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    DEPARTMENT OF MECHANICAL ENGINEERING

    B.E. III SEM

    MATERIAL TESTING LAB

    1. To determine the Rockwell Hardness of given materials.

    2. To determine the hardness by Vicker Hardness Testing machine.3. To determine the Brinell Hardness Number of given materials.

    4. To determine impact strength of material by impact testing machine using

    Izod Test.

    5. To determine impact strength of material by impact testing machine using

    Chary Test.

    6. To study of Universal Testing Machine.

    7. To perform Tensile Test of mild steel and to draw stress-strain curve.8. To determined the Compressive Test strength of wood (1) along the

    grains, (2) across the grains.

    9. To determine Shear Test strength of given mild steel specimen.

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    EXPERIMENT NO. .

    SHEAR TESTOBJECT : To determine Shear strength of given mild steel specimen. Using UTM.

    THEORY : A type of force which causes or tends to cause two continues parts of the

    body to slide relative to each other in a direction parallel to their plane of

    contact is called the shear force. The stress required to produce fracturein the plane of cross-section, acted on by shear force is called shear

    strength.

    For determining shear strength, a suitable length of steel

    specimen in uniform cross-section is subjected to double shear, using a

    suitable test-rig as shown in figure in universal testing machine under a

    compressive test. The shear strength shall be calculated from the formula

    F = ---------------- =

    2. ----- d24

    where F is the shear force and d is the diameter of specimen.

    For metals, cross shearing tests are usually made in rivets other

    bars of circular cross-section. Shearing tests have not been specified to any

    appreciable extent for acceptance purpose and they are rarely used.

    Shear Test

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    PROCEDURE:(1) Prepare the specimen as per standards.

    (2) Measure the diameter of the test specimen by means of micrometer at

    each of the section to be sheared.

    (3) Insert the specimen in the shear-rig properly.

    (4) Fix the shear-rig in between the fixed head and movable head of theuniversal testing machine.

    (5) Start the machine load at slowest speed to the ultimate which is indicated

    by an abrupt reduction in load. Record this reading and stop the machine

    as soon as the specimen fractures.

    OBSERVATION:

    Diameter of test specimen, ---------- d = -------mm

    Area of the cross-section, -------d2 = ------mm2

    4

    Ultimate shearing load, --------F = -------N

    CALCULATION:

    The shear stress will be given by the formula

    F = ------------------ =

    2. ----- d2

    4RESULT:

    Shear strength of mild steel specimen = --------- N/mm2

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    EXPERIMENT NO.

    STUDY OF UNIVERSAL TESTING MACHINE

    DESCRIPTION : Some types of testing machine are used to evaluates properties of

    materials. The primary tests in tension, compression, flexure and

    hardness performed on so called universal testing machine.The universal testing machines are of many types, all of them consisting

    essentially of two parts (1) the straining mechanism (2) the load weighing

    mechanism. With suitable arrangements of gripping of bearing device, the

    specimen to be tested is interposed between fixed head and movable head.

    The measurement or weighing of the load on the specimen is accomplished by

    means of lever system, by pressure cells or by other devices through which the

    straining load or some known portion of it must pass.

    The movable head of the universal testing machine actuated

    either by a gear and screw system or by hydraulically. The load is weighed

    either by levers and a scale beam on which is mounted a movable pointer or by

    an hydraulic gauge.

    STUDY OF MACHINE:

    Study the machine assigned giving special attention to each of

    the following features.

    (1) Capacity, make type and other main features of machine.

    (2) Starting, stopping, reversing and speed controls.

    (3) Straining mechanism.

    (4) Provision for taking care of eccentric positioning of specimen in the

    machine.

    (5) Provision for adjusting the plane of the head to parallelism with the plane of

    the specimen in compression test.

    (6) Provision for gripping tensile specimens.

    (7) Weighing or load-measuring arrangement.

    (8) Various attachment and fixtures used for different type of specimens and

    for different tests.

    DETERMINATIONS TO BE MADE AND RECORDED :

    (1) Types of tests for which machine may be used.

    (2) Maximum size of specimen of each type which the machine can

    accommodate.

