Job ID: 680-70758-1

roject/Site: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-MW13-072611 (Continued) Lab Sample ID: 680-70758-4

Analyte Result Qualifier RL MDL Unit DII Fac D Method Prep Type

Chloroform 210 10 ug/L 10 826DB Total/NA

14-Dioxane 470 49 ugIL 5 8270C Total/NA

ooo-Triethylphosphorolhioate 190 49 ug/L 5 8270C Total/NA

alpha-BHC 025 0051 ug/L 1 8081A 8082 Total/NA

Arsenic 5 7 25 ugiL 1 6020 Total/NA

Banum 49 50 ug/L 1 6020 Total/NA

Cobalt 1 5 0 50 ug/L 1 6020 Total/NA

Zinc 41 20 ug/L 1 6020 Total/NA

Client Sample ID: ASH-MWI7-072611 Lab Sample ID: 680-70758-5

Analyte Result Qualifier ML EDL TEF TEQ unit Dii Fac D Method Prep Type

Total TCDF 100 10 80 pg/L 1 8290 Total

Analyte Result Qualifier RL MDL unit Oil Fac 0 Method Prep Type

Benzene 3600 200 ug/L 200 8260B Total/NA

Carbon tetrachloride 25000 * 200 ug/L 200 82608 Total/NA

Chlorobenzene 770 200 ug)L 200 826DB Total/NA

Chloroform 3000 200 ug/L 200 826DB Total/NA

o,o’,o”-Triethylphosphorothioale 12000 1000 ug/L 100 8270C Total/NA

alpha-BHC 1 5 p 049 ug/L 10 8081A_8082 Total/NA

Arsenic 28 2 5 ug/L 1 6020 Total/NA


Cobalt 0 69 0 50 ug/L 1 6020 Total/NA

Anatyte -

_____________

Result Qualifier RL RL unit oi Fac D Method Prep Type



Analyte Result Qualifier RL MDL Unit Oil Fac D Method Prep Type

Benzene 8800 100 ug/L 100 82600 Total/NA

Carbon disulfide 390 200 ug/L 100 826DB Total/NA

Chlorobenzene 140 100 ug/L 100 82606 Total/NA

Chloroform 3200 100 ug/L 100 82609 Total/NA

4-Methyl-2-pentanone (MIBK) 1100 1000 ug/L 100 82608 Total/NA

Toluene 1300 100 ug/L 100 826DB Total/NA


3 & 4 Meihylphenol 660 97 ug/L 10 8270C Total/NA

Phenol 140 97 uq/L 10 82/DC Total/NA

2,4-0 60 E p 0 50 ug/L I 8l51A Total/NA

2,4-0 - DL 10 0 20 ug/L 4 8151A Total/NA

Arsenic 19 25 uq/L 1 6020 Total/NA


Beryllium 3 3 0 50 ug/L 1 6020 Total/NA

Chromium 50 5 0 ug)L 1 6020 Total/NA

Cobalt 071 050 ug/L 1 6020 Total/NA

Vanadium 16 10 ug/L 1 6020 Total/NA

Analyte Result Qualifier RL RL Unit Oil Fac 0 Method Prep Type


Client Sample ID: ASH-MWI 9-072611

_____

Lab Sample ID: 680-70758-7

Qe -- R 0; - it - - - Ott c DM PTy

Benzene 54 1 0 ug/L 1 826GB Total/NA

TestAmertca Savannah

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Detection SummaryClient: Ashland Inc.Project/Site: Hercules Hattiesburg APIX 7/26/11

TestAmerica Job ID 680-70758-1

Client Sample ID: ASH-MWI9-072611 (Continued) Lab Sample ID: 680-70758-7

Analyte

Carbon tetrachloride

Chlorobenzerte

Chloroform

Ethylbenzene

Toluene

11-Biphenyl

Arsenic

Barium

Zinc

Prep Type

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Client Sample ID: Trip Blank Lab Sample ID: 680-70758-9

No Detections.


C

0

Result Qualifier RL MDL Unit Dii Fac D Method

3.5 1.0 ug)L 1 8260B

9.9 1.0 ugiL 1 8260B

3.3 1.0 ug!L 1 82608

1.3 1.0 ug/L 1 8260B

2.4 1.0 ug/L 1 826DB

770 99 ug/L 10 8270C

14 2.5 ugIL 1 6020

51 5.0 ug/L 1 6020

57 20 ug/L 1 6020

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Client Sample ResultsClient: Ashland Inc. TestAmerica Job ID: 680-70758-1

(‘yroiectlSite: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-MWO8-072611 Lab Sample ID: 680-70758-1

Date Collected: 07126111 09:25 Matrix: Water

Date Received: 07127111 09:20

Method: 826DB - Volatile Organic Compounds (GCIMS)Analyte

_____________—

Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

Acetone <1300 1300 ug/L 07/30)11 06:36 50

Acetonitnle <2000 2000 ug/L 07/30/11 06:36 50

Acrolein <1000 1000 ugIL 07/30/11 06:36 50

Acrylonitrile <1000 1000 ugIL 07/30/11 06:36 50

Benzene 4600 50 ug/L 07/30/11 06:36 50

Dichlorobromomethane <50 50 ug/L 07/30/11 06:36 50

Bromoform <50 50 ugIL 07/30/11 06:36 50

Bromomethane <50 50 ug/L 07)30/11 06:36 50

2-Butanone(MEK) <500 500 ug)L 07/30)11 06:36 50

Carbon disulfide <100 100 ug/L 07/30/11 06:36 50

Carbon tetrachloride 2600 50 ug)L 07/30/11 06:36 50

Chlorobenzene 220 50 ug)L 07/30/11 0636 50

2-Chloro-1,3-butadiene <50 50 ug/L 07/30/11 06:36 50

Chloroethane <50 50 ug/L 07/30/11 06:36 50

Chloroform 640 50 ugIL 07/30/11 06:36 50

Chloromethane <50 50 ug/L 07/30/11 06:36 50

3-Chloro-i-propene <50 50 uglL 07/30/11 06:36 50

Chlorodibromomethane <50 50 ug/L 07/30/11 06:36 50

i,2-Dibromo-3-Chloropropane <50 50 ug/L 07)30/11 06.36 50

Ethylene Dibromide <50 50 ug/L 07/30/11 06:36 50

Dibromomethane <50 50 ug’L 07/30/11 06:36 50

trans-1,4-Dichloro-2-butene <100 100 ug)L 07/30/11 06:36 50

Dichlorodifluoromethane <50 50 ug/L 07/30/11 06:36 50

1,1-Dichloroethane <50 50 ug/L 07/30/11 06:36 50

1,2-Dichloroethane <50 50 ug/L 07/30/11 06:36 50

cis-1,2-Dichloroethene <50 50 ug/L 07/30/11 06:36 50

trans-1,2-Dichloroethene <50 50 ug/L 07)30/11 06:36 50

1,1-Dichloroethene <50 50 ug/L 07/30/11 06:36 50

1,2-Dichloropropane <50 50 ug/L 07/30/11 06:36 50

cis-1,3-Dichloropropene <50 50 ug/L 07/30/11 06:36 50

trans-i ,3-Dichloropropene <50 50 ug/L 07)30/11 06:36 50

Ethylbenzene 55 50 ug/L 07/30/11 0636 50

Ethyl methacrylate <50 50 uglL 07/30/11 06:36 50

2-Hexanone <500 500 ug/L 07/30/11 0636 50

lodomethane <250 250 ug/L 07/30/11 06.36 50

Isobutyl alcohol <2000 2000 ug/L 07/30/11 06 36 50

Methacryloniihle <1000 1000 ugIL 07/30/11 0636 50

Methylene Chloride 340 250 ugIL 07)30/11 06.36 50

Methyl methacrylate <50 50 ug/L 07/30/11 06:36 50

4-Methyl-2-pentanone (MIBK) <500 500 ug/L 07/30/11 06.36 50

Pentachloroethane <250 250 ug/L 07/30/il 06:36 50

Propionitnle <1000 1000 ugiL 07/30/il 0636 50

Styrene <50 50 ug/L 07130/il 06:36 50

1,11,2-Tetrachloroethane <50 50 ug/L 07/30)11 0636 50

1,1,2,2-Teirachloroethane <50 50 ug/L 07/30/li 0636 50

Tetrachloroethene <50 50 ug/L 07/30/11 0636 50

Toluene <50 50 ugIL 07/30/11 0636 50

1,1 ,1-Tnchloroethane <50 50 ugIL 07/30/11 0636 50

1,1,2-Trichloroethane <50 50 ug/L 07)30/11 0636 50

Trichloroethene <50 50 ug/L 07/30/11 06:36 50


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CHent Sample ResultsClient: Ashland Inc. TestAmerica Job ID: 680-70758-1


CiientSampleiD:ASH-MWO8-072611 Lab Sample ID:68Ô-70758-1 0Date Collected: 07126/11 09:25 Matrix: Water

Date Received: 07/27/11 09:20

Method: 8260B - Volatile Organic Compounds (GCIMS) (Continued)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Far

Trichlorofluoromethane <50 50 ug!L 07/30/11 06.36 50

1 23-Thchloropropane <50 50 ugiL 07/30/11 06:36 50

Vinyl acetate <100 100 ug/L 07/30/11 06:36 50

Vinyl chloride <50 50 uglL 07/30/11 06:36 50

Xylenes, Total <100 100 ugiL 07130/11 06:36 50

Surrogate % Recovery Qualifier Limits Prepared Analyzed DII Fac

4-Bromofluorobenzene - 94 - 70 130 07/30/11 06:36 50

Dibromofluoromethane 108 70- 130 07/30/11 06:36 50

Toluene-d8 (Surr) 97 70- 130 07/30/11 06:36 50

Method: 8270C - Semivolatile Organic Compounds (GCIMS)Anatyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Far

Acenaphthene <1000 1000 — ug/L 07/28/11 14:42 08/04/11 13:18 100 /--

Acenaphthylene <1000 1000 ugIL 07128/11 14:42 08/04/11 13:18 100

Acetophenone <1000 1000 uglL 07/28/11 14:42 08/04/11 13:18 100

2-Acetylaminotluorene <1000 1000 ug/L 07/28/11 14:42 08/04/11 13:18 100

alpha,alpha-Dimethyt phenethylamine <210000 210000 ug/L 07/28/11 14:42 08/04/11 13:18 100

4-Aminobiphenyl <1000 1000 ugIL 07/28/11 14:42 08/04/11 13:18 100

Aniline <2100 2100 ugfL 07/28/11 14.42 08/04/11 13:18 100

Anthracene <1000 1000 ug/L 07/28/11 14:42 08/04/11 13:18 100

Aramite, Total <1000 1000 ug/L 07/28/11 14:42 08/04/11 13:18 100

Benzo[a]anthracene <1000 1000 ug)L 07/28/11 14:42 08/04/11 13:18 100

Benzo[a]pyrene <1000 1000 ug/L 07/28/11 14:42 08/04/11 13:18 100

Benzo[blfluoranthene <1000 1000 ug/L 07/28/11 14:42 08/04/11 13:18 100

Benzo[gh,i]perylene <1000 1000 ug/L 07)28/11 14.42 08/04/11 13:18 100

Benzo[k]tluoranthene <1000 1000 ug)L 07/28/11 14:42 08/04/11 13:18 100

Benzyl alcohol <1000 1000 uglL 07/28/11 14:42 08/04/11 13:18 100

1,1-Biphenyl <1000 1000 ug/L 07/28/11 14.42 08/04/11 13:18 100

Bis(2-chloroethoxy)methane <1000 1000 uglL 07/28/11 1442 08/04/11 13.18 100

$is(2-chloroelhyl)ether <1000 1000 ug/L 07/28/11 14.42 08/04/11 13:18 100

bis(chloroisopropyl) ether <1000 1000 ug/L 07/28/11 14:42 08/04/11 13:18 100

Bis(2-ethylhexyl) phthalale <1000 1000 ugIL 07/28/11 1442 08/04/11 13.18 100

4-Bromophenyl phenyl ether <1000 1000 ug/L 07/28/11 14.42 08/04/11 13:18 100

Butyl benzyl phlhalate <1000 1000 ug/L 07/28/11 1442 08/04/11 1318 100

4-Chloroaniline <2100 2100 ug/L 07/28/11 1442 08/04/11 1318 100

4-Chloro-3-melhylphenol <1000 1000 ug/L 07/28/11 1442 08/04/11 1318 100

2-Chloronaphthaene <1000 1000 ugIL 07/28/11 1442 08/04/11 13 18 100

2-Chlorophenol <1000 1000 ug/L 07)28/11 1442 08/04/11 1318 100

4-Chiorophenyl phenyl ether <1000 1000 ug/L 07/28/11 1442 08/04/11 1318 100

Chrysene <1000 1000 ug/L 07/28/111442 08/04/11 1318 100

Diallate <1000 1000 ug/L 07/28/111442 08/04/1113:18 100

Dibenz(a,h)anlhracene <1000 1000 ug/L 07/28/11 14:42 08/04/11 13:18 100

Dibenzofuran <1000 1000 ug/L 07/28/11 14:42 08/04/11 13:18 100

1,2-Dichlorobenzene <1000 1000 ug/L 07/28/11 1442 08/04/11 13 18 100

13-Dichlorobenzene <1000 1000 ug/L 07/28/11 14:42 08/04/11 1318 100

14-Dichlorobenzene <1000 1000 ug/L 07/28/11 14.42 08/04/11 1318 100

3,3’-Dichlorobenzidine <6200 6200 ug/L 07/28/111442 08/04/11 1318 100

2,4-Dichlorophenol <1000 1000 ugIL 07)28/11 14:42 08)04)11 1318 100 7’

2,6-Dichlorophenol <1000 1000 ug/L 07/28/11 1442 08/04/1113:18 100


of 92

Client Sample Results

0 Prepared

07/28/11 14:42

07/28/11 1442

07/28/11 1442

07/28/11 14:42

07/28/11 14:42

07/28/11 14.42

07/28/11 14:42

07/28/11 14.42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07)28)11 14:42

07)28/11 14:42

07/28/11 14.42

07/28/11 1442

07/28/11 1442

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 1442

07/28)11 1442

07)28/11 14:42

07/28/11 14:42

07/28/1114.42

07/28/11 14:42

07/28/11 14:42

07/28/11 1442

07/28/111442

07/28/11 1442

07/28/111442

07/28)111442

07/28/11 1442

07/28/il 1442

07)28/111442

07/28/11 1442

07/28/11 14:42

07/28/11 1442

07/28/11 1442

07/28/11 14:42

07)28/111442

07/28/11 1442

07/28/111442

07/28/111442

07/28/11 1442

07/28/111442

07/28/11 1442

07/28/111442

Analyzed

08/04/11 13.18

08/04/11 13:18

08/04/11 13:18

08/04/11 1318

08/04/11 13:18

08/04/11 1318

08/04/11 13:18

08/04/11 13,18

08/04/11 13:18

08/04/11 13:18

08)04/11 13:18

08/04/11 13:18

08/04)11 1318

08/04/11 13:18

08/04)11 13:18

08/04/11 13:18

08/04/11 13:18

08/04/11 13.18

08)04/11 13 18

08)04/11 1318

08/04)11 13.18

08/04/11 13:18

08/04/11 1318

08/04/11 13:18

08/04/11 13:18

08/04/11 13:18

08/04/11 1318

08/04/11 13:18

08/04/11 13.18

08/04/11 1318

08/04/11 1318

08/04/11 1318

08/04/11 13 18

08/04/11 1318

08/04/11 13.18

08/04/11 13 18

08/04/11 13:18

08/04/11 13 18

08/04/11 13 18

08/04/11 13.18

08/04/11 1318

08/04/11 1318

08/04/11 1318

08/04/11 1318

08/04/11 1318

08/04/11 13 18

08/04/11 1318

08/04/11 13.18

08/04/11 13.18

08/04/11 1318

0/I Fac

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100


TestAmeñca Job ID: 680-70758-1

‘ILab Sample ID: 680-70758-1

Matrix: Water

Client: Ashland Inc.roject/Site: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-MWO8-072611Date Collected: 07/26)11 09:25Date Received: 07/27)11 09:20

Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)Analyte Result Qualifier RL MDL Unit

Diethyl phthalate <1000 1000 ug)L

Dimethoate <1000 * 1000 ug/L

7,1 2-Dimethylbenz(a)anthracene <1000 1000 ug/L

3,3’-Dimethylbenzidine <2100 2100 ug/L

2,4-Dimethylphenol <1000 1000 ug/L

Dimethyl phlhalate <1000 1000 ug)L

Di-n-butyl phthalate <1000 1000 ug/L

1,3-Dinitrobenzene <1000 1000 ug/L

4,6-Dinitro-2-methy/phenol <5200 5200 ug/L

2,4-Dinitrophenol <5200 5200 ug/L

2,4-Dinitrotoluene <1000 1000 ug/L


Di-rt-octyl phthalate <1000 1000 ug!L

Dinoseb <1000 1000 ug/L

1,4-Dioxane 13000 1000 ug/L

Disulfoton <1000 * 1000 ug/L

Ethyl methanesulfonate <1000 1000 ug/L

Ethyl Parathion <1000 1000 ug/L

Famphur <1000 * 1000 ug/L

QFluoranthene

<1000 1000 ug)L

Fluorene <1000 1000 ug/L

Hexachlorobenzene <1000 1000 ug/L

Hexachlorobutadiene <1000 1000 ug/L

Hexachlorocyc/opentadiene <1000 1000 ug/L

Hexachloroethane <1000 1000 ug/L

Hexachlorophene <520000 520000 ug/L

Hexachloropropene <1000 1000 uq/L

lndeno12,3-cdjpyrene <1000 1000 ug/L

lsophorone <1000 1000 ug/L

sosafrole <1000 1000 ug/L

Methapyrilene <210000 210000 ug/L

3-Methylcholanthrene <1000 1000 ug/L

Methyl methanesulfonate <1000 1000 ug/L

2-Methylnaphthalene <1000 1000 ug/L

Methyl parathion <1000 • 1000 ug/L

2-Methylphenol <1000 1000 ug/L

3 & 4 Methylphenol <1000 1000 ug/L

Naphthalene <1000 1000 ug/L

1,4-Naphthoquinone <1000 1000 ug/L

1-Naphthylamine <1000 1000 ug/L

2-Naphthylamine <1000 1000 ug/L

2-Nitroaniline <5200 5200 ug/L



Nitrobenzene <1000 1000 ug/L

2-Nitrophenol <1000 1000 ug/L

4-Nitrophenol <5200 5200 ug/L

O4-Nitroquinohne-1-oxide <2100 2100 ug/L

N-Nitro-o-toluidne <1000 1000 ug/L

N-Nitrosodiethylamine <1000 1000 ug/L

of92

Client: Ashland Inc.Project/Site: Hercules Hattiesburg APIX 7/26/11

Phorate

2-Picoline

p-Phenylene diamine

Pronarnide

Pyrene

Pyridine

Safrole, Total

Sulfotepp

1 ,2,4,5-Tetrachlorobenzene

2,3,4,6-Tetrachlorophenol

Thionazin

2-Toluidine

1 ,2,4-Trichlorobenzene

2,4, 5-Trichlorophenol

2,4,6-Trichlorophenol

1 3,5-Trinitrobenzene

alpha-BHC

beta-BHC

Chiordane (technical)

Chlorobenzilate

44-ODD

4,4-DOE

TestAmerica Job ID: 680-70758-1 IALab Sample ID: 680-70758-1 6)

Matrix: Water

Prepared Analyzed Dii Fac

07/28111 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07(28/11 1442 08/04/11 1318 100

07/28111 1442 08/04/11 1318 100

07/28/11 1442 08)04/11 1318 100

07/28111 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07/28111 1442 08/04/11 13 18 100

07/28/11 1442 08/04/11 1318 100

07/28/111442 08/04/11 1318 100

07/28/11 14.42 08/04/11 1318 100

07/28/11 14.42 08/04/11 1318 100 ,

07/28/11 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100 “‘

07/28/11 1442 08/04/11 1318 100

07/28/111442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07/28(11 1442 08/04/11 1318 100

07/28/111442 08/04/11 1318 100

07)28/11 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07/28/111442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100

07/28/111442 08/04/11 1318 100

07)28/11 1442 08/04/11 1318 100

07/28/11 1442 08/04/11 1318 100



Client Sample ID: ASH-MWO8-072611Date Collected: 07/26111 09:25


Method: 8270C - Semivolatile Organic Compounds (GCIMS) (Continued)

Analyte Result Qualifier RL MDL Unit 0

N-Nitrosodimethylamine <1000 1000 ug/L

N-Nitrosodi-n-butylamine <1000 1000 ug/L

N-Nitrosodi-n-propylamine <1000 1000 ug/L

N-Nitrosodiphenylamine <1000 1000 ugIL

N-Nitrosomethylethylamine <1000 1000 ugIL

N-Nitrosomorpholine <1000 1000 ugIL

N-Nitrosopiperidine <1000 1000 ug/L

N-Nitrosopyrrolidine <1000 1000 ug/L

o,o’,o’-Triethylphosphorothioate 3400 1000 ug/L

p-Dimelhylamino azobenzene <1000 1000 ug/L

Pentachlorobenzene <1000 1000 ug/L

Perttachlororiitrobenzene <1000 1000 ug/L

Pentachlorophenol <5200 5200 ug/L

Phenacetin <1000 1000 ug/L

Phenanthrene <1000 1000 ug/L

Phenol <1000 1000 ug/L

<1000 1000 ug/L

<1000 1000 ug/L

<210000 210000 ug/L

<1000 1000 ug/L

<1000 1000 ugIL

<5200 5200 ugfL

<1000 1000 ug/L

<1000 1000 ug/L

<1000 1000 ug/L

<1000 1000 ug/L

<1000 1000 ug)L

<1000 1000 ug)L

<1000 1000 ug/L

<1000 1000 ug/L

<1000 1000 uglL

<1000 1000 ug/L

Surrogate % Recovery Qualifier Limits

2-Fluorobiphenyl 0 D 38 - 130

2-Fluorophenol 0 D 25 130

N,trobenzene-d5 0 0 39 130

Phenol-d5 0 0 25 130

Terphenyl-d14 0 0 10- 143

2,4,6-Thbromophenol 0 D 31 - 141

Method: 8081A_8082 - Organochiorine Pesticides & PCBs (GC)Analyte Result Qualifier RL

Aldrin <0 051 0 051

Analyzed

08/04/11 13.18

08/04111 13.18

08/04/11 13/8

08/04/11 1318

08/04/11 13.18

08/04/11 13.18

Dii Fec

100

100

100

100

100

100

Prepared

07/28111 14:42

07/28/1114:42

07/28/111442

07/28/1114.42

07/28/1114:42

07/28/Il 1442

Prepared

07/28/11 1442

07)28/11 1442

07/28/11 14:42

07/28)11 14:42

07/28/111442

07/28/11 1442

07/28/111442

0.61

<0.05 1

<0 51

<0 51

<0 10

<0 10

0051

0051

0 51

051

0.10

010

MDL Unit D

ug/L

ug/L

Ug/L

ug/L

ug/L

ugiL

ug/L

Analyzed Dii Fac

08/01/11 2020 1

08/01/11 20.20 1

08/01/11 2020 1

08/01/11 20:20 1

08/01/11 20:20 1

08/01/11 2020

08/01/11 2020

of 92

106 p

Method: 8290 - Dioxins/Furans, HRGCII-IRMS (8290)

0 37

0 28

1.0

6.0

031

14



rojectlSite: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-MWO8-07261 I Lab Sample ID: 680-70758-I

Date Collected: 07I26I11 09:25 Matrix: Water


Method: 8081A_8082 - Organochiorine Pesticides & PCBs (GC) (Continued)Analyte Result Qualifier RL MDL

4,4-DDT <0.10 0.10

delta-BHC <0.051 0.051

Dieldrin <0.10 0.10

Endosulfan I <0.051 0.051

Endosulfan II <0.10 0,10

Endosulfan sulfate <0.10 0.10

Endrin <0.10 0.10

Enddn aldehyde <0.10 0.10

Endrin ketone <0.10 0.10

gamma-BHC (Lindane) 0.30 0.051

Heptachlor <0.051 0.051

I Heptachior epoxide <0.051 0.051

Isodrin <0.051 0.051

Kepone <1 0 1.0

Methoxychlor <0.10 0.10

Toxaphene <5 1 5.1

PCB-1016 <1 0 1.0

PCB-1221 <2.0 2.0

PCB-1232 <1.0 1.0

c: PCB-1242 <1 0 1.0

PCB-1248 <1.0 1.0

PCB-1254 <1.0 1.0

PCB-1260 <1.0 1.0

El

Unit

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ugh

ugIL

ugIL

ug)L

ug/L

ug/L

ugIL

ug/L

ug/L

ugiL

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Surrogate % Recovery

Tefrachloro-m-xyiene 41

Tefrachloro-m-xylene 55

DCB Decachlorobiphenyl 11

DCB Decachlorobiphenyl 5

Qualifier Limits

36. 130

36- 130

X 40.130

pX 40.130

Method: B15IA - Herbicides (GC)Analyte

0 Prepared Analyzed Oil Fac

07128/11 14:42 08/01/11 20:20 1

07/28/11 14:42 08/01/11 20:20 1

07)28/11 14:42 08/01/11 20:20 1

07/28/11 14:42 08/01/11 20:20 1

07/28/11 14:42 08/01/11 20.20 1

07/28/11 14.42 08/01/11 20:20 1

07/28/11 14:42 08)01/11 20:20 1

07/28)11 1442 08)01/11 2020 1

07/28/11 14:42 08/01/11 20:20 1

07/28/11 14:42 08)01)11 20:20 1

07)28)11 14:42 08/01/11 20:20 1

07/28/11 14:42 08/01/11 2020 1

07/28)11 14.42 08/01)11 20:20 1

07/28/11 14:42 08/01)11 20:20 1

07/28/11 14:42 08)01/11 20:20 1

07/28/11 14:42 08/01/11 20.20 1

07/28/11 14:42 08)01/11 20.20 1

07/28/11 14:42 08/01/11 20:20 1

07/28/11 14:42 08/01/11 2020 1

07/28/11 14:42 08/01/11 20:20 1

07/28/11 14:42 08/01/11 20:20 1

07/28/11 1442 08/01/11 20.20 1

07/28/11 1442 08/01/11 2020 1


07/28111 14:42 08/01/11 2020

07/28/11 1442 08/0I/1I20:20

07/28/11 14:42 08/01/11 20:20 1

07/28/11 14:42 08/01/112020 1

Prepared Analyzed Oil Fac

07128/11 0804 07/29/11 1837 1

07/28/11 0804 07/29/11 18 37 1

07/28/11 0804 07/29/11 1837 1

Prepared Analyzed Dii Fec

07/28/110804 07/29/11 1837 1

07/28/11 08:04 07/29/11 1817

D Prepared Analyzed Oil Fac

07)28/11 0900 07/30/11 1039 1.05

pg/L 07/28/11 09.00 07)30/11 1039 1 05

pg/L 07/28/11 0900 07/30/11 1039 105

pg/L 07/28/11 0900 07/30/11 1039 1.05

pg/L 07/28/11 0900 07/30)11 1039 1 05

pg/L 07/28/11 0900 07/30/11 1039 1 05

pg/L 07/28/11 0900 07/30/11 1039 1 05

2,4-D

Silvex (2 4,5-TP)

2,4 5-T

Surrogate

DCAA

DCAA

Result Qualifier RL

<051 — 0.51

<0 51 0.51

<0 51 0.51

% Recovery Qualifier Limits

395 X 52.151

MDL Unit 0

ugIL

ugfL

ug/L

52. 151

EDL TEF TEQ Unit

030 1 pgiLAnalyte Result Qualifier ML

2,3,7,8-TCDD ND 11

Total HxCDD ND 53

Total HxCDF ND 53

Total PeCDD ND 53

Total PeCDF ND 53

Total TCDD ND 11

Total TCDF 60 14

Total TEQ (EPA 1989) 0.00

of92

Client Sample ResultsClient: Ashland Inc. TestAmerica Job ID: 680-70758-1Project/Site: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-MWO8-072611 Lab Sample ID: 680-70758-1Date Collected: 07/26/11 09:25 Matrix: WaterDate Received: 07/27/11 09:20 I!I

Internal Standard % Recovery Qualifier Limits Prepared Analyzed Dii Fac ILl13C-2,3,78-TCDD 76 40- 135 07/28/11 09:00 07/30/11 10:39 1.05 ..

13C-1,2,3,7,8-PeCDD 74 40- 135 07/28/11 09:00 07/30/11 10:39 1.05

13C-12,3,6,78-HxCDD 80 40- 135 07/28111 09:00 07/30/11 10:39 1.05

13C-23,7,8-TCDF 82 40- 135 07/28111 09:00 07/30/11 10:39 1.05

13C-12,3,78-PeCDF 78 40- 135 07/28/11 09:00 07/30/11 10:39 1.05

13C-1,23,478-HxCDF 77 40- 135 07/28111 09:00 07/30/11 10:39 1.05

Method: 6020 - Metals (ICPIMS)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Antimony <5.0 5.0 ugIL 08/01/11 08:48 08/06111 22:18 1

Arsenic 42 2.5 ugIL 08/01/11 08:48 08/06111 22:18 1

Barium 260 50 ug/L 08/01/11 08:48 08/06/11 22:18 1

Beryllium <0.50 0.50 ug/L 08/01/11 08:48 08/06111 22:18 1 :Cadmium <0.50 0.50 ugIL 08/OlIll 08:48 08/06/11 22:18 1

Chromium <5.0 5.0 ug/L 08/01/11 08:48 08/06/11 22:18 1

Cobalt <0.50 0.50 ugIL 08/01/11 08:48 08/06/11 22:18 1

Copper <5.0 5.0 ug/L 08/01/11 08:48 08/06/11 22:18 1

Lead <1.5 1.5 ug/L 08/01/11 08:48 08/06/11 22:18 1

Nickel <5.0 5.0 ugIL 08/01/11 08:48 08/06/11 22:18 1

Selenium <2.5 25 ugIL 08/01/11 08:48 08/06/11 22:18 1

Silver <1.0 1.0 ugiL 08/01/11 08:48 08/06/11 22:18 1

Thallium <1.0 1.0 ug/L 08/01/11 0848 08/06/11 22:18 1

Tin <5.0 5.0 ugiL 08/01/11 08:48 08/06/11 22:18 1

Vanadium <10 10 ugIL 08/01/11 0848 08/06/11 22:18 1

Zinc <20 20 ug/L 08/01/11 08:48 08/06/11 22:18 1

Method: 7470A - Mercury (CVAA)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac

Mercury <0.20 020 ug/L 08/02/11 09:42 08/02/11 1637 1

General ChemistryAnalyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

Cyanide, Total <0.010 0.010 mgIL 08/01/11 07.51 08/02/11 06:47 1

Analyte- Result Qualifier RL RL Unit D Prepared Analyzed Dii Fac

Sulfide 6.0 1 0 mgfL 07/27/11 14.10 1


0192


(DroitISte:Hercules Hattiesburg APIX 7l26111 . -

Client Sample ID: ASH-DUP-072611 Lab Sample ID: 680-70758-2Date Collected: 07/26/11 00:00 Matrix: Water


Method: 8260B - Volatile Organic Compounds (GCIMS)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Acetone <1300 1300 ugiL 07130/11 2103 50

Acetonitrile <2000 2000 ug/L 07/30/11 21:03 50

Acrolein <1000 1000 ug/L 07/30/11 21:03 50

Acrylonitnle <1000 1000 ugiL 07/30)11 2103 50

Benzene 5100 50 ug/L 07/30/11 21.03 50

Dichlorobromomethane <50 50 ug/L 07/30/11 21:03 50

Bromoform <50 * 50 ug/L 07/30/11 21.03 50

Bromomethane <50 50 ug/L 07/30/11 21 03 50

2-Butanone (MEK) <500 500 ug/L 07/30/11 2103 50

Carbon disultide <100 100 ug/L 07/30/11 21:03 50

Carbon tetrachloride 2700 • 50 ugIL 07/30/11 21:03 50

Chlorobenzene 240 50 ug/L 07/30/11 21:03 50

2-Chloro-1,3-butadiene <50 50 ug/L 07/30/11 21.03 50

Chloroethane <50 50 ug/L 07/30/11 21.03 50

Chloroform 640 50 ug/L 07/30/11 21:03 50

Chiorornelhane <50 50 ug/L 07/30/11 2103 50

3-Chloro-1-propene <50 50 ug/L 07/30/11 21 03 50

Chlorodibomomelhane <50 • 50 ugIL 07/30/11 2103 50

1,2-Dibromo-3-Chloropropane <50 50 ugIL 07/30/11 21 03 50

(4S\EthYlene Dibromide <50 50 ugIL 07/30/11 21:03 50

.,1Dibromomelhane <50 50 ugIL 07/30/11 21:03 50

trans-1,4-Dichloro-2-butene <100 100 ugIL 07/30/11 21:03 50


1,1-Dichloroethane <50 50 ug/L 07/30/11 21.03 50

1,2-Dichloroethane <50 50 ug/L 07/30/11 21 03 50

cis-1,2-Dichloroethene <50 50 ug/L 07/30/11 2103 50

trans-i 2-Dichloroethene <50 50 ug/L 07)30)11 2103 50

1,1-Dichloroelhene <50 50 ug/L 07/30/11 21.03 50

1,2-Dichloropropane <50 50 ug/L 07/30/11 21:03 50

cis-1,3-Dichloropropene <50 50 ug/L 07/30/11 21.03 50

trans-i,3-Dichloropropene <50 50 ug/L 07/30/11 2103 50

Ethylbenzene 61 50 ug/L 07/30/11 21.03 50

Ethyl methacrylate <50 50 ug/L 07/30/11 21 03 50

2-Hexarione <500 500 ugfL 07/30/11 21:03 50

lodomelhane <250 250 ug/L 07/30)11 2103 50

Isobutyl alcohol <2000 2000 ugfL 07/30/11 2103 50

Methacrylonhtrile <1000 1000 ug/L 07/30/11 21.03 50

Methylene Chloride 350 250 ug/L 07/30/11 21 03 50

Methyl melhacrylale <50 50 ug/L 07/30/11 21 03 50

4-Methyl-2-penlanone (MIBK) <500 500 ugfL 07/30/11 21 03 50

Penlachloroethane <250 250 ug/L 07/30/il 21 03 50

Propionllrile <1000 1000 ug/L 07)30/11 21 03 50

Styrene <50 50 ug/L 07/30/11 21 03 50

1,1,1,2-Tetrachloroethane <50 50 uglL 07/30)11 2103 50

1,1,2,2-Tetrachloroethane <50 50 ug)L 07/30/11 21.03 50

Telrachioroethene <50 50 ug!L 07/30/11 21:03 50

Toluene <50 50 ug/L 07/30/11 21.03 50

Q i,1,1-Trichloroelhane <50 50 ug/L 07/30/il 2103 50

1,l,2-Trichloroelhane <50 50 ug/L 07)30/11 2103 50

Trichloroethene <50 50 ug/L 07/30/11 21.03 50


of 92


Client Sample ID: ASH-DUP-072611 Lab Sample ID: 680-70758-2 —

Date Collected: 07/26111 00:00 Matrix: WaterDate Received: 07/27/11 09:20

Method: 8260B - Volatile Organic Compounds (GCIMS) (Continued)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Trichlorofluoromethane <50 50 ug/L 07/30/11 21:03 50

1,2,3-Trichloropropane <50 50 ug/L 07/30/11 21:03 50

Vinyl acetate <100 100 uglL 07/30/11 21:03 50

Vinyl chloride <50 50 ug/L 07/30/11 21:03 50

Xylenes, Total <100 100 uglL 07/30/11 21:03 50

Surrogate % Recoveiy Qualifier Limits Prepared Analyzed Dii Fac

4-romof1uorobenzene 104 70- 130 07/30/11 21:03 50

Dibromofluoromethane 103 70. 130 07/30/11 21:03 50

Toluene-dS (Surr) 104 70. 130 07/30/11 21:03 50

Method: 8270C - Semivolatile Organic Compounds (GCIMS)Analyse Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

Acenaphthene <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

Acenaphthylene <510 510 ug/L 07/28/11 14.42 08/03/11 13:21 50

Acetophenone <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

2-Acetylaminofluorene <510 510 ug/L 07)28/11 14:42 08/03/11 13:21 50

alpha,alpha-Dimethyl phenethylamine <100000 100000 ug/L 07/28/11 14:42 08/03/11 13:21 50

4-Aminobiphenyl <510 510 ug/L 07/28/11 1442 08/03/11 13:21 50

Aniline <1000 1000 ug/L 07/28/11 14:42 08/03/11 13:21 50

Anthracene <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

Aramite, Total <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

Benzo[a]anthracene <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

Benzo[a]pyrene <510 510 ugIL 07/28/11 14:42 08/03/11 13:21 50

Benzo[b)fluoranthene <510 510 ug/L 07/28/11 14:42 08)03/11 13:21 50

Benzo[g,h,i]perylene <510 510 ugfL 07/28/11 14:42 08/03/11 13:21 50

Benzo[k]fluoranthene <510 510 ug/L 07/28/11 1442 08/03/11 13:21 50

Benzyl alcohol <510 510 uglL 07/28/11 1442 08/03/11 13:21 50

11-Biphenyl <510 510 ug/L 07/28/11 1442 08/03/11 13:21 50

Bis(2-chloroelhoxy)methane <510 510 ug/L 07)28/11 14:42 08/03/11 13:21 50

Bis(2-chloroethyl)ether <510 510 ug/L 07/28/11 1442 08/03/11 13:21 50

bis(chloroisopropyl) ether <510 510 ug/L 07/28/11 14.42 08/03/11 13.21 50

Bis(2.ethylhexyl) phlhalate <510 510 ug/L 07/28/11 1442 08/03/11 13:21 50

4-Bromophenyl phenyl ether <510 510 ug/L 07/28/11 1442 08/03/11 13:21 50

Butyl benzyl phthalate <510 510 ug/L 07/28/11 1442 08)03/11 1321 50

4-Chloroaniline <1000 1000 ug/L 07/28/11 1442 08/03/11 13:21 50

4.Chloro-3-methylphenol <510 510 ug/L 07/28/11 1442 08/03/11 13:21 50

2-Chloronaphlhalene <510 510 uglL 07/28/11 1442 08/03/11 13.21 50

2-Chlorophenol <510 510 ug)L 01/28/111442 08/03/11 1321 50

4-Chiorophenyl phenyl ether <510 510 ug/L 07/28/li 1442 08/03/11 13.21 50

Chrysene <510 510 ug/L 07/28/11 1442 08/03/il 13:21 50

Diallate <510 510 ug/L 07)28/11 1442 08/03/11 13:21 50

Dibenz(ah)anlhracene <510 510 ug/L 07/28/11 14-42 08)03/11 13-21 50

Dibenzofuran <510 510 ug/L 07)28/11 1442 08)03/11 1321 50

12-Dichlorobenzene <510 510 ug/L 07)28/li 1442 08)03)11 13:21 50

13-Dichlorobenzene <510 510 ug/L 07)28)11 14-42 08)03/11 1321 50

1,4-Dichlorobenzene <510 510 ug/L 07/28)11 1442 08)03/11 13:21 50

3,3’-Dichlorobenzidine <3000 3000 ug/L 07/28/11 14:42 08)03)11 1321 50

2,4-Dich]orophenol <510 510 ug/L 07)28)11 14 42 08/03/11 13:21 50

2,6-Dichlorophenol <510 510 ug/L 07/28)11 1442 08/03)11 1321 50


of 92


Method: 8270C - Semivolatile Organic Compounds (GCIMS) (Continued)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

