SOURCE REMOVAL REPORT€¦ · source removal report . former florida highway patrol property . 7651...

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Prepared by: 1408 North Westshore Boulevard, Suite 115 Tampa, Florida 33607 (813) 289-9338 www.ectinc.com ECT No. 150202-0100 April 2015 SOURCE REMOVAL REPORT FORMER FLORIDA HIGHWAY PATROL PROPERTY 7651 U.S. HIGHWAY 19 NORTH PINELLAS PARK, PINELLAS COUNTY, FLORIDA Prepared for: PINELLAS COUNTY Real Estate Management Department 500 East Avenue Clearwater, Florida 33756 Exhibit E

Transcript of SOURCE REMOVAL REPORT€¦ · source removal report . former florida highway patrol property . 7651...

Prepared by:

1408 North Westshore Boulevard, Suite 115 Tampa, Florida 33607

(813) 289-9338www.ectinc.com

ECT No. 150202-0100

April 2015

SOURCE REMOVAL REPORT

FORMER FLORIDA HIGHWAY PATROL PROPERTY 7651 U.S. HIGHWAY 19 NORTH

PINELLAS PARK, PINELLAS COUNTY, FLORIDA

Prepared for:

PINELLAS COUNTY Real Estate Management Department

500 East Avenue Clearwater, Florida 33756

Exhibit E

Former Florida Highway Patrol Property7651 US Highway 19, Pinellas County, Florida

PROFESSIONAL CERTIFICATION

Soil Removal Report

Date

Mona P. Joh1?on, P.Florida P.G. No. PG-I

Date

ENVIRONMENTAL CONSULTING & TECHNOLOGY, INC.1408 North Westshore Boulevard, Suite 115, Tampa, Florida 33607

Telephone: (813) 289-9338Fax: (813) 289-9388

www.ectinc.comFlorida Engineering Business Certificate No. 5520

Florida Geology Business Certificate No. GP42

1

The technical contents of this Soil Removal Report represent our professional

interpretations and were derived in accordance with generally accepted engineering

practices as they apply to the subject facility: the former Florida Highway Patrol property

located at 7651 US Highway 19 in Pinellas County, Florida. The findings and results of

this report are for the sole use and benefit of the site owner, Pinellas County. Utilization

of this report by other parties, for other purposes, or when the information is obsolete is at

their risk, and neither Environmental Consulting & Technology, Inc. nor the undersigned

are liable for consequences or damages extending therefrom. No warranties are implied

or intended.

This is to certify that geological interpretations in this source removal report have been

prepared by me and by individuals under my direct supervision.

Prepared by:

_________________

Dat/en L. Stowe, LEPProject Manager

Reviewed by:

___________ ____

P:\P1 1 52-PinellasCounty\1 50202-0100 Former Highway Patrol\Source Removal\5_Reports\SRtextdocx4/14/15

Exhibit E

Former Florida Highway Patrol Property Soil Removal Report 7651 US Highway 19, Pinellas County, Florida

P:\P1152-PinellasCounty\150202-0100 Former Highway Patrol\Source Removal\5_Reports\SRtext.docx 4/14/15

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TABLE OF CONTENTS PROFESSIONAL CERTIFICATION ............................................................................. i 1.  INTRODUCTION ........................................................................................................................... 1-1 

2.  WASTE PROFILE .......................................................................................................................... 2-1 

3.  SOIL REMOVAL ACTIVITIES .................................................................................................... 3-1 

4.  CONCLUSION ................................................................................................................................ 4-1 

APPENDICES

APPENDIX A— LABORATORY ANALYTICAL RESULTS APPENDIX B— WASTE PROFILE APPENDIX C— PHOTOGRAPHS AND WEIGH TICKET

Exhibit E

Former Florida Highway Patrol Property Soil Removal Report 7651 US Highway 19, Pinellas County, Florida

P:\P1152-PinellasCounty\150202-0100 Former Highway Patrol\Source Removal\5_Reports\SRtext.docx 4/14/15