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    REPORT ;

    (1) Tabulate the main characteristics of machine.

    (2) Draw a line diagram showing loading arrangement and load measuring

    arrangement.

    (3) Draw line sketch of fixing arrangement of specimen in different tests.

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    EXPERIMENT No. ..

    THE ROCKWELL HARDNESS TESTING MACHINE

    OBJECT : To determine the Rockwell hardness of given materials.

    THEORY : This test utilize the depth of indentation under standard loading condition, as

    a measure of hardness. The scale of the dial is reversed so that deepimpressions give low reading and shallow impression a high to that high

    number; high number indicates hard material.

    PROCEDURE :

    (1) Keep lever (eccentric knob stud) at unload position A.

    (2) Select the suitable indenter according to scale.

    (3) Select weight according to the scale.

    (4) Place the test block on testing table as per requirement.

    (5) Turn the main screw nut clockwise direction to raise the test block making

    contact with the clamping cone.

    (6) Continue turning, first the block will get clamped, turn the main screw nut,

    so that test block push the indenter further turn the main screw nut until the

    long pointer of the dial gauge has made two and half turn turns than it stop

    at 0 on black scale and 30 on red scale.

    (7) Turn the lever from unload position A to load position at B so that total

    load is brought into action.

    (8) When the long pointer of the dial gauge reaches the steady position the

    take by the lever to unload position A slowly.

    (9) Read the figure against the long pointer on proper scale. That is the direct

    reading of hardness of test block.

    (10) Then turn anticlockwise the main screw nut to release the specimen and

    select next surface of test block and carry on the same procedure until dial

    gauge give reading marked on test block than release the test block and

    the machine is ready for the next test of the job.

    NOTE :

    (1) Loading lever should be pulled towards A.

    (2) Place the specimen below the indenter rotate the main screw nut clockwise

    direction till the big hand of the dial gauge rests at 0 while small at 3 red

    spot.

    (3) Gently the turn lever towards B wait till the dial show the steady reading

    push the lever towards A position, note down the reading.

    (4) Rotate screw nut anticlockwise to release the job..

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    (5) Take two or three reading initially to get set ready the indenter sits on the

    holder

    OBSERVATION:

    RESULT:

    (1) Average Rockwell hardness number of mild steel test specimen is found to

    be ---

    (2) Average Rockwell hardness number of Brass test specimen if found to be

    --------

    PRECAUTIONS:

    (1) The place where the hardness tester is installed should be away from themachine, which causes vibrations.

    (2) The temperature of the room should be maintained at 200 C, if possible.

    (3) The surface of the test specimen should be free from oil, grease before

    testing.

    (4) Several reading should be taken on a dummy specimen when the machine

    is newly installed. This will stabilize the apparatus.

    (5) Do not test the surface, which are not leveled.

    (6) Maintain correct oil level in the dashpot replace oil whenever it needed.

    (7) Adjust the time of operation of the dashpot to six second in beginning.

    (8) The machine should be maintained free from dust and dirt.

    Sr.NO.

    Material

    of TestSpecimen

    Penetrator

    Total

    Load(N)

    ScaleSymbol

    Rockwell

    HardnessNumber

    MeanValue

    1.1.2.3.

    2.1.2.3.

    3.1.2.3.

    4.1.2.

    3.

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    EXPERIMENT No. .

    TENSILE TEST

    OBJECT: - To perform tensile test of mild steel and to draw stress-strain curve.

    THEORY: - Tensile test are employed to obtain the tensile strength, elasticity and ductility of the

    material. This test consists in straining a test piece by tensile stress, generally to fracture.

    Deformation or elongations of specimen at different loads are noted and a stress-straindiagram is prepared with the help of this diagram various elastic and strength properties

    of material are found.

    The standard from of tensile test specimen various with the nature of the

    material. Acceptance tests of ductile metals are usually performed on a length of the

    material if it is in the form of a rod and of a strip if it is a sheet material. Brittle materials

    are usually formed into special shapes to permit the use of gripping device which

    minimizes bending and to make certain that fracture occurs within the gauge length

    selected.