Diethyl phthalate <510 510 ugIL 07/28/11 14.42 08/03/11 13.21 50

Dimethoate <510 * 510 ugIL 07/28/11 1442 08/03/11 13.21 50

7.12-Dimethylbenz(a)anthracene <510 510 ug/L 07/28/111442 08/03/11 13:21 50

33’-Dimethylbenzidine <1000 1000 ug/L 07/28/11 14:42 08/03111 13:21 50

2,4-Dimethylphenol <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

Dimethyl phthalate <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

Di-n-butyl phthalate <510 510 ug/L 07/28111 14:42 08/03/11 1321 50

1,3-Dinitrobenzene <510 510 ugIL 07/28/11 1442 08)03/11 13:21 50

4,6-Dinitro-2-methylphenol <2500 2500 ugIL 07/28/11 14.42 08/03/11 13:21 50

2,4-Dinitrophenol <2500 2500 ug/L 07/28/11 1442 08/03/11 13:21 50

2,4-Dinitrotoluene <510 510 ugIL 07/28/11 14:42 08103/11 13:21 50

2,6-Dinitrotoluene <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

Di-n-octyl phthalate <510 510 ug/L 07/28)11 14:42 08/03/11 13.21 50

Dinoseb <510 510 ugIL 07/28/11 14-42 08/03/11 13:21 50

9400 510 ug/L 07/28)11 14:42 08/03/11 13:21 50

<510 * 510 ugIL 07/28/11 14:42 08/03/11 13:21 50

<510 510 ugIL 07/28/11 1442 08/03/11 13:21 50

<510 510 ug/L 07/28/11 1442 08)03/11 13:21 50

<510 * 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

<510 510 ug/L 07/28/11 14.42 08/03/11 1321 50

<510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

<510 510 ugIL 07/28/11 1442 08/03/11 13.21 50

<510 510 ug/L 07/28/11 14-42 08/03/11 1321 50

<510 510 ug/L 07/28/11 1442 08/03/11 13-21 50

<510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

<250000 250000 ug/L 07/28/11 14:42 08)03/11 13-21 50

<510 510 ug/L 07/28/11 14:42 08/03/11 13.21 50

<510 510 ug/L 07/28/11 14.42 08/03/11 13.21 50

<510 510 ug/L 07/28/11 14.42 08/03/11 1321 50

<510 510 ug/L 07/28/11 1442 08/03/11 13.21 50

<100000 100000 ugIL 07/28/11 1442 08/03/11 13-21 50

<510 510 ugIL 07)28/11 14.42 08/03/11 1321 50

<510 510 ug/L 07/28/11 1442 08/03/11 13:21 50

<510 510 ug/L 07/28/11 1442 08/03/11 13-21 50

<510 * 510 ug/L 07/28/111442 08/03/11 1321 50

<510 510 ugIL 07/28/111442 08/03/11 1321 50

<510 510 ug/L 07i28/1 1 1442 08/03/11 13.21 50

<510 510 ugIL 07/28/11 14.42 08/03/11 ‘321 50

<510 510 ug/L 07/28/11 14-42 08/03/11 1321 50

<510 510 ugIL 07/28/11 14.42 08/03/11 13-21 50

<510 510 ug/L 07/28/11 1442 08/03/11 1321 50

<2500 2500 ug/L 07/28/11 14:42 08/03/11 1321 50

<2500 2500 ugIL 07/28/11 14:42 08/03111 13-21 50

<2500 2500 ug/L 07/28/1114:42 08/03/11 13 21 50

<510 510 ug/L 07/28/11 1442 08/03/11 ‘3-21 50

<510 510 ug/L 07/28/11 1442 08/03/11 1321 50

<2500 2500 ug/L 07/28/11 14.42 08/03/11 13.21 50

<1000 1000 ug/L 07/28/11 14.42 08/03/11 1321 50

<510 510 ug/L 07)28)11 14.42 08/03/11 1321 50

<510 510 ug/L 07/28/11 1442 08/03/11 1321 50

Test.America Savannah


Client Sample ID: ASH-DUP-072611Date Collected: 07/26111 00:00



Lab Sample ID: 680-70758-2Matrix: Water

--U

1,4-Dioxane

Disulfoton

Ethyl methanesulfonate

Ethyl Parathion

Famphur

Q Fluoranthene

Fluorene

Hexachlorobenzene

- Hexachiorobutadiene

Hexachlorocyctopentadiene

Hexachloroethane

Hexachiorophene

Hexachloropropene

tndeno[1 2,3-cd]pyrene

Isophorone

lsosaurole

Methapyrilene

3-Methylcholanthrene

Methyl methanesulfonate

2-Methylnaphthalene

Methyl parathion

2-Methylphenol

3 & 4 Methylphenol

Naphihalene

1 ,4-Naphthoquinone

1 -Naphthylamine

2-Naphthylamine

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Nitrobenzene

2-Nitrophenol

4-Nitrophenot

Q 4-Nitroquinoline-1-oxide

N-Nitro-o-toluidine

N-Nitrosodiethylamine

of92

Client Sample ResultsClient: Ashland Inc. TestArnerica Job ID: 680-70758-1


Client Sample ID: ASH-DUP-07261 I Lab Sample ID: 680-70758-2

Date Collected: 07/26111 00:00 Matrix: Water


Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed —_Dii Fac

N-Nitrosodimethylamne <510 510 vg/L 07/28/1114:42 08/03/11 13:21 50

N-Nitrosodi-n-butylamine <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

N-Nitrosodi-n-propylamine <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

N-Nitrosodiphenylamine <510 510 ugiL 07/28/11 14:42 08/03/11 13:21 50

N-Nitrosomethylethylamine <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

N-Nitrosomorpholine <510 510 ugIL 07/28/11 14:42 08/03/11 13:21 50

N-Nitrosopipendine <510 510 ugIL 07/28/11 14:42 08/03/11 13:21 50

N-Nitrosopyrrolidine <510 510 ugIL 07/28/11 14:42 08/03/1113:21 50

o,o’,o”-Triethylphosphorothioate 3300 510 ugiL 07/28/11 14:42 08/03/11 13:21 50

p-Dimethylamino azobenzene <510 510 ug/L 07/28/11 14:42 08/03/1113:21 50

Penlachlorobenzene <510 510 uglL 07/28/11 14:42 08/03/11 13:21 50

Pentachlororiitrobenzene <510 510 uglL 07/28/11 14:42 08/03/11 13:21 50

Pentachlorophenol <2500 2500 ugIL 07/28/11 14:42 08/03/11 13:21 50

Phenacetin <510 510 ug!L 07/28/11 14:42 08/03/11 13:21 50

Phenanthrene <510 510 ugIL 07/28/11 14:42 08/03/11 13:21 50

Phenol <510 510 ugIL 07/28/11 14:42 08/03/11 13:21 50

Phorale <510 510 ugIL 07/28/11 14:42 08/03/11 13:21 50

2-Picoline <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

p-Phenylenediarn,ne <100000 100000 ugIL 07/28/11 14:42 08/03/11 1321 50

Pronamide <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

Pyrene <510 510 ug/L 07/28/11 14.42 08/03/11 13:21 50

Pyridine <2500 2500 ug/L 07/28/11 14:42 08/03/11 13:21 50

Safrole, Total <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

Sulfotepp <510 510 ug/L 07/28/11 1442 08/03/11 1321 50

1,2,4,5-Tetrachlorobenzene <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

2,3,4,6-Tetrachlorophenol <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

Thionazin <510 510 ug/L 07/28/11 14:42 08/03/11 13:21 50

2-Tolijidine <510 510 ugIL 07/28/11 14:42 08/03/11 1321 50

1,2,4-Trichlorobenzene <510 510 ugIL 07)28/11 14:42 08/03/11 13:21 50

2,4,5-Trichlorophenol <510 510 ugIL 07/28/11 1442 08/03/11 1321 50

2,4,6-Thchlorophenol <510 510 ugfL 07/28/11 14:42 08/03/11 13:21 50

1,3,5-Trinitrobenzene <510 510 ug/L 07/28/11 14:42 08/03/11 13.21 50

Surrogate % Recovery Qualifier Limits Prepared Analyzed Dii Fac

2-Fluorobiphenyl 0 0 38-130 07/28111 14:42 08/03/11 1321 50

2-Fluorophenol 0 0 25 130 07/28/Il 14.42 08/03/lI 1321 50

Nitrobenzene-d5 0 0 39 130 07/28/11 1442 08/03/11 1321 50

Phenol-d5 0 0 25- 130 07/28/11 14:42 08/03/11 1321 50

Terphenyl-d14 0 0 10- 143 07/28/11 14:42 08/03/11 13:21 50

2,4,6-Tribromophenol 0 0 31141 07/281111442 08/03/111321 50

Method: 8081A_8082 - Organochiorine Pesticides & PCBs (GC)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac

Aldrin <0.049 0.049 ug/L 07/28/11 14:42 08/01/11 20:39 1

alpha-BHC 0.75 0049 ugIL 07/28/11 1442 08/01/11 20:39 1

beta-BHC <0.049 0049 ug/L 07/28)11 1442 08/01/11 2039 1

Chlordane (technical) <049 049 ugIL 07/28/11 1442 08/01/11 20:39 1

Chlorobenzilate <0.49 049 ugIL 07/28/11 14:42 08/01/11 20.39 1

44-ODD <0.098 0098 ug/L 07128)11 14:42 08/01/11 2039 1

4,4-DDE <0098 0 098 ug/L 07/28)1114:42 08/01/11 2039 1


of 92



Client Sample ID: ASH-DUP-072611 Lab Sample ID: 680-70758-2

Date Collected: 07/26/11 00:00 Matrix: Water

Date Received: 07127/11 09:20

Surrogate

Tetrachloro-m-xylene


DCB Decachlorobiphenyl


% Recovery Qualifier

44

35 X

/4 X

2 pX

Limits

36. 130

36. 130

40.. 130

40 130


409 X 52- 151

92 p 52. 151

Method: 8290 - DioxinslFurans, HRGCIHRMS (8290)

Prepared

07/28/11 1442

07/28/11 1442

07/28/Il 14:42

07/28/11 14:42

Analyzed

08/01/11 20.39

08/01/11 20.39

08/01/Il 2039

08/01/11 20.39


Method: 8081A_8082 - Organochiorine Pesticides & PCBs (GC) (Continued)Analyte Result Qualifier RL MDL Unit

4,4’-DDT

delta-BHC

Dieldrin

Endosulfan I

Endosulfan II

Endosulfan sulfate

Endrin

End tin aldehyde

Endrin ketone

gamma-BHc (Lindane)

Heptachlor

Heptachlor epoxide

Isodrin

Kepone

Methoxychior

Toxaphene

PCB-1016

PCB-1221

PCB-1 232

OPCB-1242

PCB-1 248

PCB-1254

PCB-1 260

<0.098

<0.049

<0.098

<0.049

<0.098

<0.098

<0.098

<0.098

<0.098

0.45

<0.049

<0.049

<0,049

<0.98

<0.098

<4.9

<0.98

<2.0

<0.98

<0.98

<0.98

<0.98

<0.98

0.098

0.049

0.098

0.049

0.098

0.098

0.098

0.098

0.098

0.049

0.049

0.049

0.049

0.98

0.098

4,9

0.98

2.0

0,98

0,98

0.98

0.98

0.98

O Prepared

— 07/28/11 14:42

07/28/11 14:42

07/28/11 14.42

07/28/1114:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07)28/11 14:42

07)28/11 1442

07/28/11 14:42

07/28/11 14:42

07/28/11 1442

07/28/11 14:42

Analyzed

08/01/11 20:39

08/01/11 20:39

08/01/11 20:39

08/01/11 20:39

08/01/11 2039

08101/11 20:39

08/01/11 20:39

08101/il 20:39

08/01/11 20:39

08/01/11 20:39

08/01/11 20:39

08/01/11 20:39

08/01/11 20:39

08)01/11 20:39

08/01/11 20:39

08/01/11 20:39

08/01111 20:39

08/01/11 20:39

08/01/11 2039

08/01/11 20:39

08/01/11 20.39

08/01/11 20:39

08/01/11 2039

ug/L

ug/L

ug/L

ug/L

ug’L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ugIL

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug)L

ug/L

ug/L

u9/L

MDL tin/I

Ug/L

ug/L

ug/L

Method: 8151A - Herbicides (GC)Analyte

2,4-D

Silvex (2,4,5-TP)

2 4,5-T

Surrogate

DCAA

DCAA

Oil Fac

Dil Fec

Oil Fac

Dil Fac

Oil Fac

1.01

1.01

1 01

1.01

1.01

1.01

1.01

Result Qualifier

<0 50

<0 50

<0 50

RL

0 50

0.50

0 50

Analyte Result Qualifier ML EDL TEF TEQ

2,3,78-TCDD ND 10 039 1

Total HXCDD ND 51 056

Total HxCDF ND

Total PeCOD ND

Total PeCDF ND

QTotal TCDD ND

Total TCDF 66

13 Prepared

07)28/11 08 04

07/28/11 0804

07/28/11 08 04

Prepared

07/28/11 0804

07/28/li 08.04

Unit D Prepared

pg/L 07/28/11 0900

pg/L 07/28/11 09 00

pg/L 07/28/11 0900

pg/L 07/28/11 09 00

pg/L 07/28/11 09 00

pg/L 07/28/11 0900

pg/L 07/28/11 0900

Analyzed

07/29/11 1853

07/29/11 1853

07/29/11 18.53

Analyzed

07/29/11 /853

07/29/11 1853

Analyzed

07/30/11 11.24

07/30/11 11.24

07/30/11 1124

07/30/11 11.24

07/30/11 1124

07/30/11 11.24

07/30/11 1124

Total TEQ (EPA 1989)

51 015

51 0.49

51 8.0

10 0,57

10 60

0.00

of 92


Client Sample ResultsTestAmerica Job ID: 680-70758-1

Client Sample ID: ASH-DUP-072611Date Collected: 07/26I11 00:00Date Received: 07127111 09:20


0

Method: 6020 - Metals (ICP1MS)Analyte

Antimony

Arsenic

Barium

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Nickel

Selenium

Silver

Thallium

Tin

Vanadium

Zinc

% Recoveiy Qualifier Limits

79 40135

Method: 7470A - Mercury (CVAA)Analyte

Mercury

Result Qualifier RL

<0 20 0.20

MDL Unit 0 Prepared Analyzed

ug/L 08/02/11 09.42 08/02/11 16.40

Dil Fac

RL Unit D Prepared Analyzed Oil Fac

mg/L 07/27/11 1410 1


0

Internal Standard

i3C-2,3,78-TCDD

13C-1,2,3, 78-PeCDD

13C-1,2,3,6, 7,8-HxCDD

13C-23,7,8-TCDF

l3C-12,3, 7,8-PeCDF

13C-12,34, 78-HxCDF

75 40135

85 40135

86 40135

79 40135

81 40.135

Result Qualifier RI

<5.0 5.0

44 2.5

260 5.0

<0.50 0.50

<0.50 0.50

<5.0 5.0

<0.50 050

<5.0 5.0

<1.5 1.5

<5.0 5.0

<2.5 2.5

<1.0 10

<1.0 1.0

<5.0 5.0

<10 10

<20 20

Prepared Analyzed

07128./li 09:00 07/30/11 11:24

07/28.1110900 07/30/11 11:24

07128111 09:00 07/30/11 11:24

07/281110900 07/30/11 11:24

07/28/Il 09-00 07/30/11 11:24

07128111 09:00 07/30/11 11:24

Prepared Analyzed

08/01/11 08:48 08/06111 22:51

08/01/11 08:48 08/06/11 22:51

08/01/11 08:48 08/06/11 22:51

08/01/11 08:48 08/06/11 22:51

08/01/11 08:48 08/06/11 22:51

08/01/11 08:48 08/06/11 22:51

08/01/11 08.43 08/06/11 22:51

08/01/11 08:48 08/06/11 22:51

08/01/11 08:48 08/06/11 22:51

08/01/11 08-48 08/06/11 22:51

08/01/11 08:48 08/06/11 22:51

08/01/11 08:48 08/06/11 22.51

08/01/11 08:48 08/06/11 22:51

08/01/11 08:48 08/06/11 22.51

08/01/11 08:48 08/06/11 22:51

08/01/11 08:48 08/06/11 22:51

Dii Fac

1.01

1.01

1.01

1.01

1.01

1.01

Oil FacMDL Unit 0

ug/L

ugIL

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

uglL

General ChemistryAnalyte Result Qualifier

Cyanide, Total <0010

0

Analyte

Sulfide

Result Qualifier

17

RL

10

RL MDL Unit 0 Prepared Analyzed Dii Fac

0 010 mg/I 08/01/Il 07:51 08/02/11 06:48 1

of 92


Qroject/Site: Hercules Hattiesburg APIX 7/26/11

...

....

Client Sample ID: ASH-RSI-07261 i Lab Sample ID: 680-70758-3



Method: 8260B -Volatile Organic Compounds (GCIMS)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Acetone <25 25 ug/L 07129/11 19:04 1

Acetonitnle <40 40 ug/L 07)29/11 1904 1

Acrolein <20 20 ugil 07129111 19:04 1

Acrylonitrile <20 20 ug/L 07/29/11 19:04 1

Benzene <1.0 1 0 ug/L 07/29/11 19.04 1

Dichlorobromomethane <1.0 1.0 ugIL 07/29/11 19:04 1

Bromoform <1.0 * 1.0 ug/L 07/29111 19:04 1

Bromomethane <1.0 1.0 ug/L 07/29/11 19:04 1

2-Butanone (MEK) <10 10 ug)L 07/29/11 19:04 1

Carbon disulfide <2.0 2.0 ug/L 07/29/11 19.04 1

Carbontetrachloride <1.0 1.0 ugIL 07/29/11 1904 1

Chlorobenzene <1.0 1.0 ug)L 07/29/11 1904 1

2-Chloro-13-butadiene <1.0 1 0 ug/L 07/29111 19,04 1

Chloroethane <1.0 1.0 ug/L 07/29/11 19.04 1

Chloroform <1.0 1 0 ug/L 07/29/11 19:04 1

Chloromethane <1.0 1.0 ug)L 07/29/11 19:04 1

3.Chloro-1-propene <1 0 1.0 ug/L 07/29/11 19:04 1

Chlorodibromomethane <1.0 1.0 ug/L 07/29)11 1904 1

1,2-Dibromo-3-Chloropropane <1.0 * 1.0 ug/L 07/29/11 19:04 1

Ethylene OibromIde <1.0 1.0 ug/L 07)29/11 1904 1

Dibromomethane <1.0 1.0 ug/L 07/29/11 1904 1

trans-14-Dichloro-2-butene <20 2.0 ugIL 07/29/11 19:04 1

Dichlorodifluoromethane <1.0 1.0 ug)L 07)29/11 19.04 1

11-Dichloroethane <1.0 1.0 ugIL 07/29/11 19:04 1

1,2-Dichloroethane <1 0 1.0 ug/L 07/29/11 19.04 1

cis-1,2-Dichloroelhene <1 0 1.0 ug)L 07/29)11 1904 1

trans-12-Dichloroethene <1 0 1 0 ug/L 07/29/11 1904 1

1.1-Dichloroethene <1 0 1 0 ug/L 07/29/11 19.04 1

1,2-Dichloropropane <10 1.0 ug/L 07/29)11 1904 1

cis-1,3-Dichloropropene <10 1 0 ug)L 07/29/11 1904 1

trans-1,3-Dichloropropene <1.0 1.0 ug/L 07/29)11 19:04 1

Ethylbenzene <1.0 1.0 ug/L 07/29/11 1904 1

Ethyl methacrylate <1 0 1 0 ug/L 07/29)11 1904 1

2-Hexanone <10 10 ug/L 07/29/11 1904 1

lodomelhane <50 50 ug/L 07/29/11 1904 1

Isobutyl alcohol <40 40 ug/L 07/29/11 1904 1

Methacrylorntrile <20 20 ug/L 07/29/11 1904 1

Melhylene Chloride <50 5.0 ug)L 07)29/1119:04 1

Methyl methacrylate <1 0 1 0 ug/L 07/29/11 1904 1

4-Methyl-2-penlanone (MIBK) <10 10 ug/L 07/29/H 1904 1

Pentachloroelhane <5 0 5 0 ug)L 07/29/111904 1

Propionitrile <20 20 ug)L 07/29/11 1904 1

Styrene <10 1.0 ug/L 07/29/11 1904 1

1,1,1,2-Tetrachloroethane <10 1.0 ug/L 07/29/11 1904 1

1,1,2,2-Tetracl,loroethane <1 0 1.0 ug)L 07/291111904 1

Tetrachloroelhene <1 0 1 0 ug/L 07/29/11 19:04 1

Toluene <1 0 1 0 ug/L 07/29/11 1904 1

1,1,1-Tnchloroethane <1 0 1.0 ug/L 07/29/11 19:04 1

1,1,2-Trichloroethane <1 0 1.0 ug/L 07/29/11 19:04 1

Tnchloroethene <1 0 1 0 ug/L 07/29/11 19.04 1


of 92

Client: Ashland Inc TestAmerica Job ID: 680-70758-1 IhSáProject/Site: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-RSI-072611 Lab Sample ID: 680-70758-3 . )Date Collected: 07126/Il 08:57 Matrix: Water



07129/11 19.04 1

07129/11 19:04 1

70130 07/29/111904 1

Method: 8270C - Semivolatile Organic Compounds (GCIMS)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fat

A <10 10 ug/L 07/28/11 14:42 08/02111 18.32 1

Acenaphthylene <10 10 ug/L 07/28111 14:42 08/02/11 18:32 1

Acetophenone <10 10 ug/L 07/28/11 14:42 08/02/11 1832 1

2-Acetylaminofluorene <10 10 ugIL 07/28/11 14:42 08/02111 1832 1

apha,alpha-Dimethyl phenelbyJamine <2100 2100 ugIL 07/28/11 14:42 08/02111 18:32 1

4 Aminobiphenyl <10 10 ug)L 07/28/11 14:42 08/02/11 18.32 1

An/me <21 21 ug/L 07/28/11 14.42 08/02/11 1832 1

Anthracene <10 10 ug/L 07/28/11 14:42 08/02/11 18.32 1

Aramite, Total <10 10 ug/L 07/28/11 1442 08/0211118:32 1

Benzo[a]anthracene <10 10 ugIL 07/28/11 14.42 08/02/11 18.32 1

Benzoa]pyrene <10 10 <gIL 07/28/11 14.42 08/0211118:32 1

Benzo(b)f/uoranthene <10 10 ug)L 07/28/11 14:42 08)02/11 18.32 1

Benzo[g,h,i]perylene <10 10 ug)L 07/28/11 14:42 08/0211118.32 1

Benzo[kjfluoranthene <10 10 ug/L 07/28/11 1442 08/02)11 1832 1

Benzyl alcohol <10 10 ug/L 07/28/11 1442 08/02/11 18:32 1

1,1-Biphenyl <10 10 ug/L 07/28/11 14.42 08/02/11 1832 1

Bis(2-chloroethoxy)methane <10 10 ug/L 07/28/11 14.42 08/02/11 18.32 1

Bis(2-chloroethyl)ether <10 10 <gIL 07/28/11 1442 08)02/11 18.32 1

bis(chloroisopropyl) ether <10 10 ugIL 07/28/1114 42 08/02/111832 1

Bis(2-ethylhexyl) phthalate <10 10 uglL 07/28/11 14.42 08/021111832 1

4-Bromophenyl phenyl ether <10 10 <gIL 07)28/11 1442 08/02/111832 1

Bulyl benzyl phlhalate <10 10 ugIL 07/28/11 14:42 08/02/11 1832 1

4-Chloroaniline <21 21 ug/L 07/28)1114 42 08)02/111832 1

4-Chloro-3-methylphenol <10 10 <gIL 07/28/11 1442 08/02/1118.32 1

2-Chloronaphlhalene <10 10 ugIL 07/28/11 1442 08/02111 1832 1

2-Chlorophenol <10 10 ug/L 07/28/111442 08/021111832 1

4-Chlorophenyl phenyl ether <10 10 ugIL 07/28/1114:42 08/02/11 1832 1

Chryserie <10 10 ug/L 07/28/11 1442 08/02/11 1832 1

Dial/ate <10 10 <gIL 07/28)11 1442 08/021111832 1

Dibenz(a.h)anthracene <10 10 ug/L 07/28/11 1442 08/02/11 1832 1

Dibenzofuran <10 10 ugIL 07)28/11 1442 08/02)11 1832 1

1,2-Dichlorobenzene <10 10 ug/L 07/28/11 14.42 08/02/111832 1

1 ,3-Dichlorobenzene </0 10 ugIL 07/28/1114 42 08/02/1118 32 1

1,4-Dichlorobenzene <10 10 ugIL 07/28/11 1442 08/02)11 1832 1

3,3’-Dichlorobenzidine <62 62 ugIL 07/28/11 1442 08/02/11 1832 1

2,4-Dichlorophenol <10 10 <g/L 07)28/11 1442 08)02/11 18.32 1

2,6-Dichlorophenol <10 10 <gIL 07/28)11 1442 08/02/11 1832 1



Method: 8260B Volatile Organic Compounds (GC!MS) (Continued)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed

Trichlorofluoromethane <10 10 <gIL - 07/29/11 1904

1,2,3-Trichloropropane <10 1.0 ugIL 07/29/11 19:04

Vinyl acetate <2.0 2 0 ug/L 07/29/11 1904

Vinyl chloride <1.0 1 0 ug)L 07/29/11 19:04

Xylenes. Total <20 20 ug/L 07/29/11 19.04

Swrogate % Recovery Qualifier

4-Bromofluorobenzerte 94

Dibromofluommethane 103

Toiuene-d8 (Surr) 100

Limits

70- 130

70 130

-

Dii Fac

1‘p

of 92






Method: 8270C - Semivolatile Organic Compounds (GCIMS) (Continued)Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fac

Diethyl phthalate -— — <10 - 10 ug/L — 07/28/11 14:42 08/02111 18:32 1

Dimethoate <10 10 ugIL 07/28/11 14:42 08/02111 18:32 1

7, 12-Dimethylbenz(a)anthracene <10 10 ugh 07/2811114:42 08/02111 18:32 1

33-Dimethylbenzidine <21 21 ug/L 07/28/11 14:42 08102/11 18:32 1

24-Dimethylphenol <10 10 ug/L 07/28/11 14:42 08/02)11 18:32 1

Dimethyl phthalate <10 10 ug/L 07/28/11 14:42 08/02)11 18:32 1

Di-n-butyl phthalate <10 10 ugIL 07/28/11 14:42 08/0211118:32 1

13-Dinttrobenzene <10 10 ugIL 07/28/11 14:42 08/02/1118:32 1

46-Dinltro-2-methylphenol <52 52 ugIL 07/28/11 14:42 08/02/1118:32 1

24-Dinitrophenol <52 52 ugIL 07/28/11 14:42 08/0211118:32 1

24-Dinitrotoluene <10 10 ug/L 07/28/11 14:42 08/02/11 18:32 1

26-Dinitrotoluene <10 10 ug/L 07/28/11 14:42 08/02/1118:32 1

Di-n-octyl phthalate <10 10 ug/L 07/28/11 14:42 08/02/11 18:32 1

Dinoseb <10 10 ug/L 07/28/11 14:42 08/02)11 18:32 1

14-Dioxane <10 10 ug/L 07)28/11 14:42 08/02/1118:32 1

Disulfoton <10 * 10 ug/L 07/28/11 14:42 08/02/11 18:32 1

Ethyl methanesulfonate <10 10 ugIL 07/28/11 14:42 08/02/1118:32 1

Ethyl Parathion <10 10 ugIL 07/28/11 14:42 08/02/11 18:32 1

Famphur <10 * 10 ug)L 07/28/11 14:42 08/02/1118:32 1

OFluoranthene <10 10 ug/L 07/28/11 14:42 08/02/11 18:32 1

Fluorene <10 10 ug/L 07/28/11 14:42 08/02/11 18:32 1

Hexachlorobenzene <10 10 ugh 07/28/11 1442 08/02/11 18.32 1

Hexachlorobutadiene <10 10 ugIL 07/28/11 14:42 08/02/11 18:32 1

Hexachlorocyclopentadiene <10 10 ug/L 07/28/11 14:42 08/02/11 18:32 1

Hexachloroethane <10 10 ug/L 07/28/11 1442 08/02/11 18:32 1

Hexachlorophene <5200 5200 ug/L 07/28/11 1442 08/02/11 18:32 1

Hexachloropropene <10 10 ug/L 07/28/11 1442 08/02/11 18:32 1

lndeno[123-cd]pyrene <10 10 ug/L 07/28/11 14:42 08/02/11 18:32 1

Isophorone <10 10 ug/L 07/28/11 14:42 08/02/1118:32 1

Isosafrole <10 10 ug/L 07/28/11 1442 08/02/11 18:32 1

Methapyrilene <2100 2100 ug/L 07/28/11 1442 08/02/11 1832 1

3-Methylcholanthrene <10 10 ugIL 07/28/11 1442 08/02)11 1832 1

Methyl methanesulfonate <10 10 ug/L 07/28/11 1442 08/02/11 1832 1

2-Methylnaphthalene <10 10 ug/L 07/28/11 14.42 08/02/11 18:32 1

Methyl parathion <10 10 ug/L 07/28/11 1442 08/02/111832 1

2-Methylphenol <10 10 ug/L 07/28/11 14.42 08/02/11 18.32 1

3 & 4 Methylphenol <10 10 ug/L 07/28/111442 08/02/11 1832 1

Naphthalene <10 10 ug/L 07/28/11 14.42 08/02/11 1832 1

1,4-Naphthoquinone <10 10 ug/L 07/28/11 1442 08/02/11 1832 1

1-Naphthylamine <10 10 ug/L 07/28/11 1442 08/02)1118:32 1

2-Naphthylarnine <10 10 ug/L 07/28/11 14.42 08/02/11 18.32 1

2-Nitroaniline <52 52 ug/L 07/28/11 1442 08/02/11 1832 1

3-Nitroaniline <52 52 ug/L 07/28/11 1442 08)02/11 18:32 1

4-Nitroanilne <52 52 ugIL 07/28/11 1442 08/02/11 18.32 1

Nitrobenzene <10 10 ug/L 07/28/11 1442 08/02/11 1832 1

2-Nitrophenol <10 10 ug/L 07/28/11 14.42 08/02/11 18:32 1

4.Nitrophenol <52 52 ug/L 07/28/11 14.42 08/02/11 1832 1

(7N14-NitroquinoHne-1-oxide <21 21 ug/L 07/28/11 1442 08/02/11 1832 1

j’N-Nltro-o.toludine <10 10 ug/L 07/28/11 1442 08/02/11 1832 1

N-Nitrosodiethylamtne <10 10 ug/L 07/28/111442 08/02/11 18:32 1


of 92

Client Sample ResultsClient: Ashland Inc.ProjecUSite: Hercules Hattiesburg APIX 7/26/11

TestAmerica Job ID: 680-70758-1

Pyrene

Pyncline

Safrole, Total

Sulfotepp



Thionazin

2-Toluidine


2,4,5-Tnchlorophenol

2,4,6-Trichiorophenol

1 ,3,5-Trinitrobenzene

ThLab Sample ID: 680-70758-3 j

Matrix: Water <‘

‘1


Client Sample ID: ASH-RSI-072611Date Collected: 07126111 08:57Date Received: 07I27111 09:20

Method: 8270C - Semivolatile Organic Compounds (GCIMS) (Continued)AnalySe Result Qualifier RL MDL Unit - D Prepared —

N-Nitrosodimethylamine <10 10 ug/L 0712811114:42

N-Nitrosodi-n-butylamine <10 10 ugIL 07/28/11 14:42

N-Nitrosodi-n-propylamine <10 10 ugIL 07/28/11 14:42

N-Nitrosodiphenylamine <10 10 ug/L 07/28/11 14:42

N-Nitrosomethylethylamine <10 10 ug/L 07/28/11 1442

N-Nitrosomorpholine <10 10 ugIL 07)28/11 14.42

N-Nitrosopiperidine <10 10 ugIL 07/28/11 14:42

N-Nitrosopyrrolidine <10 10 ugiL 07/28/11 14:42

o,o,o”-Trjethylphosphorothioate <10 10 ug/L 07/28)11 1442

p-Dimethylaminoazobenzene <10 10 ugIL 07/28/11 14:42

Pentachlorobenzene <10 10 ugIL 07/28/11 14:42

Pentachloronitrobenzene <10 10 ug/L 07/28/11 14:42

Pentachlorophenol <52 52 ugIL 07/28/11 14:42

Phenacetin <10 10 ug/L 07)28/11 14:42

Phenanthrene <10 10 ug/L 07/28/11 14:42

Phenol <10 10 ugIL 07128)11 14:42

Phorate <10 10 ugIL 07)28/11 14:42

<10 10 ug)L 07/28/11 14:42

<2100 2100 ugIL 07/28/11 1442

<10 10 ug/L 07)28/11 1442

<10 10 ugIL 07/28/11 1442

<52 52 ug/L 07/28/11 14:42

<10 10 ugIL 07/28/11 14:42

<10 10 ug/L 07/28)11 14.42

<10 10 ug/L 07/28/11 14:42

<10 10 ugIL 07/28)11 14:42

<10 10 ug/L 07/28)11 1442

<10 10 ug/L 07/28/11 1442

<10 10 ug/L 07)28)11 14:42

<10 10 ug/L 07/28/11 1442

<10 10 ug/L 07/28/11 1442

<10 10 ugIL 07/28/11 14:42

2-Picoline

p-Phenylene diamine

Pronamide

Analyzed Dii Fac

08)02)11 18:32 1

08/02/11 18:32 1

08/02/11 18:32 1

08/02)11 18:32 1

08/02/11 18:32 1

08/02/11 18:32 1

08/02/11 18:32 1

08/0211118:32 1

08/02/11 18:32 1 =08/02)1118:32 1

08/02/1118:32 1

08/0211118:32 1

08/02)1118:32 1

08/02/11 18:32 1

08/02)1118:32 1

08/0211118:32 1 ),

08/02/11 18:32 1

08/0211118:32 1

08/0211118:32 1

08/0211118:32 1

08)0211118.32 1

08(02/11 18:32 1

08/02/11 18:32 1

08/02/11 18:32 1

08/02/11 18:32 1

08/02/11 1832 1

08/02/11 18:32 1

08/02/11 18:32 1

08/02/11 18:32 1

08/02/11 18:32 1

08(02/11 18:32 1

08/02/11 1832 1


2-Fluorobiphenyl 63 38 130

2.Fluorophenol 67 25. 130

Nitrobenzene-d5 74 39 - 130

Phenol-d5 63 25l30

Terphenyl-d14 81 10.143

2,4,6-Tnbromophenol 76 31 - 141

Method: 8081 A_8082 - Organochlorine Pesticides & PCBs (GC)Analyte Result Qualifier RL

Aldrin <0 051 0 051

alpha-BHC <0 051

beta BHC <0 051

Chiordane (technical) <o 51

Chlorobenzilate - 51

4,4’-DDD <0 10

4.4-DDE

Prepared

07/28/11 1442

07,28/11 1442

07/28/11 1442

07/28/11 1442

07/28/lI 1442

07/28/11 1442

MDL Unit D Prepared

ugIL 07/28)11 1442

ugIL 07/28)1114:42

iig/L 07/28/11 1442

ug/L 07)28/11 14:42

ug/L 07/28/11 1442

ug/L 07/28/11 14.42

ug/L 07/28/11 1442

Analyzed

08/02/11 18:32

08/02/11 18.32

08/02/11 1832

08/02/1 I 1832

08/02111 18.32

08/02/1118.32

Analyzed

08/01/11 20:58

08/01/11 2058

08/01/11 20:58

08/01/11 2058

08/01/11 2058

08/01/11 20.58

08/01/11 2058

0051

0051

0 51

051

0.10

0 10<0 10

Dil Fac

Dii Fac

of 92


(roject/Site: Hercules Hattiesburg APIX 7/26/11


bate Collected: 07/26/11 08:57 Matrix: Water


Method: 8081A_8082 - Organochiorine Pesticides & PCBs (GC) (Continued)

Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed DII Fac

44-DDT <010 010 ug/L 07/28/11 14:42 08/01/11 20:58 1

delta-BHC <0.051 0051 ug/L 07/28/11 14:42 08/01/11 20:58 1

I DieldrIn <0.10 0.10 ugIL 07/28/11 14:42 08/01/11 20:58 1

Endosulfan I <0.051 0.051 ug/L 07/28/11 14:42 08/01/11 20:58 1

Endosulfan II <0.10 0.10 ug/L 07/28/11 14:42 08/01/11 20:58 1

Endosulfan sulfate <0.10 0.10 ug/L 07/28/11 14.42 08/01/11 20:58 1

Endrin <0.10 0.10 ug/L 07/28/11 14.42 08/01/11 20:58 1

Endrin aldehyde <0.10 0.10 ugh 07/28/1114:42 08)01/11 20:58 1

Endrin ketone <0.10 0.10 ug/L 07/28111 14:42 08/01111 20:58 1

gamma-BHC (Lindane) <0051 0.051 ugiL 07/28/11 14:42 08101/11 20:58 1

Heptachlor <0.051 0.051 ugIL 07)28/11 14:42 08/01/11 20:58 1

Heptachlorepoxide <0.051 0.051 ug/L 07/28/11 14:42 08/01/11 20:58 1

Isodrin <0.051 0.051 ug/L 07/28/11 14:42 08/01/11 20:58 1

Kepone <1.0 1.0 ug/L 07/28/11 14:42 08/01/11 20:58 1

Methoxychlor <0.10 0.10 ug/L 07/28/11 14:42 08I01/il 20:58 1

Toxaphene <5.1 5.1 ug/L 07/28/11 1442 08/01/11 20:58 1

PCB-1016 <1.0 1.0 ug/L 07/28/11 14:42 08/01111 20:58 1

PCB.1221 <2.1 2.1 ug/L 07/28/11 14:42 08/01/11 20:58 1

PCB-1232 <1.0 1.0 ug)L 07/28/11 14:42 08/01/11 20:58 1

O PCB-1242 <1.0 1.0 ugIL 07/28/11 14:42 08/01/11 2058 1

PCB-1 248 <1.0 1.0 ug/L 07/28/11 14.42 08/01/11 20:58 1

PCB-1254 <1.0 1.0 ug)L 07)28/11 14:42 08/01111 20:58 1

PCB-1260 <1.0 1.0 ug/L 07/28/11 14:42 08101/11 20:58 1

Surrogate % Recovery Qualifier Limits Prepared Ana(yzed Dii Fac

Tetrachloro-m-xylene 63 — 36. 130 07/28111 14:42 08/01/11 20:58

Tetrachhzro-m-xylene 64 36 - 130 07/28/11 1442 08/01/11 20 58 1

DCB Decachlorob,phenyl 51 40 130 07/28111 14.42 08/01/11 20:58

DCB Decachlorobiphenyl 48 40. 130 07/28/1114:42 08/01/11 20:58 1

Method: 8151A - Herbicides (GC)

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac

24-0 <0.50 050 ug/L — 07/28/11 08:04 07/29/11 19:08 1

Silvex (2,4,5-TP) <0.50 0.50 ug/L 07/28/11 08.04 07/29/11 19.08 1

2,4,5-T <0.50 0.50 ug/L 07)28/11 08:04 07/29/11 19:08 1


DCAA 77 52.151 07/281110804 07/29/11 1908 1

DCAA 73 52. 151 07/28/110804 07/29/11 1908 1

Method: 8290 - DioxinslFurans, HRGC/HRMS (8290)

Analyte Result Qualifier ML EDL TEF — TEQ Unit D Prepared Analyzed DII Fac

2,3.7,8-TODD ND 10 0.38 1 pgIL 07/28/11 0900 07)30111 1209 1 03

Total HxCDD ND 52 0.53 pg/L 07128)11 09:00 07/30/11 1209 1 03

Total HxCDF ND 52 0.21 pg/L 07/28/11 09:00 07/30/11 12:09 1.03

Total PeCDD ND 52 0.70 pg/L 07128)11 0900 07/30/11 1209 1 03

Total PeCDF ND 52 0.23 pg/L 07/28/11 09.00 07/30/111209 1 03

Total TCDD ND 10 038 pg/L 07)28/11 09.00 07/30)11 12:09 1.03

Total TCDF ND 10 034 pg/L 07/28/11 09:00 07/30/11 12.09 1 03



of 92

Client Sample ResultsClient Ashland Inc TestAmerica Job ID 680-70758-1


Client Sample ID: Ai-sI-o761i Lab Sample ID: 680-70758-3Date Collected: 07/26/11 08:57 Matrix: Water <P


Internal Standard % Recovery Qualifier Limits Prepared Analyzed Dii Fac

13C-2,3,7,8-TCDD 82 40 135 07/26/11 0900 07/30/11 1209 103 #

13C-1,2,3,7,8-PeCDD 83 40 135 07728)110900 07/30/11 1209 103

13C-1,2.3,6,7,8-HxCDD 87 40135 07/26/110900 07/30/111209 103

13C-2,3,7,8-TCDF 89 40 135 07728)110900 07/30/111209 103

13C-12,3,7,8-PeCDF 85 40 135 07/28/110900 07/30/11 1209 103

13C-1,2,3,4,7,8-HvCDF 82 40 135 07/28/110900 07/30/11 1209 103

Method: 6020 - Metals (ICPIMS)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Antimony <50 50 ug/L 08101111 08.48 08/06111 22:58 1

Arsenic <25 25 ug/L 08/01/11 0848 08/06/11 22.58 1

Barium 12 50 ug/L 08/01/11 0848 08/06/11 22:58 1

Beryllium <050 050 ug/L 08/01/11 08:48 08/06/11 22:58 1

Cadmium <050 050 ugIL 08/01/11 0848 08/06/11 22.58 1

Chromium <50 50 ug/L 08/01/11 0848 08/06/11 2258 1

Cobalt <050 050 ugIL 08/01/11 0848 08/06/11 2258 1

Copper <50 5 0 ugiL 08/01/11 0848 08/06/11 2258 1

Lead <15 1 5 ugiL 08/01/11 0848 08/06/11 2258 1

Nickel <50 50 ugIL 08/01/11 0848 08/06/11 2258 1

Selenium <25 25 ugIL 08/01)11 0848 08/06)11 2258 1

Silver <1 0 1 0 ugIL 08/01/11 0848 08/06/11 2258 1

Thallium <1 0 1 0 ug/L 08/01/11 0848 08/06/11 2258 1

Tin <50 50 ug/L 08/01/11 0848 08/06(11 2258 1

Vanadium <10 10 ug)L 08/01/11 0848 08/06/11 2258 1

Zinc <20 20 ug!L 08/01/Il 0848 08/06/11 2258 1

Method: 7470A - Mercury (CVAA)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac

Mercury <0 20 0 20 uglL 08/02/11 0942 08/02/1116 50 1

General ChemistryAnalyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Cyanide, Total <0010 0010 mg/L 08/01)11 0751 08/02/11 0649 1

Analyte — Result Qualifier RL RL Unit D Prepared Analyzed Dii Fac

Sulfide 23 1 0 mg)L 07/27/11 14 10 1


of 92


Client Sample ID: ASH-MWI 3-072611Date Collected: 07126111 09:20Date Received: 07/27/11 09:20


