SHEALY ENVIRONMENTAL SERVICES, INC.€¦ · Kelly M. Nance Project Manager This report shall not be...

SHEALY ENVIRONMENTAL SERVICES, INC.Report of Analysis

NuEarth Solutions, LLC2041 Industrial Blvd.Lexington, SC 29072Attention: Jono Rabley

SC21057Lot Number:52561Project Number:SCDHEC - SCEG Fleet Maintenance SiteProject Name:

04/04/2017Date Completed:

Kelly M. NanceProject Manager

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.

Page: 1 of 87106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.comShealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.

Case NarrativeNuEarth Solutions, LLCLot Number: SC21057

SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329

This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample.All results listed in this report relate only to the samples that are contained within this report.Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.

SemivolatilesThe LCS associated with prep batch 38153 had 3,3'-dichlorobenzidine recovered below the acceptance limits. This demonstrates a low bias on analytical results. Samples -013, -014 and -016 were re-extracted and re-analyzed outside of the holding time for confirmation. All compounds were ND in both runs.The MS/MSD associated with sample -004 had compounds recovered outside of the acceptance limits and RPDs exceeded method control limits. The LCS was recovered within the required acceptance limits; therefore, this demonstrates a matrix effect and data quality is not impacted.


SHEALY ENVIRONMENTAL SERVICES, INC.Sample SummaryNuEarth Solutions, LLCLot Number: SC21057

Sample Number Sample ID Matrix Date Sampled Date Received001 03/21/2017 1050CR-SW-01 Aqueous 03/21/2017002 03/21/2017 1030CR-SW-02 Aqueous 03/21/2017003 03/21/2017 1215CR-SW-03 Aqueous 03/21/2017004 03/21/2017 1015CR-SW-04 Aqueous 03/21/2017005 03/21/2017 1202CR-SW-05 Aqueous 03/21/2017006 03/21/2017 1155CR-SW-06 Aqueous 03/21/2017007 03/21/2017 1105CR-SW-07 Aqueous 03/21/2017008 03/21/2017 1057CR-SW-08 Aqueous 03/21/2017009 03/21/2017 1050CR-SW-09 Aqueous 03/21/2017010 03/21/2017 1040CR-SW-10 Aqueous 03/21/2017011 03/21/2017 1030CR-SW-11 Aqueous 03/21/2017012 03/21/2017 1040CR-SW-12 Aqueous 03/21/2017013 03/21/2017 1230CR-SW-13 Aqueous 03/21/2017014 03/21/2017 1415CR-SW-14 Aqueous 03/21/2017015 03/21/2017Trip Blank Aqueous 03/21/2017016 03/21/2017 1202CR-SW-05 DUP Aqueous 03/21/2017

(16 samples)


SHEALY ENVIRONMENTAL SERVICES, INC.Executive SummaryNuEarth Solutions, LLC

Lot Number: SC21057

Sample Sample ID Matrix Parameter Method Result Q Units Page005 CR-SW-05 Aqueous bis(2-Ethylhexyl)phthalate 8270D 150 ug/L 23(1 detection)


Volatile Organic Compounds by GC/MSDescription: Matrix:

Date Received:

Client: Laboratory ID:Date Sampled:

NuEarth Solutions, LLCCR-SW-01

SC21057-00103/21/2017 105003/21/2017

Aqueous

Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch1 5030B 8260B 1 03/22/2017 2229 ECP 37834AnalyticalCASParameter Number Method Result Q PQL Units Run

Acetone 67-64-1 8260B ND 1ug/L20Benzene 71-43-2 8260B ND 1ug/L1.0Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0Bromoform 75-25-2 8260B ND 1ug/L1.0Bromomethane (Methyl bromide) 74-83-9 8260B ND 1ug/L2.02-Butanone (MEK) 78-93-3 8260B ND 1ug/L10Carbon disulfide 75-15-0 8260B ND 1ug/L1.0Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0Chlorobenzene 108-90-7 8260B ND 1ug/L1.0Chloroethane 75-00-3 8260B ND 1ug/L2.0Chloroform 67-66-3 8260B ND 1ug/L1.0Chloromethane (Methyl chloride) 74-87-3 8260B ND 1ug/L1.0Cyclohexane 110-82-7 8260B ND 1ug/L1.01,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260B ND 1ug/L1.0Dibromochloromethane 124-48-1 8260B ND 1ug/L1.01,2-Dibromoethane (EDB) 106-93-4 8260B ND 1ug/L1.01,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.01,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.01,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.01,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.01,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.01,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.01,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0Ethylbenzene 100-41-4 8260B ND 1ug/L1.02-Hexanone 591-78-6 8260B ND 1ug/L10Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0Methyl acetate 79-20-9 8260B ND 1ug/L1.0Methyl tertiary butyl ether (MTBE) 1634-04-4 8260B ND 1ug/L1.04-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0Methylene chloride 75-09-2 8260B ND 1ug/L1.0Styrene 100-42-5 8260B ND 1ug/L1.01,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0Toluene 108-88-3 8260B ND 1ug/L1.01,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.01,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.01,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.01,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0

J = Estimated result < PQL and > MDLPQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range

P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQLWhere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"

N = Recovery is out of criteria_H = Out of holding time



Date Received:



SC21057-00103/21/2017 105003/21/2017

Aqueous


Trichloroethene 79-01-6 8260B ND 1ug/L1.0Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0Vinyl chloride 75-01-4 8260B ND 1ug/L1.0Xylenes (total) 1330-20-7 8260B ND 1ug/L1.0

AcceptanceRun 1Surrogate Q % Recovery Limits1,2-Dichloroethane-d4 95 70-130Bromofluorobenzene 94 70-130Toluene-d8 101 70-130





Semivolatile Organic Compounds by GC/MSDescription: Matrix:

Date Received:



SC21057-00103/21/2017 105003/21/2017

Aqueous

Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch1 3520C 8270D 1 03/30/2017 1659 RBH 03/23/2017 1235 37862AnalyticalCASParameter Number Method Result Q PQL Units Run

1,1'-Biphenyl 92-52-4 8270D ND 1ug/L4.02,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/L4.02,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/L4.02,4-Dichlorophenol 120-83-2 8270D ND 1ug/L8.02,4-Dimethylphenol 105-67-9 8270D ND 1ug/L4.02,4-Dinitrophenol 51-28-5 8270D ND 1ug/L202,4-Dinitrotoluene 121-14-2 8270D ND 1ug/L8.02,6-Dinitrotoluene 606-20-2 8270D ND 1ug/L8.02-Chloronaphthalene 91-58-7 8270D ND 1ug/L4.02-Chlorophenol 95-57-8 8270D ND 1ug/L4.02-Methylnaphthalene 91-57-6 8270D ND 1ug/L0.802-Methylphenol 95-48-7 8270D ND 1ug/L4.02-Nitroaniline 88-74-4 8270D ND 1ug/L8.02-Nitrophenol 88-75-5 8270D ND 1ug/L4.03,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/L4.03+4-Methylphenol 106-44-5 8270D ND 1ug/L4.03-Nitroaniline 99-09-2 8270D ND 1ug/L8.04,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/L204-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/L4.04-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/L4.04-Chloroaniline 106-47-8 8270D ND 1ug/L8.04-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/L4.04-Nitroaniline 100-01-6 8270D ND 1ug/L8.04-Nitrophenol 100-02-7 8270D ND 1ug/L20Acenaphthene 83-32-9 8270D ND 1ug/L0.80Acenaphthylene 208-96-8 8270D ND 1ug/L0.80Acetophenone 98-86-2 8270D ND 1ug/L4.0Anthracene 120-12-7 8270D ND 1ug/L0.80Atrazine 1912-24-9 8270D ND 1ug/L4.0Benzaldehyde 100-52-7 8270D ND 1ug/L8.0Benzo(a)anthracene 56-55-3 8270D ND 1ug/L0.80Benzo(a)pyrene 50-32-8 8270D ND 1ug/L0.80Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/L0.80Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/L0.80Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/L0.80bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/L4.0bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/L4.0bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/L4.0bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/L4.0Butyl benzyl phthalate 85-68-7 8270D ND 1ug/L4.0Caprolactam 105-60-2 8270D ND 1ug/L8.0Carbazole 86-74-8 8270D ND 1ug/L4.0Chrysene 218-01-9 8270D ND 1ug/L0.80Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/L0.80






Date Received:



SC21057-00103/21/2017 105003/21/2017

Aqueous


Dibenzofuran 132-64-9 8270D ND 1ug/L4.0Diethylphthalate 84-66-2 8270D ND 1ug/L4.0Dimethyl phthalate 131-11-3 8270D ND 1ug/L4.0Di-n-butyl phthalate 84-74-2 8270D ND 1ug/L4.0Di-n-octylphthalate 117-84-0 8270D ND 1ug/L4.0Fluoranthene 206-44-0 8270D ND 1ug/L0.80Fluorene 86-73-7 8270D ND 1ug/L0.80Hexachlorobenzene 118-74-1 8270D ND 1ug/L4.0Hexachlorobutadiene 87-68-3 8270D ND 1ug/L4.0Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/L20Hexachloroethane 67-72-1 8270D ND 1ug/L4.0Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/L0.80Isophorone 78-59-1 8270D ND 1ug/L4.0Naphthalene 91-20-3 8270D ND 1ug/L0.80Nitrobenzene 98-95-3 8270D ND 1ug/L4.0N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/L4.0N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270D ND 1ug/L4.0Pentachlorophenol 87-86-5 8270D ND 1ug/L20Phenanthrene 85-01-8 8270D ND 1ug/L0.80Phenol 108-95-2 8270D ND 1ug/L4.0Pyrene 129-00-0 8270D ND 1ug/L0.80

AcceptanceRun 1Surrogate Q % Recovery Limits2-Fluorobiphenyl 76 37-1292-Fluorophenol 55 24-127Nitrobenzene-d5 86 38-127Phenol-d5 75 28-128Terphenyl-d14 79 10-1482,4,6-Tribromophenol 73 41-144






Date Received:



SC21057-00203/21/2017 103003/21/2017

Aqueous








Date Received:



SC21057-00303/21/2017 121503/21/2017

Aqueous








Date Received:



SC21057-00403/21/2017 101503/21/2017

Aqueous








Date Received:



SC21057-00503/21/2017 120203/21/2017

Aqueous








Date Received:



SC21057-00503/21/2017 120203/21/2017

Aqueous

Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch1 3520C 8270D 1 03/30/2017 1924 RBH 03/23/2017 1235 378622 3520C 8270D 5 04/03/2017 0942 RBH 03/23/2017 1235 37862

AnalyticalCASParameter Number Method Result Q PQL Units Run1,1'-Biphenyl 92-52-4 8270D ND 1ug/L4.02,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/L4.02,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/L4.02,4-Dichlorophenol 120-83-2 8270D ND 1ug/L8.02,4-Dimethylphenol 105-67-9 8270D ND 1ug/L4.02,4-Dinitrophenol 51-28-5 8270D ND 1ug/L202,4-Dinitrotoluene 121-14-2 8270D ND 1ug/L8.02,6-Dinitrotoluene 606-20-2 8270D ND 1ug/L8.02-Chloronaphthalene 91-58-7 8270D ND 1ug/L4.02-Chlorophenol 95-57-8 8270D ND 1ug/L4.02-Methylnaphthalene 91-57-6 8270D ND 1ug/L0.802-Methylphenol 95-48-7 8270D ND 1ug/L4.02-Nitroaniline 88-74-4 8270D ND 1ug/L8.02-Nitrophenol 88-75-5 8270D ND 1ug/L4.03,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/L4.03+4-Methylphenol 106-44-5 8270D ND 1ug/L4.03-Nitroaniline 99-09-2 8270D ND 1ug/L8.04,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/L204-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/L4.04-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/L4.04-Chloroaniline 106-47-8 8270D ND 1ug/L8.04-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/L4.04-Nitroaniline 100-01-6 8270D ND 1ug/L8.04-Nitrophenol 100-02-7 8270D ND 1ug/L20Acenaphthene 83-32-9 8270D ND 1ug/L0.80Acenaphthylene 208-96-8 8270D ND 1ug/L0.80Acetophenone 98-86-2 8270D ND 1ug/L4.0Anthracene 120-12-7 8270D ND 1ug/L0.80Atrazine 1912-24-9 8270D ND 1ug/L4.0Benzaldehyde 100-52-7 8270D ND 1ug/L8.0Benzo(a)anthracene 56-55-3 8270D ND 1ug/L0.80Benzo(a)pyrene 50-32-8 8270D ND 1ug/L0.80Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/L0.80Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/L0.80Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/L0.80bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/L4.0bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/L4.0bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/L4.0bis(2-Ethylhexyl)phthalate 117-81-7 8270D 150 2ug/L20Butyl benzyl phthalate 85-68-7 8270D ND 1ug/L4.0Caprolactam 105-60-2 8270D ND 1ug/L8.0Carbazole 86-74-8 8270D ND 1ug/L4.0Chrysene 218-01-9 8270D ND 1ug/L0.80






Date Received:



SC21057-00503/21/2017 120203/21/2017

Aqueous

Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch1 3520C 8270D 1 03/30/2017 1924 RBH 03/23/2017 1235 378622 3520C 8270D 5 04/03/2017 0942 RBH 03/23/2017 1235 37862

AnalyticalCASParameter Number Method Result Q PQL Units RunDibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/L0.80Dibenzofuran 132-64-9 8270D ND 1ug/L4.0Diethylphthalate 84-66-2 8270D ND 1ug/L4.0Dimethyl phthalate 131-11-3 8270D ND 1ug/L4.0Di-n-butyl phthalate 84-74-2 8270D ND 1ug/L4.0Di-n-octylphthalate 117-84-0 8270D ND 1ug/L4.0Fluoranthene 206-44-0 8270D ND 1ug/L0.80Fluorene 86-73-7 8270D ND 1ug/L0.80Hexachlorobenzene 118-74-1 8270D ND 1ug/L4.0Hexachlorobutadiene 87-68-3 8270D ND 1ug/L4.0Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/L20Hexachloroethane 67-72-1 8270D ND 1ug/L4.0Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/L0.80Isophorone 78-59-1 8270D ND 1ug/L4.0Naphthalene 91-20-3 8270D ND 1ug/L0.80Nitrobenzene 98-95-3 8270D ND 1ug/L4.0N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/L4.0N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270D ND 1ug/L4.0Pentachlorophenol 87-86-5 8270D ND 1ug/L20Phenanthrene 85-01-8 8270D ND 1ug/L0.80Phenol 108-95-2 8270D ND 1ug/L4.0Pyrene 129-00-0 8270D ND 1ug/L0.80

AcceptanceAcceptance Run 2Run 1Surrogate Q % Recovery Limits % Recovery LimitsQ2-Fluorobiphenyl 73 37-129 74 37-1292-Fluorophenol 51 24-127 35 24-127Nitrobenzene-d5 84 38-127 54 38-127Phenol-d5 72 28-128 47 28-128Terphenyl-d14 78 10-148 72 10-1482,4,6-Tribromophenol 73 41-144 82 41-144






Date Received:



SC21057-00603/21/2017 115503/21/2017

Aqueous








Date Received:



SC21057-00703/21/2017 110503/21/2017

Aqueous








Date Received:



SC21057-00803/21/2017 105703/21/2017

Aqueous








Date Received:



SC21057-00903/21/2017 105003/21/2017

Aqueous








Date Received:



SC21057-01003/21/2017 104003/21/2017

Aqueous








Date Received:



SC21057-01103/21/2017 103003/21/2017

Aqueous








Date Received:



SC21057-01203/21/2017 104003/21/2017

Aqueous








Date Received:



SC21057-01303/21/2017 123003/21/2017

Aqueous








Date Received:



SC21057-01403/21/2017 141503/21/2017

Aqueous








Date Received:


NuEarth Solutions, LLCTrip Blank

SC21057-01503/21/201703/21/2017

Aqueous








Date Received:


NuEarth Solutions, LLCCR-SW-05 DUP

SC21057-01603/21/2017 120203/21/2017

Aqueous








Date Received:



SC21057-01603/21/2017 120203/21/2017

Aqueous








QC Summary


Volatile Organic Compounds by GC/MS - MBBatch: Prep Method:Sample ID: SQ37834-001

