Technical Report - NYCEDCTOC_3]Metals by ICP[TOC] Sample Prepared by Method: EPA 200.7 CAS No....
Transcript of Technical Report - NYCEDCTOC_3]Metals by ICP[TOC] Sample Prepared by Method: EPA 200.7 CAS No....
Technical Report
prepared for:
Applemon Corporation151 S. Mountain Road
New City NY, 10956
Attention: Fuad Adib
Report Date: 01/22/2018
Client Project ID: Coney Island 3B, Brooklyn
York Project (SDG) No.: 18A0630
CT Cert. No. PH-0723 New Jersey Cert. No. CT005 and NY037 PA Cert. No. 68-04440
120 RESEARCH DRIVE
FAX (203) 357-0166(203) 325-1371
STRATFORD, CT 06615
New York Cert. Nos. 10854 and 12058
132-02 89th AVENUE RICHMOND HILL, NY 11418
www.YORKLAB.com [email protected]
Page 1 of 6
Client Sample IDYork Sample ID Matrix Date Collected Date Received
OF-118A0630-01 Water 01/18/2018 01/19/2018
OF-1 Filter18A0630-02 Water 01/18/2018 01/19/2018
Client Project ID: Coney Island 3B, Brooklyn
York Project (SDG) No.: 18A0630
Report Date: 01/22/2018
Attention: Fuad Adib
New City NY, 10956
151 S. Mountain Road
Applemon Corporation
Purpose and Results
This report contains the analytical data for the sample(s) identified on the attached chain-of-custody received in our laboratory
on January 19, 2018 and listed below. The project was identified as your project: Coney Island 3B, Brooklyn.
The analyses were conducted utilizing appropriate EPA, Standard Methods, and ASTM methods as detailed in the data
summary tables.
All samples were received in proper condition meeting the customary acceptance requirements for environmental samples
except those indicated under the Sample and Analysis Qualifiers section of this report.
All analyses met the method and laboratory standard operating procedure requirements except as indicated by any data flags,
the meaning of which are explained in the Sample and Data Qualifiers Relating to This Work Order section of this report and
case narrative if applicable.
The results of the analyses, which are all reported on dry weight basis (soils) unless otherwise noted, are detailed in the
following pages.
Please contact Client Services at 203.325.1371 with any questions regarding this report.
[TOC_1] Introduction and Sample Cross Reference [
Page 2 of 6
General Notes for York Project (SDG) No.: 18A0630
1. The RLs and MDLs (Reporting Limit and Method Detection Limit respectively) reported are adjusted for any dilution necessary due to
the levels of target and/or non-target analytes and matrix interference. The RL(REPORTING LIMIT) is based upon the lowest
standard utilized for the calibration where applicable.
2. Samples are retained for a period of thirty days after submittal of report, unless other arrangements are made.
3. York's liability for the above data is limited to the dollar value paid to York for the referenced project .
4. This report shall not be reproduced without the written approval of York Analytical Laboratories , Inc.
5. All analyses conducted met method or Laboratory SOP requirements. See the Sample and Data Qualifiers Section for further information.
6. It is noted that no analyses reported herein were subcontracted to another laboratory, unless noted in the report.
7. This report reflects results that relate only to the samples submitted on the attached chain-of-custody form(s) received by York.
8. Analyses conducted at York Analytical Laboratories, Inc. Stratford, CT are indicated by NY Cert. No. 10854; those conducted at York
Analytical Laboratories, Inc., Richmond Hill, NY are indicated by NY Cert. No. 12058.
Approved By:
Laboratory Director
Date: 01/22/2018
Benjamin Gulizia
OC_2]General Notes Relating to this Report[TOC]
Page 3 of 6
OF-1
York Project (SDG) No.
18A0630
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
January 18, 2018 2:00 pm 01/19/2018WaterConey Island 3B, Brooklyn
[TOC_2]OF-1[TOC]
18A0630-01
[TOC_3]Metals by ICP[TOC]
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Iron by EPA 200.7
0.316 mg/L 17439-89-6 BML01/22/2018 09:48 01/22/2018 12:590.0222 EPA 200.7Iron
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Manganese by EPA 200.7
0.137 mg/L 17439-96-5 BML01/22/2018 09:48 01/22/2018 12:590.00556 EPA 200.7Manganese
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
[TOC_3]Miscellaneous Physical Parameters[TOC]
Sample Prepared by Method: % Solids Prep
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Total Suspended Solids (EPA)
34.0 mg/L 1 TJM01/22/2018 12:06 01/22/2018 15:141.00 EPA 160.2* Total Suspended Solids
Certifications:
OF-1 Filter
York Project (SDG) No.
18A0630
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
January 18, 2018 2:00 pm 01/19/2018WaterConey Island 3B, Brooklyn
[TOC_2]OF-1 Filter[TOC]
18A0630-02
[TOC_3]Metals by ICP[TOC]
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Iron, Dissolved by EPA 200.7
0.945 mg/L 17439-89-6 BML01/22/2018 09:49 01/22/2018 13:480.0222 EPA 200.7Iron
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Manganese, Dissolved by EPA 200.7
0.137 mg/L 17439-96-5 BML01/22/2018 09:49 01/22/2018 13:480.00556 EPA 200.7Manganese
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
[TOC_1]Sample Results[TOC]
120 RESEARCH DRIVE
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STRATFORD, CT 06615 132-02 89th AVENUE RICHMOND HILL, NY 11418
www.YORKLAB.com [email protected] 4 of 6
[TOC_1]Notes and Specific Data Flags[Sample and Data Qualifiers Relating to This Work Order
Relative Percent DifferenceRPD
Not reportedNR
NOT DETECTED - the analyte is not detected at the Reported to level (LOQ/RL or LOD/MDL)ND
Low Bias flag indicates that the recovery of the flagged analyte is below the laboratory or regulatory lower control limit. The data user should take note
that this analyte may be biased low but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias
conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.