Method: 8260B - Volatile Organic Compounds (GCIMS)Analyte Result Qualifier RL

Acetone <250 250

Acetonitrile <400 400

Acrolein <200 200

Acrylonitrile <200 200

Benzene 390 10

Dichlorobromomethane <10 10

Bromoform <10 * 10

Bromomethane <10 10

2-Butanone (MEK) <100 100

Carbon disulfide <20 20

Carbon tetrachloride 620 10

Chlorobenzene 24 10

2-Chloro-i,3-butadiene <10 10

Chloroethane <10 10

Chloroform 210 10

Chloromethane <10 10

3-Chloro-1-propene <10 10

Chlorodibromomethane <10 10

1,2-Dibromo-3-Chloropropane <10 * 10

QEthylene Dibromide <10 10

Dibromomethane <10 10

trans-i ,4-Dichloro-2-butene <20 20

Dichlorodifluoromethane <10 10

11-Dichloroethar,e <10 10

l,2-Dichloroelhane <10 10

cis-l2-Dichloroethene <10 10

trans-i 2-Dichloroethene <10 10

1,1-Dichloroethene <10 10

12-Dichloropropane <10 10

cis-i3-Dichloropropene <10 10

trans-1,3-Dichloropropene <10 10

Ethylbenzene <10 10

Ethyl methacrylate <10 10

2-Hexanone <100 100

lodomethane <50 50

lsobutyl alcohol <400 400

Methacrylonitrile <200 200

Methylene Chloride <50 50

Methyl methacrylate <10 10

4-Methyl-2-pentanone (MIBK) <100 100

Pentachloroethane <50 50

Propionitnle <200 200

Styrene <10 10

1,1i2-Telrachloroethane <10 10

i,i22-Tetrachloroethane <10 10

Tetrachloroelhene <10 10

Toluene <10 10

1,1 ,i-Thchloroelhane

1 ,i2-Trichloroethane

Trichloroethene

D Prepared



ii

0

MDL Unit

ugIL

ug/L

ugIL

ug/L

ug/L

ug/L

ug/L

ug/L

ugIL

ug/L

ugIL

ug/L

ugIL

ugIL

ugIL

ug/L

ug/L

uglL

ug/L

ugiL

ug/L

ug/L

ug/L

ugiL

ugIL

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Analyzed

07/29111 20:03

07/29/11 20:03

07/29/11 20:03

07/29/11 20:03

07/29/11 2003

07/29/11 20:03

07/29/il 20:03

07/29/11 20:03

07/29/il 20:03

07/29/11 20:03

07/29/11 20:03

07/29/11 20:03

07129/il 20:03

07/29/11 20:03

07/29/11 20:03

07/29/il 20:03

07/29/11 20:03

07/29/11 2003

07/29/11 2003

07/29/11 20:03

07/29/li 20:03

07/29/li 20:03

07/29/11 20:03

07/29/11 20:03

07/29/11 20.03

07/29/il 20:03

07/29/11 20:03

07/29/il 2003

07/29/11 20.03

07/29/11 20:03

07/29/11 20 03

07/29/11 20.03

07/29/11 2003

07/29/11 2003

07/29/li 2003

07/29/11 2003

07/29/11 20.03

07/29/li 2003

07/29/li 20.03

07/29/li 2003

07/29/11 2003

07/29/11 2003

07/29/11 2003

07/29/11 2003

07/29/il 2003

07/29/11 20:03

07/29/li 2003

07/29/11 20.03

07/29/11 2003

07/29/11 2003

Dil Fac

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

<10

<10

<10

10

10

10

TestAmertca Savannah

of 92

Client Sample ResultsClient: Ashland Inc. TestAmerica Job ID: 680-70758-1 <1ProjectlSite: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-MWI3-072611 Lab Sample ID: 680-70758-4 -



Method: 8260B - Volatile Organic Compounds (GCIMS) (Continued)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Trichlorofluoromethane <10 10 ugIL 07/29111 20:03 10

1,2,3-Trichloropropane <10 10 ugIL 07129/11 20:03 10

Vinyl acetate <20 20 ugIL 07/29/11 20:03 10

Vinyl chlonde <10 10 ugIL 07/29111 20:03 10

Xylenes, Total <20 20 ugIL 07/29111 20:03 10

Surrogate % Recovery Qualifier Limits Prepared Analyzed Di! Fac

4-Bromofluorobenzene 102 70130 07/29/1120:03 10

Dibromofluoromethane 101 70 130 07/29/11 20:03 10

Toluene-d8(Surr) 101 70 130 07/29/11 20:03 10

Method: 8270C - Semivolatile Organic Compounds (GCIMS)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac

I Acenaphthene <49 49 ugIL 07/28/11 14:42 08/03111 13:50 5

Acenaphthylene <49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

Acalophenone <49 49 ug/L 07/28/11 1442 08/03/11 13:50 5

2-Acetylaminofluorene <49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

alphaalpha-Dimethyl phenethylamine <9800 9800 ug/L 07/28/11 1442 08/03/11 13:50 5

4-Aminobiphenyl <49 49 ug/L 07/28/11 1442 08/03/11 13:50 5

Aniline <98 98 ugIL 07/28/11 1442 08/03/11 13.50 5

<49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 1442 08/03/11 13:50 5

<49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

<49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 1442 08/03/11 13:50 5

<49 49 ugIL 07/28/11 14:42 08/03/11 1350 5

<49 49 ug/L 07/28/11 14:42 08/03/11 1350 5

<49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 1442 08/03/11 13:50 5

<49 49 ug/L 07/28/11 14.42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 1442 08/03/11 13.50 5

<49 49 ug/L 07/28/11 1442 08/03/11 1350 5

<49 49 ug/L 07/28/11 1442 08/03/1113.50 5

<49 49 ug/L 07/28/11 14.42 08/03/11 1350 5

<49 49 ug/L 07/28/11 1442 08/03/11 1350 5

<98 98 ug/L 07/28/11 1442 08/03/11 1350 5

<49 49 ug/L 07/28/11 1442 08/03/11 1350 5

<49 49 ug/L 07/28/11 1442 08/03/11 1350 5

<49 49 ug/L 07/28/11 1442 08/03/11 1350 5

<49 49 ug/L 07/28/11 1442 08/03/11 13:50 5

Chrysene <49 49 ug/L 07/28/11 14.42 08/03/11 1350 5

Diallate <49 49 ug/L 07/28/11 14:42 08/03/11 1350 5

Dibenz(a,h)anlhracene <49 49 ug/L 07/28/11 1442 08/03/11 1350 5

Dibenzofuran <49 49 ug/L 07/28/11 14:42 08/03/11 13.50 5

12-Dichlorobenzene <49 49 ug/L 07/28/11 1442 08/03/11 1350 5


1,4-Dichlorobenzene <49 49 ugIL 07/28)11 1442 08/03/11 13.50 5

33’-Dichlorobenzidine <290 290 ug/L 07/28/11 1442 08/03/11 1350 5

2.4-Dichlorophenol <49 49 ug)L 07/28/11 1442 08/03/11 1350 5

26-Dichlorophenol <49 49 ug/L 07/28/111442 08)03/11 1350 5


Anthracene

Aramite, Total

Benzo[ajanthracene

Benzo[a]pyrene

Benzo[b]fluoranthene

Benzo[g,h,i]perylene

Benzo[k]fluoranthene

Benzyl alcohol

1,1’-Biphenyl

Bis(2-chloroethoxy)melhane

Bis(2-chloroethyl)elher

bis(chloroisopropyl) elher

Bis(2-ethylhexyl) phthalate

4-Bromophenyl phenyl ether

Bulyl benzyl pnthatate

4-Chtoroaniline

4-Chloro-3-methylphenol

2-Chloronaphthalene

2-Chlorophenol

4-Chlorophenyl phenyl elher

0

of 92


(j)roiectISite: Hercules Hattiesburg APIX 7/26/11





Diethyl phthalate <49 49 ug/L 07/28111 1442 08103/11 13:50 5

Dimethoate <49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

712-Dimethylbenz(a)anthracene <49 49 ug/L 07128/il 14:42 08/03(11 13:50 5

33-Dimethylbenzidine <98 98 ug/L 07/28/11 14:42 08/03/11 13:50 5

2,4-Dimethylphenol <49 49 ugIL 07/28/11 1442 08/03/11 13:50 5

Dimethyl phthalate <49 49 ugIL 07/28/11 1442 08/03/11 13:50 5

Di-n-butyl phthalate <49 49 ugIL 07/28/11 1442 08/03/11 13:50 5

1,3-Dinitrobenzerie <49 49 ugIL 07/28)11 14:42 08/03/11 13:50 5

4,6-Dinhtro-2-methylphenol <250 250 ugIL 07/28/11 14:42 08/03/11 13:50 5

2,4-Dinitrophenol <250 250 ug/L 07/28111 14:42 08)03/11 13:50 5

2,4-Dinitrotoluene <49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

2,6-DInitrotoluene <49 49 ug/L 07/28/11 1442 08/03/11 13:50 5

Di-n-octyl phthalate <49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

Dinoseb <49 49 LJgIL 07/28/11 14:42 08/03/11 13:50 5

1,4-Dioxane 470 49 Ugh.. 07/28111 14.42 08/03)11 13:50 5

Disulfoton <49 * 49 ug/L 07)28/11 14:42 08/03/11 13:50 5

Ethyl methanesulfonate <49 49 ughL 07)28/11 14:42 08103/11 13:50 5

Ethyl Parathion <49 49 ug/L 07/28/11 14:42 08/03/11 1350 5

Famphur <49 * 49 ug/L 07/28/11 14:42 08/03)11 13:50 5

O Fluoranthene <49 49 ug)L 07/28/11 14:42 08/03/11 13:50 5

Fluorene <49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

Hexachlorobenzene <49 49 ug!L 07/28/11 14:42 08/03/11 13:50 5

Hexachlorobutadiene <49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

Hexachtorocydopentadiene <49 49 ughL 07/28/11 14:42 08/03/11 13:50 5

Hexachloroethane <49 49 ug/L 07/28/11 14:42 08/03/11 1350 5

Hexachlorophene <25000 25000 ug/L 07/28/11 14:42 08/03/11 13:50 5

Hexachloropropene <49 49 ugIL 07/28/11 1442 08/03/11 13.50 5

Indeno[1,23-cd}pyrene <49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

Isophorone <49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

Isosafrole <49 49 ug/L 07/28/11 1442 08/03/11 13:50 5

Methapyrilene <9800 9800 ugIL 07/28/11 14:42 08/03/11 13.50 5

3-Melhylcholanthrene <49 49 ug/L 07/28/11 14:42 06/03/11 13:50 5

Methyl methanesutfonate <49 49 ugIL 07/28(11 1442 08/03(11 1350 5

2-Methylnaphthalene <49 49 ugIL 07/28/11 14.42 08103/11 13.50 5

Methyl parathion <49 * 49 ugIL 07/28/11 14:42 08/03/11 13.50 5

2-Methylphenol <49 49 ugIL 07/28/11 1442 08/03/11 1350 5

3 & 4 Methylphenol <49 49 ug/L 07/28/11 14.42 08/03/11 1350 5

Naphthalene <49 49 ug/L 07/28/11 1442 08/03/11 13:50 5

1,4-Naphthoquinone <49 49 ug/L 07/28/11 1442 08/03/11 13.50 5

1-Naphlhylamine <49 49 ug/L 07/28/11 14:42 08/03)11 13:50 5

2-Naphthylamine <49 49 ug/L 07/28/11 1442 08/03/11 13.50 5

2-Nitroaniline <250 250 ug/L 07/28(11 14:42 08/03(11 13.50 5

3-Nitroaniline <250 250 ug/L 07/28/11 14.42 08/03/11 13.50 5

4-Nitroaniline <250 250 ug/L 07/28/11 1442 08/03/11 13:50 5

Nitrobenzene <49 49 ugk 07/28/11 1442 08/03/11 13.50 5

2-Nitrophenol <49 49 ugIL 07/28111 1442 08/03/11 13:50 5

4-Nitropheno -250 250 ug)L 07/28/11 1442 08/03/11 13:50 5

O 4-Nitroquinoline-1-oxide <98 98 ugbL 07/28/11 1442 08/03)11 13.50 5

N-Nitro-o-toluidine <49 49 UgIL 07/28/11 14:42 08/03/11 13 50 5

N-Nitrosodiethylamine <49 49 ug/L 07/28/11 14:42 08/03/11 1350 5


of 92






Method: 827CC - Semivolatile Organic Compounds (GCIMS) (Continued)

Analyte Result Qualifier - RL MDL Unit 0 Prepared Analyzed Dii Fac

N-Nitrosodimethylamine <49 49 ugIL 07/28/11 14:42 0810311113:50 5

N.Nitrosodi-n-butylamine <49 49 ugiL 07/28/1114:42 08/03/1113:50 5

N-Nitrosodi-n-propylamine <49 49 ug/L 07/28111 14:42 08/03/11 13:50 5

N-Nitrosodiphenylamine <49 49 ugiL 07/28/11 14:42 08/03/11 13:50 5

N-Nitrosomethylethylamine <49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

N-Nitrosomorphoiine <49 49 ugIL 07/28/1114:42 08/03/1113:50 5

N-Nitrosopiperidine <49 49 uglL 07/28/11 14:42 08/03/11 13:50 5

N-Nitrosopyrrolidine <49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

o,o’,o”-Triethylphosphorothioate 190 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

p-Dimethylaminoazobenzene <49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

Pentachlorobenzene <49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

Pentachloronitrobenzene <49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

Pentachlorophenol <250 250 ugIL 07/28/11 14:42 08/03/11 13:50 5

Phenacetin <49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

Phenanthrene <49 49 ug)L 07/28/11 14:42 08/03/11 13:50 5

Phenol <49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

<9800 9800 ug/L 07/28/11 14:42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 14.42 08/03/11 13:50 5

<49 49 ugIL 07/28)11 14:42 08103/11 13:50 5

<250 250 ug/L 07/28/11 14:42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

<49 49 ugIL 07/28/11 14:42 08/03/11 13:50 5

<49 49 ug/L 07)28/11 14:42 08/03/11 1350 5

<49 49 ug/L 07/2811114.42 08/03/11 13:50 5

<49 49 ug/L 07/28/11 14:42 08/03/11 13:50 5

<49 49 uglL 07/28/11 14:42 08/03/11 13:50 5

<49 49 ugIL 07/28/11 14:42 08/03/11 1350 5

<49 49 ug/L 07)28/11 14:42 08)03/11 1350 5

Surrogate Prepared Dii Fec

2-Fluorobiphenyl 07/28/1114.42 5

2-Fluorophenol 07/28/1114:42 5

Nitrobenzene-d5 07/28/1114.42 5

Phenof-d5 07/28/1114:42 5

Terphenyl-d14 07/28/1113:42 5

2,4,6- Tnbromophenol 5


:

0

Phorate

2-Picoline

p-Phenylene diamine

Pronamide

Pyiene

Pyridine

Safrole, Total

Sulfotepp



Thionazin

2-Toluidine


2,4,5-Thchlorophenol

2,4, 6-Thchlorophenol

1 ,3,5-Thnitroberizene

% Recovery Qualifier -. Limits

61 38130

40 25130

50 39130

51 25-130

65 10143

85 31-141

Analyzed

08/03/Il 13:50

08/03/11 1350

08/03/11 1350

08/03/1113 50

08/03/11 1350

07/28/1114:42 08/03/111350

Method: 8081 A_8082 - Organochlorine Pesticides & PCBs (GC)Analyte Result Qualifier RL

AIdrin <0051 0051

alpha-BHC 0.25 0051

beta-BHC <0 051 0051

Chiordane (technical) <051 0.51

Chlorobenzilate 0.51 0 51

4,4’-DDD <0.10 0 10

4.4-DDE 0 10 0 10

MDL Unit 0 Prepared

ug/L 07/28/11 14:42

ug/L 07/28/11 1442

ugIL 07/28/1114.42

ugfL 07/28/11 14:42

ug/L 07/28/11 1442

ug/L 07/28/11 1442

ug/L 07/28)11 1442

- Analyzed

08/01/11 2117

08/01/11 21.17

06/01111 21 17

08/01/11 2117

08/01/11 2117

08/01/11 21.17

08/01111 2117

Dii Fac

of 92

Client: Ashland Inc.

oject/Site: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-MWI3-072611Date Collected: 07/2&Ill 09:20




Method: 8290 - DioxinslFurans, HRGCIHRMS (8290)

Analyte

23,7,8-TCDD

Total HxCDD

Total HXCDF

Total PeCDD

Total PeCDF

QTotal TCDD

Total TCDF

Prepared

07/2 8/11 0804

07/28(1 / 08 04


Method: 8081A_8082 - Organochiorine Pesticides & PCBs (GC) (Continued)Analyte Result Qualifier RL MDL

4,4-DDT <0.10 0.10

delta-BHC <0.051 0.051

Dieldrin <0.10 0.10

Endosulfan I <0.051 0.051

Endosulfan II <0.10 0.10

Endosulfan sulfate <0.10 0.10

Endnn <0.10 0.10

Endiin aldehyde <0.10 0.10

Endnn ketone <0.10 0.10

gamma-BHC (Lindane) <0.051 0.051

Heptachlor <0.051 0.051

Heptachlor epoxide <0.051 0.051

Isodrin <0.051 0.051

Kepone <1 0 1.0

Methoxychlor <0.10 0.10

Toxaphene <5.1 5.1

PCB-1016 <1.0 1.0

PCB-1221 <2.0 20

PCB-1232 <1.0 1 0

OPCB-1242 <1.0 1.0

PCB-1248 <1.0 1.0

PCB-1254 <1.0 1 0

PCB-1260 <1.0 1.0

unitug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ugiL

ugIL

ug/L

ug/L

ug/L

ugIL

ug/L

ug/L

ugIL

ugIL

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

D Prepared

07/28/11 14:42

07/28/11 1442

07(28(11 14:42

07/28/11 14:42

07/28/11 14:42

07/28(11 14:42

07/28/11 14.42

07(28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14.42

07/28(11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 1442

Prepared

7/28/lI 14.42

07/28/11 14:42

07/28J11 14:42

07/28/11 1442

Prepared

07/28(11 08:04

07/28/11 0804

07/28/11 08 04

Analyzed

08/01/11 21:17

08/01/11 21:17

08/01/11 21:17

08/01/11 21:17

08/01/11 21:17

08/01/11 21.17

08)01/11 21:17

08101/11 21:17

08/01/11 21:17

08)01/11 21:17

08/01111 21:17

08/01)11 21:17

08/01/11 21:17

08/01/11 21:17

08/01/11 21:17

08/01/11 21:17

08/01/11 21.17

08/01/11 21:17

08/01111 21:17

08/01)11 21:17

08/01/11 21:17

08/01/11 21:17

08/01/11 21:17

Analyzed

08/01/112117

08/01/1121:17

08/01/112117

08/01/11 21:17

Analyzed

07/29/11 19.24

07/29)11 19:24

07/29/11 19:24

Dil Fac

1

DII Fac

Dii Fac

% Recovery

37

302

19

8

Qualifier

p

xxpX

Surrogate

Tefrachloro-m-xylene


DCB Decach/orobiphenyl

DCB Decachiorob;phenyl

Method: 8151A - Herbicides (GC)Analyte

2,4-D

Silvex (2,4,5-TP)

2,45-T

Surrogate

DCAA

DCAA

Limits

36- 130

36- 130

40- 130

40- 130

RL

0.50

0.50

0.50

Result Qualifier

<0.50

<0 50

<0.50


80

87

MDL Unit 0

ug/L

ug/L

ug/L

Analyzed DII Fac

07/29/11 19.24 1

07/29/11 1924 1

Result Qualifier ML

ND 10

ND 50

ND 50

ND 50

ND 50

ND

17

Limits

52- 151

52 151

EDL TEF TEQ

023 1

042

0.36

0.69

2.6

10 0.23

10 33

0.00Total TEQ (EPA 1989)

Unit D Prepared

pg/L 07/28/11 09 00

pgIL 07/28/11 09 00

pg/L 07/28/11 0900

pg)L 07/28/11 0900

pg)L 07/28/11 09:00

pg/L 07/28/11 09:00

pg/L 07/28/11 09:00

Analyzed

07/30/11 12.53

07/30)11 12.53

07/30/11 1253

07/30/11 1253

07/30/11 1253

07/30/11 1253

07/30/11 1253

Dii Fac

of 92

Internal Standard % Recovery Qualifier - Limits Prepared Analyzed Oil Fac

13C-2,3,7,8-TCDD 79 40 135 07/28.111 09:00 07/30/11 12:53 1

13C-12,3,7,8-PeCDD 76 40- 135 07128/11 09.00 07/30/11 12:53 1

13C-1,2,3,6,7,8-HxCDD 86 40- 135 07/28/11 09:00 07/30/11 12:53 1

13C-2,3,7,8-TCDF 85 40- 135 07128/11 09:00 07/30./Il 1253 1

13C-1,2,3,7,8-PeCDF 78 40 135 07/28/11 09.00 07/30/11 12:53 1

13C-1,2,3,4,7,8-HxCDF 80 40 135 07/28/11 09:00 07/30/11 12:53 1

Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

<5.0 5.0 ug/L 08I01/ll 08:48 08106/11 23:05 1

5.7 2.5 ugh.. 08/01/11 08:48 08/06/11 23:05 1

49 5.0 ugIL 08/01/11 08:48 08/06/11 23:05 1

<0.50 0.50 ugIL 08/01/11 08:48 08106/11 23.05 1

<050 0.50 ug/L 08/01/11 08:48 08106/11 23:05 1

<5.0 5.0 ugIL 08/01/11 0848 08/06/11 23:05 1

15 0.50 ugIL 08/01/11 08:48 08/06111 2305 1

<50 5.0 ugIL 08/01/11 08:48 08/06/11 2305 1

<1.5 1.5 ug/L 08/01/11 08:48 08/06/11 23:05 1

<5.0 5.0 ugIL 08/01/11 08:48 OB/06/11 2305 1

<25 2.5 uglL 08/01/11 08:48 08/06/11 2305 1

<1 0 1.0 ug/L 08/01/11 08:48 08/06/11 23.05 1

<1 0 1.0 ugIL 08/01/11 08:48 08106/11 23:05 1

<50 50 ug/L 08/01/11 0848 08/06/11 23.05 1

<10 10 ug/L 08/01/11 0848 08/06/11 23:05 1

41 20 ugIL 08/01/11 08:48 08/06/11 2305 1

Result Qualifier RL MDL Unit - D Prepared Analyzed DII Fac

<020 0.20 ug/L 08/02/11 0942 08/02/11 1654 1

General ChemistryAnalyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil FacCyanide, Total <0.010 0010 mg/L 08/01/11 0751 08/02/11 0650 1


Client Sample ID: ASH-MWI3-072611Date Collected: 07/26111 09:20Date Received: 07/27/11 09:20


-

- Lab Sample ID: 680-70758-4 CDMatrix: Water

Method: 6020 - Metals (ICPIMS)Analyte

Antimony

Arsenic

BariumBeryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Nickel

Selenium

Silver

Thallium

Tin

Vanadium

Zinc


Mercury

Analyte Result Qualifier

Sulfide <1 .0

0

0

RL RL Unit B Prepared Analyzed Dii Fac

1 0 mg/L 07/27/11 1410 1


of 92

Client Sample ResultsClient: Ashland Inc. TestAmerica Job ID: 680-70758-1 1

CNjroiectlSite:Hercules Hattiesburg APIX 7/26/1 1 i:.




..

j/17

Method: 8260B - Volatile Organic Compounds (GCIMS)Analyte Result Qualifier - RL MDL Unit - 0 Prepared Analyzed Oil Fac

Acetone <5000 5000 ug/L 07/30/11 20:34 200

Acetonitrile <8000 8000 ugiL 07/30/11 20 34 200 I

Acrolein <4000 4000 ug/L 07/30/11 20:34 200


Benzene 3600 200 ug/L 07/30/11 2034 200

Dichlorobromomethane <200 200 vgIL 07/30111 2034 200

Bromoform <200 • 200 ug/L 07/30/11 20.34 200

Bromomethane <200 200 ug/L 07/30/11 20:34 200

2-Butanone (MEK) <2000 2000 ug/L 07/30/11 20:34 200

Carbon disulfide <400 400 ug/L 07/30/1 1 20:34 200

Carbon tetrachloride 25000 200 ugiL 07/30/11 20:34 200

Chlorobenzene 770 200 ug)L 07/30/11 20:34 200

2-Chloro-1,3-butadiene <200 200 ugiL 07/30/11 20:34 200

Chloroethane <200 200 ug/L 07/30/11 20.34 200

Chloroform 3000 200 ug)L 07/30/11 20:34 200

Chloromethane <200 200 ug!L 07/30/11 20:34 200

3-Chloro-1-propene <200 200 ug/L 07/30/11 20.34 200

Chlorodibromomethane <200 * 200 ug/L 07/30/11 20:34 200

12-Dibromo-3-Chloropropane <200 200 ug/L 07/30/11 20.34 200

O Ethylene Dibromide <200 200 ug/L 07/30/11 2034 200

• Dibromomethane <200 200 ug/L 07/30/11 20:34 200

trans-i ,4-Dichloro-2-butene <400 400 ug/L 07/30/11 20:34 200


11-Dichloroethane <200 200 ug)L 07/30/11 20.34 200

12-Dichloroethane <200 200 ug/L 07/30/11 20:34 200

cis-12-Dichloroethene <200 200 ug/L 07/30/11 20:34 200

trans-12-Dichloroethene <200 200 ug/L 07/30/11 20:34 200

11-Dichloroethene <200 200 ugfL 07/30/11 20:34 200

12-Dichtoropropane <200 200 ug/L 07/30/il 20:34 200

ds-13-Dchloropropane <200 200 ugfL 07/30/11 2034 200

trans-13-Dichloropropene <200 200 ug/L 07/30/11 20.34 200

Ethylbenzene <200 200 ug/L 07/30/11 20.34 200

Ethyl methacrylate <200 200 ug/L 07/30/11 20:34 200

2-Hexanone <2000 2000 ugfL 07/30/11 2034 200

lodomethane <1000 1000 ug/L 07/30/11 2034 200

Isobulyl alcohol <8000 8000 ug/L 07/30/il 20 34 200

Methacrylondrile <4000 4000 ug/L 07/30/11 20:34 200

Methytene Chloride <1000 1000 ug)L (17/30)11 20:34 200

Methyl metliacrytate <200 200 ug/L 07/30/11 20:34 200

4-Methyl-2-pentanone (MIBK) <2000 2000 ug/L 07/30/11 20 34 200

Pentachloroethane <1000 1000 ug/L 07/30)11 20:34 200

Propionitrile <4000 4000 ug/L 07/30/11 20:34 200

Styrene <200 200 ug/L 07/30/11 20.34 200

1l12-Tetrachloroetharre <200 200 ug/L 07/30)11 2034 200

11,2 2-Tetrachloroethane <200 200 ug/L 07/30/11 2034 200

Tetrachloroethene <200 200 ug/L 07/30/11 20.34 200

Toluene <200 200 ug/L 07/30)11 2034 200

( lii-Trichloroelhane <200 200 ug/L 07/30/11 2034 200

12-Trichloroethane <200 200 ug/L 07)30/11 20.34 200

Trichloroethene <200 200 ug/L 07)30/11 2034 200


of 92




Client Sample ID: ASH-MWI7-072611Date Collected: 07126/11 11:45



Lab Sample ID: 680-70758-5 6)Matrix: Water

Method: 8270C - Semivolatile Organic Compounds (GCIMS)Analyte Result Qualifier RL MDL Unit 0 prepared

Acenaphthene <1000 1000 ugiL 07/28/11 14:42

Acenaphthylene <1000 1000 ugfL 07/28/11 14:42

Acetophenone <1000 1000 ug/L 07/28111 14.42

2-Acetylaminofluorene <1000 1000 ugIL 07/28/11 14:42

alpha,alpha-Dimelhyl phenethylamine <200000 200000 ug/L 07)28/11 14:42

4-Aminobiphenyl <1000 1000 ug/L 07/28/11 14:42

Aniline <2000 2000 ug/L 07/28/11 14:42

Anthracene <1000 1000 ug/L 07/28/11 14:42

Aramite, Total <1000 1000 ugIL 07/28)11 14:42

Benzo[a]anthracene <1000 1000 ug/L 07/28/1114:42

Benzo[a]pyrene <1000 1000 ug/L 07/28/11 14:42

Benzo[b]fluoranthene <1000 1000 ug/L 07/28/11 14:42

Benzog,h,i]perylene <1000 1000 ug/L 07/28/11 14:42

Benzo[k]fluoranthene <1000 1000 ug/L 07/28/11 14.42

Benzyl alcohol <1000 1000 ug/L 07)28/11 14.42

11-Biphenyl <1000 1000 ug)L 07/28/11 1442

Bis(2-chloroethoxy)methane <1000 1000 ug/L 07/28/11 14 42

Bis(2-chloroethyl)ether <1000 1000 ug/L 07/28/11 14.42

bis(chloroisopropyl) ether <1000 1000 ug/L 07/28/11 14.42

Bis(2-ethylhexyl) phthalate <1000 1000 ug/L 07/28/11 1442

4-Bromophenyt phenyl ether <1000 1000 ug/L 07/28/11 1442

Sutyl benzyl phthalale <1000 1000 ug/L 07/28/11 1442

4-Chloroantline <2000 2000 ug/L 07/28/11 14.42

4-Chloro-3-methylphenol <1000 1000 ug/L 07/28/11 1442

2-Chloronaphthalene <1000 1000 ug/L 07/28/11 14.42

2-Chlorophenol <1000 1000 ug/L 07/28/11 1442

4-Chlorophetyl phenyl ether <1000 1000 ug/L 07/28/11 1442

Chrysene <1000 1000 uq/L 07)28/11 1442

Diallate <1000 1000 ug)L 07/28/11 14 42

Dibenz(ah)anthracene <1000 1000 ug/L 07/28/11 1442

Dibenzofuran <1000 1000 ug/L 07/28/11 1442

1,2-Dichlorobenzene <1000 1000 ug/L 07/28/11 14.42

1,3-Dichlorobenzene <1000 1000 ug/L 07/28/11 1442

1,4-Dichlorobenzere <1000 1000 ug/L 07/28/11 14.42

3,3’-Dichlorobenz:drne <6000 6000 ug/L 07/28/11 1442

2,4-Dichlorophenol <1000 1000 ug/L 07/28/1114 42

2,6-Dichlorophenol <1000 1000 ug/L 07/28/11 1442

Method: 8260B - Volatile Organic Compounds (GCIMS) (Continued)Anatyte -- -— — Result Qualifier RL MDL Unit D Prepared

Trichlorofluoromethane <200 200 ug/L

1,2,3-Tiichloropropane <200 200 ug/L

Vinyl acetate <400 400 ug/L

Vinyl chloride <200 200 ug/L

Xylenes, Total <400 400 ugIL

Surrogate

4-flromofluorobenzene

IDibromofluoromethane

Toluene-d8 (Surr)


106 — 70130

96 70130

106 70130

Analyzed

07/30/11 20:34

07/30/11 20.34

07/30/11 20:34

07)30/11 20:34

07/30/11 20:34

DII Fac

200

200

200

200

200

Prepared Analyzed Dil Fac

07/30/11 20.34 200

07/30/11 20:34 200

07/30/11 20:34 200

0

Analyzed —— Dii Fac

08103/11 16:12 100

08/03/11 16:12 100

08/03)11 16.12 100

08/03/11 16:12 100

08/03/11 16:12 100

08)03/11 16:12 100

08)03/11 16:12 100

08/03/11 1612 100

08/03/11 1612 100

08/03/11 1612 100

08/03/11 16:12 100

08/03/11 1612 100

08/03/11 16:12 100

08/03/11 16:12 100

08/03/11 16:12 100

08/03/11 1612 100

08/03/11 16 12 100

08/03/11 1612 100

08/03/11 16.12 100

08/03/11 1612 100

08/03/11 1612 100

08/03/il 1612 100

08/03/11 1612 100

08/03/11 1612 100

08/03/11 16 12 100

08/03/11 1612 100

08)03/11 16.12 100

08/03/11 16.12 100

08/03/11 6.12 100

08/03/11 16:12 100

08/03/11 1612 100

08/03/11 1612 100

08/03/11 1612 100

08/03/11 1612 100

08/03/il 1612 100

08/03/11 1612 100

08/03/11 1612 100


of 92

Client Sample ResultsClient; Ashland Inc. TestAmerica Job ID: 680-70758-1

c5.o1t/S1teHercules Hattiesburg APIX 7/26/11 —

—





Diethyl phthalale <1000 1000 ug/L 07/28111 14:42 08/03/11 16:12 100

Dimethoale <1000 * 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

712-Dimethytbenz(a)anthracene <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

3,3-Dimethylbenzidine <2000 2000 ugIL 07/28/11 1442 08/03/11 16:12 100

24-Dimelhyiphenol <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

Dimethyl phthalate <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

Di-n-butyl phthalate <1000 1000 ug)L 07/28/11 14:42 08/03/11 16:12 100

13-Dinitrobenzene <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

4,6-Dinitro-2-methylphenol <5000 5000 ug/L 07/28/11 14:42 08/03/11 16:12 100

2,4-Dinitrophenol <5000 5000 ug/L 07/28/11 14:42 08/03/11 16:12 100

2,4-Dinitrotoluene <1000 1000 ug/L 07)28/11 14:42 08/03/11 16:12 100

2,6-Dinitrotoluene <1000 1000 ug/L 07/28/11 14:42 08/03)11 16:12 100

Di-n-octyl phthalate <1000 1000 ug)L 07/28/11 14:42 08/03/11 16:12 100

Dinoseb <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

14-Dioxane <1000 1000 ug/L 07/28/11 14:42 08/03/11 16.12 100

Disulfoton <1000 • 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

Ethyl methanesulforiate <1000 1000 ug/L 07/28/11 14.42 08/03/1116:12 100

Ethyl Parathion <1000 1000 ugIL 07)28/111442 08/03/1116:12 100

Famphiir <1000 1000 ug/L 07/28/11 14.42 08/03/11 16:12 100

OFluoranthene <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

Fluorene <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

Hexachtorobenzene <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

Hexachlorobutadiene <1000 1000 ugIL 07)28/11 14:42 08/03/1116:12 100

Hexachlorocyclopentadiene <1000 1000 ugfL 07/28/11 14:42 08/03/1116:12 100

Hexachloroethane <1000 1000 ug/L 07)28/11 14:42 08/03/11 16:12 100

Hexachlorophene <500000 500000 ug/L 07)28/11 1442 08103/11 16:12 100

Hexachloropropene <1000 1000 ug/L 07)28/11 1442 08/03/11 16:12 100

lndeno[1,2,3-cd]pyrene <1000 1000 ug/L 07)28/11 14.42 08/03/11 16.12 100

Isophorone <1000 1000 ug/L 07/28/11 1442 08/03/11 16.12 100

Isosafrole <1000 1000 ug/L 07/28/11 1442 08/03/11 16 12 100

Melhapyrilene <200000 200000 ug/L 07/28/1114.42 08/03)11 16:12 100

3-Melhylcholanlhrene <1000 1000 ug/L 07/28/11 1442 08/03/11 16:12 100

Melhyl melhanesulfonate <1000 1000 ug/L 07/28/11 14:42 08/03)11 16:12 100

2-Melhylnaphthalene <1000 1000 ug/L 07/28/11 14:42 08/03/11 16.12 100

Methyl parathion <1000 * 1000 ug/L 07)28/11 14:42 08/03)1116:12 100

2-Methylphenol <1000 1000 ug/L 07/28)11 14.42 08)03)11 1612 100

3 & 4 Methytpheriol <1000 1000 ug/L 07/28/11 1442 08/03/11 16:12 100

Naphlhalene <1000 1000 ug/L 07)28/11 1442 08/03/11 16 12 100

14-Naphthoquinone <1000 1000 ug/L 07/28/11 1442 08/03/11 1612 100

1-Naphthylamine <1000 1000 ug/L 07/28/111442 08/03/11 16 12 100

2-Naphthylamine <1000 1000 ug/L 07/28/11 14:42 08/03/11 16 12 100

2-Nitroan:Iine (5000 5000 ug/L 07/28/11 14.42 08/03/11 16:12 100

3-Nitroaniline <5000 5000 ug/L 07/28/11 14.42 08/03/11 1612 100

4-Nitroanilifle <5000 5000 ug/L 07/28/11 1442 08/03/11 16.12 100

Nitrobenzene <1000 1000 ug/L 07)28/1114.42 08/03/11 1612 100

2-Nitrophenol <1000 1000 ug/L 07)28/111442 08/03/11 16.12 100

4-Nitrophenol <5000 5000 ug/L 07)28/11 1442 08/03/11 1612 100

4-Nitroquinohne-1-oxide <2000 2000 ug/L 07/28/11 14:42 08/03/11 1612 100

N-Nilro-o-toluidine <1000 1000 ugIL 07/28/111442 08/03)11 ‘6 12 100

N-Nitrosodiethylamine <1000 1000 ug/L 07/28/111442 08)03)11 16 12 100


of 92

Client Sample ResultsClient: Ashland Inc.Project/Site: Hercules Hattiesburg APIX 7/26/11



Client Sample ID: ASH-MWI7-072611 Lab Sample ID: 680-70758-5Date Collected: 07126111 11:45 Matrix: Water

Date Received: 07/27111 09:20.‘

..

-..-- .--.

‘ Method 8270C Semivolatile Organic Compounds (GCIMS) (Continued) IAnalyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

NNilrosodimethylamine — — — <1000 1000 — ug/L 07/28/111442 08/03/111612 100

N-Nitrosodi-n-butylamine <1000 1000 uglL 07/28/11 14.42 08/03/11 16.12 100

N Nitrosodi ri propylamine <1000 1000 ug/L 07/28/11 1442 08/03/11 16 12 100

N-Nitrosodiphenylamine <1000 1000 ugIL 07/28/li 14:42 08/03/11 16.12 100 <>s

N-Nitrosomethyleihylamine <1000 1000 ugIL 07/28/11 14.42 08/03/11 16:12 100

N-Nitrosomorpholine <1000 1000 ug/L 07/28/11 1442 08/03/11 1612 100

N-Nitrosopipendine <1000 1000 ugIL 07/28/11 14:42 08/03/11 1612 100

N-Nitroscipyrrohdine <1000 1000 ug/L 07/28/11 14.42 08/03/11 16:12 100

o,o’,o”-Triethyiphosphorothioate 12000 1000 ug/L 07/28/11 14.42 08/03/11 1612 100

p-Dimethylamino azobenzene <1000 1000 ug/L 07/28/11 1442 08/03/11 16 12 100

: Pentachlorobenzene <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

Pentachloronitrobenzene <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

Pentachlorophenol <5000 5000 ug/L 07/28/11 1442 08/03/11 16:12 100

Phenacelin <1000 1000 ug/L 07/28/11 14:42 08/03/11 1612 100

Phenanthrene <1000 1000 ug/L 07/28/11 1442 08/03/11 1612 100

Phenol <1000 1000 ugIL 07/28/11 1442 08/03/11 1612 100

: Phorate <1000 1000 ugIL 07/28/11 1442 08/03/11 16.12 100

2-Picoline <1000 1000 ugIL 07/28/11 14.42 08/03/11 1612 100

p-Phenylene diamine <200000 200000 ug/L 07/28/11 1442 08/03/11 1612 100

Pronarnide <1000 1000 ug/L 07/28/11 14:42 08/03/11 1612 100

Pyrene <1000 1000 ug/L 07/28/11 14:42 08/03/11 16:12 100

: Pyridine <5000 5000 ug/L 07/28/11 14:42 08/03/11 1612 100

Safrole, Total <1000 1000 ug/L 07/28/11 14:42 08/03/11 1612 100

Sulfotepp <1000 1000 ug/L 07/28/11 1442 08/03/11 1612 100

1,24,5-Tetrachlorobenzene <1000 1000 ug/L 07/28/11 14:42 08/03/11 1612 100

23,4,6-Tetrachlorophenol <1000 1000 ug/L 07/28/11 14:42 08/03/11 16 12 100

Thionazin <1000 1000 ug/L 07/28/11 1442 08/03/11 16.12 100

2-Toluidine <1000 1000 ug/L 07/28/11 14.42 08/03/11 16 12 100

124-Trichlorobenzene <1000 1000 ug/L 07/28/11 1442 08/03/11 1612 100

2,45-Trichlorophenol <1000 1000 ug/L 07/28/11 1442 08/03/11 1612 100

246-Trichlorophenol <1000 1000 ug/L 07/28/11 14.42 08/03/il 16 12 100

1 35-Trinilroberizene <1000 1000 ug/L 07/28/11 14:42 08/03/11 16 12 100

Surrogate % Recove,y Qualifier Limits Prepared Analyzed Dii Fac

2-Fluorobiphenyl 0 D 38 130 07/28/Il 1442 08/03/11 76 12 100

2-Fluorophenol 0 D 25 130 07/28/11 1442 08/03/11 1612 100

Nifrobenzene-d5 0 0 39. 130 07/28/11 1442 08/03/11 1612 100

Pheno/-cj5 0 D 25 130 07/28/Il 1442 08/03/11 1612 100

Terpheny/-d14 0 D 10 143 07/28/11 14.42 08/03/11 16 12 100

2,46-Tribromophenol 0 0 31 141 07/28/Il 1442 08/03/111612 100

Method: 8081 A_8082 - Organochlorine Pesticides & PCBs {GC)Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed 06 Fac

AIdrin <049 0.49 ug/L 07/28/11 1442 08/08/11 1227 10

aipha-BHc 1.5 p 0.49 Lig/L 07/28/li 14:42 08/08/11 1227 10

beta-BHC <049 049 ug/L 07/28/11 1442 08/08/11 1227 10

Chlordane (technical) <4 9 49 ug/L 07/28/11 14:42 08/08/11 1227 10

Chlorobenzilate <4 9 4 9 ug/L 07/28/11 1442 08/08/11 1227 10

44-DDD <0 99 0 99 ug/L 07/28/11 1442 08/08/11 1227

44-DDE <0 99 0 99 ug/L 07/28,11 1442 08/08/11 12 27 10\)

of 92



Client Sample ID: ASH-MWI7-072611

Date Collected: 07/26/lI 11:45




Analyte - Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

4,4’-DDT <0.99 0.99 ug!L 07128/11 14:42 08/08/11 12:27 10

delta-BHC <0.49 049 ug)L 07/28/11 14:42 08/08/11 12:27 10

Dieldiin <0.99 0.99 ug/L 07/28/11 14:42 08/08/11 12:27 10

Endosiiltan I <049 0.49 ugIL 07/28/11 14:42 08/08/11 12:27 10

Endosulfan II <0.99 099 uglL 07/28111 14:42 08/08/11 12:27 10

Endosulfan sulfate <0.99 0.99 ug/L 07/28/11 14:42 08/08/11 1227 10

<0.99 0.99 ug)L 07/28/11 14:42 08/08/11 12:27 10

<0.99 0.99 ug/L 07/28/11 14:42 oaloaiii 12:27 10

<0.99 0.99 ug/L 07/28/11 14-42 08/08/11 12:27 10

<0.49 0.49 ut/L 07/28/11 14:42 08/08/11 12:27 10

<0.49 0.49 ug/L 07/28/11 14:42 08/08/11 12:27 10

<0.49 0.49 ug/L 07/28/11 14:42 08/08/11 12:27 10

<0.49 0.49 ugIL 07/28/11 14:42 08/08/11 12:27 10

<9.9 9.9 ug/L 07/28/11 14:42 08/08/11 1227 10

<0.99 0.99 ug/L 07/28/11 14:42 08/08/11 12:27 10

<49 49 ug/L 07/28111 14:42 08/08/11 12:27 10

<9.9 9.9 ug/L 07/28/11 14:42 08/08/11 12:27 10

<20 20 ug/L 07/28)11 14:42 08/08/11 12:27 10

<9.9 9.9 ug/L 07/28/11 14:42 08)08/11 12:27 10

<9.9 9.9 ug/L 07/28/11 14:42 08/08/11 12:27 10

<9.9 9.9 ug/L 07/28/11 14:42 08)08/11 12:27 10

<9.9 9.9 ug/L 07)28/11 14:42 08/08/11 12.27 10

<9.9 9.9 ug/L 07/28/11 14.42 08/08/11 12-27 10

Analyzed Dii Fac

07/29/11 19:40

07/29/11 19-40

TestAmenca Savannah


-:: -.