37834 5030BAnalytical Method: 8260B

Matrix: Aqueous

Parameter Result Q PQL Units Analysis DateDilAcetone ND 03/22/2017 215120 ug/L1Benzene ND 03/22/2017 21511.0 ug/L1Bromodichloromethane ND 03/22/2017 21511.0 ug/L1Bromoform ND 03/22/2017 21511.0 ug/L1Bromomethane (Methyl bromide) ND 03/22/2017 21512.0 ug/L12-Butanone (MEK) ND 03/22/2017 215110 ug/L1Carbon disulfide ND 03/22/2017 21511.0 ug/L1Carbon tetrachloride ND 03/22/2017 21511.0 ug/L1Chlorobenzene ND 03/22/2017 21511.0 ug/L1Chloroethane ND 03/22/2017 21512.0 ug/L1Chloroform ND 03/22/2017 21511.0 ug/L1Chloromethane (Methyl chloride) ND 03/22/2017 21511.0 ug/L1Cyclohexane ND 03/22/2017 21511.0 ug/L11,2-Dibromo-3-chloropropane (DBCP) ND 03/22/2017 21511.0 ug/L1Dibromochloromethane ND 03/22/2017 21511.0 ug/L11,2-Dibromoethane (EDB) ND 03/22/2017 21511.0 ug/L11,2-Dichlorobenzene ND 03/22/2017 21511.0 ug/L11,3-Dichlorobenzene ND 03/22/2017 21511.0 ug/L11,4-Dichlorobenzene ND 03/22/2017 21511.0 ug/L1Dichlorodifluoromethane ND 03/22/2017 21512.0 ug/L11,1-Dichloroethane ND 03/22/2017 21511.0 ug/L11,2-Dichloroethane ND 03/22/2017 21511.0 ug/L11,1-Dichloroethene ND 03/22/2017 21511.0 ug/L1cis-1,2-Dichloroethene ND 03/22/2017 21511.0 ug/L1trans-1,2-Dichloroethene ND 03/22/2017 21511.0 ug/L11,2-Dichloropropane ND 03/22/2017 21511.0 ug/L1cis-1,3-Dichloropropene ND 03/22/2017 21511.0 ug/L1trans-1,3-Dichloropropene ND 03/22/2017 21511.0 ug/L1Ethylbenzene ND 03/22/2017 21511.0 ug/L12-Hexanone ND 03/22/2017 215110 ug/L1Isopropylbenzene ND 03/22/2017 21511.0 ug/L1Methyl acetate ND 03/22/2017 21511.0 ug/L1Methyl tertiary butyl ether (MTBE) ND 03/22/2017 21511.0 ug/L14-Methyl-2-pentanone ND 03/22/2017 215110 ug/L1Methylcyclohexane ND 03/22/2017 21515.0 ug/L1Methylene chloride ND 03/22/2017 21511.0 ug/L1Styrene ND 03/22/2017 21511.0 ug/L11,1,2,2-Tetrachloroethane ND 03/22/2017 21511.0 ug/L1Tetrachloroethene ND 03/22/2017 21511.0 ug/L1Toluene ND 03/22/2017 21511.0 ug/L11,1,2-Trichloro-1,2,2-Trifluoroethane ND 03/22/2017 21511.0 ug/L11,2,4-Trichlorobenzene ND 03/22/2017 21511.0 ug/L11,1,1-Trichloroethane ND 03/22/2017 21511.0 ug/L11,1,2-Trichloroethane ND 03/22/2017 21511.0 ug/L1

Note: Calculations are performed before rounding to avoid round-off errors in calculated results

PQL = Practical quantitation limitND = Not detected at or above the PQLWhere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"

J = Estimated result < PQL and > MDLN = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%+ = RPD is out of criteria_


Volatile Organic Compounds by GC/MS - MBBatch: Prep Method:Sample ID: SQ37834-001


Matrix: Aqueous

Parameter Result Q PQL Units Analysis DateDilTrichloroethene ND 03/22/2017 21511.0 ug/L1Trichlorofluoromethane ND 03/22/2017 21511.0 ug/L1Vinyl chloride ND 03/22/2017 21511.0 ug/L1Xylenes (total) ND 03/22/2017 21511.0 ug/L1Surrogate Q % Rec Acceptance LimitBromofluorobenzene 96 70-1301,2-Dichloroethane-d4 97 70-130Toluene-d8 103 70-130





Volatile Organic Compounds by GC/MS - LCSBatch: Prep Method:Sample ID: SQ37834-002


Matrix: Aqueous

Parameter Result Q % RecSpike Amount Analysis Date% Rec LimitDil(ug/L) (ug/L)

Acetone 62 03/22/2017 205162100 60-1401Benzene 46 03/22/2017 20519250 70-1301Bromodichloromethane 49 03/22/2017 20519750 70-1301Bromoform 44 03/22/2017 20518750 70-1301Bromomethane (Methyl bromide) 45 03/22/2017 20519050 60-14012-Butanone (MEK) 83 03/22/2017 205183100 60-1401Carbon disulfide 43 03/22/2017 20518750 60-1401Carbon tetrachloride 49 03/22/2017 20519750 70-1301Chlorobenzene 46 03/22/2017 20519150 70-1301Chloroethane 44 03/22/2017 20518750 60-1401Chloroform 43 03/22/2017 20518650 70-1301Chloromethane (Methyl chloride) 39 03/22/2017 20517950 60-1401Cyclohexane 42 03/22/2017 20518550 70-13011,2-Dibromo-3-chloropropane (DBCP) 44 03/22/2017 20518850 70-1301Dibromochloromethane 50 03/22/2017 205110150 70-13011,2-Dibromoethane (EDB) 47 03/22/2017 20519450 70-13011,2-Dichlorobenzene 46 03/22/2017 20519250 70-13011,3-Dichlorobenzene 47 03/22/2017 20519450 70-13011,4-Dichlorobenzene 45 03/22/2017 20519050 70-1301Dichlorodifluoromethane 46 03/22/2017 20519250 60-14011,1-Dichloroethane 44 03/22/2017 20518850 70-13011,2-Dichloroethane 45 03/22/2017 20518950 70-13011,1-Dichloroethene 45 03/22/2017 20519050 70-1301cis-1,2-Dichloroethene 45 03/22/2017 20519050 70-1301trans-1,2-Dichloroethene 46 03/22/2017 20519150 70-13011,2-Dichloropropane 49 03/22/2017 20519850 70-1301cis-1,3-Dichloropropene 52 03/22/2017 205110550 70-1301trans-1,3-Dichloropropene 50 03/22/2017 205110050 70-1301Ethylbenzene 47 03/22/2017 20519350 70-13012-Hexanone 95 03/22/2017 205195100 60-1401Isopropylbenzene 49 03/22/2017 20519850 70-1301Methyl acetate 43 03/22/2017 20518650 15-1281Methyl tertiary butyl ether (MTBE) 40 03/22/2017 20518050 70-13014-Methyl-2-pentanone 99 03/22/2017 205199100 60-1401Methylcyclohexane 49 03/22/2017 20519850 70-1301Methylene chloride 42 03/22/2017 20518450 70-1301Styrene 51 03/22/2017 205110350 70-13011,1,2,2-Tetrachloroethane 46 03/22/2017 20519150 60-1401Tetrachloroethene 48 03/22/2017 20519550 70-1301Toluene 48 03/22/2017 20519750 70-13011,1,2-Trichloro-1,2,2-Trifluoroethane 43 03/22/2017 20518650 70-13011,2,4-Trichlorobenzene 50 03/22/2017 205110050 70-13011,1,1-Trichloroethane 43 03/22/2017 20518750 70-13011,1,2-Trichloroethane 46 03/22/2017 20519250 70-1301





Volatile Organic Compounds by GC/MS - LCSBatch: Prep Method:Sample ID: SQ37834-002


Matrix: Aqueous


Trichloroethene 48 03/22/2017 20519650 70-1301Trichlorofluoromethane 44 03/22/2017 20518950 70-1301Vinyl chloride 40 03/22/2017 20518150 70-1301Xylenes (total) 95 03/22/2017 205195100 70-1301Surrogate Q % Rec Acceptance LimitBromofluorobenzene 95 70-1301,2-Dichloroethane-d4 93 70-130Toluene-d8 101 70-130





Volatile Organic Compounds by GC/MS - DuplicateBatch: Prep Method:Sample ID: SC21057-001DU


Matrix: Aqueous

Parameter Result Q Analysis Date% RPD % RPD LimitSample Amount Dil(ug/L) (ug/L)