Low Bias
High Bias flag indicates that the recovery of the flagged analyte is above the laboratory or regulatory upper control limit. The data user should take
note that this analyte may be biased high but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias
conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.
High Bias
Non-Dir. Non-dir. flag (Non-Directional Bias ) indicates that the Relative Percent Difference (RPD) (a measure of precision) among the MS and MSD data is
outside the laboratory or regulatory control limit. This alerts the data user where the MS and MSD are from site-specific samples that the RPD is high
due to either non-homogeneous distribution of target analyte between the MS/MSD or indicates poor reproducibility for other reasons.
Wet The data has been reported on an as-received (wet weight) basis
REPORTING LIMIT - the minimum reportable value based upon the lowest point in the analyte calibration curve.
METHOD DETECTION LIMIT - a statistically derived estimate of the minimum amount of a substance an analytical system can reliably detect with a
99% confidence that the concentration of the substance is greater than zero. This is based upon 40 CFR Part 136 Appendix B and applies only to EPA
600 and 200 series methods.
RL
MDL
If EPA SW-846 method 8270 is included herein it is noted that the target compound N-nitrosodiphenylamine (NDPA) decomposes in the gas chromatographic inlet
and cannot be separated from diphenylamine (DPA). These results could actually represent 100% DPA, 100% NDPA or some combination of the two. For this
reason, York reports the combined result for n-nitrosodiphenylamine and diphenylamine for either of these compounds as a combined concentration as
Diphenylamine.
If Total PCBs are detected and the target aroclors reported are "Not detected", the Total PCB value is reported due to the presence of either or both Aroclors 1262 and
1268 which are non-target aroclors for some regulatory lists.
2-chloroethylvinyl ether readily breaks down under acidic conditions. Samples that are acid preserved, including standards will exhibit breakdown. The data user
should take note.
Semi-Volatile and Volatile analyses are reported down to the LOD/MDL, with values between the LOD/MDL and the LOQ being "J" flagged as estimated results.
Certification for pH is no longer offered by NYDOH ELAP.
*
LOQ LIMIT OF QUANTITATION - the minimum concentration of a target analyte that can be reported within a specified degree of confidence . This is the
lowest point in an analyte calibration curve that has been subjected to all steps of the processing/analysis and verified to meet defined criteria. This is
based upon NELAC 2009 Standards and applies to all analyses.
LOD LIMIT OF DETECTION - a verified estimate of the minimum concentration of a substance in a given matrix that an analytical process can reliably
detect. This is based upon NELAC 2009 Standards and applies to all analyses conducted under the auspices of EPA SW-846.
Reported to This indicates that the data for a particular analysis is reported to either the LOD/MDL, or the LOQ/RL. In cases where the "Reported to" is located
above the LOD/MDL, any value between this and the LOQ represents an estimated value which is "J" flagged accordingly. This applies to volatile and
semi-volatile target compounds only.
Analyte is not certified or the state of the samples origination does not offer certification for the Analyte .
For analyses by EPA SW-846-8270D, the Limit of Quantitation (LOQ) reported for benzidine is based upon the lowest standard used for calibration and is not a
verified LOQ due to this compound's propensity for oxidative losses during extraction/concentration procedures and non-reproducible chromatographic performance.
Definitions and Other Explanations
120 RESEARCH DRIVE
FAX (203) 357-0166(203) 325-1371
STRATFORD, CT 06615 132-02 89th AVENUE RICHMOND HILL, NY 11418
www.YORKLAB.com [email protected] 5 of 6
Technical Report
prepared for:
Applemon Corporation151 S. Mountain Road
New City NY, 10956
Attention: Fuad Adib
Report Date: 12/11/2017
Client Project ID: Coney Island 3B, Brooklyn
York Project (SDG) No.: 17L0294
CT Cert. No. PH-0723 New Jersey Cert. No. CT005 and NY037 PA Cert. No. 68-04440
120 RESEARCH DRIVE
FAX (203) 357-0166(203) 325-1371
STRATFORD, CT 06615
New York Cert. Nos. 10854 and 12058
132-02 89th AVENUE RICHMOND HILL, NY 11418
www.YORKLAB.com [email protected]
Page 1 of 8
Client Sample IDYork Sample ID Matrix Date Collected Date Received
OF-117L0294-01 Water 12/07/2017 12/08/2017
Client Project ID: Coney Island 3B, Brooklyn
York Project (SDG) No.: 17L0294
Report Date: 12/11/2017
Attention: Fuad Adib
New City NY, 10956
151 S. Mountain Road
Applemon Corporation
Purpose and Results
This report contains the analytical data for the sample(s) identified on the attached chain-of-custody received in our laboratory
on December 08, 2017 and listed below. The project was identified as your project: Coney Island 3B, Brooklyn.
The analyses were conducted utilizing appropriate EPA, Standard Methods, and ASTM methods as detailed in the data
summary tables.
All samples were received in proper condition meeting the customary acceptance requirements for environmental samples
except those indicated under the Sample and Analysis Qualifiers section of this report.
All analyses met the method and laboratory standard operating procedure requirements except as indicated by any data flags,
the meaning of which are explained in the Sample and Data Qualifiers Relating to This Work Order section of this report and
case narrative if applicable.
The results of the analyses, which are all reported on dry weight basis (soils) unless otherwise noted, are detailed in the
following pages.
Please contact Client Services at 203.325.1371 with any questions regarding this report.
[TOC_1] Introduction and Sample Cross Reference [
Page 2 of 8
General Notes for York Project (SDG) No.: 17L0294
1. The RLs and MDLs (Reporting Limit and Method Detection Limit respectively) reported are adjusted for any dilution necessary due to
the levels of target and/or non-target analytes and matrix interference. The RL(REPORTING LIMIT) is based upon the lowest
standard utilized for the calibration where applicable.