    The length of test piece between the grips of the testing machine should not be

    less then 9 d in case of bars of dia. less the 2.5 cm, 4.5 d in case of bars of dia more then

    2.5 cm. The gauge length of specimen should be taken equal to 5.65 S0, where S0 it the

    original cross sectional area of the specimen.

    d

    L 0L0 + 2d

    PROCEDURE:-

    (1) Prepare the specimen as explained above.

    (2) Measure the diameter of test specimen by means of a micrometer at least at three

    places and determine the mean value. Also mark the gauge length with the help of acentre punch.

    (3) Insert suitable jaws in the grips.

    (4) Insert the test specimen in the grips.

    (5) Take the initial reading on vernier scale provided in the machine.

    (6) Note the initial zero error in the dial of machine.

    (7) Start the machine. Apply the load at the slowest speed.

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    (8) Take the reading on vernier scale at the various load stages and record.

    (9) Continue applying the load till the specimen breaks and then stop the machine.

    (10) Take out the fractured specimen from the grips. Measure the final length in between

    the punch marks.

    (11) Record the probable yield point during test by observing the point at which pointer of

    load dial is stationary for some time and move backward slightly.

    OBSERVATION :-

    Initial diameter specimen, d0 --------------------- = mm

    Diameter of test specimen after fracture, du ----------------- = mm

    Gauge length, L0 --------------------- = mm

    Final length after facture, Lu --------------------- = mm

    Initial area of cross section, A0 = /4d20 --------------------- = mm2

    Final area of cross section Au = /4d2u --------------------------------= mm2

    Probable yield point --------------------- = N/mm2

    Type of fracture --------------------- =

    TENSILE TEST

    CALCULATIONS:-P

    Stress = --------- N/mm2 Strain = --------A0 l0

    Sr.No.

    LoadP

    VernierReading

    Elong-ation Stress Strain

    Sr.No.

    LoadP

    VernierReading

    Elonga-tion Stress Strain

    15

    26

    37

    48

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    Draw the graph taking stress on Y axis and strain on X axis.

    Ultimate loadUltimate stress = ------------------- N/mm2

    A0

    Lu Lo% elongation = -------------- X 100 =

    L0

    Au A0% reduction in area = -------------- X 100 =

    A0

    For calculation of value of modulus of elasticity take any two points on stress-strain curve withinelastic range. Find the corresponding stress and strain i.e. and .

    2E = ------- = ------ = ------, ------- = -------- = --------, Mean value of E = ------ kgf/sq. cm. 2RESULT:

    Ultimate stress = ------------------------- N/mm2

    Yield stress = ------------------------- N/mm2

    Proportional limit = ----------------------

    Modulus of elasticity = -------------------------- N/mm2

    Percentage of elongation = -------------

    Percentage reduction in area = ------------

    DISCUSSION:

    (1)Discuss the shapes of stress-strain diagram.(2)Discuss the type of fracture obtained.

    (3)Compare the results with standard values.

    (4)Discuss the effect of various variables on the test results.

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    EXPERIMENT No. ..

    VICKER HARDNESS TESTING MACHINE

    OBJECT : To determine the hardness by Vicker Hardness Testing machine.

    THEORY : The vicker pyramid hardness test utilizes quadrilateral diamond pyramid an

    angle of 1360 between the opposite faces, so that it is useable over the wholerange of material hardness, since the diamond is the hardest known

    substance. Moreover the adoption of the square base pyramid shape provides

    freedom from distortion under load.

    In the case of ball indention the total impression is obtained

    when the diameter of impression is 0.375 times the ball diameter. If pyramidal

    tangent planes are taken of the ball, the pyramidal angle would be 1360. In the

    Vickers method the indention made are all pyramids of similar angle, and the

    Vickers hardness HV is obtained as follow.

    Applied loadVicker Hardness HV = Area of indation

    = F/(d2/sin136/2)

    = 1.854 F/d2

    The thickness of the test specimen should be at least 1.2d the distance

    of the center of indention from edge of the test piece and between centers of

    indention should be at 2.5d. the load should be applied for a period of 10 to 15

    seconds. The accuracy of the microscope should be 0.001mm.