Acetone ND 03/23/2017 06120.00 20ND 1Benzene ND 03/23/2017 06120.00 20ND 1Bromodichloromethane ND 03/23/2017 06120.00 20ND 1Bromoform ND 03/23/2017 06120.00 20ND 1Bromomethane (Methyl bromide) ND 03/23/2017 06120.00 20ND 12-Butanone (MEK) ND 03/23/2017 06120.00 20ND 1Carbon disulfide ND 03/23/2017 06120.00 20ND 1Carbon tetrachloride ND 03/23/2017 06120.00 20ND 1Chlorobenzene ND 03/23/2017 06120.00 20ND 1Chloroethane ND 03/23/2017 06120.00 20ND 1Chloroform ND 03/23/2017 06120.00 20ND 1Chloromethane (Methyl chloride) ND 03/23/2017 06120.00 20ND 1Cyclohexane ND 03/23/2017 06120.00 20ND 11,2-Dibromo-3-chloropropane (DBCP) ND 03/23/2017 06120.00 20ND 1Dibromochloromethane ND 03/23/2017 06120.00 20ND 11,2-Dibromoethane (EDB) ND 03/23/2017 06120.00 20ND 11,4-Dichlorobenzene ND 03/23/2017 06120.00 20ND 11,3-Dichlorobenzene ND 03/23/2017 06120.00 20ND 11,2-Dichlorobenzene ND 03/23/2017 06120.00 20ND 1Dichlorodifluoromethane ND 03/23/2017 06120.00 20ND 11,2-Dichloroethane ND 03/23/2017 06120.00 20ND 11,1-Dichloroethane ND 03/23/2017 06120.00 20ND 1trans-1,2-Dichloroethene ND 03/23/2017 06120.00 20ND 1cis-1,2-Dichloroethene ND 03/23/2017 06120.00 20ND 11,1-Dichloroethene ND 03/23/2017 06120.00 20ND 11,2-Dichloropropane ND 03/23/2017 06120.00 20ND 1trans-1,3-Dichloropropene ND 03/23/2017 06120.00 20ND 1cis-1,3-Dichloropropene ND 03/23/2017 06120.00 20ND 1Ethylbenzene ND 03/23/2017 06120.00 20ND 12-Hexanone ND 03/23/2017 06120.00 20ND 1Isopropylbenzene ND 03/23/2017 06120.00 20ND 1Methyl acetate ND 03/23/2017 06120.00 20ND 1Methyl tertiary butyl ether (MTBE) ND 03/23/2017 06120.00 20ND 14-Methyl-2-pentanone ND 03/23/2017 06120.00 20ND 1Methylcyclohexane ND 03/23/2017 06120.00 20ND 1Methylene chloride ND 03/23/2017 06120.00 20ND 1Styrene ND 03/23/2017 06120.00 20ND 11,1,2,2-Tetrachloroethane ND 03/23/2017 06120.00 20ND 1Tetrachloroethene ND 03/23/2017 06120.00 20ND 1Toluene ND 03/23/2017 06120.00 20ND 11,1,2-Trichloro-1,2,2-Trifluoroethane ND 03/23/2017 06120.00 20ND 11,2,4-Trichlorobenzene ND 03/23/2017 06120.00 20ND 11,1,2-Trichloroethane ND 03/23/2017 06120.00 20ND 11,1,1-Trichloroethane ND 03/23/2017 06120.00 20ND 1





Volatile Organic Compounds by GC/MS - DuplicateBatch: Prep Method:Sample ID: SC21057-001DU


Matrix: Aqueous

Parameter Result Q Analysis Date% RPD % RPD LimitSample Amount Dil(ug/L) (ug/L)

Trichloroethene ND 03/23/2017 06120.00 20ND 1Trichlorofluoromethane ND 03/23/2017 06120.00 20ND 1Vinyl chloride ND 03/23/2017 06120.00 20ND 1Xylenes (total) ND 03/23/2017 06120.00 20ND 1Surrogate Q % Rec Acceptance Limit1,2-Dichloroethane-d4 94 70-130Bromofluorobenzene 93 70-130Toluene-d8 100 70-130





Volatile Organic Compounds by GC/MS - MSBatch: Prep Method:Sample ID: SC21057-002MS


Matrix: Aqueous

Parameter Result Q % RecSpike Amount Analysis Date% Rec Limit

Sample Amount Dil(ug/L) (ug/L) (ug/L)Acetone 76 03/23/2017 063676100 60-140ND 1Benzene 50 03/23/2017 063610050 72-127ND 1Bromodichloromethane 51 03/23/2017 063610350 71-143ND 1Bromoform 43 03/23/2017 06368650 65-131ND 1Bromomethane (Methyl bromide) 48 03/23/2017 06369750 36-168ND 12-Butanone (MEK) 88 03/23/2017 063688100 60-140ND 1Carbon disulfide 45 03/23/2017 06369150 60-140ND 1Carbon tetrachloride 54 03/23/2017 063610950 37-166ND 1Chlorobenzene 50 03/23/2017 06369950 78-129ND 1Chloroethane 49 03/23/2017 06369750 60-140ND 1Chloroform 47 03/23/2017 06369450 63-123ND 1Chloromethane (Methyl chloride) 46 03/23/2017 06369250 20-158ND 1Cyclohexane 48 03/23/2017 06369750 70-130ND 11,2-Dibromo-3-chloropropane (DBCP) 45 03/23/2017 06369150 70-130ND 1Dibromochloromethane 51 03/23/2017 063610250 74-134ND 11,2-Dibromoethane (EDB) 50 03/23/2017 063610150 70-130ND 11,4-Dichlorobenzene 47 03/23/2017 06369450 70-130ND 11,3-Dichlorobenzene 48 03/23/2017 06369650 70-130ND 11,2-Dichlorobenzene 48 03/23/2017 06369750 70-130ND 1Dichlorodifluoromethane 51 03/23/2017 063610150 10-158ND 11,2-Dichloroethane 48 03/23/2017 06369650 59-143ND 11,1-Dichloroethane 49 03/23/2017 06369850 69-132ND 1trans-1,2-Dichloroethene 50 03/23/2017 063610150 67-141ND 1cis-1,2-Dichloroethene 49 03/23/2017 06369950 70-130ND 11,1-Dichloroethene 51 03/23/2017 063610350 50-132ND 11,2-Dichloropropane 53 03/23/2017 063610550 71-126ND 1trans-1,3-Dichloropropene 51 03/23/2017 063610250 73-131ND 1cis-1,3-Dichloropropene 53 03/23/2017 063610750 69-130ND 1Ethylbenzene 51 03/23/2017 063610150 79-132ND 12-Hexanone 98 03/23/2017 063698100 60-140ND 1Isopropylbenzene 53 03/23/2017 063610750 70-130ND 1Methyl acetate 41 03/23/2017 06368250 15-128ND 1Methyl tertiary butyl ether (MTBE) 44 03/23/2017 06368850 60-140ND 14-Methyl-2-pentanone 100 03/23/2017 0636105100 60-140ND 1Methylcyclohexane 54 03/23/2017 063610750 70-130ND 1Methylene chloride 46 03/23/2017 06369350 69-129ND 1Styrene 54 03/23/2017 063610750 70-130ND 11,1,2,2-Tetrachloroethane 48 03/23/2017 06369650 60-155ND 1Tetrachloroethene 51 03/23/2017 063610250 70-130ND 1Toluene 53 03/23/2017 063610550 75-125ND 11,1,2-Trichloro-1,2,2-Trifluoroethane 48 03/23/2017 06369650 70-130ND 11,2,4-Trichlorobenzene 52 03/23/2017 063610450 70-130ND 11,1,2-Trichloroethane 48 03/23/2017 06369650 77-132ND 11,1,1-Trichloroethane 49 03/23/2017 06369850 77-132ND 1





Volatile Organic Compounds by GC/MS - MSBatch: Prep Method:Sample ID: SC21057-002MS


Matrix: Aqueous


Sample Amount Dil(ug/L) (ug/L) (ug/L)Trichloroethene 52 03/23/2017 063610450 73-124ND 1Trichlorofluoromethane 50 03/23/2017 06369950 41-173ND 1Vinyl chloride 45 03/23/2017 06369050 29-159ND 1Xylenes (total) 100 03/23/2017 0636103100 70-130ND 1Surrogate Q % Rec Acceptance Limit1,2-Dichloroethane-d4 94 70-130Bromofluorobenzene 98 70-130Toluene-d8 103 70-130