Lab Sample ID: 680-70758-5 Wk)Matrix: Water

- Endrin

Endrin aldehyde

Endrin ketone

gamma-BHC (Lindarie)

Heptachlor

Heptachlor epoxide

Isodrin

Kepone

Methoxychior

Toxaphene

PCB-1 016

PCB-1 221

PCB- 1232

O PCB-1242

PCB-1248

PCB-1254

PCB-1 260

Analyzed

08/08/1112:27

08/08/1112:27

08/08/11 12:27

08/08/1112:27

Di! Fac

10

10

10

10

Prepared

07/28/1114-42

07/28/1114:42

07/28/1114-42

07/28/1114-42

Prepared

07/28/11 08:04

07)28/11 08.04

07/28/11 0804

Prepared

07/28/11 0804

07/28/11 0804


Tetrachloro-m-xylene 0 0 36- 130

Telrachloro-m-xy)ene 0 D 36 - 130

DCB Decachlorobiphenyl 0 D 40 - 130

DOS Oecachlorobiphenyl 0 0 40- 130

Method: 8151A - Herbicides (GC)Analyte Result Qualifier RL MDL Unit 0

2,4-D <0.51 0.51 ugIL

S/vex (2,4,5-TP) <0.51 0.51 ug/L

2,4,5-T <0.51 0 51 ug/L


DCAA 10096 EX 52-151

DCAA 289 pX 52-151

Method: 8290 - Dioxins/Furans, HRGCIHRMS (8290)

Anatyte Result Qualifier ML EDL TEF TEQ Unit

2,3,7,8-TODD ND 10 1 2 1 pq/L

Total HxCDD ND 50 1.6 pg/L

Total HXCDF ND 50 1.6 pg/L

Total PeCDD ND 50 0.93 pg/L

Total PeCDc ND 50 5.8 pg)L

Total TCDD ND 10 1.2 pg/L

T0taITCDF 100 10 80 pylL


Analyzed Oil Fac

07/29/11 19:40 1

07/29/11 19-40 1

07/29)11 19:40 1

D Prepared Analyzed Dii Fac

07128/11 0900 07/30)11 13:38 1

07)28/11 0900 07)30/11 13.38 1

07/28/11 0900 07/30/11 13:38 1

07)28/11 09.00 07)30/11 1338 1

07/28/11 09.00 07/30/11 1338 1

07)28/11 0900 07/30/11 13.38 1

07/28/1 1 09 00 07/30/1 1 13 38 1

of 92


Mercury

Result Qualifier RL MDL Unit D Prepared Analyzed

<0.20 0.20 ug/L 08/02/11 09:42 08)02/11 1657

Dii Fac

General ChemistryAnalyte

Cyanide, Total

Analyte

Sulfide

RL MDL Unit D Prepared - Analyzed Dil Fac

0.010 mgIL 08/01/11 07.51 08/02/11 0651 1

Result Qualifier RL RL Unit — D Prepared Analyzed Dii Fac

4.2 1 0 mg/L 07127111 1410 1


78

80

88

81

75

Limits

40- 135

40-135

40l35

40-135

40-135

40 135

Prepared

07/28/11 09:00

07/28111 09:00

07/28/11 09:00

07/28/11 09:00

07/28/11 09:00

07/28/11 09:00

Client: Ashland Inc. TestAmerica Job ID: 680-70758-1

Project/Site: Hercules Hattiesburg APIX 7/26/1 1

/.

Client Sample ID: ASH-MWI7-072611 Lab Sample ID: 680-70758-5Date Collected: 07/26111 11:45 Matrix: Water


internal Standard % Recovery Qualifier Analyzed Dii Fec

13C-23,7,8-TCDD 81 07/30/11 13:38 1

13C-1,2,37,8-PeCDD 07/30/11 13:38 1

13C-1,2,3,6,7,8-HxCDD 07/30/11 13:38 1

13C-2,3, 7,8-TCDF 07/30/11 13:38 1

13C-12,3,7,8-PeCDF 07/30/11 13.38 1

13C-1,2,3,4,7,8-HxCDF 07/30/11 13:38 1

Method: 6020 - Metals (ICPIMS)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac

Antimony <5.0 5.0 ugIL 08/01/11 08:48 08/06/11 23:11 1

Arsenic 28 2.5 ugh. 08/01/11 08:48 08/06111 23:11 1

Barium 120 50 ugIL 08/01/11 08:48 08/06/11 23.11 1

Beryllium <0.50 0.50 ug/L 08/01/11 08:48 08/06/11 23:11

Cadmium <0.50 0.50 ug/L 08/01/11 08:48 08/06/11 23:11 1

Chromium <5.0 5.0 ugIL 08/01/11 08:48 08/06/11 23:11 1

Cobalt 0.69 0.50 ug/L 08/01/11 08:48 08/06/11 23:11 1

Copper <5.0 5.0 ug/L 08/01/11 08:48 08/06)11 23:11 1

Lead <1.5 1.5 ug/L 08/01/11 08:48 06/06/11 23:11 1

Nickel <5.0 5.0 ug/L 08/01/11 08:48 08/06/11 23:11 1

Selenium <25 25 ug/L 08/01/11 08:48 08/06/11 23:11 1

Silver <1.0 1.0 ug)L 08/01/11 08:48 08/06/11 23.11 1

Thallium <1.0 1 0 ug/L 08/01/11 08:48 08/06/11 23:11 1

Tin <5.0 5.0 ugIL 08/01/11 08:48 08/06/11 23.11 1

Vanadium <10 10 ug/L 08/01/11 08:48 08/06/11 23:11 1

Zinc <20 20 ugIL 08/01/11 08:48 08/06/11 23:11 1

Result Qualifier

<0010

0


of 92

Client Sample ResultsClient: Ashland inc. TestAmerica Job ID 680-70758-1

(roiectISite: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-MW3O72611 Lab Sample ID: 680-70758-6Date Collected: 07/26/1112:51 Matrix: Water


Method: 8260B - Volatile Organic Compounds (GC/MS)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Acetone - <2500 2500 ugiL — 07130/11 0735 100

Acetonitnle <4000 4000 ugIL 07130/11 0735 100

Acrolein <2000 2000 ug/L 07/30/11 0735 100

Acrylonitnle <2000 2000 ugiL 07/30/11 0735 100

Benzene 8800 100 ugIL 07/30)11 0735 100

Dichtorobromomethane <100 100 ug/L 07/30/11 0735 100

Bromoform <100 100 ugIL 07)30/11 0735 100

Bromomethane <100 100 ug!L 07/30/11 0735 100

2-Butanone (MEK) <1000 1000 ug/L 07/30/11 0735 100

Carbon disulfide 390 200 ug)L 07/30/11 073S 100

Carbon tetrachloride <100 100 uglL 07/30/11 0735 100

Chlorobenzene 140 100 ug/L 07/30/11 0735 100

2-Chloro-1,3-butadiene <100 100 ug/L 07/30/11 0735 100

Chloroethane <100 100 ug/L 07/30/11 0735 100

Chloroform 3200 100 iig/L 07/30/11 0735 100

Chloromethane <100 100 ug/L 07/30/11 0735 100

3-Chloro-1-propene <100 100 ug/L 07/30/11 0735 100

Chlorodibromomethane <100 100 ug/L 07/30/11 0735 100

i2-Dibromo-3-Chloropropane <100 100 ug/L 07/30/11 0735 100

OEthylene Dibromide <100 100 ug)L 07/30/11 0735 100

Dibromomethane <100 100 ug/L 07/30/11 0735 100

trans-i 4-Dichloro-2-butene <200 200 ug/L 07/30/11 0735 100

Dichlorodifluoromethane <100 100 ug/L 07/30/11 0735 100

1,i-Dichloroethane <100 100 ug/L 07/30/11 0735 100

12-Dichloroethane <100 100 ug/L 07/30/11 0735 100

cis-1,2-Dichloroethene <100 100 ug/L 07/30)11 0735 100

trans-12-Dichloroethene <100 100 ug/L 07/30/11 0735 100

1,1-Dichloroethene <100 100 ug/L 07/30/11 0735 100

1,2-Dichloropropane <100 100 ug/L 07/30/11 0735 100

cis-1,3-Dichlocopropene <100 100 ug/L 07/30/11 0735 100

trans-i 3-Dichloropropene <100 100 ug/L 07/30/11 0735 100

Ethylbenzene <100 100 ug/L 07/30/11 0735 100

Ethyl melhacrylale <100 100 ugIL 07/30/11 0735 100

2-Hexanone <1000 1000 ug/L 07/30/11 0735 100

lodomethane <500 500 ug/L 07/30/11 0735 100


Methacrylonilnle <2000 2000 ug/L 07/30/11 0735 100

Methylene Chloride <500 500 ug/L 07/30/li 0735 100

Methyl methacrylate <100 100 ug/L 07/30/11 0735 100

4-Methyl-2-pentanone (MIBK) 1100 1000 ug/L 07/30/11 0735 100

Pentachloroethane <500 500 ug/L 07/30/11 0735 100

Propionitrile <2000 2000 ug/L 07/30/11 0735 100

Styrene <100 100 ug/L 07/30/11 0735 100

i,1,1,2-Tetrachloroethane <100 100 ug/L 07/30/11 0735 100

1,1,2,2-Telrachloroethane <100 100 ug/ 07)30/11 0735 100

Telrachloroethene <100 100 ug/L 07/30/11 0735 100

Toluene 1300 100 ugIL 07/30/11 0735 100

O 1,1,1-Trchloroethane <100 100 ug/L 07/30/11 0735 100

1 1,2-Trichioroethane <100 100 ug/L 07/30/11 0735 100

Tnchloroethene <100 100 ug/L 07/30/11 0735 100


of92

Client Sample ResultsClient: Ashland Inc. TestAmerica Job ID: 680-70758-1 L111Project/Site: Hercules Hattiesburg APIX 7/26/11




Method: 8260B - Volatile Organic Compounds (GCIMS) (Continued)Analyte Result Qualifier - RL MDL Unit D Prepared Analyzed Oil Fac

Trichlorofluorometharie <100 100 ugIL 07/30/11 07:35 100

1,2,3-Trichloropropane <100 100 ugiL 07/30111 07.35 100

Vinyl acetate <200 200 ugIL 07/30/11 07:35 100

Vinyl chloride <100 100 ug/L 07130/11 07:35 100

Xylenes, Total <200 200 ugIL 07/30/11 07.35 100

Sunogate % Recovery Qualifier Limits Prepared Analyzed Dii Fac

4-Bromofiuorobenzene 94 70- 130 07/30/11 07.35 100

Dibromofiuommethane 109 70- 130 07/30/11 07-35 100

Toluene-d8 (Surr) 99 70- 130 07/30/11 07:35 100

Method: 8270C - Semivolatile Organic Compounds (GC/MS)Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fac

Acenaphthene <97 97 ug/L 07/28/11 14:42 08/03/11 16.39 10

Acenaphthylene <97 97 ug/L 07/28/11 14:42 08/03/11 16:39 10

Acetophenone <97 97 ugIL 07/28/11 14.42 08/03/11 16:39 10

2-Acetylaminofluorene <97 97 ugIL 07128/11 14:42 08/03/11 16:39 10

alpha,alpha-Dimethyl phenethylamine <19000 19000 ug/L 07/28/11 14:42 08)03/11 16.39 10

4-Aminobiphenyl <97 97 ugIL 07/28/11 14.42 08)03/11 16:39 10

Aniline <190 190 ugfL 07/28/11 14.42 08/03/11 16.39 10

Anthracene <97 97 ug/L 07/28/11 14:42 08/03/11 16:39 10

Aramite, Total <97 97 ug/L 07/28/11 14:42 08/03/11 1639 10

Benzo[alanthracene <97 97 ug/L 07/28/11 14:42 08/03/11 16:39 10

- Benzo[a]pyrene <97 97 ug/L 07/28/11 14:42 08/03/11 16.39 10

Benzo[b}fluorarithene <97 97 ug/L 07/28/11 1442 08/03/11 16:39 10

Benzo[g,hi]perylene <97 97 ugIL 07)28/11 1442 08/03/11 1639 10

Benzo[k]fluoranthene <97 97 ugIL 07/28)11 1442 08/03/11 1639 10

Benzyl alcohol <97 97 ug)L 07/28/11 14:42 08/03/11 16:39 10

1,1-Biphenyl <97 97 ugIL 07/28/11 1442 08/03/11 1639 10

Bis(2-chloroethoxy)methane <97 97 ug/L 07/28/11 1442 08/03/11 1639 10

Bis(2-chloroethyl)elher <97 97 ug/L 07/28/11 1442 08/03)11 16:39 10

bis(chloroisopropyl) ether <97 97 ug/L 07/28/11 14:42 08/03/11 16.39 10

81s(2-ethylhexyl) phthalate <97 97 ug/L 07/28/11 1442 08/03/11 16 39 10

4-Bromophenyl phenyl elher <97 97 ug/L 07/28/11 1442 08/03/11 16:39 10

Butyt benzyl phthalate <97 97 ug/L 07/28/11 1442 08/03/11 1639 10

4-Chloroaniline <190 190 ug/L 07)28/11 1442 08/03/11 1639 10

4-Chtoro-3-methylphenol <97 97 ug/L 07/28/11 1442 08/03/11 1639 10

2-Chloronaphthatene <97 97 ug/L 07/28/il 1442 08/03/11 16.39 10

2-Chlorophenol <97 97 ugIL 07/28/11 1442 08/03/11 1639 10


Chrysene <97 97 ug/L 07/28/11 1442 08)03/11 1639 10

Diallate <97 97 ugIL 07/28/11 1442 08/03)11 1639 10

Dibenz(a,h)anthracene <97 97 ug/L 07/28/111442 08/03/11 1639 10

Dibenzofuran <97 97 ug/L 07/28)11 1442 08/03/11 1639 10

12-Dichlorobenzene <97 97 ug/L 07/28/11 14:42 08/03/11 1639 10

13-Dichlorobenzene <97 97 ug/L 07)28/11 1442 08/03/11 16.39 10


3,3’-Dichlorobenzdine <580 580 ug/L 07/28/11 14 42 08/03/11 1639 10

2,4-Dichlorophenol <97 97 ug/L 07/28)11 1442 08/03/11 1639 10

2,6-Dichlorophenol <97 97 ug/L 07/28/11 1442 08/03/11 1639 10


of 92

Client Sample ResultsClient: Ashland Inc.


Client Sample ID: ASH-MW23-07261 IDate Collected: 07126/11 12:51


Hexachioroethane

Hexachlorophene

Hexachloropropene

Indenoll 2,3-cd]pyrene

Isophorone

Isosafrole

Methapyrilene

3-Methyicholanthrene

Methyl methanesulfonate

2-Methylnaphthalene

Methyl parathion

2-Methy/phenol

3 & 4 Methylphenol

Naphlhalene

1 4-Naphthoquinone

1 -Naphlhylamine

2-Naphlhylamine

2-Nitroanihne

3-Nitroanihne

4-Nitroaniline

Nitrobenzene

2-Nitropheno!

4-Nitrophenol

O 4-Nitroquinoline-1-oxide

N-Nilro-o-toluidine

N.Nitrosode1hylamine

D Prepared

07/28111 1442

07/28/11 1442

07/28/11 14:42

07/28/11 14.42

07/28/11 14:42

07/28111 14:42

07/28/11 14:42

07/28/11 14-42

07/28/11 14:42

07128/11 14:42

07/28/11 14.42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07128111 14:42

07/28/11 14:42

07/28/11 1442

07)28/11 14:42

07/28/11 14-42

07/28/11 14-42

07/28/11 14:42

07/28/11 1442

07/28/11 1442

07/28/11 1442

07/28/11 14-42

07/28/11 14.42

07/28/11 14:42

07/28/11 14:42

07/28/11 14.42

07/28/11 14:42

07/28/111442

07/28/11 1442

07)28/11 14.42

07/28/1: 1442

07/28/11 1442

07/28/11 1442

07/28/11 14:42

07)28/11 14.42

07/28/11 14-42

07/28/11 14.42

07/28)1114-42

07/28)11 1442

07)28/11 14:42

07/28/11 1442

07/28/11 14-42

07/28/11 1442

07)28/11 1442

07/28/111442

Analyzed Dii Fac

08/03/11 1639 10

08/03)11 16.39 10

08/03/11 16:39 10

08/03/11 16.39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 1639 10

08/03/11 16:39 10

08/03/11 16.39 10

08/03/11 16:39 10

08/03/11 16-39 10

08/03(11 1639 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16.39 10

08/03/11 16:39 10

08/03/11 1639 10

08/03/11 16.39 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 16-39 10

08(03/11 16-39 10

08/03/11 1639 10

08/03/11 16-39 10

08/03)11 16:39 10

08/03/11 1639 10

08/03/11 1639 10

08/03/11 1639 10

08/03/11 1639 10

08/03/11 16:39 10

08/03/11 16:39 10

08/03/11 1639 10

08/03/11 1639 10

08/03/11 1639 10

08/03/11 1639 10

08/03/11 1639 10

08/03/11 1639 10

08/03/11 16-39 10

08/03/11 16:39 10

08/03/11 1639 10


TestAmerica Job ID: 680-70758-1 <..

iiLab Sample ID: 680-70758-6

Matrix: Water i-4

Method: 8270C - Semivolatile Organic Compounds (GCIMS) (Continued)Analyte Result Qualifier RL MDL tin/I

Diethyl phthatate <97 97 uq/L

Dimethoate <97 * 97 ug/L

712-Dimethylbenz(a)anthracene <97 97 ug/L

33’-Dimethylbenzidine <190 190 ug/L

2,4-Dimethylphenol <97 97 ug/L

0/methyl phthalate <97 97 uglL

Di-n-butyl phthalate <97 97 ug/L

1,3-Dinitrobenzene <97 97 ug/L

4,6-Dinitro-2-melhylphenol <480 480 ug/L

2,4-Dinitrophenol <480 480 ug/L

2,4-Dinitrotoluene <97 97 ug)L


Di-n-octyi phthalate <97 97 ug/L

Dinoseb <97 97 ug/L

1,4-Dioxane 890 97 ug/L

Disulfoton <97 • 97 ut/L

Ethyl methanesulfonate <97 97 ug/L

Ethyl Parathion <97 97 ug/L

Famphur <97 • 97 ug/L

OFluoranthene <97 97 ug/L

Fluorene <97 97 ug/L

Hexachlorobenzene <97 97 ug/L

Hexachlorobutadierie <97 97 ug/L

Hexachlorocvclooentadiena <97 97 ug/L

<97 97 ug)L

<48000 48000 ug/L

<97 97 ug/L

<97 97 ug/L

<97 97 ug/L

<97 97 ug/L

<19000 19000 ug/L

<97 97 ug/L

<97 97 ug/L

<97 97 ug/L

<97 97 ug/L

<97 97 ug/L

660 97 ug/L

<97 97 ug/L

<97 97 ug/L

<97 97 ug/L

<97 97 ug/L

<480 480 ug)L

<480 480 ug/L

<480 480 ug/L

<97 97 ug/L

<97 97 ug/L

<480 480 ug)L

<190 190 ug/L

<97 97 ug/L

<97 97 ug/L

of 92

Chent Sample ResultsClient: Ashland Inc.


Client Sample ID: ASH-MW23-072611Date Collected: 07/26/11 12:51

Date Received: 07127/lI 09:20

Pheno’

Phorate

2-Picoline

p-Phenylene diamine

Pronamide

Pyrene

Pyridine

Safrole, Total

Sulfolepp



Thionazin

2-Toluidine


2,4, 5-Trichlorophenol

2,4,6-Trichlorophenol

1 ,3,5-Trinitrobenzene

D Prepared Analyzed Dii Fac

07/28/11 14:42 08/03/11 16:39 10

07/28/11 1442 08/03/11 15:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03111 16:39 10

07/28/11 14:42 08/03111 1639 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07128/lI 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16.39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07)28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 1639 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 14:42 08/03/11 16:39 10

07/28/11 1442 08/03/11 1639 10

07/28/11 14:42 08/03/11 16.39 10

Analyzed Oil Fac

08/01/11 2155 1

08/01/11 21 55 1

08/01/11 21 55 1

08/01/11 2155 1

08/01/112155 1

08/01/11 21 55

08/01/11 21 55




-

i_- 6.

JIL:

Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)

Analyte Result Qualifier RL MDL Unit

N-Nitrosodimethytamine <97 97 ug/L

N-Nitrosodi-n-butylamine <97 97 ugIL

N-Nitrosodi-n-propylamine <97 97 ugiL

N-Nilrosodiphenylamine <97 97 ug/L

N-Nitrosomethylethylamine <97 97 ug/L

N-Nitrosomorpholine <97 97 ug/L

N-Nitrosopiperidine <97 97 ug/L

N-Nitrosopyrrolidine <97 97 ug/L

o,o,o-Tdetflylphosphorothioate <97 97 ug/L

p-Dimethylamino azobenzene <97 97 ug/L

Pentachlorobenzene <97 97 ug/L

Pentachloronitrobenzene <97 97 ug/L

Pentachlorophenol <480 480 ug/L

Phenacetin <97 97 ug!L

Phenanthrene <97 97

140 97 ug/L

<97 97 ug/L

<97 97 ugIL

<19000 19000 ugIL

<97 97 ug/L

<97 97 ug/L

<480 480 ug!L

<97 97 ug/L

<97 97 ugfL

<97 97 ug/L

<97 97 ug/L

<97 97 ugIL

<97 97 ug/L

<97 97 ug/L

<97 97 ug)L

<97 97 ug)L

<97 97 ug/L

0

Surrogate % Recoveiy Qualifier Limits

2-Fluombiphenyl 0 0 38 130

2-Fluorophenol 0 0 25- 130

N,trobenzene-d5 0 D 39 130

Phenol-d5 0 0 25 130

Terphenyl-d14 0 0 10 143

2,4,6-Tribromophenol 0 0 31 - 141

Method: 8081A_8082 - Organochlorine Pesticides & PCBs (GC)Analyte Result Qualifier RL MDL Unit D

Aldr/n <0.049 0049 ug/L

alpha-BHC <0049 0049 ug/L

beta-BHC (0049 0.049 ug/L

Chlordane (technical) <0 49 0.49 ug)L

Chlorobenzilale <0 49 049 ug/L

4,4’-DDD <0099 0.099 ug)L

4,4-DOE <0099 0099 ug/L

Analyzed

08/03/11 1639

08/03/11 16.39

08/03/11 16.39

08/03/11 1639

08/03/11 1639

08/03/11 1639

Dii Fac

10

10

10

10

10

10

Prepared

07/28/1114.42

07/28/111442

07/28/11 14.42

07/28/11 14:42

07/28/1114:42

07/28/1114 42

Prepared

07/28)11 14:42

07/28/11 1442

07/28/11 1442

07/28)11 1442

07/28/11 1442

07/28/11 1442

07)28/11 1442

of 92






Method: 8081A_8082 - Organochlorine Pesticides & PCBs (GC) (Continued)

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac

4.4’-DDT <0099 0099 ugIL 07/28111 14:42 08/01/11 21:55 1

delta-BHC <0.049 0 049 ug/L 07/28/11 14:42 08/01/11 21.55 1

Djefdrin <0.099 0.099 ug/L 07/28111 14:42 08101111 21:55 1

Endosulfan I <0.049 0049 ugh 07/28/11 14:42 08/01/11 21:55 1

Endosulfan II <0.099 0.099 ugIL 07128/11 14:42 08/01/11 21:55 1

Endosulfan sulfate <0.099 0.099 ugIL 07/28111 14:42 08101/11 21:55 1

Endnn <0.099 0.099 ug/L 07/28/11 14:42 08/01/11 21:55 1

Endrin aldehyde <0.099 0.099 uglL 07/28I11 14:42 08/01111 21:55 1

Endrin ketone <0.099 0.099 ugIL 07)28/11 14:42 08/01/11 21:55 1

gamma-BHC (Lindane) <0.049 0.049 ug/L 07/28/11 14:42 08/01/11 21:55 1

Heptachlor <0.049 0.049 ug/L 07/28111 14:42 08/01/11 21:55 1


Isodrin <0.049 0.049 ugIL 07/28/11 14:42 08/01/11 21:55 1

Keporle <0.99 0.99 ug/L 07/28/11 1442 08/01)11 21:55 1

Methoxychlor <0.099 0.099 ug/L 07/28/11 14:42 08/01)11 21:55 1

Toxaphene <4.9 4.9 ugIL 07/28/11 14:42 08)01/11 21:55 1

PCB-1 016 <0.99 0.99 ug/L 07/28/11 14:42 08/01/11 21:55 1

PCB-1221 <20 2.0 ug/L 07)28/11 14:42 08/01/11 21:55 1

PCB-1 232 <0.99 0.99 ug/L 07/28/11 1442 08)01/11 21:55 1

Q PCB-1242 <0.99 0.99 ugIL 07/28/11 14:42 08/01/11 21:55 1

PC8-1248 <0.99 0.99 ug/L 07/28111 1442 08/01111 21:55 1

PCB-1254 <0.99 0.99 ug/L 07/28/11 14:42 08/01/11 21:55 1

PCB-1260 <0.99 0.99 ug/L 07/28/11 14:42 08/01/11 21:55 1


Tetrachloro-m-xylene 109 36 130 07/28/11 1442 08/01/11 21:55 1

Tetrachloro-m-xylene 4 p X 36 130 07/28/11 1442 08/01/11 21:55 1

DCB Decachlorob,phenyl 11 X 40. 130 07/28/11 14.42 08/01/1121:55 1

DCB Decachlorobiphenyl 0.5 pX 40. 130 07/28/11 1442 08/0 7/11 21:55 1

Method: 8151A - Herbicides (GC)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

2,4-D 6.0 E p 0.50 ug/L 07/28/11 08:04 07)29/11 19:56 1

Silvex (2,4,5-TP) <050 050 ug/L 07/28/11 0804 07/29/11 1956 1

2,4,5-1 <0 50 050 ug/L 07/28/11 08 04 07/29/111956 1


DCAA 4231 EX 52151 07/28/110804 07/29/11 7956

DCAA 356 pX 52. 751 07/28/1108.04 07/29/11 19:56 1

Method: 8151A - Herbicides (GC) - DLAnalyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

2,4-D 10 0 20 ug/L 07/28/11 08.04 08/01/17 1639 4

Silvex (2,4,5.TP) <20 2.0 ug/L 07/28/11 08:04 08/01111 16.39 4

2,4,5-T <2.0 2.0 ug/L 07/28/11 08.04 08/01/11 16:39 4


DCAA 215 X 52.751 07/28/1108.04 08/01/171639 4

DCAA 2867 EX 52. 151 07/28/110804 08/01/Il 16.39 4


of 92

Client Sample ResultsClient: Ashland Inc. TestAmerjca Job ID: 680-70758-1

Project/Site: Hercules Hattiesburg APIX 7/26/11I


Date Collected: D7!26I11 12:51 Matrix: Water


Method: 8290 - Dioxins/Furans, HRGCIHRMS (8290)

Analyte Result Qualifier ML EDL TEF TEQ Unit 0 Prepared Analyzed Oil Fac

2,3,7,8-TcDD ND 10 0.40 1 pgIL 07/28/11 09.00 07/30/11 14:22 1 01

Total l-IxCDD ND 51 0.43 pgIL 07)28/11 09.00 07/30/11 14:22 1.01

Total HxCDF ND 51 0.40 pgIL 07/28/11 09:00 07/30/11 14:22 1.01

Total PecDD ND 51 0.47 pg/L 07/28/11 09:00 07/30/11 14:22 1.01

Total PeCDF ND 51 0.42 pgIL 07/28/11 09:00 07/30/11 14:22 1.01

Total TCDD ND 10 0.40 pg/L 07/28/11 09:00 07/30/11 14:22 1.01

Total TCDF ND 10 0.29 pgIL 07/28/11 0900 07/30)11 14:22 1.01


Internal Standard 6 Recovery Qualifier Limits Prepareil Analyzed Dii Fec

13C-2,3,7,8-TCDD 79 40- 135 07/28/11 09:00 07/30/11 14:22 1.01

13C- 1,2,3,7, 8-PeCDD 75 40- 135 07/28/11 09:00 07/30/1114:22 1.01

13C-1,2,3,6,7,8-HxCDD 87 40 135 07/28111 09:00 07/30/11 14:22 1.01

13C-2,3,7,8-TCDF 86 40- 135 07/28/Il 09:00 07/30/11 14:22 1.01

13C-1,2,3,7,8-PeCDF 79 40. 135 07,28/Il 09:00 07/30/11 14:22 1.01

13C-1,2,3,4,7,8-HxCDF 76 40-135 07)28/Il 09:00 07/30/11 1422 1.01

Method: 6020 - Metals (ICP/MS)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Antimony <5.0 50 ug/L 08/01/11 08:48 08/06/11 23:18 1

Arsenic 19 2.5 ug/L 08/01/11 0848 08/06/11 23:18 1

Barium 240 5.0 ug/L 08101/1108:48 08/06/11 23.18 1

Beryllium 3.3 050 ug/L 08/01/11 0848 08/06/11 23:18 1

Cadmium <0.50 0.50 ug/L 08/01/11 08:48 08)06/11 23:18 1

Chromium 5.0 50 ug/L 08/01)11 0848 08/06/11 2318 1

Cobalt 0.71 050 ug/L 08/01/11 08:48 08/06/11 23.18 1

Copper <50 5.0 ug/L 08/01/11 08.48 08/06/11 23:18 1

Lead <1 5 1 5 ug/L 08/01/11 0848 08/06/11 23:18 1

Nickel <50 50 ug)L 08/01/11 0848 08/06/11 23:18 1

Selenium <2.5 25 ug/L 08/01/11 08:48 08/06)11 23:18 1

Silver <1 0 1 0 ug/L 08/01/11 0848 08/06/11 23:18 1

Thallium <1 0 1 0 ug/L 08/01/11 08.48 08/06/11 23 18 1

Tin <50 50 ug)L 08/01/11 0848 08/06/11 23:18 1

Vanadium 16 10 ug/L 08/01/11 0848 08/06)11 2318 1

Zinc <20 20 ug/L 08101/11 0848 08/06/11 2318 1

Method: 7470A - Mercury (CVAA)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac

Mercury <020 020 ugiL 08/02)11 0942 08/02)11 1700 1

General ChemistryAnalyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac

Cyanide, Total <0.010 0010 mg/L 08/01/11 07.51 08/02/11 06:51 1

Analyte Result Qualifier RL RL Unit 0 Prepared Analyzed Dii Fac

Sulfide 7.9 1 0 mg/L -07127)11 1410 — 1


of 92


Client Sample ID: ASH-MWI9-072611 Lab Sample ID: 680-70758-7Date Collected: 07/26111 14:20 Matrix: WaterDate Received: 07/27/11 09:20

Carbon tetrachloride

Chlorobenzene

2-Chloro-1 ,3-butadiene

Chloroethane

Chloroform

Chioromethane

3-Chloro-i-propene

Chlorodbromomethane

1 2-Dibromo-3-Chloropropane

OEthylene Dibromide

Dibromomethane

trans-i 4-Dichloro-2-butene

Dichlorodifluoromethane

1 ,i-Dichtoroethane

1 ,2-Dichloroethane

cis-i ,2-Dichloroethene

trans-i ,2-Dichloroethene

1 .1-Dichloroethene

1 .2-Dichloropropane

cis-i ,3-Dichloropropene

trans-i ,3-Dichloropropene

Ethylbenzene

Ethyl methacrylate

2-Hexanorie

lodomethane

Isobutyl alcohol

Methacrylonitrile

Methylene Chloride

Methyl methacrylate

4-Methyl-2-pentanone (MISK)

Pentachloroethane

Propionilrile

Styrene

1,1,1 ,2-Tetrachloroethane

1,1 ,2,2-Tetrachloroethane

Tetrachioroethene

Toluene

11, 1-Tnchloroethane

1 1 ,2-Trichloroethane

Trichloroethene

3.3

<1.0<1.0

<1.0

<1.0

<1.0

<1.0

<2.0

<1.0

<1.0

<1.0

<1.0

<1.0

<1.0

<1.0

<1.0

<1 0

1.3

<1.0

<10

<5.0

<40

<20

<5.0

<1.0

<10

<5.0

<20

<1.0

<1.0

<1.0

<1.0

2.4

<1.0

<1.0

<1 0

1.0

1.0

1.0

1.0

1.0

10

1.0

2.0

1.0

1.0

1.0

1.0

1.0

10

1.0

1.0

1.0

1.0

1.0

10

50

40

20

5.0

1.0

10

5.0

20

1.0

1.0

10

1.0

1.0

10

1.0

1.0

MDL Unit D Prepared

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug!L

ug)L

ugiL

ug)L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Analyzed Oil Fat

07129/11 19:34

07/29/11 19:34 1

07/29111 19:34 1

07/29/11 19:34 1

07/29/11 19:34 1

07/29/il 19:34 1

07129111 19:34 1

07/29/11 19:34 1

07/29/li 19:34 1

07/29/11 19:34 1

07/29/11 19:34 1

07/29/11 19:34

07/29/11 19:34

07/29/li 19:34

07/29/11 19:34 1

07/29/11 19:34 1

07/29/11 19:34

07/29/11 19:34

07/29/11 19:34

07/29/11 19:34 1

07/29/11 19:34 1

07/29/il 19:34 1

07/29/11 19:34

07/29/li 19:34 1

07/29/11 19:34

07/29/il 19:34

07/29/11 19:34 1

07/29/11 19:34

07/29/11 19:34

07/29/11 19:34

07/29/11 19:34

07/29/11 19:34 1

07/29/11 19:34 1

07129/11 19:34

07/29/11 19:34

07)29/11 19:34

07/29/11 1934 1

07)29/il 1934 1

07/29)11 19:34 1

07/29/11 1934 1

07)29/11 1934 1

07)29/11 19:34

07)29)11 19:34

07/29)11 19:34

07/29)11 19:34

07/29/11 19:34 1

07129/11 19:34 1

07129/11 19:34 1

07)29/li 1934 1

07)29/11 19:34 1


Method: 826DB - Volatile Organic Compounds (GCIMS)Analyte Result Qualifier RL

Acetone -— <25 25

Acetonitrile <40 40

Acrolein <20 20

Acrylonitrite <20 20

Benzene 54 1.0

Dichlorobromomethane <1.0 1.0

Bromoform <1.0 * 1.0

Bromomethane <1.0 1.0


Carbon disulfide <2.0 2.0

3.5 1.0

9.9 1.0

<1.0 1.0

<1.0 10

of 92


ProjectlSite: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-MWI9-072611Date Collected: 07126111 14:20



Lab Sample ID 680-70758-7Matrix: Water

Method: 82608 - Volatile Organic Compounds (GC!MS) (Continued)

Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed

Trichlorofluoromethane <1,0 10 ugIL 07/29/11 19:34

1,2,3-Trichloropropane <1 0 1 0 ug/L 07/29/11 19:34

Vinyl acetate <2.0 2.0 ug/L 07/29111 19.34

Vinyl chloride <1 0 1.0 ug/L 07/29/11 19.34

Xylenes, Total <20 2.0 ug/L 07/2911119.34


4-Bromofluorobenzene 95 70 - 130

Dibromofluoromethane 109 70 - 130

Toluene-d8(Surr) 101 70- 130

Method: 8270C - Semivolatile Organic Compounds (GC/MS)Analyte Result Qualifier RL MDL

Acenaphthene <99 99

Acenaphlhylene <99 99

Acetophenone <99 99

2-Acetytaminofluorene <99 99

alpha,alpha-Dimethyl phenethylamine <20000 20000

4-Aminobiphenyl <99 99

Aniline <200 200

Anthracene <99 99

Aramite, Total <99 99

Benzo[ajanlhracene <99 99

Benzo[a]pyrene <99 99

Benzo[b]fluoranthene <99 99

Benzog,h,i1perylene <99 99

Benzo[k]fluoranthene <99 99

Benzyl alcohol <99 99

1,1’-Biphenyl 770 99

Bis(2-chloroethoxy)methane <99 99

Bis(2-chloroethyl)ether <99 99

bls(chloroisopropyl) ether <99 99

Bis(2-ethylhexyl) phthalate <99 99

4-Bromophenyl phenyl ether <99 99

Butyl benzyl phthalate <99 99

4-Chloroaniline <200 200

4-Chloro-3-methylphenol 99 99

2-Chloronaphthalene <99 99

2-Chlorophenol <99 99

4-Chlorophenyl phenyl ether <99 99

Chrysene <99 99

Diallate <99 99

Dibenz(ah)anttiracene <99 99

Dibenzoturan <99 99

1 ,2-Dichlorobenzene <99 99

I ,3-Dichlorobenzene <99 99

1 ,4-Dichlorobenzene <99 99

3,3-Dichlorobenzidirre <600 600

24-Dichlorophenol <99 99

2,6-Dichlorophenol <99 99


07/29/11 19:34 1

07/29/11 19.34 1

07/29/Il 19:34

Unit D Prepared Analyzed Oil Fac

ug/L 07/28/11 14:42 08/04/11 1347 10

ug/L 07)28)11 14:42 08/04)11 13.47 10

ug/L 07/28111 14.42 08/04/11 13:47 10

ug)L 07/28/11 14,42 08/04/11 13,47 10

ug/L 07/28/11 14.42 08/04/11 13:47 10

ug/L 07/28/11 14:42 08/04/11 1347 10

ug/L 07/28/11 14:42 08/04/11 13:47 10

ug/L 07/28/11 1442 08/04/11 13:47 10

ug)L 07/28/11 14:42 08/04/11 1347 10

ug/L 07/28/11 14.42 08/04/11 13:47 10

ug/L 07/28/11 1442 08/04/11 1347 10

ug)L 07/28/11 14:42 08/04/11 13:47 10

ug)L 07128/11 1442 08/04/11 13:47 10

ug/L 07/28/11 1442 08/04/11 1347 10

ugIL 07/28/11 14:42 08/04/11 13.47 10

ug/L 07/28)11 1442 08/04/11 13.47 10

ug/L 07/28/11 14.42 08/04/11 13:47 10

uQ/L 07/28/11 1442 08/04/11 13.47 10

ug/L 07/28/11 1442 08/04/11 13.47 10

ug/L 07/28/11 1442 08/04/11 1347 10

ug/L 07/28/11 1442 08/04/11 13.47 10

ug/L 07/28/11 1442 08/04/1113:47 10

ug/L 07/28/11 14:42 08/04/11 13:47 10

ug/L 07/28/Il 1442 08/04/11 13.47 10

ug/L 07/28/111442 08/04/111347 10

ug/L 07/28)11 14:42 08/04/11 1347 10

UQIL 07/28/Il 14 42 08/04/1113.47 10

ug/L 07/28/11 14:42 08/04/11 1347 10

ug/L 07/28/11 1442 08/04/11 1347 10

ug/L 07/28/111442 08/04/11 1347 10

ug/L 07/28/11 1442 08/04/11 13.47 10

ug/L 07/28/11 14.42 08/04/11 13.47 10

ug/L 07/28/111442 08/04/11 1347 10

ug/L 07/28/11 1442 08/04/11 13 47 10

ugIL 07)28)11 1442 08/04/11 1347 10

ug/L 07/28/11 1442 08)04/11 1347 10

u9/L 07/28/11 1442 08/04/11 1347 10


Oil Fac

0

of 92

MDL Unit

ug/L

ug/L

ug/L

ug/L

ug/L

ug)L

ug/L

ug/L

uq/L

ugIL

ug/L

ug)L

ugIL

ug/L

ug/L

ug/L

ugIL

ug/L

ug/L

ug/L

ug/L

ug/L

ugIL

ug/L

ug/L

ug/L

ug/L

ug)L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ugiL

D Prepared

07/28/11 14:42

07/28/11 1442

07/28111 1442

07/28/11 14:42

07/28/11 14.42

07/28/11 14.42

07/28/11 14:42

07/28/11 14.42

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07)28/11 14:42

07/28/11 1442

07/28/11 14:42

07/28/11 14:42

07/28/11 14:42

07/28/11 1442

07/28/11 14.42

07/28)11 1442

07/28/11 14:42

07/28/11 14:42

07/28/11 1442

07(28/11 14:42

07/28/11 14:42

07/28/11 1442

07/28/11 14:42

07128/11 1442

07/28/11 14.42

07/28/11 1442

07/28/11 1442

07/28/11 1442

07/28)111442

07)28/111442

07)28/11 14.42

07/28/111442

07)28/11 14.42

07/28/11 14 42

07/28/111442

07/28/11 1442

07/28/11 14.42

07/28/11 14:42

07)28/11 14.42

07/28/1114.42

07/28/11 1442

07/28/111442

07/28/111442

07/28/11 1442

07/28/ti 1442

07/28/11 14:42

07/28/11 1442

Analyzed Dli Fac

08/04/11 13:47 10

08/04)11 13.47 10

08/04/11 13:47 10

08/04/11 13:47 10

08/04/Il 13:47 10

08/04)11 13:47 10

08/04/11 13:47 10

08/04/11 13:47 10

08)04/11 13:47 10

08/04/11 13:47 10

08(04/11 13:47 10

08/04111 1347 10

08/04/11 13:47 10

08/04/11 13:47 10

08)04/11 13:47 10

08/04/11 13:47 10

08)04/1113:47 10

08/04/11 13:47 10

08)04)11 13:47 10

08/04/11 13:47 10

08/04/11 13:47 10

08/04)11 13:47 10

08/04/11 1347 10

08/04/11 13:47 10

08/04/11 13:47 10

08/04)11 13:47 10

08/04/11 13:47 10

08/04/11 13:47 10

08/04/11 13:47 10

08)04)11 13:47 10

08/04)11 13:47 10

08/04/11 13.47 10

08/04/11 13.47 10

08)04)11 1347 10

08/04/11 13.47 10

08/04/11 1347 10

08/04)11 13.47 10

08/04/11 1347 10

08/04)11 1347 10

08/04/11 1347 10

08/04/11 13.47 10

08/04/11 13:47 10

08)04)1113:47 10

08/04/11 1347 10

08/04/11 13.47 10

08)04)11 13.47 10

08/04/11 1347 10

08/04/11 13:47 10

08)04/11 13:47 10

08/04)11 1347 10


Client Sample ResultsTestAmerica Job ID. 680-70758-1

LJ- Lab Sample ID: 680-70758-7

Matrix: Water

Client: Ashland Inc.rojectlSite: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: ASH-MWI9-072611

Date Collected: 07126/11 14:20


Method: 8270C - Semivolatile Organic Compounds (GCIMS) (Continued)Analyte Result Qualifier RL

Dielhyl phthalate <99 99

Dimethoale <99 • 99

7,12-Dimethylbenz(a)anthracene <99 99

3,3-Dimethylbenzidine <200 200

2,4-Dimethylphenol <99 99

Dimethyl phthalale <99 99

Di-n-butyl phthalate <99 99

1,3-Dinitrobenzene <99 99

4,6-Dinitro-2-methylphenol <500 500

2,4-Dinitrophenol <500 500

2,4-Dinitrotoluene <99 99

2,6-Dinitrotoluene <99 99

Di-n-octyl phthalate <99 99

Dinoseb <99 99

14-Dioxane <99 99

Disulfoton <99 * 99

Ethyl methanesulfonate <99 99

Ethyl Parathion <99 99

Famphur <99 * 99

OFluoranthene <99 99

Fluorene <99 gg

Hexachlorobenzene <99 99

Hexachlorobutadiene <99 99

Hexachlorocyciopentadiene <99 99

Hexachloroethane <99 99

Hexachlorophene <50000 50000

Hexachloropropene <99 99

lndeno[12,3-cd]pyrene <99 99

Isophorone <99 99

tsosaf role <99 99

Methapyrilene <20000 20000

3-Methylcholanthrene <99 99

Methyl methar3esulfonate <99 99

2-Methylnaphlha/ene <99 99

Methyl paralhion <99 99

2-Methylpherrol <99 99

3 & 4 Methylphenol <99 99

Naphthalene <99 99

1,4-Naphlhoquinone <99 99

1-Naphlhylarnine <99 99

2-Naphthylamine <99 99

2-Nitroaniline <500 500



Nitrobenzene <99 99

2-Nilrophenol <99 99

4-Nitrophenoi <500 500

4-Nitroquinolre- 1 -oxide <200 200

N-Ntlro-o loluidine <99 gg

N-Nitrosodiethylamine <99 99

of 92

Client Sample ResultsClient: Ashland Inc.ProjectlSite: Hercules Hattiesburg APIX 7/26/11



Client Sample ID: ASH-MWI 9-072611 Lab Sample ID: 680-70758-7Date Collected: 07/26/11 14:20 Matrix: Water


tJ

Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed DII Fac

N-Nitrosodimethylamine <99 99 - - ug/L 07/28/11 1442 08/04/11 1347 10

N-Nitrosodi-n-butylamine <99 99 ugIL 07/28111 1442 08104/11 1347 10

N-Nitrosodi-n-propylamine <99 99 ug/L 07/28111 14:42 08/04/11 1347 10

N-Nitrosodiphenylamine <99 99 ugIL 07/28/11 14.42 08/04/11 1347 10

. N-Nitrosomethylethylamine <99 99 ug/L 07/28/li 14:42 08/04/11 1347 10

N-Nitrosomorpholine <99 99 ugIL 07/28)11 1442 08/04/11 1347 10

N-Nitrosopiperidine <99 99 uq,’L 07/28/11 1442 08/04/11 13.47 10 43//

N-Nitrosopyrrolidine <99 99 ug)L 07/28/11 1442 08/04/11 13:47 10

o,o’,o”-Triethylphosphorothioate <99 99 ug/L 07/28(11 14.42 08/04/11 13:47 10

p-Dimethylaminoazobenzene <99 99 ug/L 07/28/11 1442 08104111 1347 10 .;<

Pentachlorobenzene <99 99 ug/L 07/28/11 14:42 08)04/11 13.47 10

Pentachloronitrobenzene <99 99 ug/L 07/28/11 1442 08/04/11 13.47 10

Pentachlorophenol <500 500 ug)L 07/28/11 1442 08/04/11 1347 10 ....