    The indenter profile should be occasionally checked, and the maximum

    variation at the center should not exceed 0.002mm as shown.

    F

    INDENTERTEST

    Specimen

    Platform

    Principal of Vickers hardness machine

    Diagonal

    d1

    d2

    Measurement of indention

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    D1 + D2

    ---------------2

    CHOICE OF LOAD FOR VARIOUS HARDNESS RANGE

    The machine carrying out Vickers hardness tests against load50, 30, 20, 10, & 5. These load are selected as per requirement. An optical

    device is provided for projecting the impression on front screen with 70 times

    magnification, which is capable to project 1.6 mm impression maximum. The

    micrometer thimble provided on front screen enable to measure diagonal of

    impression. It is advisable to select the load in relation to expected hardness

    range of the metal in such a way that impression produced should be to 0.50 mm

    across diagonal as for as possible.

    PROCEDURE:For carrying out tests, the following procedure should be adapted very

    carefully. Any negligence may lead to spoil the indenter.

    (1) Select the weights according to the expected hardness of specimen to be

    tested.

    (2) Place the specimen securely on testing table.

    (3) Turn the hand wheel clockwise so that specimen will get focused on front

    screen shapely. At this sage a gap of above 0.2 to 0.25 mm expected

    between tip of diamond indenter and top face of specimen.

    (4) Press start push button. Keep it pressed till inside START button will be ONeven after release of push button. The loading cycle starts gradually.

    The cycle is as under

    Load is transferred on specimen gradually maximum time about 6

    second.

    The load is kept constant on specimen as per dwell time adjustment.

    Adjustment range is 30 2 sec.

    (5) The indention is now projected on front focusing screen. Measure diagonal of

    impression is both the axis one after other. Find out mean value. Refer

    corresponding table and find out vicker hardness value.(6) To have next test, index the head to original position and bring back indenter

    on specimen, before starting loading / unloading. Vicker hardness value is

    always mentioned with the reference to load applied.

    HV 30 = 610 30 denots applied load in kgf.

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    PRECAUTIONS:

    (1) The machine should be maintained free from dust and dirt.

    (2) The moving parts of machine like loading mechanism are locked so that this

    should not move in transit.

    (3) It should free from outside vibration.

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    EXPERIMENT NO.

    IMPACT TEST

    OBJECT : To determine impact strength of material by impact testing machine using

    Charpy Test.

    THEORY : To determine the notch beam impact strength of steel, three types of notches

    are used (a) V-notch (b) U-notch (c) key hole notch. The test piece should bemachined all over and 55 mm long square cross section with 10 mm sides.

    Three notches is made at the centre of the piece. The notches should be

    prepared carefully by any machining method like milling shaping but no grooves

    should be visible to the necked eye. The test piece should lie squarely against

    the supports the supports with the plane of symmetry of the notch within 0.5 mm

    of the plane midway between them shown in fig. It should be struck by the

    hammer in the plane of symmetry of the notch and on the side opposite to the

    notch the speed of striking should be 5m/s to 5.5m/s.

    PROCEDURE :1. Lift the hammer to an appropriate knife-edge position and note down the

    energy stored in the hammer. For the standard test the energy stored should

    be 300 N-m.

    2. Fit the striker with the central vertical edge in striking position.

    3. Release the hammer. The hammer will break the test piece and shut up to

    the other side of the machine.

    4. Note the residual energy indicated on the scale by the hammer.

    5. The impact strength of the test piece is the difference of the initial energy

    stored in the hammer and the residual energy.

    40mm

    Striking Edge

    10 X 10 X 55mm

    V Notch Specimen Charpy Test

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    6. Calculate the impact modulus given by the ratio of the apparent energy of the

    rapture of the volume of the test piece below the notch.

    OBSERVATION:

    The experimental data may be tabulated as following.

    Material of the test piece = -----------

    Type of notch = -----------

    Dimension of the test piece = -----------

    Velocity of striking = -----------

    Test No Initial energy ( N-m) Residual energy (N-m) Energy absorbed (N-m)

    1

    2

    3

    4

    5

    Means value of impact strength = ----------

    CALCULATION:

    Impact strength (N/m2) I = K/AK = energy stored by the specimen in joules

    A = cross-section are of the specimen below the notch before test in m2

    PRECAUTION:

    1. The machine should be installed in such a way that the swinging range of the

    pendulum does, by no means, project into the area of common use.

