TEKLAB, INC. - Ameren · PDF fileteklab, inc. environmental testing laboratory 5445 horseshoe...

TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY

5445 HORSESHOE LAKE ROAD

COLLINSVILLE, ILLINOIS 62234

TEL: 618-344-1004

FAX: 618-344-1005

June 22, 2009

NELAP Accredited #100226

Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. IL ELAP and NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column.

All quality control criteria applicable to the test methods employed for this project have been satisfactorily met and are in accordance with NELAP except where noted. The following report shall not be reproduced, except in full, without the written approval of Teklab, Inc.

If you have any questions regarding these tests results, please feel free to call.

Sincerely,

WorkOrder: 09060783A831-735002-012901-225/Ameren Champaign 62403053

RE:

Dear Pete Sazama:

TEKLAB, INC received 3 samples on 6/18/2009 5:55:00 PM for the analysis presented in the following report.

210 West Sand Bank RoadColumbia, IL 62236-0230

(618) 281-7173(618) 281-5120

TEL:FAX:

Pete SazamaPSC Industrial Outsourcing, LP

Heather A. WhiteProject Manager

(618)344-1004 ex 20

IL ELAP and NELAP Accredited - Accreditation #100226 of 54

Project: A831-735002-012901-225/Ameren Champaign 62403053Client: PSC Industrial Outsourcing, LP

Lab Order: 09060783

SAMPLE SUMMARY

Report Date: 22-Jun-09

Lab Sample ID Client Sample ID Collection Date




TEL: 618-344-1004

FAX: 618-344-1005

Fractions

09060783-001 CBA-01 6/18/2009 1:30:00 PM6

09060783-002 CBA-02 6/18/2009 1:50:00 PM6

09060783-003 CBA-03 6/18/2009 2:10:00 PM6





TEL: 618-344-1004

FAX: 618-344-1005

A831-735002-012901-225/Ameren Champaign 624030530906078322-Jun-09

Project:LabOrder:

Client:

Report Date:

CASE NARRATIVEPSC Industrial Outsourcing, LP

Cooler Receipt Temp: 4.2 °C

State accreditations:

KS: NELAP #E-10347 | KY: UST #0073 | MO: DNR #00930 | AR: ADEQ #70-028-0

Qualifiers

- Analyte detected below reporting limits

- Analyte detected in the associated Method Blank

- Spike Recovery outside accepted recovery limits

- RPD outside accepted recovery limits- Not Detected at the Reporting Limit - Value above quantitation range

- Value exceeds Maximum Contaminant Level

- Reporting Limit

- Dilution Factor

- Too numerous to count ( > 200 CFU )

- Diluted out of sample

- Holding time exceeded- Surrogate Standard added by lab

- Matrix interference

- IL Dept. of Public Health- IL ELAP and NELAP Accredited Field of Testing

DF

RL

TNTC

Surr

IDPH

B

J

R

S

X

NELAP

E

MI

H

ND

D

- Did not igniteDNI- Unknown hydrocarbon#- QC criteria failed or noncompliant CCVQ

- Client requested RL below PQLC


Client Project: A831-735002-012901-225/Ameren C

Collection Date: 6/18/2009 1:30:00 PM

Matrix: SOLID

Client: PSC Industrial Outsourcing, LP


LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-001

Client Sample ID: CBA-01

Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual




TEL: 618-344-1004

FAX: 618-344-1005

ASTM D2974Percent Moisture 6/18/2009 7:00:00 PM0.1 % 122.9 MAB

STANDARD METHODS 18TH ED. 2540 GTotal Solids 6/18/2009 7:00:00 PM0.1 % 177.1 MAB

SW-846 3050B, 6010B, METALS BY ICPArsenic 6/19/2009 1:14:06 PM2.36 mg/Kg-dry 15.04 LALNELAP

Barium 6/19/2009 1:14:06 PM0.47 mg/Kg-dry 1124 LALNELAP

Cadmium 6/19/2009 1:14:06 PM0.19 mg/Kg-dry 10.35 LALNELAP

Chromium 6/19/2009 1:14:06 PM0.94 mg/Kg-dry 119.8 LALNELAP

Lead 6/19/2009 1:00:26 PM3.77 mg/Kg-dry 116.8 LALNELAP

Silver 6/19/2009 1:14:06 PM0.52 mg/Kg-dry 1< 0.52 LALNELAP

SW-846 3050B, METALS BY GFAASelenium 7740 J 6/19/20090.556 mg/Kg-dry 10.33 MEKNELAP

SW-846 3550B, 8081A, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

4,4´-DDE 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

4,4´-DDT 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Alachlor 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Aldrin 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

alpha-BHC 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

alpha-Chlordane 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

beta-BHC 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Chlordane 6/19/2009 9:40:00 PM4.27 µg/Kg-dry 1ND HENELAP

delta-BHC 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Dieldrin 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Endosulfan I 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Endosulfan II 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Endosulfan sulfate 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Endrin 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Endrin aldehyde 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Endrin ketone 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

gamma-BHC 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

gamma-Chlordane 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HE

Heptachlor 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Heptachlor epoxide 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Methoxychlor 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP

Toxaphene 6/19/2009 9:40:00 PM38.4 µg/Kg-dry 1ND HENELAP

Surr: Decachlorobiphenyl 6/19/2009 9:40:00 PM48-149 %REC 153.6 HE

Surr: Tetrachloro-m-xylene 6/19/2009 9:40:00 PM19-145 %REC 129.7 HE




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-001






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 6/19/2009 10:25:00 AM47.9 µg/Kg-dry 1ND MAMNELAP

Aroclor 1221 6/19/2009 10:25:00 AM47.9 µg/Kg-dry 1ND MAMNELAP






Surr: Decachlorobiphenyl 6/19/2009 10:25:00 AM5-156 %REC 159.6 MAM

Surr: Tetrachloro-meta-xylene 6/19/2009 10:25:00 AM7.35-123 %REC 128.5 MAM

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 1ND MAMNELAP

Acenaphthylene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 1ND MAMNELAP

Anthracene J 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.004 MAMNELAP

Benzo(a)anthracene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.036 MAMNELAP

Benzo(a)pyrene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.042 MAMNELAP

Benzo(b)fluoranthene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.063 MAMNELAP

Benzo(g,h,i)perylene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.032 MAMNELAP

Benzo(k)fluoranthene R 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.023 MAMNELAP

Bis(2-ethylhexyl)phthalate S 6/19/2009 10:54:00 AM0.087 mg/Kg-dry 10.166 MAMNELAP

Chrysene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.049 MAMNELAP

Dibenzo(a,h)anthracene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.007 MAMNELAP

Fluoranthene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.111 MAMNELAP

Fluorene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 1ND MAMNELAP

Indeno(1,2,3-cd)pyrene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.027 MAMNELAP

Naphthalene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 1ND MAMNELAP

Phenanthrene R 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.039 MAMNELAP

Pyrene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.088 MAMNELAP

Surr: 2-Fluorobiphenyl 6/19/2009 10:54:00 AM10-131 %REC 147.5 MAM

Surr: Nitrobenzene-d5 6/19/2009 10:54:00 AM10-132 %REC 150.1 MAM

Surr: p-Terphenyl-d14 6/19/2009 10:54:00 AM30.6-131 %REC 168.5 MAM

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

1,2-Dichlorobenzene 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP



2,4,5-Trichlorophenol 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP


2,4-Dichlorophenol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-001






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2,4-Dimethylphenol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

2,4-Dinitrophenol 6/20/2009 2:55:00 PM6.52 mg/Kg-dry 5ND DMHNELAP

2,4-Dinitrotoluene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP


2-Chloronaphthalene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

2-Chlorophenol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

2-Methoxy-4-methylphenol 6/20/2009 2:55:00 PM4.24 mg/Kg-dry 5ND DMH

2-Methylnaphthalene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

2-Nitroaniline 6/20/2009 2:55:00 PM6.52 mg/Kg-dry 5ND DMHNELAP

2-Nitrophenol 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

3,3´-Dichlorobenzidine 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP


4,6-Dinitro-2-methylphenol 6/20/2009 2:55:00 PM6.52 mg/Kg-dry 5ND DMHNELAP

4-Bromophenyl phenyl ether 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

4-Chloro-3-methylphenol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

4-Chloroaniline 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

4-Chlorophenyl phenyl ether 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP



Aniline 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

Azobenzene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMH

Benzidine 6/20/2009 2:55:00 PM6.89 mg/Kg-dry 5ND DMHNELAP

Benzoic acid 6/20/2009 2:55:00 PM9.78 mg/Kg-dry 5ND DMHNELAP

Benzyl alcohol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

Bis(2-chloroethoxy)methane 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

Bis(2-chloroethyl)ether 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

Bis(2-chloroisopropyl)ether 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

Butyl benzyl phthalate 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

Carbazole 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMH

Dibenzofuran 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

Diethyl phthalate 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

Dimethyl phthalate 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

Di-n-butyl phthalate 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

Di-n-octyl phthalate 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

Hexachlorobenzene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

Hexachlorobutadiene 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

Hexachlorocyclopentadiene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

Hexachloroethane 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-001






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSIsophorone 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

m,p-Cresol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

Nitrobenzene 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

N-Nitrosodimethylamine 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

N-Nitroso-di-n-propylamine 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

N-Nitrosodiphenylamine 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

o-Cresol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

Pentachlorophenol 6/20/2009 2:55:00 PM13.0 mg/Kg-dry 5ND DMHNELAP

Phenol 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP

Pyridine 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP

1,2-Diphenylhydrazine 6/20/2009 2:55:00 PM5.48 mg/Kg-dry 5ND DMH

Surr: 2,4,6-Tribromophenol 6/20/2009 2:55:00 PM32.7-130 %REC 569.0 DMH

Surr: 2-Fluorobiphenyl 6/20/2009 2:55:00 PM34.1-116 %REC 556.9 DMH

Surr: 2-Fluorophenol 6/20/2009 2:55:00 PM30.5-99 %REC 565.0 DMH

Surr: Nitrobenzene-d5 6/20/2009 2:55:00 PM34.1-101 %REC 562.9 DMH

Surr: Phenol-d5 6/20/2009 2:55:00 PM34.9-110 %REC 569.3 DMH

Surr: p-Terphenyl-d14 6/20/2009 2:55:00 PM41.7-124 %REC 574.7 DMH

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

1,1,1-Trichloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

1,1,2,2-Tetrachloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

1,1,2-Trichloro-1,2,2-trifluoroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSA


1,1-Dichloro-2-propanone 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSA

1,1-Dichloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

1,1-Dichloroethene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

1,1-Dichloropropene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

1,2,3-Trichlorobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

1,2,3-Trichloropropane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP

1,2,3-Trimethylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSA


1,2,4-Trimethylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

1,2-Dibromo-3-chloropropane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

1,2-Dibromoethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

1,2-Dichlorobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP


1,2-Dichloropropane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP





Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-001






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,3-Dichlorobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP



1-Chlorobutane J 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 11.6 JSANELAP


2-Butanone 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP

2-Chlorotoluene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

2-Hexanone 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP

2-Nitropropane 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP


4-Methyl-2-pentanone 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP

Acetone J 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 130 JSANELAP

Acrolein 6/18/2009 7:17:00 PM109 µg/Kg-dry 1ND JSANELAP

Acrylonitrile 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP

Allyl chloride 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Benzene 6/18/2009 7:17:00 PM1.1 µg/Kg-dry 1ND JSANELAP

Bromobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Bromochloromethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Bromodichloromethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Bromoform 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Bromomethane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP

Carbon disulfide 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Carbon tetrachloride 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Chlorobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Chloroethane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP

Chloroform 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Chloromethane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP

cis-1,2-Dichloroethene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

cis-1,3-Dichloropropene 6/18/2009 7:17:00 PM4.4 µg/Kg-dry 1ND JSANELAP

Cyclohexanone 6/18/2009 7:17:00 PM109 µg/Kg-dry 1ND JSA

Dibromochloromethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Dibromomethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Dichlorodifluoromethane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP

Ethyl acetate 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP

Ethyl ether 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Ethyl methacrylate 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Ethylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Heptane 6/18/2009 7:17:00 PM21.9 µg/Kg-dry 1ND JSA




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-001






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorobutadiene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Hexachloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Iodomethane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP

Isopropylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

m,p-Xylenes 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Methacrylonitrile 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP

Methyl Methacrylate 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Methyl tert-butyl ether 6/18/2009 7:17:00 PM2.2 µg/Kg-dry 1ND JSANELAP

Methylacrylate 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSA

Methylene chloride J 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 12.3 JSANELAP

Naphthalene 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP

n-Butylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

n-Hexane J 6/18/2009 7:17:00 PM21.9 µg/Kg-dry 12.5 JSA

Nitrobenzene 6/18/2009 7:17:00 PM109 µg/Kg-dry 1ND JSANELAP

n-Propylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

o-Xylene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Pentachloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

p-Isopropyltoluene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Propionitrile 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP

sec-Butylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Styrene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

tert-Butylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Tetrachloroethene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Tetrahydrofuran 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP

Toluene J 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 12.1 JSANELAP

trans-1,2-Dichloroethene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

trans-1,3-Dichloropropene 6/18/2009 7:17:00 PM4.4 µg/Kg-dry 1ND JSANELAP

Trichloroethene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Trichlorofluoromethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP

Vinyl acetate 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP

Vinyl chloride 6/18/2009 7:17:00 PM2.2 µg/Kg-dry 1ND JSANELAP

Surr: 1,2-Dichloroethane-d4 6/18/2009 7:17:00 PM61-128 %REC 1122.5 JSA

Surr: 4-Bromofluorobenzene S 6/18/2009 7:17:00 PM78.2-117 %REC 171.3 JSA

Surr: Dibromofluoromethane 6/18/2009 7:17:00 PM66.6-130 %REC 1110.0 JSA

Surr: Toluene-d8 6/18/2009 7:17:00 PM80.1-122 %REC 1117.4 JSA

SW-846 7471AMercury 6/19/20090.013 mg/Kg-dry 10.041 MEKNELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-001






TEL: 618-344-1004

FAX: 618-344-1005

Sample NarrativeSW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS

Elevated reporting limit due to high levels of target and/or non-target analytes.SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS

Matrix spike and RPD did not recover within control limits because of sample composition.SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS

Surrogate and Internal recoveries were outside QC limits due to matrix interference.




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-002






TEL: 618-344-1004

FAX: 618-344-1005









SW-846 3050B, METALS BY GFAASelenium 7740 6/19/20090.600 mg/Kg-dry 1< 0.600 MEKNELAP









Chlordane 6/19/2009 10:05:00 PM102 µg/Kg-dry 25ND HENELAP














Toxaphene 6/19/2009 10:05:00 PM916 µg/Kg-dry 25ND HENELAP






Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-002






TEL: 618-344-1004

FAX: 618-344-1005










SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 2ND MAMNELAP

Acenaphthylene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 2ND MAMNELAP

Anthracene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.011 MAMNELAP

Benzo(a)anthracene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.054 MAMNELAP

Benzo(a)pyrene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.082 MAMNELAP

Benzo(b)fluoranthene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.122 MAMNELAP

Benzo(g,h,i)perylene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.038 MAMNELAP

Benzo(k)fluoranthene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.042 MAMNELAP

Bis(2-ethylhexyl)phthalate 6/19/2009 2:44:00 PM0.168 mg/Kg-dry 2ND MAMNELAP

Chrysene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.076 MAMNELAP

Dibenzo(a,h)anthracene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.009 MAMNELAP

Fluoranthene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.158 MAMNELAP

Fluorene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 2ND MAMNELAP

Indeno(1,2,3-cd)pyrene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.027 MAMNELAP

Naphthalene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 2ND MAMNELAP

Phenanthrene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.064 MAMNELAP

Pyrene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.124 MAMNELAP

Surr: 2-Fluorobiphenyl 6/19/2009 2:44:00 PM10-131 %REC 248.3 MAM

Surr: Nitrobenzene-d5 6/19/2009 2:44:00 PM10-132 %REC 263.1 MAM

Surr: p-Terphenyl-d14 6/19/2009 2:44:00 PM30.6-131 %REC 273.9 MAM











Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-002






TEL: 618-344-1004

FAX: 618-344-1005


2,4-Dinitrophenol 6/20/2009 3:25:00 PM6.11 mg/Kg-dry 5ND DMHNELAP








































Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-002






TEL: 618-344-1004

FAX: 618-344-1005








Pentachlorophenol 6/20/2009 3:25:00 PM12.2 mg/Kg-dry 5ND DMHNELAP




















1,2,3-Trichloropropane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP













Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-002






TEL: 618-344-1004

FAX: 618-344-1005













Acrolein 6/18/2009 7:44:00 PM99.8 µg/Kg-dry 1ND JSANELAP

Acrylonitrile 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP


Benzene 6/18/2009 7:44:00 PM1.0 µg/Kg-dry 11.3 JSANELAP





Bromomethane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP

Carbon disulfide J 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 13.2 JSANELAP



Chloroethane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP


Chloromethane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP



Cyclohexanone 6/18/2009 7:44:00 PM99.8 µg/Kg-dry 1ND JSA



Dichlorodifluoromethane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP









Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-002






TEL: 618-344-1004

FAX: 618-344-1005



Iodomethane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP


m,p-Xylenes 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP




Methylacrylate 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSA


Naphthalene 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP



Nitrobenzene 6/18/2009 7:44:00 PM99.8 µg/Kg-dry 1ND JSANELAP




p-Isopropyltoluene J 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 11.2 JSANELAP






















Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-002






TEL: 618-344-1004

FAX: 618-344-1005

Sample NarrativeSW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD

Elevated reporting limit due to high levels of target and/or non-target analytes.SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS

Elevated reporting limit due to high levels of target and/or non-target analytes.SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS

Perylene-d12 was outside of QC limits due to matrix interference, subsequent analysis showed same results.Elevated reporting limit due to high levels of target and/or non-target analytes.

SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS





Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-003






TEL: 618-344-1004

FAX: 618-344-1005




Barium 6/19/2009 1:27:39 PM0.48 mg/Kg-dry 196.9 LALNELAP





SW-846 3050B, METALS BY GFAASelenium 7740 6/19/20090.577 mg/Kg-dry 1< 0.577 MEKNELAP























Toxaphene 6/19/2009 10:29:00 PM870 µg/Kg-dry 25ND HENELAP






Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-003






TEL: 618-344-1004

FAX: 618-344-1005












Anthracene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 2ND MAMNELAP

Benzo(a)anthracene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 20.015 MAMNELAP

Benzo(a)pyrene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 20.017 MAMNELAP

Benzo(b)fluoranthene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 20.026 MAMNELAP

Benzo(g,h,i)perylene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 20.012 MAMNELAP

Benzo(k)fluoranthene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 20.009 MAMNELAP


Chrysene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 20.011 MAMNELAP

Dibenzo(a,h)anthracene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 2ND MAMNELAP

Fluoranthene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 20.029 MAMNELAP


Indeno(1,2,3-cd)pyrene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 2ND MAMNELAP


Phenanthrene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 20.012 MAMNELAP

Pyrene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 20.024 MAMNELAP














Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-003






TEL: 618-344-1004

FAX: 618-344-1005


2,4-Dinitrophenol S 6/20/2009 3:55:00 PM5.86 mg/Kg-dry 5ND DMHNELAP








































Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-003






TEL: 618-344-1004

FAX: 618-344-1005








Pentachlorophenol S 6/20/2009 3:55:00 PM11.7 mg/Kg-dry 5ND DMHNELAP




















1,2,3-Trichloropropane 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP



1,2,4-Trimethylbenzene J 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 11.7 JSANELAP










Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-003






TEL: 618-344-1004

FAX: 618-344-1005













Acrolein 6/18/2009 8:11:00 PM91.1 µg/Kg-dry 1ND JSANELAP

Acrylonitrile 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP


Benzene 6/18/2009 8:11:00 PM0.9 µg/Kg-dry 12.4 JSANELAP





Bromomethane J 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 12.2 JSANELAP

Carbon disulfide 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP



Chloroethane 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP


Chloromethane 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP



Cyclohexanone 6/18/2009 8:11:00 PM91.1 µg/Kg-dry 1ND JSA



Dichlorodifluoromethane 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP




Ethylbenzene J 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 11.4 JSANELAP





Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-003






TEL: 618-344-1004

FAX: 618-344-1005



Iodomethane 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP


m,p-Xylenes J 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 12.0 JSANELAP




Methylacrylate 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSA


Naphthalene 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP



Nitrobenzene 6/18/2009 8:11:00 PM91.1 µg/Kg-dry 1ND JSANELAP




p-Isopropyltoluene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP







Toluene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 14.8 JSANELAP















Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09060783

Lab ID: 09060783-003






TEL: 618-344-1004

FAX: 618-344-1005

Sample NarrativeSW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD

Elevated reporting limit due to high levels of target and/or non-target analytes.SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS

Matrix spike did not recover within control limits because of sample dilution.Elevated reporting limit due to high levels of target and/or non-target analytes.

SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS

Perylene-d12 was outside of QC limits due to matrix interference, subsequent analysis showed same results.Elevated reporting limit due to high levels of target and/or non-target analytes.




Sample ID Client Sample ID Collection Date MatrixAnalysis

Date/Time

DATES REPORT

Lab Order: 09060783

Client: PSC Industrial Outsourcing, LPProject: A831-735002-012901-225/Ameren Champaign 62403053

Test NamePrep

Date/Time




TEL: 618-344-1004

FAX: 618-344-1005

22-Jun-09Report Date:

09060783-001A CBA-01 6/18/2009 Solid SW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD

6/19/2009 9:40:00 PM

6/18/2009 7:44:41 PM

SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD

6/19/2009 10:25:00 AM

6/18/2009 7:44:41 PM


6/19/2009 10:54:00 AM

6/18/2009 6:53:02 PM

SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS

6/20/2009 2:55:00 PM

6/18/2009 6:15:00 PM

09060783-001B SW-846 3050B, 6010B, Metals by ICP 6/19/2009 1:00:26 PM

6/19/2009 7:18:14 AM

SW-846 3050B, 6010B, Metals by ICP 6/19/2009 1:14:06 PM

6/19/2009 7:18:14 AM

SW-846 3050B, Metals by GFAA 6/19/20096/19/2009 7:17:04 AM

SW-846 7471A 6/19/20096/19/2009 8:31:07 AM

09060783-001C ASTM D2974 6/18/2009 7:00:00 PM

Standard Methods 18th Ed. 2540 G 6/18/2009 7:00:00 PM

09060783-001F SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS

6/18/2009 7:17:00 PM

6/18/2009 6:25:00 PM

09060783-002A CBA-02 SW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD

6/19/2009 10:05:00 PM

6/18/2009 7:44:41 PM


6/19/2009 10:42:00 AM

6/18/2009 7:44:41 PM


6/19/2009 1:31:00 PM

6/18/2009 6:53:02 PM


6/19/2009 2:44:00 PM

6/18/2009 6:53:02 PM


6/19/2009 3:57:00 PM

6/18/2009 6:53:02 PM


6/20/2009 3:25:00 PM

6/18/2009 6:15:00 PM


6/19/2009 7:18:14 AM


6/19/2009 7:18:14 AM


SW-846 7471A 6/19/20096/19/2009 8:31:07 AM

09060783-002C ASTM D2974 6/18/2009 7:00:00 PM

of 54IL ELAP and NELAP Accredited - Accreditation #100226


Date/Time

DATES REPORT

Lab Order: 09060783


Test NamePrep

Date/Time




TEL: 618-344-1004

FAX: 618-344-1005


09060783-002C CBA-02 6/18/2009 Solid Standard Methods 18th Ed. 2540 G 6/18/2009 7:00:00 PM


6/18/2009 7:44:00 PM

6/18/2009 6:25:00 PM

09060783-003A CBA-03 SW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD

6/19/2009 10:29:00 PM

6/18/2009 7:44:41 PM


6/19/2009 11:34:00 AM

6/18/2009 7:44:41 PM


6/19/2009 2:08:00 PM

6/18/2009 6:53:02 PM


6/19/2009 3:20:00 PM

6/18/2009 6:53:02 PM


6/19/2009 4:34:00 PM

6/18/2009 6:53:02 PM


6/20/2009 3:55:00 PM

6/18/2009 6:15:00 PM


6/19/2009 7:18:14 AM


6/19/2009 7:18:14 AM


SW-846 7471A 6/19/20096/19/2009 8:31:07 AM

09060783-003C ASTM D2974 6/18/2009 7:00:00 PM



6/18/2009 8:11:00 PM

6/18/2009 6:25:00 PM

of 54IL ELAP and NELAP Accredited - Accreditation #100226

TEKLAB, INC 5445 HORSESHOE LAKE ROADCOLLINSVILLE, ILLINOIS 62234

ANALYTICAL QC SUMMARY REPORT

Qualifiers






- Reporting Limit

- Dilution Factor





- IL Dept. of Public Health

- IL ELAP and NELAP Accredited

DF

RL

TNTC

Surr

IDPH

B

J

R

S

X NELAP

E

MI

H

ND

D - Did not igniteDNI

- Unknown hydrocarbon#

- QC criteria failedQ


CCV

DF

DUP

ICV

LCS

MS

MSD

MDL

MB/LCB

PQL

RL

RPD

Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.

Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilutions factors.Laboratory duplicate is an aliquot of a sample taken from the same container under laboratory conditions for independent processing and analysis independently of the original aliquot. (NELAC)Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.

Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. (NELAC) The acceptable recovery range is listed in this report.Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in this report.Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in this report.Method detection limit or limit of detection (LOD) means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.Method blank or lab control blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences are present at concentrations that impact the analytical results for sample analyses. (NELAC)Practical quantitation limit or limit of quantitation (LOQ) means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in this report.The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in this report.

SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes. (NELAC)

Surr Surrogates are an organic compound which is similar to the analytes of interest in chemical composition and behavior in the analytical process, but which is not normally found in environmental samples.

Key QC concepts:

of 54

IL ELAP and NELAP Accredited - Accreditation #100226

Project: A831-735002-012901-225/Ameren Champaign 62403053


Lab Order: 09060783

ANALYTICAL QC SUMMARY REPORTTestCode: I_TS_M_MT


Sample ID: LCS-R123687

Batch ID: R123687 Analysis Date: 6/18/2009

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: %

PQL

Client ID: ZZZZZZ

RunNo: 123687

SeqNo: 2312130

LCSSampType:

Total Solids 1.000 100 90 1100.1 01.0

Sample ID: LCSQC


Prep Date:


Units: %

PQL

Client ID: ZZZZZZ

RunNo: 123687

SeqNo: 2312131

LCSQCSampType:

Total Solids 1.000 100 90 1100.1 01.0

Sample ID: 09060783-001CDUP


Prep Date:


Units: %

PQL

Client ID: CBA-01DUP

RunNo: 123687

SeqNo: 2312152

DUPSampType:

Total Solids 150.1 77.14 0.94277.9

of 54




Lab Order: 09060783

ANALYTICAL QC SUMMARY REPORTTestCode: M_HG_SOLID


Sample ID: MB-53683

Batch ID: 53683 Analysis Date: 6/19/2009

Prep Date: 6/19/2009


Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123669

SeqNo: 2311746

MBLKSampType:

SOP 3063

Mercury 0.01000 30.0 -100 100 J0.010 00.003

Sample ID: LCS-53683




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123669

SeqNo: 2311747

LCSSampType:

SOP 3063

Mercury 0.2500 97.0 85 1150.010 00.243

Sample ID: 09060783-001BMS




Units: mg/Kg-dry

PQL

Client ID: CBA-01MS

RunNo: 123669

SeqNo: 2311749

MSSampType:

SOP 3063

Mercury 0.3201 93.2 75 1250.013 0.040970.339

Sample ID: 09060783-001BMSD




Units: mg/Kg-dry

PQL

Client ID: CBA-01MSD

RunNo: 123669

SeqNo: 2311750

MSDSampType:

SOP 3063

Mercury 0.3201 92.2 75 125 150.013 0.04097 0.3393 0.9480.336

of 54




Lab Order: 09060783

ANALYTICAL QC SUMMARY REPORTTestCode: M_SOLID_GF


Sample ID: MB-53674




Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 123678

SeqNo: 2311985

MBLKSampType:

SOP 3042

Selenium 7740 0.6000 0 -100 1000.600 0< 0.600





Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 123678

SeqNo: 2311986

LCSSampType:

SOP 3042

Selenium 7740 3.000 105.4 80 1200.600 03.16





Units: mg/Kg-dry

PQL

Client ID: CBA-02MS

RunNo: 123678

SeqNo: 2311988

MSSampType:

SOP 3042

Selenium 7740 3.000 83.6 70 1300.600 02.51





Units: mg/Kg-dry

PQL


RunNo: 123678

SeqNo: 2311989

MSDSampType:

SOP 3042

Selenium 7740 3.000 79.8 70 130 200.600 0 2.507 4.632.39

of 54




Lab Order: 09060783

ANALYTICAL QC SUMMARY REPORTTestCode: M_SOLIDS_ICP


Sample ID: MB-53675




Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 123642

SeqNo: 2311887

MBLKSampType:

SOP 3032

Lead 4.000 0 -100 1004.00 0< 4.00





Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 123642

SeqNo: 2311888

LCSSampType:

SOP 3032

Lead 50.00 93.9 85 1154.00 047.0





Units: mg/Kg-dry

PQL

Client ID: CBA-03MS

RunNo: 123642

SeqNo: 2311893

MSSampType:

SOP 3032

Lead 48.08 82.6 75 1253.85 13.6953.4





Units: mg/Kg-dry

PQL


RunNo: 123642

SeqNo: 2311894

MSDSampType:

SOP 3032

Lead 48.08 97.2 75 125 203.85 13.69 53.39 12.360.4

Sample ID: MB-53675




Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 123641

SeqNo: 2311908

MBLKSampType:

SOP 3032

Arsenic 2.500 0 -100 1002.50 0< 2.50

Barium 0.5000 0 -100 1000.50 0< 0.50

Cadmium 0.2000 0 -100 1000.20 0< 0.20

Chromium 1.000 0 -100 1001.00 0< 1.00

Silver 1.000 0 -100 1000.55 0< 0.55

of 54




Lab Order: 09060783







Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 123641

SeqNo: 2311909

LCSSampType:

SOP 3032

Arsenic 200.0 102.0 85 1152.50 0204

Barium 200.0 111.0 85 1150.50 0222

Cadmium 5.000 102.2 85 1150.20 05.11

Chromium 20.00 112.7 85 1151.00 022.5

Silver 5.000 94.2 85 1150.55 04.71





Units: mg/Kg-dry

PQL

Client ID: CBA-03MS

RunNo: 123641

SeqNo: 2311914

MSSampType:

SOP 3032

Arsenic 192.3 93.9 75 1252.40 6.558187

Barium 192.3 90.4 75 1250.48 96.92271

Cadmium 4.808 86.4 75 1250.19 0.32694.48

Chromium 19.23 97.0 75 1250.96 20.1438.8

Silver 4.808 105.8 75 1250.53 05.09





Units: mg/Kg-dry

PQL


RunNo: 123641

SeqNo: 2311915

MSDSampType:

SOP 3032

Arsenic 192.3 96.2 75 125 202.40 6.558 187.2 2.34192

Barium 192.3 95.7 75 125 200.48 96.92 270.7 3.73281

Cadmium 4.808 89.0 75 125 200.19 0.3269 4.481 2.754.61

Chromium 19.23 116.2 75 125 200.96 20.14 38.80 9.0842.5

Silver 4.808 102.6 75 125 200.53 0 5.087 3.074.93

of 54




Lab Order: 09060783

ANALYTICAL QC SUMMARY REPORTTestCode: SV_8081S_S


Sample ID: MB-53670




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123709

SeqNo: 2312609

MBLKSampType:

SW3550B

4,4´-DDD 1.67ND

4,4´-DDE 1.67ND

4,4´-DDT 1.67ND

Alachlor 1.67ND

Aldrin 1.67ND

alpha-BHC 1.67ND

alpha-Chlordane 1.67ND

beta-BHC 1.67ND

Chlordane 3.34ND

delta-BHC 1.67ND

Dieldrin 1.67ND

Endosulfan I 1.67ND

Endosulfan II 1.67ND

Endosulfan sulfate 1.67ND

Endrin 1.67ND

Endrin aldehyde 1.67ND

Endrin ketone 1.67ND

gamma-BHC 1.67ND

gamma-Chlordane 1.67ND

Heptachlor 1.67ND

Heptachlor epoxide 1.67ND

Methoxychlor 1.67ND

Toxaphene 30.0ND

Surr: Decachlorobiphenyl 8.330 88.7 73.5 1507.39

Surr: Tetrachloro-m-xylene 8.330 78.3 14.4 1136.52

Sample ID: LCSPST-53670




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123709

SeqNo: 2312610

LCSSampType:

SW3550B

4,4´-DDD 8.330 91.4 36 2081.67 07.61

of 54




Lab Order: 09060783







Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123709

SeqNo: 2312610

LCSSampType:

SW3550B

4,4´-DDE 8.330 101.4 26 1911.67 08.45

4,4´-DDT 8.330 107.3 3 2151.67 08.94

Alachlor 8.330 87.2 30 1701.67 07.27

Aldrin 8.330 86.9 46 1731.67 07.24

alpha-BHC 8.330 83.5 37 1791.67 06.96

alpha-Chlordane 8.330 97.9 38 1871.67 08.16

beta-BHC 8.330 94.7 51 1851.67 07.88

delta-BHC 8.330 61.1 46 1661.67 05.09

Dieldrin 8.330 94.6 26 2161.67 07.88

Endosulfan I 8.330 97.9 31 2051.67 08.16

Endosulfan II 8.330 78.1 42 1871.67 06.51

Endosulfan sulfate 8.330 102.8 29 2301.67 08.56

Endrin 8.330 98.0 30 2151.67 08.16

Endrin aldehyde 8.330 59.3 42 2021.67 04.94

Endrin ketone 8.330 71.9 19 2441.67 05.99

gamma-BHC 8.330 86.4 55 1661.67 07.20

gamma-Chlordane 8.330 96.5 23 1861.67 08.04

Heptachlor 8.330 94.7 43 1721.67 07.89

Heptachlor epoxide 8.330 95.7 39 2041.67 07.97

Methoxychlor 8.330 110.9 3 2211.67 09.24


Surr: Tetrachloro-m-xylene 8.330 76.3 10 1076.36

Sample ID: LCSPSTD-53670




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123709

SeqNo: 2312611

LCSDSampType:

SW3550B

4,4´-DDD 8.330 87.5 36 208 401.67 0 7.612 4.377.29

4,4´-DDE 8.330 96.5 26 191 401.67 0 8.449 4.978.04

4,4´-DDT 8.330 102.8 3 215 401.67 0 8.939 4.268.57

Alachlor 8.330 92.8 30 170 401.67 0 7.266 6.167.73

of 54




Lab Order: 09060783



Sample ID: LCSPSTD-53670




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123709

SeqNo: 2312611

LCSDSampType:

SW3550B

Aldrin 8.330 79.8 46 173 401.67 0 7.242 8.516.65

alpha-BHC 8.330 76.1 37 179 401.67 0 6.957 9.336.34

alpha-Chlordane 8.330 93.1 38 187 401.67 0 8.159 5.067.76

beta-BHC 8.330 89.9 51 185 401.67 0 7.885 5.127.49

delta-BHC 8.330 57.7 46 166 401.67 0 5.091 5.764.81

Dieldrin 8.330 90.7 26 216 401.67 0 7.879 4.217.55

Endosulfan I 8.330 93.1 31 205 401.67 0 8.159 5.067.76

Endosulfan II 8.330 74.3 42 187 401.67 0 6.507 4.946.19

Endosulfan sulfate 8.330 97.8 29 230 401.67 0 8.560 4.978.15

Endrin 8.330 93.0 30 215 401.67 0 8.164 5.247.75

Endrin aldehyde 8.330 55.7 42 202 401.67 0 4.942 6.274.64

Endrin ketone 8.330 68.6 19 244 401.67 0 5.991 4.665.72

gamma-BHC 8.330 79.7 55 166 401.67 0 7.197 8.126.64

gamma-Chlordane 8.330 91.7 23 186 401.67 0 8.035 5.097.64

Heptachlor 8.330 87.5 43 172 401.67 0 7.885 7.917.29

Heptachlor epoxide 8.330 93.6 39 204 401.67 0 7.968 2.227.79

Methoxychlor 8.330 106.4 3 221 401.67 0 9.237 4.148.86

Surr: Decachlorobiphenyl 8.330 89.6 50.4 176 4007.46

Surr: Tetrachloro-m-xylene 8.330 74.0 10 107 4006.16

of 54




Lab Order: 09060783



Sample ID: MB-53670




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123671

SeqNo: 2311838

MBLKSampType:

SW3550B

Aroclor 1016 37.5ND

Aroclor 1221 37.5ND

Aroclor 1232 37.5ND

Aroclor 1242 37.5ND

Aroclor 1248 37.5ND

Aroclor 1254 37.5ND

Aroclor 1260 37.5ND


Surr: Tetrachloro-meta-xylene 8.300 85.9 21 98.97.1

Sample ID: LCSPCB-53670




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123671

SeqNo: 2311839

LCSSampType:

SW3550B

Aroclor 1016 166.7 116.0 54.9 12137.5 0193

Aroclor 1260 166.7 115.5 65.5 13337.5 0192



Sample ID: 09060783-002AMS




Units: µg/Kg-dry

PQL

Client ID: CBA-02MS

RunNo: 123671

SeqNo: 2311842

MSSampType:

SW3550B

Aroclor 1016 208.8 104.4 35.8 14347.0 0218

Aroclor 1260 208.8 97.5 22.3 15247.0 0204

Surr: Decachlorobiphenyl 10.40 91.0 5 1569.5

Surr: Tetrachloro-meta-xylene 10.40 86.0 7.35 1238.9

of 54




Lab Order: 09060783



Sample ID: 09060783-002AMSD




Units: µg/Kg-dry

PQL


RunNo: 123671

SeqNo: 2311843

MSDSampType:

SW3550B

Aroclor 1016 212.7 103.9 35.8 143 4047.9 0 218.0 1.34221

Aroclor 1260 212.7 91.4 22.3 152 4047.9 0 203.7 4.58195

Surr: Decachlorobiphenyl 10.59 86.5 5 156 4009.2

Surr: Tetrachloro-meta-xylene 10.59 83.1 7.35 123 4008.8

of 54




Lab Order: 09060783



Sample ID: MB-53651




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123696

SeqNo: 2312251

MBLKSampType:

SW3550B

1,2,4-Trichlorobenzene 0.500ND

1,2-Dichlorobenzene 0.500ND



2,4,5-Trichlorophenol 0.350ND


2,4-Dichlorophenol 0.500ND

2,4-Dimethylphenol 0.500ND

2,4-Dinitrophenol 1.00ND

2,4-Dinitrotoluene 0.350ND


2-Chloronaphthalene 0.350ND

2-Chlorophenol 0.500ND

2-Methoxy-4-methylphenol 0.650ND

2-Methylnaphthalene 0.350ND

2-Nitroaniline 1.00ND

2-Nitrophenol 0.350ND

3,3´-Dichlorobenzidine 0.350ND


4,6-Dinitro-2-methylphenol 1.00ND

4-Bromophenyl phenyl ether 0.350ND

4-Chloro-3-methylphenol 0.500ND

4-Chloroaniline 0.500ND

4-Chlorophenyl phenyl ether 0.350ND



Acenaphthene 0.350ND

Acenaphthylene 0.350ND

Aniline 0.500ND

Anthracene 0.350ND

Azobenzene 0.350ND

of 54




Lab Order: 09060783



Sample ID: MB-53651




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123696

SeqNo: 2312251

MBLKSampType:

SW3550B

Benzidine 1.06ND

Benzo(a)anthracene 0.350ND

Benzo(a)pyrene 0.350ND

Benzo(b)fluoranthene 0.350ND

Benzo(g,h,i)perylene 0.350ND

Benzo(k)fluoranthene 0.350ND

Benzoic acid 1.50ND

Benzyl alcohol 0.500ND

Bis(2-chloroethoxy)methane 0.350ND

Bis(2-chloroethyl)ether 0.500ND

Bis(2-chloroisopropyl)ether 0.350ND

Bis(2-ethylhexyl)phthalate 0.350ND

Butyl benzyl phthalate 0.350ND

Carbazole 0.500ND

Chrysene 0.350ND

Dibenzo(a,h)anthracene 0.350ND

Dibenzofuran 0.350ND

Diethyl phthalate 0.500ND

Dimethyl phthalate 0.350ND

Di-n-butyl phthalate 0.350ND

Di-n-octyl phthalate 0.350ND

Fluoranthene 0.350ND

Fluorene 0.350ND

Hexachlorobenzene 0.350ND

Hexachlorobutadiene 0.500ND

Hexachlorocyclopentadiene 0.350ND

Hexachloroethane 0.500ND

Indeno(1,2,3-cd)pyrene 0.350ND

Isophorone 0.350ND

m,p-Cresol 0.500ND

Naphthalene 0.350ND

of 54




Lab Order: 09060783



Sample ID: MB-53651




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123696

SeqNo: 2312251

MBLKSampType:

SW3550B

Nitrobenzene 0.500ND

N-Nitrosodimethylamine 0.500ND

N-Nitroso-di-n-propylamine 0.500ND

N-Nitrosodiphenylamine 0.500ND

o-Cresol 0.500ND

Pentachlorophenol 2.00ND

Phenanthrene 0.350ND

Phenol 0.350ND

Pyrene 0.500ND

Pyridine 0.500ND

1,2-Diphenylhydrazine 0.840ND

Surr: 2,4,6-Tribromophenol 1.670 86.8 52.1 1131.45

Surr: 2-Fluorobiphenyl 0.8350 92.6 46.3 1060.773

Surr: 2-Fluorophenol 1.670 80.8 50.6 891.35

Surr: Nitrobenzene-d5 0.8350 80.5 42.4 99.20.672

Surr: Phenol-d5 1.670 83.1 55.9 98.51.39

Surr: p-Terphenyl-d14 0.8350 93.4 45.5 1150.780





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123696

SeqNo: 2312252

LCSSampType:

SW3550B

1,2,4-Trichlorobenzene 1.670 89.4 43.9 92.20.500 01.49

1,4-Dichlorobenzene 1.670 72.3 43.8 84.10.500 01.21

2,4,5-Trichlorophenol 3.330 95.8 38.6 1230.350 03.19


2,4-Dimethylphenol 3.330 56.4 38.3 880.500 01.88

2,4-Dinitrophenol 3.330 77.0 1.88 1621.00 02.56

2,4-Dinitrotoluene 1.670 93.0 48.6 1020.350 01.55

2-Chlorophenol 3.330 74.5 46.6 840.500 02.48

4-Chloro-3-methylphenol 3.330 86.5 51.5 94.90.500 02.88

of 54




Lab Order: 09060783







Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123696

SeqNo: 2312252

LCSSampType:

SW3550B

4-Nitrophenol 3.330 85.4 53.2 1040.350 02.84

Acenaphthene 1.670 84.7 50.8 1130.350 01.41

Acenaphthylene 1.670 122.6 52.8 121 S0.350 02.05

Anthracene 1.670 80.4 53.3 1150.350 01.34

Benzo(a)anthracene 1.670 77.9 62.3 1100.350 01.30

Benzo(a)pyrene 1.670 84.0 58.2 1090.350 01.40

Benzo(b)fluoranthene 1.670 73.4 51.8 1070.350 01.23

Benzo(g,h,i)perylene 1.670 89.4 49.6 1210.350 01.49

Benzo(k)fluoranthene 1.670 94.8 63.1 1290.350 01.58

Bis(2-ethylhexyl)phthalate 1.670 79.5 56.3 1090.350 01.33

Chrysene 1.670 96.3 58.4 1150.350 01.61

Dibenzo(a,h)anthracene 1.670 88.2 54.9 1200.350 01.47

Diethyl phthalate 3.330 81.3 51.7 1060.500 02.71

Dimethyl phthalate 3.330 86.7 58.8 1040.350 02.89

Di-n-butyl phthalate 1.670 84.7 54.3 1050.350 01.41

Fluoranthene 1.670 84.8 61.6 1130.350 01.42

Fluorene 1.670 87.7 52.2 1160.350 01.46

Hexachlorobenzene 3.330 84.9 55.9 1060.350 02.83

Hexachlorobutadiene 3.330 91.2 35.7 1000.500 03.04

Hexachloroethane 3.330 73.1 38.9 89.90.500 02.43

Indeno(1,2,3-cd)pyrene 1.670 87.5 52.7 1150.350 01.46

m,p-Cresol 1.670 70.6 37.6 93.70.500 01.18

Naphthalene 1.670 74.9 45.7 1010.350 01.25

Nitrobenzene 3.330 75.7 51.8 1040.500 02.52

N-Nitroso-di-n-propylamine 1.670 74.2 49.1 94.50.500 01.24

o-Cresol 1.670 73.4 43 1010.500 01.23

Pentachlorophenol 3.330 77.8 42.2 1022.00 02.59

Phenanthrene 1.670 87.0 52.9 1130.350 01.45

Phenol 3.330 70.9 41.6 81.30.350 02.36

Pyrene 1.670 93.2 60.7 1150.500 01.56

Pyridine 3.330 49.3 3.61 74.30.500 01.64

of 54




Lab Order: 09060783







Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123696

SeqNo: 2312252

LCSSampType:

SW3550B





Surr: Phenol-d5 1.670 71.0 55.9 98.51.19






Units: mg/Kg-dry

PQL

Client ID: CBA-03MS

RunNo: 123696

SeqNo: 2312256

MSSampType:

SW3550B

1,2,4-Trichlorobenzene 1.974 78.2 35.9 102 J2.96 01.5

1,4-Dichlorobenzene 1.974 56.8 29.8 95.5 J2.96 01.1



2,4-Dimethylphenol 3.937 64.3 38.3 88 J2.96 02.5

2,4-Dinitrotoluene 1.974 67.8 37.5 107 J2.07 01.3

2-Chlorophenol 3.937 60.5 22.6 108 J2.96 02.4

4-Chloro-3-methylphenol 3.937 71.9 19.3 131 J2.96 02.8

4-Nitrophenol 3.937 65.8 27.6 1232.07 02.59

Benzoic acid 0 0 0 08.87 0ND

Diethyl phthalate 3.937 72.5 51.7 106 J2.96 02.8


Di-n-butyl phthalate 1.974 73.1 54.3 105 J2.07 01.4



Hexachloroethane 3.937 53.6 38.9 89.9 J2.96 02.1

m,p-Cresol 1.974 66.8 37.6 93.7 J2.96 01.3

Nitrobenzene 3.937 68.6 51.8 104 J2.96 02.7

N-Nitroso-di-n-propylamine 1.974 66.4 45.5 99.1 J2.96 01.3

o-Cresol 1.974 63.7 43 101 J2.96 01.3

of 54




Lab Order: 09060783







Units: mg/Kg-dry

PQL

Client ID: CBA-03MS

RunNo: 123696

SeqNo: 2312256

MSSampType:

SW3550B

Phenol 3.937 61.7 20.8 1102.07 02.43

Pyridine 3.937 40.8 3.61 74.3 J2.96 01.6




Surr: Nitrobenzene-d5 0.9871 57.9 34.1 1010.571

Surr: Phenol-d5 1.974 59.5 34.9 1101.17






Units: mg/Kg-dry

PQL


RunNo: 123696

SeqNo: 2312257

MSDSampType:

SW3550B

1,2,4-Trichlorobenzene 1.944 81.4 35.9 102 40 J2.91 0 1.544 01.6

1,4-Dichlorobenzene 1.944 68.0 29.8 95.5 40 J2.91 0 1.122 01.3

2,4,5-Trichlorophenol 3.876 81.2 38.6 123 402.04 0 2.884 8.773.15


2,4-Dimethylphenol 3.876 67.2 38.3 88 40 J2.91 0 2.530 02.6

2,4-Dinitrotoluene 1.944 70.3 37.5 107 40 J2.04 0 1.339 01.4

2-Chlorophenol 3.876 63.2 22.6 108 40 J2.91 0 2.380 02.4

4-Chloro-3-methylphenol 3.876 72.0 19.3 131 40 J2.91 0 2.830 02.8

4-Nitrophenol 3.876 66.7 27.6 123 402.04 0 2.591 0.1742.59

Benzoic acid 0 0 0 0 08.73 0 0 0ND

Diethyl phthalate 3.876 75.4 51.7 106 402.91 0 2.853 2.392.92

Dimethyl phthalate 3.876 76.4 58.8 104 402.04 0 2.895 2.322.96

Di-n-butyl phthalate 1.944 76.7 54.3 105 40 J2.04 0 1.444 01.5

Hexachlorobenzene 3.876 81.9 55.9 106 402.04 0 3.198 0.7513.17

Hexachlorobutadiene 3.876 82.4 35.7 100 402.91 0 3.157 1.133.19

Hexachloroethane 3.876 62.9 38.9 89.9 40 J2.91 0 2.111 02.4

m,p-Cresol 1.944 68.6 37.6 93.7 40 J2.91 0 1.318 01.3

Nitrobenzene 3.876 73.2 51.8 104 40 J2.91 0 2.701 02.8

of 54




Lab Order: 09060783







Units: mg/Kg-dry

PQL


RunNo: 123696

SeqNo: 2312257

MSDSampType:

SW3550B

N-Nitroso-di-n-propylamine 1.944 66.7 45.5 99.1 40 J2.91 0 1.312 01.3

o-Cresol 1.944 65.4 43 101 40 J2.91 0 1.257 01.3

Phenol 3.876 63.2 20.8 110 402.04 0 2.427 0.9762.45

Pyridine 3.876 44.8 3.61 74.3 40 J2.91 0 1.604 01.7

Surr: 2,4,6-Tribromophenol 1.944 65.8 32.7 130 4001.28

Surr: 2-Fluorobiphenyl 0.9720 62.9 34.1 116 4000.611

Surr: 2-Fluorophenol 1.944 58.9 30.5 99 4001.14

Surr: Nitrobenzene-d5 0.9720 47.1 34.1 101 4000.458

Surr: Phenol-d5 1.944 62.2 34.9 110 4001.21

Surr: p-Terphenyl-d14 0.9720 75.8 41.7 124 4000.737

of 54




Lab Order: 09060783

ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S_SIMS


Sample ID: MB-53669




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123660

SeqNo: 2311601

MBLKSampType:

SW3550B



Anthracene 0.003ND







Chrysene 0.003ND



Fluorene 0.003ND


Naphthalene 0.003ND


Pyrene 0.003ND


Surr: Nitrobenzene-d5 0.1670 66.9 35 1050.112






Units: mg/Kg-dry

PQL

Client ID: CBA-01MS

RunNo: 123660

SeqNo: 2311715

MSSampType:

SW3550B

Acenaphthene 0.2176 48.3 36 1350.004 00.105

Acenaphthylene 0.2176 53.0 17.2 1670.004 00.115

Anthracene 0.2176 49.3 39.3 1240.004 0.0043600.112

Benzo(a)anthracene 0.2176 55.7 10 1830.004 0.036300.157

Benzo(a)pyrene 0.2176 69.2 10 2040.004 0.042260.193

Benzo(b)fluoranthene 0.2176 71.9 10.6 1780.004 0.063330.220

of 54




Lab Order: 09060783







Units: mg/Kg-dry

PQL

Client ID: CBA-01MS

RunNo: 123660

SeqNo: 2311715

MSSampType:

SW3550B

Benzo(g,h,i)perylene 0.2176 57.6 10 1680.004 0.031560.157

Benzo(k)fluoranthene 0.2176 66.0 27.6 1810.004 0.022840.167

Bis(2-ethylhexyl)phthalate 0.2176 -14.1 50 150 S0.087 0.16620.136

Chrysene 0.2176 62.2 10 1760.004 0.048910.184

Dibenzo(a,h)anthracene 0.2176 54.6 12.2 1560.004 0.0072520.126

Fluoranthene 0.2176 74.6 10 2270.004 0.11060.273

Fluorene 0.2176 49.8 35.2 1480.004 00.108

Indeno(1,2,3-cd)pyrene 0.2176 63.1 10 1640.004 0.027150.164

Naphthalene 0.2176 43.3 14.7 1280.004 00.094

Phenanthrene 0.2176 58.1 32.8 1430.004 0.038510.165

Pyrene 0.2176 71.5 10 1800.004 0.088190.244

Surr: 2-Fluorobiphenyl 0.2176 44.9 10 1310.098







Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123660

SeqNo: 2311874

LCSSampType:

SW3550B

Acenaphthene 0.1670 62.8 56.3 1150.003 00.105

Acenaphthylene 0.1670 66.6 60.3 1430.003 00.111

Anthracene 0.1670 61.1 52.1 1090.003 00.102


Benzo(a)pyrene 0.1670 67.7 40.8 1270.003 00.113



Benzo(k)fluoranthene 0.1670 73.6 52 1530.003 00.123

Bis(2-ethylhexyl)phthalate 0.1670 77.2 50 1500.067 00.129

Chrysene 0.1670 68.0 60.8 1280.003 00.114


Fluoranthene 0.1670 73.6 58.7 1250.003 00.123

of 54




Lab Order: 09060783







Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123660

SeqNo: 2311874

LCSSampType:

SW3550B

Fluorene 0.1670 66.9 57.8 1250.003 00.112

Indeno(1,2,3-cd)pyrene 0.1670 73.7 52 1470.003 00.123

Naphthalene 0.1670 59.0 54.8 1130.003 00.099

Phenanthrene 0.1670 66.8 60.4 1210.003 00.112

Pyrene 0.1670 76.1 57.9 1290.003 00.127








Units: mg/Kg-dry

PQL


RunNo: 123660

SeqNo: 2311875

MSDSampType:

SW3550B

Acenaphthene 0.2150 69.7 36 135 49.70.004 0 0.1051 35.10.150

Acenaphthylene 0.2150 70.8 17.2 167 33.30.004 0 0.1153 27.70.152

Anthracene 0.2150 76.0 39.3 124 51.10.004 0.004360 0.1117 40.20.168

Benzo(a)anthracene 0.2150 91.7 10 183 40.60.004 0.03630 0.1575 38.80.233

Benzo(a)pyrene 0.2150 110.5 10 204 56.40.004 0.04226 0.1929 36.80.280

Benzo(b)fluoranthene 0.2150 139.6 10.6 178 49.70.004 0.06333 0.2198 49.20.363

Benzo(g,h,i)perylene 0.2150 58.7 10 168 36.50.004 0.03156 0.1569 0.5580.158

Benzo(k)fluoranthene 0.2150 110.6 27.6 181 42.6 R0.004 0.02284 0.1665 44.10.261

Bis(2-ethylhexyl)phthalate 0.2150 14.4 50 150 60.3 S0.086 0.1662 0.1356 37.00.197

Chrysene 0.2150 105.3 10 176 45.10.004 0.04891 0.1842 39.60.275

Dibenzo(a,h)anthracene 0.2150 60.1 12.2 156 39.90.004 0.007252 0.1259 8.010.136

Fluoranthene 0.2150 155.9 10 227 66.20.004 0.1106 0.2729 48.10.446

Fluorene 0.2150 72.7 35.2 148 65.60.004 0 0.1084 36.20.156

Indeno(1,2,3-cd)pyrene 0.2150 70.2 10 164 36.50.004 0.02715 0.1644 7.980.178

Naphthalene 0.2150 64.1 14.7 128 39.60.004 0 0.09411 37.70.138

Phenanthrene 0.2150 114.4 32.8 143 35.4 R0.004 0.03851 0.1649 53.20.284

Pyrene 0.2150 140.8 10 180 60.10.004 0.08819 0.2437 46.40.391

Surr: 2-Fluorobiphenyl 0.2150 61.1 10 131 4000.131

of 54




Lab Order: 09060783







Units: mg/Kg-dry

PQL


RunNo: 123660

SeqNo: 2311875

MSDSampType:

SW3550B

Surr: Nitrobenzene-d5 0.2150 65.3 10 132 4000.140


of 54




Lab Order: 09060783

ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S


Sample ID: LCS-F090618-2




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123640

SeqNo: 2311283

LCSSampType:

SW5035

1,1,1-Trichloroethane 50.00 105.1 77.5 1215.0 052.5

1,1-Dichloroethene 50.00 103.5 52 1335.0 051.8

1,2-Dibromoethane 50.00 101.2 85.2 1195.0 050.6

1,2-Dichlorobenzene 50.00 107.9 84.2 1225.0 054.0

1,2-Dichloroethane 50.00 108.9 71.1 1255.0 054.5



2-Butanone 100.0 56.0 39.1 10550.0 056.0

Benzene 50.00 104.4 77.9 1231.0 052.2

Bromodichloromethane 50.00 115.9 87.9 1195.0 057.9

Carbon tetrachloride 50.00 112.4 77.5 1285.0 056.2

Chlorobenzene 50.00 108.2 87.8 1205.0 054.1

Chloroform 50.00 100 81.5 1195.0 050.0

Dibromochloromethane 50.00 109.6 88.6 1195.0 054.8

Ethylbenzene 50.00 108.7 80.9 1195.0 054.4

m,p-Xylenes 50.00 104.9 77.6 1205.0 052.5

Methyl tert-butyl ether 50.00 104.6 69.8 1212.0 052.3

Methylene chloride 50.00 99.3 71.5 1245.0 049.7

Naphthalene 50.00 118.1 75.7 12310 059.0

o-Xylene 50.00 101.2 82.4 1245.0 050.6

Tetrachloroethene 50.00 96.3 74.2 1135.0 048.2

Toluene 50.00 104.4 80.2 1155.0 052.2

Trichloroethene 50.00 105.3 83.3 1185.0 052.6

Surr: 1,2-Dichloroethane-d4 50.00 109.3 61 12854.6

Surr: 4-Bromofluorobenzene 50.00 96.5 78.2 11748.3

Surr: Dibromofluoromethane 50.00 102.6 66.6 13051.3

Surr: Toluene-d8 50.00 93.9 80.1 12247.0

of 54




Lab Order: 09060783



Sample ID: LCSD-F090618-2




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123640

SeqNo: 2311284

LCSDSampType:

SW5035

1,1,1-Trichloroethane 50.00 102.8 77.5 121 205.0 0 52.53 2.1951.4

1,1-Dichloroethene 50.00 98.9 52 133 205.0 0 51.75 4.5149.5

1,2-Dibromoethane 50.00 97.2 85.2 119 205.0 0 50.58 4.0148.6

1,2-Dichlorobenzene 50.00 103.5 84.2 122 205.0 0 53.96 4.1851.8

1,2-Dichloroethane 50.00 107.0 71.1 125 205.0 0 54.47 1.8353.5



2-Butanone 100.0 51.5 39.1 105 2050.0 0 55.95 8.2451.5

Benzene 50.00 101.6 77.9 123 201.0 0 52.20 2.7650.8

Bromodichloromethane 50.00 113.4 87.9 119 205.0 0 57.93 2.1656.7

Carbon tetrachloride 50.00 109.0 77.5 128 205.0 0 56.19 3.0954.5

Chlorobenzene 50.00 106.0 87.8 120 205.0 0 54.11 2.0353.0

Chloroform 50.00 98.2 81.5 119 205.0 0 49.99 1.7649.1

Dibromochloromethane 50.00 106.7 88.6 119 205.0 0 54.78 2.6353.4

Ethylbenzene 50.00 105.7 80.9 119 205.0 0 54.36 2.7852.9

m,p-Xylenes 50.00 103.3 77.6 120 205.0 0 52.46 1.5851.6

Methyl tert-butyl ether 50.00 99.7 69.8 121 202.0 0 52.32 4.8449.8

Methylene chloride 50.00 97.0 71.5 124 205.0 0 49.67 2.3848.5

Naphthalene 50.00 110.5 75.7 123 2010 0 59.05 6.6155.3

o-Xylene 50.00 99.4 82.4 124 205.0 0 50.59 1.7349.7

Tetrachloroethene 50.00 92.4 74.2 113 205.0 0 48.17 4.1546.2

Toluene 50.00 102.8 80.2 115 205.0 0 52.21 1.5451.4

Trichloroethene 50.00 101.6 83.3 118 205.0 0 52.64 3.5850.8

Surr: 1,2-Dichloroethane-d4 50.00 108.5 61 128 0054.2

Surr: 4-Bromofluorobenzene 50.00 97.3 78.2 117 0048.6

Surr: Dibromofluoromethane 50.00 102.2 66.6 130 0051.1

Surr: Toluene-d8 50.00 94.5 80.1 122 0047.2

of 54




Lab Order: 09060783



Sample ID: MBLK-F090618-2




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123640

SeqNo: 2311285

MBLKSampType:

SW5035

1,1,1,2-Tetrachloroethane 5.0ND

1,1,1-Trichloroethane 5.0ND


1,1,2-Trichloro-1,2,2-trifluoroethane 5.0ND


1,1-Dichloro-2-propanone 50.0ND

1,1-Dichloroethane 5.0ND

1,1-Dichloroethene 5.0ND

1,1-Dichloropropene 5.0ND


1,2,3-Trichloropropane 10ND

1,2,3-Trimethylbenzene 5.0ND



1,2-Dibromo-3-chloropropane 5.0ND

1,2-Dibromoethane 5.0ND



1,2-Dichloropropane 5.0ND





1-Chlorobutane 5.0ND


2-Butanone 50.0ND

2-Chlorotoluene 5.0ND

2-Hexanone 50.0ND

2-Nitropropane 50.0ND


4-Methyl-2-pentanone 50.0ND

of 54




Lab Order: 09060783







Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123640

SeqNo: 2311285

MBLKSampType:

SW5035

Acetone 50.0ND

Acrolein 100ND

Acrylonitrile 10ND

Allyl chloride 5.0ND

Benzene 1.0ND

Bromobenzene 5.0ND

Bromochloromethane 5.0ND

Bromodichloromethane 5.0ND

Bromoform 5.0ND

Bromomethane 10ND

Carbon disulfide 5.0ND

Carbon tetrachloride 5.0ND

Chlorobenzene 5.0ND

Chloroethane 10ND

Chloroform 5.0ND

Chloromethane 10ND

cis-1,2-Dichloroethene 5.0ND

cis-1,3-Dichloropropene 4.0ND

Cyclohexanone 100ND

Dibromochloromethane 5.0ND

Dibromomethane 5.0ND

Dichlorodifluoromethane 10ND

Ethyl acetate 50.0ND

Ethyl ether 5.0ND

Ethyl methacrylate 5.0ND

Ethylbenzene 5.0ND

Heptane 20.0ND



Iodomethane 10ND

Isopropylbenzene 5.0ND

of 54




Lab Order: 09060783







Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 123640

SeqNo: 2311285

MBLKSampType:

SW5035

m,p-Xylenes 5.0ND

Methacrylonitrile 50.0ND

Methyl Methacrylate 5.0ND

Methyl tert-butyl ether 2.0ND

Methylacrylate 10ND

Methylene chloride 5.0ND

Naphthalene 10ND

n-Butylbenzene 5.0ND

n-Hexane 20.0ND

Nitrobenzene 100ND

n-Propylbenzene 5.0ND

o-Xylene 5.0ND

Pentachloroethane 5.0ND

p-Isopropyltoluene 5.0ND

Propionitrile 50.0ND

sec-Butylbenzene 5.0ND

Styrene 5.0ND

tert-Butylbenzene 5.0ND

Tetrachloroethene 5.0ND

Tetrahydrofuran 50.0ND

Toluene 5.0ND

trans-1,2-Dichloroethene 5.0ND

trans-1,3-Dichloropropene 4.0ND

Trichloroethene 5.0ND

Trichlorofluoromethane 5.0ND

Vinyl acetate 50.0ND

Vinyl chloride 2.0ND




Surr: Toluene-d8 50.00 96.3 80.1 12248.1

of 54



Lab Order: 09060783

RECEIVING CHECK LIST





TEL: 618-344-1004

FAX: 618-344-1005

Received By: EAHCarrier: Zach Pearce

Completed by: Reviewed by:

On:

18-Jun-09

On:

19-Jun-09

Shipping container/cooler in good condition? Yes No Not Present

Chain of custody present? Yes No

Chain of custody signed when relinquished and received? Yes No

Chain of custody agrees with sample labels? Yes No

Samples in proper container/bottle? Yes No

Sample containers intact? Yes No

Sufficient sample volume for indicated test? Yes No

All samples received within holding time? Yes No

Container/Temp Blank temperature in compliance? Yes No

Temp °C 4.2

When thermal preservation is required, samples are compliant with a temperature between 0.1°C - 6.0°C, or when samples are received on ice the same day as collected.

Any No responses must be detailed below or on the COC.

Water - VOA vials have zero headspace? Yes No No VOA vials submitted

Water - pH acceptable upon receipt? Yes No

Type of thermal preservation? None Ice Blue Ice Dry Ice

Chain of custody 1 Extra pages included 0

Reported field parameters measured: Field Lab NA

Pages to follow:

Elizabeth A. Hurley Heather A. White





TEL: 618-344-1004

FAX: 618-344-1005

August 18, 2009





Sincerely,


RE:

Dear Pete Sazama:



(618) 281-7173(618) 281-5120

TEL:FAX:


Heather A. WhiteProject Manager

(618)344-1004 ex 20

IL ELAP and NELAP Accredited - Accreditation #100226 Page 1 of 21


Lab Order: 09080556

SAMPLE SUMMARY

Report Date: 18-Aug-09





TEL: 618-344-1004

FAX: 618-344-1005

Fractions

09080556-001 JH-1 8/14/2009 10:45:00 AM6

09080556-002 JH-2 8/14/2009 11:20:00 AM6





TEL: 618-344-1004

FAX: 618-344-1005

A831-735002-012901-225/Ameren Champaign 624030530908055618-Aug-09

Project:LabOrder:

Client:

Report Date:





Qualifiers






- Reporting Limit

- Dilution Factor






DF

RL

TNTC

Surr

IDPH

B

J

R

S

X

NELAP

E

MI

H

ND

D





Collection Date: 8/14/2009 10:45:00 AM

Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09080556

Lab ID: 09080556-001

Client Sample ID: JH-1





TEL: 618-344-1004

FAX: 618-344-1005





Cadmium 8/17/2009 2:02:35 PM0.20 mg/Kg-dry 1< 0.20 LALNELAP




SW-846 3050B, METALS BY GFAASelenium 7740 8/17/2009 2:26:04 PM0.556 mg/Kg-dry 1< 0.556 JMWNELAP




Benzo(a)anthracene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP

Benzo(a)pyrene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP

Benzo(b)fluoranthene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP

Benzo(g,h,i)perylene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP

Benzo(k)fluoranthene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP


Chrysene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP


Fluoranthene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP




Phenanthrene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP

Pyrene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP




SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSBenzene 8/17/2009 1:50:00 PM1.0 µg/Kg-dry 1ND JSANELAP



Xylenes, Total J 8/17/2009 1:50:00 PM4.8 µg/Kg-dry 12.0 JSANELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09080556

Lab ID: 09080556-001






TEL: 618-344-1004

FAX: 618-344-1005

Sample Narrative

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 1,2-Dichloroethane-d4 8/17/2009 1:50:00 PM61-128 %REC 196.7 JSA

Surr: 4-Bromofluorobenzene 8/17/2009 1:50:00 PM78.2-117 %REC 191.1 JSA



SW-846 7471AMercury 8/14/20090.012 mg/Kg-dry 10.037 ALUNELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09080556

Lab ID: 09080556-002






TEL: 618-344-1004

FAX: 618-344-1005









SW-846 3050B, METALS BY GFAASelenium 7740 8/17/2009 2:29:28 PM0.588 mg/Kg-dry 1< 0.588 JMWNELAP





















SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSBenzene 8/17/2009 2:17:00 PM0.9 µg/Kg-dry 12.5 JSANELAP

Ethylbenzene J 8/17/2009 2:17:00 PM4.7 µg/Kg-dry 11.8 JSANELAP

Toluene 8/17/2009 2:17:00 PM4.7 µg/Kg-dry 15.4 JSANELAP

Xylenes, Total J 8/17/2009 2:17:00 PM4.7 µg/Kg-dry 14.0 JSANELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 09080556

Lab ID: 09080556-002






TEL: 618-344-1004

FAX: 618-344-1005

Sample Narrative

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 1,2-Dichloroethane-d4 8/17/2009 2:17:00 PM61-128 %REC 1102.3 JSA

Surr: 4-Bromofluorobenzene 8/17/2009 2:17:00 PM78.2-117 %REC 190.5 JSA



SW-846 7471AMercury 8/14/20090.011 mg/Kg-dry 10.028 ALUNELAP



Date/Time

DATES REPORT

Lab Order: 09080556


Test NamePrep

Date/Time




TEL: 618-344-1004

FAX: 618-344-1005

18-Aug-09Report Date:

09080556-001A JH-1 8/14/2009 Solid SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS

8/17/2009 9:07:00 PM

8/17/2009 8:49:43 AM


8/17/2009 8:39:34 AM

SW-846 3050B, Metals by GFAA 8/17/2009 2:26:04 PM

8/17/2009 8:37:02 AM

SW-846 7471A 8/14/20098/14/2009 5:30:00 PM

09080556-001C ASTM D2974 8/14/2009 6:00:00 PM



8/17/2009 1:50:00 PM

09080556-002A JH-2 SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS

8/17/2009 10:52:00 PM

8/17/2009 8:49:43 AM


8/17/2009 8:39:35 AM


8/17/2009 8:37:02 AM

SW-846 7471A 8/14/20098/14/2009 5:30:00 PM

09080556-002C ASTM D2974 8/14/2009 6:00:00 PM



8/17/2009 2:17:00 PM

Page 8 of 21IL ELAP and NELAP Accredited - Accreditation #100226



Qualifiers






- Reporting Limit

- Dilution Factor







DF

RL

TNTC

Surr

IDPH

B

J

R

S

X NELAP

E

MI

H

ND





CCV

DF

DUP

ICV

LCS

MS

MSD

MDL

MB/LCB

PQL

RL

RPD



Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. (NELAC) The acceptable recovery range is listed in this report.

Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in this report.Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in this report.Method detection limit or limit of detection (LOD) means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.Method blank or lab control blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences are present at concentrations that impact the analytical results for sample analyses. (NELAC)Practical quantitation limit or limit of quantitation (LOQ) means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in this report.The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in this report.



Key QC concepts:

LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in this report.

Page 9 of 21




Lab Order: 09080556

ANALYTICAL QC SUMMARY REPORTTest Number: M2540 G




Prep Date:


Units: %

PQL

Client ID: ZZZZZZ

RunNo: 125818

SeqNo: 2361452

LCSSampType:

Total Solids 1.000 100 90 1100.1 01.0

Sample ID: LCSQC


Prep Date:


Units: %

PQL

Client ID: ZZZZZZ

RunNo: 125818

SeqNo: 2361453

LCSQCSampType:

Total Solids 1.000 100 90 1100.1 01.0

Sample ID: 09080556-001CDUP


Prep Date:


Units: %

PQL

Client ID: JH-1DUP

RunNo: 125818

SeqNo: 2361492

DUPSampType:

Total Solids 150.1 81.75 0.30681.5

Page 10 of 21




Lab Order: 09080556

ANALYTICAL QC SUMMARY REPORTTest Number: SW6010B


Sample ID: MB-54890




Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 125822

SeqNo: 2362135

MBLKSampType:

SOP 3032

Arsenic 2.500 0 -100 1002.50 0< 2.50

Barium 0.5000 0 -100 1000.50 0< 0.50

Cadmium 0.2000 0 -100 1000.20 0< 0.20

Chromium 1.000 0 -100 1001.00 0< 1.00

Lead 4.000 0 -100 1004.00 0< 4.00

Silver 1.000 0 -100 1000.55 0< 0.55





Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 125822

SeqNo: 2362136

LCSSampType:

SOP 3032

Arsenic 200.0 102.4 85 1152.50 0205

Barium 200.0 104.2 85 1150.50 0208

Cadmium 5.000 102.4 85 1150.20 05.12

Chromium 20.00 104.4 85 1151.00 020.9

Lead 50.00 103.0 85 1154.00 051.5

Silver 5.000 89.8 85 1150.55 04.49





Units: mg/Kg-dry

PQL

Client ID: JH-2MS

RunNo: 125822

SeqNo: 2362140

MSSampType:

SOP 3032

Arsenic 188.7 99.7 75 1252.36 2.953191

Barium 188.7 98.2 75 1250.47 161.4347

Cadmium 4.717 97.6 75 1250.19 0.32084.92

Chromium 18.87 111.1 75 1250.94 20.9241.9

Lead 47.17 95.8 75 1253.77 11.3356.5

Silver 4.717 90.6 75 1250.52 04.27

Page 11 of 21




Lab Order: 09080556







Units: mg/Kg-dry

PQL

Client ID: JH-2MSD

RunNo: 125822

SeqNo: 2362141

MSDSampType:

SOP 3032

Arsenic 188.7 95.4 75 125 202.36 2.953 191.1 4.34183

Barium 188.7 99.1 75 125 200.47 161.4 346.7 0.489348

Cadmium 4.717 94.4 75 125 200.19 0.3208 4.925 3.114.77

Chromium 18.87 102.7 75 125 200.94 20.92 41.88 3.8640.3

Lead 47.17 92.2 75 125 203.77 11.33 56.54 3.0754.8

Silver 4.717 84.8 75 125 200.52 0 4.274 6.614.00

Page 12 of 21




Lab Order: 09080556

ANALYTICAL QC SUMMARY REPORTTest Number: SW7000 G


Sample ID: MB-54889




Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 125859

SeqNo: 2362160

MBLKSampType:

SOP 3042

Selenium 7740 0.6000 0 -100 1000.600 0< 0.600





Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 125859

SeqNo: 2362161

LCSSampType:

SOP 3042

Selenium 7740 3.000 99.9 80 1200.600 03.00





Units: mg/Kg-dry

PQL

Client ID: JH-2MS

RunNo: 125859

SeqNo: 2362167

MSSampType:

SOP 3042

Selenium 7740 2.941 86.7 70 1301.18 02.55





Units: mg/Kg-dry

PQL

Client ID: JH-2MSD

RunNo: 125859

SeqNo: 2362168

MSDSampType:

SOP 3042

Selenium 7740 2.941 86.1 70 130 201.18 0 2.551 0.7422.53

Page 13 of 21




Lab Order: 09080556

ANALYTICAL QC SUMMARY REPORTTest Number: SW7471 A


Sample ID: MB-54887




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 125846

SeqNo: 2361957

MBLKSampType:

SOP 3063

Mercury 0.01000 0 -100 1000.010 0< 0.010





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 125846

SeqNo: 2361958

LCSSampType:

SOP 3063

Mercury 0.2500 94.8 85 1150.010 00.237





Units: mg/Kg-dry

PQL

Client ID: JH-2MS

RunNo: 125846

SeqNo: 2361961

MSSampType:

SOP 3063

Mercury 0.2800 100 75 1250.011 0.028000.308





Units: mg/Kg-dry

PQL

Client ID: JH-2MSD

RunNo: 125846

SeqNo: 2361962

MSDSampType:

SOP 3063

Mercury 0.2800 106.4 75 125 150.011 0.02800 0.3080 5.650.326

Page 14 of 21




Lab Order: 09080556



Sample ID: LCS-G090817-1




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 125856

SeqNo: 2362109

LCSSampType:

SW5035

Benzene 50.00 79.8 77.9 1231.0 039.9

Toluene 50.00 83.4 80.2 1155.0 041.7

Ethylbenzene 50.00 86.7 80.9 1195.0 043.4

Xylenes, Total 100.0 81.5 77.6 1245.0 081.5




Surr: Toluene-d8 50.00 98.1 80.1 12249.0

Sample ID: LCSD-G090817-1




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 125856

SeqNo: 2362110

LCSDSampType:

SW5035

Benzene 50.00 84.4 77.9 123 201.0 0 39.90 5.6342.2

Toluene 50.00 86.8 80.2 115 205.0 0 41.69 4.0043.4

Ethylbenzene 50.00 89.0 80.9 119 205.0 0 43.35 2.6444.5

Xylenes, Total 100.0 84.7 77.6 124 205.0 0 81.51 3.8084.7

Surr: 1,2-Dichloroethane-d4 50.00 90.2 61 128 0045.1



Surr: Toluene-d8 50.00 97.7 80.1 122 0048.9

Sample ID: MBLK-G090817-1




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 125856

SeqNo: 2362112

MBLKSampType:

SW5035

Benzene 1.0ND

Toluene 5.0ND

Ethylbenzene 5.0ND

Xylenes, Total 5.0ND

Page 15 of 21




Lab Order: 09080556







Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 125856

SeqNo: 2362112

MBLKSampType:

SW5035




Surr: Toluene-d8 50.00 94.4 80.1 12247.2

Page 16 of 21




Lab Order: 09080556

ANALYTICAL QC SUMMARY REPORTTest Number: SW8270C


Sample ID: MB-54886




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 125866

SeqNo: 2362345

MBLKSampType:

SW3550B



Anthracene 0.003ND







Chrysene 0.003ND



Fluorene 0.003ND


Naphthalene 0.003ND


Pyrene 0.003ND








Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 125866

SeqNo: 2362346

LCSSampType:

SW3550B

Acenaphthene 0.1670 63.3 56.3 1150.003 00.106

Acenaphthylene 0.1670 69.0 60.3 1430.003 00.115

Anthracene 0.1670 62.4 52.1 1090.003 00.104


Benzo(a)pyrene 0.1670 67.9 40.8 1270.003 00.113

Page 17 of 21




Lab Order: 09080556







Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 125866

SeqNo: 2362346

LCSSampType:

SW3550B





Chrysene 0.1670 70.7 60.8 1280.003 00.118


Fluoranthene 0.1670 70.5 58.7 1250.003 00.118

Fluorene 0.1670 67.9 57.8 1250.003 00.113

Indeno(1,2,3-cd)pyrene 0.1670 73.6 52 1470.003 00.123

Naphthalene 0.1670 65.6 54.8 1130.003 00.110

Phenanthrene 0.1670 67.0 60.4 1210.003 00.112

Pyrene 0.1670 71.5 57.9 1290.003 00.119








Units: mg/Kg-dry

PQL

Client ID: JH-1MS

RunNo: 125866

SeqNo: 2362348

MSSampType:

SW3550B

Acenaphthene 0.2048 68.4 36 1350.004 00.140

Acenaphthylene 0.2048 71.7 17.2 1670.004 00.147

Anthracene 0.2048 62.5 39.3 1240.004 00.128

Benzo(a)anthracene 0.2048 63.6 10 1830.004 00.130

Benzo(a)pyrene 0.2048 66.8 10 2040.004 00.137


Benzo(g,h,i)perylene 0.2048 73.8 10 1680.004 00.151



Chrysene 0.2048 79.6 10 1760.004 00.163

Page 18 of 21




Lab Order: 09080556







Units: mg/Kg-dry

PQL

Client ID: JH-1MS

RunNo: 125866

SeqNo: 2362348

MSSampType:

SW3550B


Fluoranthene 0.2048 67.7 10 2270.004 00.139

Fluorene 0.2048 69.8 35.2 1480.004 00.143

Indeno(1,2,3-cd)pyrene 0.2048 77.1 10 1640.004 00.158

Naphthalene 0.2048 42.7 14.7 1280.004 00.088

Phenanthrene 0.2048 67.4 32.8 1430.004 00.138

Pyrene 0.2048 70.0 10 1800.004 00.143








Units: mg/Kg-dry

PQL

Client ID: JH-1MSD

RunNo: 125866

SeqNo: 2362349

MSDSampType:

SW3550B

Acenaphthene 0.1984 71.3 36 135 49.70.004 0 0.1402 0.9230.141

Acenaphthylene 0.1984 76.8 17.2 167 33.30.004 0 0.1468 3.750.152

Anthracene 0.1984 67.7 39.3 124 51.10.004 0 0.1280 4.910.134

Benzo(a)anthracene 0.1984 68.2 10 183 40.60.004 0 0.1303 3.750.135

Benzo(a)pyrene 0.1984 74.2 10 204 56.40.004 0 0.1368 7.320.147

Benzo(b)fluoranthene 0.1984 82.2 10.6 178 49.70.004 0 0.1620 0.6230.163

Benzo(g,h,i)perylene 0.1984 80.2 10 168 36.50.004 0 0.1512 5.080.159

Benzo(k)fluoranthene 0.1984 85.3 27.6 181 42.60.004 0 0.1668 1.450.169

Bis(2-ethylhexyl)phthalate 0.1984 106.9 50 150 60.30.080 0 0.2142 1.000.212

Chrysene 0.1984 87.3 10 176 45.10.004 0 0.1631 5.980.173

Dibenzo(a,h)anthracene 0.1984 78.3 12.2 156 39.90.004 0 0.1509 2.910.155

Fluoranthene 0.1984 76.6 10 227 66.20.004 0 0.1388 9.050.152

Fluorene 0.1984 71.1 35.2 148 65.60.004 0 0.1430 1.380.141

Indeno(1,2,3-cd)pyrene 0.1984 79.7 10 164 36.50.004 0 0.1580 0.1180.158

Naphthalene 0.1984 61.0 14.7 128 39.60.004 0 0.08753 32.10.121

Page 19 of 21




Lab Order: 09080556







Units: mg/Kg-dry

PQL

Client ID: JH-1MSD

RunNo: 125866

SeqNo: 2362349

MSDSampType:

SW3550B

Phenanthrene 0.1984 74.8 32.8 143 35.40.004 0 0.1380 7.210.148

Pyrene 0.1984 74.1 10 180 60.10.004 0 0.1433 2.570.147




Page 20 of 21



Lab Order: 09080556






TEL: 618-344-1004

FAX: 618-344-1005

Received By: EAHCarrier: J. Crompton


On:

14-Aug-09

On:

17-Aug-09










Temp °C 2.8



Water - VOA vials have zero headspace? Yes No No VOA vials submitted





Pages to follow:

Marvin L. Darling Heather A. White


P2-Borrow 2

Date Collected 10/20/2009 2:45:00 PM

Sample P2-Borrow 2

Analyte Unit

Cyanide, Amenable to Chlorination mg/Kg-dry < Interference

Cyanide mg/Kg-dry < 0.61

Total Solids % 84.1

Mercury mg/Kg-dry 0.024

Selenium mg/Kg-dry < 0.6

Arsenic mg/Kg-dry 5.87

Barium mg/Kg-dry 114

Cadmium mg/Kg-dry 0.28

Chromium mg/Kg-dry 24.3

Lead mg/Kg-dry 16.5

Silver mg/Kg-dry < 0.55

Percent Moisture % 15.9

1,2,4-Trichlorobenzene mg/Kg-dry < 0.582

1,2-Dichlorobenzene mg/Kg-dry < 0.582

1,2-Diphenylhydrazine mg/Kg-dry < 0.978



2,4,5-Trichlorophenol mg/Kg-dry < 0.407


2,4-Dichlorophenol mg/Kg-dry < 0.582

2,4-Dimethylphenol mg/Kg-dry < 0.582

2,4-Dinitrophenol mg/Kg-dry < 1.16

2,4-Dinitrotoluene mg/Kg-dry < 0.407 S

2,6-Dinitrotoluene mg/Kg-dry < 0.407

2-Chloronaphthalene mg/Kg-dry < 0.407

2-Chlorophenol mg/Kg-dry < 0.582

2-Methoxy-4-methylphenol mg/Kg-dry < 0.757

2-Methylnaphthalene mg/Kg-dry < 0.407

2-Nitroaniline mg/Kg-dry < 1.16

2-Nitrophenol mg/Kg-dry < 0.407

3,3´-Dichlorobenzidine mg/Kg-dry < 0.407


4,6-Dinitro-2-methylphenol mg/Kg-dry < 1.16

4-Bromophenyl phenyl ether mg/Kg-dry < 0.407

4-Chloro-3-methylphenol mg/Kg-dry < 0.582

4-Chloroaniline mg/Kg-dry < 0.582

4-Chlorophenyl phenyl ether mg/Kg-dry < 0.407



Aniline mg/Kg-dry < 0.582

Azobenzene mg/Kg-dry < 0.407

Benzidine mg/Kg-dry < 1.23

Benzoic acid mg/Kg-dry < 1.75

Benzyl alcohol mg/Kg-dry < 0.582

Bis(2-chloroethoxy)methane mg/Kg-dry < 0.407

Bis(2-chloroethyl)ether mg/Kg-dry < 0.582

Bis(2-chloroisopropyl)ether mg/Kg-dry < 0.407

Butyl benzyl phthalate mg/Kg-dry < 0.407

Result

Page 5

P2-Borrow 2

Carbazole mg/Kg-dry < 0.582

Dibenzofuran mg/Kg-dry < 0.407

Diethyl phthalate mg/Kg-dry < 0.582

Dimethyl phthalate mg/Kg-dry < 0.407

Di-n-butyl phthalate mg/Kg-dry < 0.407

Di-n-octyl phthalate mg/Kg-dry < 0.407

Hexachlorobenzene mg/Kg-dry < 0.407

Hexachlorobutadiene mg/Kg-dry < 0.582

Hexachlorocyclopentadiene mg/Kg-dry < 0.407

Hexachloroethane mg/Kg-dry < 0.582

Isophorone mg/Kg-dry < 0.407

m,p-Cresol mg/Kg-dry < 0.582

Nitrobenzene mg/Kg-dry < 0.582

N-Nitrosodimethylamine mg/Kg-dry < 0.582

N-Nitroso-di-n-propylamine mg/Kg-dry < 0.582

N-Nitrosodiphenylamine mg/Kg-dry < 0.582

o-Cresol mg/Kg-dry < 0.582

Pentachlorophenol mg/Kg-dry < 2.33

Phenol mg/Kg-dry < 0.407

Pyridine mg/Kg-dry < 0.582

Acenaphthene mg/Kg-dry < 0.004

Acenaphthylene mg/Kg-dry < 0.004

Anthracene mg/Kg-dry < 0.004

Benzo(a)anthracene mg/Kg-dry 0.019

Benzo(a)pyrene mg/Kg-dry 0.033

Benzo(b)fluoranthene mg/Kg-dry 0.037

Benzo(g,h,i)perylene mg/Kg-dry 0.036

Benzo(k)fluoranthene mg/Kg-dry 0.011

Bis(2-ethylhexyl)phthalate mg/Kg-dry < 0.078

Chrysene mg/Kg-dry 0.024

Dibenzo(a,h)anthracene mg/Kg-dry 0.007

Fluoranthene mg/Kg-dry 0.041

Fluorene mg/Kg-dry < 0.004

Indeno(1,2,3-cd)pyrene mg/Kg-dry 0.018

Naphthalene mg/Kg-dry < 0.004

Phenanthrene mg/Kg-dry 0.013

Pyrene mg/Kg-dry 0.039

1,1,1,2-Tetrachloroethane µg/Kg-dry < 4.9

1,1,1-Trichloroethane µg/Kg-dry < 4.9


1,1,2-Trichloro-1,2,2-trifluoroethane µg/Kg-dry < 4.9


1,1-Dichloro-2-propanone µg/Kg-dry < 48.7

1,1-Dichloroethane µg/Kg-dry < 4.9

1,1-Dichloroethene µg/Kg-dry < 4.9

1,1-Dichloropropene µg/Kg-dry < 4.9

1,2,3-Trichlorobenzene µg/Kg-dry < 4.9

1,2,3-Trichloropropane µg/Kg-dry < 9.7

1,2,3-Trimethylbenzene µg/Kg-dry < 4.9



1,2-Dibromo-3-chloropropane µg/Kg-dry < 4.9

Page 6

P2-Borrow 2

1,2-Dibromoethane µg/Kg-dry < 4.9

1,2-Dichlorobenzene µg/Kg-dry < 4.9


1,2-Dichloropropane µg/Kg-dry < 4.9





1-Chlorobutane µg/Kg-dry < 4.9


2-Butanone µg/Kg-dry < 48.7

2-Chlorotoluene µg/Kg-dry < 4.9

2-Hexanone µg/Kg-dry < 48.7

2-Nitropropane µg/Kg-dry < 48.7


4-Methyl-2-pentanone µg/Kg-dry < 48.7

Acetone µg/Kg-dry < 48.7

Acrolein µg/Kg-dry < 97.3

Acrylonitrile µg/Kg-dry < 9.7

Allyl chloride µg/Kg-dry < 4.9

Benzene µg/Kg-dry < 1

Bromobenzene µg/Kg-dry < 4.9

Bromochloromethane µg/Kg-dry < 4.9

Bromodichloromethane µg/Kg-dry < 4.9

Bromoform µg/Kg-dry < 4.9

Bromomethane µg/Kg-dry < 9.7

Carbon disulfide µg/Kg-dry < 4.9

Carbon tetrachloride µg/Kg-dry < 4.9

Chlorobenzene µg/Kg-dry < 4.9

Chloroethane µg/Kg-dry < 9.7

Chloroform µg/Kg-dry < 4.9

Chloromethane µg/Kg-dry 2.8 J

cis-1,2-Dichloroethene µg/Kg-dry < 4.9

cis-1,3-Dichloropropene µg/Kg-dry < 3.9

Cyclohexanone µg/Kg-dry < 97.3

Dibromochloromethane µg/Kg-dry < 4.9

Dibromomethane µg/Kg-dry < 4.9

Dichlorodifluoromethane µg/Kg-dry < 9.7

Ethyl acetate µg/Kg-dry < 48.7

Ethyl ether µg/Kg-dry < 4.9

Ethyl methacrylate µg/Kg-dry < 4.9

Ethylbenzene µg/Kg-dry < 4.9

Heptane µg/Kg-dry < 19.5

Hexachlorobutadiene µg/Kg-dry < 4.9

Hexachloroethane µg/Kg-dry < 4.9

Iodomethane µg/Kg-dry < 9.7

Isopropylbenzene µg/Kg-dry < 4.9

m,p-Xylenes µg/Kg-dry 1.1 J

Methacrylonitrile µg/Kg-dry < 48.7

Methyl Methacrylate µg/Kg-dry < 4.9

Methyl tert-butyl ether µg/Kg-dry < 1.9

Methylacrylate µg/Kg-dry < 9.7

Page 7

P2-Borrow 2

Methylene chloride µg/Kg-dry 1.4 J

Naphthalene µg/Kg-dry < 9.7

n-Butylbenzene µg/Kg-dry < 4.9

n-Hexane µg/Kg-dry < 19.5

Nitrobenzene µg/Kg-dry < 97.3

n-Propylbenzene µg/Kg-dry < 4.9

o-Xylene µg/Kg-dry < 4.9

Pentachloroethane µg/Kg-dry < 4.9

p-Isopropyltoluene µg/Kg-dry < 4.9

Propionitrile µg/Kg-dry < 48.7

sec-Butylbenzene µg/Kg-dry < 4.9

Styrene µg/Kg-dry < 4.9

tert-Butylbenzene µg/Kg-dry < 4.9

Tetrachloroethene µg/Kg-dry < 4.9

Tetrahydrofuran µg/Kg-dry < 48.7

Toluene µg/Kg-dry < 4.9

trans-1,2-Dichloroethene µg/Kg-dry < 4.9

trans-1,3-Dichloropropene µg/Kg-dry < 3.9

Trichloroethene µg/Kg-dry < 4.9

Trichlorofluoromethane µg/Kg-dry < 4.9

Vinyl acetate µg/Kg-dry < 48.7

Vinyl chloride µg/Kg-dry < 1.9

Page 8

P2-Borrow 1

Date Collected 10/20/2009 2:30:00 PM

Sample P2-Borrow 1

Analyte Unit

Cyanide, Amenable to Chlorination mg/Kg-dry < 0.597

Cyanide mg/Kg-dry < 0.6 R

Total Solids % 83.8

Mercury mg/Kg-dry 0.019

Selenium mg/Kg-dry < 0.545

Arsenic mg/Kg-dry 6.29

Barium mg/Kg-dry 106

Cadmium mg/Kg-dry 0.29

Chromium mg/Kg-dry 26

Lead mg/Kg-dry 16.5

Silver mg/Kg-dry < 0.55

Percent Moisture % 16.2

1,2,4-Trichlorobenzene mg/Kg-dry < 0.59


1,2-Diphenylhydrazine mg/Kg-dry < 0.992





2,4-Dichlorophenol mg/Kg-dry < 0.59

2,4-Dimethylphenol mg/Kg-dry < 0.59

2,4-Dinitrophenol mg/Kg-dry < 1.18



2-Chloronaphthalene mg/Kg-dry < 0.413

2-Chlorophenol mg/Kg-dry < 0.59

2-Methoxy-4-methylphenol mg/Kg-dry < 0.767

2-Methylnaphthalene mg/Kg-dry < 0.413



3,3´-Dichlorobenzidine mg/Kg-dry < 0.413


4,6-Dinitro-2-methylphenol mg/Kg-dry < 1.18

4-Bromophenyl phenyl ether mg/Kg-dry < 0.413

4-Chloro-3-methylphenol mg/Kg-dry < 0.59

4-Chloroaniline mg/Kg-dry < 0.59

4-Chlorophenyl phenyl ether mg/Kg-dry < 0.413



Aniline mg/Kg-dry < 0.59

Azobenzene mg/Kg-dry < 0.413

Benzidine mg/Kg-dry < 1.25

Benzoic acid mg/Kg-dry < 1.77

Benzyl alcohol mg/Kg-dry < 0.59

Bis(2-chloroethoxy)methane mg/Kg-dry < 0.413

Bis(2-chloroethyl)ether mg/Kg-dry < 0.59

Bis(2-chloroisopropyl)ether mg/Kg-dry < 0.413

Butyl benzyl phthalate mg/Kg-dry < 0.413

Result

Page 1

P2-Borrow 1

Carbazole mg/Kg-dry < 0.59

Dibenzofuran mg/Kg-dry < 0.413

Diethyl phthalate mg/Kg-dry < 0.59

Dimethyl phthalate mg/Kg-dry < 0.413

Di-n-butyl phthalate mg/Kg-dry < 0.413

Di-n-octyl phthalate mg/Kg-dry < 0.413

Hexachlorobenzene mg/Kg-dry < 0.413

Hexachlorobutadiene mg/Kg-dry < 0.59

Hexachlorocyclopentadiene mg/Kg-dry < 0.413

Hexachloroethane mg/Kg-dry < 0.59

Isophorone mg/Kg-dry < 0.413

m,p-Cresol mg/Kg-dry < 0.59

Nitrobenzene mg/Kg-dry < 0.59

N-Nitrosodimethylamine mg/Kg-dry < 0.59

N-Nitroso-di-n-propylamine mg/Kg-dry < 0.59

N-Nitrosodiphenylamine mg/Kg-dry < 0.59

o-Cresol mg/Kg-dry < 0.59

Pentachlorophenol mg/Kg-dry < 2.36

Phenol mg/Kg-dry < 0.413

Pyridine mg/Kg-dry < 0.59

Acenaphthene mg/Kg-dry < 0.004

Acenaphthylene mg/Kg-dry < 0.004

Anthracene mg/Kg-dry < 0.004

Benzo(a)anthracene mg/Kg-dry 0.006

Benzo(a)pyrene mg/Kg-dry 0.004

Benzo(b)fluoranthene mg/Kg-dry 0.006

Benzo(g,h,i)perylene mg/Kg-dry 0.004

Benzo(k)fluoranthene mg/Kg-dry < 0.004

Bis(2-ethylhexyl)phthalate mg/Kg-dry < 0.079

Chrysene mg/Kg-dry 0.004

Dibenzo(a,h)anthracene mg/Kg-dry < 0.004

Fluoranthene mg/Kg-dry 0.008

Fluorene mg/Kg-dry < 0.004

Indeno(1,2,3-cd)pyrene mg/Kg-dry < 0.004

Naphthalene mg/Kg-dry < 0.004

Phenanthrene mg/Kg-dry < 0.004

Pyrene mg/Kg-dry 0.007




1,1,2-Trichloro-1,2,2-trifluoroethane µg/Kg-dry < 4.1


1,1-Dichloro-2-propanone µg/Kg-dry < 41.4


1,1-Dichloroethene µg/Kg-dry < 4.1

1,1-Dichloropropene µg/Kg-dry < 4.1


1,2,3-Trichloropropane µg/Kg-dry < 8.3




1,2-Dibromo-3-chloropropane µg/Kg-dry < 4.1

Page 2

P2-Borrow 1

1,2-Dibromoethane µg/Kg-dry < 4.1








1-Chlorobutane µg/Kg-dry < 4.1


2-Butanone µg/Kg-dry < 41.4


2-Hexanone µg/Kg-dry < 41.4

2-Nitropropane µg/Kg-dry < 41.4


4-Methyl-2-pentanone µg/Kg-dry < 41.4

Acetone µg/Kg-dry 31 J

Acrolein µg/Kg-dry < 82.8

Acrylonitrile µg/Kg-dry < 8.3

Allyl chloride µg/Kg-dry < 4.1

Benzene µg/Kg-dry < 0.8

Bromobenzene µg/Kg-dry < 4.1

Bromochloromethane µg/Kg-dry < 4.1

Bromodichloromethane µg/Kg-dry < 4.1

Bromoform µg/Kg-dry < 4.1

Bromomethane µg/Kg-dry < 8.3

Carbon disulfide µg/Kg-dry < 4.1

Carbon tetrachloride µg/Kg-dry < 4.1

Chlorobenzene µg/Kg-dry < 4.1

Chloroethane µg/Kg-dry < 8.3

Chloroform µg/Kg-dry < 4.1

Chloromethane µg/Kg-dry < 8.3

cis-1,2-Dichloroethene µg/Kg-dry < 4.1

cis-1,3-Dichloropropene µg/Kg-dry < 3.3

Cyclohexanone µg/Kg-dry < 82.8

Dibromochloromethane µg/Kg-dry < 4.1

Dibromomethane µg/Kg-dry < 4.1

Dichlorodifluoromethane µg/Kg-dry < 8.3

Ethyl acetate µg/Kg-dry < 41.4

Ethyl ether µg/Kg-dry < 4.1

Ethyl methacrylate µg/Kg-dry < 4.1

Ethylbenzene µg/Kg-dry < 4.1

Heptane µg/Kg-dry < 16.6

Hexachlorobutadiene µg/Kg-dry < 4.1

Hexachloroethane µg/Kg-dry < 4.1

Iodomethane µg/Kg-dry < 8.3

Isopropylbenzene µg/Kg-dry < 4.1

m,p-Xylenes µg/Kg-dry 1 J

Methacrylonitrile µg/Kg-dry < 41.4

Methyl Methacrylate µg/Kg-dry < 4.1

Methyl tert-butyl ether µg/Kg-dry < 1.7

Methylacrylate µg/Kg-dry < 8.3

Page 3

P2-Borrow 1

Methylene chloride µg/Kg-dry 1.2 J

Naphthalene µg/Kg-dry < 8.3

n-Butylbenzene µg/Kg-dry < 4.1

n-Hexane µg/Kg-dry 1.9 J

Nitrobenzene µg/Kg-dry < 82.8

n-Propylbenzene µg/Kg-dry < 4.1

o-Xylene µg/Kg-dry < 4.1

Pentachloroethane µg/Kg-dry < 4.1

p-Isopropyltoluene µg/Kg-dry < 4.1

Propionitrile µg/Kg-dry < 41.4

sec-Butylbenzene µg/Kg-dry < 4.1

Styrene µg/Kg-dry < 4.1

tert-Butylbenzene µg/Kg-dry < 4.1

Tetrachloroethene µg/Kg-dry < 4.1

Tetrahydrofuran µg/Kg-dry < 41.4

Toluene µg/Kg-dry < 4.1

trans-1,2-Dichloroethene µg/Kg-dry < 4.1

trans-1,3-Dichloropropene µg/Kg-dry < 3.3

Trichloroethene µg/Kg-dry < 4.1

Trichlorofluoromethane µg/Kg-dry < 4.1

Vinyl acetate µg/Kg-dry < 41.4

Vinyl chloride µg/Kg-dry < 1.7

Page 4




TEL: 618-344-1004

FAX: 618-344-1005

April 21, 2010





Sincerely,


RE:

Dear Pete Sazama:



(618) 281-7173(618) 281-5120

TEL:FAX:


Shelly A. HennessyProject Manager

(618)344-1004 ex 36



Lab Order: 10040597

SAMPLE SUMMARY

Report Date: 21-Apr-10





TEL: 618-344-1004

FAX: 618-344-1005

Fractions

10040597-001 P4-Borrow #1 4/14/2010 10:00:00 AM5

10040597-002 P4 Borrow #2 4/14/2010 10:15:00 AM5





TEL: 618-344-1004

FAX: 618-344-1005

A831-735002-012901-225/Ameren Champaign 62490801201004059721-Apr-10

Project:LabOrder:

Client:

Report Date:





Qualifiers






- Reporting Limit

- Dilution Factor






DF

RL

TNTC

Surr

IDPH

B

J

R

S

X

NELAP

E

MI

H

ND

D






Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-001

Client Sample ID: P4-Borrow #1





TEL: 618-344-1004

FAX: 618-344-1005

EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 4/15/2010 4:10:00 PM0.1 % 111.2 JMT

STANDARD METHODS 18TH ED. 2540 GTotal Solids 4/15/2010 4:10:00 PM0.1 % 188.8 JMT



Cadmium J 4/16/2010 2:29:18 PM0.19 mg/Kg-dry 10.13 LALNELAP




SW-846 3050B, METALS BY GFAASelenium 7740 4/16/2010 1:41:26 PM0.556 mg/Kg-dry 1< 0.556 MEKNELAP

SW-846 3550B, 8081A, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

4,4´-DDE 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

4,4´-DDT 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Alachlor 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Aldrin 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

alpha-BHC 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

alpha-Chlordane 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

beta-BHC 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Chlordane 4/16/2010 10:51:00 AM3.85 µg/Kg-dry 1ND HENELAP

delta-BHC 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Dieldrin 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 13.89 HENELAP

Endosulfan I 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Endosulfan II 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Endosulfan sulfate 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Endrin 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Endrin aldehyde 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Endrin ketone 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

gamma-BHC 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

gamma-Chlordane 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Heptachlor 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Heptachlor epoxide 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Methoxychlor 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP

Toxaphene 4/16/2010 10:51:00 AM34.5 µg/Kg-dry 1ND HENELAP

Surr: Decachlorobiphenyl 4/16/2010 10:51:00 AM48-149 %REC 188.9 HE

Surr: Tetrachloro-m-xylene 4/16/2010 10:51:00 AM19-145 %REC 182.5 HE




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-001






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 4/16/2010 10:47:00 AM43.2 µg/Kg-dry 1ND HENELAP

Aroclor 1221 4/16/2010 10:47:00 AM43.2 µg/Kg-dry 1ND HENELAP







Surr: Tetrachloro-meta-xylene 4/16/2010 10:47:00 AM7.35-123 %REC 175.3 HE

SW-846 3550B, 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

2,4,5-TP (Silvex) 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

2,4-D 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

2,4-DB 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

3,5-Dichlorobenzoic Acid 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

4-Nitrophenol 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

Bentazon 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

Chloramben 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

Dalapon 4/16/2010 4:36:00 PM161 µg/Kg-dry 1ND HE

DCPA 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

Dicamba 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

Dichlorprop 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

MCPA 4/16/2010 4:36:00 PM1610 µg/Kg-dry 1ND HE

MCPP 4/16/2010 4:36:00 PM1610 µg/Kg-dry 1ND HE

Pentachlorophenol 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

Picloram 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE

Surr: 2,4-Dichlorophenylacetic acid 4/16/2010 4:36:00 PM18.1-118 %REC 147.6 HE

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 1ND MAMNELAP

Acenaphthylene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 1ND MAMNELAP

Anthracene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.005 MAMNELAP

Benzo(a)anthracene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.015 MAMNELAP

Benzo(a)pyrene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.013 MAMNELAP

Benzo(b)fluoranthene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.020 MAMNELAP

Benzo(g,h,i)perylene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.010 MAMNELAP

Benzo(k)fluoranthene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.007 MAMNELAP

Bis(2-ethylhexyl)phthalate 4/16/2010 11:39:00 AM0.075 mg/Kg-dry 1ND MAMNELAP

Chrysene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.018 MAMNELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-001






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSDibenzo(a,h)anthracene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 1ND MAMNELAP

Fluoranthene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.046 MAMNELAP

Fluorene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 1ND MAMNELAP

Indeno(1,2,3-cd)pyrene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.008 MAMNELAP

Naphthalene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 1ND MAMNELAP

Phenanthrene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.030 MAMNELAP

Pyrene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.036 MAMNELAP

Surr: 2-Fluorobiphenyl 4/16/2010 11:39:00 AM10-131 %REC 163.4 MAM

Surr: Nitrobenzene-d5 4/16/2010 11:39:00 AM10-132 %REC 165.5 MAM

Surr: p-Terphenyl-d14 4/16/2010 11:39:00 AM30.6-131 %REC 178.8 MAM

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

1,2-Dichlorobenzene 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP



2,4,5-Trichlorophenol 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP


2,4-Dichlorophenol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

2,4-Dimethylphenol S 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

2,4-Dinitrophenol 4/16/2010 10:03:00 AM1.12 mg/Kg-dry 1ND DMHNELAP

2,4-Dinitrotoluene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP


2-Chloronaphthalene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

2-Chlorophenol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

2-Methoxy-4-methylphenol 4/16/2010 10:03:00 AM0.725 mg/Kg-dry 1ND DMH

2-Methylnaphthalene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

2-Nitroaniline 4/16/2010 10:03:00 AM1.12 mg/Kg-dry 1ND DMHNELAP

2-Nitrophenol 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

3,3´-Dichlorobenzidine 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP


4,6-Dinitro-2-methylphenol 4/16/2010 10:03:00 AM1.12 mg/Kg-dry 1ND DMHNELAP

4-Bromophenyl phenyl ether 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

4-Chloro-3-methylphenol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

4-Chloroaniline 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

4-Chlorophenyl phenyl ether 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP



Aniline 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-001






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAzobenzene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMH

Benzidine 4/16/2010 10:03:00 AM1.18 mg/Kg-dry 1see note DMHNELAP

Benzoic acid 4/16/2010 10:03:00 AM1.67 mg/Kg-dry 1ND DMHNELAP

Benzyl alcohol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

Bis(2-chloroethoxy)methane 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

Bis(2-chloroethyl)ether 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

Bis(2-chloroisopropyl)ether 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

Butyl benzyl phthalate 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

Carbazole 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMH

Dibenzofuran 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

Diethyl phthalate 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

Dimethyl phthalate 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

Di-n-butyl phthalate 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

Di-n-octyl phthalate 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

Hexachlorobenzene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

Hexachlorobutadiene 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

Hexachlorocyclopentadiene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

Hexachloroethane 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

Isophorone 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

m,p-Cresol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

Nitrobenzene 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

N-Nitrosodimethylamine 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

N-Nitroso-di-n-propylamine 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

N-Nitrosodiphenylamine 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

o-Cresol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

Pentachlorophenol 4/16/2010 10:03:00 AM2.23 mg/Kg-dry 1ND DMHNELAP

Phenol 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP

Pyridine 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP

1,2-Diphenylhydrazine 4/16/2010 10:03:00 AM0.937 mg/Kg-dry 1ND DMH

Surr: 2,4,6-Tribromophenol 4/16/2010 10:03:00 AM32.7-130 %REC 174.0 DMH

Surr: 2-Fluorobiphenyl 4/16/2010 10:03:00 AM34.1-116 %REC 164.8 DMH

Surr: 2-Fluorophenol 4/16/2010 10:03:00 AM30.5-99 %REC 166.2 DMH

Surr: Nitrobenzene-d5 4/16/2010 10:03:00 AM34.1-101 %REC 160.9 DMH

Surr: Phenol-d5 4/16/2010 10:03:00 AM34.9-110 %REC 172.3 DMH

Surr: p-Terphenyl-d14 4/16/2010 10:03:00 AM41.7-124 %REC 179.6 DMH

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

1,1,1-Trichloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-001






TEL: 618-344-1004

FAX: 618-344-1005


1,1,2-Trichloro-1,2,2-trifluoroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWE


1,1-Dichloro-2-propanone 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWE

1,1-Dichloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

1,1-Dichloroethene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

1,1-Dichloropropene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

1,2,3-Trichlorobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

1,2,3-Trichloropropane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP

1,2,3-Trimethylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWE


1,2,4-Trimethylbenzene J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 10.8 RWENELAP

1,2-Dibromo-3-chloropropane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

1,2-Dibromoethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

1,2-Dichlorobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP


1,2-Dichloropropane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

1,3,5-Trimethylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP




1-Chlorobutane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP


2-Butanone 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP

2-Chlorotoluene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

2-Hexanone 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP

2-Nitropropane 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP


4-Methyl-2-pentanone 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP

Acetone 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP

Acrolein 4/16/2010 1:26:00 PM81.5 µg/Kg-dry 1ND RWENELAP

Acrylonitrile 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP

Allyl chloride 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Benzene 4/16/2010 1:26:00 PM0.8 µg/Kg-dry 11.8 RWENELAP

Bromobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Bromochloromethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Bromodichloromethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Bromoform 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-001






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSBromomethane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP

Carbon disulfide J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 12.5 RWENELAP

Carbon tetrachloride 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Chlorobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Chloroethane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP

Chloroform 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Chloromethane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP

cis-1,2-Dichloroethene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

cis-1,3-Dichloropropene 4/16/2010 1:26:00 PM3.3 µg/Kg-dry 1ND RWENELAP

Cyclohexanone 4/16/2010 1:26:00 PM81.5 µg/Kg-dry 1ND RWE

Dibromochloromethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Dibromomethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Dichlorodifluoromethane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP

Ethyl acetate 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP

Ethyl ether 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Ethyl methacrylate 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Ethylbenzene J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 11.1 RWENELAP

Heptane 4/16/2010 1:26:00 PM16.3 µg/Kg-dry 1ND RWE

Hexachlorobutadiene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Hexachloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Iodomethane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP

Isopropylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

m,p-Xylenes J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 12.7 RWENELAP

Methacrylonitrile 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP

Methyl Methacrylate 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Methyl tert-butyl ether 4/16/2010 1:26:00 PM1.6 µg/Kg-dry 1ND RWENELAP

Methylacrylate 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWE

Methylene chloride J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 10.9 RWENELAP

Naphthalene 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP

n-Butylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

n-Hexane J 4/16/2010 1:26:00 PM16.3 µg/Kg-dry 13.4 RWE

Nitrobenzene 4/16/2010 1:26:00 PM81.5 µg/Kg-dry 1ND RWENELAP

n-Propylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

o-Xylene J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 11.0 RWENELAP

Pentachloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

p-Isopropyltoluene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Propionitrile 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP

sec-Butylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-001






TEL: 618-344-1004

FAX: 618-344-1005

Sample NarrativeSW-846 3550B, 8151A, Chlorinated Herbicides by GC/ECD

Method blank show some PCP contamination, Result are below clients limits.SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS

Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.2,4-Dimethylphenol, 4-Nitrophenol, and 4-Chloro-3-methylphenol were outside upper QC limits in the LCS. Sample results are below reporting limit - data is reportable.2,4-Dimethylphenol was outside upper QC limits in the MS.

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSStyrene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

tert-Butylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Tetrachloroethene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Tetrahydrofuran 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP

Toluene J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 13.6 RWENELAP

trans-1,2-Dichloroethene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

trans-1,3-Dichloropropene 4/16/2010 1:26:00 PM3.3 µg/Kg-dry 1ND RWENELAP

Trichloroethene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Trichlorofluoromethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP

Vinyl acetate 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP

Vinyl chloride 4/16/2010 1:26:00 PM1.6 µg/Kg-dry 1ND RWENELAP

Surr: 1,2-Dichloroethane-d4 4/16/2010 1:26:00 PM72.2-131 %REC 198.5 RWE

Surr: 4-Bromofluorobenzene 4/16/2010 1:26:00 PM82.1-116 %REC 183.0 RWE

Surr: Dibromofluoromethane 4/16/2010 1:26:00 PM77.7-120 %REC 1101.7 RWE

Surr: Toluene-d8 4/16/2010 1:26:00 PM86-116 %REC 1115.7 RWE

SW-846 7471AMercury 4/16/20100.011 mg/Kg-dry 10.020 JMWNELAP

SW-846 9012A (TOTAL)Cyanide 4/20/20100.53 mg/Kg-dry 1< 0.53 MVSNELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-002

Client Sample ID: P4 Borrow #2





TEL: 618-344-1004

FAX: 618-344-1005

EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 4/15/2010 4:10:00 PM0.1 % 19.9 JMT

STANDARD METHODS 18TH ED. 2540 GTotal Solids 4/15/2010 4:10:00 PM0.1 % 190.1 JMT



Cadmium J 4/16/2010 1:49:54 PM0.19 mg/Kg-dry 10.12 LALNELAP



Silver 4/16/2010 1:49:54 PM0.52 mg/Kg-dry 10.54 LALNELAP

SW-846 3050B, METALS BY GFAASelenium 7740 S 4/16/2010 1:44:48 PM0.588 mg/Kg-dry 1< 0.588 MEKNELAP











Dieldrin 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 12.49 HENELAP








gamma-Chlordane 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP




Toxaphene 4/16/2010 12:04:00 PM32.9 µg/Kg-dry 1ND HENELAP






Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-002






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 4/16/2010 11:05:00 AM41.1 µg/Kg-dry 1ND HENELAP








Surr: Tetrachloro-meta-xylene 4/16/2010 11:05:00 AM7.35-123 %REC 160.7 HE

SW-846 3550B, 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

2,4,5-TP (Silvex) 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

2,4-D 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

2,4-DB 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

3,5-Dichlorobenzoic Acid 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

4-Nitrophenol 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

Bentazon 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

Chloramben 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

Dalapon 4/16/2010 5:08:00 PM158 µg/Kg-dry 1ND HE

DCPA 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

Dicamba 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

Dichlorprop 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

MCPA 4/16/2010 5:08:00 PM1580 µg/Kg-dry 1ND HE

MCPP 4/16/2010 5:08:00 PM1580 µg/Kg-dry 1ND HE

Pentachlorophenol 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

Picloram 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE

Surr: 2,4-Dichlorophenylacetic acid 4/16/2010 5:08:00 PM18.1-118 %REC 156.6 HE














Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-002






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSDibenzo(a,h)anthracene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP










SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP






2,4-Dichlorophenol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

2,4-Dimethylphenol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

2,4-Dinitrophenol 4/16/2010 10:32:00 AM1.11 mg/Kg-dry 1ND DMHNELAP



2-Chloronaphthalene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

2-Chlorophenol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

2-Methoxy-4-methylphenol 4/16/2010 10:32:00 AM0.720 mg/Kg-dry 1ND DMH

2-Methylnaphthalene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP



3,3´-Dichlorobenzidine 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP


4,6-Dinitro-2-methylphenol 4/16/2010 10:32:00 AM1.11 mg/Kg-dry 1ND DMHNELAP

4-Bromophenyl phenyl ether 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

4-Chloro-3-methylphenol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

4-Chloroaniline 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

4-Chlorophenyl phenyl ether 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP



Aniline 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-002






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAzobenzene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMH

Benzidine 4/16/2010 10:32:00 AM1.17 mg/Kg-dry 1see note DMHNELAP

Benzoic acid 4/16/2010 10:32:00 AM1.66 mg/Kg-dry 1ND DMHNELAP

Benzyl alcohol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

Bis(2-chloroethoxy)methane 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

Bis(2-chloroethyl)ether 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

Bis(2-chloroisopropyl)ether 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

Butyl benzyl phthalate 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

Carbazole 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMH

Dibenzofuran 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

Diethyl phthalate 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

Dimethyl phthalate 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

Di-n-butyl phthalate 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

Di-n-octyl phthalate 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

Hexachlorobenzene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

Hexachlorobutadiene 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

Hexachlorocyclopentadiene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

Hexachloroethane 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

Isophorone 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

m,p-Cresol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

Nitrobenzene 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

N-Nitrosodimethylamine 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

N-Nitroso-di-n-propylamine 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

N-Nitrosodiphenylamine 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

o-Cresol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

Pentachlorophenol 4/16/2010 10:32:00 AM2.22 mg/Kg-dry 1ND DMHNELAP

Phenol 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP

Pyridine 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP

1,2-Diphenylhydrazine 4/16/2010 10:32:00 AM0.931 mg/Kg-dry 1ND DMH

Surr: 2,4,6-Tribromophenol 4/16/2010 10:32:00 AM32.7-130 %REC 179.5 DMH

Surr: 2-Fluorobiphenyl 4/16/2010 10:32:00 AM34.1-116 %REC 170.0 DMH

Surr: 2-Fluorophenol 4/16/2010 10:32:00 AM30.5-99 %REC 166.7 DMH

Surr: Nitrobenzene-d5 4/16/2010 10:32:00 AM34.1-101 %REC 166.7 DMH

Surr: Phenol-d5 4/16/2010 10:32:00 AM34.9-110 %REC 169.9 DMH

Surr: p-Terphenyl-d14 4/16/2010 10:32:00 AM41.7-124 %REC 179.7 DMH






Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-002






TEL: 618-344-1004

FAX: 618-344-1005


1,1,2-Trichloro-1,2,2-trifluoroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWE


1,1-Dichloro-2-propanone 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWE


1,1-Dichloroethene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

1,1-Dichloropropene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP


1,2,3-Trichloropropane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP

1,2,3-Trimethylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 121.9 RWE


1,2,4-Trimethylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 123.5 RWENELAP

1,2-Dibromo-3-chloropropane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

1,2-Dibromoethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP




1,3,5-Trimethylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP




1-Chlorobutane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP


2-Butanone 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP


2-Hexanone 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP

2-Nitropropane 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP


4-Methyl-2-pentanone 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP

Acetone 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP

Acrolein 4/16/2010 1:54:00 PM97.4 µg/Kg-dry 1ND RWENELAP

Acrylonitrile 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP

Allyl chloride 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Benzene 4/16/2010 1:54:00 PM1.0 µg/Kg-dry 12.7 RWENELAP

Bromobenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Bromochloromethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Bromodichloromethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Bromoform 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-002






TEL: 618-344-1004

FAX: 618-344-1005

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSBromomethane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP

Carbon disulfide 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Carbon tetrachloride 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Chlorobenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Chloroethane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP

Chloroform 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Chloromethane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP

cis-1,2-Dichloroethene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

cis-1,3-Dichloropropene 4/16/2010 1:54:00 PM3.9 µg/Kg-dry 1ND RWENELAP

Cyclohexanone 4/16/2010 1:54:00 PM97.4 µg/Kg-dry 1ND RWE

Dibromochloromethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Dibromomethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Dichlorodifluoromethane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP

Ethyl acetate 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP

Ethyl ether 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Ethyl methacrylate 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Ethylbenzene J 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 11.6 RWENELAP

Heptane 4/16/2010 1:54:00 PM19.5 µg/Kg-dry 1ND RWE

Hexachlorobutadiene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Hexachloroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Iodomethane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP

Isopropylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

m,p-Xylenes J 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 14.2 RWENELAP

Methacrylonitrile 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP

Methyl Methacrylate 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Methyl tert-butyl ether 4/16/2010 1:54:00 PM1.9 µg/Kg-dry 1ND RWENELAP

Methylacrylate 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWE

Methylene chloride 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Naphthalene 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP

n-Butylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

n-Hexane J 4/16/2010 1:54:00 PM19.5 µg/Kg-dry 13.7 RWE

Nitrobenzene 4/16/2010 1:54:00 PM97.4 µg/Kg-dry 1ND RWENELAP

n-Propylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 19.3 RWENELAP

o-Xylene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 18.6 RWENELAP

Pentachloroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

p-Isopropyltoluene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Propionitrile 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP

sec-Butylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP




Matrix: SOLID



LABORATORY RESULTS

WorkOrder: 10040597

Lab ID: 10040597-002






TEL: 618-344-1004

FAX: 618-344-1005

Sample NarrativeSW-846 9012A (Total)

RPD was outside of QC limit.Matrix interference present in sample.

SW-846 3050B, Metals by GFAA

Se- Matrix interference present in sample.SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS

Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.2,4-Dimethylphenol, 4-Nitrophenol, and 4-Chloro-3-methylphenol were outside upper QC limits in the LCS. Sample results are below reporting limit - data is reportable.


Surrogate recovery was outside QC limits due to matrix interference.

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSStyrene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

tert-Butylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Tetrachloroethene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Tetrahydrofuran 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP

Toluene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 15.8 RWENELAP

trans-1,2-Dichloroethene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

trans-1,3-Dichloropropene 4/16/2010 1:54:00 PM3.9 µg/Kg-dry 1ND RWENELAP

Trichloroethene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Trichlorofluoromethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP

Vinyl acetate 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP

Vinyl chloride 4/16/2010 1:54:00 PM1.9 µg/Kg-dry 1ND RWENELAP

Surr: 1,2-Dichloroethane-d4 4/16/2010 1:54:00 PM72.2-131 %REC 1101.5 RWE

Surr: 4-Bromofluorobenzene S 4/16/2010 1:54:00 PM82.1-116 %REC 176.8 RWE

Surr: Dibromofluoromethane 4/16/2010 1:54:00 PM77.7-120 %REC 1104.4 RWE

Surr: Toluene-d8 S 4/16/2010 1:54:00 PM86-116 %REC 1124.9 RWE

SW-846 7471AMercury 4/16/20100.011 mg/Kg-dry 10.011 JMWNELAP

SW-846 9012A (TOTAL)Cyanide SR 4/20/20100.56 mg/Kg-dry 1< 0.56 MVSNELAP



Date/Time

DATES REPORT

Lab Order: 10040597


Test NamePrep

Date/Time




TEL: 618-344-1004

FAX: 618-344-1005

21-Apr-10Report Date:

10040597-001A P4-Borrow #1 4/14/2010 Solid SW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD

4/16/2010 10:51:00 AM

4/15/2010 6:43:00 PM


4/16/2010 10:47:00 AM

4/15/2010 6:43:00 PM

SW-846 3550B, 8151A, Chlorinated Herbicides by GC/ECD

4/16/2010 4:36:00 PM

4/15/2010 4:56:37 PM


4/19/2010 3:18:00 PM

4/15/2010 4:56:37 PM


4/16/2010 11:39:00 AM

4/15/2010 4:57:58 PM


4/16/2010 10:03:00 AM

4/15/2010 4:57:22 PM

10040597-001B EPA SW846 3550C, 5035A, ASTM D2974 4/15/2010 4:10:00 PM



4/16/2010 8:03:41 AM


4/16/2010 8:03:41 AM


4/16/2010 8:01:46 AM

SW-846 7471A 4/16/20104/16/2010 8:45:49 AM

SW-846 9012A (Total) 4/20/2010

10040597-001E SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS

4/16/2010 1:26:00 PM

10040597-002A P4 Borrow #2 SW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD

4/16/2010 12:04:00 PM

4/15/2010 6:43:00 PM


4/16/2010 11:05:00 AM

4/15/2010 6:43:00 PM


4/16/2010 5:08:00 PM

4/15/2010 4:56:37 PM


4/16/2010 1:24:00 PM

4/15/2010 4:57:58 PM


4/16/2010 10:32:00 AM

4/15/2010 4:57:22 PM

10040597-002B EPA SW846 3550C, 5035A, ASTM D2974 4/15/2010 4:10:00 PM



4/16/2010 8:03:41 AM



Date/Time

DATES REPORT

Lab Order: 10040597


Test NamePrep

Date/Time




TEL: 618-344-1004

FAX: 618-344-1005


10040597-002B P4 Borrow #2 4/14/2010 Solid SW-846 3050B, Metals by GFAA 4/16/2010 1:44:48 PM

4/16/2010 8:01:46 AM

SW-846 7471A 4/16/20104/16/2010 8:45:49 AM

SW-846 9012A (Total) 4/20/2010

10040597-002E SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS

4/16/2010 1:54:00 PM




Qualifiers






- Reporting Limit

- Dilution Factor







DF

RL

TNTC

Surr

IDPH

B

J

R

S

X NELAP

E

MI

H

ND





CCV

DF

DUP

ICV

LCS

MS

MSD

MDL

MB/LCB

PQL

RL

RPD



Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. (NELAC) The acceptable recovery range is listed in this report.

Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in this report.Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in this report.Method detection limit or limit of detection (LOD) means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.Method blank or lab control blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences are present at concentrations that impact the analytical results for sample analyses. (NELAC)Practical quantitation limit or limit of quantitation (LOQ) means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in this report.The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in this report.



Key QC concepts:

LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in this report.

Page 20 of 53




Lab Order: 10040597

ANALYTICAL QC SUMMARY REPORTTestCode: A_TCND_S_MT_9012A


Sample ID: MB-R134671


Prep Date:


Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134671

SeqNo: 2586402

MBLKSampType:

Cyanide 0.01< 0.01



Prep Date:


Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134671

SeqNo: 2586403

LCSSampType:

Cyanide 0.1000 96.9 85 1150.01 00.10



Prep Date:


Units: mg/Kg-dry

PQL

Client ID: P4 Borrow #2MS

RunNo: 134671

SeqNo: 2586406

MSSampType:

Cyanide 2.775 37.5 75 125 S0.56 01.04



Prep Date:


Units: mg/Kg-dry

PQL

Client ID: P4 Borrow #2MSD

RunNo: 134671

SeqNo: 2586407

MSDSampType:

Cyanide 2.775 59.0 75 125 15 SR0.56 0 1.042 44.41.64

Page 21 of 53




Lab Order: 10040597

ANALYTICAL QC SUMMARY REPORTTestCode: I_TS_M_MT




Prep Date:


Units: %

PQL

Client ID: ZZZZZZ

RunNo: 134542

SeqNo: 2581567

LCSSampType:

Total Solids 1.000 100 90 1100.1 01.0

Sample ID: 10040597-002BDUP


Prep Date:


Units: %

PQL

Client ID: P4 Borrow #2DUP

RunNo: 134542

SeqNo: 2581622

DUPSampType:

Total Solids 150.1 90.08 1.5688.7

Sample ID: LCSQC


Prep Date:


Units: %

PQL

Client ID: ZZZZZZ

RunNo: 134542

SeqNo: 2581625

LCSQCSampType:

Total Solids 1.000 100 90 1100.1 01.0

Page 22 of 53




Lab Order: 10040597

ANALYTICAL QC SUMMARY REPORTTestCode: M_HG_SOLID


Sample ID: MB-59794




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134501

SeqNo: 2580526

MBLKSampType:

SOP 3063

Mercury 0.01000 0 -100 1000.010 0< 0.010





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134501

SeqNo: 2580527

LCSSampType:

SOP 3063

Mercury 0.2500 105.6 85 1150.010 00.264





Units: mg/Kg-dry

PQL


RunNo: 134501

SeqNo: 2580532

MSSampType:

SOP 3063

Mercury 0.2708 107.8 75 1250.011 0.011370.303





Units: mg/Kg-dry

PQL


RunNo: 134501

SeqNo: 2580533

MSDSampType:

SOP 3063

Mercury 0.2708 103.8 75 125 150.011 0.01137 0.3033 3.640.292

Page 23 of 53




Lab Order: 10040597

ANALYTICAL QC SUMMARY REPORTTestCode: M_SOLID_GF


Sample ID: MB-59792




Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 134537

SeqNo: 2581516

MBLKSampType:

SOP 3042

Selenium 7740 0.6000 0 -100 1000.600 0< 0.600





Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 134537

SeqNo: 2581517

LCSSampType:

SOP 3042

Selenium 7740 3.000 83.8 80 1200.600 02.51





Units: mg/Kg-dry

PQL


RunNo: 134537

SeqNo: 2581520

MSSampType:

SOP 3042

Selenium 7740 2.941 38.4 70 130 JS1.18 01.1





Units: mg/Kg-dry

PQL


RunNo: 134537

SeqNo: 2581521

MSDSampType:

SOP 3042

Selenium 7740 2.941 38.8 70 130 20 JS1.18 0 1.130 01.1

Page 24 of 53




Lab Order: 10040597



Sample ID: MB-59793




Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 134503

SeqNo: 2581304

MBLKSampType:

SOP 3032

Arsenic 2.500 0 -100 1002.50 0< 2.50

Barium 0.5000 0 -100 1000.50 0< 0.50

Cadmium 0.2000 0 -100 1000.20 0< 0.20

Chromium 1.000 0 -100 1001.00 0< 1.00

Lead 4.000 0 -100 1004.00 0< 4.00

Silver 1.000 0 -100 1000.55 0< 0.55





Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 134503

SeqNo: 2581305

LCSSampType:

SOP 3032

Arsenic 200.0 109.8 85 1152.50 0220

Barium 200.0 105.0 85 1150.50 0210

Cadmium 5.000 106.4 85 1150.20 05.32

Chromium 20.00 113.4 85 1151.00 022.7

Lead 50.00 109.6 85 1154.00 054.8

Silver 5.000 108.2 85 1150.55 05.41





Units: mg/Kg-dry

PQL


RunNo: 134503

SeqNo: 2581309

MSSampType:

SOP 3032

Arsenic 188.7 100.8 75 1252.36 5.094195

Barium 188.7 87.7 75 1250.47 23.99190

Cadmium 4.717 88.8 75 1250.19 0.12264.31

Chromium 18.87 111.0 75 1250.94 16.8137.7

Lead 47.17 89.3 75 1253.77 11.5453.7

Silver 4.717 102.2 75 1250.52 0.53775.36

Page 25 of 53




Lab Order: 10040597







Units: mg/Kg-dry

PQL


RunNo: 134503

SeqNo: 2581408

MSDSampType:

SOP 3032

Arsenic 188.7 100.2 75 125 202.36 5.094 195.3 0.630194

Barium 188.7 85.0 75 125 200.47 23.99 189.5 2.72184

Cadmium 4.717 88.2 75 125 200.19 0.1226 4.311 0.6594.28

Chromium 18.87 100.7 75 125 200.94 16.81 37.75 5.2835.8

Lead 47.17 87.2 75 125 203.77 11.54 53.65 1.8652.7

Silver 4.717 102.6 75 125 200.52 0.5377 5.358 0.3515.38

Sample ID: MB-59793




Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 134602

SeqNo: 2583846

MBLKSampType:

SOP 3032

Chromium 1.000 58.0 -100 100 J1.00 00.58





Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 134602

SeqNo: 2583847

LCSSampType:

SOP 3032

Chromium 20.00 101.2 85 1151.00 020.2

Sample ID: MB-59793




Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 134602

SeqNo: 2584281

MBLKSampType:

SOP 3032

Lead 4.000 0 -100 1004.00 0< 4.00





Units: mg/Kg-dry

PQL

Client ID: ZZZZZZ

RunNo: 134602

SeqNo: 2584282

LCSSampType:

SOP 3032

Lead 50.00 101.2 85 1154.00 050.6

Page 26 of 53




Lab Order: 10040597



Sample ID: MB-59787




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134530

SeqNo: 2581259

MBLKSampType:

SW3550B

4,4´-DDD 1.67ND

4,4´-DDE 1.67ND

4,4´-DDT 1.67ND

Alachlor 1.67ND

Aldrin 1.67ND

alpha-BHC 1.67ND

alpha-Chlordane 1.67ND

beta-BHC 1.67ND

Chlordane 3.34ND

delta-BHC 1.67ND

Dieldrin 1.67ND

Endosulfan I 1.67ND

Endosulfan II 1.67ND

Endosulfan sulfate 1.67ND

Endrin 1.67ND

Endrin aldehyde 1.67ND

Endrin ketone 1.67ND

gamma-BHC 1.67ND

gamma-Chlordane 1.67ND

Heptachlor 1.67ND

Heptachlor epoxide 1.67ND

Methoxychlor 1.67ND

Toxaphene 30.0ND


Surr: Tetrachloro-m-xylene 8.330 67.2 14.4 1135.60





Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134530

SeqNo: 2581260

LCSSampType:

SW3550B

4,4´-DDD 8.330 96.7 36 2081.67 08.06

Page 27 of 53




Lab Order: 10040597







Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134530

SeqNo: 2581260

LCSSampType:

SW3550B

4,4´-DDE 8.330 94.1 26 1911.67 07.84

4,4´-DDT 8.330 102.8 3 2151.67 08.57

Alachlor 8.330 109.8 30 1701.67 09.14

Aldrin 8.330 84.8 46 1731.67 07.06

alpha-BHC 8.330 77.1 37 1791.67 06.43

alpha-Chlordane 8.330 102.1 38 1871.67 08.51

beta-BHC 8.330 97.9 51 1851.67 08.15

delta-BHC 8.330 95.2 46 1661.67 07.93

Dieldrin 8.330 93.2 26 2161.67 07.76

Endosulfan I 8.330 88.8 31 2051.67 07.39

Endosulfan II 8.330 97.5 42 1871.67 08.12


Endrin 8.330 99.0 30 2151.67 08.25

Endrin aldehyde 8.330 92.5 42 2021.67 07.70

Endrin ketone 8.330 102.9 19 2441.67 08.57

gamma-BHC 8.330 87.2 55 1661.67 07.26

gamma-Chlordane 8.330 92.8 23 1861.67 07.73

Heptachlor 8.330 86.7 43 1721.67 07.22


Methoxychlor 8.330 107.2 3 2211.67 08.93







Units: µg/Kg-dry

PQL

Client ID: P4-Borrow #1MS

RunNo: 134530

SeqNo: 2581262

MSSampType:

SW3550B

4,4´-DDD 9.251 91.8 36 2081.85 08.49

4,4´-DDE 9.251 83.8 26 1911.85 07.75

4,4´-DDT 9.251 95.5 3 2151.85 08.83

Alachlor 9.251 117.1 30 1701.85 010.8

Page 28 of 53




Lab Order: 10040597







Units: µg/Kg-dry

PQL


RunNo: 134530

SeqNo: 2581262

MSSampType:

SW3550B

Aldrin 9.251 79.3 46 1731.85 07.34

alpha-BHC 9.251 74.6 37 1791.85 06.90

alpha-Chlordane 9.251 89.4 38 1871.85 08.27

beta-BHC 9.251 86.6 51 1851.85 08.01

delta-BHC 9.251 83.6 46 1661.85 07.74

Dieldrin 9.251 73.9 26 2161.85 3.89010.7

Endosulfan I 9.251 83.0 31 2051.85 07.67

Endosulfan II 9.251 86.2 42 1871.85 07.98


Endrin 9.251 88.5 30 2151.85 08.18

Endrin aldehyde 9.251 82.0 42 2021.85 07.59

Endrin ketone 9.251 99.0 19 2441.85 09.16

gamma-BHC 9.251 82.6 55 1661.85 07.64

gamma-Chlordane 9.251 84.5 23 1861.85 07.82

Heptachlor 9.251 81.1 43 1721.85 07.51


Methoxychlor 9.251 93.5 3 2211.85 08.65







Units: µg/Kg-dry

PQL

Client ID: P4-Borrow #1MSD

RunNo: 134530

SeqNo: 2581263

MSDSampType:

SW3550B

4,4´-DDD 9.200 98.0 36 208 401.84 0 8.493 5.949.01

4,4´-DDE 9.200 90.0 26 191 401.84 0 7.753 6.598.28

4,4´-DDT 9.200 98.0 3 215 401.84 0 8.830 2.099.02

Alachlor 9.200 107.3 30 170 401.84 0 10.83 9.299.87

Aldrin 9.200 83.0 46 173 401.84 0 7.339 4.027.64

alpha-BHC 9.200 76.4 37 179 401.84 0 6.902 1.847.03

alpha-Chlordane 9.200 95.0 38 187 401.84 0 8.266 5.588.74

Page 29 of 53




Lab Order: 10040597







Units: µg/Kg-dry

PQL


RunNo: 134530

SeqNo: 2581263

MSDSampType:

SW3550B

beta-BHC 9.200 90.7 51 185 401.84 0 8.008 4.108.34

delta-BHC 9.200 89.1 46 166 401.84 0 7.738 5.798.20

Dieldrin 9.200 81.5 26 216 401.84 3.890 10.73 5.9711.4

Endosulfan I 9.200 87.1 31 205 401.84 0 7.674 4.288.01

Endosulfan II 9.200 90.4 42 187 401.84 0 7.977 4.168.32

Endosulfan sulfate 9.200 87.1 29 230 401.84 0 7.782 2.988.02

Endrin 9.200 92.8 30 215 401.84 0 8.183 4.298.54

Endrin aldehyde 9.200 85.7 42 202 401.84 0 7.587 3.877.89

Endrin ketone 9.200 102.7 19 244 401.84 0 9.159 3.149.45

gamma-BHC 9.200 85.1 55 166 401.84 0 7.638 2.447.83

gamma-Chlordane 9.200 90.0 23 186 401.84 0 7.816 5.798.28

Heptachlor 9.200 86.9 43 172 401.84 0 7.505 6.277.99

Heptachlor epoxide 9.200 93.0 39 204 401.84 0 8.246 3.738.56

Methoxychlor 9.200 97.0 3 221 401.84 0 8.648 3.128.92


Surr: Tetrachloro-m-xylene 9.200 71.2 19 145 4006.55

Page 30 of 53




Lab Order: 10040597



Sample ID: MB-59787




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134528

SeqNo: 2581179

MBLKSampType:

SW3550B

Aroclor 1016 37.5ND

Aroclor 1221 37.5ND

Aroclor 1232 37.5ND

Aroclor 1242 37.5ND

Aroclor 1248 37.5ND

Aroclor 1254 37.5ND

Aroclor 1260 37.5ND



Sample ID: LCSPCB-59787




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134528

SeqNo: 2581180

LCSSampType:

SW3550B

Aroclor 1016 166.7 107.7 54.9 12137.5 0180

Aroclor 1260 166.7 117.1 65.5 13337.5 0195







Units: µg/Kg-dry

PQL


RunNo: 134528

SeqNo: 2581183

MSSampType:

SW3550B

Aroclor 1016 185.0 88.7 35.8 14341.6 0164

Aroclor 1260 185.0 101.3 22.3 15241.6 0187


Surr: Tetrachloro-meta-xylene 9.211 66.0 7.35 1236.1

Page 31 of 53




Lab Order: 10040597







Units: µg/Kg-dry

PQL


RunNo: 134528

SeqNo: 2581184

MSDSampType:

SW3550B

Aroclor 1016 182.4 91.9 35.8 143 4041.0 0 164.1 2.09168

Aroclor 1260 182.4 100.9 22.3 152 4041.0 0 187.3 1.80184


Surr: Tetrachloro-meta-xylene 9.081 66.2 7.35 123 4006.0

Page 32 of 53




Lab Order: 10040597



Sample ID: MB-59782




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134530

SeqNo: 2583232

MBLKSampType:

SW8151A

2,4,5-T 10.0ND

2,4,5-TP (Silvex) 10.0ND

2,4-D 10.0ND

2,4-DB 10.0ND

3,5-Dichlorobenzoic Acid 10.0ND


Bentazon 10.0ND

Chloramben 10.0ND

Dalapon 100ND

DCPA 10.0ND

Dicamba 10.0ND

Dichlorprop 10.0ND

MCPA 1000ND

MCPP 1000ND


Picloram 10.0ND

Surr: 2,4-Dichlorophenylacetic acid 13.33 60.0 18.1 1187.99





Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134530

SeqNo: 2583233

LCSSampType:

SW8151A

2,4,5-T 13.33 66.1 34.9 160 J10.0 08.8

2,4,5-TP (Silvex) 13.33 73.8 30.2 161 J10.0 09.8

2,4-D 13.33 71.5 27.4 139 J10.0 09.5

2,4-DB 13.33 68.7 13.6 174 J10.0 09.2

3,5-Dichlorobenzoic Acid 13.33 56.4 18.4 146 J10.0 07.5

4-Nitrophenol 13.33 62.5 18.6 153 J10.0 08.3

Bentazon 13.33 103.7 29.2 15710.0 013.8

Chloramben 13.33 50.3 10.6 130 J10.0 06.7

Dalapon 133.3 19.6 5 56.4 J100 026

Page 33 of 53




Lab Order: 10040597







Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134530

SeqNo: 2583233

LCSSampType:

SW8151A

DCPA 13.33 68.3 10 171 J10.0 09.1

Dicamba 13.33 54.9 23.4 136 J10.0 07.3

Dichlorprop 13.33 80.6 19.5 14110.0 010.7

MCPA 1333 88.6 9.86 1811000 01180

MCPP 1333 63.9 4.61 171 J1000 0850

Pentachlorophenol 13.33 39.9 29.7 128 J10.0 05.3

Picloram 13.33 107.1 33.3 13810.0 014.3


Sample ID: LCSD-59782




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134530

SeqNo: 2583234

LCSDSampType:

SW8151A

2,4,5-T 13.33 70.1 34.9 160 30 J10.0 0 8.818 09.3

2,4,5-TP (Silvex) 13.33 79.9 30.2 161 3010.0 0 9.838 7.9410.7

2,4-D 13.33 77.6 27.4 139 3010.0 0 9.539 8.0710.3

2,4-DB 13.33 79.6 13.6 174 3010.0 0 9.158 14.710.6

3,5-Dichlorobenzoic Acid 13.33 56.5 18.4 146 30 J10.0 0 7.522 07.5

4-Nitrophenol 13.33 69.7 18.6 153 30 J10.0 0 8.333 09.3

Bentazon 13.33 85.2 29.2 157 3010.0 0 13.83 19.711.4

Chloramben 13.33 55.4 10.6 130 30 J10.0 0 6.707 07.4

Dalapon 133.3 22.3 5 56.4 30 J100 0 26.15 030

DCPA 13.33 77.7 10 171 3010.0 0 9.112 12.810.4

Dicamba 13.33 60.6 23.4 136 30 J10.0 0 7.324 08.1

Dichlorprop 13.33 79.6 19.5 141 3010.0 0 10.74 1.1910.6

MCPA 1333 99.7 9.86 181 301000 0 1182 11.71330

MCPP 1333 63.6 4.61 171 30 J1000 0 851.6 0850

Pentachlorophenol 13.33 45.3 29.7 128 30 J10.0 0 5.325 06.0

Picloram 13.33 113.7 33.3 138 3010.0 0 14.28 5.9515.2

Surr: 2,4-Dichlorophenylacetic acid 13.33 53.6 18.1 118 3007.15

Page 34 of 53




Lab Order: 10040597







Units: µg/Kg-dry

PQL


RunNo: 134530

SeqNo: 2583237

MSSampType:

SW8151A

2,4,5-T 43.07 64.9 34.9 16016.2 027.9

2,4,5-TP (Silvex) 43.07 73.6 30.2 16116.2 031.7

2,4-D 43.07 71.2 27.4 13916.2 030.7

2,4-DB 43.07 82.2 13.6 17416.2 035.4

3,5-Dichlorobenzoic Acid 43.07 45.9 18.4 14616.2 019.8

Bentazon 43.07 57.1 29.2 15716.2 024.6

Chloramben 43.07 44.3 10.6 13016.2 019.1

Dalapon 430.7 20.7 5 56.4 J162 089

DCPA 43.07 72.1 10 17116.2 031.1

Dicamba 43.07 57.1 23.4 13616.2 024.6

Dichlorprop 43.07 73.8 19.5 14116.2 031.8

MCPA 4307 102.5 9.86 1811620 04410

MCPP 4307 57.6 4.61 1711620 02480

Picloram 43.07 102.7 33.3 13816.2 044.2






Units: µg/Kg-dry

PQL


RunNo: 134530

SeqNo: 2583238

MSDSampType:

SW8151A

2,4,5-T 42.45 57.3 34.9 160 015.9 0 27.94 13.824.3

2,4,5-TP (Silvex) 42.45 63.8 30.2 161 015.9 0 31.71 15.827.1

2,4-D 42.45 59.0 27.4 139 015.9 0 30.67 20.225.0

2,4-DB 42.45 78.9 13.6 174 015.9 0 35.40 5.5433.5

3,5-Dichlorobenzoic Acid 42.45 42.7 18.4 146 015.9 0 19.77 8.8118.1

Bentazon 42.45 45.1 29.2 157 015.9 0 24.61 24.919.2

Chloramben 42.45 44.1 10.6 130 015.9 0 19.10 2.0418.7

Dalapon 424.5 18.2 5 56.4 0 J159 0 89.34 077

DCPA 42.45 46.3 10 171 015.9 0 31.06 45.019.7

Dicamba 42.45 52.5 23.4 136 015.9 0 24.61 9.9822.3

Dichlorprop 42.45 51.3 19.5 141 015.9 0 31.78 37.421.8

Page 35 of 53




Lab Order: 10040597







Units: µg/Kg-dry

PQL


RunNo: 134530

SeqNo: 2583238

MSDSampType:

SW8151A

MCPA 4245 117.2 9.86 181 01590 0 4415 11.94980

MCPP 4245 57.2 4.61 171 01590 0 2483 2.142430

Picloram 42.45 92.2 33.3 138 015.9 0 44.23 12.239.1

Surr: 2,4-Dichlorophenylacetic acid 42.45 42.1 18.1 118 0017.9

Page 36 of 53




Lab Order: 10040597



Sample ID: MB-59753




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134531

SeqNo: 2581283

MBLKSampType:

SW3550B







2,4-Dichlorophenol 0.500ND

2,4-Dimethylphenol 0.500ND

2,4-Dinitrophenol 1.00ND



2-Chloronaphthalene 0.350ND

2-Chlorophenol 0.500ND

2-Methoxy-4-methylphenol 0.650ND




3,3´-Dichlorobenzidine 0.350ND


4,6-Dinitro-2-methylphenol 1.00ND

4-Bromophenyl phenyl ether 0.350ND

4-Chloro-3-methylphenol 0.500ND

4-Chloroaniline 0.500ND

4-Chlorophenyl phenyl ether 0.350ND





Aniline 0.500ND

Anthracene 0.350ND

Azobenzene 0.350ND

Page 37 of 53




Lab Order: 10040597



Sample ID: MB-59753




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134531

SeqNo: 2581283

MBLKSampType:

SW3550B

Benzidine 1.06ND






Benzoic acid 1.50ND

Benzyl alcohol 0.500ND

Bis(2-chloroethoxy)methane 0.350ND

Bis(2-chloroethyl)ether 0.500ND

Bis(2-chloroisopropyl)ether 0.350ND


Butyl benzyl phthalate 0.350ND

Carbazole 0.500ND

Chrysene 0.350ND


Dibenzofuran 0.350ND


Dimethyl phthalate 0.350ND


Di-n-octyl phthalate 0.350ND


Fluorene 0.350ND

Hexachlorobenzene 0.350ND


Hexachlorocyclopentadiene 0.350ND



Isophorone 0.350ND

m,p-Cresol 0.500ND

Naphthalene 0.350ND

Page 38 of 53




Lab Order: 10040597



Sample ID: MB-59753




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134531

SeqNo: 2581283

MBLKSampType:

SW3550B

Nitrobenzene 0.500ND

N-Nitrosodimethylamine 0.500ND

N-Nitroso-di-n-propylamine 0.500ND

N-Nitrosodiphenylamine 0.500ND

o-Cresol 0.500ND



Phenol 0.350ND

Pyrene 0.500ND

Pyridine 0.500ND

1,2-Diphenylhydrazine 0.840ND





Surr: Phenol-d5 1.670 76.8 55.9 98.51.28






Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134531

SeqNo: 2581284

LCSSampType:

SW3550B

1,2,4-Trichlorobenzene 1.670 78.7 43.9 92.20.500 01.31




2,4-Dimethylphenol 3.330 97.0 38.3 88 S0.500 03.23

2,4-Dinitrophenol 3.330 84.5 1.88 1621.00 02.81

2,4-Dinitrotoluene 1.670 72.2 48.6 1020.350 01.21

2-Chlorophenol 3.330 81.7 46.6 840.500 02.72

4-Chloro-3-methylphenol 3.330 99.1 51.5 94.9 S0.500 03.30

Page 39 of 53




Lab Order: 10040597







Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134531

SeqNo: 2581284

LCSSampType:

SW3550B

4-Nitrophenol 3.330 105.9 53.2 104 S0.350 03.53

Acenaphthene 1.670 78.9 50.8 1130.350 01.32

Acenaphthylene 1.670 83.5 52.8 1210.350 01.39

Anthracene 1.670 77.9 53.3 1150.350 01.30


Benzo(a)pyrene 1.670 82.8 58.2 1090.350 01.38




Bis(2-ethylhexyl)phthalate 1.670 84.5 56.3 1090.350 01.41

Chrysene 1.670 84.9 58.4 1150.350 01.42





Fluoranthene 1.670 87.3 61.6 1130.350 01.46

Fluorene 1.670 74.7 52.2 1160.350 01.25




Indeno(1,2,3-cd)pyrene 1.670 100.3 52.7 1150.350 01.68

m,p-Cresol 1.670 86.1 37.6 93.70.500 01.44

Naphthalene 1.670 73.9 45.7 1010.350 01.23

Nitrobenzene 3.330 78.0 51.8 1040.500 02.60


o-Cresol 1.670 73.3 43 1010.500 01.22


Phenanthrene 1.670 83.1 52.9 1130.350 01.39

Phenol 3.330 77.3 41.6 81.30.350 02.57

Pyrene 1.670 83.6 60.7 1150.500 01.40

Pyridine 3.330 45.7 3.61 74.30.500 01.52

Page 40 of 53




Lab Order: 10040597







Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134531

SeqNo: 2581284

LCSSampType:

SW3550B





Surr: Phenol-d5 1.670 80.0 55.9 98.51.34






Units: mg/Kg-dry

PQL


RunNo: 134531

SeqNo: 2581287

MSSampType:

SW3550B

1,2,4-Trichlorobenzene 1.885 74.3 35.9 1020.564 01.40




2,4-Dimethylphenol 3.759 97.2 38.3 88 S0.564 03.65

2,4-Dinitrophenol 3.759 54.1 1.88 1621.13 02.03

2,4-Dinitrotoluene 1.885 73.3 37.5 1070.395 01.38

2-Chlorophenol 3.759 81.0 22.6 1080.564 03.04

4-Chloro-3-methylphenol 3.759 96.8 19.3 1310.564 03.64

4-Nitrophenol 3.759 95.3 27.6 1230.395 03.58





Hexachlorocyclopentadiene 0 0 0 00.395 0ND


m,p-Cresol 1.885 86.4 37.6 93.70.564 01.63

Nitrobenzene 3.759 75.3 51.8 1040.564 02.83


o-Cresol 1.885 75.8 43 1010.564 01.43

Page 41 of 53




Lab Order: 10040597







Units: mg/Kg-dry

PQL


RunNo: 134531

SeqNo: 2581287

MSSampType:

SW3550B


Phenol 3.759 77.1 20.8 1100.395 02.90

Pyridine 3.759 61.1 3.61 74.30.564 02.30





Surr: Phenol-d5 1.885 75.7 34.9 1101.43






Units: mg/Kg-dry

PQL


RunNo: 134531

SeqNo: 2581288

MSDSampType:

SW3550B

1,2,4-Trichlorobenzene 1.870 79.6 35.9 102 400.560 0 1.401 6.011.49

1,4-Dichlorobenzene 1.870 66.8 29.8 95.5 400.560 0 1.184 5.291.25



2,4-Dimethylphenol 3.729 104.2 38.3 88 40 S0.560 0 3.653 6.133.88

2,4-Dinitrophenol 3.729 58.1 1.88 162 401.12 0 2.032 6.392.17

2,4-Dinitrotoluene 1.870 74.6 37.5 107 400.392 0 1.382 1.011.40

2-Chlorophenol 3.729 83.6 22.6 108 400.560 0 3.043 2.433.12

4-Chloro-3-methylphenol 3.729 94.7 19.3 131 400.560 0 3.639 3.033.53

4-Nitrophenol 3.729 98.4 27.6 123 400.392 0 3.583 2.383.67

Diethyl phthalate 3.729 90.1 51.7 106 400.560 0 3.471 3.223.36

Dimethyl phthalate 3.729 91.2 58.8 104 400.392 0 3.504 2.953.40

Di-n-butyl phthalate 1.870 95.7 54.3 105 400.392 0 1.567 13.31.79

Hexachlorobutadiene 3.729 84.3 35.7 100 400.560 0 3.025 3.803.14

Hexachlorocyclopentadiene 0 0 0 0 00.392 0 0 0ND

Hexachloroethane 3.729 79.2 38.9 89.9 400.560 0 2.898 1.902.95

m,p-Cresol 1.870 89.8 37.6 93.7 400.560 0 1.628 3.051.68

Page 42 of 53




Lab Order: 10040597







Units: mg/Kg-dry

PQL


RunNo: 134531

SeqNo: 2581288

MSDSampType:

SW3550B

Nitrobenzene 3.729 80.9 51.8 104 400.560 0 2.829 6.483.02

N-Nitroso-di-n-propylamine 1.870 86.4 45.5 99.1 400.560 0 1.615 0.05301.62

o-Cresol 1.870 75.6 43 101 400.560 0 1.430 1.141.41

Pentachlorophenol 3.729 77.6 18.5 113 402.24 0 2.725 6.082.90

Phenol 3.729 76.9 20.8 110 400.392 0 2.900 1.132.87

Pyridine 3.729 57.3 3.61 74.3 400.560 0 2.298 7.352.14

Surr: 2,4,6-Tribromophenol 1.870 67.5 32.7 130 4001.26

Surr: 2-Fluorobiphenyl 0.9350 59.8 34.1 116 4000.560

Surr: 2-Fluorophenol 1.870 65.3 30.5 99 4001.22

Surr: Nitrobenzene-d5 0.9350 66.1 34.1 101 4000.618

Surr: Phenol-d5 1.870 71.1 34.9 110 4001.33


Page 43 of 53




Lab Order: 10040597



Sample ID: MB-59754




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134462

SeqNo: 2580336

MBLKSampType:

SW3550B




Anthracene 0.003ND







Chrysene 0.003ND



Dimethyl phthalate J0.0340.014



Fluorene 0.003ND


m,p-Cresol 0.010ND

Naphthalene 0.003ND

o-Cresol 0.003ND


Pyrene 0.003ND


Surr: 2-Fluorophenol 1.670 53.3 23 1170.890


Surr: Phenol-d5 1.670 60.6 33.2 1251.01


Page 44 of 53




Lab Order: 10040597







Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134462

SeqNo: 2580337

LCSSampType:

SW3550B

2-Methylnaphthalene 0.1670 69.1 50 1500.003 00.115

Acenaphthene 0.1670 74.3 56.3 1150.003 00.124

Acenaphthylene 0.1670 69.3 60.3 1430.003 00.116

Anthracene 0.1670 73.7 52.1 1090.003 00.123


Benzo(a)pyrene 0.1670 74.6 40.8 1270.003 00.125





Chrysene 0.1670 77.4 60.8 1280.003 00.129


Diethyl phthalate 0.1670 79.2 50 1500.034 00.132

Dimethyl phthalate 0.1670 95.0 50 1500.034 00.159

Di-n-butyl phthalate 0.1670 89.7 50 1500.034 00.150

Fluoranthene 0.1670 80.4 58.7 1250.003 00.134

Fluorene 0.1670 73.6 57.8 1250.003 00.123

Indeno(1,2,3-cd)pyrene 0.1670 78.3 52 1470.003 00.131

m,p-Cresol 0.1670 75.6 50 1500.010 00.126

Naphthalene 0.1670 64.8 54.8 1130.003 00.108

o-Cresol 0.1670 74.6 50 1500.003 00.125

Phenanthrene 0.1670 72.5 60.4 1210.003 00.121

Pyrene 0.1670 80.9 57.9 1290.003 00.135




Surr: Phenol-d5 1.670 84.7 33.7 1291.41


Page 45 of 53




Lab Order: 10040597







Units: mg/Kg-dry

PQL


RunNo: 134536

SeqNo: 2581316

MSSampType:

SW3550B

Acenaphthene 0.1896 74.5 36 1350.004 00.141

Acenaphthylene 0.1896 70.2 17.2 1670.004 00.133

Anthracene 0.1896 74.7 39.3 1240.004 0.0049080.147

Benzo(a)anthracene 0.1896 61.4 10 1830.004 0.015280.132

Benzo(a)pyrene 0.1896 74.9 10 2040.004 0.013160.155

Benzo(b)fluoranthene 0.1896 74.4 10.6 1780.004 0.019520.161

Benzo(g,h,i)perylene 0.1896 73.1 10 1680.004 0.010110.149

Benzo(k)fluoranthene 0.1896 76.6 27.6 1810.004 0.0070640.152


Chrysene 0.1896 70.9 10 1760.004 0.017990.152


Fluoranthene 0.1896 60.9 10 2270.004 0.046100.162

Fluorene 0.1896 71.8 35.2 1480.004 00.136

Indeno(1,2,3-cd)pyrene 0.1896 75.2 10 1640.004 0.0076960.150

Naphthalene 0.1896 64.8 14.7 1280.004 00.123

Phenanthrene 0.1896 61.0 32.8 1430.004 0.029560.145

Pyrene 0.1896 68.0 10 1800.004 0.036170.165








Units: mg/Kg-dry

PQL


RunNo: 134536

SeqNo: 2581317

MSDSampType:

SW3550B

Acenaphthene 0.1860 78.5 36 135 49.70.004 0 0.1413 3.340.146

Acenaphthylene 0.1860 74.4 17.2 167 33.30.004 0 0.1331 3.980.138

Anthracene 0.1860 78.0 39.3 124 51.10.004 0.004908 0.1466 2.270.150

Benzo(a)anthracene 0.1860 62.9 10 183 40.60.004 0.01528 0.1317 0.4560.132

Benzo(a)pyrene 0.1860 77.5 10 204 56.40.004 0.01316 0.1552 1.310.157

Benzo(b)fluoranthene 0.1860 77.7 10.6 178 49.70.004 0.01952 0.1606 2.180.164

Page 46 of 53




Lab Order: 10040597







Units: mg/Kg-dry

PQL


RunNo: 134536

SeqNo: 2581317

MSDSampType:

SW3550B

Benzo(g,h,i)perylene 0.1860 67.2 10 168 36.50.004 0.01011 0.1488 9.590.135

Benzo(k)fluoranthene 0.1860 80.6 27.6 181 42.60.004 0.007064 0.1523 2.970.157

Bis(2-ethylhexyl)phthalate 0.1860 96.7 50 150 60.30.075 0 0.1769 1.660.180

Chrysene 0.1860 71.6 10 176 45.10.004 0.01799 0.1524 0.8690.151

Dibenzo(a,h)anthracene 0.1860 74.8 12.2 156 39.90.004 0 0.1448 4.020.139

Fluoranthene 0.1860 66.1 10 227 66.20.004 0.04610 0.1616 4.530.169

Fluorene 0.1860 77.2 35.2 148 65.60.004 0 0.1362 5.310.144

Indeno(1,2,3-cd)pyrene 0.1860 72.3 10 164 36.50.004 0.007696 0.1504 5.650.142

Naphthalene 0.1860 69.0 14.7 128 39.60.004 0 0.1228 4.400.128

Phenanthrene 0.1860 66.9 32.8 143 35.40.004 0.02956 0.1452 5.840.154

Pyrene 0.1860 75.1 10 180 60.10.004 0.03617 0.1650 6.380.176




Page 47 of 53




Lab Order: 10040597



Sample ID: LCS-G100416-1




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134558

SeqNo: 2582007

LCSSampType:

SW5035

1,1,1-Trichloroethane 50.00 100 85.6 1245.0 050.0

1,1-Dichloroethene 50.00 80.6 60.1 1315.0 040.3

1,2-Dibromoethane 50.00 95.3 86.9 1195.0 047.7

1,2-Dichlorobenzene 50.00 97.0 88 1195.0 048.5

1,2-Dichloroethane 50.00 89.2 73 1175.0 044.6



2-Butanone 100.0 55.9 45.3 13650.0 055.9

Benzene 50.00 88.0 73.9 1091.0 044.0

Bromodichloromethane 50.00 101.6 91.3 1265.0 050.8

Carbon tetrachloride 50.00 100.1 83.3 1275.0 050.0

Chlorobenzene 50.00 97.8 85.8 1165.0 048.9

Chloroform 50.00 94.6 80 1135.0 047.3

Dibromochloromethane 50.00 90.7 89.1 1195.0 045.4

Ethylbenzene 50.00 97.0 84.1 1155.0 048.5

m,p-Xylenes 50.00 94.9 79.1 1115.0 047.5

Methyl tert-butyl ether 50.00 97.7 80 1282.0 048.8

Methylene chloride 50.00 88.1 73.9 1165.0 044.0

Naphthalene 50.00 80.2 73.1 13510 040.1

o-Xylene 50.00 93.7 82 1175.0 046.8

Tetrachloroethene 50.00 88.9 74.6 1155.0 044.5

Toluene 50.00 88.8 79.1 1125.0 044.4

Trichloroethene 50.00 92.5 81 1115.0 046.2

Surr: 1,2-Dichloroethane-d4 50.00 95.3 72.2 13147.6



Surr: Toluene-d8 50.00 99.1 86 11649.6

Page 48 of 53




Lab Order: 10040597



Sample ID: LCSD-G100416-1




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134558

SeqNo: 2582008

LCSDSampType:

SW5035

1,1,1-Trichloroethane 50.00 100.4 85.6 124 205.0 0 50.01 0.39950.2

1,1-Dichloroethene 50.00 80.2 60.1 131 205.0 0 40.32 0.57240.1

1,2-Dibromoethane 50.00 100.6 86.9 119 205.0 0 47.66 5.3550.3

1,2-Dichlorobenzene 50.00 98.3 88 119 205.0 0 48.51 1.3549.2

1,2-Dichloroethane 50.00 91.1 73 117 205.0 0 44.58 2.1145.5



2-Butanone 100.0 61.5 45.3 136 2050.0 0 55.88 9.5661.5

Benzene 50.00 88.4 73.9 109 201.0 0 44.01 0.40844.2

Bromodichloromethane 50.00 103.4 91.3 126 205.0 0 50.82 1.6851.7

Carbon tetrachloride 50.00 99.2 83.3 127 205.0 0 50.05 0.86349.6

Chlorobenzene 50.00 97.8 85.8 116 205.0 0 48.91 048.9

Chloroform 50.00 95.0 80 113 205.0 0 47.30 0.44347.5

Dibromochloromethane 50.00 92.7 89.1 119 205.0 0 45.37 2.1846.4

Ethylbenzene 50.00 96.4 84.1 115 205.0 0 48.51 0.60048.2

m,p-Xylenes 50.00 93.5 79.1 111 205.0 0 47.46 1.5346.7

Methyl tert-butyl ether 50.00 102.6 80 128 202.0 0 48.84 4.8951.3

Methylene chloride 50.00 89.2 73.9 116 205.0 0 44.04 1.2644.6

Naphthalene 50.00 86.7 73.1 135 2010 0 40.10 7.8143.4

o-Xylene 50.00 93.0 82 117 205.0 0 46.85 0.75046.5

Tetrachloroethene 50.00 89.1 74.6 115 205.0 0 44.47 0.20244.6

Toluene 50.00 88.4 79.1 112 205.0 0 44.41 0.45144.2

Trichloroethene 50.00 92.5 81 111 205.0 0 46.24 046.2

Surr: 1,2-Dichloroethane-d4 50.00 96.8 72.2 131 0048.4



Surr: Toluene-d8 50.00 98.9 86 116 0049.4

Page 49 of 53




Lab Order: 10040597







Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134558

SeqNo: 2582009

MBLKSampType:

SW5035




1,1,2-Trichloro-1,2,2-trifluoroethane 5.0ND


1,1-Dichloro-2-propanone 50.0ND


1,1-Dichloroethene 5.0ND

1,1-Dichloropropene 5.0ND


1,2,3-Trichloropropane 10ND




1,2-Dibromo-3-chloropropane 5.0ND

1,2-Dibromoethane 5.0ND








1-Chlorobutane 5.0ND


2-Butanone 50.0ND


2-Hexanone 50.0ND

2-Nitropropane 50.0ND


4-Methyl-2-pentanone 50.0ND

Page 50 of 53




Lab Order: 10040597







Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134558

SeqNo: 2582009

MBLKSampType:

SW5035

Acetone 50.0ND

Acrolein 100ND

Acrylonitrile 10ND

Allyl chloride 5.0ND

Benzene 1.0ND

Bromobenzene 5.0ND

Bromochloromethane 5.0ND

Bromodichloromethane 5.0ND

Bromoform 5.0ND

Bromomethane 10ND

Carbon disulfide 5.0ND

Carbon tetrachloride 5.0ND

Chlorobenzene 5.0ND

Chloroethane 10ND

Chloroform 5.0ND

Chloromethane 10ND

cis-1,2-Dichloroethene 5.0ND

cis-1,3-Dichloropropene 4.0ND

Cyclohexanone 100ND

Dibromochloromethane 5.0ND

Dibromomethane 5.0ND

Dichlorodifluoromethane 10ND

Ethyl acetate 50.0ND

Ethyl ether 5.0ND

Ethyl methacrylate 5.0ND

Ethylbenzene 5.0ND

Heptane 20.0ND



Iodomethane 10ND

Isopropylbenzene 5.0ND

Page 51 of 53




Lab Order: 10040597







Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134558

SeqNo: 2582009

MBLKSampType:

SW5035

m,p-Xylenes 5.0ND

Methacrylonitrile 50.0ND

Methyl Methacrylate 5.0ND

Methyl tert-butyl ether 2.0ND

Methylacrylate 10ND

Methylene chloride 5.0ND

Naphthalene 10ND

n-Butylbenzene 5.0ND

n-Hexane 20.0ND

Nitrobenzene 100ND

n-Propylbenzene 5.0ND

o-Xylene 5.0ND

Pentachloroethane 5.0ND

p-Isopropyltoluene 5.0ND

Propionitrile 50.0ND

sec-Butylbenzene 5.0ND

Styrene 5.0ND

tert-Butylbenzene 5.0ND

Tetrachloroethene 5.0ND

Tetrahydrofuran 50.0ND

Toluene 5.0ND

trans-1,2-Dichloroethene 5.0ND

trans-1,3-Dichloropropene 4.0ND

Trichloroethene 5.0ND

Trichlorofluoromethane 5.0ND

Vinyl acetate 50.0ND

Vinyl chloride 2.0ND

Surr: 1,2-Dichloroethane-d4 50.00 96.2 72.2 13148.1



Surr: Toluene-d8 50.00 98.4 86 11649.2

Page 52 of 53



Lab Order: 10040597






TEL: 618-344-1004

FAX: 618-344-1005

Received By: MLDCarrier: Susan Duffe


On:

15-Apr-10

On:

15-Apr-10










Temp °C 1.4



Water - VOA vials have zero headspace? Yes No No VOA vials





Pages to follow:

Water - TOX containers have zero headspace? Yes No No TOX containers

Marvin L. Darling Heather A. White


http://www.teklabinc.com/

July 14, 2011

WorkOrder: 11070042A831-735002-012901-225Ameren Champaign 62409080120

RE:

Dear Pete Sazama:


Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column.

All tests are performed in the Collinsville, IL laboratory unless otherwise noted in the Case Narrative.



Sincerely,


(618) 281-7173(618) 281-5120

TEL:FAX:


Heather A. WhiteProject Manager(618)344-1004 ex [email protected]

Page 1 of 58


This reporting package includes the following:

Report Contents

Client Project: A831-735002-012901-225Ameren Champaign 62409080120


Report Date: 14-Jul-11

Work Order: 11070042


Cover Letter 1

Report Contents 2

Definitions 3

Case Narrative 4

Laboratory Results 5

Sample Summary 35

Dates Report 36

Quality Control Results 39

Receiving Check List 58

Chain of Custody Appended

Page 2 of 58


____TeklabHdrP

Definitions






Abbr DefinitionCCV Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.

DF Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilutions factors.

DNI Did not ignite

DUP Laboratory duplicate is an aliquot of a sample taken from the same container under laboratory conditions for independent processing and analysis independently of the original aliquot.

ICV Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.

IDPH IL Dept. of Public Health

LCS Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. The acceptable recovery range is in the QC Package (provided upon request).

LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).

MB Method blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences should present at concentrations that impact the analytical results for sample analyses.

MDL Method detection limit means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.

MS Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in the QC Package (provided upon request).

MSD Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).

MW Molecular weight

ND Not Detected at the Reporting Limit

NELAP NELAP Accredited

PQL Practical quantitation limit means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in the QC Package (provided upon request).

RL The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.

RPD Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in the QC Package (provided upon request).

SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes.

Surr Surrogates are compounds which are similar to the analytes of interest in chemical composition and behavior in the analytical process, but which are not normally found in environmental samples.

TNTC Too numerous to count ( > 200 CFU )

Qualifiers# - Unknown hydrocarbon B - Analyte detected in associated Method Blank

E - Value above quantitation range H - Holding times exceeded

M - Manual Integration used to determine area response ND - Not Detected at the Reporting Limit

R - RPD outside accepted recovery limits S - Spike Recovery outside recovery limits

X - Value exceeds Maximum Contaminant Level

Page 3 of 58


AbbrDefinition

CCVContinuing

Case Narrative







Herbicide analysis performed by Keystone Laboratories, Inc. See attached report for QC data.

NELAPState Cert # Exp Date LabDept

Locations and Accreditations

____________________________________Collinsville

Address 5445 Horseshoe Lake Road

Collinsville, IL 62234-7425

Phone (618) 344-1004

Fax (618) 344-1005

Email [email protected]

____________________________________Springfield

Address 3920 Pintail Dr

Springfield, IL 62711-9415

Phone (217) 698-1004

Fax (217) 698-1005


____________________________________Kansas City

Address 8421 Nieman Road

Lenexa, KS 66214

Phone (913) 541-1998

Fax (913) 541-1998


Illinois 100226 1/31/2012 CollinsvilleNELAPIEPA

Kansas E-10374 1/31/2012 CollinsvilleNELAPKDHE

Louisiana 166493 6/30/2012 CollinsvilleNELAPLDEQ

Louisiana 166578 6/30/2012 SpringfieldNELAPLDEQ

Arkansas 88-0966 3/14/2012 CollinsvilleADEQ

Illinois 17584 4/30/2012 CollinsvilleIDPH

Kentucky 0073 5/26/2012 CollinsvilleUST

Missouri 00930 4/13/2013 CollinsvilleMDNR

Oklahoma 9978 8/31/2011 CollinsvilleODEQ

Page 4 of 58


TeklabHdrP

Laboratory Results






Analyses Result Units Date AnalyzedRL DFCertification Qual

Collection Date: 06/29/2011 16:00

Lab ID: 11070042-001 Client Sample ID: SBA-C3-01 (5-6)

Matrix: SOLID

Batch

EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/01/2011 16:000.1 % 120.6 R151546

STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/01/2011 16:000.1 % 179.4 R151526

SW-846 9012A (TOTAL)Cyanide 07/02/2011 12:170.63 mg/Kg-dry 1< 0.63NELAP R151533

SW-846 3050B, 6010B, METALS BY ICPArsenic 07/05/2011 12:252.50 mg/Kg-dry 111.3NELAP 69348

Barium 07/05/2011 12:250.50 mg/Kg-dry 1130NELAP 69348

Cadmium 07/05/2011 12:250.20 mg/Kg-dry 10.24NELAP 69348

Chromium 07/05/2011 12:251.00 mg/Kg-dry 123.2NELAP 69348

Lead 07/05/2011 12:254.00 mg/Kg-dry 120.4NELAP 69348

Silver 07/05/2011 12:250.55 mg/Kg-dry 1< 0.55NELAP 69348

SW-846 3050B, METALS BY GFAASelenium 7740 07/05/2011 11:550.577 mg/Kg-dry 1< 0.577NELAP 69349

SW-846 7471AMercury 07/05/2011 12:220.012 mg/Kg-dry 10.024NELAP 69355

SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/04/2011 12:426.28 mg/Kg-dry 1NDNELAP 69330

Kerosene 07/04/2011 12:426.28 mg/Kg-dry 1NDNELAP 69330

Mineral Spirits 07/04/2011 12:426.28 mg/Kg-dry 1NDNELAP 69330

Motor Oil 07/04/2011 12:426.28 mg/Kg-dry 1NDNELAP 69330

Surr: n-Tetracontane 07/04/2011 12:4250.6-140 %REC 178.3 69330

SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

4,4´-DDE 07/05/2011 23:062.10 µg/Kg-dry 16.64NELAP 69344

4,4´-DDT J 07/05/2011 23:062.10 µg/Kg-dry 11.4NELAP 69344

Alachlor 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Aldrin 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

alpha-BHC 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

alpha-Chlordane 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

beta-BHC 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Chlordane 07/05/2011 23:064.20 µg/Kg-dry 1NDNELAP 69344

delta-BHC 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Dieldrin 07/05/2011 23:062.10 µg/Kg-dry 14.12NELAP 69344

Endosulfan I 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Endosulfan II 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Endosulfan sulfate 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Endrin 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Endrin aldehyde 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Endrin ketone 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

gamma-BHC 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

gamma-Chlordane 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Heptachlor 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Heptachlor epoxide 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Methoxychlor 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344

Toxaphene 07/05/2011 23:0637.8 µg/Kg-dry 1NDNELAP 69344

Page 5 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD Surr: Decachlorobiphenyl 07/05/2011 23:0648-149 %REC 198.4 69344

Surr: Tetrachloro-m-xylene 07/05/2011 23:0619-145 %REC 175.4 69344

SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/05/2011 10:2547.2 µg/Kg-dry 1NDNELAP 69344

Aroclor 1221 07/05/2011 10:2547.2 µg/Kg-dry 1NDNELAP 69344






Surr: Decachlorobiphenyl 07/05/2011 10:255-156 %REC 199.3 69344

Surr: Tetrachloro-meta-xylene 07/05/2011 10:257.35-123 %REC 174.2 69344

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/05/2011 9:280.004 mg/Kg-dry 1NDNELAP 69347

Acenaphthylene 07/05/2011 9:280.004 mg/Kg-dry 1NDNELAP 69347

Anthracene 07/05/2011 9:280.004 mg/Kg-dry 10.005NELAP 69347

Benzo(a)anthracene 07/05/2011 9:280.004 mg/Kg-dry 10.022NELAP 69347

Benzo(a)pyrene 07/05/2011 9:280.004 mg/Kg-dry 10.025NELAP 69347

Benzo(b)fluoranthene 07/05/2011 9:280.004 mg/Kg-dry 10.033NELAP 69347

Benzo(g,h,i)perylene 07/05/2011 9:280.004 mg/Kg-dry 10.019NELAP 69347

Benzo(k)fluoranthene 07/05/2011 9:280.004 mg/Kg-dry 10.012NELAP 69347

Bis(2-ethylhexyl)phthalate J 07/05/2011 9:280.084 mg/Kg-dry 10.043NELAP 69347

Chrysene 07/05/2011 9:280.004 mg/Kg-dry 10.026NELAP 69347

Dibenzo(a,h)anthracene 07/05/2011 9:280.004 mg/Kg-dry 10.005NELAP 69347

Fluoranthene 07/05/2011 9:280.004 mg/Kg-dry 10.054NELAP 69347

Fluorene 07/05/2011 9:280.004 mg/Kg-dry 1NDNELAP 69347

Indeno(1,2,3-cd)pyrene 07/05/2011 9:280.004 mg/Kg-dry 10.015NELAP 69347

Naphthalene 07/05/2011 9:280.004 mg/Kg-dry 1NDNELAP 69347

Phenanthrene 07/05/2011 9:280.004 mg/Kg-dry 10.029NELAP 69347

Pyrene 07/05/2011 9:280.004 mg/Kg-dry 10.048NELAP 69347

Surr: 2-Fluorobiphenyl 07/05/2011 9:2810-131 %REC 188.4 69347

Surr: Nitrobenzene-d5 07/05/2011 9:2810-132 %REC 176.9 69347

Surr: p-Terphenyl-d14 07/05/2011 9:2880.2-138 %REC 1122.5 69347

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

1,2-Dichlorobenzene 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346



2,4,5-Trichlorophenol 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346


2,4-Dichlorophenol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

2,4-Dimethylphenol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

2,4-Dinitrophenol 07/05/2011 15:101.26 mg/Kg-dry 1NDNELAP 69346

2,4-Dinitrotoluene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346


2-Chloronaphthalene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

2-Chlorophenol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

Page 6 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Methoxy-4-methylphenol 07/05/2011 15:100.818 mg/Kg-dry 1ND 69346

2-Methylnaphthalene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

2-Nitroaniline 07/05/2011 15:101.26 mg/Kg-dry 1NDNELAP 69346

2-Nitrophenol 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

3,3´-Dichlorobenzidine 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346


4,6-Dinitro-2-methylphenol 07/05/2011 15:101.26 mg/Kg-dry 1NDNELAP 69346

4-Bromophenyl phenyl ether 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

4-Chloro-3-methylphenol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

4-Chloroaniline 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

4-Chlorophenyl phenyl ether 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346



Aniline 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

Azobenzene 07/05/2011 15:100.441 mg/Kg-dry 1ND 69346

Benzidine 07/05/2011 15:101.33 mg/Kg-dry 1See noteNELAP 69346

Benzoic acid 07/05/2011 15:101.89 mg/Kg-dry 1NDNELAP 69346

Benzyl alcohol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

Bis(2-chloroethoxy)methane 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

Bis(2-chloroethyl)ether 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

Bis(2-chloroisopropyl)ether 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

Butyl benzyl phthalate 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

Carbazole 07/05/2011 15:100.629 mg/Kg-dry 1ND 69346

Dibenzofuran 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

Diethyl phthalate 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

Dimethyl phthalate 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

Di-n-butyl phthalate 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

Di-n-octyl phthalate 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

Hexachlorobenzene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

Hexachlorobutadiene 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

Hexachlorocyclopentadiene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

Hexachloroethane 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

Isophorone 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

m,p-Cresol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

Nitrobenzene 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

N-Nitrosodimethylamine 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

N-Nitroso-di-n-propylamine 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

N-Nitrosodiphenylamine 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

o-Cresol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

Pentachlorophenol 07/05/2011 15:102.52 mg/Kg-dry 1NDNELAP 69346

Phenol 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346

Pyridine 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346

1,2-Diphenylhydrazine 07/05/2011 15:101.06 mg/Kg-dry 1ND 69346

Surr: 2,4,6-Tribromophenol 07/05/2011 15:1032.7-130 %REC 194.9 69346

Surr: 2-Fluorobiphenyl 07/05/2011 15:1034.1-116 %REC 182.1 69346

Surr: 2-Fluorophenol 07/05/2011 15:1030.5-99 %REC 176.5 69346

Surr: Nitrobenzene-d5 07/05/2011 15:1034.1-101 %REC 183.9 69346

Page 7 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Phenol-d5 07/05/2011 15:1034.9-110 %REC 175.8 69346


Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.LCS was outside upper QC limits. Sample was ND.