Semivolatile Organic Compounds by GC/MS - MBBatch: Prep Method:

Prep Date:Sample ID: SQ37862-001

37862 3520C03/23/2017 1235Analytical Method: 8270D

Matrix: Aqueous

Parameter Result Q PQL Units Analysis DateDil1,1'-Biphenyl ND 03/30/2017 14344.0 ug/L12,4,5-Trichlorophenol ND 03/30/2017 14344.0 ug/L12,4,6-Trichlorophenol ND 03/30/2017 14344.0 ug/L12,4-Dichlorophenol ND 03/30/2017 14348.0 ug/L12,4-Dimethylphenol ND 03/30/2017 14344.0 ug/L12,4-Dinitrophenol ND 03/30/2017 143420 ug/L12,4-Dinitrotoluene ND 03/30/2017 14348.0 ug/L12,6-Dinitrotoluene ND 03/30/2017 14348.0 ug/L12-Chloronaphthalene ND 03/30/2017 14344.0 ug/L12-Chlorophenol ND 03/30/2017 14344.0 ug/L12-Methylnaphthalene ND 03/30/2017 14340.80 ug/L12-Methylphenol ND 03/30/2017 14344.0 ug/L12-Nitroaniline ND 03/30/2017 14348.0 ug/L12-Nitrophenol ND 03/30/2017 14344.0 ug/L13+4-Methylphenol ND 03/30/2017 14344.0 ug/L13,3'-Dichlorobenzidine ND 03/30/2017 14344.0 ug/L13-Nitroaniline ND 03/30/2017 14348.0 ug/L14,6-Dinitro-2-methylphenol ND 03/30/2017 143420 ug/L14-Bromophenyl phenyl ether ND 03/30/2017 14344.0 ug/L14-Chloro-3-methyl phenol ND 03/30/2017 14344.0 ug/L14-Chloroaniline ND 03/30/2017 14348.0 ug/L14-Chlorophenyl phenyl ether ND 03/30/2017 14344.0 ug/L14-Nitroaniline ND 03/30/2017 14348.0 ug/L14-Nitrophenol ND 03/30/2017 143420 ug/L1Acenaphthene ND 03/30/2017 14340.80 ug/L1Acenaphthylene ND 03/30/2017 14340.80 ug/L1Acetophenone ND 03/30/2017 14344.0 ug/L1Anthracene ND 03/30/2017 14340.80 ug/L1Atrazine ND 03/30/2017 14344.0 ug/L1Benzaldehyde ND 03/30/2017 14348.0 ug/L1Benzo(a)anthracene ND 03/30/2017 14340.80 ug/L1Benzo(a)pyrene ND 03/30/2017 14340.80 ug/L1Benzo(b)fluoranthene ND 03/30/2017 14340.80 ug/L1Benzo(g,h,i)perylene ND 03/30/2017 14340.80 ug/L1Benzo(k)fluoranthene ND 03/30/2017 14340.80 ug/L1bis (2-Chloro-1-methylethyl) ether ND 03/30/2017 14344.0 ug/L1bis(2-Chloroethoxy)methane ND 03/30/2017 14344.0 ug/L1bis(2-Chloroethyl)ether ND 03/30/2017 14344.0 ug/L1bis(2-Ethylhexyl)phthalate ND 03/30/2017 14344.0 ug/L1Butyl benzyl phthalate ND 03/30/2017 14344.0 ug/L1Caprolactam ND 03/30/2017 14348.0 ug/L1Carbazole ND 03/30/2017 14344.0 ug/L1Chrysene ND 03/30/2017 14340.80 ug/L1Di-n-butyl phthalate ND 03/30/2017 14344.0 ug/L1








Matrix: Aqueous

Parameter Result Q PQL Units Analysis DateDilDi-n-octylphthalate ND 03/30/2017 14344.0 ug/L1Dibenzo(a,h)anthracene ND 03/30/2017 14340.80 ug/L1Dibenzofuran ND 03/30/2017 14344.0 ug/L1Diethylphthalate ND 03/30/2017 14344.0 ug/L1Dimethyl phthalate ND 03/30/2017 14344.0 ug/L1Fluoranthene ND 03/30/2017 14340.80 ug/L1Fluorene ND 03/30/2017 14340.80 ug/L1Hexachlorobenzene ND 03/30/2017 14344.0 ug/L1Hexachlorobutadiene ND 03/30/2017 14344.0 ug/L1Hexachlorocyclopentadiene ND 03/30/2017 143420 ug/L1Hexachloroethane ND 03/30/2017 14344.0 ug/L1Indeno(1,2,3-c,d)pyrene ND 03/30/2017 14340.80 ug/L1Isophorone ND 03/30/2017 14344.0 ug/L1N-Nitrosodi-n-propylamine ND 03/30/2017 14344.0 ug/L1N-Nitrosodiphenylamine (Diphenylamine) ND 03/30/2017 14344.0 ug/L1Naphthalene ND 03/30/2017 14340.80 ug/L1Nitrobenzene ND 03/30/2017 14344.0 ug/L1Pentachlorophenol ND 03/30/2017 143420 ug/L1Phenanthrene ND 03/30/2017 14340.80 ug/L1Phenol ND 03/30/2017 14344.0 ug/L1Pyrene ND 03/30/2017 14340.80 ug/L1Surrogate Q % Rec Acceptance Limit2,4,6-Tribromophenol 68 41-1442-Fluorobiphenyl 79 37-1292-Fluorophenol 59 24-127Nitrobenzene-d5 90 38-127Phenol-d5 73 28-128Terphenyl-d14 94 10-148





Semivolatile Organic Compounds by GC/MS - LCSBatch: Prep Method:



Matrix: Aqueous


1,1'-Biphenyl 33 03/30/2017 15228240 30-13012,4,5-Trichlorophenol 33 03/30/2017 15228240 30-13012,4,6-Trichlorophenol 30 03/30/2017 15227540 30-13012,4-Dichlorophenol 29 03/30/2017 15227340 30-13012,4-Dimethylphenol 33 03/30/2017 15228340 30-13012,4-Dinitrophenol 56 03/30/2017 15227180 11-12612,4-Dinitrotoluene 37 03/30/2017 15229340 30-13012,6-Dinitrotoluene 37 03/30/2017 15229340 30-13012-Chloronaphthalene 32 03/30/2017 15227940 30-13012-Chlorophenol 32 03/30/2017 15228040 30-13012-Methylnaphthalene 30 03/30/2017 15227640 40-13212-Methylphenol 45 03/30/2017 152211140 30-13012-Nitroaniline 39 03/30/2017 15229840 30-13012-Nitrophenol 34 03/30/2017 15228440 30-13013+4-Methylphenol 45 03/30/2017 152211240 30-13013,3'-Dichlorobenzidine 25 03/30/2017 15226140 30-13013-Nitroaniline 31 03/30/2017 15227840 30-13014,6-Dinitro-2-methylphenol 35 03/30/2017 15228840 30-13014-Bromophenyl phenyl ether 33 03/30/2017 15228340 30-13014-Chloro-3-methyl phenol 35 03/30/2017 15228740 30-13014-Chloroaniline 27 03/30/2017 15226740 12-15714-Chlorophenyl phenyl ether 31 03/30/2017 15227840 30-13014-Nitroaniline 38 03/30/2017 15229440 30-13014-Nitrophenol 71 03/30/2017 15228880 30-1301Acenaphthene 36 03/30/2017 15229040 30-1301Acenaphthylene 37 03/30/2017 15229240 30-1301Acetophenone 43 03/30/2017 152210740 30-1301Anthracene 35 03/30/2017 15228940 30-1301Atrazine 36 03/30/2017 15228940 30-1301Benzaldehyde 29 03/30/2017 15227240 30-1301Benzo(a)anthracene 36 03/30/2017 15229040 30-1301Benzo(a)pyrene 34 03/30/2017 15228440 30-1301Benzo(b)fluoranthene 37 03/30/2017 15229240 30-1301Benzo(g,h,i)perylene 42 03/30/2017 152210540 30-1301Benzo(k)fluoranthene 35 03/30/2017 15228840 30-1301bis (2-Chloro-1-methylethyl) ether 42 03/30/2017 152210540 30-1301bis(2-Chloroethoxy)methane 36 03/30/2017 15229040 30-1301bis(2-Chloroethyl)ether 40 03/30/2017 15229940 30-1301bis(2-Ethylhexyl)phthalate 46 03/30/2017 152211440 30-1301Butyl benzyl phthalate 45 03/30/2017 152211340 30-1301Caprolactam 37 03/30/2017 15229140 30-1301Carbazole 37 03/30/2017 15229240 30-1301Chrysene 36 03/30/2017 15229040 30-1301Di-n-butyl phthalate 42 03/30/2017 152210640 30-1301








