AP42 Section: 11.3

Background Chapter Reference:

4 18

Title: Particulate Compliance Analysis For The Coal-Fired Brick Kiln, The Mogul Corporation, Charloffe, NC, January24, 1978.

I I I I I I I I I I I I I I I

., . . . A P 4 2 Section Reference ~eportsect . Reference

MOGUL a envirof e fvice

MOGUL

ENVIRONMENTAL CONTROL SERVICES

THE MOGUL CORPORATION

' * +W4y

A!! e+ The Mogul Corporation W A T E R T R E A T M E N T PRODUCTS A N D SERVICES SINCE 1915

CHAGRIN FALLS onio 44022 I?lbl 2.17 SO00 TELEX NUMBER 980324

m0GUL @ 1

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lV, I

February 13, 1978

REPLY TO:

Southern Division 1201 S. Graham Street Chwloffe. North Carolina 28203 17041 375-5726

t&. Paul S i e f f e r t Pullman-Swindell 4 4 1 Smi thf ie ld St. P i t t sbu rg , Pa. 15222

Subject: Pa r t i cu la t e Compliance Testing

Dear Mr. S i e f f e r t :

Enclosed are ,the r e s u l t s of the p a r t i c u l a t e compliance t e s t i n g performed on t h e b r i ck k i l n a t the Lee B r i c k and T i l e p l an t , Sanford, N. C. on January 24, 1978.

If you should have ques t ions which are not ' answered by. this ; r epor t , p l ease do no t hesitate ta con tac t me ,at our Char lo t te . . - of f i ce . . .

.~

i: . . .

Thank you raery much for u t i l i z i n g Mogul's Envi*oSeNices program . . .> , ' . - . . . , :. .

. . to obtain your p a r t i c u l a t e emission rates.. ... . ~ , . ~ .. . . . . . . . .

. .. , . . . ' yours very ..jxuly,', i . , . . . . . . .

. . ..

. . . .

Laboratory Manager . . . . .

WDF/sc . .

cc: In t r i p l i c a t e M r . Owen Foster Nr. B i l l McConnell

Enclosures

AIR QUALITY DIVISION CENTRAL OFFICE

I PLANTS AND LABORATORIES

Phoenix. Ar izona C A N A D A A U S T R A L I A Portland. Orcgon Winnioag, Manirnlls Thi3 Ni!ihling;~lc? Sul lo iv c o . . LKI. Inglewood. Cnli larnis M o n i r e ~ l , Qucl,crc S v d n r v . N. S. w .

Chagrin Fall%. Ohio Charlorlc. North Carolina Minnuaoolir. Minnesota Atlanta. Guorgia Arlingtori, Texas

Lconin. N e w Jersey I I

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- M OG u I, envirofe rvice

PREPARED ESPECIALLY FOR;

PDLLMAN-SWXNDJZLL LBE BRICK nt3fl TILE PLANT

8AtiFORD, Ep. C.

'PESTS: Parumlate Compliance Analysis fo r ths Cold P i r e d Brick Kiln

TESTS CONDUCTED BYa The C.4ogul Corporat$a blr . R. X. Pear-, Team Leader Mr. L e d 5 Frederick, Aesietant

TEST DATE: January 24, 1978

REPORT NUMBER1 5-12277-1

REPORT BY2 R. M. IJaaraa

TABLE OF CONTENTS

Introduction

Sampling & Analytical Procedures

Discussion

Summary of Results

Computer Printout

Raw Data

EPA Analytical Method

Calibration Data

Data From Records

.

PAGE 1

1

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1

2

Appendix I

Appendix 11

Appendix 111

Appendix IV

Appendix V

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MOGUL enviroiervne

INTRODUCTION

Partiaulate laampling of the atack gasee emittad fm.m the cold f irad brick k i l n was parformed at the Lee Bfick and T i l e plant, Sanford, N. C. on January 2 4 , 1970.

One two hour test was perfonwdl on ea& of the two stacks to deternine t \e pollutant mags rate aaaarding to the reg- ulations of the State of North Carolha. There ware no observers fran the State of North C a r o l i n a present.