2. Samples are retained for a period of thirty days after submittal of report, unless other arrangements are made.
3. York's liability for the above data is limited to the dollar value paid to York for the referenced project .
4. This report shall not be reproduced without the written approval of York Analytical Laboratories , Inc.
5. All analyses conducted met method or Laboratory SOP requirements. See the Sample and Data Qualifiers Section for further information.
6. It is noted that no analyses reported herein were subcontracted to another laboratory, unless noted in the report.
7. This report reflects results that relate only to the samples submitted on the attached chain-of-custody form(s) received by York.
8. Analyses conducted at York Analytical Laboratories, Inc. Stratford, CT are indicated by NY Cert. No. 10854; those conducted at York
Analytical Laboratories, Inc., Richmond Hill, NY are indicated by NY Cert. No. 12058.
Approved By:
Laboratory Director
Date: 12/11/2017
Benjamin Gulizia
OC_2]General Notes Relating to this Report[TOC]
Page 3 of 8
OF-1
York Project (SDG) No.
17L0294
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
December 7, 2017 5:00 pm 12/08/2017WaterConey Island 3B, Brooklyn
[TOC_2] OF-1[TOC]
17L0294-01
[TOC_3]Volatile Organic Compounds by GC/MS[TOC]
Sample Prepared by Method: EPA 5030B
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Volatile Organics, BTEX, MTBE, Naphthalene
ND ug/L 171-43-2 SS12/08/2017 14:06 12/09/2017 02:570.50 EPA 624Benzene
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
ND ug/L 1100-41-4 SS12/08/2017 14:06 12/09/2017 02:570.50 EPA 624Ethyl Benzene
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
8.4 ug/L 11634-04-4 SS12/08/2017 14:06 12/09/2017 02:570.50 EPA 624* Methyl tert-butyl ether (MTBE)
Certifications:
ND ug/L 191-20-3 SS12/08/2017 14:06 12/09/2017 02:572.0 EPA 624* Naphthalene
Certifications:
ND ug/L 195-47-6 SS12/08/2017 14:06 12/09/2017 02:570.50 EPA 624o-Xylene
Certifications: CTDOH,NELAC-NY10854,NJDEP
ND ug/L 1179601-23-1 SS12/08/2017 14:06 12/09/2017 02:571.0 EPA 624p- & m- Xylenes
Certifications: CTDOH,NELAC-NY10854,NJDEP
ND ug/L 1108-88-3 SS12/08/2017 14:06 12/09/2017 02:570.50 EPA 624Toluene
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
ND ug/L 11330-20-7 SS12/08/2017 14:06 12/09/2017 02:571.5 EPA 624Xylenes, Total
Certifications: CTDOH,NELAC-NY10854,NJDEP
Surrogate Recoveries Result Acceptance Range
65-135106 %Surrogate: 1,2-Dichloroethane-d417060-07-0
81-11495.2 %Surrogate: p-Bromofluorobenzene460-00-4
86-11898.6 %Surrogate: Toluene-d82037-26-5
[TOC_3]Metals by ICP[TOC]
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Iron by EPA 200.7
2.46 mg/L 17439-89-6 BML12/11/2017 09:42 12/11/2017 13:180.0222 EPA 200.7Iron
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Lead by EPA 200.7
ND mg/L 17439-92-1 BML12/11/2017 09:42 12/11/2017 13:180.00556 EPA 200.7Lead
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Manganese by EPA 200.7
2.26 mg/L 17439-96-5 BML12/11/2017 09:42 12/11/2017 13:180.00556 EPA 200.7Manganese
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
[TOC_1]Sample Results[TOC]
120 RESEARCH DRIVE
FAX (203) 357-0166(203) 325-1371
STRATFORD, CT 06615 132-02 89th AVENUE RICHMOND HILL, NY 11418
www.YORKLAB.com [email protected] 4 of 8
OF-1
York Project (SDG) No.
17L0294
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
December 7, 2017 5:00 pm 12/08/2017WaterConey Island 3B, Brooklyn
17L0294-01
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Zinc by EPA 200.7
0.0417 mg/L 17440-66-6 BML12/11/2017 09:42 12/11/2017 13:180.0167 EPA 200.7Zinc
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
[TOC_3]Miscellaneous Physical Parameters[TOC]
Sample Prepared by Method: % Solids Prep
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Total Suspended Solids (EPA)
40.0 mg/L 1 TJM12/11/2017 10:54 12/11/2017 15:585.00 EPA 160.2* Total Suspended Solids
Certifications:
[TOC_3]Wet Chemistry Parameters[TOC]
Sample Prepared by Method: Analysis Preparation
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Oil & Grease
8.21 mg/L 1OILGREASE TJM12/11/2017 10:50 12/11/2017 15:540.526 EPA 1664AOil & Grease
Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP
120 RESEARCH DRIVE
FAX (203) 357-0166(203) 325-1371
STRATFORD, CT 06615 132-02 89th AVENUE RICHMOND HILL, NY 11418
www.YORKLAB.com [email protected] 5 of 8
Volatile Analysis Sample Containers
Volatile Sample ContainerClient Sample IDLab ID
17L0294-01 40mL Clear Vial (pre-pres.) HCl; Cool to 4° C OF-1
120 RESEARCH DRIVE
FAX (203) 357-0166(203) 325-1371
STRATFORD, CT 06615 132-02 89th AVENUE RICHMOND HILL, NY 11418
www.YORKLAB.com [email protected] 6 of 8
[TOC_1]Notes and Specific Data Flags[Sample and Data Qualifiers Relating to This Work Order
Relative Percent DifferenceRPD
Not reportedNR
NOT DETECTED - the analyte is not detected at the Reported to level (LOQ/RL or LOD/MDL)ND
Low Bias flag indicates that the recovery of the flagged analyte is below the laboratory or regulatory lower control limit. The data user should take note
that this analyte may be biased low but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias
conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.