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LIST OF FIGURES

Figure 1. Site Vicinity Map

Figure 2. Site Map with Soil Sample Locations and Limits of Excavation

Exhibit E

Former Florida Highway Patrol Property Soil Removal Report 7651 US Highway 19, Pinellas County, Florida

P:\P1152-PinellasCounty\150202-0100 Former Highway Patrol\Source Removal\5_Reports\SRtext.docx 4/14/15

1-1

1. INTRODUCTION

Environmental Consulting & Technology, Inc. (ECT) has prepared this soil removal

report for the former Florida Highway Patrol property located at 7651 US Highway 19,

Pinellas County, Florida. Prior phase II environmental site assessment activities

conducted in connection with the transfer of the property to Pinellas County had detected

an area of soil impact associated with elevated concentrations of polynuclear aromatic

hydrocarbons (PAHs). The concentrations exceeded the soil cleanup target level (SCTL)

pursuant to Chapter 62-777 of the Florida Administrative Code (F.A.C.). A site vicinity

map is provided as Figure 1. The sample with the elevated concentrations detected

during the phase II ESA activities is depicted in Figure 2.

ECT conducted additional site assessment activities at the site. The assessments

indicated that the concentrations of tested parameters in four additional samples collected

five feet from the impacted sample were below all applicable SCTLs. An area

approximately 10 feet by 10 feet by 2 feet was delineated. Source removal activities

were recommended. As detailed in this report, that work was accomplished.

Pinellas County retained ECT to perform soil removal activities. ECT retained the

services of EnviroTek Environmental & Construction Services, Inc. (EnviroTek) to

conduct the excavation, loading, disposal, and backfilling operations. ECT personnel

staked out the area to be excavated using Global Positioning System (GPS) points

recorded during the soil sample collection activities. ECT also performed oversight and

preparation of this soil removal report. The soil removal activities were conducted on

April 6, 2015. A total of 8.3 tons of impacted soil was removed and disposed at the

Republic Industries Cedar Trail Class I Landfill facility located in Bartow, Florida. ECT

has prepared this report documenting the soil removal activities in general accordance

with Chapter 62-780, F.A.C.

Exhibit E

Former Florida Highway Patrol Property Soil Removal Report 7651 US Highway 19, Pinellas County, Florida

P:\P1152-PinellasCounty\150202-0100 Former Highway Patrol\Source Removal\5_Reports\SRtext.docx 4/14/15

2-1

2. WASTE PROFILE

ECT and EnviroTek prepared a waste profile required by Republic Industries for disposal

of the non-hazardous soil. After review of the initial laboratory analytical results,

additional analyses were requested.

ECT personnel mobilized to the subject site on March 20, 2015 and collected a shallow

soil sample (upper 2 feet) within the area of impact as close to the sample that had

exhibited the elevated concentrations of PAHs. The location was based on GPS data.

The soil sample was collected into laboratory-supplied containers, stored on wet ice and

delivered to Pace Analytical Laboratories, Inc. for laboratory analysis of volatile organic

compounds and semi-volatile organic compounds. While at the site, it was noted that the

monitoring well previously installed onsite had been destroyed. The limits of the

excavation were flagged using GPS data during the site visit.

The laboratory analytical results indicated that the concentrations of the tested parameters

were below the laboratory’s method detection limits and the cleanup target levels. The

laboratory analytical results are provided in Appendix A. The additional analytical

results were forwarded with a revised waste profile to Republic Industries for review.

The revised waste profile is provided in Appendix B.

Exhibit E

Former Florida Highway Patrol Property Soil Removal Report 7651 US Highway 19, Pinellas County, Florida

P:\P1152-PinellasCounty\150202-0100 Former Highway Patrol\Source Removal\5_Reports\SRtext.docx 4/14/15

3-1

3. SOIL REMOVAL ACTIVITIES

The objective of the project was to remove the soils within the limits of the site

assessment findings that had concentrations above the SCTL for certain PAHs. The

limits of the excavation were field delineated by ECT.