Them 8ources were tested utilizing a Nutech Corporation, -1 261-300 particulats~staclc sampling syatm, which meets the &signed opacffLcaUon of tlm ~vLronmsuitcal Pmtection -cy. The method util ized fo r partlaulate m a l y ~ h wae the Envimmental Protaaotian Agency method as presented in the F&Er& -Volume 42, 168. August 8, 1977, Method V "mtennination of Particulate emissions for Stationary SOUrcn3B'.

RESULTS

For ease of interpretat ion, the'attachwl Wles out l ine the reeu l t s of each test perform@&. The couiputerlaed aalcula- t ions and raw data sheets bawd been included i n ttte report for specific calculat ion inforxiation.

DISCUSSION

%!he meximum allowable emission rate in lbs . /hr. of proaees w a s taken from the Ruculeeand Regulations t%verninq the Control of Air Pollution, Board of Water and Air Resources, Raleigh, N. C., January 2 3 , 1972, page c-30, 0-31.

... ..

C J H E, w 2 H x 0 m H

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W W N

p1 4 0 0 rl rl

m

a m

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3 z z 3 a

2

m

m

4

m W

r- N

,

P m

0 rl

N

W

m rl

d E+ 0 H

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nrvision to Reference Mathod!, 1-8 A(:I;NCY: EnvlronmcnLnl rrotccllon AxcllCY. . .: AC-noN: FLnal Rule. : ,. , . . . SIlhfMARY: lhk nllC rCV16C8 Rrfrrence A r m & 1 through 8. Vlc detoJlcd re-

,. q u i r m ~ c ~ ~ l s used Lo rncasurc eirilsslons lr~m1 nllcctcd facilities to ,dclcnnlliC

. iv l :~ ihcr Uiey nre 111 complinticc m l l h n SIUI:!:I~CI 01 pcriormmce. n i c ~iieJlials ivt.rv wtj:ina1ly promulgnted December

1!l71, nnd'slnce U I R ~ unicseveinl re- <mi hrcnmc apparent whIc11 would

clrri l ,~. corrixt nnd lmprovc the mclli- ods. ' r h e c revirlons ,ninkc the niathods cu lc r to usc. ruidlmprovc thclr nccwncy nid roli:;blllly. ' "

EITTCI?VE DATE: September IS. 1077. ADDRESSES: COPlcs 01 .'the co~ ' ICI I t 1cttcw:trc available for public InSpcctloll nnd.cnimiiii: .:d I h c US. Envlroinientrd

.Protection Agency. .Public InlormaUon Rctcreiire Uniii'(EPA Libr:tiy). Room 29?2. . tflI. M Street, 8.W.. washliigton; D.C. ?0460. A summnry of Lhc ColnlnCnts and EP:\'s rewonses may be obtalncd uwn writkn rcquext from the EPA Pub-

~ lic Inlormntion' Center (PM-215J. 401 ' M Strect. S.w:. Washington. D.C. 20460 , (s11ccify "Publlc" Comnient' Summnry: Rcvkions to Relcrcncc Method? 1-8 In Aplh2nJi.y A 01 Stnndtirds 01 PCrformniiCC for s e w Stnllonnry Sources") . FOR FLIRTHER,'INFORMATION CON- TACT: ' " . . .

Don R. Goodwln. Ernlsslon StRndnrds and EnElncerlng DIvk$lnn. Envlron- nwiitnl ProLectlon Agency. Rqcwcll

: Trinni:lc Park. North CnroIlna.27711. . ' telephone No. 918-841-5311.

SUPPLEMENTARY' INFbRhrATION:. l l i e nmcndments wcrc proposed on 3unc R . i w ~ ' ( 4 0 En 23oGO). A totnl oe 55 eom- mcnt lcltcrs were rccclvcd durlnu the comn~riit period-34 from IndudrY. 15 lrom jiovcrnmentnl hficncirs. niid 6 froin othcr inlrrcsted purtlcs: Thry conlnlnc(l numrrom supgcslions wl~Ich mere incor- p0;ntcd In Llic fiiml revisions.