Low Bias
High Bias flag indicates that the recovery of the flagged analyte is above the laboratory or regulatory upper control limit. The data user should take
note that this analyte may be biased high but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias
conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.
High Bias
Non-Dir. Non-dir. flag (Non-Directional Bias ) indicates that the Relative Percent Difference (RPD) (a measure of precision) among the MS and MSD data is
outside the laboratory or regulatory control limit. This alerts the data user where the MS and MSD are from site-specific samples that the RPD is high
due to either non-homogeneous distribution of target analyte between the MS/MSD or indicates poor reproducibility for other reasons.
Wet The data has been reported on an as-received (wet weight) basis
REPORTING LIMIT - the minimum reportable value based upon the lowest point in the analyte calibration curve.
METHOD DETECTION LIMIT - a statistically derived estimate of the minimum amount of a substance an analytical system can reliably detect with a
99% confidence that the concentration of the substance is greater than zero. This is based upon 40 CFR Part 136 Appendix B and applies only to EPA
600 and 200 series methods.
RL
MDL
If EPA SW-846 method 8270 is included herein it is noted that the target compound N-nitrosodiphenylamine (NDPA) decomposes in the gas chromatographic inlet
and cannot be separated from diphenylamine (DPA). These results could actually represent 100% DPA, 100% NDPA or some combination of the two. For this
reason, York reports the combined result for n-nitrosodiphenylamine and diphenylamine for either of these compounds as a combined concentration as
Diphenylamine.
If Total PCBs are detected and the target aroclors reported are "Not detected", the Total PCB value is reported due to the presence of either or both Aroclors 1262 and
1268 which are non-target aroclors for some regulatory lists.
2-chloroethylvinyl ether readily breaks down under acidic conditions. Samples that are acid preserved, including standards will exhibit breakdown. The data user
should take note.
Semi-Volatile and Volatile analyses are reported down to the LOD/MDL, with values between the LOD/MDL and the LOQ being "J" flagged as estimated results.
Certification for pH is no longer offered by NYDOH ELAP.
*
LOQ LIMIT OF QUANTITATION - the minimum concentration of a target analyte that can be reported within a specified degree of confidence . This is the
lowest point in an analyte calibration curve that has been subjected to all steps of the processing/analysis and verified to meet defined criteria. This is
based upon NELAC 2009 Standards and applies to all analyses.
LOD LIMIT OF DETECTION - a verified estimate of the minimum concentration of a substance in a given matrix that an analytical process can reliably
detect. This is based upon NELAC 2009 Standards and applies to all analyses conducted under the auspices of EPA SW-846.
Reported to This indicates that the data for a particular analysis is reported to either the LOD/MDL, or the LOQ/RL. In cases where the "Reported to" is located
above the LOD/MDL, any value between this and the LOQ represents an estimated value which is "J" flagged accordingly. This applies to volatile and
semi-volatile target compounds only.
Analyte is not certified or the state of the samples origination does not offer certification for the Analyte .
For analyses by EPA SW-846-8270D, the Limit of Quantitation (LOQ) reported for benzidine is based upon the lowest standard used for calibration and is not a
verified LOQ due to this compound's propensity for oxidative losses during extraction/concentration procedures and non-reproducible chromatographic performance.
Definitions and Other Explanations
120 RESEARCH DRIVE
FAX (203) 357-0166(203) 325-1371
STRATFORD, CT 06615 132-02 89th AVENUE RICHMOND HILL, NY 11418
www.YORKLAB.com [email protected] 7 of 8
Technical Report
prepared for:
Applemon Corporation151 S. Mountain Road
New City NY, 10956
Attention: Fuad Adib
Report Date: 11/30/2017
Client Project ID: Coney Island 3B, Brooklyn
York Project (SDG) No.: 17K0879
CT Cert. No. PH-0723 New Jersey Cert. No. CT005 and NY037 PA Cert. No. 68-04440
120 RESEARCH DRIVE
FAX (203) 357-0166(203) 325-1371
STRATFORD, CT 06615
1.0Revision No.
New York Cert. Nos. 10854 and 12058
132-02 89th AVENUE RICHMOND HILL, NY 11418
www.YORKLAB.com [email protected]
Page 1 of 11
Client Sample IDYork Sample ID Matrix Date Collected Date Received
OF-117K0879-01 Water 11/21/2017 11/22/2017
OF-817K0879-02 Water 11/21/2017 11/22/2017
Client Project ID: Coney Island 3B, Brooklyn
York Project (SDG) No.: 17K0879
Report Date: 11/30/2017
Attention: Fuad Adib
New City NY, 10956
151 S. Mountain Road
Applemon Corporation
Purpose and Results
This report contains the analytical data for the sample(s) identified on the attached chain-of-custody received in our laboratory
on November 22, 2017 and listed below. The project was identified as your project: Coney Island 3B, Brooklyn.
The analyses were conducted utilizing appropriate EPA, Standard Methods, and ASTM methods as detailed in the data
summary tables.
All samples were received in proper condition meeting the customary acceptance requirements for environmental samples
except those indicated under the Sample and Analysis Qualifiers section of this report.
All analyses met the method and laboratory standard operating procedure requirements except as indicated by any data flags,
the meaning of which are explained in the Sample and Data Qualifiers Relating to This Work Order section of this report and
case narrative if applicable.
The results of the analyses, which are all reported on dry weight basis (soils) unless otherwise noted, are detailed in the
following pages.
Please contact Client Services at 203.325.1371 with any questions regarding this report.