Phenacetin <99 99 ugiL 07/28/11 14:42 08/04/11 1347 10

Phenanthrene <99 99 ug/L 07/28)11 14:42 08/04/11 13.47 10

Phenol <99 99 ugIL 07/28/11 14:42 08/04/11 13:47 10

Phorate <99 99 ugIL 07/28/11 14.42 08/04/11 13:47 10 <-

2-Picoline <99 99 ugiL 07/28/11 1442 08(04(11 1347 10

p-Phenylene diamine <20000 20000 ug/L 07/28111 14 42 08/04/11 13 47 10

Pronamide <99 99 ug/L 07)28/11 14:42 08/04/11 1347 10

Pyrene <99 99 ug/L 07)28)11 14.42 08/04/11 13.47 10

Pyridine <500 500 ug/L 07)28/11 14:42 08/04/11 13.47 10

Safrole, Total <99 99 ug/L 07/28/11 1442 08/04/11 13.47 10

Sulfotepp <99 99 ug/L 07/28/11 14.42 08/04/11 1347 10

1,2,4,5-Tetrachlorobenzene <99 99 ug/L 07/28/11 14:42 08/04/11 1347 10

2,3,46-Tetrachlorophenol <99 99 ug/L 07/28/Il 14.42 08/04/11 1347 10

Thionazin <99 99 ug/L 07/28/11 14.42 08/04/11 1347 10

2-Toluidine <99 99 ugIL 07/28)11 1442 08/04/11 1347 10

l,2,4-Trichlorobenzene <99 99 ug/L 07/28/11 14.42 08/04/11 13.47 10

2,4,5-Trichlorophenol <99 99 ug/L 07/28/11 14 42 08/04/11 1347 10

2,4,6-Trichlorophenol <99 99 ug/L 07/28/11 14-42 08/04/11 1347 10

1,3,5-Trinitrobenzene <99 99 ug/L 07/28/11 14:42 08/04/11 1347 10

Surrogate

2-Fluorobiphenyl

2-Flu orophenol

Nitrobenzene-d5

Phenol-d5

Terphenyl-d 14

2,4 6- Thbromophenol


0 0 38130

0 0 25130

0 0 39-130

0 0 25.130

0 0 10143

0 0 3114i

Prepared

07/28/11 14.42

07/28/11 14.42

07/28,/il 1442

07/28/li 1442

07/28111 1442

07/28/lI 14.42

Analyzed

08/04/11 1347

08/01/11 1347

08/04/il 1347

08/04/li 1347

08/04/li 1347

08/04/li 1347

DII Fec

10

10

10

10

10

10

Method: 8081A 8082 - Organochiorine Pesticides & PCBs (GC)Analyte Result Qualifier RL

AIdrin <0 049 0 049

alpha-BHC <0049 0049

beta-BHC 0 049 0.049

Chlordane (technical) <0 49 049

Chlorobenzilale <0 49 049

4,4’-DDD <0 099 0099

4,4-DDE <0 099 0 099

MDL Unit

Ug/L

ug/L

ug/L

ug)L

ug)L

ug/L

D Prepared

07/28/111442

07/28)11 1442

07/28)11 1442

07/28/11 1442

07)28/11 1442

07/28/11 1442

07/28/il 1442

Analyzed

101/11 2214

08/01/112214

08/01/11 2214

08/01111 2214

08/01/11 2214

08/0:/11 22.14

08/01/112214

DI Fac

of 92

Client Sample ResultsClient: Ashland Inc.


Client Sample ID: ASH-MWI9-072611 -

Date Collected: 07/26/11 14:20Date Received: 07127/11 09:20



Surrogate




OCB Decachlorobiphenyl


44

50

10 X

TX

Limits

36.. 130

36. 130

40. 130

40 130

Prepared

07/28/11 14:42

07/28/11 14:42

07/28/11 14.42

07/28/11 1442

Analyzed

08/01/11 22:14

08/01/11 22:14

08/01/11 22:14

08/01/11 22:14

TestAmenca Savannah

Method: 8081A_8082 - Organochlorine Pesticides & PCBs (GC) (Continued)Analyte Result Qualifier —- RL MDL Unit D Prepared Analyzed Dii Fac

44-DOT <0.099 0.099 ug/L 07/28/11 14:42 08101/11 22:14 1

delta-BHc <0.049 0.049 ug/L 07/28/11 1442 08/01/11 22:14 1

Dieldrin <0.099 0 099 ug/L 07/28/11 1442 08/01/11 22:14 1

Endosulfan I <0.049 0.049 ugIL 07/28/11 14:42 08/01/11 22:14 1

Endosulfan II <0.099 0.099 ug/L 07/28/11 14.42 08/01/11 22:14 1

Endosulfan sulfate <0.099 0.099 ugIL 07/28/11 14:42 08/01/11 22:14 1

Endrin <0.099 0.099 ug/L 07/28)11 14:42 08101/11 22:14 1

Endrinaldehyde <0.099 0.099 ug/L 07/28/11 14:42 08101111 22:14 1

Endrin ketone <0.099 0.099 ugIL 07/28/11 14:42 08/01/11 22:14 1

gamma-BHc (Lindane) <0.049 0.049 ug/L 07/28/11 1442 08/01/11 22:14 1

Heptachlor <0.049 0.049 ugIL 07/28/11 14:42 08/01/11 22:14 1


lsodrin <0.049 0.049 ug/L 07/28/11 14:42 08/01/11 22:14 1

Kepone <0.99 0.99 ugIL 07/28/11 14:42 08/01/11 22:14 1

Methoxychlor <0.099 0.099 ug/L 07/28/11 14:42 08/01/11 22:14 1

Toxaphene <4.9 4.9 ug)L 07128/11 14:42 08/01/11 22:14 1

PCB-1016 <0.99 0.99 ugIL 07/28/11 14:42 08/01/11 22:14 1

PCB-1 221 <20 2.0 uglL 07/28/11 1442 08/01/11 22:14 1

PCB-1232 <0.99 099 ug/L 07/28/11 1442 08/01/11 22:14 1

PCB-1242 <0.99 0.99 ug/L 07/28)11 14.42 08/01/11 22.14 1

PCB-1248 <0.99 099 ugIL 07/28)11 1442 08/01/11 22:14 1

PCB-1254 <0.99 0.99 ug/L 07)28/11 14:42 08/01/11 22:14 1

PCB-1260 <0.99 0.99 ug/L 07/28/11 14:42 08/01/11 22:14 1

Dii Fac

Method: 8151A - Herbicides (GC)Analyte MDL Unit D Analyzed —_Dil Fac

2,4-0 ug/L — 07/29/11 20:12 1

S/vex (2,4,5-TP) <050 ug/L 07/29/11 20:12 1

2.4,5-T <050 ug/L 07/29/11 20:12 1

Surrogate - % Recovery Analyzed Dil Fac

DCAA 163 07/29/1120 12 1

DCAA 07/29/1120 12 1

Method: 8290- Dioxins/Furans, HRGC/HRMS (8290)

Analyte Result Qualifier ML EDL TEF TEQ Unit D Prepared Analyzed Oil Fac

2,3,7,8-TCDD ND 10 016 1 pg/L 07)28/11 09:00 07)30/11 15:07 1

Total HxCDD ND 50 0.52 pgfL 07)28/11 0900 07/30/11 1507 1

Tolal HxCDF ND 50 0.26 pglL 07/28)11 0900 07/30/11 1507 1

Total PeCDD ND 50 044 pg/L 07)28111 09:00 07/30/11 15.07 1

Total PeCOF ND 50 0 18 pg)L 07)28/11 0900 07/30/11 15.07 1

Total TCDD ND 10 034 pg)L 07/28/11 0900 07)30/11 1507 1

Total TCDF ND 10 020 pg)L 07/28/11 09:00 07)30)11 1507 1


Result Qualifier

<050

Qualifier

x72 p

RL

0.50

0.50

0 50

Limits

52 151

52 151

Prepared

07/28/11 08 04

07/28/11 0804

07/28/11 08 04

Prepared

07/28/11 08 04

07/28111 0804

of92






Internal Standard % Recovery Qualifier Limits Prepared Analyzed Dii Fac

13C-2,3,7,8-TCDD - 76 — 40- 135 07/28/11 09:00 07/30/11 15:07

13C-12,378-PeCDD 72 40- 135 07/28/11 0900 07/30/11 15:07 1

13C-1,2,3,67,8-HxCDD 82 40-135 07728/1109:00 07/30/11 1507 1

13C-2,37,8-TCDF 83 40- 135 07/28/11 09.00 07/30/11 15:07 1

13C-1,2,3,7,8-PeCDF 77 40 135 07/28/11 09:00 07/30/11 15:07 1

13C-1,2,3,4,7.8-HxCDF 77 40- 135 07/28/11 09:00 07/30/11 15:07 1

Method: 6020 - Metals (ICP/MS)Analyte -_________

Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Antimony <5.0 5.0 ug/L 08101/11 08:48 08/06/11 23:38 1

Arsenic 14 2.5 ugIL 08/01/11 08:48 08/06/11 23:38 1

Barium 51 5.0 ug/L 08/01/11 08:48 08/06/11 23:38 1

Beryllium <0.50 ó.50 ug/L 08/01/11 08:48 08/06/11 23:38 1

Cadmium <0.50 0.50 ug/L 08/01/11 08:48 08/06111 23:38 1

Chromium <5.0 5.0 ug/L 08/01/11 08:48 08/06/11 23:38 1

Cobalt <0.50 0.50 ug)L 08/01/11 08:48 08/06/11 23:38 1

Copper <5.0 5.0 ug/L 08/01/11 0848 08/06/11 23:38 1

Lead <1.5 1.5 ug/L 08/01/11 08:48 08/06/11 23:38 1

Nickel <5.0 5.0 ug)L 08/01/11 08:48 08/06/11 23:38 1

Selenium <2.5 2.5 ug/L 08/01/11 08:48 08/06/11 23:38 1

Silver <1.0 1.0 ug/L 08/01/11 08:48 08/06/11 23:38 1

Thallium <1.0 1.0 ug/L 08/01/11 0848 08/06/11 23:38 1

Tin <5.0 5.0 ugIL 08/Ol/il 08:48 08/06/11 23:38 1

Vanadium <10 10 ug/L 08/01/11 08:48 08106/11 23:38 1

Zinc 57 20 ug/L 08/01)11 08:48 08/06/11 23:38 1

Method: 7470A - Mercury (CVAA)Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fac

Mercury <020 0.20 ug/L 08/02/11 09.42 08/02/11 17:03 1

General ChemistryAnalyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

Cyanide, Total <0.010 0010 mg/L 08/01/11 0751 08/02/11 0654 1

Anatyte Result Qualifier RL RL Unit D Prepared Analyzed Oil Fac

Sulfide <1.0 1 0 mg/L 07/27/11 14 10 1


of 92


lient Sample ID: Trip Blank Lab Sample ID: 680-70758-9Date Collected: 07/26/11 00:00 Matrix: WaterDate Received: 07127/11 09:20

Method: 8260B - Volatile Organic Compounds (GCIMS)Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac

Acetone <25 25 ug/L 07129/11 14:39 1

Acetonitnle <40 40 ug/L 07129/11 14:39 1

Acrolein <20 20 ugIL 07/29/11 14:39 1

Acrylonitrile . <20 20 ug/L 07129/11 14:39 1

Benzene <1.0 1 0 ug/L 07/29/11 14:39 1

Dichlorobromomethane <1.0 1.0 ug/L 07129/11 14:39 1

Bromoform <1.0 * 1.0 ug/L 07/29/11 14:39 1

Bromomethane <1.0 1.0 ug/L 07/29/11 14:39 1

2-Butanone (MEK) <10 10 ug/L 07/29/11 14:39 1

carbon disulfide <2.0 2.0 ug/L 07/29/11 14:39 1

Carbon tetrachloride <1.0 1.0 ug/L 07/29/11 14:39 1

Chlorobenzene <1.0 1.0 ug/L 07/29/11 14:39 1

2-Chloro-i,3-butadiene <1.0 1.0 ug/L 07/29/11 14:39 1

Chloroethane <1.0 1.0 ug/L 07/29/11 14:39 1

Chloroform <1.0 1.0 ug/L 07/29/11 14:39 1

Chloromethane <1.0 1.0 ugIL 07/29/11 14:39 1

3-Chloro-i-propene <1.0 1.0 ugIL 07/29/11 14:39 1

Chlorodbromomethane <1.0 1.0 ug/L 07/29/11 14:39 1

i,2-Dibromo-3-Chloropropane <1.0 * 1.0 ug/L 07/29/11 14:39 1

QEthylene Dibromide <1.0 1.0 ug/L 07/29/11 14:39 1

Dibromomethane <1.0 1.0 ug/L 07/29/11 14:39 1

trans-i 4-Dichloro-2-butene <2.0 2.0 ug/L 07/29/11 14:39 1

Dichlorodifluoromethane <1.0 1 0 ug/L 07/29/11 14:39 1

11-Dichloroethane <1.0 1.0 ug/L 07/29/11 14:39 1

12-Dichloroethane <1.0 1 0 ug/L 07/29/11 14:39 1

cis-i2-Dichloroethene <1.0 1.0 ug/L 07/29/11 1439 1

trans-i2-Dichloroethene <1.0 1.0 ug/L 07/29/11 14:39 1

li-Dichloroethene <1.0 1 0 ug/L 07/29/11 14.39 1

1,2-Dichloropropane <1.0 1 0 ug/L 07/29/11 14:39 1

cis-i3-Dichloropropene <1.0 1.0 ug/L 07/29/11 14.39

trans-13-Dichloropropene <1.0 1 0 ugIL 07/29/il 14:39

Ethylbenzene <1.0 1.0 ug/L 07/29/il 14:39

Ethyl methacrylate <1.0 1.0 ug/L 07/29/li 14:39

2-Hexanone <10 10 ug/L 07/29/11 14.39

lodomethane <50 5.0 ug/L 07/29111 1439 1

Isobutyl alcohol <40 40 ug/L 07/29/il 1439 1

Methacrylonitrile <20 20 ug/L 07/29/11 1439 1

Methylene Chloride <50 5.0 ug/L 07/29/il 14-39

Methyl methacrylate <1.0 1 0 ug/L 07/29/il 14.39

4-Methyl-2-pentanone (MIBK) <10 10 ug/L 07/29/li 14:39

Pentachloroethane <5.0 50 ug/L 07/29)11 14.39

Propionitrle <20 20 ug/L 07/29/li 14.39 1

Slyrene <1 0 1.0 ug/L 07/29/il 1439 1

1,1,1 2-Tetrachloroethane <1.0 1.0 ug/L 07/29/11 1439 1

li,Z2-Tetrachloroethane <1 0 1.0 ug/L 07/29)11 1439

Tetrachloroethene <1.0 1.0 ug/L 07/29/li 14.39

Toluene <1.0 1 0 ugIL 07/29/11 1439 1

Q ii,l-Trichloroethane <1.0 1 0 ug/L 07/29/11 14:39 1

i,i2-Trichloroethane <1 0 1 0 ug/L 07/29/11 14.39 1

Trichloroethene <1.0 1.0 ug/L 07)29/il 14-39


of 92



Client Sample ID: Trip Blank Lab Sample ID: 680-70758-9



Method: 8260B - Volatile Organic Compounds (GCIMS) (Continued)

Analyte — Result Qualifier RL MDL Unit - D Prepared Analyzed Dii Fac

Trichlorofluoromethane <10 1.0 ug/L 07129/11 1439 1

1,23-Trichloropropane <1 0 1 0 ug/L 07/29/11 14:39 1

Vinyl acetate <2.0 20 ug/L 07/29/11 14:39 1

Vinyl chloride <1 0 1 0 ug/L 07/29111 14:39 1

Xylenes, Total <2.0 2.0 ugIL 07/29/11 1439 1

Surrogate % Recovery Qualifier Limits Prepared Analyzed Dii Fec

4-Bromofluorobenzene 97 70 130 07/29/11 14:39 1

Dibromofluoromefhane 107 70 130 07/29/1114:39 1

Toluene-d8 (Surr) 98 70 130 07/29/1114:39 1

C


of 92

Surrogate SummaryCflent: Ashland Inc. TestAmerica Job ID. 680-70758-1

C_5rojectlSite:Hercules Hattiesburg APIX 7/26/11

Method: 8260B - Volatile Organic Compounds (GCIMS)Matrix:Water - -

PrepType:TotaIINA

Percent Surrogate Recovery (Acceptance Limits)

BFB DBFM TOL

Lab Sample ID CllentSamplelD (70-130) (70-130) (70-130)

680-70758-1 ASH-MWO8-072611 94 108 97

680-70758-2 ASH-DUP-072611 104 103 104 :T680-70758-3 ASH-RSI-072611 94 103 100

680-70758-4 ASI-t-MW13-072611 102 101 101

680-70758-5 ASH-MW17-072611 106 96 106

680-70758-6 ASH-MW23-072611 94 109 99

680-70758-7 ASH-MW19-072611 95 109 101

680-70758-9 Tnp Blank 97 107 98

LCS 680-210523110 Lab Control Sample 96 104 98

LCS 680-210543/4 Lab Control Sample 104 108 101

LCS 680-210665/8 Lab Control Sample 92 89 92

LCSD 680-210523/11 Lab Control Sample Dup 107 112 106

LCSD 680-210543/5 Lab Control Sample Dup 102 103 101

LCSO 680-210665/9 Lab Control Sample Dup 110 109 107

MB 680-210523/13 Method Blank 101 104 99

MB 680-210543/7 Method Blank 93 107 100

MB 680-210665/11 Method Blank 103 103 102

Surrogate Legend

BFB = 4-Bromofluorobenzene

DBFM = Dibromolluoromethane

TOL = Toluene-d8 (Surr)

Method: 8270C - Semivolatile Organic Compounds (GCIMS)Matrix: Water Prep Type:T0taUNA


FBP 2FP NBZ PHL TPH TBP

Lab Sample ID Client Sample ID (38-130) (25-130) (39-130) (25-1 30) (10.143) (31.141)

680-70758-1 ASH-MWO8-072611 0 D 00 0 D 0 D 0 D 0 D

680-70758-2 ASH-DUP-072611 00 0 D 00 0 D 0 D 00

680-70758-3 ASH-RSI-072611 63 67 74 63 81 76

680-70758-4 ASH-MW13-072611 61 40 50 51 65 85

680-70758-5 ASH-M Wi 7-072611 00 00 0 D 00 00 00

680-70758-6 ASH-MW23-07261 1 0 0 00 0 0 0 D 0 D 00

680-70758-7 ASH-MW19-072611 0 D 00 00 00 0 D 00

LCS 680-210278/15-A Lab Control Sample 72 77 87 80 87 87

LCS 680-210278/18-A Lab Control Sample 70 65 74 70 84 93

MEl 680-210278/14-A Method Blank 75 76 83 83 87 80

Surrogate Legend

FBP = 2-Fluorobiphenyl

2FP = 2-Fluorophenol

NBZ = Nitrobenzene-d5

PHL = Phenol-dS

TPH = Terphenyl-d14

TOP = 2,4 6-Tribromophenol


of 92

Surrogate SummaryClient: Ashland Inc. TestAmerica Job ID: 680-70758-1


Method: 8081 A_8082 - Organochiorine Pesticides & PCBs (GC) D.Matrix: Water

Prep Type: TotalINA


TCX1 TCX2 DCBI DCB2

Lab Sample ID Client Sample ID (36-130) (36.130) (40-130) (40-130)

680-70756-i ASH-MW08-072611 41 - 55 - lix — - 5 pX —

680-70758-2 ASI-I-DUP-07261i 44 35X 14X 2px

680-70758-3 ASH-RSI-072611 63 64 51 48

680-70758-4 ASH-MW13-072611 37p 302X iox 8pX

680-70758-5 ASH-MW17-072611 0 D 00 00 0 D

680-70758-6 ASH-MW23-072611 109 4 pX lix 0.5 pX

680-70758-7 ASI-t-M Wi 9-072611 44 50 1OX 7 X

LCS 680-210285/19-A Lab Control Sample 59 58 37 X 37 X

LCS 680-210285124-A Lab Control Sample 78 80 63 51

LCS 680-210285/27-A Lab Control Sample 71 67 54 41

LCSD 680-210285/28-A Lab Control Sample Dup 77 69 69 53

MB 680-210285/18-A Method Blank 70 67 55 43

Surrogate Legend

______________ _________________________________________________-

TCX = Tetrachloro-m-xylene

DCB = DCB Decachlorobiphenyl

Method: 8151A - Herbicides (GC)Matrix: Water

Prep Type: Total/NA


DCPAI DCPA2

Lab Sample ID Client Sample ID (52-151) (52-151)

_________

680-70758-i ASH-MWO8-072611 106 p 395 X

680-70758-2 ASH-DUP-072611 92p 409X

680-70758-3 ASH-RSI-07261 1 73 77

680-70758-4 ASH-MW13-072611 87 80

680-70758-5 ASH-MW17-07261 1 289 p X 10096 E

x

680-70758-6 ASH-MW23-07261 1 356 p X 4231 E X

680-70758-6 - DL ASH-MW23-072611 215 X 28672 x

680-70758-7 ASH-MW19-072611 72 p 163X

LCS 680-210266/19-A Lab Control Sample 88 114

MB 680-210266/18-A Method Blank 80 92

Surrogate Legend

DCPA = DCAA


of 92

QC Sample ResultsClient: Ashland Inc. TestAmerica Job ID: 680-70758-1


Method: 8260B - Volatile Organic Compounds (GC/MS)

Lab Sample ID: MB 680-210523/13 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 210523MB MB

Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Dii Fac

Acetone <25 25 ug/L 07129/11 12:13 1

Acetonitrile <40 40 ug/L 07/29111 12:13 1

Acrolein <20 20 ugIL 07/29111 12:13 1

Acrylonitrile <20 20 ug/L 07129/11 12:13 1

Benzene <1.0 1.0 ugIL 07/29/11 12:13 1

Dichlorobromomethane <1.0 1.0 ugIL 07/2911112:13 1

Bromoform <1.0 1.0 ug/L 07/29/11 12:13 1

Bromomethane <1.0 1.0 ug/L 07/29)11 12:13 1

2-Butanone (MEK) <10 10 ug/L 07/29/11 12:13 1

Carbon disulfide <2.0 20 ugIL 07/29/11 12:13 1

Carbon tetrachloride <1.0 1.0 ugIL 07)29/11 12:13 1

Chlorobenzene <1.0 1.0 ug/L 07)29/11 12:13 1

2-Chloro-1,3-butadiene <1.0 1.0 ugIL 07/29111 12:13 1

Chloroethane <1.0 1.0 ug/L 07I29/11 12:13 1

Chloroform <1.0 1.0 ugIL 07/29/11 12.13 1

Chloromelhane <1.0 1.0 ug)L 07)29/11 12:13 1

3-Chloro-1-propene <1.0 1.0 ug/L 07/29/11 12:13 1

Chlorodibromomelhane <1.0 1.0 ug/L 07/29/11 12:13 1

1,2-Dibromo-3-Chloropropane <1.0 1 0 ug/L 07)29/11 12:13 1

O Ethylene Dibromide <1.0 1.0 ug/L 07129/11 1213 1

Dibromomethane <1.0 1 0 ugIL 07/29/11 12:13 1

trans-1,4-Dichloro-2-butene <2.0 2.0 ug/L 07129/11 12:13 1

Dichlorodifluoromethane <1.0 1 0 ug/L 07/29/11 12:13 1

1,1-Dichloroethane <1.0 1.0 ug/L 07/29/11 12:13 1

1,2-Dichloroethane <1.0 1 0 ug/L 07/29/11 12:13 1

cis-1,2-Dichloroethene <1 0 1 0 ug/L 07/29)11 12:13 1

trans-1,2-ljichloroethene <1 0 1 0 ug/L 07/29/11 12:13 1

1,1-Dichloroethene <1.0 1.0 ug/L 07/29/11 12:13 1

1,2-Dichloropropane <1.0 1.0 ug/L 07/29/11 12:13 1

cjs-1,3-Dichloropropene <1.0 1 0 ug/L 07/29/11 1213 1

trans-1,3-Dichloropropene <1 0 1.0 ug/L 07/29/11 12:13 1

Ethylbenzene <1 0 1 0 ug/L 07/29/11 1213 1

Ethyl methacrylate <1.0 1.0 ugiL 07/29/11 12.13 1

2-Hexanone <10 10 ug/L 07/29/11 12:13 1

lodomelhane <50 50 ug/L 07/29/11 12:13 1

Isobutyl alcohol <40 40 ug/L 07/29/11 12.13 1

Methacrylonitrile <20 20 ug/L 07/29/11 1213 1

Methylene Chloride <5.0 5.0 ug/L 07/29/11 12:13 1

Methyl methacrylate <1.0 1.0 ug/L 07/29/11 12 13 1

4-Methyl-2-pentanone(MIBK) <10 10 ug/L 07/29/11 1213 1

Pentachloroethane <5.0 50 ug/L 07/29/11 12:13 1

Propionitrile <20 20 ug/L 07/29/11 12 13 1

Styrene <1.0 1.0 ug/L 07/29/11 1213 1

11,1,2-Tetrachloroethane <1 0 1 0 ug/L 07/29/11 12.13 1

11,2,2-Tetrachloroethane <1 0 1 0 ug/L 07/29/11 1213 1

Tetrachloroethene <1 0 1 0 ug/L 07/29/11 12:13 1

Toluene <1.0 1.0 ugIL 07/29(11 1213 1

1,1,1-Trichloroethane <1 0 1 0 ugIL 07/29/11 1213 1

1,1,2-Trichloroetharre <1.0 1 0 ug/L 07)29)11 1213 1


of 92

QC Sample ResultsClient: Ashland Inc.Project/Site: Hercules Hattiesburg APIX 7/26/11

Method: 826DB - Volatile Organic Compounds (GCIMS) (Continued)

Lab Sample ID: MB 680-210523)13

Matrix: Water


Analyte Result

Trichloroethene <1.0

Trichlorofluoromethane <1.0

12,3-Trichloropropane <1 0

Vinyl acetate <2 0

Vinyl chloride <1.0

Xylenes. Total <2.0

MB MB

Surrogate % Recovei’y

4-Bromofluorobenzene 101

Dibromofluoromethane 104

Toluene-d8 (Surr) 99

Client Sample ID: Method Blank

Prep Type: TotailNA

Analyzed

07129/11 1213

07/29/11 12:13

07/29/11 12.13

07/29/11 12:13

07/29/11 12.13

07/29/11 12:13


07/29/11 12.13 1

07/29/Il 12:13 1

07/29/11 1213 1


0


Qualifier RL

1.0

1.0

10

2.0

1.0

20

Qualifier Limits

70- 130

70 130

70 130

MDL Unit D Prepared

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

-oDFac

1

1 ‘- -

0

Lab Sample ID: LCS 680-210523)10 Client Sample ID: Lab Control Sample


Analysis Batch: 210523Spike LCS Lcs % Rec.

Analyte Added Result Qualifier Unit D % Rec Limits

Acetone 100 129 ug/L 129 26.180

, Benzene 500 464 ug/L 93 70.130

Dichiorobromomelhane 500 42.5 ug/L 85 70- 130

Bromoforrn 50.0 33.4 * ug/L 67 70- 130

Bromomethane 50.0 24.6 ug/L 49 23 165

2-Butanone (MEK) 100 106 ug/L 106 49 172

Carbon disulfide 50.0 46.7 ug/L 93 54 132

Carbon tetrachloride 50.0 36.9 ug/L 74 70 130

Chlorobenzene 500 48.6 ug/L 97 70. 130

Chloroethane 500 49.2 ug/L 98 56. 152

Chloroform 500 49.9 ug/L 100 70. 130

Chloromethane 50.0 53.7 ug/L 107 70- 130

Chlorodibromomethane 500 39.3 ug/L 79 70. 130

1 ,2-Dibromo-3-Chloropropane 500 33.5 ug/L 67 70. 130

Ethylene Dibromide 50 0 49 7 ug/L 99 70. 130

Dibromomethane 500 492 ug/L 98 70. 130

Dichlorodifluoromethane 500 51 0 ug/L 102 44- 146

1.1-Dichloroethane 500 486 ugiL 97 70. 130

1,2-Dichloroelhane 500 482 ug/L 96 70. 130

cis-1,2-Dichloroelhene 50.0 49.8 ug/L 100 70. 130

trans-1,2-Dichloroethene 500 499 <gIL 100 70- 130

1,1-Dichioroethene 500 51 1 ugIL 102 66 131

1 ,2-Dichloropropane 500 45 9 ug/L 92 70. 130

cis-1,3-Dichloropropene 500 444 ug/L 89 70. 130

trans-i ,3-Dichioropropene 50.0 430 ugiL 86 70. 130

Ethylbenzene 50.0 46.0 ug/L 92 70- 130

2-Hexanone 100 107 <gIL 107 42. 185

Methylene Chloride 500 504 ug/L 101 67 130

4-Methyl-2-pentanone (MIBK) 100 91.1 ugIL 91 70- 130

Styrene 500 49 7 ugIL 99 70 130

1,1,1,2-Telrachioroethane 500 405 <gIL 81 70- 130

i,1,2,2-Telrachloroethane 50.0 469 ug/L 94 70 130

of 92



Method: 82608 -Volatile Organic Compounds (GCIMS) (Continued) -

Lab Sample ID: LCS 680-210523/10 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: TotalINA

Analysis Batch: 210523Spike LCS LIDS % Rec.

Analyte____________________

___________

- Added Result Qualifier Unit 0 %Rec Limits

Tetrachloroethene 50.0 502 ugiL 100 70.130

Toluene 500 46.9 uglL 94 70-130

1i,1-Tdchloroelhane 500 43.9 ugIL 88 70- 130

1,12-Trichloroethane 500 480 ugiL 96 70-130

Trichloroethene 500 49.1 ugIL 98 70- 130

Trichlorofluoromethane 50.0 51.0 ug/L 102 55 156

1,2,3-Trichloropropane 500 47.8 ugiL 96 70. 130

Vinyl acetate 100 94.0 ug/L 94 60. 176

Vinyl chloride 500 50.7 uglL 101 67 134

Xylenes, Total 150 144 ugIL 96 70-130

LCS LCS


4-Bromofluombenzene 96 70- 130

Dibromofluoromethane 104 70 130

Toluene-d8 (Surr) 98 70- 130

Lab Sample ID: LCSD 680-210523/11 Client Sample ID: Lab Control Sample Dup


Analysis Batch: 210523Spike LCSD LCSD % Rec. RPD

Analyte Added Result Qualifier Unit U % Rec Limits RPO Limit

Acetone 100 135 ug/L 135 26-180 4 50

Benzene 500 51.7 ugIL 103 70-130 11 30

Dichlorobromomethane 50.0 486 ug/L 97 70. 130 13 30

Bromoform 500 38.1 ugIL 76 70-130 13 30

Bromomethane 50 0 35 2 ugIL 70 23- 165 35 50

2-Butanone(MEK) 100 115 ug/L 115 49. 172 8 30

Carbon ctisulfide 50.0 49.9 ugiL 100 54.. 132 7 30

Carbon tetrachloride 50.0 42.6 uglL 85 70-130 14 30

Chlorobenzene 500 53 0 jgIL 106 70- 130 9 30

Chloroethane 500 548 ugIL 110 56. 152 11 40

Chloroform 500 545 ug/L 109 70. 130 9 30

Chloromethane 500 56.8 ug/L 114 70- 130 6 30

Chlorodbromomethane 500 427 ug/L 85 70. 130 8 50

1,2-Dibromo-3-Chloropropane 500 387 ug/L 77 70-130 14 50

Ethylene Dibromide 500 552 ug/L 110 70- 130 10 30

Dibromornelhane 500 544 uq/L 109 70. 130 10 30

Dchlorodufluoromelhane 500 550 ug/L 110 44. 146 8 50

1,1-Dichloroethane 500 525 ug/L 105 70. 130 8 30

1,2-Dichloroethane 500 52.8 ug/L 106 70-130 9 30

cis-1,2-Dichloroethene 500 550 ugIL 110 70-130 10 30

trans-i ,2-Dichloroelhene 500 53.0 ug/L 106 70. 130 6 30

i,1-Dichloroethene 500 556 ugIL iii 66- 131 8 30

i,2.Dichloropropane 500 51 5 ugIL 103 70. 130 12 30

cis-1,3-Dichloropropene 500 488 ugIL 98 70- 130 9 30

trans-i ,3-Dichloropropene 500 47 9 ugIL 96 70. 130 11 50

Ethylbenzene 50 0 51 3 ugiL 103 70- 130 ii 30

2-Hexanone 100 115 ugfL 115 42. 185 7 30

Methylene Chloride 500 54 6 ugIL 109 67 - 130 8 30


of 92

QC Sample ResultsClient: Ashland Inc. TestAmerica Job ID: 680-70758-1Project/Site: Hercules Hattiesburg APIX 7/26/11

Method 8260B- Volatile Organic Compounds (GCIMS)(Contmued) -- C

Lab Sample ID: LCSD 680-21 0523111 Client Sample ID: Lab Control Sample Dup

Matrix: Water Prep Type: TotaIINA

Analysis Batch: 210523Spike LCSD LCSD % Ret. RPD

Analyte —- Added Result Qualifler Unit D % Ret Limits RPD Limit

4-Methyl-2-pentanone(MIBK) 100 103 — ug/L 103 70. 130 12 30 ., .

Styrene 500 549 ugIL 110 70130 10 30

1 ,1,1,2-Tetrachloroethane 500 458 ug/L 92 70- 130 12 30

1,1 22-Tetrachloroethane 500 51.5 ugiL 103 70_ 130 9 30

Tetrachloroethene 500 53 6 uglL 107 70. 130 7 30 I. -

Toluene 500 513 ugIL 103 70. 130 9 30

11,1-Tnchloroethane 500 504 ug/L 101 70- 130 14 30

1,12-Tnchloroethane 50.0 533 ugIL 107 70-130 10 30

Tnchloroethene 500 546 ug/L 109 70.130 11 30

Tnchlorofluoromethane 50 0 556 ugIL 111 55.. 156 9 30

123-Tnchloropropane 500 531 ugIL 106 70. 130 11 30

Vinyl acetate 100 100 ugIL 100 60- 176 6 30

Vinyl chlonde 500 55.0 uglL 110 67- 134 8 30

Xylenes, Total 150 159 ugIL 106 70.130 10 30

LCSD LCSD

Surrogate % Recoverj Qualifier Limits

4-Bromofluorobenzene 107 — 70. 130

D,Liromofluoromethane 112 70- 130

Toluene-dS(Surr) 106 70- 130

Lab Sample ID: MB 680-21054317 Client Sample ID: Method Blank



Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac

Acetone <25 25 ug/L 07130/11 0043 1

Aceton4nle <40 40 ug/L 07/30/11 0043 1

Acrolein <20 20 ug/L 07/30/11 0043 1

Acrylonitnle <20 20 ug/L 07/30/11 0043 1

Benzene <1 0 10 ug/L 07/30/11 0043 1

Dichlorobromomethane <1 0 1 0 ugIL 07/30/11 0043 1

Bromoform <1 0 1 0 ug/L 07/30/11 0043 1

Bromomethane <1 0 1 0 ugIL 07/30/11 0043 1

2-Bulanone (MEK) <10 10 ugIL 07/30/11 0043 1

Carbon disulfide <2 0 20 uglL 07/30/11 0043 1

Carbon telrachioride <1 0 1 0 ugIL 07/30/11 0043 1

Chlorobenzene <1 0 10 ug/L 07/30/11 0043 1

2-Chloro-1,3 butadierie <1 0 1 0 ug/L 07/30/11 0043 1

Chloroethane <1 0 1 0 ug/L 07/30/11 0043 1

Chloroform rl 0 1 0 ugIL 07/30/11 0043 1

Chloromethane <1 0 1 0 ugIL 07/30/11 0043 1

3-Chloro-i-propene <1 0 1 0 ug/L 07/30/11 0043 1

Chlorodibromomethane 1 0 1 0 ug/L 07/30/11 0043 1

1,2-Dibromo-3-Chloropropane 1 0 1 0 ug/L 07/30/11 0043 1

Ethylene Dibromide <1 0 1 0 ug/L 07/30/11 00 43 1

Dibromomethane <1 0 1 0 ug/L 07/30/11 0043 1

trans-i ,4-Dichloro-2-butene <2 0 2 0 ug/L 07/30/11 0043 1

Dichlorodifluoromelhane <1 0 1 0 ug/L 07/30/11 0043 1

I 1-Dichioroethane 1 0 1 0 ugIL 07/30/11 0043 1 0TestAmerica Savannah

of 92

QC Sample ResultsClient: Ashland Inc TestAmerica Job ID: 680-70758-1


.