Ch:tnr.cs ci,ninion l o nll eight of tho rcrcrrncc methotls i:rc: ( 1 ) tl?! rlnllncn- (.ion ol proccdorcs ~ i i d noiliimcnt wec- i ~ i ~ ; , t . i u ~ ~ s rciulting. from t l ~ c comincnL% 1 2 ~ Uir adtlilioii 01 guldcllncs for &I-

nntl eiiui~xn~!iit lo 01 the Ailliihilslra- (3 ) Uic odditlori of

an inlrcxnhiction lo ench rclcrcilcc IIICCII- "d tit:.rw:iin,{ lhc wncral ILIC or tlic nicLImI :uld d~ll~!c:tllna the ~woccrlllrC i m W:,>IK nltcrnntlvc mcthoils hind cclulu- I l l C I I t .

sl,t~rlflc chnnfics to tho nirthods nrc: Mmion 1

1. Thr r,rovlslon for 'the u.w 01 IIIO~C t h i l ~ l LC'O Lrnvcrsc dlmiclerti. wlicn RIWC-

. '

, ,

i&\triinr; has h h tlelcl.ol. I f 11110 1rnren;c dlnniclrr b In n i h i u wnitdiilii~ lhc trrcnlwt rxrrrctcd w ~ ~ ~ r i ~ t r ~ ~ l i ~ i n vnrlnllon. LIic Inlciidrd

.. iwrrxma: ui thc i i c i ~ ~ e t i p11rtt~ru1111 wili h fll11111,.d ' '

3. JI1c::rd 011 rccilll dnln Iroin Fluldync tl'iwllriilnw Snintrllnr:' Strntwles for IAU'KO l'nwc!r P l n i i ~ ~ Incltidiuu .Nonut - lorin, Flow. EPA-GOQ/2-70-170, June 1070) nnd Enlrouy EnvlronmentnlL.ts (Lktcrmlnntion of Llrc Opllmum N u m h r Of Tritvcrsc k'oliib: A n Annlynls o f Mcllirul 1 CrlLcrln IdmIL). Coritrncl No. 68-Q1-3172)). the, number or Lravcrsc polnLI. for vclorlty inensurcnicnlr lips bccn reIJuccil und the ?:l lcnglh to uldL11 rallo rcriulreincrrt fur cros-secllonnl lny- 0111 01 r e # ! h n ~ ~ ~ I n ~ 'dilcts has bccn. rc- plncetl by n "bdlniicrd nintrix" scheme. 3. 0uldi:lluep . fo r sn1npUn8 In stncka

contntiiliic C ~ C I O I U C 'now nnd stncks smnller Llinn iiboiit 0.31 melrr in diam- ctcr or U.071 m' In craw-h~ctlonnl nrcx wlll ba liiibllslicd nt n Inter date. . 4. Clnrinu~tlon .Iir becn mndc NI .k,

when n elicck for cyclonlc llow Is ncccs- m y : nho. uio a s t : w L e d imwedure for delcrmiiintlon of unncceptuble flow con- dltlons hns bccn rcviscd.

'

. ' MrnloD 2 ' .

1. Thc cnllbrnllon of certain pltot tube8 h m bcen mnde optlond. ApProlwlnle con- ~ t r u c l l o n nnd oyiillcntloi~ guidelines have been Incllldcd.

' .z. A delnll?d cnlibrntlon bro&iire ror tenipernturc gnlwes bns becn Included. 3. A lcnk .check Procedure ior Pitot

: lln.c? lius bccii lncludcd. . -M&IIOD 3 ...

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1: Tlie nvplicnitlllitrool the rneUiod has becn conrincd 'tu fos%ll-Iiicl roinbustloll procrssrs nnd to nlher proccsscs where I t hna b e n daltrrinlncd lhnt components othcr thnn 0:. CO,. CO. niid N, nre not present in conccntrntiom sufficient to .ancct tlic fliinl results.

2. Dnpd on rcccnt rcsearch Inlormn- tlon (PnrLlculnte Snrniiliiig Strntcgles for Lnrpu Powr? rlnttb Inchulir~s Noiiunl- 'iornt Plow. EI'A-GOO~2-7G-liil. Jlinc ~ ' J ~ u I . (he rixwircincnt for Iwoi)ortlonnl saml)linpl Iiiu 1)ccn druriued nnd rcplnccd. U.IUI L lw rcqiilrciiienl for conslnnt rate S W I I ~ I I I I ~ : , l'rolmr'tlonnl nnd eor:stniit mtc s n ~ , ~ l , i ~ n g h ~ : brrn roittld to give CSSCII- Unity 1.11~ snmc rcwlt .

3. The "tlirce culisrcullvc" require- ment l i i u be?n rolilnwd by "nny three"

. .. . . . , .. . -. c: 'nie &IC oi 'polycl.liylcne wu11 I,,,,. 11. The ilse of deslrcalik uthrr li?,...