[TOC_1] Introduction and Sample Cross Reference [
Page 2 of 11
General Notes for York Project (SDG) No.: 17K0879
1. The RLs and MDLs (Reporting Limit and Method Detection Limit respectively) reported are adjusted for any dilution necessary due to
the levels of target and/or non-target analytes and matrix interference. The RL(REPORTING LIMIT) is based upon the lowest
standard utilized for the calibration where applicable.
2. Samples are retained for a period of thirty days after submittal of report, unless other arrangements are made.
3. York's liability for the above data is limited to the dollar value paid to York for the referenced project .
4. This report shall not be reproduced without the written approval of York Analytical Laboratories , Inc.
5. All analyses conducted met method or Laboratory SOP requirements. See the Sample and Data Qualifiers Section for further information.
6. It is noted that no analyses reported herein were subcontracted to another laboratory, unless noted in the report.
7. This report reflects results that relate only to the samples submitted on the attached chain-of-custody form(s) received by York.
8. Analyses conducted at York Analytical Laboratories, Inc. Stratford, CT are indicated by NY Cert. No. 10854; those conducted at York
Analytical Laboratories, Inc., Richmond Hill, NY are indicated by NY Cert. No. 12058.
Approved By:
Laboratory Director
Date: 11/30/2017
Benjamin Gulizia
OC_2]General Notes Relating to this Report[TOC]
Page 3 of 11
OF-1
York Project (SDG) No.
17K0879
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
November 21, 2017 3:00 pm 11/22/2017WaterConey Island 3B, Brooklyn
[TOC_2]OF-1[TOC]
17K0879-01
[TOC_3]Volatile Organic Compounds by GC/MS[TOC]
Sample Prepared by Method: EPA 5030B
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Volatile Organics, BTEX, MTBE, Naphthalene
ND ug/L 171-43-2 SR11/30/2017 07:30 11/30/2017 13:070.50 EPA 624Benzene
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
ND ug/L 1100-41-4 SR11/30/2017 07:30 11/30/2017 13:070.50 EPA 624Ethyl Benzene
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
2.2 ug/L 11634-04-4 SR11/30/2017 07:30 11/30/2017 13:070.50 EPA 624* Methyl tert-butyl ether (MTBE)
Certifications:
ND ug/L 191-20-3 SR11/30/2017 07:30 11/30/2017 13:072.0 EPA 624* Naphthalene
Certifications:
ND ug/L 195-47-6 SR11/30/2017 07:30 11/30/2017 13:070.50 EPA 624o-Xylene
Certifications: CTDOH,NELAC-NY10854,NJDEP
ND ug/L 1179601-23-1 SR11/30/2017 07:30 11/30/2017 13:071.0 EPA 624p- & m- Xylenes
Certifications: CTDOH,NELAC-NY10854,NJDEP
ND ug/L 1108-88-3 SR11/30/2017 07:30 11/30/2017 13:070.50 EPA 624Toluene
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
ND ug/L 11330-20-7 SR11/30/2017 07:30 11/30/2017 13:071.5 EPA 624Xylenes, Total
Certifications: CTDOH,NELAC-NY10854,NJDEP
Surrogate Recoveries Result Acceptance Range
65-135113 %Surrogate: 1,2-Dichloroethane-d417060-07-0
81-11499.7 %Surrogate: p-Bromofluorobenzene460-00-4
86-11897.0 %Surrogate: Toluene-d82037-26-5
[TOC_3]Metals by ICP[TOC]
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Iron by EPA 200.7
0.283 mg/L 17439-89-6 BML11/27/2017 11:22 11/27/2017 19:430.0222 EPA 200.7Iron
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Lead by EPA 200.7
ND mg/L 17439-92-1 BML11/27/2017 11:22 11/27/2017 19:430.00556 EPA 200.7Lead
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Manganese by EPA 200.7
0.528 mg/L 17439-96-5 BML11/27/2017 11:22 11/27/2017 19:430.00556 EPA 200.7Manganese
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
[TOC_1]Sample Results[TOC]
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OF-1
York Project (SDG) No.
17K0879
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
November 21, 2017 3:00 pm 11/22/2017WaterConey Island 3B, Brooklyn
17K0879-01
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Zinc by EPA 200.7
0.101 mg/L 17440-66-6 BML11/27/2017 11:22 11/27/2017 19:430.0167 EPA 200.7Zinc
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
[TOC_3]Miscellaneous Physical Parameters[TOC]
Sample Prepared by Method: % Solids Prep
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Total Suspended Solids (EPA)
25.2 mg/L 1 AA11/27/2017 17:45 11/27/2017 17:454.00 EPA 160.2* Total Suspended Solids
Certifications:
[TOC_3]Wet Chemistry Parameters[TOC]
Sample Prepared by Method: Analysis Preparation
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Oil & Grease
ND mg/L 1OILGREASE AA11/29/2017 19:22 11/30/2017 02:200.541 EPA 1664AOil & Grease
Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP
OF-8
York Project (SDG) No.
17K0879
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
November 21, 2017 3:00 pm 11/22/2017WaterConey Island 3B, Brooklyn
[TOC_2]OF-8[TOC]
17K0879-02
[TOC_3]Volatile Organic Compounds by GC/MS[TOC]
Sample Prepared by Method: EPA 5030B
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Volatile Organics, BTEX, MTBE, Naphthalene
ND ug/L 171-43-2 SR11/30/2017 07:30 11/30/2017 13:350.50 EPA 624Benzene
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
ND ug/L 1100-41-4 SR11/30/2017 07:30 11/30/2017 13:350.50 EPA 624Ethyl Benzene
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
ND ug/L 11634-04-4 SR11/30/2017 07:30 11/30/2017 13:350.50 EPA 624* Methyl tert-butyl ether (MTBE)
Certifications:
ND ug/L 191-20-3 SR11/30/2017 07:30 11/30/2017 13:352.0 EPA 624* Naphthalene
Certifications:
ND ug/L 195-47-6 SR11/30/2017 07:30 11/30/2017 13:350.50 EPA 624o-Xylene
Certifications: CTDOH,NELAC-NY10854,NJDEP
ND ug/L 1179601-23-1 SR11/30/2017 07:30 11/30/2017 13:351.0 EPA 624p- & m- Xylenes
Certifications: CTDOH,NELAC-NY10854,NJDEP
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OF-8
York Project (SDG) No.