EnviroTek and ECT mobilized to the subject site on April 6, 2015. Soils were excavated

from an area approximately 8 feet (east to west) by 10 feet (north to south). The eastern

extent of the excavation was shortened in order to avoid excavating or damaging a

subsurface drainage pipe. The depth of the excavation was 2 feet resulting in the

excavation of about 6 cubic yards or 8.3 tons. The soil was direct loaded into a truck and

transported to the Cedar Trail Class I Landfill facility. The excavation was backfilled

with clean soil and compacted using excavation equipment. Two photographs and a copy

of the weigh ticket and landfill manifest are provided in Appendix C. Given the one-

truckload minimum of 20 tons, the weigh ticket indicates the load at 20 tons.

Exhibit E

Former Florida Highway Patrol Property Soil Removal Report 7651 US Highway 19, Pinellas County, Florida

P:\P1152-PinellasCounty\150202-0100 Former Highway Patrol\Source Removal\5_Reports\SRtext.docx 4/14/15

4-1

4. CONCLUSION

In keeping with the scope of work, soil was excavated from the delineated area of impact.

A total of 8.3 tons of soil was excavated and loaded and disposed at the Republic

Industries Cedar Trail facility in Bartow, Florida. Clean backfill was brought onsite the

same day and compacted with the available onsite equipment.

Exhibit E

FIGURES

Exhibit E

Environmental Consulting & Technology, Inc.

SITE LOCATION

Sources: Labins.org USGS Quad Map of ST. Petersburg (NE), Fl., 1987; ECT, 2013.

FIGURE 1.SITE VICINITY MAP7651 US HIGHWAY 19 NORTH PROPERTYPINELLAS PARK, FLORIDA

By: jstebniskyQ:\projects\US_Hwy_Property\130735\0100\Vicinity_Map.mxd Date: 10/7/2013

0 2,000

Feet

Exhibit E

!.

!.!.!.

!.SS-3

FIGURE 2.SITE MAP WITH SOIL SAMPLE LOCATIONS AND LIMITS OF EXCAVATION(PHASE II ESA AND ADDITIONAL ASSESSMENTS)FORMER FLORIDA HIGHWAY PATROL PROPERTY7651 US HIGHWAY 19 NORTH PROPERTYPINELLAS PARK, PINELLAS COUNTY, FLORIDASources: FDOT Imagery 2014; ECT, 2015.

O:\_PROJECTS\_CADGIS\150202\Soil_Sample_2015.mxd mcruz 4/9/2015 3:38:37 PMNAD 1983 StatePlane Florida West FIPS 0902 FeetTransverse Mercator

I

!.

!.!.

!.

!.LIMITS OF

EXCAVATIONSS-3N 5'

SS-3W 5'

SS-3E 5'

SS-3S 5'

SS-3

LegendSoil Sampled for Laboratory Analysis (Phase II ESA)

!. Sample Locations (Additional Assessments)Project Boundary

0 7035

Feet

Exhibit E

APPENDIX A

LABORATORY ANALYTICAL RESULTS

Exhibit E

#=CL#

March 27, 2015

LIMS USE: FR - DARREN STOWE

LIMS OBJECT ID: 35180345

35180345

Project:

Pace Project No.:

RE:

Darren Stowe

1408 N. Westshore BlvdSuite 115Tampa, FL 33607

Former FHP

Dear Darren Stowe:

Enclosed are the analytical results for sample(s) received by the laboratory on March 20, 2015. Theresults relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unlessotherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Mike Valder

[email protected]

Project Manager

Enclosures

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc.5460 Beaumont Center Blvd - Suite 520

Tampa, FL 33634

(813)881-9401

Page 1 of 12

Exhibit E

#=CP#

CERTIFICATIONS

Pace Project No.:

Project:

35180345

Former FHP

Ormond Beach Certification IDs8 East Tower Circle, Ormond Beach, FL 32174Alabama Certification #: 41320Connecticut Certification #: PH-0216Delaware Certification: FL NELAC ReciprocityFlorida Certification #: E83079Georgia Certification #: 955Guam Certification: FL NELAC ReciprocityHawaii Certification: FL NELAC ReciprocityIllinois Certification #: 200068Indiana Certification: FL NELAC ReciprocityKansas Certification #: E-10383Kentucky Certification #: 90050Louisiana Certification #: FL NELAC ReciprocityLouisiana Environmental Certificate #: 05007Maryland Certification: #346Massachusetts Certification #: M-FL1264Michigan Certification #: 9911Mississippi Certification: FL NELAC ReciprocityMissouri Certification #: 236

Montana Certification #: Cert 0074Nebraska Certification: NE-OS-28-14Nevada Certification: FL NELAC ReciprocityNew Hampshire Certification #: 2958New Jersey Certification #: FL765New York Certification #: 11608North Carolina Environmental Certificate #: 667Pennsylvania Certification #: 68-00547Puerto Rico Certification #: FL01264South Carolina Certification: #96042001Tennessee Certification #: TN02974Texas Certification: FL NELAC ReciprocityUS Virgin Islands Certification: FL NELAC ReciprocityVirginia Environmental Certification #: 460165Washington Certification #: C955West Virginia Certification #: 9962CWisconsin Certification #: 399079670Wyoming (EPA Region 8): FL NELAC Reciprocity

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc.5460 Beaumont Center Blvd - Suite 520

Tampa, FL 33634

(813)881-9401

Page 2 of 12

Exhibit E

#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

35180345

Former FHP

Lab ID Sample ID Matrix Date Collected Date Received

35180345001 CS-1 Solid 03/20/15 09:20 03/20/15 10:05

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc.5460 Beaumont Center Blvd - Suite 520

Tampa, FL 33634

(813)881-9401

Page 3 of 12

Exhibit E

#=SA#

SAMPLE ANALYTE COUNT

Pace Project No.:

Project:

35180345

Former FHP

Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts

35180345001 CS-1 EPA 8270 7 PASI-OEAO

EPA 8260 6 PASI-OBCH

ASTM D2974-87 1 PASI-ORPM

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc.5460 Beaumont Center Blvd - Suite 520

Tampa, FL 33634

(813)881-9401

Page 4 of 12

Exhibit E

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

35180345

Former FHP

Sample: CS-1 Lab ID: 35180345001 Collected: 03/20/15 09:20 Received: 03/20/15 10:05 Matrix: Solid

Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.

Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL

Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Full List Microwave

Pyridine 0.058 U mg/kg 03/25/15 17:08 110-86-103/24/15 23:300.44 0.058 1

SurrogatesNitrobenzene-d5 (S) 63 % 03/25/15 17:08 4165-60-003/24/15 23:3010-110 1

2-Fluorobiphenyl (S) 76 % 03/25/15 17:08 321-60-803/24/15 23:3018-110 1

Terphenyl-d14 (S) 88 % 03/25/15 17:08 1718-51-003/24/15 23:3010-123 1

Phenol-d6 (S) 70 % 03/25/15 17:08 13127-88-303/24/15 23:3010-110 1

2-Fluorophenol (S) 65 % 03/25/15 17:08 367-12-403/24/15 23:3018-110 1

2,4,6-Tribromophenol (S) 86 % 03/25/15 17:08 118-79-603/24/15 23:3010-110 1

Analytical Method: EPA 82608260 MSV 5030 Low Level

Benzene 0.0035 U mg/kg 03/23/15 18:41 71-43-20.0068 0.0035 1

2-Butanone (MEK) 0.0034 U mg/kg 03/23/15 18:41 78-93-30.0068 0.0034 1

Trichloroethene 0.0038 U mg/kg 03/23/15 18:41 79-01-60.0068 0.0038 1

Surrogates4-Bromofluorobenzene (S) 99 % 03/23/15 18:41 460-00-455-148 1

1,2-Dichloroethane-d4 (S) 86 % 03/23/15 18:41 17060-07-080-131 1

Toluene-d8 (S) 99 % 03/23/15 18:41 2037-26-584-117 1

Analytical Method: ASTM D2974-87Percent Moisture

Percent Moisture 23.3 % 03/27/15 10:290.10 0.10 1

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..Date: 03/27/2015 06:30 PM

Pace Analytical Services, Inc.5460 Beaumont Center Blvd - Suite 520

Tampa, FL 33634

(813)881-9401

Page 5 of 12

Exhibit E

#=QC#

QUALITY CONTROL DATA

Pace Project No.:

Project:

35180345

Former FHP

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:

QC Batch Method:

Analysis Method:

Analysis Description:

MSV/14407

EPA 8260

EPA 8260

8260 MSV 5030 Low

Associated Lab Samples: 35180345001

Parameter Units

Blank

Result

Reporting

Limit Qualifiers

METHOD BLANK: 1163671

Associated Lab Samples: 35180345001

Matrix: Solid

Analyzed

2-Butanone (MEK) mg/kg 0.0025 U 0.0050 03/23/15 10:58

Benzene mg/kg 0.0025 U 0.0050 03/23/15 10:58

Trichloroethene mg/kg 0.0028 U 0.0050 03/23/15 10:58

1,2-Dichloroethane-d4 (S) % 85 80-131 03/23/15 10:58

4-Bromofluorobenzene (S) % 99 55-148 03/23/15 10:58

Toluene-d8 (S) % 98 84-117 03/23/15 10:58

Parameter Units

LCS

Result

% Rec

Limits Qualifiers% RecConc.

1163672LABORATORY CONTROL SAMPLE:

LCSSpike

2-Butanone (MEK) mg/kg 0.040.039 102 51-161

Benzene mg/kg 0.019.019 97 70-130

Trichloroethene mg/kg 0.018.019 94 69-130

1,2-Dichloroethane-d4 (S) % 84 80-131

4-Bromofluorobenzene (S) % 101 55-148

Toluene-d8 (S) % 99 84-117

Parameter Units

MS

Result

% Rec

Limits Qual% RecConc.

1163673MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpike

Result

35180345001

1163674

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

2-Butanone (MEK) mg/kg .056 90 20-21785 8 40.0550.0034 U 0.050 0.047

Benzene mg/kg .027 97 24-141111 11 40.0270.0035 U 0.027 0.030

Trichloroethene mg/kg .027 96 42-130109 11 40.0270.0038 U 0.027 0.030

1,2-Dichloroethane-d4 (S) % 88 80-13186 40

4-Bromofluorobenzene (S) % 101 55-14899 40

Toluene-d8 (S) % 100 84-11798 40

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..Date: 03/27/2015 06:30 PM

Pace Analytical Services, Inc.5460 Beaumont Center Blvd - Suite 520

Tampa, FL 33634

(813)881-9401

Page 6 of 12

Exhibit E

#=QC#

QUALITY CONTROL DATA

Pace Project No.:

Project:

35180345

Former FHP

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:

QC Batch Method:

Analysis Method:

Analysis Description:

OEXT/21518

EPA 3546

EPA 8270

8270 Solid MSSV Microwave

Associated Lab Samples: 35180345001

Parameter Units

Blank

Result

Reporting

Limit Qualifiers

METHOD BLANK: 1164674

Associated Lab Samples: 35180345001

Matrix: Solid

Analyzed

Pyridine mg/kg 0.023 U 0.17 03/25/15 13:19

2,4,6-Tribromophenol (S) % 87 10-110 03/25/15 13:19

2-Fluorobiphenyl (S) % 80 18-110 03/25/15 13:19

2-Fluorophenol (S) % 75 18-110 03/25/15 13:19

Nitrobenzene-d5 (S) % 71 10-110 03/25/15 13:19

Phenol-d6 (S) % 76 10-110 03/25/15 13:19

Terphenyl-d14 (S) % 88 10-123 03/25/15 13:19

Parameter Units

LCS

Result

% Rec

Limits Qualifiers% RecConc.