. .-

ethod: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: MB 680-21054317 Client Sample ID: Method Blank



Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Dii Fac

i,2-Dichloroelhane <1.0 1 0 ug/L 07/30111 00:43 1

cjs-1,2-Dichloroethene <1.0 1 0 ug/L 07/30/11 00:43 1

trans-i 2-Dichloroethene <1.0 1.0 ug/L 07/30/11 00:43 1

1l-Dichloroethene <1 0 1.0 ug/L 07/30/11 00:43 1

12-Dichioropropane <1.0 1 0 ug/L 07/30/11 0043 1

cis-13-Dichloropropene <1.0 1.0 ug/L 07/30/11 00:43 1

trans-i.3-Dlchloropropene <1,0 1 0 ug/L 07/30/11 00:43 1

Ethylbenzene <1.0 1.0 ug/L 07/30/11 00:43 1‘<4:,-

Ethyl methacrylate <1,0 1.0 ug/L 07/30/11 00:43 1

2-Hexanone <10 10 ug/L 07/30/11 00:43 1

lodomethane <50 5.0 ugIL 07/30/11 0043 1

Isobutyl alcohol <40 40 ug/L 07/30/li 00:43 1

Methacrylonitrile <20 20 ug/L 07/30/11 00:43

Methylene Chloride <5.0 5.0 ug/L 07/30/li 00:43

Methyl melhacrylate <1 0 1 0 ug/L 07/30/11 00:43 1

4-Methyt-2-penlanone (MIBK) <10 10 ug/L 07/30/11 00:43

Pentachloroethane <5.0 5.0 ug/L 07/30/11 00:43 1

Propionitnle <20 20 ugIL 07/30/il 00:43 1

Styrene <1.0 1 0 ug/L 07/30/il 00:43

O1ii2-Tetrachloroethane <1.0 1 0 uglL 07/30/11 00:43 1

1i22-Telrachloroethane <1.0 1 0 ug/L 07/30/il 00.43 1

Telrachloroethene <1.0 1 0 ug/L 07/30/il 00:43 1

Toluene <1.0 1 0 ug/L 07/30/li 00:43 1

ill-Trichloroethane <1.0 1 0 ugIL 07/30/11 00:43 1

1,l,2-Trichloroelhane <1 0 1.0 ug/L 07/30/il 00,43

Trichloroethene <1 0 1 0 ugiL 07/30/11 00:43

Trichlorofluoromethane <1 0 1 0 ug/L 07130/il 00:43 1

i,23-Trichloropropane <1.0 1 0 ug/L 07/30/11 00,43 1

Vinyl acetate <20 20 ugIL 07/30/il 00:43 1

Vinyl chloride <1 0 1.0 ugIL 07/30/li 00:43 1

Xylenes, Total <2.0 20 ug/L 07/30/11 00.43 1

MB MB

Surrogate % Recovery Qualifier Lim/ts Prepared Analyzed Dii Faa

4-Brornof!uorobenzene 93 70- 130 07/30/I 1 00:43 1

Dibromofiuoromethane 107 70- 130 07/30/11 00,43 1

Toluene-d8 (Surr) 100 70. 130 07/30/11 00,43 1



Analysis Batch: 210543Spike LCS LCS % Ret.

Analyte Added Result Qualifier Unit 0 % Rec Limits

Acetone 100 129 ugfL 129 26-180

Benzene 50 0 50 0 ug/L 100 70 130

Dichlorobromomethane 500 463 ug/L 93 70 130

Bromoform 50.0 381 ug/L 76 70- 130

Bromornethane 50 0 25 4 U9/L 51 23. 165

2-Butanor.e (MEK) 100 111 uglL 111 49 - 172

\.)Carbon disullide 500 480 iig/L 96 54 132


o192

Lab Sample ID: LCSD 680-21 054315

Matrix: Water

Analysis Batch: 210543

Analyte

Acetone

Oenzene

Dichiorobromomethane

LCSD LCSD

Result Qualifier

131

48 4

466

Client Sample ID: Lab Control Sample Dup

Prep Type: Total/NA

%Rec. RPD


QC Sample ResultsClient: Ashland IncProject/Site: Hercules Hattiesburg APIX 7/26/11

Method: 826DB -Volatile Organic Compounds (GCIMS) (Continued)

Lab Sample ID: LCS 680-210543/4

Matrix: WaterAnalysis Batch: 210543


Client Sample ID: Lab Control SamplePrep Type: Total/NA

Spike LCS LCS % Rec.

Analyte Added Result Qualifier unit o % Rec Limits

Carbon tetrachloride 50.0 41.3 ugIL 83 70. 130

Chlorobenzene 500 52.5 ug/L 105 70- 130

Chloroethane 500 50.0 ugiL 100 56- 152

Chloroform 50.0 52.0 ugIL 104 70- 130

Chlorometharie 50.0 50.7 ugIL 101 70. 130

Chlorodibromomethane 500 433 ugIL 87 70- 130

12-Dibromo-3-Chloropropane 500 41.0 uglL 82 70- 130

Ethylene Dibromide 500 496 ugIL 99 70- 130

Dibromomethane 50.0 51.6 ugiL 103 70. 130

Dichlorodifluoromethane 50.0 49.9 ugIL 100 44. 146

11-Dichloroethane 50.0 49.8 ugIL 100 70- 130

1,2-Dichtoroethane 50.0 50.7 ugIL 101 70. 130

cia-i 2-Dichloroethene 50.0 51.7 ug/L 103 70. 130

trans-1,2-Dichloroethene 50.0 51.5 ugIL 103 70. 130

li-Dichloroethene 50.0 52.0 ugIL 104 66- 131

1 2-Dichloroproparre 50.0 49.4 ugIL 99 70- 130

cis-i3-Dichloropropene 50.0 45.8 ugIL 92 70- 130

trans-i ,3-Dichloropropene 50.0 43.9 ugiL 88 70 - 130

Ethylbenzene 50.0 51.1 ugIL 102 70. 130

2-Hexanone 100 114 ugIL 114 42.185

Methylene Chloride 50.0 53.2 ugiL 106 67- 130

4-Methyl-2.pentanone (MIBK) 100 94.4 ugIL 94 70. 130

Styrene 50.0 543 ugIL 109 70- 130

i,1,i,2-Tetrachloroethane 50.0 46.0 ugIL 92 70. 130

1,12,2-Tetrachloroethane 50.0 51.3 ugIL 103 70. 130

Tetrachloroethene 50.0 54.7 ugIL 109 70- 130

Toluene 500 48.5 UQIL 97 70.130

1,1,1-Trichloroethane 50.0 47.9 ug/L 96 70- 130

i,12-Tnchloroethane 50.0 48.9 ugIL 98 70. 130

Trichloroethene 500 532 ugIL 106 70 130

Trichlorolluoromethane 50 0 52.1 ugIL 104 55- 156

12,3-Tnchloroproparre 50.0 534 ugIL 107 70. 130

Vinyl acetate 100 95.3 ugJL 95 60. 176

Vinyl chloride 50.0 50.8 ug/L 102 67. 134

Xylenes. Total 150 159 uglL 106 70 130

LCS LCS


4-Bromofluorobenzene 104 70. 130

Dibromofluoromelhane 08 70. 130

Toluene-d& (Surr) 101 70. 130

Spike

Added

100

50 0

50 0

0

Unit 0 % Rec Limits RPD Limit

ug/L 131 26180 1 50

uglL 97 70 130 3 30

ug/L 93 70- 130 1 30

of 92


(5roiect/Site. Hercules Hattiesburg APIX 7/26/11





Analyte Added Result Qualifier Unit 0 % Rec Limits RPD Limit

Bromoform 50.0 38.7 ug/L 77 70.130 2 30

Bromomethane 50.0 24.5 ug/L 49 23- 165 4 50

2-Butanone(MEK) 100 111 uglL 111 49-172 0 30

Carbon disulfide 500 44.8 ug/L 90 54. 132 7 30

Carbon tetrachloride 500 402 ugIL 80 70. 130 3 30

Chlorobenzene 500 51.2 uglL 102 70- 130 3 30

Chloroethane 500 386 ug/L 77 56- 152 26 40

Chloroform 50.0 49.8 ugiL 100 70-130 4 30

Chloromethane 50.0 48.1 ug!L 96 70.130 5 30

Chlorodibromomethane 50.0 42.6 ug/L 85 70.130 2 50

1,2-Dibromo-3-Chloropropane 50.0 39.3 ugiL 79 70.130 4 50

Ethylene Dibromide 50.0 524 uglL 105 70. 130 6 30

Dibromornethane . 50.0 52.1 ugiL 104 70.130 1 30

Dichlorodifluoromethane 50.0 46.8 ug/L 94 44.146 6 50

1,1-Dichloroethane 50.0 468 ug/L 94 70-130 6 30

1,2-Dichloroethane 500 50.8 uglL 102 70. 130 0 30

cis-1,2-Dichloroethene 50.0 497 ugIL 99 70-130 4 30

trans-i ,2-Dichloroethene 50.0 488 ugIL 98 70.130 5 30

1,1-Dichloroethene 50.0 49.4 ug/L 99 66.131 5 30

1,2-Dichloropropane 50.0 48.7 ugIL 97 70.130 2 30

cis-i,3-Dichloropropene 50.0 465 ugIL 93 70. 130 2 30

trans-i ,3-Dichloropropene 50.0 455 ug/L 91 70.130 4 50

Ethylbenzene 50.0 480 U9IL 96 70-130 6 30

2-Hexanone 100 112 ug!L 112 42. 185 2 30

Methylene Chloride 50.0 508 ugIL 102 67.130 5 30

4-Methyl-2-pentanone(MIBK) 100 98.5 ug/L 98 70.130 4 30

Styrene 50 0 53 6 ug/L 107 70. 130 1 30

1,11,2-Tetrachloroethane 500 448 ug/L 90 70. 130 3 30

1,i,2,2-Tetrachloroethane 50.0 509 ug/L 102 70. 130 1 30

Tetrachloroethene 50.0 51 6 ug/L 103 70. 130 6 30

Toluene 50 0 49.1 ugIL 98 70- 130 1 30

I ,i,1-Trichloroethane 50.0 467 ug/L 93 70- 130 3 30

1,i,2-Trichloroethane 50.0 51 6 ugIL 103 70.130 6 30

Trichloroethene 500 505 ug/L 101 70. 130 5 30

Trichlorofluoromethane 500 48 3 ug/L 97 55 156 8 30

1,2,3-Trichloropropane 500 533 ugIL 107 70-130 0 30

Vinyl acetate 100 943 ug/L 94 SQ. 176 1 30

Vinyl choride 500 47 8 ugIL 96 67. 134 6 30

Xylenes, Total 150 153 ug/L 102 70. 130 4 30

LCSD LCSD



Dibromofluoromethane 103 70- 130

Toluene-d8 (Surr) 101 70 - 130


of 92

QC Sample ResultsClient: Ashland Inc TestAmerica Job ID 680-70758-1


Method 8260B Volatile Organic Compounds (GCIMS) (Continued) (DLab Sample ID: MB 680-210665111 Client Sample ID: Method Blank



Analyte Result Qualifier RL MDL unit 0 Prepared Analyzed Dii Fac

Acetone <2 25 ug/L 07/30/11 14.10 1

Acetonitrile <40 40 ug/L 07)30/11 14.10 1

Acrolein <20 20 ugiL 07/30111 14 10 1

Acrylonitrile <20 20 ug/L 07)30/11 14 10 1

Benzene <I 0 1 0 ug/L 07/3011114 10 1

Dichlorobromomethane <1.0 1 0 ug/L 07/30/11 14 10 1

Brornoform <1 0 1 0 ugiL 07/30/11 14 10 1

Bromomelhane <1 0 1.0 ugiL 07130/11 1410 1

2-Butanone (MEK) <10 10 ug/L 07/30/1114 10 1

Carbon disulfide <2.0 20 ug!L 07/30/11 14 10 1

Carbon letrachloride <1 0 1 0 ug)L 07/30/1114:10 1

Chtorobenzene <1.0 1.0 ug/L 07/30/11 14.10 1

2-Cliloro-1,3-butadiene <1.0 1.0 ugIL 07/30)11 1410 1

Chloroethane <1.0 1 0 ugIL 07/30/11 14 10 1

Chloroform <1 0 1.0 ug)L 07)30/11 14 10 1

Chioromelhane <1.0 1.0 ug/L 07/30/11 1410 1

3-Chloro-1-propene <1.0 1.0 ug/L 07/30/11 1410 1

Chlorodibromomethane <1 0 1 0 ug)L 07130/11 1410 1

12-Dibromo-3-Chloropropane <1 0 1.0 ugIL 07/30111 1410 1

Ethylene 0/bromide <1 0 1 0 ug/L 07/30111 14 10 1

Dibromomethane <1.0 1,0 ugIL 07/30/11 1410 1

trans-1,4-Dichloro-2-butene <20 2,0 ugIL 07/30)11 14 10 1

Dichlorodifluoromethane <1 0 1 0 vg/L 07/30)1114 10 1

11-D,chloroelhane <1 0 1.0 ug/L 07/30/11 1410 1

1,2-Dichloroethane <1 0 1.0 ut/L 07/30/11 14 10 1

c/s-i ,2-Dichloroethene <1 0 1 0 ugIL 07/30)11 1410 1

lrans-1,2-Dichloroethene <1.0 1 0 ug/L 07/30/11 14 10 1

1,1-Dichloroethene <1 0 1.0 ug/L 07/30/11 1410 1

1,2-Dichloropropane <1 0 1 0 ug/L 07)30/11 1410 1

cis-1,3-Dichloropropene <1.0 1.0 ug/L 07/30)11 14 10 1

trans-1,3-Dichloropropene <1 0 1 0 ug/L 07/30/111410 1

Elhylbenzene 1 0 1 0 ug/L 07/30)11 14 10 1

Ethyl methacrylate <1 0 1 0 ug/L 07)30/11 14 10 1

2-Hexanone <10 10 ug/L 07/30/11 14 10 1

Iodomelharre <50 5.0 ug)L 07/30/11 1410 1


Methacrylonilnle <20 20 ug/L 07/30/1114 0 1

Methylene Chloride <50 50 ug/L 07/30/11 14 10 1

Methyl melhacrylate <1 0 1 0 ug/L 07/30/11 1410 1

4-Melhyl.2-penlanone (MIBK) <10 10 ugIL 07)30/11 14 10 1

Penlachloroetharre <50 50 ug/L 07/30/11 14 10 1

Propionitrile <20 20 ug/L 07/30/1114 10 1

Styrene <1 0 1 0 ug/L 07)30/11 14 10 1

1 .1,1 ,2-Tetrachloroethane <1 0 1 0 ugIL 07/30)11 14 10

1,1,2,2-Tetrachtoroelhane <I 0 1 0 ug/L 07/30/lI 14 10 1

Telrachioroethene <1 0 1.0 ug/L 07/30/11 14 10 1

Toluene <1 0 1 0 ug/L 07/30/1114 0 1

1,1,1-Tnchloroelhane <1 0 1 0 ug/L 07/30111 14 10 1

11,2-Tdchloroelhane <1 0 1 0 ugIL 07/30/11 14 1010


of 92



- ethod: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

_______

Lab Sample ID: MB 680-210665111Matrix: WaterAnalysis Batch: 210665

Surrogate

4-Bromofluorobenzene

Dibromofluoromethane

Toluene-dO (Surr)

ugIL

ugIL

ugIL

ugIL

ug/L

Prepared Analyzed — Dii Fac

07/30/11 14:10 1

07/30/11 14:10 1

07/30/11 14:10 1


MB MB

Analyte Result

Trichloroethene <1.0

Thchlorofluoromethane <1.0

I 23-Trichloropropane <1.0

Vinyl acetate <2.0

Vinyl chloride <1.0

Xylenes Total <2.0

MB

Client Sample ID: Method BlankPrep Type: TotalINA

MDL unit o Prepared

ugIL

Qualifier RL

1.0

1.0

1.0

2.0

1.0

2.0

MB

Qualifier Limits

70- 130

% Recovery

103

Analyzed

07130/il 14:10

07/30/11 14:10

07/30/11 14:10

07/30/11 14:10

07/30/11 14:10

07/30/11 14:10

Dil Fac

103 70. 130

102 70-130

Lab Sample ID: LCS 680-210665/8 Client Sample ID: Lab Control SampleMatrix: Water Prep Type: Total/NAAnalysis Batch: 210665



Acetone 100 118 — ug/L — 118 26- 180

Benzene 50.0 43.6 ug/L 87 70. 130

ODichlorobromomethane 500 38.7 ugIL 77 70_i 30

Bromoform 50.0 306 * ug/L 61 70. 130

Bromomethane 500 384 ug/L 77 23. 165

2-Butanone (MEK) 100 101 ug/L 101 49. 172

Carbon disulfide 50.0 44.4 ugIL 89 54. 132

Carbon tetrachloride 50.0 31.7 * ug/L 63 70. 130

Chlorobenzene 500 47.2 ugIL 94 70- 130

Chloroethane 50.0 47.2 ugIL 94 56. 152

Chloroform 50.0 43.4 ugIL 87 70. 130

Chloromethane 50.0 53.9 ug/L 108 70. 130

Chlorodibromomethane 50.0 34.5 uglL 69 70- 130

12-Dibromo-3-Chloropropane 50.0 403 ug/L 81 70. 130

Ethylene Dibromide 500 45.9 ug/L 92 70- 130

Dibromomethane 50.0 43.8 ug/L 88 70. 130

Dichlorodifluoromethane 500 49 1 Ug/L 98 44 146

il-Dichloroethane 500 41.8 ug/L 84 70- 130

1 ,2-Dichloroethane 50.0 425 uglL 85 70. 130

cis-1 ,2-Dichloroethene 50 0 43.3 ugIL 87 70. 130

trans-1,2-Dichloroethene 50.0 430 ugIL 86 70. 130

1,1-Dichloroethene 50.0 436 ug/L 87 66- 131

1,2-Dichloropropane 50.0 422 ugIL 84 70- 130

cis-1,3-Dichloropropene 50.0 39.6 ug/L 79 70- 130

trans-13-Dichloropropene 50.0 397 ug/L 79 70. 130

Ethylbenzene 50.0 43.8 ug/L 88 70- 130

2-Hexanone 100 937 ug/L 94 42. 185

Methylene Chloride 500 46 1 ugIL 92 67- 130

4-Methyl-2-pentanone (MIBK) 100 883 ugIL 88 70- 130

Slyrene 50.0 46.5 ug/L 93 70. 130

1 1 1.2-Telrachloroethane 50.0 37.4 ugfL 75 70. 130

1,1,2,2-Tetrachloroelhane 50.0 464 ugIL 93 70. 130

of 92

QC Sample ResultsClient: Ashland Inc TestAmerica Job ID 680-70758-1 JIj

Project/Site. Hercules Hattiesburg APIX 7/26/11

Method: 8260B - Volatile Organic Compounds (GCIMS) (Continued) C)Lab Sample ID: LCS 680-210665/8 Client Sample ID: Lab Control Sample


Analysis Batch: 210665Spike Lcs Lcs % Rec.

Analyte Added Result Qualifier unit D % Rec Limits

Tetrachloroethene 500 45 1 uglL 90 70 130

Toluene 500 44 2 ugIL 88 70- 130

111-Tnchloroethane 500 398 uglL 80 70- 130

1 1,2-Tnchloroethane 500 446 uglL 89 70- 130

Tnchloroethene 500 436 ug/L 87 70- 130

Tnchlorofluoromethane 500 460 ugIL 92 55- 156

1 2,3-Tnchloropropane 500 47 1 uglL 94 71L 130

Vinyl acetate 100 832 uglL 83 60 176

Vinyl chlonde 500 468 ugIL 94 67_ 134

Xylenes, Total 150 136 uglL 90 70-130

LCS LCS


4-Bromofluorobenzene 92 70- 130


Toluene-d8 (Surr) 92 70- 130

Lab Sample ID: LCSD 680-21 066519 Client Sample ID: Lab Control Sample DUP


Analysis Batch: 210665Spike LcSD LCSD % Rec. RPD

Analyte-

Added Result Qualifier Unit 0 % Rec Limits RPD Limit

Acetone 100 130 ugIL 130 26.180 10 50

Benzene 500 506 ugIL 101 70-130 15 30

Dichlorobromomethane 50 0 474 ugIL 95 70- 130 20 30

Bromoform 500 406 ug/L 81 70 130 28 30

Brorriomethane 500 423 Ug/L 85 23- 165 10 50

2-flutanone (MEK) 100 120 uglL 120 49 172 17 30

Carbon disulfide 500 51 4 ug!L 103 54 132 15 30

Carbon tetrachloride 500 39 5 ugIL 79 70- 130 22 30

Chlorobenzene 50 0 564 UgIL 113 70 130 18 30

Chloroethane 50 0 55 3 ug/L 111 56 - 152 16 40

Chloroform 500 527 ug/L 105 70- 130 19 30

Chloromethane 50 0 626 ugIL 125 70- 130 15 30

Chlorodibromomethane 500 456 ugfL 91 70- 130 28 50

1.2-Drbromo-3-Chloropropane 500 501 ugiL 100 70- 130 22 50

Ethylene Dibromide 500 548 ugIL 110 70- 130 18 30

Dibromomathane 50 0 53 6 ug/L 107 70- 130 20 30

Dichlorodifluoromethane 500 553 ugIL 111 44 146 12 50

1,1-Dichloroethane 500 511 ug/L 102 70- 130 20 30

1,2-Dichloroethane 500 498 ug/L 100 70- 130 16 30

cs-i 2-Dichioroethene 500 522 ugIL 104 70 130 19 30

trans-I ,2-Dichloroethene 500 514 uglL 103 70 130 18 30

1,1-Dichloroethene 500 531 ug/L 106 66 131 20 30

1 ,2-Dichloropropane 500 509 ugIL 102 70- 130 19 30

cis-1 3-Dichloropropene 500 484 ug/L 97 70. 130 20 30

trans-i 3-Dichloropropene 50 0 47 9 ugfL 96 70 - 130 19 50

Ethylbenzene 500 536 ugIL 107 70- 130 20 30

2-Hexanorie 100 113 uglL 113 42.185 19 30

Methylene Chloride 500 529 ug/L 106 67 130 14 30Q

TestAmerlca Savannah

of 92



Method: 826DB - Volatile Organic Compounds (GCIMS) (Continued)

Lab Sample ID: LCSD 680-21 066519 Client Sample ID: Lab Control Sample DupMatrix: Water Prep Type: TotalINAAnalysis Batch: 210665

Spike LCSD LCSD %Rec. RPD

AnalySe Added Result Qualifier Unit D % Rec Limits RPD Limit

4-Methyt-2-pentanone (MIBK) 100 101 ugIL 101 70.. 130 14 30

Styrene 50.0 55.7 ug/1 111 70-130 18 30

1,1,1,2-Tetractiloroethane 50.0 48.6 ugiL 97 70. 130 26 30

1,1,2,2-Tetrachloroethane 500 54.8 ugIL 110 70. 130 17 30

Tetrachloroethene 50.0 57.0 ugIL 114 70-130 23 30

Toluene 500 50.5 ugIL 101 70-130 13 30

1,1,1-Trichtoroethane 50.0 48.0 ug/L 96 70.130 19 30

1,1,2-Trichloroethane 50.0 52.2 UgIL 104 70.. 130 16 30

Trichloroethene 50.0 53.1 ug/L 106 70. 130 20 30

Trichlorofluoromethane 50.0 55.8 ugIL 112 55. 156 19 30

1,2,3-Trichloropropane 50.0 55.4 ug/L 111 70. 130 16 30

Vinyl acetate 100 987 ug/L 99 60. 176 17 30

Vinyl chloride 50.0 54.6 ugIL 109 67. 134 15 30

Xylenes, Total 150 165 ugIL 110 70- 130 20 30

LCSD LCSD



Dibromofluoromethane 109 70. 130

Toluene-d8(Surr 107 70- 130

Oethoth827OC -Semivolatile Organic Compounds (GCIMS)

Lab Sample ID: MB 680-210278/14-A Client Sample ID: Method BlankMatrix: Water Prep Type: Total/NAAnalysis Batch: 210829 Prep Batch: 210278

MB MB

Analyte Result Qualifier RL — MDL Unit D Prepared Analyzed Dii Fac

Acenaphthene — <10 10 ug/L 07/28/11 1442 08/02111 13:33 1

Acenaphthylene <10 10 ug/L 07(28/11 14.42 08/02/11 13:33 1

Acetophenone <10 10 ug/L 07/26/11 14:42 08/02/11 13.33 1

2-Acetylaminofluorene <10 10 ug/L 07/28/11 14:42 08/02/11 13:33 1

alphaalpha-Dimeihyl phenethylamine <2000 2000 ugiL 07/28)11 1442 08/02/11 13:33 1

4-Aminobiphenyl <10 10 ug/L 07/28)11 14:42 08)02/11 13:33 1

Aniline <20 20 ug/L 07/28)11 14.42 08/02/11 13:33 1

Anthracene <10 10 ug/L 07/28/11 1442 08/02/11 13:33 1

Aramite, Total <10 10 ug/L 07/28)11 1442 08/02/11 1333 1

Benzo[a]anthracene <10 10 ug/L 07)28/11 14:42 08/02)11 1333 1

Benzo[a]pyrene <10 10 ug/L 07/28/11 1442 08/02/11 1333 1

Benzo[b]fluoranthene <10 10 ugIL 07/28/11 1442 08/02/11 13.33 1

Benzo[g,h,ijperylene <10 10 ugIL 07/28/11 14:42 08/02)11 13:33 1

Benzo[k]fluoranthene <10 10 ug/L 07/28/11 14:42 08)02/11 13.33 1

Benzyl alcohol <10 10 ug/L 07/28/11 14:42 08/02/11 1333 1

1,1’-Biphenyl <10 10 ug/L 07/28)11 1442 08/02/11 13:33 1

Bis(2-chloroethoxy)metharie <10 10 ugiL 07(28111 1442 08(02)111333

Bis(2-chloroethyl)ether <10 10 ug/L 07/28/11 1442 08)02)11 1333 1

bis(chloroisopropyl) ether <10 10 ug/L 07/28/11 1442 08/02)1113:33 1

QBis(2-ethylhexyl) phthalate <10 10 ug/L 07)28/11 14:42 08/02)11 1333 1

4.Bromophenyl phenyl ether <10 10 ug/L 07/28/11 1442 08/02/11 13.33 1

Butyl benzyl phthalate <10 10 ug/L 07/28/11 1442 08/02/11 1333 1


of 92


Project/Site Hercules Hattiesburg APIX 7)26/11

Method: 8270C - Semivolatile Organic Compounds (GCIMS) (Continued) - (_)Lab Sample ID: MB 680-210278/14-A Client Sample ID: Method Blank


Analysis Batch: 210829 Prep Batch: 210278

MB MB

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac

4-Chtoroaniline <20 20 ugIL 07/28/11 1442 08/02)11 1333 1

4-Chloro-3-methylphenol <10 10 ugIL 07/28/11 1442 08/02111 1333 1

2-Chloronaphthalene <10 10 ug/L 07/28/11 1442 08102111 1333 1

2-Chlorophenol <10 10 ugIL 07/28/11 1442 08/02/11 1333 1


Chrysene <10 10 ug/L 07)28/11 1442 08102)11 1333 1

Diallate <10 10 ug)L 07/28/11 1442 08102/11 1333 1

Dibenz(a,h)anthracene <10 10 ug/L 07/28/11 1442 08102)11 1333 1

Dibenzofuran <10 10 ug/L 07128/11 1442 08/02111 1333 1

1,2-Dichlorobenzene <10 10 ugIL 07/28/11 1442 08/02111 1333 1

13-Dichlorobenzene <10 10 ugIL 07/28111 1442 08102/11 1333 1

1,4-Dichtorobenzene <10 10 ug/L 07/28/11 1442 08/02/11 1333 1

33-Dichlorobenzidine <60 60 ug/L 07/28111 1442 08/02)11 1333 1

24-Dichlorophenol <10 10 ug)L 07/28/11 1442 08/02)111333 1

26-Dichlorophenol <10 10 ug/L 07)26/11 1442 08/02/11 1333 1

Diethyl phthalate <10 10 ugIL 07/28/11 1442 08/02/11 1333 1

Dimethoate <10 10 ugIL 07/28/11 1442 08/02/11 1333 1

7, 12-Dimethytbenz(a)anthracene <10 10 ug/L 07/28/11 14 42 08/02/11 13 33 1

33-Dimethylbenzicline <20 20 ugIL 07)28/11 1442 08/02/11 1333 1

24-Dimethylphenol <10 10 ug)L 07/28/11 1442 08/02/11 1333 1

Dimethyl phthalate <10 10 ug/L 07)28/11 1442 08/02/11 1333 1

Di-n-butyl phthalate <10 10 ugIL 07)28/11 1442 08/02/11 1333 1

1,3-Dinitrobenzene <10 10 ug/L 07/28/11 1442 081021111333 1

46-Dinitro-2-methylphenol <50 50 ugIL 07/28/11 1442 08/02)111333 1

24-Dinitrophenol <50 50 ug/L 07/28/11 1442 08/02/11 1333 1

24-Dinitrotoluene <10 10 ug/L 07/28/11 1442 08/02/11 1333 1

26-Dinitrotoluene <10 10 ug/L 07/28)11 1442 08/02/11 1333 1

Di-n-octyl phthalate <10 10 ugIL 07/28/11 1442 08/02/11 1333 1

Dinoseb <10 10 ug)L 07/28/11 1442 08/02)111333 1

14-Dioxane <10 10 ug/L 07/28/11 1442 08/02/11 1333 1

Disulloton <10 10 ugIL 07/28/11 1442 08/02/11 1333 1

Ethyl methanesulfonate <10 10 ug/L 07/28/11 1442 08/02111 1333 1

Ethyl Parathion <10 10 ug/L 07)28/11 1442 08102/111333 1

Famphur <10 10 ug)L 07/28/11 1442 08/02/11 1333 1

Fluoranthene <10 10 ug/L 07/28/111442 08/02/111333 1

Fluorene <10 10 ug/L 07)28/11 1442 08/02/11 1333 1

Hexachlorobenzene <10 10 ugIL 07/28/111442 08/02/11 1333 1

Hexachlorohutadiene <10 10 ug/L 07/28/11 1442 08/02/111333 1

Hexachlorocyclopentadiene <10 10 ug/L 07)28/11 1442 08)02/11 1333 1

Hexachloroethane <10 10 ug/L 07/28/11 1442 08/02/11 1333 1

Hexachlorophene <5000 5000 ug/L 07/28/11 1442 08/02)111333 1

Hexachloropropene <10 10 ug/L 07/28/111442 08/02/111333 1

Indeno[1 23-cd]pyrene <10 10 ugIL 07/28/111442 08)02/111333 1

isophorone <10 10 ug/L 07/28/11 1442 08/02)11 1333 1

Isosafrole <10 10 ug/L 07/28/1 1442 08/02/11 1333 1

Methapynlene <2000 2000 ug/L 07/28/11 1442 08/02/11 1333 1

3-Methylcholanthrene <10 10 ugiL 07)28)111442 08102/111333 1

Methyl methanesulfonate <10 10 ug/L 07/28/11 14 42 08/02/1113 33 1

2-Methylnaphthalene <10 10 ug/L 07/28/11 1442 08/02/11 1333 1

Methyl parathion <10 10 ug/L 07)28/11 14 42 08/02/11 13 33 1


of 92




Lab Sample ID: MB 680-210278114-A Client Sample ID: Method Blank


Analysis Batch: 210829 Prep Batch: 210278MB MB

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

2-Methylphenol <10 10 ugIL — 07/28111 14:42 08/02111 13:33 1

3&4 Methylphenol <10 10 ugIL 07/28/11 14:42 08/02/11 1333 1

Naphthalene <10 10 ugIL 07/28/11 14:42 08/02/11 13:33 1

1,4-Naphthoquinone <10 10 ugIL 07/28/11 14:42 08102111 13:33 1

1-Naphthylamine <10 10 ug/L 07/28111 14:42 08)02/11 13:33 1

2-Naphthylamine <10 10 ug/L 07/28111 14:42 08/02/11 13:33 1

2-Nitroaniline <50 50 uglL 07/28/11 14:42 08/02/11 13:33 1

3-Nitroaniline <50 50 ug/L 07/28/11 14:42 08/02/1113:33 1

4-Nitroanhline <50 50 ug/L 07/28/11 14:42 08/02/11 1333 1

Nitrobenzene <10 10 ug/L 07/28/11 14:42 08/02/11 13:33 1

2-Nitrophenol <10 10 ug/L 07)28/11 14:42 08/02/11 13:33 1

4-Nitrophenol <50 50 ug)L 07/28/11 14:42 08/0211113:33 1

4-Nitroquinoline-1-oxide <20 20 ug/L 07/28/11 14:42 08/02/1113:33 1

N-Nitro-o-toluidine <10 10 ug/L 07/28/11 14:42 08/0211113:33 1

N-Nilrosodiethylamine <10 10 ug/L 07/28/11 14.42 08/02/11 13:33 1

N-Nitrosodimethylamine <10 10 ug)L 07/28/11 14:42 08/02/11 1333 1

N-Nitrosodi-n-butylamine <10 10 ug/L 07/28/11 14:42 08/0211113:33 1

N-Nilrosodi-n-propylamine <10 10 ug/L 07/28/11 1442 08/02/11 13:33 1

N-Nitrosodiphenylamine <10 10 ug/L 07/28/11 1442 08/02/11 13:33 1

N-Nitrosomethylethylamine <10 10 ug/L 07/28/11 14:42 08/02/11 13:33 1

N-Nitrosomorpholine <10 10 ug/L 07/28/11 14:42 08/02/11 1333 1

N-N/trosopiperidine <10 10 ug/L 07/28/11 14:42 08/02/11 13:33 1

N-Nitrosopyrrolidine <10 10 ug/L 07/28/11 14:42 08/0211113:33 1

o,oo-Triethylphosphorothioate <10 10 ug)L 07/28/11 14:42 08/02/11 1333 1

p-Dimethylaminoazobenzene <10 10 ug/L 07/28/11 14:42 08/02/11 1333 1

Pentachlorobenzene <10 10 ug)L 07/28/11 14:42 08/02/11 13:33 1

Penlachloron,trobenzene <10 10 ig)L 07)28/11 14:42 08102/11 1333

Pentachlorophenol <50 50 ug/L 07)28/11 14:42 08)02/11 13:33 1

Phenacetin <10 10 ug)L 07/28/11 14:42 08/02/11 1333 1

Phenanthrene <10 10 ug/L 07/28/11 14:42 08/02/11 1333 1

Phenol <10 10 ug/L 07/28/11 14:42 08/02/11 13:33 1

Phorate <10 10 ug/L 07/28/11 14:42 08)02/11 1333 1

2-Picoline <10 10 ug/L 07)28/11 14.42 08)02/11 1333 1

p-Phenylene diarnine <2000 2000 ug/L 07/2811114:42 08/02/11 1333 1

Pronamide <10 10 ug/L 07/28)11 1442 08102/111333 1

Pyrene <10 10 ug/L 07/28/11 1442 08/02/11 1333 1

Pyridine <50 50 ug)L 07/28,11 1442 08/02/111333 1

Safrole, Total <10 10 ug)L 07/28/11 1442 08/02)11 1333 1

Sulfolepp <10 10 ug)L 07/28/11 14.42 08/02/11 1333 1

1,2,4,5-Tetrachlorobenzene <10 10 ug)L 07/28)11 1442 08/02/11 1333 1

2,3,4,6-Tetrachlorophenol <10 10 ug)L 07/28/11 14.42 08(02/11 1333 1

Thionazin <10 10 ug)L 07/28)11 1442 08/02/11 13:33 1

2-Toluid,ne <10 10 ug)L 07/28/11 1442 08/021111333 1

1,2,4-Trichlorobenzene <10 10 ug)L 07/281111442 08/02/11 1333 1

2,4.5-Trichlorophenol <10 10 ug/L 07)28/11 1442 08/02/11 1333 1

2.4,6-Thchlorophenol <10 10 ug)L 07)28/11 1442 08/02/11 13:33 1

1,3,5-Trinitrobenzene <10 10 ug/L 07/28/11 14:42 08/02/11 1333 1


of 92



Method: 8270C - Semivolatile Organic Compounds (GcIMS) (Continued)

Lab Sample ID: MB 680-210278/14-A Client Sample ID: Method Blank



MB MB


2-Fluorobiphenyl 75 38 130 07/28/1114:42 08/02/1113:33

2-Fluorophenol 76 25- 130 07/28/1114:42 08/02/11 13:33

Nitrobenzene-d5 83 39 130 07/28/11 14:42 08/02/11 13:33

Phenol-d5 83 25- 130 07128/11 14:42 08102/11 13:33

Terphenyl-d14 87 10 143 07/28/11 1442 08102/11 13:33

2,4,6-Tribromophenol 80 31- 141 07/28/11 14:42 08/02/11 1333

Lab Sample ID: LCS 680-21 027811 5-A Client Sample ID: Lab Control Sample





Acenaphthene 100 76.9 ugIL 77 55-130

Acenaphthylene 100 79.2 ug/L 79 60- 130

Acetophenone 100 785 ug/L 78 54- 130

Aniline 100 80 5 ugIL 80 10- 130

Anthracene 100 84.7 ugIL 85 61 -130

Benzo[alanthracene 100 99.4 ug/L 99 58-130

Benzoja]pyrene 100 959 ug/L 96 61 - 130

Benzo[blfluoranthene 100 965 ug/L 97 51 - 130

Benzo[ghi]perylene 100 87.7 ugIL 88 54- 130

Benzo[klfluoranthene 100 82.1 u/L 82 53- 130

Benzyl alcohol 100 83.1 ug/L 83 53- 130

1,1-Biphenyl 100 73.0 ugIL 73 54- 130

Bis(2-chloroethoxy)methane 100 91.4 ug/L 91 64- 130

Bis(2-chloroethyl)ether 100 804 ug/L 80 56- 130

bis(chloroisopropyl) ether 100 92.8 ugIL 93 55 130

Bis(2-ethylhexyl) phthalate 100 103 uglL 103 62-130

4-Bromophenyl phenyl ether 100 89.9 uglL 90 61 - 130

Butyl benzyl phthalate 100 110 uglL 110 66 130

4-Chloroaniline 100 778 ugIL 78 42-130

4-Chloro-3-methylphenol 100 852 ugIL 85 60- 130

2-Chloronaphlhalene 100 724 ug/L 72 53 130

2-Chlorophenol 100 76.6 uglL 77 57 130

4-Chlorophenyl phenyl ether 100 824 u9/L 82 57 130

Chrysene 100 95.6 ug/L 96 59 - 130

Dibenz(a,h)anthracene 100 858 uglL 86 55 130

Dibenzoturan 100 786 u9IL 79 58 130

1 ,2-Dichlorobenzene 100 640 ugIL 64 43. 130

1,3-Dichlorobenzene 100 61 7 ug/L 62 41- 130

1 ,4-DichIc,robenzene 100 62 1 ug/L 62 43 - 130

3,3-Dichlorobenzidine 100 64.6 ug/L 65 27- 130

2,4-Dichlorophenol 100 790 ugIL 79 54 130

Oiethyt phlhalate 100 94.3 ugIL 94 70- 130

2 4-Dimethylphenol 100 663 uglL 66 40- 130

Dimethyl phthalate 100 88.8 UgIL 89 69- 130

Di-n-butyl phthalate 100 93.2 ug/L 93 66- 130

4,6-Dinitro-2-methylphenol 100 868 ugIL 87 45 134

2,4-Dinitrophen 100 94 1 uglL 94 20 165 0TestAmerica Savannah

of 92


Project/Site: Hercules Hattiesburg APIX 7/26111


Lab Sample ID: LCS 680-210278/15-A Client Sample ID: Lab Control Sample


Analysis Batch: 210829 Prep Batch: 210278Spike LCS LCS % Rec.