17K0879
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
November 21, 2017 3:00 pm 11/22/2017WaterConey Island 3B, Brooklyn
17K0879-02
Sample Prepared by Method: EPA 5030B
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Volatile Organics, BTEX, MTBE, Naphthalene
ND ug/L 1108-88-3 SR11/30/2017 07:30 11/30/2017 13:350.50 EPA 624Toluene
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
ND ug/L 11330-20-7 SR11/30/2017 07:30 11/30/2017 13:351.5 EPA 624Xylenes, Total
Certifications: CTDOH,NELAC-NY10854,NJDEP
Surrogate Recoveries Result Acceptance Range
65-135101 %Surrogate: 1,2-Dichloroethane-d417060-07-0
81-114106 %Surrogate: p-Bromofluorobenzene460-00-4
86-11899.0 %Surrogate: Toluene-d82037-26-5
[TOC_3]Metals by ICP[TOC]
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Iron by EPA 200.7
0.303 mg/L 17439-89-6 BML11/27/2017 11:22 11/27/2017 19:510.0222 EPA 200.7Iron
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Lead by EPA 200.7
ND mg/L 17439-92-1 BML11/27/2017 11:22 11/27/2017 19:510.00556 EPA 200.7Lead
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Manganese by EPA 200.7
0.196 mg/L 17439-96-5 BML11/27/2017 11:22 11/27/2017 19:510.00556 EPA 200.7Manganese
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Zinc by EPA 200.7
0.0191 mg/L 17440-66-6 BML11/27/2017 11:22 11/27/2017 19:510.0167 EPA 200.7Zinc
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
[TOC_3]Miscellaneous Physical Parameters[TOC]
Sample Prepared by Method: % Solids Prep
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Total Suspended Solids (EPA)
4.40 mg/L 1 AA11/27/2017 17:45 11/27/2017 17:454.00 EPA 160.2* Total Suspended Solids
Certifications:
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OF-8
York Project (SDG) No.
17K0879
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
November 21, 2017 3:00 pm 11/22/2017WaterConey Island 3B, Brooklyn
17K0879-02
[TOC_3]Wet Chemistry Parameters[TOC]
Sample Prepared by Method: Analysis Preparation
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Oil & Grease
ND mg/L 1OILGREASE AA11/29/2017 19:22 11/30/2017 02:200.571 EPA 1664AOil & Grease
Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP
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Volatile Analysis Sample Containers
Volatile Sample ContainerClient Sample IDLab ID
17K0879-01 40mL Clear Vial (pre-pres.) HCl; Cool to 4° COF-1
17K0879-02 40mL Clear Vial (pre-pres.) HCl; Cool to 4° COF-8
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[TOC_1]Notes and Specific Data Flags[Sample and Data Qualifiers Relating to This Work Order
QL-02 This LCS analyte is outside Laboratory Recovery limits due the analyte behavior using the referenced method. The reference
method has certain limitations with respect to analytes of this nature.
Relative Percent DifferenceRPD
Not reportedNR
NOT DETECTED - the analyte is not detected at the Reported to level (LOQ/RL or LOD/MDL)ND
Low Bias flag indicates that the recovery of the flagged analyte is below the laboratory or regulatory lower control limit. The data user should take note
that this analyte may be biased low but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias
conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.
Low Bias
High Bias flag indicates that the recovery of the flagged analyte is above the laboratory or regulatory upper control limit. The data user should take
note that this analyte may be biased high but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias
conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.
High Bias
Non-Dir. Non-dir. flag (Non-Directional Bias ) indicates that the Relative Percent Difference (RPD) (a measure of precision) among the MS and MSD data is
outside the laboratory or regulatory control limit. This alerts the data user where the MS and MSD are from site-specific samples that the RPD is high
due to either non-homogeneous distribution of target analyte between the MS/MSD or indicates poor reproducibility for other reasons.
Wet The data has been reported on an as-received (wet weight) basis
REPORTING LIMIT - the minimum reportable value based upon the lowest point in the analyte calibration curve.
METHOD DETECTION LIMIT - a statistically derived estimate of the minimum amount of a substance an analytical system can reliably detect with a
99% confidence that the concentration of the substance is greater than zero. This is based upon 40 CFR Part 136 Appendix B and applies only to EPA
600 and 200 series methods.
RL
MDL
If EPA SW-846 method 8270 is included herein it is noted that the target compound N-nitrosodiphenylamine (NDPA) decomposes in the gas chromatographic inlet
and cannot be separated from diphenylamine (DPA). These results could actually represent 100% DPA, 100% NDPA or some combination of the two. For this
reason, York reports the combined result for n-nitrosodiphenylamine and diphenylamine for either of these compounds as a combined concentration as
Diphenylamine.
If Total PCBs are detected and the target aroclors reported are "Not detected", the Total PCB value is reported due to the presence of either or both Aroclors 1262 and
1268 which are non-target aroclors for some regulatory lists.
2-chloroethylvinyl ether readily breaks down under acidic conditions. Samples that are acid preserved, including standards will exhibit breakdown. The data user
should take note.
Semi-Volatile and Volatile analyses are reported down to the LOD/MDL, with values between the LOD/MDL and the LOQ being "J" flagged as estimated results.
Certification for pH is no longer offered by NYDOH ELAP.