1164675LABORATORY CONTROL SAMPLE:

LCSSpike

Pyridine mg/kg 1.11.7 63 10-130

2,4,6-Tribromophenol (S) % 83 10-110

2-Fluorobiphenyl (S) % 77 18-110

2-Fluorophenol (S) % 67 18-110

Nitrobenzene-d5 (S) % 72 10-110

Phenol-d6 (S) % 75 10-110

Terphenyl-d14 (S) % 86 10-123

Parameter Units

MS

Result

% Rec

Limits Qual% RecConc.

1165154MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpike

Result

35179538002

1165155

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Pyridine mg/kg 6.2 57 10-11058 3 406.2 3.5 3.6

2,4,6-Tribromophenol (S) % 88 10-11087

2-Fluorobiphenyl (S) % 73 18-11073

2-Fluorophenol (S) % 60 18-11062

Nitrobenzene-d5 (S) % 64 10-11065

Phenol-d6 (S) % 68 10-11072

Terphenyl-d14 (S) % 86 10-12385

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..Date: 03/27/2015 06:30 PM

Pace Analytical Services, Inc.5460 Beaumont Center Blvd - Suite 520

Tampa, FL 33634

(813)881-9401

Page 7 of 12

Exhibit E

#=QC#

QUALITY CONTROL DATA

Pace Project No.:

Project:

35180345

Former FHP

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:

QC Batch Method:

Analysis Method:

Analysis Description:

PMST/3385

ASTM D2974-87

ASTM D2974-87

Dry Weight/Percent Moisture

Associated Lab Samples: 35180345001

Parameter Units

Dup

Result

Max

RPD QualifiersRPDResult

35179251001

1167767SAMPLE DUPLICATE:

Percent Moisture % 98.8 0 1098.8

Parameter Units

Dup

Result

Max

RPD QualifiersRPDResult

35180345001

1167768SAMPLE DUPLICATE:

Percent Moisture % 24.7 6 1023.3

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..Date: 03/27/2015 06:30 PM

Pace Analytical Services, Inc.5460 Beaumont Center Blvd - Suite 520

Tampa, FL 33634

(813)881-9401

Page 8 of 12

Exhibit E

#=QL#

QUALIFIERS

Pace Project No.:

Project:

35180345

Former FHP

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.

ND - Not Detected at or above adjusted reporting limit.

MDL - Adjusted Method Detection Limit.

PQL - Practical Quantitation Limit.

RL - Reporting Limit.

S - Surrogate

1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.

Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.

LCS(D) - Laboratory Control Sample (Duplicate)

MS(D) - Matrix Spike (Duplicate)

DUP - Sample Duplicate

RPD - Relative Percent Difference

NC - Not Calculable.

SG - Silica Gel - Clean-Up

U - Indicates the compound was analyzed for, but not detected.

N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.

Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.

TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - Ormond BeachPASI-O

ANALYTE QUALIFIERS

The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. I

Compound was analyzed for but not detected. U

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..Date: 03/27/2015 06:30 PM

Pace Analytical Services, Inc.5460 Beaumont Center Blvd - Suite 520

Tampa, FL 33634

(813)881-9401

Page 9 of 12

Exhibit E

#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Pace Project No.:

Project:

35180345

Former FHP

Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch

35180345001 OEXT/21518 MSSV/7531CS-1 EPA 3546 EPA 8270

35180345001 MSV/14407CS-1 EPA 8260

35180345001 PMST/3385CS-1 ASTM D2974-87

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..Date: 03/27/2015 06:30 PM

Pace Analytical Services, Inc.5460 Beaumont Center Blvd - Suite 520

Tampa, FL 33634

(813)881-9401

Page 10 of 12

Exhibit E

Page 11 of 12

Exhibit E

Page 12 of 12

Exhibit E

APPENDIX B

WASTE PROFILE

Exhibit E

Exhibit E

Exhibit E

Exhibit E

APPENDIX C

PHOTOGRAPHS AND WEIGH TICKET

Exhibit E

P:\P1152-PinellasCounty\150202-0100 Former Highway Patrol\Source Removal\5_Reports\Photos.doc--4/13/2015

Exhibit E

Exhibit E