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

1,1,1-Trichloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

1,1,2,2-Tetrachloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/2011 11:514.9 µg/Kg-dry 1ND 69368


1,1-Dichloro-2-propanone 07/05/2011 11:5149.1 µg/Kg-dry 1ND 69368

1,1-Dichloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

1,1-Dichloroethene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

1,1-Dichloropropene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

1,2,3-Trichlorobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

1,2,3-Trichloropropane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368

1,2,3-Trimethylbenzene J 07/05/2011 11:514.9 µg/Kg-dry 11.4 69368


1,2,4-Trimethylbenzene J 07/05/2011 11:514.9 µg/Kg-dry 13.5NELAP 69368

1,2-Dibromo-3-chloropropane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

1,2-Dibromoethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

1,2-Dichlorobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368


1,2-Dichloropropane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

1,3,5-Trimethylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368




1-Chlorobutane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368


2-Butanone 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368

2-Chlorotoluene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

2-Hexanone 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368

2-Nitropropane 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368


4-Methyl-2-pentanone 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368

Acetone 07/05/2011 11:5149.1 µg/Kg-dry 163.7NELAP 69368

Acrolein 07/05/2011 11:5198.3 µg/Kg-dry 1NDNELAP 69368

Acrylonitrile 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368

Allyl chloride 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Benzene 07/05/2011 11:511.0 µg/Kg-dry 12.1NELAP 69368

Bromobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Bromochloromethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Bromodichloromethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Bromoform 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Bromomethane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368

Carbon disulfide 07/05/2011 11:514.9 µg/Kg-dry 15.3NELAP 69368

Page 8 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSCarbon tetrachloride 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Chlorobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Chloroethane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368

Chloroform 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Chloromethane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368

cis-1,2-Dichloroethene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

cis-1,3-Dichloropropene 07/05/2011 11:513.9 µg/Kg-dry 1NDNELAP 69368

Cyclohexanone 07/05/2011 11:5198.3 µg/Kg-dry 1ND 69368

Dibromochloromethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Dibromomethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Dichlorodifluoromethane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368

Ethyl acetate 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368

Ethyl ether 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Ethyl methacrylate 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Ethylbenzene J 07/05/2011 11:514.9 µg/Kg-dry 11.8NELAP 69368

Heptane 07/05/2011 11:5119.7 µg/Kg-dry 1ND 69368

Hexachlorobutadiene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Hexachloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Iodomethane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368

Isopropylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

m,p-Xylenes J 07/05/2011 11:514.9 µg/Kg-dry 13.3NELAP 69368

Methacrylonitrile 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368

Methyl Methacrylate 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Methyl tert-butyl ether 07/05/2011 11:512.0 µg/Kg-dry 1NDNELAP 69368

Methylacrylate 07/05/2011 11:519.8 µg/Kg-dry 1ND 69368

Methylene chloride 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Naphthalene J 07/05/2011 11:519.8 µg/Kg-dry 12.5NELAP 69368

n-Butylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

n-Hexane J 07/05/2011 11:5119.7 µg/Kg-dry 111 69368

Nitrobenzene 07/05/2011 11:5198.3 µg/Kg-dry 1NDNELAP 69368

n-Propylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

o-Xylene J 07/05/2011 11:514.9 µg/Kg-dry 11.3NELAP 69368

Pentachloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

p-Isopropyltoluene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Propionitrile 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368

sec-Butylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Styrene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

tert-Butylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Tetrachloroethene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Tetrahydrofuran 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368

Toluene J 07/05/2011 11:514.9 µg/Kg-dry 14.4NELAP 69368

trans-1,2-Dichloroethene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

trans-1,3-Dichloropropene 07/05/2011 11:513.9 µg/Kg-dry 1NDNELAP 69368

Trichloroethene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Trichlorofluoromethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368

Vinyl acetate 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368

Vinyl chloride 07/05/2011 11:512.0 µg/Kg-dry 1NDNELAP 69368

Page 9 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 1,2-Dichloroethane-d4 07/05/2011 11:5172.2-131 %REC 1105.6 69368

Surr: 4-Bromofluorobenzene 07/05/2011 11:5182.1-116 %REC 189.5 69368

Surr: Dibromofluoromethane 07/05/2011 11:5177.7-120 %REC 1102.4 69368

Surr: Toluene-d8 07/05/2011 11:5186-116 %REC 1103.0 69368

Marginal Exceedance for trichloroethene in LCS is verified per Volume 1 Module 4 section 1.7.4.2 of the 2009 TNI standard.

SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

2,4,5-TP (Silvex) 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

2,4-D 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

2,4-DB 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

3,5-Dichlorobenzoic Acid 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

Acifluorfen 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

Bentazon 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

Chloramben 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

Dalapon 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

DCPA 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

Dicamba 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

Dichlorprop 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

Dinoseb 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

Pentachlorophenol 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875

Picloram 07/11/2011 16:550.05 mg/Kg-dry 1NDNELAP R151875

Surr: DCAA 07/11/2011 17:4224-140 %REC 171.7 R151875

The blank spike recovery and/or blank spike duplicate recovery were outside the established acceptance limits for 3,5-Dichlorobenzoic Acid and 2,4,5-T. Batch was accepted based on acceptable MS/MSD/RPD results.

Page 10 of 58


TeklabHdrP

Laboratory Results








Lab ID: 11070042-002 Client Sample ID: SBA-B4-01 (5-6)

Matrix: SOLID

Batch






Cadmium J 07/05/2011 12:420.18 mg/Kg-dry 10.17NELAP 69348












4,4´-DDE 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344

4,4´-DDT J 07/05/2011 23:302.01 µg/Kg-dry 11.0NELAP 69344








Dieldrin S 07/05/2011 23:302.01 µg/Kg-dry 123.7NELAP 69344













Page 11 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch



Matrix spike and matrix spike duplicate did not recover within control limits for dieldrin because of sample composition.












Anthracene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347

Benzo(a)anthracene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347

Benzo(a)pyrene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347

Benzo(b)fluoranthene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347

Benzo(g,h,i)perylene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347

Benzo(k)fluoranthene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347

Bis(2-ethylhexyl)phthalate 07/05/2011 10:030.081 mg/Kg-dry 1NDNELAP 69347

Chrysene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347

Dibenzo(a,h)anthracene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347

Fluoranthene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347

Fluorene 07/05/2011 10:030.004 mg/Kg-dry 10.015NELAP 69347

Indeno(1,2,3-cd)pyrene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347


Phenanthrene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347

Pyrene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
















Page 12 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Chlorophenol 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346

2-Methoxy-4-methylphenol 07/05/2011 13:270.782 mg/Kg-dry 1ND 69346














































Page 13 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Nitrobenzene-d5 07/05/2011 13:2734.1-101 %REC 178.5 69346

Surr: Phenol-d5 07/05/2011 13:2734.9-110 %REC 179.2 69346


































Acetone J 07/05/2011 12:2444.4 µg/Kg-dry 120NELAP 69368










Page 14 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSCarbon disulfide 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368

Carbon tetrachloride 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368




























n-Hexane J 07/05/2011 12:2417.8 µg/Kg-dry 15.4 69368


















Page 15 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSVinyl chloride 07/05/2011 12:241.8 µg/Kg-dry 1NDNELAP 69368

Surr: 1,2-Dichloroethane-d4 07/05/2011 12:2472.2-131 %REC 1104.9 69368




















Surr: DCAA 07/11/2011 18:3024-140 %REC 164.0 R151875


Page 16 of 58


TeklabHdrP

Laboratory Results








Lab ID: 11070042-003 Client Sample ID: SBA-D5-01 (5-6)

Matrix: SOLID

Batch





Barium 07/05/2011 12:480.47 mg/Kg-dry 147.2NELAP 69348






SW-846 7471AMercury J 07/05/2011 12:220.011 mg/Kg-dry 10.005NELAP 69355








4,4´-DDT 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344








Dieldrin 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344













Page 17 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch












SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/05/2011 10:390.004 mg/Kg-dry 10.052NELAP 69347














Naphthalene 07/05/2011 10:390.004 mg/Kg-dry 10.021NELAP 69347



















Page 18 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch


























Dimethyl phthalate S 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346



Hexachlorobenzene S 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346






Nitrobenzene S 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346













Page 19 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch



Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.Matrix spike duplicate was outside QC limits.LCS was outside upper QC limits. Sample was ND.










































Page 20 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSCarbon disulfide 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368















































Page 21 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSVinyl chloride 07/05/2011 12:541.7 µg/Kg-dry 1NDNELAP 69368








2,4-D R 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875










Dinoseb R 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875



Surr: DCAA 07/11/2011 19:1724-140 %REC 149.6 R151875

The MS/MSD RPD result exceeded the QC control limits for 2,4-D and Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.The blank spike recovery and/or blank spike duplicate recovery were outside the established acceptance limits for 3,5-Dichlorobenzoic Acid and 2,4,5-T. Batch was accepted based on acceptable MS/MSD/RPD results.

Page 22 of 58


TeklabHdrP

Laboratory Results








Lab ID: 11070042-004 Client Sample ID: SBA-A3-01 (5-6)

Matrix: SOLID

Batch











SW-846 7471AMercury J 07/05/2011 12:220.011 mg/Kg-dry 10.003NELAP 69355





























Page 23 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch


















Benzo(g,h,i)perylene J 07/05/2011 11:150.004 mg/Kg-dry 10.004NELAP 69347



























Page 24 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch
















































Page 25 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch















1,2,3-Trimethylbenzene 07/05/2011 13:224.0 µg/Kg-dry 1ND 69368






























Carbon disulfide 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368

Page 26 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch





Chloromethane J 07/05/2011 13:227.9 µg/Kg-dry 14.1NELAP 69368










Ethylbenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368

















o-Xylene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
















Page 27 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch





















Surr: DCAA 07/11/2011 20:0524-140 %REC 148.7 R151875


Page 28 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch



SW-846 9012A (TOTAL)Cyanide R 07/02/2011 12:170.58 mg/Kg-dry 1< 0.58NELAP R151533

RPD for MS/MSD was outside of QC limit due to sample composition.



Cadmium 07/05/2011 13:000.19 mg/Kg-dry 1< 0.19NELAP 69348


































Page 29 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch


















Benzo(g,h,i)perylene J 07/05/2011 13:030.004 mg/Kg-dry 10.004NELAP 69347





Fluoranthene J 07/05/2011 13:030.004 mg/Kg-dry 10.004NELAP 69347




Phenanthrene J 07/05/2011 13:030.004 mg/Kg-dry 10.004NELAP 69347


















Page 30 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch
















































Page 31 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch














































Page 32 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch


























Methylene chloride J 07/05/2011 14:254.3 µg/Kg-dry 11.2NELAP 69368



n-Hexane 07/05/2011 14:2517.2 µg/Kg-dry 1ND 69368



















Page 33 of 58


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch





Surrogate and/or internal standard recovery was outside QC limits due to matrix interference.Marginal Exceedance for trichloroethene in LCS is verified per Volume 1 Module 4 section 1.7.4.2 of the 2009 TNI standard.
















Surr: DCAA 07/11/2011 20:5224-140 %REC 141.9 R151875


Page 34 of 58


Lab Sample ID Client Sample ID Collection DateFractions

TeklabHdrP

Matrix

Sample Summary






11070042-001 SBA-C3-01 (5-6) 06/29/2011 16:006Solid

11070042-002 SBA-B4-01 (5-6) 06/30/2011 8:006Solid

11070042-003 SBA-D5-01 (5-6) 06/30/2011 9:006Solid

11070042-004 SBA-A3-01 (5-6) 06/30/2011 10:006Solid

11070042-005 SBA-A5-01 (5-6) 06/30/2011 11:006Solid

Page 35 of 58


11070042-001

Analysis Date/TimeTest Name Prep Date/Time

____TeklabHdrP

Sample ID Client Sample ID Collection Date Received Date

Dates Report






11070042-001A SBA-C3-01 (5-6) 06/29/2011 16:00 7/1/2011 3:50:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/01/2011 16:00

Standard Methods 18th Ed. 2540 G 07/01/2011 16:00

SW-846 3050B, 6010B, Metals by ICP 07/05/2011 12:2507/01/2011 20:08

SW-846 3050B, Metals by GFAA 07/05/2011 11:5507/01/2011 19:57

SW-846 7471A 07/05/2011 12:2207/05/2011 8:45

SW-846 9012A (Total) 07/02/2011 12:17

11070042-001B SBA-C3-01 (5-6) 06/29/2011 16:00 7/1/2011 3:50:00 PM

SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/04/2011 12:4207/01/2011 17:42

SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/05/2011 23:0607/01/2011 18:31

SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/05/2011 10:2507/01/2011 18:31

SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 9:2807/01/2011 19:51

SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 15:1007/01/2011 19:47

11070042-001C SBA-C3-01 (5-6) 06/29/2011 16:00 7/1/2011 3:50:00 PM

SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 16:55


11070042-001F SBA-C3-01 (5-6) 06/29/2011 16:00 7/1/2011 3:50:00 PM

SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/05/2011 11:51

11070042-002A SBA-B4-01 (5-6) 06/30/2011 8:00 7/1/2011 3:50:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/01/2011 16:00




SW-846 7471A 07/05/2011 12:2207/05/2011 8:45

SW-846 9012A (Total) 07/02/2011 12:17

11070042-002B SBA-B4-01 (5-6) 06/30/2011 8:00 7/1/2011 3:50:00 PM






11070042-002C SBA-B4-01 (5-6) 06/30/2011 8:00 7/1/2011 3:50:00 PM



11070042-002F SBA-B4-01 (5-6) 06/30/2011 8:00 7/1/2011 3:50:00 PM


Page 36 of 58


11070042-001A


____TeklabHdrP


Dates Report






11070042-003A SBA-D5-01 (5-6) 06/30/2011 9:00 7/1/2011 3:50:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/01/2011 16:00




SW-846 7471A 07/05/2011 12:2207/05/2011 8:45

SW-846 9012A (Total) 07/02/2011 12:17

11070042-003B SBA-D5-01 (5-6) 06/30/2011 9:00 7/1/2011 3:50:00 PM






11070042-003C SBA-D5-01 (5-6) 06/30/2011 9:00 7/1/2011 3:50:00 PM



11070042-003F SBA-D5-01 (5-6) 06/30/2011 9:00 7/1/2011 3:50:00 PM


11070042-004A SBA-A3-01 (5-6) 06/30/2011 10:00 7/1/2011 3:50:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/01/2011 16:00




SW-846 7471A 07/05/2011 12:2207/05/2011 8:45

SW-846 9012A (Total) 07/02/2011 12:17

11070042-004B SBA-A3-01 (5-6) 06/30/2011 10:00 7/1/2011 3:50:00 PM






11070042-004C SBA-A3-01 (5-6) 06/30/2011 10:00 7/1/2011 3:50:00 PM



11070042-004F SBA-A3-01 (5-6) 06/30/2011 10:00 7/1/2011 3:50:00 PM


Page 37 of 58


11070042-003A


____TeklabHdrP


Dates Report






11070042-005A SBA-A5-01 (5-6) 06/30/2011 11:00 7/1/2011 3:50:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/01/2011 16:00




SW-846 7471A 07/05/2011 12:2207/05/2011 8:45

SW-846 9012A (Total) 07/02/2011 12:17

11070042-005B SBA-A5-01 (5-6) 06/30/2011 11:00 7/1/2011 3:50:00 PM






11070042-005C SBA-A5-01 (5-6) 06/30/2011 11:00 7/1/2011 3:50:00 PM



11070042-005F SBA-A5-01 (5-6) 06/30/2011 11:00 7/1/2011 3:50:00 PM


Page 38 of 58


11070042-005A

Quality Control Results






STANDARD METHODS 18TH ED. 2540 G

SampID: LCS-R151526

SampType: LCS %UnitsR151526Batch

Analyses Result

Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit

Total Solids 07/01/20110.1 1.01.0 1000 90 110

SampID: LCSQC-R151526

SampType: LCSQC %UnitsR151526Batch

Analyses Result


Total Solids 07/01/20110.1 1.01.0 1000 90 110

SampID: 11070042-001ADUP

SampType: DUP %UnitsR151526Batch RPD Limit 15

Analyses Result

Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD

Total Solids 07/01/20110.1 80.0 0.7779.38

SW-846 9012A (TOTAL)

SampID: MB-R151533

SampType: MBLK mg/KgUnitsR151533Batch

Analyses Result


Cyanide 07/02/20110.01 < 0.01

SampID: LCS-R151533

SampType: LCS mg/KgUnitsR151533Batch

Analyses Result


Cyanide 07/02/20110.01 0.020.02 99.20 85 115

SampID: 11070042-005AMS

SampType: MS mg/Kg-dryUnitsR151533Batch

Analyses Result


Cyanide 07/02/20110.63 1.461.10 75.60 75 125

SampID: 11070042-005AMSD

SampType: MSD mg/Kg-dryUnitsR151533Batch RPD Limit 15

Analyses Result


Cyanide R 07/02/20110.58 1.461.39 95.4 23.140 1.105

SampID: MB-R151616

SampType: MBLK mg/KgUnitsR151616Batch

Analyses Result


Cyanide 07/06/20110.01 < 0.01

SampID: LCS-R151616


Analyses Result


Cyanide 07/06/20110.01 0.020.02 86.40 85 115

Page 39 of 58









SampID: LCS-R151616


Analyses Result


SW-846 3050B, 6010B, METALS BY ICP

SampID: MB-69348

SampType: MBLK mg/Kg-dryUnits69348Batch

Analyses Result


Arsenic 07/05/20112.50 2.50< 2.50 00 -100 100

Barium 07/05/20110.50 0.50< 0.50 00 -100 100

Cadmium 07/05/20110.20 0.20< 0.20 00 -100 100

Chromium 07/05/20111.00 1.00< 1.00 00 -100 100

Lead 07/05/20114.00 4.00< 4.00 00 -100 100

Silver 07/05/20110.55 0.55< 0.55 00 -100 100

SampID: LCS-69348

SampType: LCS mg/Kg-dryUnits69348Batch

Analyses Result


Arsenic 07/05/20112.50 200195 97.60 85 115

Barium 07/05/20110.50 200194 97.00 85 115

Cadmium 07/05/20110.20 5.004.90 98.00 85 115

Chromium 07/05/20111.00 20.019.7 98.50 85 115

Lead 07/05/20114.00 50.049.4 98.70 85 115

Silver 07/05/20110.55 5.004.95 99.00 85 115

SampID: 11070042-001AMS

SampType: MS mg/Kg-dryUnits69348Batch

Analyses Result


Arsenic 07/05/20112.50 200207 97.711.30 75 125

Barium 07/05/20110.50 200324 96.7130.2 75 125

Cadmium 07/05/20110.20 5.005.00 95.20.2400 75 125

Chromium 07/05/20111.00 20.045.5 111.523.20 75 125

Lead 07/05/20114.00 50.068.2 95.720.36 75 125

Silver 07/05/20110.55 5.004.79 95.80 75 125


SampType: MSD mg/Kg-dryUnits69348Batch RPD Limit 20

Analyses Result


Arsenic 07/05/20112.50 200209 98.8 1.1511.30 206.6

Barium 07/05/20110.50 200318 94.1 1.65130.2 323.6

Cadmium 07/05/20110.20 5.005.06 96.4 1.190.2400 5.000

Chromium 07/05/20111.00 20.044.8 107.9 1.6023.20 45.50

Lead 07/05/20114.00 50.068.0 95.3 0.2620.36 68.19

Silver 07/05/20110.55 5.004.87 97.4 1.660 4.790

SW-846 3050B, METALS BY GFAA

Page 40 of 58









SampID: MB-69349


Analyses Result


Selenium 7740 07/05/20110.600 0.600< 0.600 00 -100 100

SampID: LCS-69349


Analyses Result


Selenium 7740 07/05/20110.600 3.003.16 105.40 80 120

SampID: 11070042-004AMS


Analyses Result


Selenium 7740 07/05/20110.588 2.942.86 97.10 70 130



Analyses Result


Selenium 7740 07/05/20110.588 2.942.72 92.5 4.820 2.856

SW-846 7471A

SampID: MB-69355

SampType: MBLK mg/KgUnits69355Batch

Analyses Result


Mercury 07/05/20110.010 0.010< 0.010 00 -100 100

SampID: LCS-69355

SampType: LCS mg/KgUnits69355Batch

Analyses Result


Mercury 07/05/20110.010 0.2500.272 109.00 85 115

SampID: 11070042-001AMS


Analyses Result


Mercury 07/05/20110.012 0.3000.367 114.40.02400 75 125



Analyses Result


Mercury 07/05/20110.012 0.3000.361 112.2 1.810.02400 0.3671

SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FID

Page 41 of 58









SampID: MB-69330


Analyses Result


Diesel 07/04/20115.00 NDKerosene 07/04/20115.00 NDMineral Spirits 07/04/20115.00 NDMotor Oil 07/04/20115.00 ND Surr: n-Tetracontane 07/04/20110.670.50 74.3 54.8 128

SampID: LCS-69330


Analyses Result


Diesel 07/04/20115.00 16.714.4 86.40 40.4 121

Surr: n-Tetracontane 07/04/20110.670.53 79.0 54.8 128

SampID: 11070042-005BMS


Analyses Result


Diesel 07/04/20115.82 19.418.0 92.70 20.3 167


SampID: 11070042-005BMSD


Analyses Result


Diesel 07/04/20115.84 19.519.6 100.3 8.170 18.03

Surr: n-Tetracontane 07/04/20110.780.55 70.6

SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD

SampID: MB-69344

SampType: MBLK µg/KgUnits69344Batch

Analyses Result


4,4´-DDD 07/05/20111.67 ND4,4´-DDE 07/05/20111.67 ND4,4´-DDT 07/05/20111.67 NDAlachlor 07/05/20111.67 NDAldrin 07/05/20111.67 NDalpha-BHC 07/05/20111.67 NDalpha-Chlordane 07/05/20111.67 NDbeta-BHC 07/05/20111.67 NDdelta-BHC 07/05/20111.67 NDDieldrin 07/05/20111.67 NDEndosulfan I 07/05/20111.67 NDEndosulfan II 07/05/20111.67 NDEndosulfan sulfate 07/05/20111.67 NDEndrin 07/05/20111.67 NDEndrin aldehyde 07/05/20111.67 NDEndrin ketone 07/05/20111.67 NDgamma-BHC 07/05/20111.67 ND

Page 42 of 58









SampID: MB-69344


Analyses Result


gamma-Chlordane 07/05/20111.67 NDHeptachlor 07/05/20111.67 NDHeptachlor epoxide 07/05/20111.67 NDMethoxychlor 07/05/20111.67 ND Surr: Decachlorobiphenyl 07/05/20118.339.10 109.3 73.5 150

Surr: Tetrachloro-m-xylene 07/05/20118.335.33 64.0 14.4 113

SampID: LCSPST-69344

SampType: LCS µg/KgUnits69344Batch

Analyses Result


4,4´-DDD 07/05/20111.67 8.336.94 83.30 36 208

4,4´-DDE 07/05/20111.67 8.336.54 78.50 26 191

4,4´-DDT 07/05/20111.67 8.337.20 86.50 3 215

Alachlor 07/05/20111.67 8.339.53 114.50 30 170

Aldrin 07/05/20111.67 8.335.40 64.80 46 173

alpha-BHC 07/05/20111.67 8.335.09 61.10 37 179

alpha-Chlordane 07/05/20111.67 8.336.64 79.70 38 187

beta-BHC 07/05/20111.67 8.336.63 79.60 51 185

delta-BHC 07/05/20111.67 8.336.85 82.20 46 166

Dieldrin 07/05/20111.67 8.336.48 77.80 26 216

Endosulfan I 07/05/20111.67 8.336.37 76.50 31 205

Endosulfan II 07/05/20111.67 8.338.19 98.30 42 187

Endosulfan sulfate 07/05/20111.67 8.337.98 95.90 29 230

Endrin 07/05/20111.67 8.337.30 87.60 30 215

Endrin aldehyde 07/05/20111.67 8.337.55 90.70 42 202

Endrin ketone 07/05/20111.67 8.337.50 90.00 19 244

gamma-BHC 07/05/20111.67 8.335.26 63.20 55 166

gamma-Chlordane 07/05/20111.67 8.336.07 72.80 23 186

Heptachlor 07/05/20111.67 8.335.97 71.60 43 172

Heptachlor epoxide 07/05/20111.67 8.335.96 71.60 39 204

Methoxychlor 07/05/20111.67 8.338.76 105.10 3 221

Surr: Decachlorobiphenyl 07/05/20118.338.06 96.8 50.4 176

Surr: Tetrachloro-m-xylene 07/05/20118.334.33 51.9 10 107

SampID: 11070042-002BMS

SampType: MS µg/Kg-dryUnits69344Batch

Analyses Result


4,4´-DDD 07/05/20112.01 10.08.69 86.60 36 208

4,4´-DDE 07/05/20112.01 10.08.07 80.40 26 191

4,4´-DDT 07/05/20112.01 10.08.34 72.81.027 3 215

Alachlor 07/05/20112.01 10.010.8 107.50 30 170

Aldrin 07/05/20112.01 10.07.28 72.60 46 173

alpha-BHC 07/05/20112.01 10.07.28 72.60 37 179

alpha-Chlordane 07/05/20112.01 10.08.12 80.90 38 187

beta-BHC 07/05/20112.01 10.08.53 85.00 51 185

delta-BHC 07/05/20112.01 10.08.48 84.50 46 166

Page 43 of 58









SampID: 11070042-002BMS


Analyses Result


Dieldrin S 07/05/20112.01 10.019.2 -45.323.73 26 216

Endosulfan I 07/05/20112.01 10.07.06 70.30 31 205

Endosulfan II 07/05/20112.01 10.09.57 95.40 42 187


Endrin 07/05/20112.01 10.09.28 92.40 30 215

Endrin aldehyde 07/05/20112.01 10.09.14 91.10 42 202

Endrin ketone 07/05/20112.01 10.08.83 88.00 19 244

gamma-BHC 07/05/20112.01 10.07.36 73.30 55 166

gamma-Chlordane 07/05/20112.01 10.07.24 72.20 23 186

Heptachlor 07/05/20112.01 10.07.51 74.80 43 172


Methoxychlor 07/05/20112.01 10.09.71 96.70 3 221

Surr: Decachlorobiphenyl 07/05/201110.010.6 105.2 48 149



SampType: MSD µg/Kg-dryUnits69344Batch RPD Limit 40

Analyses Result


4,4´-DDD 07/06/20112.01 10.07.47 74.4 15.060 8.690

4,4´-DDE 07/06/20112.01 10.07.27 72.3 10.390 8.066

4,4´-DDT 07/06/20112.01 10.07.54 64.9 10.031.027 8.339

Alachlor 07/06/20112.01 10.09.78 97.3 9.910 10.80

Aldrin 07/06/20112.01 10.06.54 65.1 10.800 7.285

alpha-BHC 07/06/20112.01 10.06.32 62.9 14.160 7.283

alpha-Chlordane 07/06/20112.01 10.07.43 73.9 8.970 8.123

beta-BHC 07/06/20112.01 10.08.13 80.9 4.750 8.528

delta-BHC 07/06/20112.01 10.08.06 80.3 5.050 8.481

Dieldrin S 07/06/20112.01 10.026.3 25.9 31.4423.73 19.18

Endosulfan I 07/06/20112.01 10.06.83 68.0 3.260 7.057

Endosulfan II 07/06/20112.01 10.08.86 88.2 7.760 9.573

Endosulfan sulfate 07/06/20112.01 10.08.03 79.9 5.530 8.488

Endrin 07/06/20112.01 10.08.29 82.5 11.270 9.275

Endrin aldehyde 07/06/20112.01 10.08.48 84.4 7.480 9.143

Endrin ketone 07/06/20112.01 10.08.11 80.7 8.610 8.834

gamma-BHC 07/06/20112.01 10.06.39 63.6 14.100 7.356

gamma-Chlordane 07/06/20112.01 10.06.40 63.7 12.320 7.244

Heptachlor 07/06/20112.01 10.06.50 64.7 14.500 7.513

Heptachlor epoxide 07/06/20112.01 10.06.69 66.5 12.140 7.550

Methoxychlor 07/06/20112.01 10.08.81 87.7 9.740 9.711

Surr: Decachlorobiphenyl 07/06/201110.09.87 98.3

Surr: Tetrachloro-m-xylene 07/06/201110.06.29 62.6

SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECD

Page 44 of 58









SampID: MB-69344


Analyses Result


Aroclor 1016 07/05/201137.5 NDAroclor 1221 07/05/201137.5 NDAroclor 1232 07/05/201137.5 NDAroclor 1242 07/05/201137.5 NDAroclor 1248 07/05/201137.5 NDAroclor 1254 07/05/201137.5 NDAroclor 1260 07/05/201137.5 ND Surr: Decachlorobiphenyl 07/05/20118.38.4 101.6 86.4 159

Surr: Tetrachloro-meta-xylene 07/05/20118.34.7 56.2 31.6 114

SampID: LCSPCB-69344


Analyses Result


Aroclor 1016 07/05/201137.5 167118 70.70 54.9 121

Aroclor 1260 07/05/201137.5 167143 86.10 65.5 133



SampID: 11070042-001BMS


Analyses Result


Aroclor 1016 07/05/201147.1 209168 80.10 35.8 143

Aroclor 1260 07/05/201147.1 209181 86.20 22.3 152





Analyses Result


Aroclor 1016 07/05/201147.2 210163 77.9 2.640 167.6

Aroclor 1260 07/05/201147.2 210176 84.1 2.360 180.5

Surr: Decachlorobiphenyl 07/05/201110.410 96.3

Surr: Tetrachloro-meta-xylene 07/05/201110.46.0 57.1

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS

SampID: MB-69347


Analyses Result


Acenaphthene 07/05/20110.003 NDAcenaphthylene 07/05/20110.003 NDAnthracene 07/05/20110.003 NDBenzo(a)anthracene 07/05/20110.003 NDBenzo(a)pyrene 07/05/20110.003 NDBenzo(b)fluoranthene 07/05/20110.003 NDBenzo(g,h,i)perylene 07/05/20110.003 ND

Page 45 of 58









SampID: MB-69347


Analyses Result


Benzo(k)fluoranthene 07/05/20110.003 NDBis(2-ethylhexyl)phthalate 07/05/20110.067 NDChrysene 07/05/20110.003 NDDibenzo(a,h)anthracene 07/05/20110.003 NDFluoranthene 07/05/20110.003 NDFluorene 07/05/20110.003 NDIndeno(1,2,3-cd)pyrene 07/05/20110.003 NDNaphthalene 07/05/20110.003 NDPhenanthrene 07/05/20110.003 NDPyrene 07/05/20110.003 ND Surr: 2-Fluorobiphenyl 07/05/20110.1670.136 81.4 45.7 89.2

Surr: Nitrobenzene-d5 07/05/20110.1670.112 66.9 31.4 100

Surr: p-Terphenyl-d14 07/05/20110.1670.207 124.0 53.3 124

SampID: LCS-69347


Analyses Result


Acenaphthene 07/05/20110.003 0.1670.161 96.40 56.3 115

Acenaphthylene 07/05/20110.003 0.1670.163 97.80 60.3 143

Anthracene 07/05/20110.003 0.1670.128 76.60 52.1 109

Benzo(a)anthracene 07/05/20110.003 0.1670.148 88.40 52.8 112

Benzo(a)pyrene 07/05/20110.003 0.1670.152 90.80 40.8 127

Benzo(b)fluoranthene 07/05/20110.003 0.1670.168 100.60 50.1 150

Benzo(g,h,i)perylene 07/05/20110.003 0.1670.167 1000 52.8 145

Benzo(k)fluoranthene 07/05/20110.003 0.1670.172 102.80 52 153

Bis(2-ethylhexyl)phthalate 07/05/20110.067 0.1670.178 106.80 50 150

Chrysene 07/05/20110.003 0.1670.158 94.80 60.8 128

Dibenzo(a,h)anthracene 07/05/20110.003 0.1670.176 105.20 54.9 150

Fluoranthene 07/05/20110.003 0.1670.152 90.80 58.7 125

Fluorene 07/05/20110.003 0.1670.169 101.00 57.8 125

Indeno(1,2,3-cd)pyrene 07/05/20110.003 0.1670.173 103.60 52 147

Naphthalene 07/05/20110.003 0.1670.142 85.00 54.8 113

Phenanthrene 07/05/20110.003 0.1670.163 97.60 60.4 121

Pyrene 07/05/20110.003 0.1670.158 94.60 57.9 129

Surr: 2-Fluorobiphenyl 07/05/20110.1670.122 73.3 45.7 89.2



SampID: 11070042-004BMS


Analyses Result


Acenaphthene 07/05/20110.004 0.1900.182 95.80 36 135

Acenaphthylene 07/05/20110.004 0.1900.186 98.00 17.2 167

Anthracene 07/05/20110.004 0.1900.149 78.20 39.3 124

Benzo(a)anthracene 07/05/20110.004 0.1900.170 87.40.004173 10 183

Benzo(a)pyrene 07/05/20110.004 0.1900.186 98.00 10 204

Page 46 of 58









SampID: 11070042-004BMS


Analyses Result



Benzo(g,h,i)perylene 07/05/20110.004 0.1900.170 87.40.003794 10 168

Benzo(k)fluoranthene 07/05/20110.004 0.1900.192 101.00 27.6 181

Bis(2-ethylhexyl)phthalate 07/05/20110.076 0.1900.218 114.60 50 150

Chrysene 07/05/20110.004 0.1900.183 96.00 10 176


Fluoranthene 07/05/20110.004 0.1900.174 91.40 10 227

Fluorene 07/05/20110.004 0.1900.183 96.40 35.2 148

Indeno(1,2,3-cd)pyrene 07/05/20110.004 0.1900.185 97.40 10 164

Naphthalene 07/05/20110.004 0.1900.172 90.40 14.7 128

Phenanthrene 07/05/20110.004 0.1900.188 98.80 32.8 143

Pyrene 07/05/20110.004 0.1900.183 96.00 10 180

Surr: 2-Fluorobiphenyl 07/05/20110.1900.120 62.9 10 131

Surr: Nitrobenzene-d5 07/05/20110.1900.118 62.1 10 132



SampType: MSD mg/Kg-dryUnits69347Batch RPD Limit 49.7

Analyses Result


Acenaphthene 07/05/20110.004 0.1900.178 93.8 2.470 0.1822

Acenaphthylene 07/05/20110.004 0.1900.178 93.8 4.730 0.1863

Anthracene 07/05/20110.004 0.1900.138 73.1 7.220 0.1488

Benzo(a)anthracene 07/05/20110.004 0.1900.162 83.2 5.150.004173 0.1704

Benzo(a)pyrene 07/05/20110.004 0.1900.184 97.2 1.180 0.1863

Benzo(b)fluoranthene 07/05/20110.004 0.1900.189 99.6 3.710 0.1958

Benzo(g,h,i)perylene 07/05/20110.004 0.1900.164 84.4 3.770.003794 0.1700

Benzo(k)fluoranthene 07/05/20110.004 0.1900.185 97.4 3.990 0.1920

Bis(2-ethylhexyl)phthalate 07/05/20110.076 0.1900.196 103.2 10.810 0.2178

Chrysene 07/05/20110.004 0.1900.175 92.2 4.390 0.1826

Dibenzo(a,h)anthracene 07/05/20110.004 0.1900.183 96.4 3.820 0.1898

Fluoranthene 07/05/20110.004 0.1900.161 85.2 7.370 0.1738

Fluorene 07/05/20110.004 0.1900.184 97.2 0.460 0.1833

Indeno(1,2,3-cd)pyrene 07/05/20110.004 0.1900.176 92.8 5.190 0.1852

Naphthalene 07/05/20110.004 0.1900.155 81.8 10.330 0.1719

Phenanthrene 07/05/20110.004 0.1900.177 93.2 6.190 0.1879

Pyrene 07/05/20110.004 0.1900.170 89.8 7.020 0.1826

Surr: 2-Fluorobiphenyl 07/05/20110.1900.115 60.9

Surr: Nitrobenzene-d5 07/05/20110.1900.108 57.1

Surr: p-Terphenyl-d14 07/05/20110.1900.210 111.0

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS

SampID: MB-69346


Analyses Result


1,2,4-Trichlorobenzene 07/05/20110.500 ND1,2-Dichlorobenzene 07/05/20110.500 ND

Page 47 of 58









SampID: MB-69346


Analyses Result


1,3-Dichlorobenzene 07/05/20110.500 ND1,4-Dichlorobenzene 07/05/20110.500 ND2,4,5-Trichlorophenol 07/05/20110.350 ND2,4,6-Trichlorophenol 07/05/20110.350 ND2,4-Dichlorophenol 07/05/20110.500 ND2,4-Dimethylphenol 07/05/20110.500 ND2,4-Dinitrophenol 07/05/20111.00 ND2,4-Dinitrotoluene 07/05/20110.350 ND2,6-Dinitrotoluene 07/05/20110.350 ND2-Chloronaphthalene 07/05/20110.350 ND2-Chlorophenol 07/05/20110.500 ND2-Methoxy-4-methylphenol 07/05/20110.650 ND2-Methylnaphthalene 07/05/20110.350 ND2-Nitroaniline 07/05/20111.00 ND2-Nitrophenol 07/05/20110.350 ND3,3´-Dichlorobenzidine 07/05/20110.350 ND3-Nitroaniline 07/05/20111.00 ND4,6-Dinitro-2-methylphenol 07/05/20111.00 ND4-Bromophenyl phenyl ether 07/05/20110.350 ND4-Chloro-3-methylphenol 07/05/20110.500 ND4-Chloroaniline 07/05/20110.500 ND4-Chlorophenyl phenyl ether 07/05/20110.350 ND4-Nitroaniline 07/05/20110.500 ND4-Nitrophenol 07/05/20110.350 NDAniline 07/05/20110.500 NDAzobenzene 07/05/20110.350 NDBenzidine 07/05/20111.06 NDBenzoic acid 07/05/20111.50 NDBenzyl alcohol 07/05/20110.500 NDBis(2-chloroethoxy)methane 07/05/20110.350 NDBis(2-chloroethyl)ether 07/05/20110.500 NDBis(2-chloroisopropyl)ether 07/05/20110.350 NDButyl benzyl phthalate 07/05/20110.350 NDCarbazole 07/05/20110.500 NDDibenzofuran 07/05/20110.350 NDDiethyl phthalate 07/05/20110.500 NDDimethyl phthalate 07/05/20110.350 NDDi-n-butyl phthalate 07/05/20110.350 NDDi-n-octyl phthalate 07/05/20110.350 NDHexachlorobenzene 07/05/20110.350 NDHexachlorobutadiene 07/05/20110.500 NDHexachlorocyclopentadiene 07/05/20110.350 NDHexachloroethane 07/05/20110.500 NDIsophorone 07/05/20110.350 NDm,p-Cresol 07/05/20110.500 NDNitrobenzene 07/05/20110.500 NDN-Nitrosodimethylamine 07/05/20110.500 ND

Page 48 of 58









SampID: MB-69346


Analyses Result


N-Nitroso-di-n-propylamine 07/05/20110.500 NDN-Nitrosodiphenylamine 07/05/20110.500 NDo-Cresol 07/05/20110.500 NDPentachlorophenol 07/05/20112.00 NDPhenol 07/05/20110.350 NDPyridine 07/05/20110.500 ND1,2-Diphenylhydrazine 07/05/20110.840 ND Surr: 2,4,6-Tribromophenol 07/05/20111.671.64 98.3 52.1 113