Matrix: Aqueous


Di-n-octylphthalate 46 03/30/2017 152211440 30-1301Dibenzo(a,h)anthracene 32 03/30/2017 15227940 30-1301Dibenzofuran 35 03/30/2017 15228840 30-1301Diethylphthalate 40 03/30/2017 152210040 30-1301Dimethyl phthalate 37 03/30/2017 15229340 30-1301Fluoranthene 36 03/30/2017 15229140 30-1301Fluorene 34 03/30/2017 15228540 30-1301Hexachlorobenzene 34 03/30/2017 15228540 30-1301Hexachlorobutadiene 25 03/30/2017 15226240 24-1101Hexachlorocyclopentadiene 100 03/30/2017 152250200 22-1221Hexachloroethane 30 03/30/2017 15227540 30-1301Indeno(1,2,3-c,d)pyrene 38 03/30/2017 15229640 30-1301Isophorone 40 03/30/2017 15229940 30-1301N-Nitrosodi-n-propylamine 46 03/30/2017 152211640 30-1301N-Nitrosodiphenylamine (Diphenylamine) 31 03/30/2017 15227840 18-1801Naphthalene 33 03/30/2017 15228240 30-1301Nitrobenzene 40 03/30/2017 152210140 30-1301Pentachlorophenol 59 03/30/2017 15227480 30-1301Phenanthrene 36 03/30/2017 15229140 30-1301Phenol 34 03/30/2017 15228640 30-1301Pyrene 41 03/30/2017 152210140 30-1301Surrogate Q % Rec Acceptance Limit2,4,6-Tribromophenol 82 41-1442-Fluorobiphenyl 78 37-1292-Fluorophenol 67 24-127Nitrobenzene-d5 94 38-127Phenol-d5 84 28-128Terphenyl-d14 84 10-148





Semivolatile Organic Compounds by GC/MS - MSBatch: Prep Method:

Prep Date:Sample ID: SC21057-004MS


Matrix: Aqueous


Sample Amount Dil(ug/L) (ug/L) (ug/L)1,1'-Biphenyl 64 03/30/2017 18368080 30-130ND 12,4,5-Trichlorophenol 62 03/30/2017 18367780 30-130ND 12,4,6-Trichlorophenol 58 03/30/2017 18367380 30-130ND 12,4-Dichlorophenol 58 03/30/2017 18367280 30-130ND 12,4-Dimethylphenol 60 03/30/2017 18367580 30-130ND 12,4-Dinitrophenol 110 03/30/2017 183670160 30-130ND 12,4-Dinitrotoluene 70 03/30/2017 18368880 30-130ND 12,6-Dinitrotoluene 71 03/30/2017 18368880 30-130ND 12-Chloronaphthalene 62 03/30/2017 18367880 30-130ND 12-Chlorophenol 63 03/30/2017 18367880 30-130ND 12-Methylnaphthalene 60 03/30/2017 18367580 40-132ND 12-Methylphenol 88 03/30/2017 183611080 30-130ND 12-Nitroaniline 75 03/30/2017 18369480 30-130ND 12-Nitrophenol 65 03/30/2017 18368280 30-130ND 13,3'-Dichlorobenzidine 48 03/30/2017 18366080 30-130ND 13+4-Methylphenol 88 03/30/2017 183611180 30-130ND 13-Nitroaniline 56 03/30/2017 18367080 30-130ND 14,6-Dinitro-2-methylphenol 63 03/30/2017 18367880 30-130ND 14-Bromophenyl phenyl ether 63 03/30/2017 18367980 30-130ND 14-Chloro-3-methyl phenol 66 03/30/2017 18368380 30-130ND 14-Chloroaniline 46 03/30/2017 18365780 10-130ND 14-Chlorophenyl phenyl ether 61 03/30/2017 18367780 30-130ND 14-Nitroaniline 70 03/30/2017 18368780 30-130ND 14-Nitrophenol 150 03/30/2017 183691160 30-130ND 1Acenaphthene 69 03/30/2017 18368780 30-130ND 1Acenaphthylene 70 03/30/2017 18368780 30-130ND 1Acetophenone 83 03/30/2017 183610480 30-130ND 1Anthracene 67 03/30/2017 18368380 30-130ND 1Atrazine 68 03/30/2017 18368680 30-130ND 1Benzaldehyde 44 03/30/2017 18365680 30-130ND 1Benzo(a)anthracene 70 03/30/2017 18368780 30-130ND 1Benzo(a)pyrene 69 03/30/2017 18368680 30-130ND 1Benzo(b)fluoranthene 85 03/30/2017 183610680 30-130ND 1Benzo(g,h,i)perylene 52 03/30/2017 18366580 30-130ND 1Benzo(k)fluoranthene 81 03/30/2017 183610180 30-130ND 1bis (2-Chloro-1-methylethyl) ether 83 03/30/2017 183610380 30-130ND 1bis(2-Chloroethoxy)methane 69 03/30/2017 18368780 30-130ND 1bis(2-Chloroethyl)ether 77 03/30/2017 18369780 30-130ND 1bis(2-Ethylhexyl)phthalate 87 03/30/2017 183610980 70-131ND 1Butyl benzyl phthalate 86 03/30/2017 183610880 30-130ND 1Caprolactam 73 03/30/2017 18369180 30-130ND 1Carbazole 70 03/30/2017 18368880 30-130ND 1Chrysene 69 03/30/2017 18368680 30-130ND 1Dibenzo(a,h)anthracene 44 03/30/2017 18365580 30-130ND 1





Semivolatile Organic Compounds by GC/MS - MSBatch: Prep Method:

Prep Date:Sample ID: SC21057-004MS


Matrix: Aqueous


Sample Amount Dil(ug/L) (ug/L) (ug/L)Dibenzofuran 68 03/30/2017 18368580 30-130ND 1Diethylphthalate 79 03/30/2017 18369880 30-130ND 1Dimethyl phthalate 72 03/30/2017 18369080 30-130ND 1Di-n-butyl phthalate 83 03/30/2017 183610480 30-130ND 1Di-n-octylphthalate 120 03/30/2017 1836N 15280 30-130ND 1Fluoranthene 71 03/30/2017 18368980 30-130ND 1Fluorene 66 03/30/2017 18368280 30-130ND 1Hexachlorobenzene 64 03/30/2017 18368180 30-130ND 1Hexachlorobutadiene 51 03/30/2017 18366480 24-110ND 1Hexachlorocyclopentadiene 140 03/30/2017 183634400 22-122ND 1Hexachloroethane 57 03/30/2017 18367280 30-130ND 1Indeno(1,2,3-c,d)pyrene 53 03/30/2017 18366780 30-130ND 1Isophorone 77 03/30/2017 18369780 30-130ND 1Naphthalene 62 03/30/2017 18367880 30-130ND 1Nitrobenzene 78 03/30/2017 18369880 30-130ND 1N-Nitrosodi-n-propylamine 90 03/30/2017 183611380 30-130ND 1N-Nitrosodiphenylamine (Diphenylamine) 58 03/30/2017 18367380 30-130ND 1Pentachlorophenol 120 03/30/2017 183672160 30-130ND 1Phenanthrene 70 03/30/2017 18368780 30-130ND 1Phenol 66 03/30/2017 18368380 30-130ND 1Pyrene 75 03/30/2017 18369480 30-130ND 1Surrogate Q % Rec Acceptance Limit2-Fluorobiphenyl 75 37-1292-Fluorophenol 66 24-127Nitrobenzene-d5 92 38-127Phenol-d5 80 28-128Terphenyl-d14 79 10-1482,4,6-Tribromophenol 78 41-144





Semivolatile Organic Compounds by GC/MS - MSDBatch: Prep Method:

Prep Date:Sample ID: SC21057-004MD


Matrix: Aqueous

Parameter Result Q % RecSpike Amount Analysis Date% RPD % Rec Limit % RPD Limit

Sample Amount Dil(ug/L) (ug/L) (ug/L)1,1'-Biphenyl 63 03/30/2017 19007880 30-1302.3 40ND 12,4,5-Trichlorophenol 62 03/30/2017 19007780 30-1300.18 40ND 12,4,6-Trichlorophenol 58 03/30/2017 19007380 30-1300.39 40ND 12,4-Dichlorophenol 55 03/30/2017 19006980 30-1304.2 40ND 12,4-Dimethylphenol 58 03/30/2017 19007380 30-1302.7 40ND 12,4-Dinitrophenol 120 03/30/2017 190073160 30-1303.6 40ND 12,4-Dinitrotoluene 71 03/30/2017 19008980 30-1301.3 40ND 12,6-Dinitrotoluene 71 03/30/2017 19008880 30-1300.26 40ND 12-Chloronaphthalene 61 03/30/2017 19007680 30-1302.5 40ND 12-Chlorophenol 59 03/30/2017 19007380 30-1306.5 40ND 12-Methylnaphthalene 58 03/30/2017 19007280 40-1323.4 40ND 12-Methylphenol 86 03/30/2017 190010880 30-1302.6 40ND 12-Nitroaniline 77 03/30/2017 19009680 30-1302.4 40ND 12-Nitrophenol 65 03/30/2017 19008180 30-1300.79 40ND 13,3'-Dichlorobenzidine 56 03/30/2017 19007080 30-13015 40ND 13+4-Methylphenol 80 03/30/2017 190010080 30-13010 40ND 13-Nitroaniline 54 03/30/2017 19006780 30-1303.5 40ND 14,6-Dinitro-2-methylphenol 64 03/30/2017 19008080 30-1301.8 40ND 14-Bromophenyl phenyl ether 62 03/30/2017 19007780 30-1302.9 40ND 14-Chloro-3-methyl phenol 66 03/30/2017 19008280 30-1300.78 40ND 14-Chloroaniline 39 03/30/2017 19004980 10-13016 40ND 14-Chlorophenyl phenyl ether 61 03/30/2017 19007680 30-1300.77 40ND 14-Nitroaniline 74 03/30/2017 19009280 30-1305.3 40ND 14-Nitrophenol 63 03/30/2017 1900+ 39160 30-13079 40ND 1Acenaphthene 69 03/30/2017 19008680 30-1300.79 40ND 1Acenaphthylene 70 03/30/2017 19008780 30-1300.48 40ND 1Acetophenone 79 03/30/2017 19009880 30-1306.0 40ND 1Anthracene 68 03/30/2017 19008480 30-1301.4 40ND 1Atrazine 71 03/30/2017 19008980 30-1303.5 40ND 1Benzaldehyde 34 03/30/2017 19004380 30-13026 40ND 1Benzo(a)anthracene 69 03/30/2017 19008780 30-1300.81 40ND 1Benzo(a)pyrene 70 03/30/2017 19008780 30-1301.4 40ND 1Benzo(b)fluoranthene 83 03/30/2017 190010480 30-1301.9 40ND 1Benzo(g,h,i)perylene 54 03/30/2017 19006880 30-1303.7 40ND 1Benzo(k)fluoranthene 80 03/30/2017 190010080 30-1300.61 40ND 1bis (2-Chloro-1-methylethyl) ether 77 03/30/2017 19009680 30-1306.9 40ND 1bis(2-Chloroethoxy)methane 68 03/30/2017 19008480 30-1302.6 40ND 1bis(2-Chloroethyl)ether 76 03/30/2017 19009580 30-1301.5 40ND 1bis(2-Ethylhexyl)phthalate 86 03/30/2017 190010780 70-1311.8 40ND 1Butyl benzyl phthalate 84 03/30/2017 190010580 30-1302.6 40ND 1Caprolactam 75 03/30/2017 19009480 30-1303.0 40ND 1Carbazole 70 03/30/2017 19008780 30-1301.1 40ND 1Chrysene 69 03/30/2017 19008680 30-1300.63 40ND 1Dibenzo(a,h)anthracene 46 03/30/2017 19005880 30-1304.6 40ND 1





Semivolatile Organic Compounds by GC/MS - MSDBatch: Prep Method:

Prep Date:Sample ID: SC21057-004MD


Matrix: Aqueous

Parameter Result Q % RecSpike Amount Analysis Date% RPD % Rec Limit % RPD Limit

Sample Amount Dil(ug/L) (ug/L) (ug/L)Dibenzofuran 68 03/30/2017 19008480 30-1300.96 40ND 1Diethylphthalate 78 03/30/2017 19009880 30-1300.14 40ND 1Dimethyl phthalate 72 03/30/2017 19009080 30-1300.13 40ND 1Di-n-butyl phthalate 81 03/30/2017 190010180 30-1302.4 40ND 1Di-n-octylphthalate 120 03/30/2017 1900N 14880 30-1302.8 40ND 1Fluoranthene 70 03/30/2017 19008880 30-1300.80 40ND 1Fluorene 65 03/30/2017 19008280 30-1300.40 40ND 1Hexachlorobenzene 63 03/30/2017 19007980 30-1301.7 40ND 1Hexachlorobutadiene 49 03/30/2017 19006180 24-1104.1 40ND 1Hexachlorocyclopentadiene 140 03/30/2017 190034400 22-1221.2 40ND 1Hexachloroethane 55 03/30/2017 19006980 30-1303.6 40ND 1Indeno(1,2,3-c,d)pyrene 55 03/30/2017 19006980 30-1303.6 40ND 1Isophorone 76 03/30/2017 19009580 30-1301.3 40ND 1Naphthalene 60 03/30/2017 19007580 30-1303.4 40ND 1Nitrobenzene 78 03/30/2017 19009780 30-1300.87 40ND 1N-Nitrosodi-n-propylamine 85 03/30/2017 190010680 30-1305.6 40ND 1N-Nitrosodiphenylamine (Diphenylamine) 61 03/30/2017 19007680 30-1304.0 40ND 1Pentachlorophenol 110 03/30/2017 1900N 14280 30-1301.6 40ND 1Phenanthrene 70 03/30/2017 19008780 30-1300.012 40ND 1Phenol 62 03/30/2017 19007780 30-1306.7 40ND 1Pyrene 74 03/30/2017 19009380 30-1300.79 40ND 1Surrogate Q % Rec Acceptance Limit2-Fluorobiphenyl 75 37-1292-Fluorophenol 62 24-127Nitrobenzene-d5 91 38-127Phenol-d5 76 28-128Terphenyl-d14 79 10-1482,4,6-Tribromophenol 80 41-144








Matrix: Aqueous

Parameter Result Q PQL Units Analysis DateDil1,1'-Biphenyl ND 03/30/2017 22374.0 ug/L12,4,5-Trichlorophenol ND 03/30/2017 22374.0 ug/L12,4,6-Trichlorophenol ND 03/30/2017 22374.0 ug/L12,4-Dichlorophenol ND 03/30/2017 22378.0 ug/L12,4-Dimethylphenol ND 03/30/2017 22374.0 ug/L12,4-Dinitrophenol ND 03/30/2017 223720 ug/L12,4-Dinitrotoluene ND 03/30/2017 22378.0 ug/L12,6-Dinitrotoluene ND 03/30/2017 22378.0 ug/L12-Chloronaphthalene ND 03/30/2017 22374.0 ug/L12-Chlorophenol ND 03/30/2017 22374.0 ug/L12-Methylnaphthalene ND 03/30/2017 22370.80 ug/L12-Methylphenol ND 03/30/2017 22374.0 ug/L12-Nitroaniline ND 03/30/2017 22378.0 ug/L12-Nitrophenol ND 03/30/2017 22374.0 ug/L13+4-Methylphenol ND 03/30/2017 22374.0 ug/L13,3'-Dichlorobenzidine ND 03/30/2017 22374.0 ug/L13-Nitroaniline ND 03/30/2017 22378.0 ug/L14,6-Dinitro-2-methylphenol ND 03/30/2017 223720 ug/L14-Bromophenyl phenyl ether ND 03/30/2017 22374.0 ug/L14-Chloro-3-methyl phenol ND 03/30/2017 22374.0 ug/L14-Chloroaniline ND 03/30/2017 22378.0 ug/L14-Chlorophenyl phenyl ether ND 03/30/2017 22374.0 ug/L14-Nitroaniline ND 03/30/2017 22378.0 ug/L14-Nitrophenol ND 03/30/2017 223720 ug/L1Acenaphthene ND 03/30/2017 22370.80 ug/L1Acenaphthylene ND 03/30/2017 22370.80 ug/L1Acetophenone ND 03/30/2017 22374.0 ug/L1Anthracene ND 03/30/2017 22370.80 ug/L1Atrazine ND 03/30/2017 22374.0 ug/L1Benzaldehyde ND 03/30/2017 22378.0 ug/L1Benzo(a)anthracene ND 03/30/2017 22370.80 ug/L1Benzo(a)pyrene ND 03/30/2017 22370.80 ug/L1Benzo(b)fluoranthene ND 03/30/2017 22370.80 ug/L1Benzo(g,h,i)perylene ND 03/30/2017 22370.80 ug/L1Benzo(k)fluoranthene ND 03/30/2017 22370.80 ug/L1bis (2-Chloro-1-methylethyl) ether ND 03/30/2017 22374.0 ug/L1bis(2-Chloroethoxy)methane ND 03/30/2017 22374.0 ug/L1bis(2-Chloroethyl)ether ND 03/30/2017 22374.0 ug/L1bis(2-Ethylhexyl)phthalate ND 03/30/2017 22374.0 ug/L1Butyl benzyl phthalate ND 03/30/2017 22374.0 ug/L1Caprolactam ND 03/30/2017 22378.0 ug/L1Carbazole ND 03/30/2017 22374.0 ug/L1Chrysene ND 03/30/2017 22370.80 ug/L1Di-n-butyl phthalate ND 03/30/2017 22374.0 ug/L1