24-Dinitrotoluene 100 85.4 ugIL 85 63 130

2,6-Dinitrotoluene 100 83.3 ugIL 83 65-130

Di-n-octyl phthalate 100 112 ugIL 112 64.130

1,4-Dioxane 100 57.7 ugIL 58 35-130

Fluoranthene 100 86.0 ugIL 86 56-130

Fluorene 100 82.4 ugIL 82 61 .130

Hexachlorobenzene 100 803 ugIL 80 52. 130

Hexachlorobutadiene 100 68.8 ugIL 69 36-130

Hexachlorocyclopentadiene 100 27.8 ugIL 28 10_ 130

Hexachloroethane 100 61.6 uglL 62 39 130

lndeno[1,2,3-cd]pyrene 100 97.9 ug/L 98 47-130

Isophorone 100 81.8 ug!L 82 59-130

2-Methylnaphthalene 100 74.6 ug/L 75 52-130

2-Methylphenol 100 80.6 ug/L 81 55-130

3 & 4 Methylphenol 100 79.7 ugIL 80 35. 130

Naphthalene 100 74.3 ugIL 74 50- 130

2-Nitroanhline 100 93.2 ugIL 93 60. 130

3-Nitroaniline 100 86.4 ugIL 86 54. 130

4-Nitroaniline 100 88.2 ugIL 88 54-130

Nitrobenzene 100 84.6 ug/L 85 56-130

2-Nitrophenol 100 78.7 ugIL 79 54. 130

4-Nitrophenol 100 85.1 ug/L 85 38-130

N-Nitrosodimethylamine 100 105 ugIL 105 54. 130

N-Nitrosodi-n-propylamine 100 97.9 ug/L 98 64. 130

N-Nitrosodiphenylamine 100 87.3 ugIL 87 68. 130

Pentachlorophenol 100 84.5 ugIL 84 42- 138

Phenanthrene 100 85.9 ugIL 86 62- 130

Phenol 100 77.7 ugIL 78 29- 130

Pyrene 100 95.0 ugIL 95 60- 130

Pyridine 100 64.2 uglL 64 10- 130

1,2,4-Trichlorobenzene 100 65.7 ugIL 66 42. 130

2,4,5-Trichlorophenol 100 81 9 ugIL 82 61 -130

2,4,6-Trichlorophenol 100 80.2 ugIL 80 57 130

LCS LCS


2-Fluorobiphenyl 72 38. 130

2-Fluorophenol 77 25. 130

Nitrobenzene-d5 87 39. 130

Phenol-d5 80 25 130

Terphenyl-d14 87 10.143

2,4,6-Thbromophenol 87 31 - 141

Lab Sample ID: LCS 680-210278118-A Client Sample ID: Lab Control Sample




2-Acetylarninofluorene 100 108 uglL 108 63-130

alpha,alpha-Dimethyl 100 <2000 ug/L 196 10. 200

phenethylamine


of 92



Method: 8270C - Semivolatile Organic Compounds (GCIMS) (Continued) 0Lab Sample ID: LCS 680-210278/18-A Client Sample ID: Lab Control Sample

I Matrix: Water Prep Type: Total/NA



Analyte Added Result Qualifier Unit C) % Rec Limits

4-Aminobiphenyl 100 43.1 - ugIL —- — -- 43 10-130 ——

Aramite, Total 100 121 ugIL 121 12- 181

Diallate 100 66.3 ug/L 66 45- 130

2,6-Dichlorophenol 100 87.6 ug/L 88 55.130

Dimethoate 100 40.6 ugIL 41 64- 130

7,12-Dimethylberiz(a)anthracene 100 81 0 ugIL 81 57.130 -

3,3-Dimethylbenzidine 250 214 E ugiL 86 10- 130

1,3-Dinitrobenzene 100 99.1 ugiL 99 61- 130

Dinoseb 100 98.4 ug/L 98 70. 138

Disulfoton 100 63.3 * ugIL 63 65-130

Ethyl methanesulfonate 100 48.4 ugiL 48 10- 156

Ethyl Parathion 100 99.4 ugIL 99 67- 153

Famphur 100 <10 ug/L 3 10-130

Hexachlorophene 500 <5000 E ugiL 68 10- 130

Hexachloropropene 100 44.2 ug!L 44 10- 130

Isosafrole 100 89.0 ugiL 89 54. 130

Methapyrilene 500 <2000 E ug/L 62 10. 155

3-Methylcholanthrene 100 28.5 ug/L 28 10- 148

Methyl melhanesulfonate 100 35.7 ug/L 36 10- 130

Methyl parathion 100 61.4 ug/L 61 65-148

1,4-Naphthoquinone 100 18.9 ugiL 19 10-132

1-Naphthylamine 100 74.0 ugiL 74 28. 130

2-Naphthylamine 100 55.0 ug/L 55 10- 130

4—Nitroquinoline-1-oxide 100 121 ugiL 121 10. 146

N-Nilro-o-toluidine 100 90.1 ugIL 90 46- 130

N-Nitrosodiethylamine 100 68 5 ug/L 69 37. 130

N-Nitrosodi-n-butylamine 100 81.3 Ug)L 81 40. 130

N-Nilrosomelhylethylamine 100 65.4 ug/L 65 22. 130

N-Nitrosomorpholine 100 971 ug/L 97 25- 130

N-Nitrosopiperidine 100 76.6 ug/L 77 55.130

N-Nitrosopyrrolidine 100 79.9 ug/L 80 36. 130

o,o’,o”-Triethylphosphorothioate 100 77.2 ug/L 77 18- 139

p-Dimethylarnino azobenzene 100 76.6 ugIL 77 49. 130

Pentachlorobenzene 100 99.2 ug/L 99 60. 130

Pentachloronilrobenzene 100 108 ug!L 108 70. 130

Phenacetin 100 97.2 ug/L 97 47. 130

Phorate 100 67 7 ug/L 68 52- 156

2-Picoline 100 57.7 ug/L 58 10- 130

p-Phenylenediamine 500 <2000 F ug/L 51 10. 130

Pronamide 100 99 5 uglL 100 70. 130

Safrole, Total 100 88 1 ugJL 88 54- 130

Sulfolepp 100 87.1 ug/L 87 65. 130

1,2,4,5-Tetrachlorobenzene 100 84.4 ug!L 84 51 - 130

2,3,4,6-Tetrachlorophenol 100 119 ug/L 119 64-130

Thionazin 100 81.5 ug/L 82 70- 130

2-Toluidine 100 642 uglL 64 22- 130

1,3.5-Trinitrobenzene 100 583 ug/L 58 21 .165


of 92




ethod: 8270C - Semivolatile_Organic Compounds (GC1MS) (Continued)

Lab Sample ID: LCS 680-21027811 8-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: TotaIlNA


Surrogate

2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

Terphenyl-d14

24, 6-Tribmmophenol

LCS LCS

%Recove,y Qualifier_- Limits

70 38-130

65 25-130

74 39-130

70 25130

84 10143

93 31141

Method: 8081A_8082 - Organochiorine Pesticides & PCBs (GC)




Analyte Result Qualifier RL MDL Unit D Prepared Analyzed -_Dii Fat

Aldtin <0.050 0.050 ug/L 07)28(11 14:42 08/01/11 16:11 1

alpha-BHC <0.050 0.050 ug/L 07)28(11 14:42 08/01/11 16:11 1

bela-BHC <0.050 0.050 uglL 07/28/11 14:42 08/01/11 16:11 1

Chiordane (technical) <0.50 0.50 ugIL 07/28/11 1442 08101/11 16:11 1

Chlorobenzilate <0.50 050 ugIL 07/28/11 14:42 08/01/11 16:11 1

4,4-DDD <0.10 0.10 ugIL 07/28/11 14.42 08/01/11 16:11 1

j4,4-DDE <0.10 0.10 ug/L 07/28/11 14.42 08/01/11 16:11 1

4,4-DDT <0.10 0.10 ugiL 07/28/11 14:42 08/01/11 16:11 1

delta-BHC <0.050 0.050 ug/L 07/28/11 14:42 08/01/11 16:11 1

Dieldnn <0 10 0 10 ug/L 07/28/11 14:42 08/01/11 16:11 1

Endosullan I <0.050 0.050 ug)L 07/28/11 14:42 08/01/11 16:11 1

Endosulfari II <0.10 010 ugh 07/28/11 14.42 08(01/11 16:11 1

Endosulfan sulfate <0.10 0.10 uglL 07)28/11 14:42 08/01/11 16:11 1

Endrin <010 0.10 ugIL 07/28/11 14:42 08/01/11 16.11 1

Endnn aldehycle <0.10 0.10 ugIL 07/28(11 14:42 08/01/11 16:11 1

Endnn ketone <010 0.10 ug/L 07/28/11 14:42 08/01/11 16.11 1

gamma-BHC (Lindane) <0.050 0.050 uglL 07128(11 1442 08/01/11 16.11 1

Heptachlor <0.050 0.050 ugIL 07)28/11 1442 08/01/11 1611 1

Heptachlorepoxide <0.050 0 050 ug/L 07/28/11 14:42 08/01/11 16:11 1

Isodrin <0 050 0 050 uglL 07/28(11 1442 08/01/11 16:11 1

Kepone <1.0 1 0 ugIL 07/28/11 1442 08/01/11 16 11 1

Methoxychlor <0.10 0.10 ugIL 07/28(11 14:42 08/01/11 1611 1

Toxaphene <50 50 ugIL 07)28/11 1442 08/01/11 1611 1

PCB-1016 <10 1.0 ugIL 07)28/11 1442 08/01/11 16:11 1

PCB-1221 <2.0 20 ug/L 07)28(11 1442 08/01/11 16.11 1

PCB-1232 <1.0 10 ugIL 07/28/11 14:42 08/01/11 1611 1

PCB-1242 <1.0 1 0 ugIL 07/28/11 1442 08/01/11 16.11 1

PCB-1248 <1.0 10 ugh 07)28/11 1442 08/01)11 16:11 1

PCB-1254 <1.0 1 0 ugIL 07/28/11 1442 08/01)11 16 11 1

PCB-1260 <1 0 1 0 ugIL 07/28/11 14:42 08/01111 1611 1

MB MB

Surrogate % Recovery Qualifier Limits Prepared Analyzed DII Fat

,..—-NTetrachlorom.xy1ene 70 36- 130 07128/11 14.42 08/01/11 16.11

Tefrachloro-rn-xylene 67 36 130 07/28/11 1442 08/01/lI 1611 1

“ DCflDecachlorobiphenyl 55 40 130 07/28/Il 14.42 08/0 1/lI 1611

of 92



QC Sample Results


Lab Sample ID: MB 680-210285/18-A


MB MB

Surrogate

_______

-- % Recovery Qualifier Limits

DCB Decachlorobiphenyl 43 40 - 130

Lab Sample ID: LCS 680-210285/24-AMatrix: WaterAnalysis Batch: 211186

Spike

Analyte Added

PCB-1016 100

PCB-1260


Client Sample ID: Method BlankPrep Type: Total/NAPrep Batch: 210285

Prepared Analyzed DII Fac

07/28/11 1442 08/01/Il 1611 1

Client Sample ID: Lab Control SamplePrep Type: Total/NAPrep Batch: 210285

LCS LcS %Rec.

Result Qualifier Unit U Rec Limits

935 ug/L 93 38. 172

905 ug/L 91 46.138


Client Sample ID: Lab Control SamplePrep Type: TotalINAPrep Batch: 210285

Spike L5 LcS % Rec.


AIdrin 0100 0.0615 ug/L 61 14- 168

alpha-BHc 0.100 00677 ug/L 68 43. 138

beta-BHC 0.100 0.0723 p ug/L 72 38.. 158

4,4’-DDD 0.200 0.130 ugIL 65 49- 144

4,4-DDE 0.200 0.128 ug/L 64 46- 144

4,4’-DDT 0.200 0.120 ug/L 60 48- 166

delta-BHC 0.100 0.0823 uglL 82 23- 191

Dieldrin 0 200 0.131 ug/L 56 61 - 136

Endosulfan I 0.100 0.0675 ug/L 68 52- 141

Endosulfan II 0.200 0.136 ug/L 68 60- 140

Endosulfan sulfate 0.200 0.137 ut/L 69 60- 151

Endnn 0200 0128 * ug/L 64 66150

Endrin aldehyde 0 200 0 188 ut/L 94 16- 200

Endrin ketone 0.200 0 140 uglL 70 55- 156

gamma-BHc (Lindane) 0 100 0.0696 uglL 70 54.. 134

Heptachlor 0.100 00730 ug/L 73 10200

Heptachlor epoxide 0 100 0.0684 ug!L 68 49 142

Methoxychlor 0.200 0,134 ug/L 67 13- 186

LCS LCS


Telrachloro-m-xylene 59 36 - 130

Tetrachloro-m-xylene 58 36 - 130

DCB Decachlorobiphenyl 37 X 40. 130

OCB Decachlorobiphenyl 37 X 40- 130

0

0

0

Lcs Lcs

100


Tetrachloro-m-xylene 78 36 - 130

Tetrachloro-m-sylene 80 36 - 730

DCB Decachlorobiphenyl 63 40 - 130

OCR Decachlorobiphenyl 51 40 130


of 92


(..roJect/Site: Hercules Hattiesburg APIX 7/26/11

Method: 8081A_8082- Organochiorine Pesticides&PCBs (GC)(Continued)


Added Result

500 5.38

Surrogate




DCB Decachiorobiphenyl


— 71 36130

67 36130

54 40130

41 40-130

Lab Sample ID: LCSD 680-21 0285/28-A

Matrix: Water


Analyte

Chiordane (technical)

Surrogate


Tetrach/oro-m-xylene

ODCB Decachlombiphenyl

DCB Decachiorobiphenyl

% Recovery

77

69

69

53

Qualifier Limits

36- 130

3& 130

40- 130

40-130

Client Sample ID: Lab Control Sample DupPrep Type: TotalINAPrep Batch: 210285

%Rec. RPD

Unit D % Roc Limits RPD Limit

uglL 122 56-144 12 50

Lab Sample ID: MB 680-210256/18-A

Matrix: Water


Client Sample ID: Method BlankPrep Type: Total/NAPrep Batch: 210266

Analyte

24-D

Silvex (245-TP)

24,5-T

Result Qualifier RL

<050 050

<050 0.50

<050 050

MB MB

MDL unit o Prepared

ug/L 07/28/11 08:04

ug/L 07/28/11 08:04

ug/L 07/28/11 08:04

Analyzed

07/29/11 16:29

07/29/11 16.29

07)29/11 16.29

Surrogate

DCAA

DC.4A


80 52151

Lab Sample ID: LCS 680-21026611 9-A

Matrix: Water

Analysis Batch: 210520Spike

Analyte Added

2,4-D 2.00

Silvex (24,5-TP) 2.00

24,5-T 2 00

LOS LCS

Result Qualifier

1 99

176

Client Sample ID: Lab Control Sample

Prep Type: Total/NA

Prep Batch: 210266

— % Recovery Qualifier

88

TestAmerca Savannah

Lab Sample ID: LCS 680-210285/27-A

Matrix: Water


Analyte

Chlordane (technical)

LCS LCS


Prep Type: TotaIINA

Prep Batch: 210285

Qualifier unit D % Roe Limits

ugIL 108 56_ 144

Spike LCSD LCSD

Added Result Qualifier

5.00 6.09

LCSD LCSD

Method: 8151A - Herbicides (GC)

92

Dii Fec

52- 151


07/28/11 0804 07/29/lI 16:29 -

07/28/11 0804 07/29/11 1629

Surrogate

DCAA

DCAA

LCS LCS

1.85 ugIL

% Rec.

Unit D % Roe Limits

ug)L 100 63130

ug/L 88 64-130

93 59-130

114

Limits

52- 151

52 151

of 92



Method: 8290 - DioxinsiFurans, HRGCIHRMS (8290) 6)Lab Sample ID: G1G280000070B Client Sample ID: Method Blank

Matrix: Water Prep Type: Total

Analysis Batch: 1209070 Prep Batch: 1209070_PMBMB

Analyte Result Qualifier ML EDL TEF TEQ Unit D — Prepared Analyzed Dii Fac

2,3,7,8-TCDD ND 10 0.22 1 pgIL 07I28111 0900 07/30/11 00:15 1

Total HXCDD ND 50 0.77 pg/L 07/28/11 0900 07/30111 00:15 1

Total HxCDF ND 50 024 pgIl.. 07/28111 09.00 07/30/11 00:15 1

Total PeCDD ND 50 061 pgIL 07/28/11 0900 07/30111 00:15 1

Total PeCDF ND 50 0.31 pg/L 07/28/11 09:00 07/30/11 0015 1

Total TCDD ND 10 0.38 pgIL 07/28/11 09:00 07/30/11 0015 1

Total TCDF ND 10 0.51 pgIL 07128/11 09:00 07/30/11 00:15 1

Total TEQ 0.00

MB MB

internal Standard % Recovery Qualifier Limits Prepared Analyzed Dii Fac

13C-2,3,7,8-TCDD 73 40- 135 07/28/11 09:00 07/30/11 00:15 1

13C-12,3,7,8-PeCDD 75 40- 135 07/28/11 09:00 07/30/11 00:15 1

13C.1,2,36,7,8-HxCDD 73 40.135 07/28/11 09:00 07/30/11 00:15 1

13C-23,7,8-TCDF 76 40. 135 07/28/1109:00 07/30/11 00:15 1

13C-1,2,3,7,8-PeCDF 75 40. 135 07/28/11 09:00 07/30/11 00:15 1

13C-1,23,4,7,8-HxCDF 74 40- 135 07/28/11 09:00 07/30/11 00:15 1

Lab Sample ID: G1G280000070C Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total

Analysis Batch: 1209070 Prep Batch: 1209070_PSpike LCS LCS % Rec.


2,3,7.8-TCDD 200 206 pg/L 103 72.144

LCS LCS

Internal Standard %Recovery Qualifier Limits

13C-2,3,78-TCDD 75 — 40- 135

13C-l,2,3,7,8-PeCDD 80 40- 135

13C-l,2,3,6,7,8-HxCDO 82 40. 135

13C-23,7,8-TCDF 80 40-135

13C-1.2,3,7,8-PeCDF 78 40- 135

13C-l,2,3,4,78-HxCDF 74 40- 135

Method: 6020 - Metals (ICP/MS)




Ariatyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

Antimony <5.0 5.0 uglL 08/01/11 0848 08/06/11 2057 1

Arsenic <25 25 ug/L 08/01/11 0848 08/06/11 2057 1

Barium <50 50 ug/L 08/01/11 0848 08/06/11 20:57 1

Beryllium <050 0.50 ug/L 08/01/11 0848 08/06/11 2057 1

Cadmium <0 50 0 50 ug/L 08/01/11 0848 08/06/11 2057 1

Chromium <5.0 5 0 ug/L 08/01/11 0848 08/06/11 2057 1

Cobalt <050 050 ug/L 08/01/11 0848 08/06/11 20:57 1

Copper <50 50 ug/L 08/01/11 0848 08/06/11 2057 1

Lead <1 5 1 5 ug/L 08/01/11 0848 08/06/11 2057 1 QTestAmerica Savannah

oF92



Method:_6020 - Metals (ICPIMS) (Continued)

_____ _____

Lab Sample ID: MB 680-21057811-A Client Sample ID: Method Blank



Analyte Result Qualifier RL - MDL Unit 0 Prepared Analyzed DII Fec

Nickel <5.0 5.0 ugiL 08/01/11 08:48 08/06/11 20:57 1

Selenium <2.5 2.5 ug/L 08/01/11 08:48 08/06/11 20:57 1

Silver <1.0 1.0 ug/L 08/01/11 08:48 08/06/11 20:57 1

Thallium <1.0 1.0 ug/L 08/01/11 08:48 08/06/11 20:57 1

Tin <5.0 5.0 ug/L 08/01/11 08.48 08/06/11 20:57 1

Vanadium <10 10 ug/L 08/01/11 08:48 08/06/11 20:57 1

Zinc <20 20 ugIL 08/01/11 08:48 08/06/11 20:57 1






Antimony 500 45.4 ug/L 91 75-125

Arsenic 100 97.9 ug/L 98 75-125

Barium 100 95.6 ug/L 96 75-125

Beryllium 50.0 48.7 ug/L 97 75. 125

Cadmium 50.0 50.0 ugiL 100 75. 125

Chromium 100 94.4 ug/L 94 75-125

OCobalt 50.0 47.4 ug/L 95 75 125

Copper 100 97.8 ug/L 98 75-125

Lead 50.0 491 ug/L 98 75 125

Nickel 100 98.4 ug/L 98 75 125

Selenium 100 104 ug/L 104 75 125

Silver 50.0 49.8 ug/L 100 75-125

Thallium 40.0 39 7 ug/L. 99 75- 125

Tin 100 95.8 ug/L 96 75-125

Vanadium 100 929 ug/L 93 75125

Zinc 100 104 ugfL 104 75125

Lab Sample ID: 680-70758-1 MS Client Sample ID: ASH-MWO8-072611



Sample Sample Spike MS MS % Rec.

Analyte —— — Result Qualifier Added Result Qualifier Unit 0 % Rec Limits

Antimony <5.0 500 51 0 ug/L 102 75 125

Arsenic 42 100 123 ug/L 81 75-125

Barium 260 100 364 ugIL 100 75 125

Beryllium <050 500 457 ug/L 91 75 125

Cadmium <050 500 485 ug/L 97 75-125

Chromium <5.0 100 101 ug/L 101 75-125

Cobalt <0 50 500 49 3 ug/L 98 75 125

Copper <50 100 734 F ug/L 72 75125

Lead <1.5 500 508 ug/L 102 75125

Nickel <5.0 100 101 ug/L 101 75_ 125

Selenium <25 100 84.1 ug/L 84 75-125

Silver <1.0 50.0 492 ug/L 98 75 125

Thallium <1.0 400 402 ug/L 100 75-125

Tin <50 100 53.1 F Ug/L 53 75 125

Vanadium <10 100 102 ug/L 102 75-125


of 92

QC Sample Results

Client Ashland Inc.Project/Site: Hercules Hattiesburg APIX 7/26/11


Method: 6020 - Metals (ICPIMS) (Continued)

Lab Sample 10: 680-70758-1 MS Client Sample ID: ASH-MWO8-072611



Sample Spike MS MS

Qualifier Added Result

100 90.5

Lab Sample ID: 680-70758-1 MSD


Sample Sample

Analyte Result Qualifier

Antimony <5.0

Arsenic 42

Barium 260

Beryllium <0.50

Cadmium <0 50

Chromium <5.0

Cobalt <0.50

Copper <5.0

Lead <1.5

Nickel <5 0

Selenium <2.5

Silver <1.0

Thallium <1.0

Tin <5.0

Vanadium <10

Zinc <20

Method: 7470A - Mercury (CVAA)

Client Sample ID: ASH-MWO8-072611Prep Type: TotalINAPrep Batch: 210578

%Rec. RPD

B % Rec Limits RPD Limit

110 75-125 8 20

98 75_125 13 20

132 75125 8 20

102 75-125 11 20

106 75125 8 20

117 75.125 14 20

107 75.125 9 20

79 75125 9 20

110 75.125 8 20

118 75.125 15 20

99 75125 16 20

106 75-125 8 20

109 75125 9 20

59 75- 125 10 20

118 75-125 14 20

96 75-125 6 20

Lab Sample ID: MB 680-210700)1 -AMatrix: WaterAnalysis Batch: 210774

Analyte

Mercury

MB MB

Result Qualifier RL MDL Unit

<0.20 0 20 UQ/L

Client Sample ID: Method BlankPrep Type: TotaIINA

Prep Batch: 210700

0 Prepared Analyzed Dii Fac

08/02/11 09:42 08/02/11 15:23 1


Analyte

Mercury

Spike

Added

2.50


Prep Type: TotalINA

Prep Batch: 210700% Rec.

D % Rec Limits

103 80120

Method: 9012A - Cyanide, Total andlor Amenable

Lab Sample ID: NiB 680-210574/1-A


MB MB

Client Sample ID: Method Blank

Prep Type: TotalINAPrep Batch: 210574

Analyte

Cyanide, Tolal

Result Qualifier RL MDL Unit

<0010 0010 mg/L-

9 Prepared Analyzed Dii Fac

08/01/11 0751 08/02/11 0631 1


0

Analyte

Zinc

Sample

Result

<20

% Rec.

Qualifier unit o % Rec Limits

ug/L 91 75125

0

Spike MSD MSD

Added Result Qualifier Unit

60.0 55.2 ug/L

100 140 ug/L

100 396 F ug/L

50.0 50.9 ug/L

50.0 52 8 ug/L

100 117 ug/L

50.0 53.9 ug/L

100 80.1 ut/L

500 54.8 ut/L

100 118 ugIL

100 99.0 ug/L

50.0 53.1 ug/L

400 43.7 ug/L

100 58.6 F ug/L

100 118 ug/L

100 96.4 ugIL

LCS LCS

Result Qualifier Unit

2.57 ug/L

of 92



ethod: 9012A - Cyanide, Total and!or Amenable (Continued)

______

Lab Sample ID: HLCS 680-21 0574/3-A Client Sample ID: Lab Control Sample


Analysis Batch: 210679 Prep Batch: 210574Spike HLCS HLCS % Rec.


Cyanide, Total 0.0751 0.0804 mgIL 107





Cyanide, Total 0.0301 0.0272 mg/L 90 85.115

Method: 9034 - Sulfide, Acid Soluble and Insoluble (Titrimetric)




Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dii Fac

Sulfide — <1.0 1.0 mgIL — 07/27/11 14:10 1

Lab Sample ID: LCS 680-21021 212 Client Sample ID: Lab Control Sample

OMatrix: Water Prep Type: Total/NA

Analysis Batch: 210212Spike LCS LCS % Rec.


Sulfide 10.0 8.62 mgiL 86 75-125

Lab Sample ID: LCSD 680-21021213 Client Sample ID: Lab Control Sample Dup



Analyte Added Result Qualifier Unit D % Rec Limits RPD Limit

Sulfide 10.0 8.72 mg/L 87 75125 1 30


of 92


QC Association SummaryTestAmerica Job ID: 680-70758-1

GCIMS VOA


Lab Sample ID

680-70758-9

LCS 680-210523/10

LCSD 680-210523111

MB 680-210523/13

680-70758-3

680-70758-7

680-70758-4

Client Sample ID

Trip Blank

Lab Control Sample

Lab Control Sample Dup

Method Blank

ASH-RSI-07261 1

ASH-MW1 9-072611

ASI-I-MW1 3-072611

Prep Type

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Matrix

Water

Water

Water

Water

Water

Water

Water

Method Prep Batch

8260B

826DB

826DB

826DB

826DB

826DB

826DB


Lab Sample ID ClIent Sample ID Prep Type

LCS 680-210543/4 Lab Control Sample Total/NA

LCSD 680-210543/5 Lab Control Sample Dup Total/NA

MB 680-210543/7 Method Blank Total/NA

680-70758-1 ASH-MWO8-07261 1 Total/NA

680-70758-6 ASH-MW23-07261 1 Total/NA


Lab Sample ID Client Sample ID Prep Type

LCS 680-210665/8 Lab Control Sample Total/NA

LCSD 680-210665/9 Lab Control Sample Dup Total/NA

MB 680-210665/11 Method Blank Total/NA

680-70758-5 ASH-M Wi 7-072611 Total/NA

680-70758-2 ASH-DUP-07261 1 Total/NA

Matrix

Water

Water

Water

Water

Water

Matrix

Water

Water

Water

Water

Water

Method - Prep Batch

826DB

826DB

826DB

8260B

826DB

Method Prep Batch

826DB

826DB

826DB

82608

8260B

Lab Sample ID

680-70758-1

680-70758-2

680-70758-3

680-70758-4

6 80-7 0758-5

680-70758-6

680-70758-7

MB 680-210278/14-A

LCS 680-210278/15-A

LCS 680-210278/18-A

Client Sample ID

ASH-MWD8-07261 1

ASH-DUP-07261 1

ASH-RSI-07261 1

ASH-MW1 3-072611

ASH-MW1 7-072611

ASH-MW23-07261 1

ASH-MW1 9-072611

Method Blank

Lab Control Sample

Lab Control Sample

Prep Type

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Matrix

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Method Prep Batch

3520C

3520C

3520C

3520C

352DC

3520C

352DC

3520C

3520C

35260



Lab Sample ID

680-70758-2

680-70758 4

Client Sample ID

ASH-DUP-07261 1

ASH-MWI 3-072611

Prep Type

Total/NA

Total/NA

Matrix

Water

Water

— Method Prep Batch

8270C 210278

82700 210278


0

Pa

0GCIMS Semi VOA

Prep Batch: 210278

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

MB 680-210278/14-A Method Blank Total/NA Water 8270C 210278

LOS 680-210278/15-A Lab Control Sample Total/NA Water 8270C 210278

LCS 680-210278/18-A Lab Control Sample Total/NA Water 8270C 210278

680-70758-3 ASH-RSI-072611 Total/NA Waler 82700 210278

of 92

QC Association SummaryClient: Ashland Inc. TestAmerica Job ID: 680-70758-1


CIMS_Semi VOA (Continued)


r Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

680-70758-5 ASH-MW17-072611 Total/NA Water 8270C 210278

680-70758-6 ASH-MW23-072611 Total/NA Water 8270C 210278



680-70758-1 ASH-MWO8-072611 Total/NA Water 8270C 210278

680-70758-7 ASH-M Wi 9-072611 Total/NA Water 8270C 210278

--—-.- ..

GC Semi VOA

Prep Batch: 210266


680-70758-1 ASH-MWO8-072611 Total/NA Water — 8151A —

680-70758-2 ASH-DUP-072611 Total/NA Water 8151A

680-70758-3 AS1-t-RSI-07261 1 Total/NA Water 8151A

680-70758-4 ASH-MW1 3-072611 Total/NA Water 815 1A

680-70758-5 ASH-MW17-072611 Total/NA Water 8151A


680-70758-6 - DL ASH-MW23-072611 Total/NA Water 8151A

680-70758-7 ASH-M Wi 9-072611 Total/NA Waler 8151A

MB 680-210266/18-A Method Blank Total/NA Waler 8151A

LCS 680-210266/19-A Lab Control Sample Total/NA Waler 8151A

0ep Batch: 210285

Lab Sample ID - Client Sample ID Prep Type Matrix Method Prep Batch

680-70758-1 ASH-MWO8-07261 1 Total/NA Water 3520C

680-70768-2 ASH-DUP-07261 1 Total/NA Water 3520C

680-70758-3 ASH-RSI-072611 Total/NA Waler 3520C

680-70758-4 ASH-MW13-072611 Total/NA Water 3520C



680-70758-7 ASt-l-MW19-072511 Total/NA Waler 3520C

MB 680-210285/18-A Method Blank Total/NA Waler 3520C

LCS 680-210285/19-A Lab Control Sample Total/NA Water 3520C



LCSD 680-210285/28-A Lab Control Sample Dup Total/NA Water 3520C



MB 680-210266/18-A Method Blank Total/NA Water 8151A 210266

LCS 680-210266/19-A Lab Control Sample Total/NA Water 8151A 210266

680-70758-1 ASH-MWO8-072611 Total/NA Waler 8151A 210266

680-70758-2 ASH-DUP-072611 Total/NA Water 8151A 210266

680-70758-3 ASH-RSI-072611 Total/NA Water 8151A 210266

680-70758-4 ASH-MW13-072611 Total/NA Water 8151A 210266



680-70758-7 ASH-MW19-072611 Tolal/NA Waler 8151A 210266


of 92


Project/Site: Hercules Hattiesburg APIX 7/26/11 4

GrnjVOA(Continued) - C).Analysis Batch: 210629


LCS 680-210285/19-A Lab Control Sample Total/NA Water 8081A_8082 210285


Lab Sample ID Client Sample ID Prep Type Matrix Method -- — Prep Batch

680-70758-6 - DL ASH-MW23-072611 Total/NA Water 8151A 210266



MB 680-210285/18-A Method Blank Total/NA Water 8081A_8082 210285

LCS 680-210285/24-A Lab Control Sample Total/NA Water 8081A 8082 210285

LCS 680-210285/27-A Lab Control Sample Total/NA Water 8081A 8082 210285

LCSD 680-210285/28-A Lab Control Sample Dup Total/NA Water 8081A_8082 210285

680-70758-1 ASH-MWOB-07261 1 Total/NA Water 808 1A_8082 210285

680-70758-2 ASH-DUP-07261 1 Total/NA Water 8081A_8082 210285

680-70758-3 ASH-RSI-07261 1 Total/NA Water 8081A 8082 210285

680-70758-4 ASH-MW13-072611 Total/NA Water 8081A 8082 210285

680-70758-6 ASH-MW23-072611 Total/NA Water 8081A_8082 210285

680-70758-7 ASH-MW19-072611 Total/NA Water BOB1A_8082 210285



680-70758-5 ASH-MW17-072611 — - Total/NA Water - 8081A 8082 — 210285

DIOXIN - - 0Analysis Batch: 1209070


G1G280000070B Method Blank Total Water 8290

G1G280000070C Lab Control Sample Total Water 8290

680-70758-1 ASH-MWO8-072611 Total Water 8290

680-70758-2 ASH-DUP-072611 Total Water 8290

680-70758-3 ASH-RSI-07261 I Total Water 8290

680-70758-4 ASH-M WI 3-072611 Total Water 8290

680-70758-5 ASH-MW17-072611 Total Water 8290

680-70758-6 ASH-MW23-072611 Total Waler 8290

680-70758-7 ASH-MW19-072611 Total Water 8290

Prep Batch: 1209070_P


G1G230000070B Method Blank Total Water 8290

131G280000070C Lab Conirol Sample Total Water 8290

680-70758-1 ASH-MWO8-072611 Total Water 8290

680-70758-2 ASH-DUP-072611 Total Waler 8290

680-70758-3 ASH-RSI-07261 1 Total Water 8290

680-70758-4 ASH-M Wi 3-072611 Total Waler 8290

680-70758-5 ASH-MW17-072611 Total Waler 8290

680-70758-6 ASH-MW23-07261 1 Total Water 8290

680-70758-7 ASH-MW19-0726ii Total Water 8290


of 92


Project/Site; Hercules Hattiesburg APIX 7)26/11

Metals

Prep Batch: 210578

Lab Sample ID client Sample ID Prep Type Matrix Method - Prep Batch

MB 680-210578/1-A Method Blank Total/NA Water 3010A

LCS 680-210578/2-A Lab Control Sample Total/NA Water 3010A

680-70758-1 ASH-MWO8-072611 Total/NA Water 3010A

680-70758-1 MS ASH-MW08-07261 1 Total/NA Water 3010A

680-70758-1 MSD ASH-MW08-072611 Total/NA Water 3010A

680-70758-2 ASI-l-DUP-07261 1 Total/NA Water 301 OA

680-70758-3 ASH-RSI-07261 1 Total/NA Water 301 OA

680-70758-4 ASH-MW1 3-072611 Total/NA Water 301 OA

680-70758-5 ASH-MW1 7-072611 Total/NA Water 301 oA

680-70758-6 ASH-MW23-07261 1 Total/NA Water 301 OA

680-70758-7 ASH-MW1 9-072611 Total/NA Water 301 OA

Prep Batch: 210700

Lab Sample ID client Sample ID Prep Type Matrix Method Prep Batch

j MB 680-210700/1-A Method Blank Total/NA Water 7470A


680-70758-1 ASH-MWO8-0726 11 Total/NA Water 7470A


680-70758-3 ASH-RSI-07261 1 Total/NA Water 7470A

680-70758-4 ASH-MW1 3-072611 Total/NA Water 7470A



680-70758-7 ASH-M Wi 9-072611 Total/NA Water 7470A



MB 680-210700/1-A Method Blank — Total/NA Water 7470A — 210700

LCS 680-210700/2-A Lab Control Sample Total/NA Waler 747oA 210700

680-70758-1 ASH-MWO8-072611 Total/NA Water 7470A 210700



Lab Sample 10 - Client Sample ID Prep Type Matrix Method Prep Batch








MB 680-210578/1-A Method Blank Total/NA Water 6020 210578

LCS 680-210578/2-A Lab Control Sample Total/NA Water 6020 210578

680-70758-1 ASH-MWO8-072611 Total/NA Water 6020 210578

680-70758-1 MS ASH-MWO8-072611 Total/NA Water 6020 210578

680-70758-I MSD ASH-MWO8-072611 Total/NA Water 6020 210578

680-70758-2 ASH-DIJP-072611 Total/NA Waler 6020 210578

680-70758-3 ASH-RSI-072611 Total/NA Water 6020 210578

680-70758-4 ASH-MW13-072611 Total/NA Waler 6020 210578

680-70758-5 ASH-MW17-072611 Total/NA Water 6020 210578

680-70758-6 ASH-MW23-072611 Total/NA Waler 6020 210578

680-70758-7 ASH-MW19-072611 Total/NA Water 6020 210578


of 92

QC Association SummaryClient: Ashland Inc TestAmerica Job ID: 680-70758-1


Gener Chemistry



MB 880-210212/1 Method Blank Total/NA Water 9034

LCS 680-21021212 Lab Control Sample TotalINA Water 9034

LCSD 680-210212)3 Lab Control Sample Dup Total/NA Water 9034

680-70758-1 ASH-MWO8-072611 Total/NA Water 9034

680-70758-2 ASH-DUP-072611 Total/NA Water 9034

680-70758-3 ASH-RSI-07261 1 Total/NA Water 9034

680-70758-4 ASH-MW13-072611 Total/NA Water 9034




Prep Batch: 210574


•MB 680-210574/1-A — Method Blank Total/NA Water 9012A


HLCS 680-210574/3-A Lab Control Sample Total/NA Water 9012A

680-70758-1 ASH-MWO8-07261 1 Total/NA Water 901 2A


680-70758-3 ASH-RSI-07261 1 Total/NA Water 901 2A

680-70758-4 ASH-MW1 3-072611 Total/NA Water 901 2A

680-70758-S ASH-MW17-072611 Total/NA Water 9012A





MB 680-210574/1-A Method Blank Total/NA Water 9012A 210574

LCS 680-210574/2-A Lab Control Sample Total/NA Water 9012A 210574

HLCS 680-210574/3-A Lab Control Sample Total/NA Water 9012A 210574

680-70758-1 ASH-MWO8-072611 Total/NA Water 9012A 210574




680-70758-5 ASH MW17-072611 Total/NA Water 9012A 210574


680-70758-7 ASH-MW19-072611 Total/NA Waler 9012A 210574


of 92



lient sample ID: ASH-MWO8-072611 Lab Sample ID: 680-70758-1

Lab Chronicle



Client Sample ID: ASH-DUP-072611ate Collected: 07/26/11 00:00

ate Received: 07/27/11 09:20



Batch Batch Dii initial Final Batch Prepared

Prep Type Type Method Run Factor Amount Amount Number Or Analyzed Analyst Lab

Total/NA Analysis 8260B 50 5 mL 5 mL 210543 07/30/11 06:38 AJMC TALSAV

Total/NA Prep 35200 969.9 mL 1 mL 210278 07/28/11 14:42 RBS TAL SAV

Total/NA Analysis 82700 100 211006 08/04/11 1318 LH TAL SAV

Total/NA Prep 8151A 985.6 mL 10 mL 210266 07/28(11 08:04 CTR TALSAV

Total/NA Analysis 8151A 1 210520 07/29(11 18:37 JK TAL SAV

Total/NA Prep 3520C 987.7 mL 10.0 mL 210285 07/28/11 14:42 RBS TAL SAV

• Total/NA Analysis 8081A_8082 1 211186 08/01/11 20:20 JK TAL SAV

Total Prep 8290 947.94 mL 20 uL 1209070_P 07/28111 09:00 BG TALWSC

Total Analysis 8290 1.05 1209070 07/30/11 10:39 SXY TALWSC

Total/NA Prep 7470A 50 mL 50 mL 210700 08/02/11 09:42 BCB TAL SAV

Total/NA Analysis 7470A 1 210774 08/02/11 16:37 cc TALSAV

Total/NA Prep 3010A 50 mL 250 mL 210578 08/01/11 08:48 BCB TALSAV

Total/NA Analysis 6020 1 211230 08/06/11 22:18 BB TALSAV

Total/NA Analysis 9034 1 250 mL 250 mL 210212 07/27/11 14:10 ON TALSAV

Total/NA Prep 9012A 50 mL 50 mL 210574 08/01/11 07:51 DAM TALSAV

Total/NA Analysis 9012A 1 210679 08/02/11 06:47 DAM TALSAV

Batch Batch Dii Initial Final Batch Prepared


Total/NA — Analysis 8260B 50 5 mL 5 mL 210665 07/30/11 2103 RB TALSAV

Total/NA Prep 35200 989.5 mL 1 mL 210278 07/28/11 14:42 RBS TAL SAV

Total/NA Analysis 82700 50 210853 08/03/11 13:21 LH TAL SAV

Total/NA Prep 8151A 994.7 mL 10 mL 210266 07/28/11 08:04 CTR TAL SAV

Total/NA Analysis 8151A 1 210520 07/29/11 18.53 JK TAL SAV


Total/NA Analysis 8081A_8082 1 211186 08/01/11 2039 JK TAL SAV

Total Prep 8290 987.06 mL 20 uL 1209070 P 07/28/11 09:00 BG TALWSC

Total Analysis 8290 101 1209070 07/30/11 11:24 SXY TALWSC

Total/NA Prep 7470A 50 mL 50 mL 210700 08/02111 0942 BOB TAL SAV

Total/NA Analysis 7470A 1 210774 08/02/11 16.40 CC TAL SAV

Total/NA Prep 3010A 50 mL 250 mL 210578 08/01/11 08:48 BOB TAL SAy

Total/NA Analysis 6020 1 211230 08/06/11 2251 SB TAL SAV

Total/NA Analysis 9034 1 250 mL 250 mL 210212 07/27/11 14 10 ON TAL SAy

Total/NA Prep 9012A 50 mL 50 mL 210574 08/01/11 07.51 DAM TAL SAV

Total/NA Analysis 9012A 1 210679 08/02/11 06.48 DAM TAL SAV

of 92


Client Sample ID: ASH-RSI-072611Date Collected: 07/26/11 08:57Date Received: 07/27/11 09:20

Lab ChronicleTestAmerica Job ID: 680-70758-1


Client Sample ID: ASH-MWI 3-072611Date Collected; 07/26/11 09:20Date Received: 07/27/11 09:20



0

Batch Batch Dii Initial Final Batch PreparedPrep Type Type Method Run Factor Amount Amount Number Or Analyzed Analyst LabTotal/NA Analysis 8260B 1 5 mL 5 mL 210523 07/29/11 19:04 RB TAL SAV

Total/NA Prep 3520C 964.8 mL 1 mL 210278 07/28/11 14.42 RBS TAL SAVTolal/NA Analysis 827CC 1 210829 08/02111 1832 LH TALSAV

Total/NA Prep 8151A 10094 mL 10 mL 210266 07/28/11 08.04 CTR TAL SAVTotal/NA Analysis 8151A 1 210520 07/29/11 19:08 JK TALSAV

Total/NA Prep 3520C 9731 mL 10.0 mL 210285 07/28/11 14:42 RBS TAL SAVTotal/NA Analysis 8081A 8082 1 211186 08/01/11 20:58 JK TAL SAV

Total Prep 8290 96837 mL 20 uL 1209070 P 07/28/11 09:00 BG TALWSCTotal Analysis 8290 1.03 1209070 07/30/11 12:09 SXY TALWSC

Total/NA Prep 7470A 50 mL 50 mL 210700 08/02111 09:42 BCB TAL SAVTotal/NA Analysis 7470A 1 210849 08/02111 16:50 CE TAL SAV

Total/NA Prep 3010A 50 mL 250 mL 210578 08/01/11 08:48 BCB TAL SAVTotal/NA Analysis 6020 1 211230 08/06/11 2258 BB TAL SAV

Total/NA Analysis 9034 1 250 mL 250 mL 210212 07/27/11 14:10 CN TAL SAV

Total/NA Prep 9012A 50 mL 50 mL 210574 08/01/11 07.51 DAM TAL SAVTotal/NA Analysis 9012A 1 210679 08/02111 06:49 DAM TAL SAV

I4

0Batch Batch Dii Initial Final Batch Prepared

Prep Type Type Method Run Factor Amount Amount Number Or Analyzed Analyst LabTolal/NA Analysis 82608 10 5 mL 5 mL 210523 07/29/11 20.03 RB TAL SAV

Total/NA Prep 3520C 1019.8 mL I mL 210278 07/28/11 1442 RBS TAL SAVTotal/NA Analysis 827CC 5 210853 08/03/11 1350 LH TAL SAV

Total/NA Prep 8151A 9982 rnL 10 mL 210266 07/28/11 08:04 CTR TAL SAVTotal/NA Analysis 8151A 1 210520 07/29/11 1924 JK TAL SAV

Total/NA Prep 352CC 979.7 mL 100 mL 210285 07/28/11 1442 RBS TAL SAVTotal/NA Analysis 8081A_8082 1 211186 08/01/11 21 17 JK TAL SAV