*
LOQ LIMIT OF QUANTITATION - the minimum concentration of a target analyte that can be reported within a specified degree of confidence . This is the
lowest point in an analyte calibration curve that has been subjected to all steps of the processing/analysis and verified to meet defined criteria. This is
based upon NELAC 2009 Standards and applies to all analyses.
LOD LIMIT OF DETECTION - a verified estimate of the minimum concentration of a substance in a given matrix that an analytical process can reliably
detect. This is based upon NELAC 2009 Standards and applies to all analyses conducted under the auspices of EPA SW-846.
Reported to This indicates that the data for a particular analysis is reported to either the LOD/MDL, or the LOQ/RL. In cases where the "Reported to" is located
above the LOD/MDL, any value between this and the LOQ represents an estimated value which is "J" flagged accordingly. This applies to volatile and
semi-volatile target compounds only.
Analyte is not certified or the state of the samples origination does not offer certification for the Analyte .
For analyses by EPA SW-846-8270D, the Limit of Quantitation (LOQ) reported for benzidine is based upon the lowest standard used for calibration and is not a
verified LOQ due to this compound's propensity for oxidative losses during extraction/concentration procedures and non-reproducible chromatographic performance.
Definitions and Other Explanations
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Revision Description: This report has been revised to correct RLs.
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Technical Report
prepared for:
Triumph Construction1354 Seneca Avenue
Bronx NY, 10474
Attention: Antonio Seminatore
Report Date: 01/19/2018
Client Project ID: Coney Island
York Project (SDG) No.: 18A0334
CT Cert. No. PH-0723 New Jersey Cert. No. CT005 and NY037 PA Cert. No. 68-04440
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132-02 89th AVENUE RICHMOND HILL, NY 11418
www.YORKLAB.com [email protected]
Page 1 of 8
Client Sample IDYork Sample ID Matrix Date Collected Date Received
Water Sample #218A0334-01 Water 01/11/2018 01/12/2018
Client Project ID: Coney Island
York Project (SDG) No.: 18A0334
Report Date: 01/19/2018
Attention: Antonio Seminatore
Bronx NY, 10474
1354 Seneca Avenue
Triumph Construction
Purpose and Results
This report contains the analytical data for the sample(s) identified on the attached chain-of-custody received in our laboratory
on January 12, 2018 and listed below. The project was identified as your project: Coney Island.
The analyses were conducted utilizing appropriate EPA, Standard Methods, and ASTM methods as detailed in the data
summary tables.
All samples were received in proper condition meeting the customary acceptance requirements for environmental samples
except those indicated under the Sample and Analysis Qualifiers section of this report.
All analyses met the method and laboratory standard operating procedure requirements except as indicated by any data flags,
the meaning of which are explained in the Sample and Data Qualifiers Relating to This Work Order section of this report and
case narrative if applicable.
The results of the analyses, which are all reported on dry weight basis (soils) unless otherwise noted, are detailed in the
following pages.
Please contact Client Services at 203.325.1371 with any questions regarding this report.
[TOC_1] Introduction and Sample Cross Reference [
Page 2 of 8
General Notes for York Project (SDG) No.: 18A0334
1. The RLs and MDLs (Reporting Limit and Method Detection Limit respectively) reported are adjusted for any dilution necessary due to
the levels of target and/or non-target analytes and matrix interference. The RL(REPORTING LIMIT) is based upon the lowest
standard utilized for the calibration where applicable.
2. Samples are retained for a period of thirty days after submittal of report, unless other arrangements are made.
3. York's liability for the above data is limited to the dollar value paid to York for the referenced project .
4. This report shall not be reproduced without the written approval of York Analytical Laboratories , Inc.
5. All analyses conducted met method or Laboratory SOP requirements. See the Sample and Data Qualifiers Section for further information.
6. It is noted that no analyses reported herein were subcontracted to another laboratory, unless noted in the report.
7. This report reflects results that relate only to the samples submitted on the attached chain-of-custody form(s) received by York.
8. Analyses conducted at York Analytical Laboratories, Inc. Stratford, CT are indicated by NY Cert. No. 10854; those conducted at York
Analytical Laboratories, Inc., Richmond Hill, NY are indicated by NY Cert. No. 12058.
Approved By:
Laboratory Director
Date: 01/19/2018
Benjamin Gulizia
OC_2]General Notes Relating to this Report[TOC]
Page 3 of 8
Water Sample #2
York Project (SDG) No.
18A0334
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
January 11, 2018 3:00 pm 01/12/2018WaterConey Island
[TOC_2]Water Sample #2[TOC]
18A0334-01
[TOC_3]Volatile Organic Compounds by GC/MS[TOC]
Sample Prepared by Method: EPA 5030B
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Volatile Organics, 624 - BTEX List-Low Level
ND ug/L 171-43-2 SS01/15/2018 07:30 01/15/2018 18:240.50 EPA 624Benzene
Certifications: CTDOH,NELAC-NY10854,NJDEP
ND ug/L 191-20-3 SS01/15/2018 07:30 01/15/2018 18:242.0 EPA 624* Naphthalene
Certifications:
ND ug/L 1100-41-4 SS01/15/2018 07:30 01/15/2018 18:240.50 EPA 624Ethyl Benzene
Certifications: CTDOH,NELAC-NY10854,NJDEP
ND ug/L 11634-04-4 SS01/15/2018 07:30 01/15/2018 18:240.50 EPA 624Methyl tert-butyl ether (MTBE)
Certifications: CTDOH,NELAC-NY10854,NJDEP
ND ug/L 1108-88-3 SS01/15/2018 07:30 01/15/2018 18:240.50 EPA 624Toluene
Certifications: CTDOH,NELAC-NY10854,NJDEP
ND ug/L 11330-20-7 SS01/15/2018 07:30 01/15/2018 18:241.5 EPA 624Xylenes, Total
Certifications: CTDOH,NELAC-NY10854,NJDEP
Surrogate Recoveries Result Acceptance Range
78-126103 %Surrogate: 1,2-Dichloroethane-d417060-07-0
71-13098.9 %Surrogate: p-Bromofluorobenzene460-00-4
84-11796.4 %Surrogate: Toluene-d82037-26-5
[TOC_3]Metals by ICP[TOC]
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Iron by EPA 200.7
0.0442 mg/L 17439-89-6 BML01/15/2018 11:39 01/15/2018 21:340.0222 EPA 200.7Iron
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Lead by EPA 200.7
ND mg/L 17439-92-1 BML01/15/2018 11:39 01/15/2018 21:340.00556 EPA 200.7Lead
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Manganese by EPA 200.7
0.137 mg/L 17439-96-5 BML01/15/2018 11:39 01/15/2018 21:340.00556 EPA 200.7Manganese
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Zinc by EPA 200.7
[TOC_1]Sample Results[TOC]
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Water Sample #2
York Project (SDG) No.