Surr: 2-Fluorobiphenyl 07/05/20110.8350.701 83.9 46.3 106

Surr: 2-Fluorophenol 07/05/20111.671.31 78.3 50.6 89

Surr: Nitrobenzene-d5 07/05/20110.8350.707 84.6 42.4 99.2

Surr: Phenol-d5 07/05/20111.671.30 78.1 55.9 98.5


SampID: LCS-69346


Analyses Result


1,2,4-Trichlorobenzene 07/05/20110.500 1.671.42 84.80 43.9 92.2

1,4-Dichlorobenzene 07/05/20110.500 1.671.35 80.80 43.8 84.1

2,4,5-Trichlorophenol 07/05/20110.350 3.332.98 89.60 38.6 123


2,4-Dimethylphenol 07/05/20110.500 3.332.54 76.20 38.3 88

2,4-Dinitrophenol 07/05/20111.00 3.334.11 123.60 1.88 162

2,4-Dinitrotoluene S 07/05/20110.350 1.672.03 121.80 48.6 102

2-Chlorophenol 07/05/20110.500 3.332.47 74.20 46.6 84

4-Chloro-3-methylphenol 07/05/20110.500 3.333.01 90.50 51.5 94.9

4-Nitrophenol S 07/05/20110.350 3.334.05 121.60 53.2 104

Diethyl phthalate 07/05/20110.500 3.333.24 97.20 51.7 106

Dimethyl phthalate 07/05/20110.350 3.332.97 89.20 58.8 104

Di-n-butyl phthalate 07/05/20110.350 1.671.70 101.90 54.3 105

Hexachlorobenzene 07/05/20110.350 3.333.03 91.00 55.9 106

Hexachlorobutadiene 07/05/20110.500 3.332.74 82.30 35.7 100

Hexachloroethane 07/05/20110.500 3.332.65 79.50 38.9 89.9

m,p-Cresol 07/05/20110.500 1.671.40 83.60 37.6 93.7

Nitrobenzene 07/05/20110.500 3.332.65 79.70 51.8 104

N-Nitroso-di-n-propylamine 07/05/20110.500 1.671.35 80.80 49.1 94.5

o-Cresol 07/05/20110.500 1.671.36 81.40 43 101

Pentachlorophenol 07/05/20112.00 3.333.22 96.80 42.2 102

Phenol 07/05/20110.350 3.332.53 75.80 41.6 81.3

Pyridine 07/05/20110.500 3.332.19 65.80 3.61 74.3

Surr: 2,4,6-Tribromophenol 07/05/20111.671.76 105.4 52.1 113




Surr: Phenol-d5 07/05/20111.671.27 76.0 55.9 98.5


Page 49 of 58









SampID: 11070042-003BMS


Analyses Result


1,2,4-Trichlorobenzene 07/05/20110.585 1.961.48 75.60 35.9 102




2,4-Dimethylphenol 07/05/20110.585 3.902.63 67.60 38.3 88

2,4-Dinitrophenol 07/05/20111.17 3.903.65 93.70 1.88 162

2,4-Dinitrotoluene 07/05/20110.410 1.962.08 106.50 37.5 107

2-Chlorophenol 07/05/20110.585 3.902.52 64.60 22.6 108

4-Chloro-3-methylphenol 07/05/20110.585 3.903.34 85.70 19.3 131

4-Nitrophenol 07/05/20110.410 3.904.51 115.70 27.6 123







m,p-Cresol 07/05/20110.585 1.961.54 78.50 37.6 93.7

Nitrobenzene 07/05/20110.585 3.902.78 71.20 51.8 104


o-Cresol 07/05/20110.585 1.961.46 74.90 43 101


Phenol 07/05/20110.410 3.902.78 71.20 20.8 110

Pyridine 07/05/20110.585 3.902.21 56.60 3.61 74.3





Surr: Phenol-d5 07/05/20111.961.41 72.3 34.9 110




Analyses Result




2,4,5-Trichlorophenol 07/05/20110.410 3.902.43 62.3 29.220 3.266


2,4-Dimethylphenol 07/05/20110.586 3.902.12 54.4 21.510 2.633

2,4-Dinitrophenol 07/05/20111.17 3.902.60 66.5 33.810 3.653

2,4-Dinitrotoluene 07/05/20110.410 1.961.46 74.7 35.050 2.082

2-Chlorophenol 07/05/20110.586 3.901.85 47.4 30.530 2.518


4-Nitrophenol 07/05/20110.410 3.903.38 86.5 28.740 4.510

Diethyl phthalate 07/05/20110.586 3.902.51 64.4 30.310 3.413

Dimethyl phthalate S 07/05/20110.410 3.902.21 56.6 34.080 3.115

Di-n-butyl phthalate 07/05/20110.410 1.961.23 63.0 35.930 1.772

Hexachlorobenzene S 07/05/20110.410 3.902.14 54.9 37.610 3.134

Page 50 of 58











Analyses Result


Hexachlorobutadiene 07/05/20110.586 3.901.99 50.9 38.480 2.932


m,p-Cresol 07/05/20110.586 1.961.14 58.5 29.150 1.535

Nitrobenzene S 07/05/20110.586 3.902.01 51.4 32.240 2.776


o-Cresol 07/05/20110.586 1.961.11 56.5 27.880 1.464

Pentachlorophenol 07/05/20112.34 3.902.51 64.3 26.480 3.275

Phenol 07/05/20110.410 3.902.09 53.5 28.350 2.777

Pyridine 07/05/20110.586 3.901.62 41.5 30.730 2.205

Surr: 2,4,6-Tribromophenol 07/05/20111.961.29 65.7


Surr: 2-Fluorophenol 07/05/20111.960.968 49.5


Surr: Phenol-d5 07/05/20111.960.992 50.7


SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS

SampID: MBLK-A110705-1


Analyses Result


1,1,1,2-Tetrachloroethane 07/05/20115.0 ND1,1,1-Trichloroethane 07/05/20115.0 ND1,1,2,2-Tetrachloroethane 07/05/20115.0 ND1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/20115.0 ND1,1,2-Trichloroethane 07/05/20115.0 ND1,1-Dichloro-2-propanone 07/05/201150.0 ND1,1-Dichloroethane 07/05/20115.0 ND1,1-Dichloroethene 07/05/20115.0 ND1,1-Dichloropropene 07/05/20115.0 ND1,2,3-Trichlorobenzene 07/05/20115.0 ND1,2,3-Trichloropropane 07/05/201110 ND1,2,3-Trimethylbenzene 07/05/20115.0 ND1,2,4-Trichlorobenzene 07/05/20115.0 ND1,2,4-Trimethylbenzene 07/05/20115.0 ND1,2-Dibromo-3-chloropropane 07/05/20115.0 ND1,2-Dibromoethane 07/05/20115.0 ND1,2-Dichlorobenzene 07/05/20115.0 ND1,2-Dichloroethane 07/05/20115.0 ND1,2-Dichloropropane 07/05/20115.0 ND1,3,5-Trimethylbenzene 07/05/20115.0 ND1,3-Dichlorobenzene 07/05/20115.0 ND1,3-Dichloropropane 07/05/20115.0 ND1,4-Dichlorobenzene 07/05/20115.0 ND1-Chlorobutane 07/05/20115.0 ND2,2-Dichloropropane 07/05/20115.0 ND2-Butanone 07/05/201150.0 ND

Page 51 of 58











Analyses Result


2-Chlorotoluene 07/05/20115.0 ND2-Hexanone 07/05/201150.0 ND2-Nitropropane 07/05/201150.0 ND4-Chlorotoluene 07/05/20115.0 ND4-Methyl-2-pentanone 07/05/201150.0 NDAcetone 07/05/201150.0 NDAcrolein 07/05/2011100 NDAcrylonitrile 07/05/201110 NDAllyl chloride 07/05/20115.0 NDBenzene 07/05/20111.0 NDBromobenzene 07/05/20115.0 NDBromochloromethane 07/05/20115.0 NDBromodichloromethane 07/05/20115.0 NDBromoform 07/05/20115.0 NDBromomethane 07/05/201110 NDCarbon disulfide 07/05/20115.0 NDCarbon tetrachloride 07/05/20115.0 NDChlorobenzene 07/05/20115.0 NDChloroethane 07/05/201110 NDChloroform 07/05/20115.0 NDChloromethane 07/05/201110 NDcis-1,2-Dichloroethene 07/05/20115.0 NDcis-1,3-Dichloropropene 07/05/20114.0 NDCyclohexanone 07/05/2011100 NDDibromochloromethane 07/05/20115.0 NDDibromomethane 07/05/20115.0 NDDichlorodifluoromethane 07/05/201110 NDEthyl acetate 07/05/201150.0 NDEthyl ether 07/05/20115.0 NDEthyl methacrylate 07/05/20115.0 NDEthylbenzene 07/05/20115.0 NDHeptane 07/05/201120.0 NDHexachlorobutadiene 07/05/20115.0 NDHexachloroethane 07/05/20115.0 NDIodomethane 07/05/201110 NDIsopropylbenzene 07/05/20115.0 NDm,p-Xylenes 07/05/20115.0 NDMethacrylonitrile 07/05/201150.0 NDMethyl Methacrylate 07/05/20115.0 NDMethyl tert-butyl ether 07/05/20112.0 NDMethylacrylate 07/05/201110 NDMethylene chloride J 07/05/20115.0 2.2Naphthalene 07/05/201110 NDn-Butylbenzene 07/05/20115.0 NDn-Hexane 07/05/201120.0 NDNitrobenzene 07/05/2011100 NDn-Propylbenzene 07/05/20115.0 ND

Page 52 of 58











Analyses Result


o-Xylene 07/05/20115.0 NDPentachloroethane 07/05/20115.0 NDp-Isopropyltoluene 07/05/20115.0 NDPropionitrile 07/05/201150.0 NDsec-Butylbenzene 07/05/20115.0 NDStyrene 07/05/20115.0 NDtert-Butylbenzene 07/05/20115.0 NDTetrachloroethene 07/05/20115.0 NDTetrahydrofuran 07/05/201150.0 NDToluene 07/05/20115.0 NDtrans-1,2-Dichloroethene 07/05/20115.0 NDtrans-1,3-Dichloropropene 07/05/20114.0 NDTrichloroethene 07/05/20115.0 NDTrichlorofluoromethane 07/05/20115.0 NDVinyl acetate 07/05/201150.0 NDVinyl chloride 07/05/20112.0 ND Surr: 1,2-Dichloroethane-d4 07/05/201150.053.3 106.7 72.2 131

Surr: 4-Bromofluorobenzene 07/05/201150.051.8 103.5 82.1 116

Surr: Dibromofluoromethane 07/05/201150.050.7 101.3 77.7 120

Surr: Toluene-d8 07/05/201150.048.1 96.2 86 116

SampID: LCS-A110705-1


Analyses Result


1,1,1,2-Tetrachloroethane 07/05/20115.0 50.052.7 105.40 0 200

1,1,1-Trichloroethane 07/05/20115.0 50.055.0 109.90 85.6 124


1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/20115.0 50.057.6 115.10 0 200

1,1,2-Trichloroethane 07/05/20115.0 50.051.0 102.00 0 200

1,1-Dichloro-2-propanone 07/05/201150.0 125124 99.20 0 200

1,1-Dichloroethane 07/05/20115.0 50.053.6 107.20 0 200

1,1-Dichloroethene 07/05/20115.0 50.056.5 112.90 60.1 131

1,1-Dichloropropene 07/05/20115.0 50.054.9 109.70 0 200

1,2,3-Trichlorobenzene 07/05/20115.0 50.051.8 103.70 0 200

1,2,3-Trichloropropane 07/05/201110 50.048.7 97.40 0 200

1,2,3-Trimethylbenzene 07/05/20115.0 50.051.2 102.50 0 200



1,2-Dibromo-3-chloropropane 07/05/20115.0 50.049.1 98.30 0 200

1,2-Dibromoethane 07/05/20115.0 50.051.4 102.70 86.9 119

1,2-Dichlorobenzene 07/05/20115.0 50.052.2 104.30 88 119

1,2-Dichloroethane 07/05/20115.0 50.052.7 105.50 73 117

1,2-Dichloropropane 07/05/20115.0 50.053.4 106.90 0 200


1,3-Dichlorobenzene 07/05/20115.0 50.054.7 109.40 85.8 125



Page 53 of 58











Analyses Result


1-Chlorobutane 07/05/20115.0 50.052.0 104.10 0 200


2-Butanone 07/05/201150.0 125124 99.60 45.3 136

2-Chlorotoluene 07/05/20115.0 50.051.6 103.20 0 200

2-Hexanone 07/05/201150.0 125125 100.30 0 200

2-Nitropropane 07/05/201150.0 500550 109.90 0 200

4-Chlorotoluene 07/05/20115.0 50.052.5 105.00 0 200

4-Methyl-2-pentanone 07/05/201150.0 125123 98.70 0 200

Acetone 07/05/201150.0 125159 126.90 0 200

Acrylonitrile 07/05/201110 50.049.8 99.50 0 200

Allyl chloride 07/05/20115.0 50.052.4 104.70 0 200

Benzene 07/05/20111.0 50.051.4 102.90 73.9 109

Bromobenzene 07/05/20115.0 50.051.5 103.00 0 200

Bromochloromethane 07/05/20115.0 50.051.6 103.20 0 200

Bromodichloromethane 07/05/20115.0 50.054.1 108.20 91.3 126

Bromoform 07/05/20115.0 50.056.1 112.20 0 200

Bromomethane 07/05/201110 50.046.4 92.80 0 200

Carbon disulfide 07/05/20115.0 50.057.0 114.10 0 200

Carbon tetrachloride 07/05/20115.0 50.056.9 113.70 83.3 127

Chlorobenzene 07/05/20115.0 50.052.1 104.10 85.8 116

Chloroethane 07/05/201110 50.045.9 91.90 0 200

Chloroform 07/05/20115.0 50.052.3 104.60 80 113

Chloromethane 07/05/201110 50.042.9 85.80 0 200

cis-1,2-Dichloroethene 07/05/20115.0 50.052.3 104.60 0 200

cis-1,3-Dichloropropene 07/05/20114.0 50.056.8 113.50 0 200

Cyclohexanone 07/05/2011100 250252 100.60 0 200

Dibromochloromethane 07/05/20115.0 50.055.7 111.40 89.1 119

Dibromomethane 07/05/20115.0 50.052.6 105.20 0 200

Dichlorodifluoromethane 07/05/201110 50.080.1 160.20 0 200

Ethyl acetate J 07/05/201150.0 50.050 99.00 0 200

Ethyl ether 07/05/20115.0 50.054.2 108.50 0 200

Ethyl methacrylate 07/05/20115.0 50.051.2 102.40 0 200

Ethylbenzene 07/05/20115.0 50.050.9 101.90 84.1 115

Heptane 07/05/201120.0 50.053.8 107.50 0 200

Hexachlorobutadiene 07/05/20115.0 50.050.4 100.80 0 200

Hexachloroethane 07/05/20115.0 50.054.5 108.90 0 200

Iodomethane 07/05/201110 50.056.9 113.90 0 200

Isopropylbenzene 07/05/20115.0 50.052.1 104.20 0 200

m,p-Xylenes 07/05/20115.0 100102 101.80 79.1 111

Methacrylonitrile 07/05/201150.0 50.050.5 101.00 0 200

Methyl Methacrylate 07/05/20115.0 50.051.8 103.60 0 200

Methyl tert-butyl ether 07/05/20112.0 50.054.2 108.30 80 128

Methylacrylate 07/05/201110 50.050.4 100.70 0 200

Methylene chloride 07/05/20115.0 50.055.4 110.90 73.9 116

Naphthalene 07/05/201110 50.045.6 91.20 73.1 135

n-Butylbenzene 07/05/20115.0 50.059.3 118.60 0 200

n-Hexane 07/05/201120.0 50.055.8 111.60 0 200

Page 54 of 58











Analyses Result


Nitrobenzene 07/05/2011100 500451 90.30 0 200

n-Propylbenzene 07/05/20115.0 50.052.6 105.20 0 200

o-Xylene 07/05/20115.0 50.050.7 101.30 82 117

Pentachloroethane 07/05/20115.0 50.057.3 114.70 0 200

p-Isopropyltoluene 07/05/20115.0 50.055.3 110.50 0 200

Propionitrile 07/05/201150.0 500493 98.70 0 200

sec-Butylbenzene 07/05/20115.0 50.052.2 104.50 0 200

Styrene 07/05/20115.0 50.052.5 104.90 0 200

tert-Butylbenzene 07/05/20115.0 50.050.8 101.60 0 200

Tetrachloroethene 07/05/20115.0 50.052.2 104.40 74.6 115

Tetrahydrofuran J 07/05/201150.0 50.046 91.00 0 200

Toluene 07/05/20115.0 50.049.3 98.60 79.1 112

trans-1,2-Dichloroethene 07/05/20115.0 50.055.1 110.10 0 200

trans-1,3-Dichloropropene 07/05/20114.0 50.053.8 107.50 0 200

Trichloroethene S 07/05/20115.0 50.055.9 111.80 81 111

Trichlorofluoromethane 07/05/20115.0 50.055.1 110.20 0 200

Vinyl acetate 07/05/201150.0 50.054.5 109.10 0 200

Vinyl chloride 07/05/20112.0 50.049.2 98.30 0 200

Surr: 1,2-Dichloroethane-d4 07/05/201150.049.8 99.7 72.2 131



Surr: Toluene-d8 07/05/201150.048.5 97.0 86 116

SampID: LCSD-A110705-1

SampType: LCSD µg/KgUnits69368Batch RPD Limit 40

Analyses Result


1,1,1,2-Tetrachloroethane 07/05/20115.0 50.050.1 100.2 5.080 52.72

1,1,1-Trichloroethane 07/05/20115.0 50.052.6 105.2 4.410 54.97


1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/20115.0 50.054.4 108.9 5.590 57.57


1,1-Dichloro-2-propanone 07/05/201150.0 125128 102.7 3.420 124.1

1,1-Dichloroethane 07/05/20115.0 50.052.1 104.1 2.900 53.59

1,1-Dichloroethene 07/05/20115.0 50.054.3 108.6 3.880 56.47

1,1-Dichloropropene 07/05/20115.0 50.053.3 106.7 2.830 54.87


1,2,3-Trichloropropane 07/05/201110 50.047.6 95.3 2.200 48.70

1,2,3-Trimethylbenzene 07/05/20115.0 50.049.9 99.8 2.650 51.25



1,2-Dibromo-3-chloropropane 07/05/20115.0 50.053.3 106.6 8.100 49.13

1,2-Dibromoethane 07/05/20115.0 50.050.2 100.5 2.240 51.37


1,2-Dichloroethane 07/05/20115.0 50.051.2 102.5 2.870 52.73

1,2-Dichloropropane 07/05/20115.0 50.052.1 104.2 2.520 53.44



Page 55 of 58











Analyses Result




1-Chlorobutane 07/05/20115.0 50.048.8 97.6 6.400 52.05


2-Butanone 07/05/201150.0 125123 98.6 1.040 124.5

2-Chlorotoluene 07/05/20115.0 50.050.6 101.3 1.840 51.58

2-Hexanone 07/05/201150.0 125124 99.3 0.990 125.4

2-Nitropropane 07/05/201150.0 500550 109.9 0.010 549.6

4-Chlorotoluene 07/05/20115.0 50.051.0 102.1 2.820 52.50

4-Methyl-2-pentanone 07/05/201150.0 125125 100 1.360 123.3

Acetone 07/05/201150.0 125153 122.8 3.290 158.6

Acrylonitrile 07/05/201110 50.048.6 97.3 2.260 49.75

Allyl chloride 07/05/20115.0 50.050.8 101.5 3.100 52.35

Benzene 07/05/20111.0 50.050.6 101.2 1.650 51.43

Bromobenzene 07/05/20115.0 50.049.9 99.8 3.100 51.49

Bromochloromethane 07/05/20115.0 50.051.3 102.6 0.640 51.62

Bromodichloromethane 07/05/20115.0 50.053.2 106.3 1.730 54.08

Bromoform 07/05/20115.0 50.054.3 108.5 3.330 56.10

Bromomethane 07/05/201110 50.051.0 102.0 9.400 46.41

Carbon disulfide 07/05/20115.0 50.054.8 109.6 3.970 57.04

Carbon tetrachloride 07/05/20115.0 50.054.7 109.5 3.820 56.86

Chlorobenzene 07/05/20115.0 50.051.1 102.2 1.880 52.07

Chloroethane 07/05/201110 50.048.7 97.4 5.830 45.93

Chloroform 07/05/20115.0 50.050.8 101.5 3.010 52.31

Chloromethane 07/05/201110 50.038.3 76.6 11.340 42.88

cis-1,2-Dichloroethene 07/05/20115.0 50.051.1 102.2 2.300 52.28

cis-1,3-Dichloropropene 07/05/20114.0 50.055.4 110.8 2.440 56.77

Cyclohexanone 07/05/2011100 250248 99.1 1.490 251.5

Dibromochloromethane 07/05/20115.0 50.053.7 107.4 3.660 55.71

Dibromomethane 07/05/20115.0 50.052.5 105.1 0.150 52.61

Dichlorodifluoromethane 07/05/201110 50.076.2 152.4 4.980 80.08

Ethyl acetate J 07/05/201150.0 50.048 97.0 0.000 49.48

Ethyl ether 07/05/20115.0 50.051.6 103.2 5.010 54.24

Ethyl methacrylate 07/05/20115.0 50.049.9 99.9 2.470 51.19

Ethylbenzene 07/05/20115.0 50.050.5 100.9 0.910 50.93

Heptane 07/05/201120.0 50.052.7 105.4 2.010 53.76



Iodomethane 07/05/201110 50.057.0 114.0 0.110 56.94

Isopropylbenzene 07/05/20115.0 50.051.0 102.1 2.070 52.12

m,p-Xylenes 07/05/20115.0 100101 100.9 0.920 101.8

Methacrylonitrile 07/05/201150.0 50.050.7 101.4 0.430 50.49

Methyl Methacrylate 07/05/20115.0 50.051.5 103.0 0.500 51.78

Methyl tert-butyl ether 07/05/20112.0 50.051.9 103.8 4.240 54.17

Methylacrylate 07/05/201110 50.050.3 100.6 0.180 50.37

Methylene chloride 07/05/20115.0 50.053.3 106.7 3.860 55.43

Naphthalene 07/05/201110 50.053.9 107.7 16.630 45.59

Page 56 of 58











Analyses Result


n-Butylbenzene 07/05/20115.0 50.056.7 113.4 4.430 59.28

n-Hexane 07/05/201120.0 50.054.0 108.1 3.220 55.80

Nitrobenzene 07/05/2011100 500518 103.7 13.840 451.3

n-Propylbenzene 07/05/20115.0 50.051.4 102.8 2.270 52.60

o-Xylene 07/05/20115.0 50.050.4 100.7 0.630 50.67

Pentachloroethane 07/05/20115.0 50.055.7 111.3 2.960 57.33

p-Isopropyltoluene 07/05/20115.0 50.053.8 107.6 2.680 55.26

Propionitrile 07/05/201150.0 500508 101.7 2.990 493.4

sec-Butylbenzene 07/05/20115.0 50.051.0 102.0 2.400 52.23

Styrene 07/05/20115.0 50.052.0 103.9 0.980 52.46

tert-Butylbenzene 07/05/20115.0 50.049.6 99.2 2.390 50.79

Tetrachloroethene 07/05/20115.0 50.051.5 103.0 1.410 52.21

Tetrahydrofuran J 07/05/201150.0 50.047 94.3 0.000 45.48

Toluene 07/05/20115.0 50.047.9 95.8 2.840 49.28

trans-1,2-Dichloroethene 07/05/20115.0 50.052.8 105.6 4.230 55.07

trans-1,3-Dichloropropene 07/05/20114.0 50.052.0 104.0 3.330 53.77

Trichloroethene 07/05/20115.0 50.054.3 108.6 2.940 55.90

Trichlorofluoromethane 07/05/20115.0 50.057.9 115.8 4.940 55.10

Vinyl acetate 07/05/201150.0 50.053.4 106.8 2.110 54.53

Vinyl chloride 07/05/20112.0 50.047.8 95.6 2.760 49.16

Surr: 1,2-Dichloroethane-d4 07/05/201150.050.3 100.6

Surr: 4-Bromofluorobenzene 07/05/201150.051.4 102.9

Surr: Dibromofluoromethane 07/05/201150.050.4 100.8

Surr: Toluene-d8 07/05/201150.048.5 97.0

Page 57 of 58


Receiving Check List






Received By: BSJCarrier: Michael Flora


On:

01-Jul-11

On:

01-Jul-11










Temp °C 5.4



Water - vials have zero headspace? Yes No No VOA vials





Pages to follow:


Timothy W. Mathis Elizabeth A. Hurley

Page 58 of 58


ANALYTICAL REPORT

July 13, 2011

Page 1 of 9Work Order: 11G0118

Project :

Project Number:

Subcontract - HW Project

11070042

Report To

Heather White

Teklab, Inc.

Collinsville, IL 62234

5445 Horseshoe Lake Road

Work Order Information

Date Received: 07/06/2011 10:15AM

Collector:

Phone: (618) 344-1004

PO Number: 16845

Analyte Result MRL Batch Method Analyst Analyzed Qualifier

11070042-001 06/29/11 16:00Collected: 11G0118-01 Matrix:Soil

Dalapon mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

Dicamba mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

2,4-D mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

Chloramben mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

2,4-DB mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

Bentazon mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

Picloram mg/kg dry EPPEPA 8151A0.05 07/11/11 16:55<0.05 1G10638

Dinoseb mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

DCPA mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638

Surrogate: 2,5-Dichlorobenzoic Acid 71.7 % 24-140 07/11/11 17:42EPP

0.1%% Solids SM 2540 G MAV 07/11/11 11:5578.5 1G10803









The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in

its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234

Work Order: 11G0118

July 13, 2011

Page 2 of 9












0.1%% Solids SM 2540 G MAV 07/11/11 11:5581.4 1G10803


















0.1%% Solids SM 2540 G MAV 07/11/11 11:5583.1 1G10803













Newton, IA 50208


Work Order: 11G0118

July 13, 2011

Page 3 of 9











0.1%% Solids SM 2540 G MAV 07/11/11 11:5586.4 1G10803


















0.1%% Solids SM 2540 G MAV 07/11/11 11:5587.7 1G10803




Newton, IA 50208


Work Order: 11G0118

July 13, 2011

Page 4 of 9

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte

Determination of Chlorinated Phenoxy Herbicides - Quality Control

Keystone Laboratories, Inc. - Newton

Batch 1G10638 - EPA 3550B

Blank (1G10638-BLK1) Prepared: 07/06/11 Analyzed: 07/11/11

mg/kg wet 0.0760000 24-140Surrogate: 2,5-Dichlorobenzoic Acid 43.60.0332

Dalapon "ND 0.05

3,5-Dichlorobenzoic acid "ND 0.05

Dicamba "ND 0.05

Dichlorprop "ND 0.05

2,4-D "ND 0.05

Pentachlorophenol "ND 0.05

2,4,5-TP (Silvex) "ND 0.05

Chloramben "ND 0.05

2,4,5-T "ND 0.05

2,4-DB "ND 0.05

Bentazon "ND 0.05

Picloram "ND 0.05

Dinoseb "ND 0.05

DCPA "ND 0.05

Acifluorfen "ND 0.05

LCS (1G10638-BS1) Prepared: 07/06/11 Analyzed: 07/11/11


Dalapon "0.088 0.05 0.208000 10-9342.3

3,5-Dichlorobenzoic acid "0.008 0.05 0.0160000 QS-0153-12952.1

Dicamba "0.013 0.05 0.0160000 38-12382.3

Dichlorprop "0.022 0.05 0.0480000 31-12744.8

2,4-D "0.019 0.05 0.0320000 23-12759.4

Pentachlorophenol "0.009 0.05 0.0160000 10-9357.3

2,4,5-TP (Silvex) "0.008 0.05 0.0160000 35-11647.9

Chloramben "0.011 0.05 0.0160000 10-9468.8

2,4,5-T "0.003 0.05 0.0160000 QS-0126-10416.7

2,4-DB "0.100 0.05 0.128000 42-12277.9

Bentazon "0.024 0.05 0.0320000 42-13374.5

Picloram "0.011 0.05 0.0160000 19-15766.7

Dinoseb "0.004 0.05 0.0320000 10-9011.5

DCPA "0.016 0.05 0.0160000 10-11796.9

Acifluorfen "0.008 0.05 0.0160000 24-11353.1




Newton, IA 50208


Work Order: 11G0118

July 13, 2011

Page 5 of 9

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte




Matrix Spike (1G10638-MS1) Prepared: 07/06/11 Analyzed: 07/11/11 Source: 11G0118-03

mg/kg dry 0.0905046 24-140Surrogate: 2,5-Dichlorobenzoic Acid 62.10.0562

Dalapon "0.186 0.05 0.247697 ND 19-15675.0

3,5-Dichlorobenzoic acid "0.017 0.05 0.0190536 ND 38.9-18191.7

Dicamba "0.019 0.05 0.0190536 ND 40-15399.0

Dichlorprop "0.034 0.05 0.0571608 ND 19.6-13859.7

2,4-D "0.021 0.05 0.0381072 ND 10-14654.7

Pentachlorophenol "0.013 0.05 0.0190536 ND 16-12770.8

2,4,5-TP (Silvex) "0.013 0.05 0.0190536 ND 31.2-15970.8

Chloramben "0.015 0.05 0.0190536 ND 10-13380.2

2,4,5-T "0.005 0.05 0.0190536 ND 16.4-15228.1

2,4-DB "0.174 0.05 0.152429 ND 35.3-156114

Bentazon "0.031 0.05 0.0381072 ND 10-15082.3

Picloram "0.015 0.05 0.0190536 ND 45-14679.2

Dinoseb "0.011 0.05 0.0381072 ND 10-9027.6

DCPA "0.019 0.05 0.0190536 ND 10-15197.9

Acifluorfen "0.013 0.05 0.0190536 ND 10-16166.7

Matrix Spike Dup (1G10638-MSD1) Prepared: 07/06/11 Analyzed: 07/11/11 Source: 11G0118-03


Dalapon "0.221 0.05 0.249093 ND 3019-15688.6 17.2

3,5-Dichlorobenzoic acid "0.017 0.05 0.0191610 ND 3038.9-18186.5 5.29

Dicamba "0.020 0.05 0.0191610 ND 3040-153106 7.67

Dichlorprop "0.038 0.05 0.0574830 ND 3019.6-13866.0 10.5

2,4-D "0.040 0.05 0.0383220 ND 30 QR-0210-146104 62.8

Pentachlorophenol "0.015 0.05 0.0191610 ND 3016-12780.2 13.0

2,4,5-TP (Silvex) "0.017 0.05 0.0191610 ND 3031.2-15986.5 20.4

Chloramben "0.017 0.05 0.0191610 ND 3010-13389.6 11.6

2,4,5-T "0.007 0.05 0.0191610 ND 3016.4-15234.4 20.6

2,4-DB "0.160 0.05 0.153288 ND 3035.3-156104 8.85

Bentazon "0.033 0.05 0.0383220 ND 3010-15084.9 3.68

Picloram "0.015 0.05 0.0191610 ND 3045-14680.2 1.87

Dinoseb "0.016 0.05 0.0383220 ND 30 QR-0210-9041.7 41.1

DCPA "0.025 0.05 0.0191610 ND 3010-151130 28.9

Acifluorfen "0.015 0.05 0.0191610 ND 3010-16180.2 19.0




Newton, IA 50208


Work Order: 11G0118

July 13, 2011

Page 6 of 9

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte




Reference (1G10638-SRM1) Prepared: 07/06/11 Analyzed: 07/12/11


Dalapon "0.208 0.05 0.208000 70-13099.8

3,5-Dichlorobenzoic acid "0.015 0.05 0.0160000 70-13092.7

Dicamba "0.018 0.05 0.0160000 70-130109

Dichlorprop "0.049 0.05 0.0480000 70-130101

2,4-D "0.032 0.05 0.0320000 70-130100


2,4,5-TP (Silvex) "0.016 0.05 0.0160000 70-13097.9

Chloramben "0.022 0.05 0.0160000 QR-0570-130134

2,4,5-T "0.012 0.05 0.0160000 70-13076.0

2,4-DB "0.138 0.05 0.128000 70-130108

Bentazon "0.035 0.05 0.0320000 70-130108

Picloram "0.018 0.05 0.0160000 70-130111

Dinoseb "0.043 0.05 0.0320000 QR-0570-130134

DCPA "0.020 0.05 0.0160000 70-130123

Acifluorfen "0.013 0.05 0.0160000 70-13079.2




Newton, IA 50208


Work Order: 11G0118

July 13, 2011

Page 7 of 9

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte

Determination of Conventional Chemistry Parameters - Quality Control


Batch 1G10803 - Wet Chem Preparation

Duplicate (1G10803-DUP1) Prepared: 07/08/11 Analyzed: 07/11/11 Source: 11G0118-05

% Solids %86.7 0.1 87.7 201.11

ND = Non Detect; REC= Recovery; RPD= Relative Percent Difference

Certified Analyses included in this Report

CertificationsAnalyteMethod/Matrix

EPA 8151A in Soil

KS-NT,NELACDalapon

KS-NT,NELAC,SIA1XDicamba

NELACDichlorprop

KS-NT,NELAC,SIA1X2,4-D

KS-NT,NELAC,SIA1X2,4,5-TP (Silvex)

KS-NT,NELAC2,4,5-T

NELAC2,4-DB

KS-NT,NELACPicloram

KS-NT,NELACDinoseb

SIA1XAcifluorfen

SM 2540 G in Soil

SIA1X% Solids

Description Number ExpiresCode

E-10110Kansas Department of Health and Environment-KC 04/30/2012KS-KC

E-10287Kansas Department of Health and Environment 10/30/2011KS-NT

140Missouri Department of Natural Resources 04/30/2012MO-KC

IA001New Jersey Department of Environmental Protection 06/30/2011NELAC

95Iowa Department of Natural Resources 02/01/2012SIA1X




Newton, IA 50208


Work Order: 11G0118

July 13, 2011

Page 8 of 9

Notes and Definitions

QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC

batch were accepted based on percent recoveries and completeness of QC data.

QR-05 The reference standard was outside of established control limits. The batch was accepted based on acceptable LCS, MS/MSD

and RPD results.

QS-01 The blank spike recovery and/or blank spike duplicate recovery were outside the established acceptance limits. Batch was

accepted based on acceptable MS/MSD/RPD results.

End of Report

Christine Dawson

Project Manager

Keystone Laboratories, Inc.




Newton, IA 50208


Work Order: 11G0118

July 13, 2011

Page 9 of 9

COC Goes Here




Newton, IA 50208


July 29, 2011


RE:

Dear Pete Sazama:






Sincerely,


(618) 281-7173(618) 281-5120

TEL:FAX:



Page 1 of 104



Report Contents






Cover Letter 1

Report Contents 2

Definitions 3

Case Narrative 4


Sample Summary 59

Dates Report 60


Receiving Check List 104


Page 2 of 104


____TeklabHdrP

Definitions








DNI Did not ignite










MW Molecular weight











J - Analyte detected below quantitation limits M - Manual Integration used to determine area response

ND - Not Detected at the Reporting Limit R - RPD outside accepted recovery limits

S - Spike Recovery outside recovery limits X - Value exceeds Maximum Contaminant Level

Page 3 of 104


AbbrDefinition

CCVContinuing

Case Narrative







Herbicide analysis performed by Keystone Laboratories, Inc. See attached report for QC data.



____________________________________Collinsville



Phone (618) 344-1004

Fax (618) 344-1005


____________________________________Springfield



Phone (217) 698-1004

Fax (217) 698-1005


____________________________________Kansas City


Lenexa, KS 66214

Phone (913) 541-1998

Fax (913) 541-1998











Page 4 of 104


TeklabHdrP

Laboratory Results








Lab ID: 11070610-001 Client Sample ID: SBA-N4 (5-6)

Matrix: SOLID

Batch



SW-846 9012A (TOTAL)Cyanide 07/19/2011 10:260.34 mg/Kg-dry 1< 0.34NELAP 69687

SW-846 3050B, 6010B, METALS BY ICPAluminum S 07/19/2011 12:214.90 mg/Kg-dry 118100NELAP 69636

Antimony 07/27/2011 11:534.72 mg/Kg-dry 1< 4.72NELAP 69908

Arsenic 07/19/2011 12:212.45 mg/Kg-dry 19.26NELAP 69636


Beryllium 07/19/2011 12:210.10 mg/Kg-dry 10.69NELAP 69636


Calcium S 07/28/2011 12:544.72 mg/Kg-dry 142300NELAP 69954


Cobalt 07/19/2011 12:210.98 mg/Kg-dry 110.2NELAP 69636

Copper 07/28/2011 12:540.94 mg/Kg-dry 115.4NELAP 69954

Iron S 07/19/2011 12:211.96 mg/Kg-dry 126800NELAP 69636


Magnesium S 07/19/2011 12:210.98 mg/Kg-dry 113600NELAP 69636

Manganese S 07/19/2011 12:210.49 mg/Kg-dry 1760NELAP 69636

Nickel 07/20/2011 15:010.98 mg/Kg-dry 119.2NELAP 69636

Potassium S 07/20/2011 15:019.80 mg/Kg-dry 12230NELAP 69636


Sodium 07/20/2011 15:014.90 mg/Kg-dry 1256NELAP 69636

Vanadium 07/20/2011 15:010.98 mg/Kg-dry 132.1NELAP 69636

Zinc 07/27/2011 10:450.98 mg/Kg-dry 175.0NELAP 69636

Ca - Sample concentration was greater than 5 times the spike concentration.K - Sample concentration was greater than 5 times the spike concentration.Al, Fe, Mg, Mn - Sample concentration was greater than 5 times the spike concentration.


Thallium 7841 JS 07/28/2011 9:090.189 mg/Kg-dry 10.17NELAP 69639

Tl-Matrix interference present in sample. Verified by Bench Spike


SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/19/2011 17:00164 mg/Kg-dry 25NDNELAP 69637

Kerosene 07/19/2011 17:00164 mg/Kg-dry 25NDNELAP 69637

Mineral Spirits 07/19/2011 17:00164 mg/Kg-dry 25NDNELAP 69637

Motor Oil 07/19/2011 17:00164 mg/Kg-dry 25NDNELAP 69637


Elevated reporting limit(s) due to sample extract composition.

SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/25/2011 21:56219 µg/Kg-dry 100NDNELAP 69671

4,4´-DDE 07/25/2011 21:56219 µg/Kg-dry 100NDNELAP 69671

4,4´-DDT 07/25/2011 21:56219 µg/Kg-dry 100NDNELAP 69671


Page 5 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDAldrin 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671

















Methoxychlor 07/25/2011 21:56219 µg/Kg-dry 100NDNELAP 69671

Toxaphene 07/22/2011 12:57197 µg/Kg-dry 5NDNELAP 69671


























Indeno(1,2,3-cd)pyrene J 07/20/2011 3:050.222 mg/Kg-dry 500.22NELAP 69628

Page 6 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSNaphthalene 07/20/2011 3:050.222 mg/Kg-dry 50NDNELAP 69628





Surr: p-Terphenyl-d14 S 07/20/2011 3:0580.2-138 %REC 5080.0 69628

Surrogate recovery was outside QC limits due to matrix interference.Elevated reporting limit(s) due to sample extract composition.





























Benzidine 07/19/2011 17:5834.5 mg/Kg-dry 25see noteNELAP 69627










Page 7 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSDimethyl phthalate 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627






















Surr: Phenol-d5 07/19/2011 17:5834.9-110 %REC 2575.6 69627


Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.Elevated reporting limit(s) due to sample extract composition.4-Nitrophenol was outside upper QC limits in the LCS. Sample was ND.




















Page 8 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,3,5-Trimethylbenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726



























Chloromethane 07/20/2011 16:469.8 µg/Kg-dry 1151NELAP 69726
















m,p-Xylenes 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726




Page 9 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSMethylacrylate 07/20/2011 16:469.8 µg/Kg-dry 1ND 69726















Tetrahydrofuran J 07/20/2011 16:4648.9 µg/Kg-dry 17.5NELAP 69726



























Surr: DCAA 07/22/2011 21:0624-140 %REC 1105.0 R152491

The LCS/LCSD RPD result exceeded the QC control limits for Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.

Page 10 of 104


TeklabHdrP

Laboratory Results








Lab ID: 11070610-002 Client Sample ID: SBA-K2 (4-5)

Matrix: SOLID

Batch




SW-846 3050B, 6010B, METALS BY ICPAluminum 07/19/2011 12:384.90 mg/Kg-dry 114800NELAP 69636






Calcium 07/19/2011 12:384.90 mg/Kg-dry 143700NELAP 69636




Iron 07/19/2011 12:381.96 mg/Kg-dry 124300NELAP 69636


Magnesium 07/19/2011 12:380.98 mg/Kg-dry 115300NELAP 69636

Manganese 07/19/2011 12:380.49 mg/Kg-dry 1584NELAP 69636


Potassium 07/20/2011 15:189.80 mg/Kg-dry 12520NELAP 69636






Thallium 7841 07/28/2011 9:190.200 mg/Kg-dry 10.358NELAP 69639















Page 11 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDChlordane 07/21/2011 21:453.97 µg/Kg-dry 1NDNELAP 69671

































Benzo(g,h,i)perylene R 07/20/2011 3:410.004 mg/Kg-dry 10.007NELAP 69628












Page 12 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Nitrobenzene-d5 07/20/2011 3:4110-132 %REC 176.3 69628


Surrogate recovery was outside QC limits due to matrix interference.Benzo(g,h,i)perylene RPD for MS/MSD was outside of QC limit due to sample composition.











































Page 13 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorobutadiene 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627


















Surr: Phenol-d5 07/19/2011 10:2534.9-110 %REC 171.8 69627


Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.4-Nitrophenol was outside upper QC limits in the LCS. Sample was ND.

























Page 14 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2,2-Dichloropropane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726

















Carbon disulfide J 07/20/2011 17:164.5 µg/Kg-dry 14.1NELAP 69726
















Heptane J 07/20/2011 17:1617.9 µg/Kg-dry 13.1 69726











Naphthalene 07/20/2011 17:168.9 µg/Kg-dry 1NDNELAP 69726



Page 15 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSNitrobenzene 07/20/2011 17:1689.3 µg/Kg-dry 1NDNELAP 69726










Tetrahydrofuran J 07/20/2011 17:1644.7 µg/Kg-dry 114NELAP 69726

Toluene 07/20/2011 17:164.5 µg/Kg-dry 14.6NELAP 69726


























Surr: DCAA 07/22/2011 21:5324-140 %REC 176.5 R152491


Page 16 of 104


TeklabHdrP

Laboratory Results








Lab ID: 11070610-003 Client Sample ID: SBA-J5 (5-6)

Matrix: SOLID

Batch








































Page 17 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch














































Page 18 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch















































Page 19 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachloroethane 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
















Surr: Phenol-d5 07/19/2011 10:5734.9-110 %REC 170.6 69627





























Page 20 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Chlorotoluene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726






Acrolein 07/20/2011 17:46100 µg/Kg-dry 1NDNELAP 69726

















Cyclohexanone 07/20/2011 17:46100 µg/Kg-dry 1ND 69726






















Nitrobenzene 07/20/2011 17:46100 µg/Kg-dry 1NDNELAP 69726


Page 21 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSo-Xylene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726



































Surr: DCAA 07/22/2011 22:4124-140 %REC 184.2 R152491


Page 22 of 104


TeklabHdrP

Laboratory Results








Lab ID: 11070610-004 Client Sample ID: SBA-H3 (5-6)

Matrix: SOLID

Batch



SW-846 9012A (TOTAL)Cyanide J 07/19/2011 10:260.30 mg/Kg-dry 10.14NELAP 69687


Antimony J 07/27/2011 12:224.46 mg/Kg-dry 12.8NELAP 69908








Copper 07/19/2011 13:000.96 mg/Kg-dry 1155NELAP 69636










Zinc 07/19/2011 13:000.96 mg/Kg-dry 1132NELAP 69636








Surr: n-Tetracontane S 07/19/2011 17:1950.6-140 %REC 500 69637









Page 23 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDbeta-BHC 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671



















SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/20/2011 19:11452 µg/Kg-dry 10NDNELAP 69671

Aroclor 1221 07/20/2011 19:11452 µg/Kg-dry 10NDNELAP 69671








Elevated reporting limit due to sample composition.

















Page 24 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSPyrene 07/20/2011 6:420.411 mg/Kg-dry 1001.65NELAP 69628













































Page 25 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSDi-n-octyl phthalate 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627












Pentachlorophenol 07/20/2011 11:14121 mg/Kg-dry 50NDNELAP 69627








Surr: Phenol-d5 07/20/2011 11:1434.9-110 %REC 5064.6 69627


Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.Elevated reporting limit(s) due to sample extract composition.























Page 26 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,4-Dichlorobenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790















































Page 27 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSn-Butylbenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790























Surr: Toluene-d8 S 07/21/2011 12:2186-116 %REC 1117.4 69790

Surrogate recovery and/or internal standard area was outside QC limits due to matrix interference.
