Matrix: Aqueous

Parameter Result Q PQL Units Analysis DateDilDi-n-octylphthalate ND 03/30/2017 22374.0 ug/L1Dibenzo(a,h)anthracene ND 03/30/2017 22370.80 ug/L1Dibenzofuran ND 03/30/2017 22374.0 ug/L1Diethylphthalate ND 03/30/2017 22374.0 ug/L1Dimethyl phthalate ND 03/30/2017 22374.0 ug/L1Fluoranthene ND 03/30/2017 22370.80 ug/L1Fluorene ND 03/30/2017 22370.80 ug/L1Hexachlorobenzene ND 03/30/2017 22374.0 ug/L1Hexachlorobutadiene ND 03/30/2017 22374.0 ug/L1Hexachlorocyclopentadiene ND 03/30/2017 223720 ug/L1Hexachloroethane ND 03/30/2017 22374.0 ug/L1Indeno(1,2,3-c,d)pyrene ND 03/30/2017 22370.80 ug/L1Isophorone ND 03/30/2017 22374.0 ug/L1N-Nitrosodi-n-propylamine ND 03/30/2017 22374.0 ug/L1N-Nitrosodiphenylamine (Diphenylamine) ND 03/30/2017 22374.0 ug/L1Naphthalene ND 03/30/2017 22370.80 ug/L1Nitrobenzene ND 03/30/2017 22374.0 ug/L1Pentachlorophenol ND 03/30/2017 223720 ug/L1Phenanthrene ND 03/30/2017 22370.80 ug/L1Phenol ND 03/30/2017 22374.0 ug/L1Pyrene ND 03/30/2017 22370.80 ug/L1Surrogate Q % Rec Acceptance Limit2,4,6-Tribromophenol 74 41-1442-Fluorobiphenyl 83 37-1292-Fluorophenol 60 24-127Nitrobenzene-d5 91 38-127Phenol-d5 78 28-128Terphenyl-d14 94 10-148








Matrix: Aqueous


1,1'-Biphenyl 36 03/31/2017 18088940 30-13012,4,5-Trichlorophenol 33 03/31/2017 18088340 30-13012,4,6-Trichlorophenol 33 03/31/2017 18088340 30-13012,4-Dichlorophenol 30 03/31/2017 18087540 30-13012,4-Dimethylphenol 36 03/31/2017 18089140 30-13012,4-Dinitrophenol 80 03/31/2017 180810080 11-12612,4-Dinitrotoluene 41 03/31/2017 180810340 30-13012,6-Dinitrotoluene 41 03/31/2017 180810240 30-13012-Chloronaphthalene 34 03/31/2017 18088540 30-13012-Chlorophenol 32 03/31/2017 18088040 30-13012-Methylnaphthalene 32 03/31/2017 18088140 40-13212-Methylphenol 42 03/31/2017 180810540 30-13012-Nitroaniline 45 03/31/2017 180811240 30-13012-Nitrophenol 35 03/31/2017 18088940 30-13013+4-Methylphenol 40 03/31/2017 180810040 30-13013,3'-Dichlorobenzidine 2.5 03/31/2017 1808N 6.340 30-13013-Nitroaniline 19 03/31/2017 18084840 30-13014,6-Dinitro-2-methylphenol 40 03/31/2017 18089940 30-13014-Bromophenyl phenyl ether 35 03/31/2017 18088840 30-13014-Chloro-3-methyl phenol 38 03/31/2017 18089440 30-13014-Chloroaniline 20 03/31/2017 18085140 12-15714-Chlorophenyl phenyl ether 34 03/31/2017 18088640 30-13014-Nitroaniline 36 03/31/2017 18088940 30-13014-Nitrophenol 91 03/31/2017 180811380 30-1301Acenaphthene 38 03/31/2017 18089540 30-1301Acenaphthylene 39 03/31/2017 18089740 30-1301Acetophenone 43 03/31/2017 180810840 30-1301Anthracene 38 03/31/2017 18089540 30-1301Atrazine 35 03/31/2017 18088740 30-1301Benzaldehyde 21 03/31/2017 18085340 30-1301Benzo(a)anthracene 38 03/31/2017 18089640 30-1301Benzo(a)pyrene 38 03/31/2017 18089440 30-1301Benzo(b)fluoranthene 40 03/31/2017 180810140 30-1301Benzo(g,h,i)perylene 47 03/31/2017 180811840 30-1301Benzo(k)fluoranthene 39 03/31/2017 18089740 30-1301bis (2-Chloro-1-methylethyl) ether 43 03/31/2017 180810840 30-1301bis(2-Chloroethoxy)methane 37 03/31/2017 18089340 30-1301bis(2-Chloroethyl)ether 42 03/31/2017 180810640 30-1301bis(2-Ethylhexyl)phthalate 48 03/31/2017 180811940 30-1301Butyl benzyl phthalate 48 03/31/2017 180812040 30-1301Caprolactam 43 03/31/2017 180810740 30-1301Carbazole 40 03/31/2017 18089940 30-1301Chrysene 39 03/31/2017 18089740 30-1301Di-n-butyl phthalate 46 03/31/2017 180811440 30-1301








Matrix: Aqueous


Di-n-octylphthalate 48 03/31/2017 180811940 30-1301Dibenzo(a,h)anthracene 36 03/31/2017 18089040 30-1301Dibenzofuran 38 03/31/2017 18089540 30-1301Diethylphthalate 45 03/31/2017 180811340 30-1301Dimethyl phthalate 41 03/31/2017 180810140 30-1301Fluoranthene 40 03/31/2017 18089940 30-1301Fluorene 36 03/31/2017 18089140 30-1301Hexachlorobenzene 36 03/31/2017 18088940 30-1301Hexachlorobutadiene 26 03/31/2017 18086540 24-1101Hexachlorocyclopentadiene 110 03/31/2017 180853200 22-1221Hexachloroethane 33 03/31/2017 18088140 30-1301Indeno(1,2,3-c,d)pyrene 43 03/31/2017 180810940 30-1301Isophorone 42 03/31/2017 180810540 30-1301N-Nitrosodi-n-propylamine 49 03/31/2017 180812140 30-1301N-Nitrosodiphenylamine (Diphenylamine) 25 03/31/2017 18086140 18-1801Naphthalene 34 03/31/2017 18088640 30-1301Nitrobenzene 41 03/31/2017 180810340 30-1301Pentachlorophenol 66 03/31/2017 18088380 30-1301Phenanthrene 40 03/31/2017 180810040 30-1301Phenol 35 03/31/2017 18088640 30-1301Pyrene 43 03/31/2017 180810640 30-1301Surrogate Q % Rec Acceptance Limit2,4,6-Tribromophenol 90 41-1442-Fluorobiphenyl 83 37-1292-Fluorophenol 66 24-127Nitrobenzene-d5 100 38-127Phenol-d5 83 28-128Terphenyl-d14 88 10-148





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