    2. The working place is to be safe-guarded against hitting by stray pieces of broken test

    specimen.

    3. Before any test, ensure the fixing of correctly end supports.

    4. Confirm the tightness of all bolts and striker, latching tube, specimen supports etc.

    5. Do not allow to stand near the machine and particularly in the range of pendulum

    swinging.

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    EXPERIMENT No.

    BRINELL HARDNESS TEST

    Object : To determine the Brinell hardness number of given materials.

    Apparatus : Brinell hardness tester machine, dynamometer, ball holder, specimen.

    Theory : The brinell hardness test consists of the application to the surface of the

    specimen under test, of a hard steel ball of known diameter load for specifiedminimum time period. The diameter of the resulting impression is measured by

    means of microscope and the Brinell hardness number is the load applied in N

    divided by the spherical area of impression (in mm2). If P is the applied load in

    N. D is the diameter of the steel ball (mm) and d is the diameter of the

    indention in (mm), then

    BHN = Load / indented area

    P/{ D/2( D-D2-d2)}N/mm2

    In order that d/D may be within reasonable limits (preferable between 0.2 and

    0.5) for different materials, standard ratio of P/D2 are used.

    00

    d = 2.1 mm

    Procedure :

    (1) Keep, clean flat and smooth surfaced specimen for the test.

    (2) Keep the specimen on the top plate, as shown in the drawing and apply

    the desire load in Kg. On the specimen by rotating the handle in the

    clockwise direction, so that the sample comes in contact with the

    ball fitted in the ball holder.

    (3) For applying the desired load, which in normally 3000 Kg, is achieved by

    deferring to the calibration chart.

    (4) The large needle of the gauge should be always in 12 O clock position

    (0) before application of the load.

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    (5) Hold desire load for 30 seconds and thereafter, release the load by

    rotating the handle in anticlockwise direction and switching of the motor

    in motorized version.

    (6) Remove the specimen from the top plate and see the diameter of the bal

    impression with the help of brinell microscope and than refer to the

    enclosed hardness conversion table for the knowing hardness value of

    the material under test.

    Observation and results :

    Material of test specimen = -----------

    Diameter of steel ball D = -----------mm

    Diameter of indentation d = -----------mm

    Applied load = -----------N

    B.H.N.=Load/Indented area

    B.H.N. = P/{ D/2( D-D2-d2)}N/mm2

    Precautions :

    (1) The thickness of the test specimen should not be less than ten times the

    depth of the impression.

    (2) Distance of the center of indention from the edge of the specimen or from the

    center adjacent indentions should be greater than three times diameter of the

    indention.

    (3) The surface on which impression is made, should be flat, the accuracy of the

    measurement of the impression will depend on the degree of finish imparted

    to the surface, which should preferably be polished.

    (4) Slow speed of load application should be used for high precision. The speed

    of application of the load is adjustable by means of the knob at the front of

    machine. Turn the knob to the left to increase and to the right to decrease thespeed.

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    EXPERIMENT NO.

    COMPRESSION TEST

    OBJECT : To determined the compressive test strength of wood

    (1) along the grains, (2) across the grains.

    THEORY : wood exhibits, under compressive loading, a behavior peculiar to it self it is

    anything but an isotropic material, being composed of cells formed by organicgrowth align themselves to from a series of tubes or columns in the direction of

    the grain. As a result of this structure the elastic limit is reality low. There is no

    definite yield point and considerable set take place before failure. For loads

    normal to the grains, the load that causes lateral collapse of the tubes or fibres

    (crushing) is the significant load. For loads parallel to the grain, not only the

    elastic strength important but also the strength at rupture. Rupture often occurs

    because of collapse of the tubular fibres as columns. Various types of failure of

    would loaded parallel with the grain are shown in figure. 1.