18A0334
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix Collection Date/Time Date Received
January 11, 2018 3:00 pm 01/12/2018WaterConey Island
18A0334-01
Sample Prepared by Method: EPA 200.7
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Zinc by EPA 200.7
0.0192 mg/L 17440-66-6 BML01/15/2018 11:39 01/15/2018 21:340.0167 EPA 200.7Zinc
Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP
[TOC_3]Miscellaneous Physical Parameters[TOC]
Sample Prepared by Method: % Solids Prep
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Total Suspended Solids
ND mg/L 1 AA01/17/2018 23:38 01/18/2018 03:355.00 SM 2540DTotal Suspended Solids
Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP
[TOC_3]Wet Chemistry Parameters[TOC]
Sample Prepared by Method: Analysis Preparation
Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time
Sample Notes:Log-in Notes:
LOQ
Reported to
Oil & Grease
ND mg/L 1OILGREASE AA01/17/2018 01:22 01/17/2018 01:280.500 EPA 1664AOil & Grease
Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP
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Volatile Analysis Sample Containers
Volatile Sample ContainerClient Sample IDLab ID
18A0334-01 40mL Clear Vial (pre-pres.) HCl; Cool to 4° CWater Sample #2
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[TOC_1]Notes and Specific Data Flags[Sample and Data Qualifiers Relating to This Work Order
Relative Percent DifferenceRPD
Not reportedNR
NOT DETECTED - the analyte is not detected at the Reported to level (LOQ/RL or LOD/MDL)ND
Low Bias flag indicates that the recovery of the flagged analyte is below the laboratory or regulatory lower control limit. The data user should take note
that this analyte may be biased low but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias
conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.
Low Bias
High Bias flag indicates that the recovery of the flagged analyte is above the laboratory or regulatory upper control limit. The data user should take
note that this analyte may be biased high but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias
conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.
High Bias
Non-Dir. Non-dir. flag (Non-Directional Bias ) indicates that the Relative Percent Difference (RPD) (a measure of precision) among the MS and MSD data is
outside the laboratory or regulatory control limit. This alerts the data user where the MS and MSD are from site-specific samples that the RPD is high
due to either non-homogeneous distribution of target analyte between the MS/MSD or indicates poor reproducibility for other reasons.
Wet The data has been reported on an as-received (wet weight) basis
REPORTING LIMIT - the minimum reportable value based upon the lowest point in the analyte calibration curve.
METHOD DETECTION LIMIT - a statistically derived estimate of the minimum amount of a substance an analytical system can reliably detect with a
99% confidence that the concentration of the substance is greater than zero. This is based upon 40 CFR Part 136 Appendix B and applies only to EPA
600 and 200 series methods.
RL
MDL
If EPA SW-846 method 8270 is included herein it is noted that the target compound N-nitrosodiphenylamine (NDPA) decomposes in the gas chromatographic inlet
and cannot be separated from diphenylamine (DPA). These results could actually represent 100% DPA, 100% NDPA or some combination of the two. For this
reason, York reports the combined result for n-nitrosodiphenylamine and diphenylamine for either of these compounds as a combined concentration as
Diphenylamine.
If Total PCBs are detected and the target aroclors reported are "Not detected", the Total PCB value is reported due to the presence of either or both Aroclors 1262 and
1268 which are non-target aroclors for some regulatory lists.
2-chloroethylvinyl ether readily breaks down under acidic conditions. Samples that are acid preserved, including standards will exhibit breakdown. The data user
should take note.
Semi-Volatile and Volatile analyses are reported down to the LOD/MDL, with values between the LOD/MDL and the LOQ being "J" flagged as estimated results.
Certification for pH is no longer offered by NYDOH ELAP.
*
LOQ LIMIT OF QUANTITATION - the minimum concentration of a target analyte that can be reported within a specified degree of confidence . This is the
lowest point in an analyte calibration curve that has been subjected to all steps of the processing/analysis and verified to meet defined criteria. This is
based upon NELAC 2009 Standards and applies to all analyses.
LOD LIMIT OF DETECTION - a verified estimate of the minimum concentration of a substance in a given matrix that an analytical process can reliably
detect. This is based upon NELAC 2009 Standards and applies to all analyses conducted under the auspices of EPA SW-846.
Reported to This indicates that the data for a particular analysis is reported to either the LOD/MDL, or the LOQ/RL. In cases where the "Reported to" is located
above the LOD/MDL, any value between this and the LOQ represents an estimated value which is "J" flagged accordingly. This applies to volatile and
semi-volatile target compounds only.
Analyte is not certified or the state of the samples origination does not offer certification for the Analyte .
For analyses by EPA SW-846-8270D, the Limit of Quantitation (LOQ) reported for benzidine is based upon the lowest standard used for calibration and is not a
verified LOQ due to this compound's propensity for oxidative losses during extraction/concentration procedures and non-reproducible chromatographic performance.
Definitions and Other Explanations
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