LIPS irnd sample StOrnKe CnntnlncF;. . . ...... -. ~~~ ~

silica a c ~ or cnlcium sulfnto. wi l l , , appropriate.

e. nit? use of stoiicock crcwe ntlirr Limn slliconc grexve. when ~ ~ I ) ~ o I M I : , I ~ I. The drylnc 01 fllwrs mid probc-liii,r

ciilcli~s nt clevntcd tclnl~craturcr. BIW,, npprourinte.

E. The comblnlng or the flltrr niid probc -mshcs intu one contnlncr. 2. The leak chcch Prlor to n tcsl ~ I I I I

hns been .inn& optlonnl. The iast.trst Icxk chcck remnins ninndntory. A niulli. od for correctlw anmple vol~iine lor rs . ccsslve lcakwe rnter I ins been Iricludnl

3. Dewled lenk.check nnd Cnlibrnliw~ 'proccdurcs for the metcrrirs sysleq Iiwr been Included.

1.. Possible interfering agents of lhe n~cthod hnve bccn dclineated. 3. The optlolls of: (8) using n Mcthnl

8 .Impingcr systen,. or (b) drlcnniillnn SO, 6lmulcnneously with Iinrtiriilntr matter. have been Included i n the method. :

'3. Cased on recent research dnta. llic rcqulrcnicnt for prowrtional snnii~llnu hnr becn dropped N I ~ replaced wilh the rcqulrernent lor constniit rmte sniii~linu.

4. Tests have shoun thnl Liolrroiinliul ab'lnlncd from conimerci:il sourcrs oc- cn!lonally hna peroxlde Impurities thnl ~1.111 cause erroneously low SO: nicnsitre- ments. Tlirrelnrc. n test tor deleclinr wroxldei in Lsoixopnnol lim bccn hi- cludcd In the method.

5. The leak clicck bcrore the k s t RIII Iins bccn ninde rWinnul: Uic lctik ell+ nltcr the nln reinalns tnnndntrry. .

'

6. A dctailed calibration 1,rocctlure lor the irieterinb: zyslmn has been incluclrd in the method.

. . METIIOU 'I I , For vnrinblc wiivc IrnqtIi P I I I - C I I I I -

yllintonielcrs. n sr:iiinii)i: i~ ro t~ t Iu~ 'c l ' w dclcrmiiilng the iu~i i t or mnxlniiitii nli- sorbancc h:is bcrii iii~orpor:~l('iI 11:; i l l l opt 1011.

blrrtl,>il 8

bwn Ilstcd to nvold ~ I I S ; I ~ ~ J ~ C ~ I ~ I I I I O f t h e nirllinl.

2. The deLermln;itlml of flllvrtlbh' ~ I I tii.uIutc innticr t i i w l i i ~ l l r i l : tw1d n t h f I

Wii nlluu,cd whon: ui8idIcnbic. 3. Slncc occns!.l~n:tlly somr comwr-

r l i i l lp nrniluble guniiUtira of kwroiu!!~~I

11. IV?? P

~ ' .M&Oo 8 . .

1. xinowi ht~rrer1tv: r u n i p ~ ~ 1 1 1 i ~ 1 ~ hiiw

sIIIIuI1;III,~oIIsI." \ V l l h so, "1111 so. I W *

I.._.......__.. ~ ~

rctl~rrer. A s dcpied I n I Ell 2 or su!uarl A, lhc "AdmlnlulrnLcd' LIlvludcs nns nu- ll~orlmcl rfprcbclllnllw or Ule AdnilnlS- t.rnlor of tlie Envli'onln~:rrLnl ProlL'clInII Agrncy, AuthorlzCil rcI~rcs~:IlLntivcs nre ETA oln&lr 61 F:PA Ikcflnnnl OfBers or SLzlr. locnl. mid rceplnll:tl zovernnlenW otklnls who have bwn drlcmlcd llle re- sponsibility 01 enInrcillg I ' C A I I I ~ ~ I O I I S UII- der 40 CPR EO. T)lcrc nftlclnb 111 COIlSllltn- Won wltli othcr &lull nirlnbers lnllllllnr wlth tcchnlenl KqICcIS 01 SOIUCe ~ S l h l f i wlll mntlcr dreldons rrnnrcllng ncccpt- able alkrnnte l e s t prwnlurck. In ncrordnnce wiui sccLlon 111 of Lhc

Act. pUbllCnIIol1 of. Ulesc rnctllods wns prareddrd by consullnllon a i lh BPproLIrl- nlo advknIy rornmlttees. Independent experts. .and hdernl dcr)urlmenla m d anenclcs. , . .