Total Prep 8290 99727 mL 20 uL 1209070_P 07/28/11 0900 BG TAL WSCTotal Analyss 8290 1 1209070 07/30/11 12 53 SXY TAL WSC

Tolal/NA Prep 7470A 50 mL 50 mL 210700 08/02/11 0942 BCB TAL SAVTotal/NA Analysis 7470A 1 210849 08)02/11 1654 CE TAL SAV

Total/NA Prep 3010A 50 rnL 250 mL 210578 08/01/11 0846 BCI3 TAL SAVTotal/NA Analysis 6020 1 211230 08106111 2305 88 TAL SAy

Total/NA Analysis 9034 1 250 mL 250 inL 210212 07/27/11 1410 CN TAL SAy

Total/NA Prep 9012A 50 mL 50 mL 210574 08/01/11 0751 DAM TAL SAVTotal/NA Analysis 9012A 1 210679 08/02)11 0650 DAM TAL SAV

of 92

Lab ChronicleClient: Ashland Inc. TestAmerica Job ID: 680-70758-1

Project/Site: Hercules Hattiesburg APIX 7126111




Batch Batch DII Initial Final Batch Prepared


Total/NA Analysis 82608 — 200 5 rnL 5 mL 210665 07/30/11 20:34 RB TAL SAy

Total/NA Prep 3520C 1000.5 mL 1 mL 210278 07/28/11 14:42 RBS TALSAV

Total/NA Analysis 8270C 100 210894 08/03111 16:12 LH TALSAV

Total/NA Prep 8151A 988.2 mL 10 mL 210266 07/28/11 08.04 CTR TALSAV

Total/NA Analysis 8151A 1 210520 07/29111 19:40 JK TAL SAy


Total/NA Analysis 8081A_8082 10 211343 08/08/11 12:27 JK TAL SAV

Total Prep 8290 1001.81 mL 20 uL 1209070_P 07/28/11 09:00 BG TALWSC

Total Analysis 8290 1 1209070 07/30/11 13:38 SXY TALWSC

Total/NA Prep 7470A 50 mL 50 mL 210700 08/02/11 09:42 BCB TALSAV

Total/NA Analysis 7470A 1 210849 08102/11 16:57 CE TAL SAV

Total/NA Prep 3010A 50 mL 250 mL 210578 08/01/11 08:48 BCB TAL SAV

Total/NA Analysis 6020 1 211230 08/06/11 23:11 BB TAL SAy

Total/NA Analysis 9034 1 250 mL 250 mL 210212 07/27/11 14.10 CN TAL SAV

Total/NA Prep 9012A 50 mL 50 mL 210574 08/01/1107:51 DAM TALSAV

Total/NA Analysis 9012A 1 210679 08/02/11 06:51 DAM TALSAV


(“?ate Collected: 07/26/11 12:51 Matrix: Water

ate Received: 07/27/11 09:20

_____________ _______________________________________

Batch Batch DII Initial Final Batch Prepared

Prep Type Type Method Run Factor Amount Amount Number Or Analyzed Analyst Lab —

Total/NA Analysis 8260B 100 5 mL 5 mL 210543 07/30/11 07:35 AJMC TAL SAy

Total/NA Prep 3520C 1032.2 mL 1 mL 210278 07/28/11 14.42 RBS TAL SAy

Total/NA Analysis 8270C 10 210894 08)03/11 16:39 LH TAL SAy

Total/NA Prep 8151A 1001.7 mL 10 mL 210266 07/28/11 08:04 CTR TAL SAy

Total/NA Analysis 8151A 1 210520 07/29/11 19:56 JK TAL SAV

Total/NA Prep 8151A DL 1001.7 mL 10 mL 210266 07)28)11 08:04 CTR TAL SAV

Total/NA Analysis 8151A DL 4 210709 08/01/11 16:39 WTE TAL SAy

Total/NA Prep 3520C 1014.9 mL 100 mL 210285 07/28/11 1442 RBS TAL SAV

Total/NA Analysis 8081A_8082 1 211186 08/01/11 21 55 JK TAL SAV

Total Prep 8290 98931 mL 20 uL 1209070_P 07/28/11 0900 BG TAL WSC

Total Analysis 8290 1 01 1209070 07/30/11 1422 SXY TALWSC

Total/NA Prep 7470A 50 mL 50 mL 210700 08/02)11 0942 BCB TAL SAy

Total/NA Analysis 7470A 1 210849 08/02/11 1700 CE TAL SAy

Total/NA Prep 3010A 50 mL 250 mL 210578 08)01)11 08:48 BCB TAL SAy

Total/NA Analysis 6020 1 211230 08/06)11 23:18 88 TAL SAV

Total/NA Analysis 9034 1 250 mL 250 mL 210212 07/27)11 1410 CN TAL SAy

Total/NA Prep 9012A 50 mL 50 mL 210574 08/01/11 07:51 DAM TAL SAy

Total/NA Analysis 9012A 1 210679 08/02111 0651 DAM TAL SAV


of 92

Lab ChronicleClient: Ashland Inc.Project/Site: Hercules Hattiesburg APIX 7/26/11

Client Sample ID: Trip BlankDate Collected: 07126111 00:00Date Received: 07/27/11 09:20

Dii

Prep Type — Type Method Run FactorTotal/NA Analysis 8260B 1



Number Or Analyzed Analyst

210523 07/29/11 14:39 RB

Laboratory References:TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858TAL WSC = TestAmerica West Sacramento, 880 Riverside Parkway, West Sacramento, CA 95605, TEL (916)373-5600


0

Client Sample ID: ASH-MWI9-072611Date Collected: 07126111 14:20Date Received: 07127/11_09:20

BatchBatch

Prep Type Type

Total/NA Analysis

Dii Initial

Method Run Factor Amount

8260B 1 5 mL


Final

Amount

5 mL

1 mL1008.1 mL

1003.9 mL

Batch

Number

210523

210278

211006

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total

Total

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Prepared

Or Analyzed Analyst

07/29/11 19:34 RB

07/28/11 14:42 RBS

08/04/11 13:47 LH

Prep 3520C

Analysis 8270C

Prep 8151A

Analysis 8151A

Prep 3520C

Analysis 8081A_8082

Prep 8290

Analysis 8290

Prep 7470A

Analysis 7470A

Prep 3010A

Analysis 6020

Analysis 9034

Prep 9012A

Analysis 9012A

10 mL 210266 07/28/11 08:04 CTR

210520 07/29/11 20:12 JK

1012.6 mL 10.0 mL 210285 07/28/11 14:42 RBS

211186 08/01/11 22:14 JK

10

I

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00243 mL 20 uL 1209070_P

1209070

50 mL 50 mL 210700

210849

50 rnL 250 mL 210578

211230

250 mL 250 mL 210212

50 mL

—-_ IiTALSAV

TALSAV

TALSAV

TALSAV

TALSAV

TALSAV

TALSAV

TALWSC

TALWSC

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TAL SAV

TAL SAV

TAL SAV

TALSAV

TALSAV .‘

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0

07/28/11 09:00 BG

07/30/11 15:07 SXY

08/02111 09:42 BCB

08/02/11 1703 CE

08/01/11 08:48 BCB

08/06/11 23:38 BB

07/27/11 14:10 CN

50 mL 210574 08)01/11 07:51 DAM

210679 08/02/11 06:54 DAM

Batch Batch Initial Final Batch

Amount —__Amount

5 mL 5 mL

Prepared

Lab

TAL SAV

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Login Sample Receipt Checklist

Client: Ashland Inc. Job Number 680-70758-1 ‘

Login Number: 70758 List Source: TestAmerica Savannah

List Number: I

Creator: Barnett, Eddie T

Question

_______—

-

_______

Answer Comment

Radioactivity either was not measured or, if measured, is at or below N/Abackground

The cooler’s custody seal, if present, is intact. True

The cooler or samples do not appear to have been compromised or Truetampered with

Samples were received on ice. True 8 coolers reed on ice

Cooler Temperature is acceptable. True

Cooler Temperature is recorded True Temp range 2.0 through 5 6 C

CCC is present Truek

CCC is filled out in ink and legible. True

CCC is filled out with all pertinent information. True

Is the Field Sampler’s name present on CCC’? N/A

There are no discrepancies between the sample IDs on the containers and TruetheCCC.

Samples are received within Holding Time. True

Sample containers have legible labels True

Containers are not broken or leaking False Samptes -2, -5 and -6 had broken Liter Ambercontainers associated with them

Sample collection date/times are provided True

Appropnate sample containers are used. True

Sample bottles are completely filled [rue

Sample Preservation Verified True

There is sufficient vol for all requested analyses, mci any requested True Insufficient volume received for MS/MSD

MS/MSDs

VCA sample vials do not have headspace or bubble is <6mm (1/4”) in Truediameter

Multiphasic samples are not present True

Samples do not require splitting or composiling True

Residual Chlorine Checked N/A


of 92

Certification SummaryClient: Ashland Inc. TestAmerica Job ID: 680-70758-1Project/Site: Hercules Hattiesburg APIX 7/26/11

Laboratory Authority Program EPA Region Certification IDTestArneijca Savannah A2LA DoD ELAP 0399-01 —

TestAmerica Savannah A2LA ISO/IEC 17025 399.01

TestAmerica Savannah Alabama Slate Program 4 41450

TestAmerica Savannah Arkansas Arkansas DOH 6 N/ATestAmerica Savannah Arkansas Slate Program 6 88-0692TestAmerica Savannah California NELAC 9 3217CA

TeslAmejica Savannah Colorado State Program 8 N/ATestAmenca Savannah Connecticut State Program 1 PH-0161

TestAmerica Savannah Delaware State Program 3 N/ATestAmerica Savannah Florida NELAC 4 E87052

TestAmerica Savannah Georgia Georgia EPD 4 N/ATestAmerica Savannah Georgia Slate Program 4 803

Test.America Savannah Guam Slate Program 9 09-005rTestAmerica Savannah Hawaii Slate Program 9 N/ATestAmerica Savannah Illinois NELAC 5 200022

TestAmerica Savannah Indiana State Program 5 N/ATestAmerica Savannah Iowa Slate Program 7 353

TestAmerica Savannah Kansas NELAC 7 E-10322

TestAmetica Savannah Kentucky Kentucky UST 4 18TestAmenca Savannah Kentucky Stale Program 4 90084

TestAmerica Savannah Louisiana NELAC 6 LA100015

TestAmerica Savannah Louisiana NELAC 6 30690

TestAmerica Savannah Maine Stale Program 1 GA00006

TestAmerica Savannah Maryland Slate Program 3 250TeslAmerica Savannah Massachusetls State Program 1 M-GAOO6

estAmerica Savannah Michigan Slate Program 5 9925

TestAmerica Savannah Mississippi Slate Program 4 N/ATestAmerica Savannah Montana Slate Program B CERTOOB1

TestAmerica Savannah Nebraska State Program 7 TestAmerica-Savannah

TestAmerica Savannah Nevada State Program 9 GA6TestAmerica Savannah New Jersey NELAC 2 GA769

TestAmerica Savannah New Mexico Slate Program 6 N/ATestAmerica Savannah New York NELAC 2 10842TestAmerica Savannah North Carolina North Carolina DENR 4 269

TestAmerica Savannah North Carolina North Carolina PHL 4 13701

TestAmerica Savannah Oklahoma Slate Program 6 9984

TestAmerica Savannah Pennsylvania NELAC 3 68-00474

TestAmerica Savannah Puerto Rico State Program 2 GA00006TeslAmerica Savannah Rhode Island Slate Program 1 LA000244

TestAmerica Savannah South Carolina State Program 4 98001TestAmerica Savannat Tennessee State Program 4 TN02961

TeslAmenca Savannah Texas NELAC 6 T104704185-08-TX

TestAmerica Savannah USDA USDA SAV 3-04TestAmerica Savannah Vermont State Program 1 87052

TestAmenca Savannah Virginia Stale Program 3 302

TestAmerica Savannah Washington State Program 10 C1794

TestAmerica Savannah West Virginia West Virginia DEP 3 94TestAmerica Savannah West Virginia West Virginia DHHR (DW) 3 9950C

TestAmerica Savannah Wisconsin State Program 5 999819810

TestAmerica Savannah Wyorrnng State Program 8 BTMS-O

TestAmerica West Sacramento USEPA UCMR CA00044

TestAmerica West Sacramento A2LA DoD ELAP 2928-01(‘NestAmerica West Sacramento Alaska Alaska UST 10 UST-055\AestAmerica West Sacramento Arizona State Program 9 A70708


of92

Certification SummaryClient: Ashland Inc. TestAmerica Job ID: 680-70758-1


____

___

_

0Laboratory Authority Program EPA Region Certification ID

TestAmerica West Sacramento Arkansas State Program 6 88-0691

TestAmerica West Sacramento California NELAC 9 111 9CA

TestAmerica West Sacramento Colorado State Program 8 N/A

TestAmerica West Sacramento Connecticut State Program 1 PH-0691

TestAmerica West Sacramento Florida NELAC 4 E87570

TestAmerica West Sacramento Georgia State Program 4 960

TestAmerica West Sacramento Guam State Program 9 N/A

TestAmerica West Sacramento Hawaii State Program 9 N/A

TestAmerjca West Sacramento Illinois NELAC 5 200060

TestAmerica West Sacramento Kansas NELAC 7 E-10375

TestAmerica West Sacramento Louisiana NELAC 6 30612

TestAmerica West Sacramento Michigan State Program 5 9947

TestAmerica West Sacramento Nevada State Program 9 CA44

TestAmerica West Sacramento New Jersey NELAC 2 CA005

TestAmerica West Sacramento New Mexico State Program 6 N/A

TestAmerica West Sacramento New York NELAC 2 11666

TestAmerica West Sacramento Oregon NELAC 10 CA200005

TestAmerica West Sacramento Pennsylvania NELAC 3 68-01272

TestAmerica West Sacramento South Carolina State Program 4 87014

TestAmerica West Sacramento Texas NELAC 6 7104704399-08-TX

TestAmerica West Sacramento US Fish & Wildlife US Fish & Wildlife LE148388-0

TestAmerica West Sacramento USDA USDA P330-09-00055

TestAmerica West Sacramento Utah NELAC 8 QUAN1

TestAmerica West Sacramento Virginia State Program 3 178

TestAmenca West Sacramento Washington Stale Program 10 C581

TestAmerica West Sacramento West Virginia West Virginia DEP 3 334

TestAmerica West Sacramento West Virginia West Virginia DHHR (D 3 9930C

TestAmerica West Sacramento Wisconsin State Program 5 998204680

TestAmerica West Sacramento Wyoming State Program 8 8TMS-Q

Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s

current list of certified methods and analyles.


of 92

TestAmericaTHE LEADER IN ENVIRONMENTAL TESTING

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Savannah5102 LaRoche AvenueSavannah, GA 31404Tel: (912)354-7858

TestAmerica Job ID: 680-70758-2Client Project/Site: Hercules Hattiesburg APIX 7/26/11

For:Ashland Inc.Ashland Hercules Research Center500 Hercules Rd Bldg 8139Wilmington, Delaware 19808

Attn: Timothy I-fassett

t1C?J2 9i2_Authorized for release by:08/10/2011 06:12:29 PM

Lidya GuliziaProject Manager IIIidya.gulizia©testamericainc.com

cc: Craig Derouen

Review your projedresults through

Results relate only to the items tested and the sample(s) as received by the laboratoiy.

The test results in this report meet all 2003 NELAC and 2009 TN! requirements for accredited

parameters, exceptions are noted in this report. This report may not be reproduced except

in full, and with written approval from the Iaborato,y. For questions please contact

the Project Manager at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatoty. Electronic signature

is intended to be the legally binding equivalent of a traditionally handwritten signature.

Page 1 of 18

[

II

LINKS

[

Chris Waters Charlie Jordan

Have a Question?

rN Ask/The

Expert- 4

visit us at:ww.teanecaJnc.&J

-—



Table of ContentsCover Page 1

Table of Contents 2

Case Narrative 3

Sample Summary 4

Method Summary 5

Definitions 6

Client Sample Results 7

Surrogate Summary 9

QC Sample Results 10

QC Association 14

Chronicle 15

Chain of Custody 16

Receipt Checklists 17

Certification Summary 18

0

0Page 2 of 18



-ob ID: 680-70758-2

___________________________________________________________________

Laboratory: TestAmerica Savannah

Narrative

Job Narrative

680-70758-2

Receipt

All samples were received in good condition within temperature requirements.

GCIMS VOA

No analytical or quality issues were noted.

VOA PrepNo analytical or quality issues were noted.

CommentsNo additional comments.

TestAmenca Savannah

Page 3 of 18

Sample SummaryClient: Ashland Inc.ProjectlSite: Hercules Hattiesburg APIX 7126/11

Lab Sample ID Client Sample ID

680-70758-8 - -— ASI-1-MW21-07261 1

Matrix Collected Received

Water 07/26/11 15:03 07/27/11 09:20


0

0


Page 4 of 18

Method SummaryClient: Ashland Inc. TestAmerica Job ID: 680-70758-2 IV

(jeHerculesHaftesburAX7/26/li

___ __

-__

Method Method Description Protocol Laboratory

82608 Volatile Organic Compounds (GC/MS) SWB4B TAL SAV

Protocol References:

SW846 = Test Methods For Evaluating Solid Waste, PhysicallChemical Methods”, Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858


Page 5 of 18

DefinitionslGlossaryClient: Ashland Inc. TestAmerica Job ID: 680-70758-2


__

________

0Abbreviation These commonly used abbreviations may or may not be present In this report.

Listed under the ‘D column to designate that the result is reported on a dry weight basis.

EPA United States Environmental Protection Agency

ND Not Detected above the reporting level

MDL Method Detection Limit

RL Reporting Umit

RE, RE1 (etc.) indicates a Re-extraction or Reanalysis of the sample.

%R Percent Recovery

RPD Relative Percent Difference, a measure of the relative difference between two points.


Page 6 of 18

Client: Ashland Inc.rojectlSite: Hercules Hattiesburg APIX 7/26/11

lient Sample ID: ASH-MW2I -072611Date Collected: 07/26111 15:03Date Received: 07127111 09:20



Method: 8260B - Volatile Organic Compounds (GCIMS)Analyte Result Qualifier RL

Acetone <1300 1300

Acetonitrile <2000 2000

Acrolein <1000 1000

Acrylonitrile <1000 1000

Benzene 3200 50

Dichlorobromomethane <50 50

Bromoform <50 50

Bromomethane <50 50


Carbon disulfide <100 100

Carbon tetrachloride <50 50

Chlorobenzene 150 50

2-Chloro-l 3-butadiene <50 50

Chloroethane <50 50

Chloroform 4300 50

Chiorornethane <50 50

3-Chloro-1-propene <50 50

Chlorodibromomethane <50 50

l2-Dibromo-3-Chloropropane <50 50

Ethylene Dibromide <50 50

Dibromomethane <50 50

trans-14-Dichloro-2-butene <100 100

Dichlorodifluoromethane <50 50

11-Dichloroethane <50 50

12-Dichloroethane <50 50

cis-1 2-Dichioroethene <50 50

trans-i 2-Dichloroethene <50 50

11-Dichioroethene <50 50

12-Dichloropropane <50 50

cia-i 3-Dichloropropene <50 50

trans-i,3-Dichloropropene <50 50

Ethylbenzene <50 50

Ethyl methacrylate <50 50

2-Hexanone <500 500

iodomethane <250 250

Isobutyl alcohol <2000 2000

Methacrylonitrile <1000 1000

Methylene Chloride <250 250

Methyl methacrylate <50 50

4-Methyi-2-pentanone (MIBK) <500 500

Pentachloroethane <250 250

Propionitrile <1000 1000

Styrone <50 50

1 1 1 2-Tetrachloroethane <50 50

1122-Tetrachloroethane <50 50

Tetrachloroethene <50 50

Toluene 2600 50

ill-Trichloroethane <50 50

1 1 2-Trichloroethane <50 50

Trichloroethene <50 50

MDL Unit P Prepared

ug/L

ug/L

ug/L

ug/L

ugIL

ug/L

ug/L

ug/L

ug/L

ug/L

ugIL

ug/L

ug/L

ug/L

ug/L

ugiL

ug/L

ugIL

ugiL

ug/L

ug/L

ug/L

ug!L

ug/L

ug/L

ug/L

ug!L

ug!L

ug!L

ug/L

ug/L

ug/L

ug!L

ug/L

ug!L

ug/L

ug/L

ug/L

ug/L

ugIL

ugiL

ug/L

ugIL

ug!L

ug/L

ugIL

ug/L

ug/L

ug!L

ug/L

Analyzed DII Fac

07/30111 07:05 50

07/30/il 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07130/11 07:05 50

07/30Il 1 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/il 07:05 50

07)30/11 07:05 50

07/30/il 07:05 50

07/30/11 07:05 50

07/30/li 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/li 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/li 07:05 50

07/30/il 07:05 50

07/30/il 07:05 50

07/30/11 07:05 50

07/30/il 07:05 50

07)30/11 07:05 50

07/30/11 07:05 50

07/30/il 07:05 50

07/30/11 07:05 50

07/30(11 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/11 07:05 50

07/30/il 07:05 50

07/30/11 07:05 50

07/30/11 0705 50

07/30/11 07:05 50

07/30/il 07:05 50

07/30/il 07:05 50

07/30/li 07:05 50

07/30/11 07:05 50

07/30/il 07:05 50

07/30/11 07:05 50

07/30/il 07:05 50


Page 7 of 18


Client: Ashland Inc.TestAmerica Job ID: 680-70758-2


Client Sample ID: ASH-MW2I-072611 Lab Sample ID:680-70758-8 CDDate Collected: 07/26I11 15:03

Matrix: Water



Analyle Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

Trichiorofluoromethane <50 50 uglt. 07130111 07:05 50

1,2,3-Trichloropropane <50 50 ugIL 07130111 07:05 50

Vinyl acetate <100 100 uglL 07130l11 07:05 50

Vinyl chloride <50 50 ug/L 07130111 07:05 50

Xylenes, Total <100 100 ugIL 07l30l11 07:05 50

Surrogate % Recovery Qualifier Limits Prepared — Analyzed DII Fac

4-Bromofluorobenzene 92 70- 130 07/30/11 07:05 50

Djbromofluoromethane 107 7O 130 07/30/1107:05 50

Toluene-d8 (Surr) 100 70 130 07/30/11 07:05 50

0


Page 8 of 18

Surrogate SummaryClient: Ashland Inc. TestAmerica Job ID: 680-70758-2


ethod: 8260B - Volatile Organic Compounds (GC!MS)Matrix: Water

__________ _______ ______ ______ _____

Prep Type: Total/NA


SF8 DBFM TOL

Lab Sample ID Client Sample ID (70-130) (70-1 30) (70-1 30)

680-70758-8 ASI-i-MW21-07261 1 92 107 100

LCS 680-21054314 Lab Control Sample 104 108 101

LCSD 680-21054315 Lab Control Sample DUP 102 103 101

MB 680-21054317 Method Blank 93 107 100

Surrogate Legend

BFB = 4-Bromofluorobenzene -

DBFM = Dibromofluoromethane

TOL = Toiuene-d8 (Surr)


Page 9 of 18

QC Sample Results



Method 8260 B - VotatleOrgarncCompounds(GCIMS)

___ ___

- — QLab Sample ID: MB 680-210543/7 Client Sample ID: Method Blank

Matnx WaterPrep Type Total/NA

Analysis Batch: 210543MBMB

Analyte Result Qualifier RL MDL unit D Prepared Analyzed DII Fac

Acetone <25 25 ug/L 07/30/11 0043 1

Acetonitrile <40 40 ug/L 07/30/11 00:43 1

I Acrolein <20 20 ug/L 07/30/11 00:43 1


Benzene <1.0 1.0 ug/L 07/30/11 00:43 1

Dichlorobromomethane <1.0 1.0 ug/L 07/30111 00:43 1

Bromoforrn <1.0 1.0 ug/L 07/30/11 00:43 1

Bromomethane <1.0 1.0 ugIL 07/30/11 00:43 1

2-Butanone (MEK) <10 10 ug/L 07/30(11 00:43 1

Carbon disulfide <2.0 2.0 UQ/L 07/30/11 00:43 1

Carbon tetrachloride <1.0 1.0 ugIL 07/30/11 00:43 1

Chlorobenzene <1.0 1.0 ugIL 07130/11 00:43 1

2-Chloro-13-butadiene <1.0 1.0 ugIL 07/30111 00:43 1

Chloroethane <1.0 1.0 ugIL 07/30(11 00:43 1

Chloroform <1.0 1.0 ug/L 07/30/11 00:43 1

Chloromethane <1.0 1.0 ug/L 07/30(11 00:43 1

3-Chloro-1-propene <1.0 1.0 ug/L 07/30/11 00:43 1

Chlorodibromomethane <1.0 1.0 ug/L 07/30/11 00:43 1

1,2-Dibromo-3-Chloropropane <1.0 1.0 ug/L 07/30/11 00:43 1

Ethylene Dibromide <1.0 1.0 ugIL 07/30(11 00:43 1

Dibromomethane <1.0 1.0 ug/L 07/30/11 00:43 1

trans-i ,4-Dicliloro-2-butene <2.0 2.0 ug/L 07/30/11 00:43

Dichlorodifluoromethane <1.0 1.0 ug/L 07/30/11 00:43 1

11-Dichloroethane <1.0 1.0 ug/L 07/30(11 00:43 1

1,2-Dichloroethane <1.0 1.0 ugIL 07/30(11 00:43 1

I cis-12-Dichloroethene <1.0 1.0 ugh 07/30/11 00:43 1

trans-1,2-Dichloroethene <1.0 1.0 ug/L 07/30/11 00:43 1

1,1-Dichloroethene <1.0 1.0 ugIL 07/30/11 00:43 1

1,2-Dichloropropane <1.0 1.0 ugIL 07/30/11 00:43 1

cis-1,3-Dichloropropene <1.0 1.0 ugIL 07/30/11 00:43

trans-1,3-Dichloropropene <1.0 1.0 ug/L 07130/11 00:43 1

Ethylbenzene <1.0 1.0 ugIL 07130/11 00:43 1

Ethyl methacrylate <1.0 1.0 ug/L 07/30/11 00:43 1

2-Hexanone <10 10 ugIL 07/30/11 00:43 1

lodomethane <5.0 5.0 ug/L 07/30/11 00:43 1

Isobutyl alcohol <40 40 ug/L 07/30/11 00:43 1

Melhacrylonhtrile <20 20 ug/L 07/30/11 00:43 1

Methylene Chloride <5.0 5.0 ug/L 07/30/11 00:43

Methyl methacrylate <1.0 1.0 ug/L 07/30/11 00:43 1

4-Methyl-2-pentanone (MIBK) <10 10 ug!L 07/30)11 00:43 1

Pentachloroethane <5.0 5.0 ugIL 07(30/11 00:43 1

Propionitrile <20 20 ug!L 07/30)11 00:43 1

Styrene <1.0 1.0 ugIL 07/30/11 00:43 1

1,1 ,1,2-Tetrachloroethane <1.0 1.0 ugIL 07/30/11 00:43 1

1,1,2,2-Tetrachloroethane <1.0 1.0 ugIL 07/30/11 00:43 1

Telrachioroethene <1.0 1.0 ug!L 07/30/11 00:43 1

Toluene <1.0 1.0 ug/L 07/30/11 00:43 1

1,11-Tnchloroethane <1.0 1.0 ug/L 07/30/11 00:43 1

1,1,2-Trichloroethane <1.0 1.0 ug/L 07/30/11 00:43 1


Page 10 of 18


,,—roject/Sfte: Hercules Hattiesburg APIX 7/26/11

1thod: 8260B - Volatile Organic Compounds (GC!MS) (Continued) —_________

________



Analysis Batch: 210543MBMB

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac

Trichloroethene <1.0 - 1.0 — ug/L 07130111 00:43 1

Tnchlorofluorornethane <1.0 1.0 ug/L 07/30/11 00:43 1

1,23-Trichloropropane <1.0 1.0 ugIL 07130111 00:43 1

I Vinyl acetate <2.0 2.0 uglI. 07130111 00:43 1

Vinyl chlonde <1.0 1.0 ugIL 07/30111 00:43 1

Xylenes, Total <2.0 2.0 uglL 07/30111 00:43 1

MB MB

Surrogate % Recovery Qualifier -__Limits Prepared Analyzed Dii Fec

4-Bromofluorobenzene — 93 70. 130 07/30/11 00:43 1

I Dibromofluoromethane 107 70. 130 07/30/11 00:43 1

Toiuene-d8 (Surr) 100 70. 130 07/30/11 00:43 1




Analyte Added Result Qualifier Unit 0 % Rec LimIts

Acetone 100 129 ugIL 129 26. 180

Benzene 50.0 50.0 ugIL 100 70. 130

Dichlorobromomethane 50.0 46.3 uglL 93 70.130

‘Bromoform 50.0 38.1 ugIL 76 70-130

Bromomethane 50.0 25.4 ugIL 51 23. 165

2.Butanone(MEK) 100 iii ug/1_ 111 49. 172

Carbon disulfide 50.0 48.0 U9IL 96 54.132

Carbon tetrachloride 50.0 41.3 u9/L 83 70. 130

Chlorobenzene 50.0 52.5 ug/L 105 70.130

Chloroethane 50.0 50.0 ugIL 100 56. 152

Chloroform 50.0 52.0 ugIL 104 70.130

Chloromethane 50.0 50.7 ugIL 101 70.130

Chlorodibromomethane 50.0 43.3 ugIL 87 70.130

I 12.Dibromo.3-Chloropropane 50.0 41.0 ug/L 82 70.130

EthyleneDibromide 50.0 49.6 ug/L 99 70.130

Dibromomethane 50.0 51.6 ug/L 103 70.130

Dichlorodifluoromethane 50.0 49.9 ugIL 100 44.146

1,1-Dichloroethane 50.0 49.8 ug/L 100 70. 130

1.2-Dichloroethane 50.0 50.7 ug/L 101 70.130

cis-1,2-Dichloroethene 50.0 51.7 uglL 103 70.130

trans-i .2-Dichloroethefle 50.0 51.5 ug/L 103 70. 130

1,1-Dichloroethene 50.0 52.0 ug/L 104 66. 131

1,2-Dichloropropane 50.0 49.4 ugIL 99 70.130

cis-1,3-Dichloropropefle 50.0 45.8 ug/L 92 70. 130

trans-i ,3.Dichloropropene 50.0 43.9 ug!L 88 70. 130

Ethylbenzene 50.0 51.1 ug/L 102 70. 130

2-HexanOfle 100 114 ugIL 114 42-185

Methylene Chloride 50.0 53,2 ug/L 106 67-130

4-Methyl.2-pentanone(MIBK) 100 94.4 ug/L 94 70. 130

Styrene 50.0 54.3 ugIL 109 70. 130

111,2-Tetrachloroethane 50.0 46.0 ugIL 92 70. 130

1,1,2,2-Tetrachloroethane 50.0 51.3 ug!L 103 70. 130


Page 11 ofl8

QC Sample ResultsClient Ashland Inc. TestAmerica Job ID: 680-70758-2



____ ______ ____

ULab Sample ID: LCS 680-21054314 Client Sample ID: Lab Control Sample



Analyte Added Result QualIfier Unit 0 % Rec Limits

Tetrachloroethene 50.0 64.7 ug/L 109 70. 130

Toluene 50.0 48.5 ugIL 97 70. 130

111-Trichloroethane 50.0 47.9 ugIL 96 70- 130

1,1,2-Tnchloroethane 50.0 48.9 ugIL 98 70- 130

Tnchloroethene 50.0 53.2 ugIL 106 70- 130

rrichlorofluoromethane 50.0 52.1 ug/L 104 55. 156

123-Thchloropropane 50.0 53.4 uglL 107 70-130

Vinyl acetate 100 95.3 ugIL 95 60-176

Vinyl chloride 50.0 50.8 uglL 102 67. 134

Xylenes, Total 150 159 uglL 106 70- 130

LCS LCS

Surrogate % Recovery Qualifier Limits__-

4-Bromofluorobenzene — 104 70- 130


Toluene-d8 (Surr) 101 70. 130




Analyte

____________ ____________

— Added Result Qualifier Unit D %Rec Limits RPD LImIt

Acetone 100 131 uglL 131 26_iSO 1 50

Benzene 50.0 48.4 ug!L 97 70. 130 3 30

Dichlorobromomethane 50.0 46.6 ug/L 93 70.130 1 30

Bromoform 50.0 38.7 ugIL 77 70.130 2 30

Bromomethane 50.0 24.5 ug/L 49 23.165 4 50

I 2-Butanone (MEK) 100 111 ug/L 111 49.172 0 30

Carbon disulfide 50.0 44.8 ug/L 90 54. 132 7 30

Carbon tetrachloride 50.0 40.2 ugIL 80 70-130 3 30

Chlorobenzene 50.0 51.2 ugiL 102 70.130 3 30

Chloroethane 50.0 38.6 ugIL 77 56. 152 26 40

Chloroform 50.0 49.8 ug/L 100 70. 130 4 30

Chloromathane 50.0 48.1 uglL 96 70-130 5 30

Chlorodibromomethane 50.0 42.6 uglL 85 70- 130 2 50

12-Dibromo-3-Chloropropane 50.0 39.3 ugIL 79 70-130 4 50

Ethylene Dibromide 50.0 52.4 ug/L 105 70-130 6 30

Dibromomethane 50.0 52.1 ugIL 104 70.130 1 30

Dichlorodifluoromethane 50.0 46.8 ugIL 94 44.146 6 50

1,1-Dichloroethane 50.0 46.8 ugiL 94 70. 130 6 30

12-Dichloroethane 50.0 50.8 ugIL 102 70.130 0 30

cia-i ,2.Dichloroothene 50.0 49.7 ugIL 99 70.130 4 30

trans-1,2-Dichloroethene 50.0 48.8 U9/L 98 70-130 5 30

I 1,1-Dichloroethene 50.0 49.4 uglL 99 66.131 5 30

1,2-Dichloropropane 50.0 48.7 uglL 97 70.130 2 30

Icis-1,3-Dichloropropene 50.0 48.5 ugh. 93 70- 130 2 30

trans-1,3-Dichloropropene 50.0 45.5 ug/L 91 70.130 4 50

Ethylberrzene 50.0 48.0 ugiL 96 70. 130 6 30

2-Hexanone 100 112 ugIL 112 42- 185 2 30

Methylene Chloride 50.0 50.8 ugIL 102 67. 130 5 30


Page 12 of 18


(__RoJectISite: Hercules Hattiesburg APIX 7/26/11

‘1ethod: 8260B - Volatile Organic Compounds (GCIMS) (Continued)

____________—

Lab Sample ID: LCSD 680-21054315 Client Sample ID: Lab Control Sample DupMatrix: Water Prep Type: Total/NAAnalysis Batch: 210543

Spike LCSD LCSD % Rec. RPD

Analyte Added Result Qualifier Unit D % Rec Limits RPD Limit

4-Methyl.-2-pentanorie(MIBK) 100 98.5 ug/L. — 98 70130 4 30

Styrene 50.0 53.6 ugIL 107 70.130 1 30

11,1,2-Tetracliloroethane 50.0 44.8 ugIL 90 70- 130 3 30

1,1,2,2-Tetraciiloroethane 50.0 50.9 ugIL 102 70.130 1 30

Tetrachloroethene 50.0 51.6 ugiL 103 70.130 6 30

Toluene 50.0 49.1 uglL 98 70. 130 1 30

1,1,1-Tnchloroethane 50.0 46.7 ugiL 93 70-130 3 30

1,1,2-Tnchloroethane 50.0 51.6 ugIL 103 70 130 6 30 0Tnchloroethene 50.0 50.5 ugIL 101 70. 130 5 30

Trichlorofluoromethane 50.0 48.3 ug/L 97 55- 156 8 30

1,2,3-Tnchloropropane 50.0 53.3 ug/L 107 70-130 0 30

Vinyl acetate 100 94.3 ugIL 94 60- 176 1 30

Vinyl chloride 50.0 47.8 ugIL 96 67- 134 6 30

Xylenes, Total 150 153 ug!L 102 70-130 4 30

LCSD LCSD

Surrogate % Recovesy Qualifier Limits

4-Bromofluombenzene 102 70- 130


Toluene-d8(Surr) 101 70.130


Page 13of18

QC Association Summary


Client Sample ID Prep Type

Lab Control Sample -Total/NA

Lab Control Sample Dup Total/NA

Method Blank Total/NA

ASHMW21-07261 1 Total/NA


Matrix Method Prep Batch

Water 826DB

Water 826GB

Water 82608

Water 8260B


0

0

Lab Sample ID

LCS 680-21054314

LCSD 680-210543/5

MB 680-210543/7

680-70758-8

GCIMS VOA

____


0

Page 14 of 18

Lab ChronicleClient: Ashland Inc.Project/Site: Hercules Hattiesburg APIX 7)26/11

lient Sample ID: ASH-MW2I -072611Date Collected: 07/26)11 15:03Date Received: 07127/11 09:20

____________

r Batch Batch Dii

Prep Type Type Method Run Factor

LT0ta Analysis 826DB 50



Initial Final Batch Prepared

Amount Amount Number Or Analyzed Analyst Lab

5 mL — 5 mL 210543 07130111 07:05 AJMC TAL SAV

Laboratory References:TAL SAV = TestAmenca Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858

TestAnierica Savannah

Page 15 of 18

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Login Sample Receipt Checklist

0Client: Ashland Inc. Job Number: 680-70758-2

Login Number: 70758 List Source: TestAmerica SavannahList Number: ‘ICreator: Barnett, Eddie T

Question Answer Comment —- —___________

Radioactivity either was not measured or, if measured, is at or below N/Abackground

The cooler’s custody seal, if present, is intact. True

The cooler or samples do not appear to have been compromised or Truetampered with.

Samples were received on ice. True 8 coolers rec’d on ice

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True Temp range 2.0 through 5.6 C

CCC is present. True

CCC is filled out in ink and legible. True

CCC is filled out with all pertinent information. True

Is the Field Sampler’s name present on CCC? N/A

There are no discrepancies between the sample IDs on the containers and Truethe CCC.

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. False Samples -2, -5 and -6 had broken Liter Amber

Q containers associated with them.

ample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

Sample Preservation Verified. True

There is sufficient vol. for all requested analyses, md. any requested True Insufficient volume received for MS/MSD.MS/MSDs

VOA sample vials do not have headspace or bubble is <6mm (1/4’) in Truediameter.

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Residual Chlorine Checked. N/A


Page 17 of 18

Certification Summary

Client: Ashland Inc.TestAmerica Job ID: 680-70758-2


__________

___-_---

_______

Laboratory Authority Program EPA Region Certification ID\_j

TestAmer/ca Savannah A2LA - DoD ELAP 0399-01

TestArnerica Savannah A2LA ISOIIEC 17025 399.01

TestAmenca Savannah Alabama State Program 4 41450

TestAmenca Savannah Arkansas Arkansas DOH 6 N/A

TestAmerica Savannah Arkansas State Program 6 88-0692

TestAmenca Savannah California NELAC 9 3217CA

TestAmenca Savannah Colorado State Program 8 N/A

TestAmenca Savannah Connecticut State Program 1 PH-0161

TestAmerica Savannah Delaware State Program 3 N/A

TestAmenca Savannah Florida NELAC 4 E87052

TestAmerica Savannah Georgia Georgia EPD 4 N/A

TestAmenca Savannah Georgia State Program 4 803

TestAmenca Savannah Guam State Program 9 09-005r

TestAmerica Savannah Hawaii State Program 9 N/A

TestAmerica Savannah Illinois NELAC 5 200022

TestAmerica Savannah Indiana State Program 5 NIA

TestAmerica Savannah Iowa State Program 7 353

TestAmenca Savannah Kansas NELAC 7 E 10322

TestAmerica Savannah Kentucky Kentucky UST 4 18

TestAmenca Savannah Kentucky State Program 4 90084

TestAmenca Savannah Louisiana NELAC 6 30690

TestAmerica Savannah Louisiana NELAC 6 LA1 00015

TeslAmerica Savannah Maine State Program 1 GA00006

TestAmerica Savannah Maryland State Program 3 250

TestAmertca Savannah Massachusetts State Program 1 M-GAOO6

TestAmerica Savannah Michigan State Program 5 9925

TestAmerica Savannah Mississippi State Program 4 N/A

TestAmerica Savannah Montana State Program 8 CERTOO81

TestAmerica Savannah Nebraska State Program 7 TestAmerica-Savannah

TestAmerica Savannah Nevada State Program 9 GA6

TestAmerica Savannah New Jersey NELAC 2 GA769

TestAmerica Savannah New Mexico Stale Program 6 N/A

TeslAmerica Savannah New York NELAC 2 10842

TestAmerica Savannah North Carolina North Carolina DENR 4 269

TestAmerica Savannah North Carolina North Carolina PHL 4 13701

TestAmerica Savannah Oklahoma State Program 6 9984

TestAmedca Savannah Pennsylvania NELAC 3 68-00474

Test.America Savannah Puerto Rico State Program 2 GA00006

TestAmerica Savannah Rhode Island State Program 1 LA000244

TestAmenca Savannah South Carolina State Program 4 98001

TestAmerica Savannah Tennessee State Program 4 TN02961

TestAmerica Savannah Texas NELAC 6 T104704185-08-TX

TestAmerica Savannah USDA USDA SAV 3-04

TestAmerica Savannah Vermont State Program 1 87052

TestAmerica Savannah Virginia State Program 3 302

TestAmer/ca Savannah Washington Stale Program 10 C1794

TestAmerica Savannah West Virginia West Virginia DEP 3 94

TestAmerica Savannah West Virginia West Virginia DHHR (OW) 3 9950C

TestAmerica Savannah Wisconsin State Program 5 999819810

TestAmerica Savannah ‘iioming State Program 8 8TMS-Q

Accreditation may not be offered or required for all methods and arialytes reported in this package. Please contact your project manager for the laboratorys

current list of certified methods and analytes.


Page 18 of 18

TestAmerica Laboratories, Inc. ANALYTICAL REPORT ...

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