    (a) Crushing (plane of rapture approx. horizontal)

    (b) Wedge split

    (c) Shearing (plane of rapture at acute angle with horizontal)

    (d) Spliting

    (e) Shearing and splitting parallel to grain.

    TEST SPECIMENS :

    Specimen for compression tests of wood parallel to the grain 5cm X 5cm X

    20cm rectangular prisms. Compression tests perpendicular to the grain are

    made on nominal 5cm X 5cm X 15cm. specimens. The load in applied through

    a metal bearing plate 5cm. with placed across the surface at right angles to the

    width placed across the upper surface at right angles to the width as shown in

    figure. 2.

    PROCEDURE :

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    (1) Measure the dimensions of test places.

    (2) Clean the bottom and top platens of the machine.

    (3) Position the specimen

    centrally on the bottom platen and screw down the top platen into contact.

    Positioning of the specimen centrally is important to ensure correct

    application of the load (fig. 3)

    (4) Open the stop valve of thepressure gauge to be used. Close other pressure gauge valves.

    (5) Open the control valve fully and start the pump motor.

    (6) Set the loose pointer of the

    gauge to zero and apply load slowly by closing the control valve.

    (7) When the specimen falls,

    the loose pointer on the gauge will indicate the maximum load reached. At

    this point the pump motor should be stopped.

    OBSERVATION AND CALCULATIONS:

    TestDimensions of

    specimenCross section

    area m2Load at failure

    NCompressivestrength N/m2

    Along the grain

    Across the grain

    Results:-

    (1) The compressive strength

    of wood specimen along the grain is ---------------

    (2) The compressive strength

    of wood specimen across the grain is ---------------

    Precautions:-

    (1) The specimen should be correctly prepared. It should be ensured that the

    end faces are at right angles to the side faces.

    (2) Specimen should be correctly placed on the bottom platen of the machine.

    (3) Load should be centrally placed on the bottom platen of the machine.

    (4) The specimen guard should be positioned to protect the operator from flying

    fragments if any.

    Discussion : Discuss the type of failure for each case.

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    EXPERIMENT NO.

    IMPACT TEST

    OBJECT : To determine impact strength of material by impact testing machine using

    Izod Test.

    THEORY : Many structures, machine and machine parts are commonly subjected to

    suddenly applied loads. Impact resistance is the capacity of a material towithstand sharp blows without fracturing. Many different procedures are used to

    evaluate the impact resistance of metals depending on the brittleness of the

    metals and of the nature of the application. The tension impact test can be used

    on the most ductile metals while the torsion impact test is suitable for extremely

    for material such as hardness tool steels.

    The most commonly used impact for steels or the charpy and the izod

    tester. These testers are made on small notched specimens broken in flexures

    by a single below. The energy absorbed in breaking the specimens is measured.

    The results are usually given in kilogram-meters without reference to the volume

    of metal involved sudden bending of the specimen cause appearance of triaxial

    tensile stress in the neighborhood of the base of the notch.

    Impact strength I = K/A

    K = energy

    A = cross section area of the specimen

    10

    10

    Striking edge for of pendulum

    100 0.5628 22

    75 8

    47

    10

    Cantilever beam specimen and mounting for the IZOD TEST.

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    PROCEDURE :

    (1) Check that the latching tube is fitted in horizontal position for izod test and

    fully tightened in place.

    (2) Check the izod striker is fitted with the hammer.

    (3) Check with the help of wedge shaped setting gauge position the test piece

    correctly and then the tighten allen ball fully to clamped the test piece tightly.

    (4) Bring the reading pointer to maximum scale reading. Latch the hammer inthe raised position and allow it to swing freely pulling the release handle.

    (5) Apply the break just then it reaches near the wise/specimen support to stop

    the hammer.

    (6) Note down the reading accurately. As absorbed energy.

    Carry out the impact tester on three specimens and take average values of the

    energy absorbed.

    OBSERVATION:

    Material --------

    Izod Value -------

    RESULT : The impact strength of mild steel specimen is

    Izod value = -------- N/m

    PRECAUTION : Three features of great importance are,

    (1) Making the notch correctly.

    (2) Locating the bottom of the notch properly.

    (3) Placing the specimen properly in machine.