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11756 RULES AND REGULATIONS

-n DUCT DIAMETERS UPSTREAM FROM'FLOW DISTURBANCE (DISTANCE A)

Figure

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1-1. traverses.

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I( ......................... <...... .... I I: ...................... : ................... 4 u ,I .............................................. 4.4 1 ,. ........................................... 5-1 ................................................. n.n :Y) ............................................ : no .:u ............................................. *.a e:.. ....................... ..! ................ 1.a w .............................................. 1.1

3.x .......

I.' -. t

0 50

. a.

iJ i

4417.57 RULES AND REOUlhTION5

DUCT DIAMETERS UPSTREAM FROM FLOW DISTURBANCE (DISTANCE A) L. 2.5 ' 2.0 1 .o 1.5

I 1 1 - I 1 I I

-

- . . -

. .

" 0

traverses.

I - I I I ' 1 I 9 10. . : I I .; . .

- 7 8 . R 4 5 . 6 . .

RULES AND REGULATIONS

4 iRAvrnsE .I POIPIT

1 2 3 4 5 6

DISIANCC, 5 O f dlnnlrt lr

D 4.4 14 .7 29.5 70.5 85.3 95.6 ? q

3 J 4 9

Figure 1-3. Example Jiowing circular rlack'crai x i i o n divided into 12 equal areas, wiIh loCalion 01 IravelY poinll indicated.

. ' ' Table 1.2. LOCATION'OF TRAVERSE POINlS IN CIRCULAR STACKS . . .

{Percent of stack diameter from inside wall t o traverse point)

Traver pofn

nmbei on a

dlamett - - 24

1.1 3.2 5.5 7.9, 10.5 13.2..

-

16.1 19.4 !1.0 17.2 12.3 19.8 80.2 t7.7

'7.0 io. 6 ,3.9 6.8 9.5

4.5 6.8

.2: 8 '.

2.1,

0.3

r tr, 10

2.1 0.:

1 4 . 1

34;; 65.1 77.1 85.4 91 . E 97.4

- -

22: I

Int , 14

1 .I 5.; 9. ! 4.1 '0.1 '6.! 16.1 83.4 3.1 9 .1 5.4 0.1 4.3 8.2

- -

awl I8

1 . d

4.4 7.!

14.1 18.f 23.f 29.f

- -

10.:

!8.2 61 .8 70.4 16.4 11 .2

99.1 P2.5 95.6 98.6

35.4

rre - 12

2. 6.

11. 17. 25. 15. 54 * 75. 32. I B . , 13.. 17.1

- in a

16

1.6 4.3 8.5 12.5 16.9 22.0 20.3 37.5 62.5 71.7 78.0 01.1 87.5 91.5 95: 1 9 8 A

- - - 22

1 . I 3.5 6.0 8.1 11.6 14.6 18.0 21 .8 26.2 31.5 39.3 60.7 58.5

13.8 18.2

12.0 35.4 B.4 n . 3 14.0 16.5 10.1

- -

20

1. 3. .6.

. 9. 12. 16.' 20.' 25.1 30.1 38.1 61 .i 69.4 75.1 79.1 OI.! 37.1 90.2 93.2 9G.l 90.7

- 1 2 3 41 5' 1 , 6

8 $ 1

. . i

9 10 11

13 14 1 5 111 16 17

121

22

24 J 23

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?SDDoAL L€Ul$l~1, VOL. '41. NO. IbO-THUISDAI. AVOUIl lI,"l977

i:

. ~ .. . . . . .. '2 ........... -.

c . .

RULES AND HtbUlAlIUNS U,.J.,

i

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Figure 2.1. Type S pitot tube manometer assembly.