Surr: DCAA 07/22/2011 23:2824-140 %REC 189.3 R152491


Page 28 of 104


TeklabHdrP

Laboratory Results








Lab ID: 11070610-005 Client Sample ID: SBA-F2 (4-5)

Matrix: SOLID

Batch































Surr: n-Tetracontane S 07/19/2011 17:3750.6-140 %REC 250 69637

Surrogate recovery was outside QC limits due to sample dilution.Elevated reporting limit(s) due to sample extract composition.








Page 29 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch





























SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/20/2011 7:190.004 mg/Kg-dry 10.022NELAP 69628

Acenaphthylene 07/20/2011 7:190.004 mg/Kg-dry 10.085NELAP 69628













Naphthalene 07/20/2011 7:190.004 mg/Kg-dry 10.028NELAP 69628



Page 30 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 2-Fluorobiphenyl 07/20/2011 7:1910-131 %REC 164.6 69628







































Carbazole J 07/19/2011 17:260.647 mg/Kg-dry 10.26 69627







Page 31 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorobutadiene 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627


















Surr: Phenol-d5 07/19/2011 17:2634.9-110 %REC 173.0 69627



























Page 32 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2,2-Dichloropropane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790

2-Butanone J 07/21/2011 13:2047.8 µg/Kg-dry 111NELAP 69790














































Page 33 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSNitrobenzene 07/21/2011 13:2095.6 µg/Kg-dry 1NDNELAP 69790





















Surr: Toluene-d8 S 07/21/2011 13:2086-116 %REC 1120.3 69790

Surrogate recovery and/or internal standard area was outside QC limits due to matrix interference.
















Surr: DCAA 07/23/2011 0:1524-140 %REC 189.3 R152491


Page 34 of 104


TeklabHdrP

Laboratory Results








Lab ID: 11070610-006 Client Sample ID: TSA-02 (8-9)

Matrix: SOLID

Batch





















Sodium 07/20/2011 15:524.72 mg/Kg-dry 155.4NELAP 69636



SW-846 3050B, METALS BY GFAASelenium 7740 J 07/19/2011 10:010.577 mg/Kg-dry 10.52NELAP 69639
















Page 35 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch













Heptachlor epoxide 07/21/2011 23:292.04 µg/Kg-dry 12.29NELAP 69671

































Page 36 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch















































Page 37 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorocyclopentadiene 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627

















Surr: Phenol-d5 07/19/2011 14:1034.9-110 %REC 170.5 69627




























Page 38 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Butanone 07/21/2011 13:4950.8 µg/Kg-dry 1NDNELAP 69790










Benzene 07/21/2011 13:491.0 µg/Kg-dry 1NDNELAP 69790





































Page 39 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSn-Propylbenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790




































Surr: DCAA 07/23/2011 1:0224-140 %REC 163.4 R152491


Page 40 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch








































Page 41 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDChlordane J 07/21/2011 23:554.05 µg/Kg-dry 13.9NELAP 69671










gamma-Chlordane 07/21/2011 23:552.02 µg/Kg-dry 13.89NELAP 69671




















Benzo(a)anthracene J 07/21/2011 4:470.004 mg/Kg-dry 10.004NELAP 69628


Benzo(b)fluoranthene J 07/21/2011 4:470.004 mg/Kg-dry 10.004NELAP 69628













Page 42 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch















































Page 43 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

















Surr: Phenol-d5 07/19/2011 14:4334.9-110 %REC 173.2 69627





























Page 44 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch
















































Page 45 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch










Toluene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790


























Surr: DCAA 07/23/2011 1:5024-140 %REC 176.1 R152491


Page 46 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch






























Motor Oil # 07/19/2011 15:296.13 mg/Kg-dry 17.37NELAP 69637










Page 47 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch














































Page 48 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch















































Page 49 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

















Surr: Phenol-d5 07/19/2011 15:1534.9-110 %REC 171.2 69627





























Page 50 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch
















































Page 51 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch




































Surr: DCAA 07/23/2011 2:3724-140 %REC 153.9 R152491


Page 52 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch
























K - Sample concentration was greater than 5 times the spike concentration.Al, Ca, Fe, Mg, Mn - Sample concentration was greater than 5 times the spike concentration.




SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel # 07/19/2011 16:246.15 mg/Kg-dry 16.19NELAP 69637












Page 53 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch


Chlordane J 07/22/2011 1:394.10 µg/Kg-dry 13.7NELAP 69671










gamma-Chlordane 07/22/2011 1:392.05 µg/Kg-dry 13.68NELAP 69671


































Page 54 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 2-Fluorobiphenyl 07/21/2011 1:5210-131 %REC 168.1 69628














































Page 55 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorocyclopentadiene 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627

















Surr: Phenol-d5 07/19/2011 15:4834.9-110 %REC 171.5 69627




























Page 56 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Butanone 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790






Acetone 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790









































Page 57 of 104


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch

SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSn-Propylbenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790










Toluene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790


























Surr: DCAA 07/23/2011 3:2424-140 %REC 195.0 R152491


Page 58 of 104



TeklabHdrP

Matrix

Sample Summary






11070610-001 SBA-N4 (5-6) 07/13/2011 10:006Solid

11070610-002 SBA-K2 (4-5) 07/13/2011 11:306Solid

11070610-003 SBA-J5 (5-6) 07/13/2011 13:156Solid

11070610-004 SBA-H3 (5-6) 07/13/2011 14:306Solid

11070610-005 SBA-F2 (4-5) 07/13/2011 15:306Solid

11070610-006 TSA-02 (8-9) 07/14/2011 9:456Solid

11070610-007 TSA-01 (5-6) 07/14/2011 10:306Solid

11070610-008 TSA-03 (3-4) 07/14/2011 11:156Solid

11070610-009 TSA-04 (4-5) 07/14/2011 12:006Solid

Page 59 of 104


11070610-001


____TeklabHdrP


Dates Report






11070610-001A SBA-N4 (5-6) 07/13/2011 10:00 7/15/2011 5:03:00 PM







11070610-001B SBA-N4 (5-6) 07/13/2011 10:00 7/15/2011 5:03:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00









SW-846 7471A 07/19/2011 12:2507/18/2011 11:31

SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10

11070610-001C SBA-N4 (5-6) 07/13/2011 10:00 7/15/2011 5:03:00 PM


11070610-001F SBA-N4 (5-6) 07/13/2011 10:00 7/15/2011 5:03:00 PM


11070610-002A SBA-K2 (4-5) 07/13/2011 11:30 7/15/2011 5:03:00 PM







11070610-002B SBA-K2 (4-5) 07/13/2011 11:30 7/15/2011 5:03:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00






Page 60 of 104


11070610-001A


____TeklabHdrP


Dates Report







SW-846 7471A 07/19/2011 12:2507/18/2011 11:31

SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10

11070610-002C SBA-K2 (4-5) 07/13/2011 11:30 7/15/2011 5:03:00 PM


11070610-002F SBA-K2 (4-5) 07/13/2011 11:30 7/15/2011 5:03:00 PM


11070610-003A SBA-J5 (5-6) 07/13/2011 13:15 7/15/2011 5:03:00 PM







11070610-003B SBA-J5 (5-6) 07/13/2011 13:15 7/15/2011 5:03:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00







SW-846 7471A 07/19/2011 12:2507/18/2011 11:31

SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10

11070610-003C SBA-J5 (5-6) 07/13/2011 13:15 7/15/2011 5:03:00 PM


11070610-003F SBA-J5 (5-6) 07/13/2011 13:15 7/15/2011 5:03:00 PM


11070610-004A SBA-H3 (5-6) 07/13/2011 14:30 7/15/2011 5:03:00 PM







11070610-004B SBA-H3 (5-6) 07/13/2011 14:30 7/15/2011 5:03:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00

Page 61 of 104



____TeklabHdrP


Dates Report












SW-846 7471A 07/19/2011 12:2507/18/2011 11:31

SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10

11070610-004C SBA-H3 (5-6) 07/13/2011 14:30 7/15/2011 5:03:00 PM


11070610-004F SBA-H3 (5-6) 07/13/2011 14:30 7/15/2011 5:03:00 PM


11070610-005A SBA-F2 (4-5) 07/13/2011 15:30 7/15/2011 5:03:00 PM







11070610-005B SBA-F2 (4-5) 07/13/2011 15:30 7/15/2011 5:03:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00







SW-846 7471A 07/19/2011 12:2507/18/2011 11:31

SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10

11070610-005C SBA-F2 (4-5) 07/13/2011 15:30 7/15/2011 5:03:00 PM


11070610-005F SBA-F2 (4-5) 07/13/2011 15:30 7/15/2011 5:03:00 PM


11070610-006A TSA-02 (8-9) 07/14/2011 9:45 7/15/2011 5:03:00 PM




Page 62 of 104



____TeklabHdrP


Dates Report









11070610-006B TSA-02 (8-9) 07/14/2011 9:45 7/15/2011 5:03:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00







SW-846 7471A 07/19/2011 12:2507/18/2011 11:31

SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10

11070610-006C TSA-02 (8-9) 07/14/2011 9:45 7/15/2011 5:03:00 PM


11070610-006F TSA-02 (8-9) 07/14/2011 9:45 7/15/2011 5:03:00 PM


11070610-007A TSA-01 (5-6) 07/14/2011 10:30 7/15/2011 5:03:00 PM







11070610-007B TSA-01 (5-6) 07/14/2011 10:30 7/15/2011 5:03:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00








SW-846 7471A 07/19/2011 12:2507/18/2011 11:31

SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10

11070610-007C TSA-01 (5-6) 07/14/2011 10:30 7/15/2011 5:03:00 PM


Page 63 of 104



____TeklabHdrP


Dates Report






11070610-007F TSA-01 (5-6) 07/14/2011 10:30 7/15/2011 5:03:00 PM


11070610-008A TSA-03 (3-4) 07/14/2011 11:15 7/15/2011 5:03:00 PM







11070610-008B TSA-03 (3-4) 07/14/2011 11:15 7/15/2011 5:03:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00








SW-846 7471A 07/19/2011 12:2507/18/2011 11:31

SW-846 9012A (Total) 07/20/2011 7:2407/19/2011 14:00

11070610-008C TSA-03 (3-4) 07/14/2011 11:15 7/15/2011 5:03:00 PM


11070610-008F TSA-03 (3-4) 07/14/2011 11:15 7/15/2011 5:03:00 PM


11070610-009A TSA-04 (4-5) 07/14/2011 12:00 7/15/2011 5:03:00 PM







11070610-009B TSA-04 (4-5) 07/14/2011 12:00 7/15/2011 5:03:00 PM

EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00





Page 64 of 104


11070610-007F


____TeklabHdrP


Dates Report









SW-846 7471A 07/19/2011 12:2507/18/2011 11:31

SW-846 9012A (Total) 07/20/2011 7:2407/19/2011 14:00

11070610-009C TSA-04 (4-5) 07/14/2011 12:00 7/15/2011 5:03:00 PM


11070610-009F TSA-04 (4-5) 07/14/2011 12:00 7/15/2011 5:03:00 PM


Page 65 of 104








STANDARD METHODS 18TH ED. 2540 G

SampID: LCS-R152054

SampType: LCS %UnitsR152054Batch

Analyses Result


Total Solids 07/18/20110.1 1.01.0 99.00 90 110

SampID: LCSQC-R152054

SampType: LCSQC %UnitsR152054Batch

Analyses Result


Total Solids 07/18/20110.1 1.01.0 99.00 90 110

SampID: 11070610-004BDUP

SampType: DUP %UnitsR152054Batch RPD Limit 15

Analyses Result


Total Solids 07/18/20110.1 82.6 0.0882.71


SampID: MB-69687


Analyses Result


Cyanide 07/20/20110.25 < 0.25

SampID: LCS-69687


Analyses Result


Cyanide 07/20/20110.25 1.251.20 96.30 85 115

SampID: 11070610-001BMS


Analyses Result


Cyanide 07/19/20110.33 1.641.71 104.40 75 125



Analyses Result


Cyanide 07/19/20110.33 1.641.52 92.7 11.870 1.712

SampID: MB-R152186


Analyses Result


Cyanide J 07/20/20110.25 0.11

Page 66 of 104









SampID: LCS-R152186


Analyses Result


Cyanide 07/20/20110.25 1.251.33 106.70 85 115


SampID: MB-69636


Analyses Result


Aluminum 07/19/20115.00 5.00< 5.00 00 -100 100

Arsenic 07/19/20112.50 2.50< 2.50 00 -100 100

Barium 07/20/20110.50 0.50< 0.50 00 -100 100

Beryllium 07/19/20110.10 0.10< 0.10 00 -100 100

Cadmium 07/19/20110.20 0.20< 0.20 00 -100 100

Calcium 07/19/20115.00 5.00< 5.00 00 -100 100

Chromium 07/19/20111.00 1.00< 1.00 00 -100 100

Cobalt 07/19/20111.00 1.00< 1.00 00 -100 100

Copper 07/19/20111.00 1.00< 1.00 00 -100 100

Iron 07/19/20112.00 2.00< 2.00 00 -100 100

Lead 07/19/20114.00 4.00< 4.00 00 -100 100

Magnesium 07/19/20111.00 1.00< 1.00 00 -100 100

Manganese 07/19/20110.50 0.50< 0.50 00 -100 100

Nickel 07/19/20111.00 1.00< 1.00 00 -100 100

Potassium 07/20/201110.0 10.0< 10.0 00 -100 100

Silver 07/21/20110.55 0.55< 0.55 00 -100 100

Silver 07/20/20110.55 0.55< 0.55 00 -100 100

Sodium 07/20/20115.00 5.00< 5.00 00 -100 100

Vanadium 07/19/20111.00 1.00< 1.00 00 -100 100

Zinc J 07/19/20111.00 1.000.51 51.00 -100 100

Page 67 of 104









SampID: LCS-69636


Analyses Result


Aluminum 07/19/20115.00 200197 98.60 85 115

Arsenic 07/19/20112.50 200208 103.80 85 115

Barium 07/20/20110.50 200212 106.10 85 115

Beryllium 07/19/20110.10 5.005.08 101.60 85 115

Cadmium 07/19/20110.20 5.005.12 102.40 85 115

Calcium 07/19/20115.00 120121 101.10 85 115

Chromium 07/19/20111.00 20.019.7 98.60 85 115

Cobalt 07/19/20111.00 50.049.7 99.40 85 115

Copper 07/19/20111.00 25.024.5 98.00 85 115

Iron 07/19/20112.00 100102 102.10 85 115

Lead 07/19/20114.00 50.051.6 103.10 85 115

Magnesium 07/19/20111.00 75.079.2 105.60 85 115

Manganese 07/19/20110.50 50.053.5 107.00 85 115

Nickel 07/19/20111.00 50.051.6 103.10 85 115

Potassium 07/20/201110.0 120133 110.80 85 115

Silver 07/21/20110.55 5.004.83 96.60 85 115

Silver 07/20/20110.55 5.005.37 107.40 85 115

Sodium 07/20/20115.00 120131 109.00 85 115

Vanadium 07/19/20111.00 50.045.8 91.70 85 115

Zinc 07/19/20111.00 50.053.0 106.00 85 115

SampID: 11070610-001BMS


Analyses Result


Aluminum S 07/19/20114.90 19618900 425.018100 75 125

Arsenic 07/19/20112.45 196194 94.19.265 75 125

Barium 07/20/20110.49 196296 80.1138.8 75 125

Beryllium 07/19/20110.10 4.905.18 91.60.6863 75 125

Cadmium 07/19/20110.20 4.904.53 83.80.4216 75 125

Chromium 07/20/20110.98 19.639.0 75.624.19 75 125

Cobalt 07/19/20110.98 49.047.9 77.010.21 75 125

Iron S 07/19/20111.96 98.020400 -655026780 75 125

Lead 07/19/20113.92 49.058.8 81.818.72 75 125

Magnesium S 07/19/20110.98 73.514700 149313630 75 125

Manganese S 07/19/20110.49 49.0734 -53.2760.5 75 125

Nickel 07/20/20110.98 49.060.0 83.219.25 75 125

Potassium S 07/20/20119.80 1182550 272.52229 75 125

Silver 07/20/20110.54 4.904.27 87.20 75 125

Sodium 07/20/20114.90 118361 89.2256.1 75 125

Vanadium 07/20/20110.98 49.077.2 91.932.15 75 125

Zinc 07/27/20110.98 49.0120 91.175.05 75 125

Page 68 of 104











Analyses Result


Aluminum S 07/19/20114.90 19619900 920.0 5.0018100 18930

Arsenic 07/19/20112.45 196204 99.3 5.139.265 193.8

Barium 07/20/20110.49 196298 81.4 0.86138.8 295.9

Beryllium 07/19/20110.10 4.905.45 97.2 5.170.6863 5.176

Cadmium 07/19/20110.20 4.904.79 89.2 5.680.4216 4.529

Chromium 07/20/20110.98 19.643.3 97.7 10.5524.19 39.00

Cobalt 07/19/20110.98 49.051.2 83.6 6.5910.21 47.94

Iron S 07/19/20111.96 98.021900 -4940 7.4626780 20360

Lead 07/19/20113.92 49.061.7 87.7 4.8018.72 58.80

Magnesium S 07/19/20110.98 73.516100 3320 8.7213630 14730

Manganese S 07/19/20110.49 49.0652 -220.6 11.83760.5 734.4

Nickel 07/20/20110.98 49.062.9 89.0 4.6419.25 60.04

Potassium S 07/20/20119.80 1182580 295.8 1.072229 2550

Silver 07/20/20110.54 4.904.01 81.8 6.390 4.275

Sodium 07/20/20114.90 118387 111.2 6.92256.1 361.0

Vanadium 07/20/20110.98 49.084.7 107.1 9.1932.15 77.22

Zinc 07/27/20110.98 49.0114 79.3 4.9575.05 119.7

SampID: 11070610-009BMS


Analyses Result


Barium 07/20/20110.46 185319 92.5147.8 75 125

Potassium S 07/20/20119.26 1113010 332.52638 75 125

Silver 07/21/20110.51 4.634.31 93.00 75 125

Sodium 07/20/20114.63 111195 120.660.81 75 125

Vanadium 07/20/20110.93 46.385.8 101.038.99 75 125



Analyses Result


Barium 07/20/20110.46 185326 96.0 2.04147.8 319.1

Potassium S 07/20/20119.26 1113040 365.0 1.192638 3007

Silver 07/21/20110.51 4.634.33 93.6 0.640 4.306

Sodium 07/20/20114.63 111198 123.8 1.8460.81 194.8

Vanadium 07/20/20110.93 46.387.2 104.1 1.6238.99 85.77

SampID: MB-69908


Analyses Result


Antimony 07/27/20115.00 5.00< 5.00 00 -100 100

Page 69 of 104









SampID: LCS-69908


Analyses Result


Antimony 07/27/20115.00 50.051.8 103.70 85 115

SampID: 11070610-002BMS


Analyses Result


Antimony 07/27/20115.00 50.047.8 95.60 75 125



Analyses Result


Antimony 07/27/20115.00 50.048.8 97.5 1.970 47.82

SampID: MB-69954


Analyses Result


Aluminum 07/28/20115.00 5.00< 5.00 00 -100 100

Calcium 07/28/20115.00 5.00< 5.00 00 -100 100

Chromium 07/28/20111.00 1.00< 1.00 00 -100 100

Copper 07/28/20111.00 1.00< 1.00 00 -100 100

Iron 07/28/20112.00 2.00< 2.00 00 -100 100

Manganese 07/28/20110.50 0.50< 0.50 00 -100 100

Potassium 07/28/201110.0 10.0< 10.0 00 -100 100

SampID: LCS-69954


Analyses Result


Aluminum 07/28/20115.00 200191 95.30 85 115

Calcium 07/28/20115.00 120117 97.60 85 115

Chromium 07/28/20111.00 20.019.6 98.00 85 115

Copper 07/28/20111.00 25.024.0 95.80 85 115

Iron 07/28/20112.00 10095.5 95.50 85 115

Manganese 07/28/20110.50 50.047.8 95.50 85 115

Potassium 07/28/201110.0 120117 97.60 85 115

SampID: 11070610-001BMS


Analyses Result


Calcium S 07/28/20114.72 11344200 165842280 75 125

Copper 07/28/20110.94 23.638.0 95.615.41 75 125

Page 70 of 104











Analyses Result


Calcium S 07/28/20114.72 11338300 -3550 14.3142280 44160

Copper 07/28/20110.94 23.636.7 90.2 3.4415.41 37.95

SampID: 11070610-009BMS

SampType: MS mg/Kg-dryUnitsR152096Batch

Analyses Result


Aluminum S 07/19/20114.63 18523400 144520750 75 125

Arsenic 07/19/20112.31 185189 97.68.704 75 125

Beryllium 07/19/20110.09 4.635.37 98.40.8148 75 125

Cadmium 07/19/20110.19 4.634.60 91.60.3611 75 125

Calcium S 07/19/20114.63 1116580 74.26495 75 125

Chromium 07/19/20110.93 18.538.7 94.221.28 75 125

Cobalt 07/19/20110.93 46.350.8 84.411.69 75 125

Copper 07/19/20110.93 23.237.3 89.416.63 75 125

Iron S 07/19/20111.85 92.624600 190.024440 75 125

Lead 07/19/20113.70 46.358.6 88.117.81 75 125

Magnesium S 07/19/20110.93 69.44250 328.04024 75 125

Manganese S 07/19/20110.46 46.3805 -94.4849.1 75 125

Nickel 07/19/20110.93 46.360.8 92.118.12 75 125

Zinc 07/19/20110.93 46.3115 102.267.40 75 125


SampType: MSD mg/Kg-dryUnitsR152096Batch RPD Limit 20

Analyses Result


Aluminum S 07/19/20114.63 18523900 1690 1.9220750 23430

Arsenic 07/19/20112.31 185194 100.0 2.328.704 189.4

Beryllium 07/19/20110.09 4.635.46 100.4 1.710.8148 5.370

Cadmium 07/19/20110.19 4.634.80 95.8 4.140.3611 4.602

Calcium 07/19/20114.63 1116590 87.5 0.226495 6578

Chromium 07/19/20110.93 18.542.0 112.0 8.1721.28 38.72

Cobalt 07/19/20110.93 46.353.3 89.8 4.8411.69 50.75

Copper 07/19/20110.93 23.238.5 94.3 2.9816.63 37.32

Iron S 07/19/20111.85 92.625400 1040 3.1524440 24610

Lead 07/19/20113.70 46.362.5 96.6 6.4517.81 58.62

Magnesium S 07/19/20110.93 69.44330 436.0 1.754024 4252

Manganese S 07/19/20110.46 46.3856 16.0 6.15849.1 805.4

Nickel 07/19/20110.93 46.363.8 98.7 4.9018.12 60.78

Zinc 07/19/20110.93 46.3115 102.4 0.0867.40 114.7

Page 71 of 104









SampID: MB-69639


Analyses Result


Selenium 7740 07/19/20110.600 0.600< 0.600 00 -100 100

Thallium 7841 07/28/20110.200 0.200< 0.200 00 -100 100

SampID: LCS-69639


Analyses Result


Selenium 7740 07/19/20110.600 3.002.81 93.60 80 120

Thallium 7841 07/28/20110.200 1.501.45 96.40 80 120

SampID: 11070610-001BMS


Analyses Result


Selenium 7740 07/20/20111.13 2.832.79 98.60 70 130

Thallium 7841 S 07/28/20110.189 1.422.12 137.90.1661 70 130



Analyses Result


Selenium 7740 07/20/20111.13 2.833.26 115.3 15.580 2.792

Thallium 7841 S 07/28/20110.189 1.422.08 135.2 1.830.1661 2.117

SW-846 7471A

SampID: MB-69631


Analyses Result


Mercury 07/19/20110.010 0.010< 0.010 00 -100 100

SampID: LCS-69631


Analyses Result


Mercury 07/19/20110.010 0.2500.254 101.40 85 115

SampID: 11070610-002BMS


Analyses Result


Mercury 07/19/20110.012 0.2940.396 92.80.1230 75 125



Analyses Result


Mercury 07/19/20110.012 0.2940.391 91.2 1.200.1230 0.3960

Page 72 of 104









SampID: MB-69637


Analyses Result


Diesel 07/19/20115.00 NDKerosene 07/19/20115.00 NDMineral Spirits 07/19/20115.00 NDMotor Oil 07/19/20115.00 ND Surr: n-Tetracontane 07/19/20110.670.52 77.9 54.8 128

SampID: LCS-69637


Analyses Result


Diesel 07/19/20115.00 16.717.7 105.90 40.4 121


SampID: 11070610-006AMS


Analyses Result


Diesel 07/19/20116.13 20.523.0 112.40 20.3 167




Analyses Result


Diesel 07/19/20116.13 20.524.5 119.7 6.380 23.01

Surr: n-Tetracontane 07/19/20110.820.84 102.3

Page 73 of 104









SampID: MB-69671


Analyses Result


4,4´-DDD 07/21/20111.67 ND4,4´-DDE 07/21/20111.67 ND4,4´-DDT 07/21/20111.67 NDAlachlor 07/21/20111.67 NDAldrin 07/21/20111.67 NDalpha-BHC 07/21/20111.67 NDalpha-Chlordane 07/21/20111.67 NDbeta-BHC 07/21/20111.67 NDChlordane 07/21/20113.34 NDdelta-BHC 07/21/20111.67 NDDieldrin 07/21/20111.67 NDEndosulfan I 07/21/20111.67 NDEndosulfan II 07/21/20111.67 NDEndosulfan sulfate 07/21/20111.67 NDEndrin 07/21/20111.67 NDEndrin aldehyde 07/21/20111.67 NDEndrin ketone 07/21/20111.67 NDgamma-BHC 07/21/20111.67 NDgamma-Chlordane 07/21/20111.67 NDHeptachlor 07/21/20111.67 NDHeptachlor epoxide 07/21/20111.67 NDMethoxychlor 07/21/20111.67 NDToxaphene 07/21/201130.0 ND Surr: Decachlorobiphenyl 07/21/20118.337.79 93.6 73.5 150

Surr: Tetrachloro-m-xylene 07/21/20118.335.12 61.5 14.4 113

Page 74 of 104









SampID: LCSPST-69671


Analyses Result


4,4´-DDD 07/21/20111.67 8.337.96 95.50 36 208

4,4´-DDE 07/21/20111.67 8.337.70 92.40 26 191

4,4´-DDT 07/21/20111.67 8.338.48 101.90 3 215

Alachlor 07/21/20111.67 8.335.23 62.80 30 170

Aldrin 07/21/20111.67 8.335.94 71.30 46 173

alpha-BHC 07/21/20111.67 8.336.46 77.50 37 179

alpha-Chlordane 07/21/20111.67 8.337.44 89.30 38 187

beta-BHC 07/21/20111.67 8.336.85 82.20 51 185

delta-BHC 07/21/20111.67 8.337.88 94.60 46 166

Dieldrin 07/21/20111.67 8.337.35 88.30 26 216

Endosulfan I 07/21/20111.67 8.337.35 88.30 31 205

Endosulfan II 07/21/20111.67 8.337.96 95.50 42 187


Endrin 07/21/20111.67 8.337.63 91.60 30 215

Endrin aldehyde 07/21/20111.67 8.338.03 96.40 42 202

Endrin ketone 07/21/20111.67 8.339.00 108.00 19 244

gamma-BHC 07/21/20111.67 8.336.02 72.20 55 166

gamma-Chlordane 07/21/20111.67 8.337.21 86.50 23 186

Heptachlor 07/21/20111.67 8.336.15 73.80 43 172


Methoxychlor 07/21/20111.67 8.338.79 105.50 3 221



Page 75 of 104









SampID: 11070610-008AMS


Analyses Result


4,4´-DDD J 07/26/201120.5 10.28.6 84.00 36 208

4,4´-DDE J 07/26/201120.5 10.29.3 91.10 26 191

4,4´-DDT J 07/26/201120.5 10.29.4 92.10 3 215

Alachlor 07/22/20112.05 10.27.15 70.00 30 170

Aldrin 07/22/20112.05 10.27.95 77.80 46 173

alpha-BHC 07/22/20112.05 10.28.44 82.60 37 179

alpha-Chlordane 07/22/20112.05 10.29.38 91.80 38 187

beta-BHC 07/22/20112.05 10.28.70 85.20 51 185

delta-BHC 07/22/20112.05 10.210.1 99.00 46 166

Dieldrin 07/22/20112.05 10.211.2 89.62.090 26 216

Endosulfan I 07/22/20112.05 10.29.10 89.00 31 205

Endosulfan II 07/22/20112.05 10.29.17 89.80 42 187


Endrin 07/22/20112.05 10.29.26 90.60 30 215

Endrin aldehyde 07/22/20112.05 10.29.43 92.30 42 202

Endrin ketone 07/22/20112.05 10.210.6 104.20 19 244

gamma-BHC 07/22/20112.05 10.28.07 79.00 55 166

gamma-Chlordane 07/22/20112.05 10.210.1 99.30 23 186

Heptachlor 07/22/20112.05 10.28.43 82.60 43 172

Heptachlor epoxide 07/22/20112.05 10.212.3 92.92.853 39 204

Methoxychlor 07/22/20112.05 10.29.61 94.10 3 221



Page 76 of 104











Analyses Result


4,4´-DDD J 07/26/201120.5 10.29.0 87.9 0.000 8.586

4,4´-DDE J 07/26/201120.5 10.210 97.7 0.000 9.310

4,4´-DDT J 07/26/201120.5 10.29.9 96.7 0.000 9.412

Alachlor 07/22/20112.05 10.27.03 68.8 1.720 7.150

Aldrin 07/22/20112.05 10.28.02 78.5 0.940 7.949

alpha-BHC 07/22/20112.05 10.28.31 81.3 1.660 8.445

alpha-Chlordane 07/22/20112.05 10.29.60 94.0 2.380 9.378

beta-BHC 07/22/20112.05 10.28.97 87.8 3.050 8.704

delta-BHC 07/22/20112.05 10.210.5 102.5 3.540 10.11

Dieldrin 07/22/20112.05 10.211.5 91.7 1.932.090 11.24

Endosulfan I 07/22/20112.05 10.29.08 88.8 0.240 9.097

Endosulfan II 07/22/20112.05 10.29.52 93.2 3.720 9.175

Endosulfan sulfate 07/22/20112.05 10.29.49 92.9 4.790 9.044

Endrin 07/22/20112.05 10.29.52 93.2 2.770 9.262

Endrin aldehyde 07/22/20112.05 10.29.70 94.9 2.830 9.428

Endrin ketone 07/22/20112.05 10.211.0 107.2 2.930 10.64

gamma-BHC 07/22/20112.05 10.28.11 79.3 0.480 8.067

gamma-Chlordane 07/22/20112.05 10.210.6 103.5 4.180 10.14

Heptachlor 07/22/20112.05 10.28.60 84.2 1.940 8.435

Heptachlor epoxide 07/22/20112.05 10.212.7 96.0 2.532.853 12.34

Methoxychlor 07/22/20112.05 10.29.88 96.7 2.750 9.610


Surr: Tetrachloro-m-xylene 07/22/201110.25.44 53.2


SampID: MB-69671


Analyses Result


Aroclor 1016 07/20/201137.5 NDAroclor 1221 07/20/201137.5 NDAroclor 1232 07/20/201137.5 NDAroclor 1242 07/20/201137.5 NDAroclor 1248 07/20/201137.5 NDAroclor 1254 07/20/201137.5 NDAroclor 1260 07/20/201137.5 ND Surr: Decachlorobiphenyl 07/20/20118.37.3 88.5 86.4 159


SampID: LCSPCB-69671


Analyses Result


Aroclor 1016 07/20/201137.5 167133 80.00 54.9 121

Aroclor 1260 07/20/201137.5 167156 93.50 65.5 133



Page 77 of 104









SampID: 11070610-007AMS


Analyses Result


Aroclor 1016 07/20/201145.5 202160 79.30 35.8 143

Aroclor 1260 07/20/201145.5 202180 88.90 22.3 152





Analyses Result


Aroclor 1016 07/20/201145.5 202167 82.6 4.120 160.4

Aroclor 1260 07/20/201145.5 202187 92.7 4.080 180.0


Surr: Tetrachloro-meta-xylene 07/20/201110.15.8 57.9


SampID: MB-69628


Analyses Result


Acenaphthene 07/18/20110.003 NDAcenaphthylene 07/18/20110.003 NDAnthracene 07/18/20110.003 NDBenzo(a)anthracene 07/18/20110.003 NDBenzo(a)pyrene 07/18/20110.003 NDBenzo(b)fluoranthene 07/18/20110.003 NDBenzo(g,h,i)perylene 07/18/20110.003 NDBenzo(k)fluoranthene 07/18/20110.003 NDChrysene 07/18/20110.003 NDDibenzo(a,h)anthracene 07/18/20110.003 NDFluoranthene 07/18/20110.003 NDFluorene 07/18/20110.003 NDIndeno(1,2,3-cd)pyrene 07/18/20110.003 NDNaphthalene 07/18/20110.003 NDPhenanthrene 07/18/20110.003 NDPyrene 07/18/20110.003 ND Surr: 2-Fluorobiphenyl 07/18/20110.1670.132 78.8 45.7 89.2



Page 78 of 104









SampID: LCS-69628


Analyses Result


Acenaphthene 07/18/20110.003 0.1670.143 85.40 56.3 115

Acenaphthylene 07/18/20110.003 0.1670.148 88.40 60.3 143

Anthracene 07/18/20110.003 0.1670.139 83.40 52.1 109

Benzo(a)anthracene 07/18/20110.003 0.1670.143 85.60 52.8 112

Benzo(a)pyrene 07/18/20110.003 0.1670.124 74.10 40.8 127


Benzo(g,h,i)perylene 07/18/20110.003 0.1670.166 99.40 52.8 145

Benzo(k)fluoranthene 07/18/20110.003 0.1670.157 93.80 52 153

Chrysene 07/18/20110.003 0.1670.149 89.20 60.8 128


Fluoranthene 07/18/20110.003 0.1670.153 91.80 58.7 125

Fluorene 07/18/20110.003 0.1670.164 98.40 57.8 125

Indeno(1,2,3-cd)pyrene 07/18/20110.003 0.1670.170 102.00 52 147

Naphthalene 07/18/20110.003 0.1670.134 80.00 54.8 113

Phenanthrene 07/18/20110.003 0.1670.145 86.80 60.4 121

Pyrene 07/18/20110.003 0.1670.153 91.60 57.9 129

Surr: 2-Fluorobiphenyl 07/18/20110.1670.115 68.9 45.7 89.2



SampID: 11070610-002AMS


Analyses Result


Acenaphthene 07/20/20110.004 0.1990.174 87.40 36 135

Acenaphthylene 07/20/20110.004 0.1990.175 88.20 17.2 167

Anthracene 07/20/20110.004 0.1990.169 85.20 39.3 124

Benzo(a)anthracene 07/20/20110.004 0.1990.177 80.80.01667 10 183

Benzo(a)pyrene 07/20/20110.004 0.1990.166 76.60.01429 10 204

Benzo(b)fluoranthene 07/20/20110.004 0.1990.207 92.80.02223 10.6 178

Benzo(g,h,i)perylene 07/20/20110.004 0.1990.126 60.10.006748 10 168

Benzo(k)fluoranthene 07/20/20110.004 0.1990.206 99.40.008733 27.6 181

Bis(2-ethylhexyl)phthalate 07/20/20110.080 0.1990.220 88.00.04565 50 150

Chrysene 07/20/20110.004 0.1990.190 87.00.01707 10 176


Fluoranthene 07/20/20110.004 0.1990.197 82.60.03255 10 227

Fluorene 07/20/20110.004 0.1990.174 87.40 35.2 148

Indeno(1,2,3-cd)pyrene 07/20/20110.004 0.1990.146 70.50.006351 10 164

Naphthalene 07/20/20110.004 0.1990.155 78.20 14.7 128

Phenanthrene 07/20/20110.004 0.1990.178 82.00.01469 32.8 143

Pyrene 07/20/20110.004 0.1990.190 82.00.02739 10 180

Surr: 2-Fluorobiphenyl 07/20/20110.1990.053 26.5 10 131

Surr: Nitrobenzene-d5 07/20/20110.1990.103 51.7 10 132


Page 79 of 104










SampType: MSD mg/Kg-dryUnits69628Batch RPD Limit 49.7

Analyses Result


Acenaphthene 07/21/20110.004 0.1990.163 81.8 6.570 0.1736

Acenaphthylene 07/21/20110.004 0.1990.166 83.6 5.310 0.1752

Anthracene 07/21/20110.004 0.1990.152 76.4 10.830 0.1693

Benzo(a)anthracene 07/21/20110.004 0.1990.165 74.4 7.390.01667 0.1772

Benzo(a)pyrene 07/21/20110.004 0.1990.166 76.2 0.440.01429 0.1665

Benzo(b)fluoranthene 07/21/20110.004 0.1990.189 83.8 8.990.02223 0.2065

Benzo(g,h,i)perylene R 07/21/20110.004 0.1990.185 89.8 37.990.006748 0.1261

Benzo(k)fluoranthene 07/21/20110.004 0.1990.183 87.6 12.000.008733 0.2061

Bis(2-ethylhexyl)phthalate 07/21/20110.080 0.1990.224 89.6 1.460.04565 0.2204

Chrysene 07/21/20110.004 0.1990.172 78.2 9.590.01707 0.1899

Dibenzo(a,h)anthracene 07/21/20110.004 0.1990.178 89.6 18.520 0.1479

Fluoranthene 07/21/20110.004 0.1990.188 78.4 4.290.03255 0.1966

Fluorene 07/21/20110.004 0.1990.166 83.6 4.400 0.1736

Indeno(1,2,3-cd)pyrene 07/21/20110.004 0.1990.184 89.4 22.840.006351 0.1463

Naphthalene 07/21/20110.004 0.1990.149 74.9 4.400 0.1554

Phenanthrene 07/21/20110.004 0.1990.167 76.4 6.420.01469 0.1776

Pyrene 07/21/20110.004 0.1990.188 80.6 1.440.02739 0.1903




Page 80 of 104









SampID: MB-69627


Analyses Result


1,2,4-Trichlorobenzene 07/19/20110.500 ND1,2-Dichlorobenzene 07/19/20110.500 ND1,3-Dichlorobenzene 07/19/20110.500 ND1,4-Dichlorobenzene 07/19/20110.500 ND2,4,5-Trichlorophenol 07/19/20110.350 ND2,4,6-Trichlorophenol 07/19/20110.350 ND2,4-Dichlorophenol 07/19/20110.500 ND2,4-Dimethylphenol 07/19/20110.500 ND2,4-Dinitrophenol 07/19/20111.00 ND2,4-Dinitrotoluene 07/19/20110.350 ND2,6-Dinitrotoluene 07/19/20110.350 ND2-Chloronaphthalene 07/19/20110.350 ND2-Chlorophenol 07/19/20110.500 ND2-Methoxy-4-methylphenol 07/19/20110.650 ND2-Methylnaphthalene 07/19/20110.350 ND2-Nitroaniline 07/19/20111.00 ND2-Nitrophenol 07/19/20110.350 ND3,3´-Dichlorobenzidine 07/19/20110.350 ND3-Nitroaniline 07/19/20111.00 ND4,6-Dinitro-2-methylphenol 07/19/20111.00 ND4-Bromophenyl phenyl ether 07/19/20110.350 ND4-Chloro-3-methylphenol 07/19/20110.500 ND4-Chloroaniline 07/19/20110.500 ND4-Chlorophenyl phenyl ether 07/19/20110.350 ND4-Nitroaniline 07/19/20110.500 ND4-Nitrophenol 07/19/20110.350 NDAniline 07/19/20110.500 NDAzobenzene 07/19/20110.350 NDBenzidine 07/19/20111.06 NDBenzoic acid 07/19/20111.50 NDBenzyl alcohol 07/19/20110.500 NDBis(2-chloroethoxy)methane 07/19/20110.350 NDBis(2-chloroethyl)ether 07/19/20110.500 NDBis(2-chloroisopropyl)ether 07/19/20110.350 NDButyl benzyl phthalate 07/19/20110.350 NDCarbazole 07/19/20110.500 NDDibenzofuran 07/19/20110.350 NDDiethyl phthalate 07/19/20110.500 NDDimethyl phthalate 07/19/20110.350 NDDi-n-butyl phthalate 07/19/20110.350 NDDi-n-octyl phthalate 07/19/20110.350 NDHexachlorobenzene 07/19/20110.350 NDHexachlorobutadiene 07/19/20110.500 NDHexachlorocyclopentadiene 07/19/20110.350 NDHexachloroethane 07/19/20110.500 NDIsophorone 07/19/20110.350 NDm,p-Cresol 07/19/20110.500 ND

Page 81 of 104









SampID: MB-69627


Analyses Result


Nitrobenzene 07/19/20110.500 NDN-Nitrosodimethylamine 07/19/20110.500 NDN-Nitroso-di-n-propylamine 07/19/20110.500 NDN-Nitrosodiphenylamine 07/19/20110.500 NDo-Cresol 07/19/20110.500 NDPentachlorophenol 07/19/20112.00 NDPhenol 07/19/20110.350 NDPyridine 07/19/20110.500 ND1,2-Diphenylhydrazine 07/19/20110.840 ND Surr: 2,4,6-Tribromophenol 07/19/20111.671.34 80.3 52.1 113