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Figure 2.2. Properly constructed Type S pitot tube, shown in: (a) end view; face opening planes perpendicular to t r a w vcrsc axis; (b) top vicw; face opcnillg planes parallel to lon- gitudinal axis; (c) side view; both legs of equal length and centerlincs coincident, whcn viowed from both sides. Base- line cocflicient values of 0.84 may be assigiled to pitot tubes constructed . . , . this way., , , , ,

. . I

. . . .

c

.

a a

CURVED OR MITERED JUNCTION

I)

STATIC HOLES\ I

(-0.10)

I I 12.. , HEM!SPHERICAl *

TIP

Figure 2.4.. Standard pitot tube design specifications.

RULES AND REGULAIIONS

-_- -.- P L A N T D A T E - R U N NO.

B A R O M E T R I C PRESSURE. mm Hy (in. 119)

OPERATORS PITOT TUBE 1.0. NO. --

STACK OIAP;ETCR O R I I I M E N S I O N S , m(ie.)

CROSS SECTIONAL A R E A , 1112(112) - -

-

A V G . C O i F F I C I E N T , C p = -- LAST D A T E CALIBRATED _-- S C I I C M A T I C O F S T A C K

CROSS S C C T I O N

’ . Averaga

1

Figure 2.5. Vclocity travcrse data. . . .

R D E U L ECGlSlEl, VOI. 42. NO. lOO--TIIUI5DAY. AUGUST 18, lW7

! RULES AND RCGULATIONS I

' I . ":

. . . . . . . . . . .

. . A. .BOTTOM VIEW; SHOWING MINIMUM PITOT-NOZZLE SEPARATION.' , . . ' . .

. . . . . . . . .

. ,

-.A,-

--.-. . . . .

. . . . .. STRf AMLINES APPROACHING THE

' . , '..NOZZLE,THE IMPACTPRESSURE , . . i

. . OPENING PLANE OFTHE PITOT TUBE SIIALL BE EVEN WITH OR ABOVE THE NOZZLE ENTRY PLAIIE.

, ,

Figure.2.6. Proper pitot'tube - sampling nozzle configuration to pr&eht aerodynamic interference; buttonhook - type nozzle:,centen of nozzle

318 in.). c

. . ,. and pitot opening aligncd; Dt between 0.48 and.0.95 cm (3/16 : . and ., .

:.. FEDLIAL UtOlSlII, V0l.I 41. NO. lbO-lHUI1DAV. AUOu$l la , 1Pr7 ' ' - '

. . . . . . . . : .I . . . . . . . . . . . . . . . . . . . , . . I , . . . . . . - ~. I . 2 . . .

1 ! , " . '. . . . , . . . . . . . . . . .. w. . . . . I.. , . .

,.-. d,,'..' .: . . .

. A . , . . I , ,. , . . . , .. ,. . 4 ;, .'.,, . . . *, . :

Ca m

, .. i , .

r I i .

TYPE SP1101 TUUC , Q bI Ot

RULES AND REGULATIONS $17(i>

Figure 2.7. Proper therrnocouplc placemcnl io prevent inlcrference: Dt bclween 0.48 and 0.95 c m I3/16 and 318 in.).

I

TYPES PITOTTUBE . I I I 1 - Y 27.62 cm (3 in.)

I I

Figure 2-8. Minimum pitot-sample probe separation needed to prevent interference; Dt between 0.48 and 0.95 cm (3/16 and 3/8 in.).

/

FEDIDAL RCGljlFl. VOL 42, NO. lb&lllURSOAV, A W U S l I D , I P 7 7 0

417tiG RULES AND REGLllATlONS

. . . .. . .

' . 3

' . . . T: IC,il).Z,IA OR 611 -C MUST BE (0.01 AVERAGE DEYlATlON 8 u IA OR 6 )

3 . "

..' Figure 2.9. Pilot tube calibrpiiondata. ..

. . I

I r;

1 " " / . . ,." PULES AND REGULATIONS

SHEATH .

(XI

.Figure 2-10. Projectdnrea models

EXTCRNAL 1

(bf

100

for typical phot tube assemblics.

EW"lh 2 5 -.v,(l-lf"J+lP.o 11,

FtDrIAL DWlS11R, VOl. 41. NO. :IbOcTHUISOAY, AUGVSl l D , 1 V T I

............. . . . . . . . . . . a'. i ? ....

, .,..

I l i M RULES AND RtGULATlONS

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RULES AND REGULATIONS I

SOUEEZE D U L B '

Figure 3.1. Grabsampling train. . .

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PRO

OUlCK DISCONNECT-

RIGID CONTAINER

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Figure 3.2, Integrated gar.sampling train.

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RULES AND REGULATIONS

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PULES AND REGULATIOM

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. 1177.1 RULES AND REGULATIONS

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R U L t S AND REGULATIONS . ' . . . . ,

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' 41775 RULES AND RCGULATIO~S

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.' . COMMENTS . . . ' ~ ' LOCATION . .

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. . . . TEST : . ' \

. . . . .'. DATE . .

. ' OPERATOR . . . .

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8AROMETRlC PRESSURE .. . . .

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41770

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. . RULES AND REGULATIONS

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* 41777 i RULES AND REGULATIONS

IMPINGER TRAIN OPTIONA1.MAY BE REPLACEO TEMPERATUnE SENSOR

BY AN EOUIVALENT CONOCNSER

THERMOMETER CHECK VALVE

VACUUM LINE

IIEATEO AREA THEnMDMCTER

BY4'ASS VALVE

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' 41770 RULES AND REGULATIONS

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RULES AND REGULATIONS

Plant-', --

Run No. -

Amoun: liquid lost,duting tiansport -

Date ' ,

F h r No.

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Acetone wash volume. ml

Acstone . . blank conccntration;mg/mg (equalio11'54) . .

. . . Acetone wash blank, . . mg (equation 5.5) , '

: . .

. . . . Weight of pa+date :mat tw

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... . ., . ... . . . . , .

. . . . VOLUME OF LIOUID

... . WATER COLLECTED .... . . .

TOTAL VOLUME COLLECTED I ml

. CONVERT WEIGHT OF WATER TO VOLUME BY DIVIDING TOTAL WEIGHT INCREASE BY DENSITY OF WATER (lg/mlj.

INCREASE' ' r'VOLUhlE WATZR. ml 1 drnl

Flgure 5-3. Analytical dala.

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RULllS AND REGULATIONS

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- ._.._ RULES AND RLCULAllONS

THERMOMETER

GEL l U B E

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417R1 RULES AND REGULATIONS

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RULES AND REGULATIONS

NECK

. . Figure 7.1. Ssmpling train. IIask valve, and flash.

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' 417137' RULES AND REGULATIONS

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1 .

LOCATION

OPERATOR L " DATE

RUM YO.

SAMPLE BOX NO.

. . ,, . METERBOXNO.

METERAHB

417W

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RULES AND RECUIA~IONS

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WIBlfNTTEMPFRATURE BAROMETRIC PRESSURE

LSIUMEOM0ISTURE.X

CROBE LENGTtl.m ( I d , '

~ V E R A G E CALIBRATEO N O n L E DIAMETER.cmlin.)- . . , .

PROBE HEATERSETTING LEAK HATE, m~/nin,bfm)

PROBE LINER MATERIAL'

NOZZLE IOENTIFICATION NO.

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RULES AND REGULATIONS

. .. Equntion 6-1

Equnlios 8-2

. . . .E:oualion 8-4

. flOCRA1 RfOlSlfR. VOL. 42, NO, lbO.--IHURSDAY,~AUOUSl, 18, 1977 I ' ,:..':: " . . . . . . .

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4 JSTOMER ADDRESS .

JOR NO. '7 ; ) > ! J , CUSTOMER N O . , L O C A T I O N

R U N N O .

P w m # VM I PG

/ / - I ' ' ~ I ~ , DATE O F TEST

VCB , VCD Meter t3ox (f

V B F , VBG , VBH , V B I

A , cp , Y WAK , Y A J , WAL

, WTT 0 Engl 1 '-h l l n i t s

O!\!t.tK I C [ I t Its I A N . e u Pa (COMBUST 1 ON ONLY ) 0 I n c i n e r a t o r

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JSTOMER A IIDK ES S

CUSTOMER NO. , L O C A T I O N --i

J O P N O :

RUN N O . // I f , DATE OF TEST

PBAR I VM I PG VCB , VCD

Meter Hox X

V B F , VBG , VBH , V B I

A , C P , y WAK , Y A J , WAL

, w r ~ , A N , e i UPR (COMBUST 1 ON ONLY )

a C o m b u s t i o n 0 Yetr I!:iits

MI:I' 1:l< i ' CI.OCK GM S T A C K S T A C K Oi< 11: I C E

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