Surr: Phenol-d5 07/19/20111.671.24 74.5 55.9 98.5


Page 82 of 104









SampID: LCS-69627


Analyses Result






2,4-Dimethylphenol 07/19/20110.500 3.332.33 70.00 38.3 88

2,4-Dinitrophenol 07/19/20111.00 3.334.25 127.50 1.88 162

2,4-Dinitrotoluene 07/19/20110.350 1.671.64 98.30 48.6 102

2-Chlorophenol 07/19/20110.500 3.332.31 69.50 46.6 84


4-Nitrophenol S 07/19/20110.350 3.334.00 120.00 53.2 104







m,p-Cresol 07/19/20110.500 1.671.30 78.00 37.6 93.7

Nitrobenzene 07/19/20110.500 3.332.47 74.20 51.8 104


o-Cresol 07/19/20110.500 1.671.29 77.20 43 101


Phenol 07/19/20110.350 3.332.37 71.20 41.6 81.3

Pyridine 07/19/20110.500 3.331.89 56.90 3.61 74.3





Surr: Phenol-d5 07/19/20111.671.24 74.0 55.9 98.5


Page 83 of 104









SampID: 11070610-003AMS


Analyses Result


1,2,4-Trichlorobenzene 07/19/20110.655 2.191.49 67.90 35.9 102




2,4-Dimethylphenol 07/19/20110.655 4.362.71 62.20 38.3 88

2,4-Dinitrophenol 07/19/20111.31 4.364.10 94.10 1.88 162

2,4-Dinitrotoluene 07/19/20110.458 2.192.07 94.50 37.5 107

2-Chlorophenol 07/19/20110.655 4.362.82 64.60 22.6 108

4-Chloro-3-methylphenol 07/19/20110.655 4.363.43 78.60 19.3 131

4-Nitrophenol 07/19/20110.458 4.364.86 111.40 27.6 123







m,p-Cresol 07/19/20110.655 2.191.62 73.90 37.6 93.7

Nitrobenzene 07/19/20110.655 4.363.08 70.50 51.8 104


o-Cresol 07/19/20110.655 2.191.55 70.80 43 101


Phenol 07/19/20110.458 4.362.92 67.10 20.8 110

Pyridine 07/19/20110.655 4.362.27 52.10 3.61 74.3





Surr: Phenol-d5 07/19/20112.191.50 68.5 34.9 110


Page 84 of 104











Analyses Result






2,4-Dimethylphenol 07/19/20110.654 4.363.07 70.5 12.410 2.712

2,4-Dinitrophenol 07/19/20111.31 4.364.31 98.9 4.920 4.102

2,4-Dinitrotoluene 07/19/20110.458 2.182.22 101.7 7.180 2.068

2-Chlorophenol 07/19/20110.654 4.363.02 69.4 7.070 2.818


4-Nitrophenol 07/19/20110.458 4.365.21 119.6 6.960 4.858

Diethyl phthalate 07/19/20110.654 4.363.81 87.4 4.560 3.636

Dimethyl phthalate 07/19/20110.458 4.363.50 80.4 5.120 3.325

Di-n-butyl phthalate 07/19/20110.458 2.182.15 98.4 3.880 2.068

Hexachlorobenzene 07/19/20110.458 4.363.48 80.0 5.660 3.292



m,p-Cresol 07/19/20110.654 2.181.75 80.1 8.000 1.616

Nitrobenzene 07/19/20110.654 4.363.36 77.1 8.820 3.076


o-Cresol 07/19/20110.654 2.181.70 78.0 9.600 1.548

Pentachlorophenol 07/19/20112.62 4.363.77 86.6 7.800 3.487

Phenol 07/19/20110.458 4.363.14 72.1 7.070 2.925

Pyridine 07/19/20110.654 4.362.39 55.0 5.250 2.272

Surr: 2,4,6-Tribromophenol 07/19/20112.181.73 79.1


Surr: 2-Fluorophenol 07/19/20112.181.42 64.9


Surr: Phenol-d5 07/19/20112.181.56 71.6


Page 85 of 104









SampID: MBLK-G110720-1


Analyses Result


1,1,1,2-Tetrachloroethane 07/20/20115.0 ND1,1,1-Trichloroethane 07/20/20115.0 ND1,1,2,2-Tetrachloroethane 07/20/20115.0 ND1,1,2-Trichloro-1,2,2-trifluoroethane 07/20/20115.0 ND1,1,2-Trichloroethane 07/20/20115.0 ND1,1-Dichloro-2-propanone 07/20/201150.0 ND1,1-Dichloroethane 07/20/20115.0 ND1,1-Dichloroethene 07/20/20115.0 ND1,1-Dichloropropene 07/20/20115.0 ND1,2,3-Trichlorobenzene 07/20/20115.0 ND1,2,3-Trichloropropane 07/20/201110.0 ND1,2,3-Trimethylbenzene 07/20/20115.0 ND1,2,4-Trichlorobenzene 07/20/20115.0 ND1,2,4-Trimethylbenzene 07/20/20115.0 ND1,2-Dibromo-3-chloropropane 07/20/20115.0 ND1,2-Dibromoethane 07/20/20115.0 ND1,2-Dichlorobenzene 07/20/20115.0 ND1,2-Dichloroethane 07/20/20115.0 ND1,2-Dichloropropane 07/20/20115.0 ND1,3,5-Trimethylbenzene 07/20/20115.0 ND1,3-Dichlorobenzene 07/20/20115.0 ND1,3-Dichloropropane 07/20/20115.0 ND1,4-Dichlorobenzene 07/20/20115.0 ND1-Chlorobutane 07/20/20115.0 ND2,2-Dichloropropane 07/20/20115.0 ND2-Butanone 07/20/201150.0 ND2-Chlorotoluene 07/20/20115.0 ND2-Hexanone 07/20/201150.0 ND2-Nitropropane 07/20/201150.0 ND4-Chlorotoluene 07/20/20115.0 ND4-Methyl-2-pentanone 07/20/201150.0 NDAcetone 07/20/201150.0 NDAcrolein 07/20/2011100 NDAcrylonitrile 07/20/201110.0 NDAllyl chloride 07/20/20115.0 NDBenzene 07/20/20111.0 NDBromobenzene 07/20/20115.0 NDBromochloromethane 07/20/20115.0 NDBromodichloromethane 07/20/20115.0 NDBromoform 07/20/20115.0 NDBromomethane 07/20/201110.0 NDCarbon disulfide 07/20/20115.0 NDCarbon tetrachloride 07/20/20115.0 NDChlorobenzene 07/20/20115.0 NDChloroethane 07/20/201110.0 NDChloroform 07/20/20115.0 NDChloromethane 07/20/201110.0 ND

Page 86 of 104











Analyses Result


cis-1,2-Dichloroethene 07/20/20115.0 NDcis-1,3-Dichloropropene 07/20/20114.0 NDCyclohexanone 07/20/2011100 NDDibromochloromethane 07/20/20115.0 NDDibromomethane 07/20/20115.0 NDDichlorodifluoromethane 07/20/201110.0 NDEthyl acetate 07/20/201150.0 NDEthyl ether 07/20/20115.0 NDEthyl methacrylate 07/20/20115.0 NDEthylbenzene 07/20/20115.0 NDHeptane 07/20/201120.0 NDHexachlorobutadiene 07/20/20115.0 NDHexachloroethane 07/20/20115.0 NDIodomethane 07/20/201110.0 NDIsopropylbenzene 07/20/20115.0 NDm,p-Xylenes 07/20/20115.0 NDMethacrylonitrile 07/20/201150.0 NDMethyl Methacrylate 07/20/20115.0 NDMethyl tert-butyl ether 07/20/20112.0 NDMethylacrylate 07/20/201110.0 NDMethylene chloride J 07/20/20115.0 1.8Naphthalene 07/20/201110.0 NDn-Butylbenzene 07/20/20115.0 NDn-Hexane 07/20/201120.0 NDNitrobenzene 07/20/2011100 NDn-Propylbenzene 07/20/20115.0 NDo-Xylene 07/20/20115.0 NDPentachloroethane 07/20/20115.0 NDp-Isopropyltoluene 07/20/20115.0 NDPropionitrile 07/20/201150.0 NDsec-Butylbenzene 07/20/20115.0 NDStyrene 07/20/20115.0 NDtert-Butylbenzene 07/20/20115.0 NDTetrachloroethene 07/20/20115.0 NDTetrahydrofuran 07/20/201150.0 NDToluene 07/20/20115.0 NDtrans-1,2-Dichloroethene 07/20/20115.0 NDtrans-1,3-Dichloropropene 07/20/20114.0 NDTrichloroethene 07/20/20115.0 NDTrichlorofluoromethane 07/20/20115.0 NDVinyl acetate 07/20/201150.0 NDVinyl chloride 07/20/20112.0 ND Surr: 1,2-Dichloroethane-d4 07/20/201150.050.2 100.3 72.2 131



Surr: Toluene-d8 07/20/201150.053.1 106.2 86 116

Page 87 of 104









SampID: LCSD-G110720-1


Analyses Result








1,1-Dichloroethane 07/20/20115.0 50.050.8 101.6 2.490 49.53

1,1-Dichloroethene 07/20/20115.0 50.054.0 108.0 2.080 52.89



1,2,3-Trichloropropane 07/20/201110.0 50.054.0 108.0 3.970 51.90





1,2-Dibromoethane 07/20/20115.0 50.054.6 109.3 3.140 52.96


1,2-Dichloroethane 07/20/20115.0 50.054.4 108.8 1.040 53.82






1-Chlorobutane 07/20/20115.0 50.054.9 109.9 0.530 55.22


2-Butanone 07/20/201150.0 125124 99.1 1.320 122.3

2-Chlorotoluene 07/20/20115.0 50.054.4 108.8 1.370 55.17

2-Hexanone 07/20/201150.0 125130 104.0 3.570 125.5

2-Nitropropane 07/20/201150.0 500505 101.1 7.740 467.7

4-Chlorotoluene 07/20/20115.0 50.055.1 110.2 2.080 56.24

4-Methyl-2-pentanone 07/20/201150.0 125123 98.6 9.180 112.4

Acetone 07/20/201150.0 125163 130.4 3.180 168.3

Acrylonitrile 07/20/201110.0 50.045.9 91.9 10.760 41.25

Allyl chloride 07/20/20115.0 50.053.9 107.9 1.360 54.68

Benzene 07/20/20111.0 50.050.5 101.1 2.360 49.35

Bromobenzene 07/20/20115.0 50.055.4 110.9 0.910 54.93



Bromoform 07/20/20115.0 50.056.0 112.0 4.890 53.32

Bromomethane 07/20/201110.0 50.053.9 107.7 2.880 52.34



Chlorobenzene 07/20/20115.0 50.054.0 108.0 1.460 53.20

Chloroethane 07/20/201110.0 50.054.8 109.5 3.850 52.70

Chloroform 07/20/20115.0 50.051.6 103.2 0.760 51.22

Chloromethane 07/20/201110.0 50.056.4 112.8 6.190 53.03


Page 88 of 104











Analyses Result



Cyclohexanone 07/20/2011100 250217 86.8 3.430 224.6


Dibromomethane 07/20/20115.0 50.051.4 102.8 1.450 50.65

Dichlorodifluoromethane 07/20/201110.0 50.070.1 140.2 0.720 69.61

Ethyl acetate 07/20/201150.0 50.050.4 100.8 11.800 44.80

Ethyl ether 07/20/20115.0 50.048.0 96.1 2.640 46.80


Ethylbenzene 07/20/20115.0 50.054.2 108.4 1.510 53.38

Heptane 07/20/201120.0 50.051.4 102.8 3.620 49.59



Iodomethane 07/20/201110.0 50.048.1 96.3 4.050 46.22


m,p-Xylenes 07/20/20115.0 100110 110.2 1.440 108.6

Methacrylonitrile J 07/20/201150.0 50.048 95.9 0.000 43.81



Methylacrylate 07/20/201110.0 50.048.5 96.9 8.990 44.30


Naphthalene 07/20/201110.0 50.046.7 93.4 3.390 48.31

n-Butylbenzene 07/20/20115.0 50.055.1 110.2 2.460 56.46

n-Hexane 07/20/201120.0 50.052.0 104.0 1.390 51.27

Nitrobenzene 07/20/2011100 500231 46.2 1.640 234.8

n-Propylbenzene 07/20/20115.0 50.055.2 110.3 1.030 55.72

o-Xylene 07/20/20115.0 50.054.7 109.4 2.270 53.49



Propionitrile 07/20/201150.0 500460 92.1 10.190 415.6


Styrene 07/20/20115.0 50.053.6 107.2 3.530 51.75




Toluene 07/20/20115.0 50.053.3 106.5 1.340 52.55





Vinyl acetate 07/20/201150.0 50.052.5 105.0 4.600 50.12

Vinyl chloride 07/20/20112.0 50.059.2 118.3 1.960 58.02




Surr: Toluene-d8 07/20/201150.052.9 105.7

Page 89 of 104









SampID: LCS-G110720-1


Analyses Result








1,1-Dichloroethane 07/20/20115.0 50.049.5 99.10 0 200

1,1-Dichloroethene 07/20/20115.0 50.052.9 105.80 60.1 131



1,2,3-Trichloropropane 07/20/201110.0 50.051.9 103.80 0 200





1,2-Dibromoethane 07/20/20115.0 50.053.0 105.90 86.9 119


1,2-Dichloroethane 07/20/20115.0 50.053.8 107.60 73 117






1-Chlorobutane 07/20/20115.0 50.055.2 110.40 0 200


2-Butanone 07/20/201150.0 125122 97.80 45.3 136

2-Chlorotoluene 07/20/20115.0 50.055.2 110.30 0 200

2-Hexanone 07/20/201150.0 125126 100.40 0 200

2-Nitropropane 07/20/201150.0 500468 93.50 0 200

4-Chlorotoluene 07/20/20115.0 50.056.2 112.50 0 200


Acetone 07/20/201150.0 125168 134.60 0 200

Acrylonitrile 07/20/201110.0 50.041.2 82.50 0 200

Allyl chloride 07/20/20115.0 50.054.7 109.40 0 200

Benzene 07/20/20111.0 50.049.4 98.70 73.9 109

Bromobenzene 07/20/20115.0 50.054.9 109.90 0 200



Bromoform 07/20/20115.0 50.053.3 106.60 0 200

Bromomethane 07/20/201110.0 50.052.3 104.70 0 200



Chlorobenzene 07/20/20115.0 50.053.2 106.40 85.8 116

Chloroethane 07/20/201110.0 50.052.7 105.40 0 200

Chloroform 07/20/20115.0 50.051.2 102.40 80 113

Chloromethane 07/20/201110.0 50.053.0 106.10 0 200


Page 90 of 104











Analyses Result



Cyclohexanone 07/20/2011100 250225 89.80 0 200


Dibromomethane 07/20/20115.0 50.050.6 101.30 0 200

Dichlorodifluoromethane 07/20/201110.0 50.069.6 139.20 0 200

Ethyl acetate J 07/20/201150.0 50.045 89.60 0 200

Ethyl ether 07/20/20115.0 50.046.8 93.60 0 200


Ethylbenzene 07/20/20115.0 50.053.4 106.80 84.1 115

Heptane 07/20/201120.0 50.049.6 99.20 0 200



Iodomethane 07/20/201110.0 50.046.2 92.40 0 200


m,p-Xylenes 07/20/20115.0 100109 108.60 79.1 111

Methacrylonitrile J 07/20/201150.0 50.044 87.60 0 200



Methylacrylate 07/20/201110.0 50.044.3 88.60 0 200


Naphthalene 07/20/201110.0 50.048.3 96.60 73.1 135

n-Butylbenzene 07/20/20115.0 50.056.5 112.90 0 200

n-Hexane 07/20/201120.0 50.051.3 102.50 0 200

Nitrobenzene 07/20/2011100 500235 47.00 0 200

n-Propylbenzene 07/20/20115.0 50.055.7 111.40 0 200

o-Xylene 07/20/20115.0 50.053.5 107.00 82 117



Propionitrile 07/20/201150.0 500416 83.10 0 200


Styrene 07/20/20115.0 50.051.8 103.50 0 200




Toluene 07/20/20115.0 50.052.6 105.10 79.1 112



Trichloroethene 07/20/20115.0 50.051.2 102.30 81 111


Vinyl acetate 07/20/201150.0 50.050.1 100.20 0 200

Vinyl chloride 07/20/20112.0 50.058.0 116.00 0 200




Surr: Toluene-d8 07/20/201150.053.2 106.3 86 116

Page 91 of 104











Analyses Result



Page 92 of 104











Analyses Result





Surr: Toluene-d8 07/20/201150.053.2 106.4 86 116

Page 93 of 104











Analyses Result








1,1-Dichloroethane 07/20/20115.0 50.047.0 94.0 0.530 47.23

1,1-Dichloroethene 07/20/20115.0 50.046.9 93.8 0.490 47.15








1,2-Dibromoethane 07/20/20115.0 50.052.6 105.3 3.910 50.61


1,2-Dichloroethane 07/20/20115.0 50.053.2 106.3 1.770 54.12






1-Chlorobutane 07/20/20115.0 50.051.1 102.2 0.630 50.79


2-Butanone 07/20/201150.0 125113 90.5 11.720 100.6

2-Chlorotoluene 07/20/20115.0 50.047.2 94.3 1.560 47.89

2-Hexanone 07/20/201150.0 125118 94.1 8.380 108.1

2-Nitropropane 07/20/201150.0 500505 101.0 4.660 482.2

4-Chlorotoluene 07/20/20115.0 50.046.4 92.8 0.820 46.79


Acetone 07/20/201150.0 125131 104.5 8.390 120.1

Acrylonitrile 07/20/201110.0 50.043.8 87.5 5.500 41.41

Allyl chloride 07/20/20115.0 50.049.5 99.0 4.330 51.71

Benzene 07/20/20111.0 50.045.6 91.1 1.110 46.08

Bromobenzene 07/20/20115.0 50.048.9 97.9 1.210 48.34



Bromoform 07/20/20115.0 50.053.8 107.7 2.860 52.33

Bromomethane 07/20/201110.0 50.045.4 90.9 4.220 47.39



Chlorobenzene 07/20/20115.0 50.049.4 98.8 1.550 48.65

Chloroethane 07/20/201110.0 50.045.2 90.5 0.620 45.53

Chloroform 07/20/20115.0 50.049.8 99.7 0.140 49.76

Chloromethane 07/20/201110.0 50.041.9 83.7 3.660 43.42


Page 94 of 104











Analyses Result



Cyclohexanone 07/20/2011100 250213 85.4 13.820 185.8


Dibromomethane 07/20/20115.0 50.048.6 97.3 0.020 48.64


Ethyl acetate J 07/20/201150.0 50.048 95.2 0.000 46.78

Ethyl ether 07/20/20115.0 50.044.5 89.1 3.920 42.82


Ethylbenzene 07/20/20115.0 50.049.2 98.3 0.240 49.05

Heptane 07/20/201120.0 50.042.1 84.2 5.110 44.33



Iodomethane 07/20/201110.0 50.042.2 84.5 1.140 41.75


m,p-Xylenes 07/20/20115.0 100103 102.5 3.360 99.12




Methylacrylate 07/20/201110.0 50.045.3 90.6 6.280 42.56


Naphthalene 07/20/201110.0 50.044.8 89.7 2.280 43.84

n-Butylbenzene 07/20/20115.0 50.044.3 88.5 3.050 45.64

n-Hexane 07/20/201120.0 50.041.4 82.8 3.770 43.01

Nitrobenzene 07/20/2011100 500221 44.2 5.130 209.7

n-Propylbenzene 07/20/20115.0 50.046.9 93.8 0.930 47.36

o-Xylene 07/20/20115.0 50.051.7 103.5 1.460 50.99



Propionitrile 07/20/201150.0 500445 88.9 8.710 407.6


Styrene 07/20/20115.0 50.048.4 96.8 0.210 48.29




Toluene 07/20/20115.0 50.049.7 99.3 2.120 48.62





Vinyl acetate J 07/20/201150.0 50.048 95.4 0.000 45.98

Vinyl chloride 07/20/20112.0 50.046.1 92.1 2.320 47.14




Surr: Toluene-d8 07/20/201150.053.9 107.8

Page 95 of 104











Analyses Result








1,1-Dichloroethane 07/20/20115.0 50.047.2 94.50 0 200

1,1-Dichloroethene 07/20/20115.0 50.047.2 94.30 60.1 131








1,2-Dibromoethane 07/20/20115.0 50.050.6 101.20 86.9 119


1,2-Dichloroethane 07/20/20115.0 50.054.1 108.20 73 117






1-Chlorobutane 07/20/20115.0 50.050.8 101.60 0 200


2-Butanone 07/20/201150.0 125101 80.50 45.3 136

2-Chlorotoluene 07/20/20115.0 50.047.9 95.80 0 200

2-Hexanone 07/20/201150.0 125108 86.50 0 200

2-Nitropropane 07/20/201150.0 500482 96.40 0 200

4-Chlorotoluene 07/20/20115.0 50.046.8 93.60 0 200


Acetone 07/20/201150.0 125120 96.00 0 200

Acrylonitrile 07/20/201110.0 50.041.4 82.80 0 200

Allyl chloride 07/20/20115.0 50.051.7 103.40 0 200

Benzene 07/20/20111.0 50.046.1 92.20 73.9 109

Bromobenzene 07/20/20115.0 50.048.3 96.70 0 200



Bromoform 07/20/20115.0 50.052.3 104.70 0 200

Bromomethane 07/20/201110.0 50.047.4 94.80 0 200



Chlorobenzene 07/20/20115.0 50.048.6 97.30 85.8 116

Chloroethane 07/20/201110.0 50.045.5 91.10 0 200

Chloroform 07/20/20115.0 50.049.8 99.50 80 113

Chloromethane 07/20/201110.0 50.043.4 86.80 0 200


Page 96 of 104











Analyses Result



Cyclohexanone 07/20/2011100 250186 74.30 0 200


Dibromomethane 07/20/20115.0 50.048.6 97.30 0 200


Ethyl acetate J 07/20/201150.0 50.047 93.60 0 200

Ethyl ether 07/20/20115.0 50.042.8 85.60 0 200


Ethylbenzene 07/20/20115.0 50.049.0 98.10 84.1 115

Heptane 07/20/201120.0 50.044.3 88.70 0 200



Iodomethane 07/20/201110.0 50.041.8 83.50 0 200


m,p-Xylenes 07/20/20115.0 10099.1 99.10 79.1 111




Methylacrylate 07/20/201110.0 50.042.6 85.10 0 200


Naphthalene 07/20/201110.0 50.043.8 87.70 73.1 135

n-Butylbenzene 07/20/20115.0 50.045.6 91.30 0 200

n-Hexane 07/20/201120.0 50.043.0 86.00 0 200

Nitrobenzene 07/20/2011100 500210 41.90 0 200

n-Propylbenzene 07/20/20115.0 50.047.4 94.70 0 200

o-Xylene 07/20/20115.0 50.051.0 102.00 82 117



Propionitrile 07/20/201150.0 500408 81.50 0 200


Styrene 07/20/20115.0 50.048.3 96.60 0 200




Toluene 07/20/20115.0 50.048.6 97.20 79.1 112





Vinyl acetate J 07/20/201150.0 50.046 92.00 0 200

Vinyl chloride 07/20/20112.0 50.047.1 94.30 0 200




Surr: Toluene-d8 07/20/201150.052.8 105.6 86 116

Page 97 of 104











Analyses Result



Page 98 of 104











Analyses Result





Surr: Toluene-d8 07/21/201150.052.8 105.6 86 116

Page 99 of 104











Analyses Result








1,1-Dichloroethane 07/21/20115.0 50.048.9 97.7 2.150 49.92

1,1-Dichloroethene 07/21/20115.0 50.048.9 97.7 2.590 50.14








1,2-Dibromoethane 07/21/20115.0 50.053.8 107.5 1.460 52.98


1,2-Dichloroethane 07/21/20115.0 50.055.7 111.4 2.530 57.14






1-Chlorobutane 07/21/20115.0 50.053.7 107.5 1.120 53.14


2-Butanone 07/21/201150.0 125135 107.7 0.640 135.5

2-Chlorotoluene 07/21/20115.0 50.054.1 108.2 0.970 54.64

2-Hexanone 07/21/201150.0 125133 106.3 0.490 132.2

2-Nitropropane 07/21/201150.0 500510 101.9 3.970 530.3

4-Chlorotoluene 07/21/20115.0 50.054.9 109.8 1.890 55.95


Acetone 07/21/201150.0 125185 148.1 2.840 190.5

Acrylonitrile 07/21/201110.0 50.042.7 85.5 1.580 43.41

Allyl chloride 07/21/20115.0 50.052.8 105.7 5.840 56.01

Benzene 07/21/20111.0 50.048.4 96.7 0.970 48.83

Bromobenzene 07/21/20115.0 50.053.5 107.0 0.060 53.55



Bromoform 07/21/20115.0 50.055.3 110.7 1.490 56.17

Bromomethane 07/21/201110.0 50.046.4 92.7 12.060 52.32



Chlorobenzene 07/21/20115.0 50.052.4 104.7 1.270 53.03

Chloroethane 07/21/201110.0 50.047.3 94.6 5.850 50.16

Chloroform 07/21/20115.0 50.051.9 103.7 2.640 53.26

Chloromethane 07/21/201110.0 50.042.4 84.8 10.460 47.08


Page 100 of 104











Analyses Result



Cyclohexanone 07/21/2011100 250224 89.7 0.050 224.1


Dibromomethane 07/21/20115.0 50.050.8 101.6 3.630 52.69


Ethyl acetate J 07/21/201150.0 50.047 93.6 0.000 47.41

Ethyl ether 07/21/20115.0 50.045.3 90.5 0.780 44.92


Ethylbenzene 07/21/20115.0 50.053.1 106.1 1.760 54.01

Heptane 07/21/201120.0 50.049.6 99.2 1.900 50.53



Iodomethane 07/21/201110.0 50.045.6 91.2 4.830 47.88


m,p-Xylenes 07/21/20115.0 100109 108.7 1.950 110.8




Methylacrylate 07/21/201110.0 50.046.3 92.7 2.180 45.34


Naphthalene 07/21/201110.0 50.049.1 98.2 5.000 51.64

n-Butylbenzene 07/21/20115.0 50.056.2 112.5 4.980 59.12

n-Hexane 07/21/201120.0 50.047.7 95.3 0.750 48.03

Nitrobenzene 07/21/2011100 500223 44.5 9.250 244.2

n-Propylbenzene 07/21/20115.0 50.054.6 109.3 0.660 54.99

o-Xylene 07/21/20115.0 50.054.7 109.3 3.200 56.44



Propionitrile 07/21/201150.0 500435 87.1 5.810 461.4


Styrene 07/21/20115.0 50.052.8 105.5 2.470 54.07




Toluene 07/21/20115.0 50.051.3 102.7 0.640 51.67





Vinyl acetate 07/21/201150.0 50.050.8 101.6 1.570 50.01

Vinyl chloride 07/21/20112.0 50.046.8 93.5 8.790 51.05




Surr: Toluene-d8 07/21/201150.053.2 106.4

Page 101 of 104











Analyses Result








1,1-Dichloroethane 07/21/20115.0 50.049.9 99.80 0 200

1,1-Dichloroethene 07/21/20115.0 50.050.1 100.30 60.1 131








1,2-Dibromoethane 07/21/20115.0 50.053.0 106.00 86.9 119


1,2-Dichloroethane 07/21/20115.0 50.057.1 114.30 73 117






1-Chlorobutane 07/21/20115.0 50.053.1 106.30 0 200


2-Butanone 07/21/201150.0 125135 108.40 45.3 136

2-Chlorotoluene 07/21/20115.0 50.054.6 109.30 0 200

2-Hexanone 07/21/201150.0 125132 105.80 0 200

2-Nitropropane 07/21/201150.0 500530 106.10 0 200

4-Chlorotoluene 07/21/20115.0 50.056.0 111.90 0 200


Acetone 07/21/201150.0 125190 152.40 0 200

Acrylonitrile 07/21/201110.0 50.043.4 86.80 0 200

Allyl chloride 07/21/20115.0 50.056.0 112.00 0 200

Benzene 07/21/20111.0 50.048.8 97.70 73.9 109

Bromobenzene 07/21/20115.0 50.053.6 107.10 0 200



Bromoform 07/21/20115.0 50.056.2 112.30 0 200

Bromomethane 07/21/201110.0 50.052.3 104.60 0 200



Chlorobenzene 07/21/20115.0 50.053.0 106.10 85.8 116

Chloroethane 07/21/201110.0 50.050.2 100.30 0 200

Chloroform 07/21/20115.0 50.053.3 106.50 80 113

Chloromethane 07/21/201110.0 50.047.1 94.20 0 200


Page 102 of 104











Analyses Result



Cyclohexanone 07/21/2011100 250224 89.60 0 200


Dibromomethane 07/21/20115.0 50.052.7 105.40 0 200


Ethyl acetate J 07/21/201150.0 50.047 94.80 0 200

Ethyl ether 07/21/20115.0 50.044.9 89.80 0 200


Ethylbenzene 07/21/20115.0 50.054.0 108.00 84.1 115

Heptane 07/21/201120.0 50.050.5 101.10 0 200



Iodomethane 07/21/201110.0 50.047.9 95.80 0 200


m,p-Xylenes 07/21/20115.0 100111 110.80 79.1 111




Methylacrylate 07/21/201110.0 50.045.3 90.70 0 200


Naphthalene 07/21/201110.0 50.051.6 103.30 73.1 135

n-Butylbenzene 07/21/20115.0 50.059.1 118.20 0 200

n-Hexane 07/21/201120.0 50.048.0 96.10 0 200

Nitrobenzene 07/21/2011100 500244 48.80 0 200

n-Propylbenzene 07/21/20115.0 50.055.0 110.00 0 200

o-Xylene 07/21/20115.0 50.056.4 112.90 82 117



Propionitrile 07/21/201150.0 500461 92.30 0 200


Styrene 07/21/20115.0 50.054.1 108.10 0 200




Toluene 07/21/20115.0 50.051.7 103.30 79.1 112





Vinyl acetate 07/21/201150.0 50.050.0 100.00 0 200

Vinyl chloride 07/21/20112.0 50.051.0 102.10 0 200




Surr: Toluene-d8 07/21/201150.052.6 105.1 86 116

Page 103 of 104


Receiving Check List






Received By: DBCarrier: Michael Flora


On:

15-Jul-11

On:

18-Jul-11










Temp °C 8.8



The samples were out of temperature compliance upon receipt. Per Michael Flora, continue with analyses out of temperature compliance. DB 7/15/11

Per Leslie Hoosier, add TCL list of metals to analysis (1 day TAT). 7/26/11 HAW

Water - vials have zero headspace? Yes No No VOA vials





Pages to follow:


Timothy W. Mathis Elizabeth A. Hurley

Page 104 of 104


ANALYTICAL REPORT

July 25, 2011

Page 1 of 12Work Order: 11G0968

Project :

Project Number:

Subcontract - HW Project

11070610

Report To

Heather White

Teklab, Inc.

Collinsville, IL 62234

5445 Horseshoe Lake Road

Work Order Information

Date Received: 07/20/2011 10:15AM

Collector:

Phone: (618) 344-1004

PO Number: 16874


















Surrogate: 2,5-Dichlorobenzoic Acid 105 % 24-140 07/22/11 21:06EPP

0.1%% Solids SM 2540 G MAV 07/20/11 16:4284.1 1G12048












Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 2 of 12












0.1%% Solids SM 2540 G MAV 07/20/11 16:4286.4 1G12048


















0.1%% Solids SM 2540 G MAV 07/20/11 16:4283.9 1G12048













Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 3 of 12











0.1%% Solids SM 2540 G MAV 07/20/11 16:4288.8 1G12048


















0.1%% Solids SM 2540 G MAV 07/20/11 16:4279.5 1G12048













Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 4 of 12











0.1%% Solids SM 2540 G MAV 07/20/11 16:4278.3 1G12048


















0.1%% Solids SM 2540 G MAV 07/20/11 16:4284.0 1G12048














Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 5 of 12










0.1%% Solids SM 2540 G MAV 07/20/11 16:4264.8 1G12048


















0.1%% Solids SM 2540 G MAV 07/20/11 16:4280.9 1G12048




Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 6 of 12

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte



Batch 1G12046 - EPA 8151A

Blank (1G12046-BLK1) Prepared: 07/20/11 Analyzed: 07/22/11


Dalapon "ND 0.05

3,5-Dichlorobenzoic acid "ND 0.05

Dicamba "ND 0.05

Dichlorprop "ND 0.05

2,4-D "ND 0.05

Pentachlorophenol "ND 0.05

2,4,5-TP (Silvex) "ND 0.05

Chloramben "ND 0.05

2,4,5-T "ND 0.05

2,4-DB "ND 0.05

Bentazon "ND 0.05

Picloram "ND 0.05

Dinoseb "ND 0.05

DCPA "ND 0.05

Acifluorfen "ND 0.05

LCS (1G12046-BS1) Prepared: 07/20/11 Analyzed: 07/22/11


Dalapon "0.081 0.05 0.208000 10-9339.1


Dicamba "0.013 0.05 0.0160000 38-12383.3

Dichlorprop "0.047 0.05 0.0480000 31-12797.9

2,4-D "0.032 0.05 0.0320000 23-12799.0


2,4,5-TP (Silvex) "0.011 0.05 0.0160000 35-11667.7

Chloramben "0.006 0.05 0.0160000 10-9437.5

2,4,5-T "0.008 0.05 0.0160000 26-10449.0

2,4-DB "0.101 0.05 0.128000 42-12278.8

Bentazon "0.028 0.05 0.0320000 42-13389.1

Picloram "0.013 0.05 0.0160000 19-15779.2

Dinoseb "0.011 0.05 0.0320000 10-9033.9

DCPA "0.009 0.05 0.0160000 10-11754.2

Acifluorfen "0.013 0.05 0.0160000 24-11383.3




Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 7 of 12

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte




LCS Dup (1G12046-BSD1) Prepared: 07/20/11 Analyzed: 07/22/11


Dalapon "0.082 0.05 0.208000 3010-9339.4 0.816


Dicamba "0.012 0.05 0.0160000 3038-12378.1 6.45

Dichlorprop "0.048 0.05 0.0480000 3031-127101 3.14

2,4-D "0.032 0.05 0.0320000 3023-127102 2.60

Pentachlorophenol "0.011 0.05 0.0160000 3010-9367.7 7.41

2,4,5-TP (Silvex) "0.010 0.05 0.0160000 3035-11664.6 4.72

Chloramben "0.006 0.05 0.0160000 3010-9434.4 8.70

2,4,5-T "0.008 0.05 0.0160000 3026-10449.0 0.00

2,4-DB "0.111 0.05 0.128000 3042-12287.0 9.90

Bentazon "0.029 0.05 0.0320000 3042-13390.1 1.16

Picloram "0.013 0.05 0.0160000 3019-15783.3 5.13

Dinoseb "0.007 0.05 0.0320000 30 QR-0210-9022.4 40.7

DCPA "0.010 0.05 0.0160000 3010-11765.6 19.1

Acifluorfen "0.016 0.05 0.0160000 3024-113103 21.2

Matrix Spike (1G12046-MS1) Prepared: 07/20/11 Analyzed: 07/22/11 Source: 11G0968-02


Dalapon "0.185 0.05 0.240824 ND 19-15676.9

3,5-Dichlorobenzoic acid "0.016 0.05 0.0185250 ND 38.9-18184.4

Dicamba "0.017 0.05 0.0185250 ND 40-15391.7

Dichlorprop "0.057 0.05 0.0555748 ND 19.6-138102

2,4-D "0.035 0.05 0.0370499 ND 10-14694.3

Pentachlorophenol "0.014 0.05 0.0185250 ND 16-12777.1

2,4,5-TP (Silvex) "0.014 0.05 0.0185250 ND 31.2-15974.0

Chloramben "0.008 0.05 0.0185250 ND 10-13343.8

2,4,5-T "0.012 0.05 0.0185250 ND 16.4-15263.5

2,4-DB "0.152 0.05 0.148200 ND 35.3-156103

Bentazon "0.028 0.05 0.0370499 ND 10-15076.0

Picloram "0.012 0.05 0.0185250 ND 45-14663.5

Dinoseb "0.012 0.05 0.0370499 ND 10-9032.3

DCPA "0.008 0.05 0.0185250 ND 10-15142.7

Acifluorfen "0.020 0.05 0.0185250 ND 10-161110




Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 8 of 12

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte




Reference (1G12046-SRM1) Prepared: 07/20/11 Analyzed: 07/22/11


Dalapon "0.233 0.05 0.208000 70-130112

3,5-Dichlorobenzoic acid "0.017 0.05 0.0160000 70-130106

Dicamba "0.018 0.05 0.0160000 70-130110

Dichlorprop "0.047 0.05 0.0480000 70-13097.9

2,4-D "0.033 0.05 0.0320000 70-130103

Pentachlorophenol "0.017 0.05 0.0160000 70-130107

2,4,5-TP (Silvex) "0.018 0.05 0.0160000 70-130109

Chloramben "0.013 0.05 0.0160000 70-13083.3

2,4,5-T "0.015 0.05 0.0160000 70-13095.8

2,4-DB "0.137 0.05 0.128000 70-130107

Bentazon "0.029 0.05 0.0320000 70-13089.6

Picloram "0.019 0.05 0.0160000 70-130117

Dinoseb "0.034 0.05 0.0320000 70-130107

DCPA "0.018 0.05 0.0160000 70-130110

Acifluorfen "0.012 0.05 0.0160000 70-13078.1




Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 9 of 12

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte

Determination of Conventional Chemistry Parameters - Quality Control


Batch 1G12048 - Wet Chem Preparation

Duplicate (1G12048-DUP1) Prepared & Analyzed: 07/20/11 Source: 11G0968-09

% Solids %80.1 0.1 80.9 201.06

ND = Non Detect; REC= Recovery; RPD= Relative Percent Difference

Certified Analyses included in this Report

CertificationsAnalyteMethod/Matrix

EPA 8151A in Soil

KS-NT,NELACDalapon

KS-NT,NELAC,SIA1XDicamba

NELACDichlorprop

KS-NT,NELAC,SIA1X2,4-D

KS-NT,NELAC,SIA1X2,4,5-TP (Silvex)

KS-NT,NELAC2,4,5-T

NELAC2,4-DB

KS-NT,NELACPicloram

KS-NT,NELACDinoseb

SIA1XAcifluorfen

SM 2540 G in Soil

SIA1X% Solids

Description Number ExpiresCode

E-10110Kansas Department of Health and Environment-KC 04/30/2012KS-KC

E-10287Kansas Department of Health and Environment 10/30/2011KS-NT

140Missouri Department of Natural Resources 04/30/2012MO-KC

IA001New Jersey Department of Environmental Protection 06/30/2011NELAC

95Iowa Department of Natural Resources 02/01/2012SIA1X

Notes and Definitions

QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC

batch were accepted based on percent recoveries and completeness of QC data.




Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 10 of 12

End of Report

Christine Dawson

Project Manager

Keystone Laboratories, Inc.




Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 11 of 12

COC Goes Here




Newton, IA 50208


Work Order: 11G0968

July 25, 2011

Page 12 of 12

COC Goes Here




Newton, IA 50208


July 28, 2011


RE:

Dear Pete Sazama:






Sincerely,


(618) 281-7173(618) 281-5120

TEL:FAX:



Page 1 of 14



Report Contents






Cover Letter 1

Report Contents 2

Definitions 3

Case Narrative 4


Sample Summary 10

Dates Report 11



Page 2 of 14


____TeklabHdrP

Definitions








DNI Did not ignite










MW Molecular weight











J - Analyte detected below quantitation limits M - Manual Integration used to determine area response

ND - Not Detected at the Reporting Limit R - RPD outside accepted recovery limits

S - Spike Recovery outside recovery limits X - Value exceeds Maximum Contaminant Level

Page 3 of 14


AbbrDefinition

CCVContinuing

Case Narrative






Cooler Receipt Temp: °C

Additional analyses to WO# 11070042.



____________________________________Collinsville



Phone (618) 344-1004

Fax (618) 344-1005


____________________________________Springfield



Phone (217) 698-1004

Fax (217) 698-1005


____________________________________Kansas City


Lenexa, KS 66214

Phone (913) 541-1998

Fax (913) 541-1998











Page 4 of 14


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch















SW-846 3050B, METALS BY GFAAThallium 7841 07/28/2011 8:280.185 mg/Kg-dry 10.435NELAP 69917

Page 5 of 14


TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch















Al, Ca, Fe, Mg Mn, K - Sample concentration was greater than 5 times the spike concentration.


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TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch
















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TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch
















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TeklabHdrP

Laboratory Results









Matrix: SOLID

Batch
















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TeklabHdrP

Matrix

Sample Summary






11071019-001 SBA-C3-01 (5-6) 06/29/2011 16:001Solid

11071019-002 SBA-B4-01 (5-6) 06/30/2011 8:001Solid

11071019-003 SBA-D5-01 (5-6) 06/30/2011 9:001Solid

11071019-004 SBA-A3-01 (5-6) 06/30/2011 10:001Solid

11071019-005 SBA-A5-01 (5-6) 06/30/2011 11:001Solid

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11071019-001


____TeklabHdrP


Dates Report






11071019-001A SBA-C3-01 (5-6) 06/29/2011 16:00 7/1/2011 3:50:00 PM




11071019-002A SBA-B4-01 (5-6) 06/30/2011 8:00 7/1/2011 3:50:00 PM




11071019-003A SBA-D5-01 (5-6) 06/30/2011 9:00 7/1/2011 3:50:00 PM




11071019-004A SBA-A3-01 (5-6) 06/30/2011 10:00 7/1/2011 3:50:00 PM




11071019-005A SBA-A5-01 (5-6) 06/30/2011 11:00 7/1/2011 3:50:00 PM




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11071019-001A








SampID: MB-69908


Analyses Result


Antimony 07/27/20115.00 5.00< 5.00 00 -100 100

SampID: LCS-69908


Analyses Result


Antimony 07/27/20115.00 50.051.8 103.70 85 115

SampID: 11071019-001AMS


Analyses Result


Antimony 07/27/20114.90 49.049.0 1000 75 125



Analyses Result


Antimony 07/27/20114.90 49.050.3 102.6 2.610 49.02

SampID: MB-69916


Analyses Result


Aluminum 07/27/20115.00 5.00< 5.00 00 -100 100

Beryllium 07/27/20110.10 0.10< 0.10 00 -100 100

Calcium 07/27/20115.00 5.00< 5.00 00 -100 100

Cobalt 07/27/20111.00 1.00< 1.00 00 -100 100

Copper 07/27/20111.00 1.00< 1.00 00 -100 100

Iron 07/27/20112.00 2.00< 2.00 00 -100 100

Magnesium 07/27/20111.00 1.00< 1.00 00 -100 100

Manganese 07/27/20110.50 0.50< 0.50 00 -100 100

Nickel 07/27/20111.00 1.00< 1.00 00 -100 100

Potassium 07/27/201110.0 10.0< 10.0 00 -100 100

Sodium 07/27/20115.00 5.00< 5.00 00 -100 100

Vanadium 07/27/20111.00 1.00< 1.00 00 -100 100

Zinc 07/27/20111.00 1.00< 1.00 00 -100 100

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SampID: LCS-69916


Analyses Result


Aluminum 07/27/20115.00 200208 104.00 85 115

Beryllium 07/27/20110.10 5.005.23 104.60 85 115

Calcium 07/27/20115.00 120124 103.70 85 115

Cobalt 07/27/20111.00 50.050.0 1000 85 115

Copper 07/27/20111.00 25.025.6 102.60 85 115

Iron 07/27/20112.00 100104 103.60 85 115

Magnesium 07/27/20111.00 75.080.8 107.80 85 115

Manganese 07/27/20110.50 50.053.0 106.00 85 115

Nickel 07/27/20111.00 50.053.3 106.60 85 115

Potassium 07/27/201110.0 120126 104.80 85 115

Sodium 07/27/20115.00 120128 106.90 85 115

Vanadium 07/27/20111.00 50.050.7 101.30 85 115

Zinc 07/27/20111.00 50.050.6 101.30 85 115

SampID: 11071019-002AMS


Analyses Result


Aluminum S 07/27/20114.55 18219000 225.018570 75 125

Beryllium 07/27/20110.09 4.545.41 102.20.7636 75 125

Calcium S 07/27/20114.55 10930000 -334233640 75 125

Cobalt 07/27/20110.91 45.452.6 89.012.13 75 125

Copper 07/27/20110.91 22.743.3 95.921.47 75 125

Iron S 07/27/20111.82 90.925500 -115026580 75 125

Magnesium S 07/27/20110.91 68.213300 426.713050 75 125

Manganese S 07/27/20110.45 45.4773 -106.2821.2 75 125

Nickel 07/27/20110.91 45.471.6 97.427.30 75 125

Potassium S 07/27/20119.09 1092950 184.22745 75 125

Sodium 07/27/20114.55 109295 108.0176.9 75 125

Vanadium 07/27/20110.91 45.477.6 104.630.00 75 125

Zinc 07/27/20110.91 45.4108 86.169.03 75 125

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Analyses Result


Aluminum S 07/27/20114.55 18218800 135.0 0.8718570 18980

Beryllium 07/27/20110.09 4.545.37 101.4 0.670.7636 5.409

Calcium S 07/27/20114.55 10932100 -1450 6.6533640 29990

Cobalt 07/27/20110.91 45.452.1 88.0 0.9012.13 52.60

Copper 07/27/20110.91 22.743.7 97.8 1.0021.47 43.26

Iron S 07/27/20111.82 90.924900 -1800 2.3426580 25540

Magnesium S 07/27/20110.91 68.212800 -360.0 4.1013050 13350

Manganese S 07/27/20110.45 45.4725 -212.6 6.46821.2 772.9

Nickel 07/27/20110.91 45.469.3 92.3 3.2527.30 71.56

Potassium S 07/27/20119.09 1092900 146.7 1.402745 2945

Sodium 07/27/20114.55 109304 116.6 3.13176.9 294.7

Vanadium 07/27/20110.91 45.474.3 97.6 4.2430.00 77.56

Zinc 07/27/20110.91 45.4107 84.3 0.7669.03 108.2


SampID: MB-69917


Analyses Result


Thallium 7841 07/28/20110.200 0.200< 0.200 00 -100 100

SampID: LCS-69917


Analyses Result


Thallium 7841 07/28/20110.200 1.501.30 86.90 80 120

SampID: 11071019-004AMS


Analyses Result


Thallium 7841 07/28/20110.182 1.362.02 128.30.2675 70 130



Analyses Result


Thallium 7841 07/28/20110.182 1.362.00 126.7 1.060.2675 2.017

Page 14 of 14


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