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Volume 79 Issue 7 (April 01, 2007) Editor: Royce W. Murray & Associate Editors

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EDITORIAL

Letters from ChicagoRoyce W. Murrayp 2599

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Audio Introduction to the April 1 CoverRajendrani Mukhopadhyayp 2599

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NEWS

Analytical Currents: Light-emitting nanofibers for lab-on-a-chip applications | Microfluidic system for dynamic microarrays | COINs for Raman-based tissue analysis | Scanning outside the NMR tube | Assessing phosphopeptide isolation methods | Breath analysis without sample pretreatment | Apoptosis probe with a quantifiable readout | Patterned paper for cheap, portable bioassays | Proteotypic peptides in the spotlightpp 2601 - 2605

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Analytical Chemistry (ACS Publications)

People: Sweedler named associate editor | 2007 ACS national award winnerspp 2605 - 2606

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Research Profile: Population studies of drug metabolites in urineLinda Sagep 2607

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Research Profile: Detecting aerosol particles on surfacesRandall C Willisp 2608

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Research Profile: Multiplexed IMS/TOFMS: the ion mobility marathonLaura Tomky Cassidayp 2609

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Analytical Chemistry (ACS Publications)

Research Profile: Measuring isoprene in breathRajendrani Mukhopadhyayp 2610

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Research Profile: Nanofluidic sieves ease separation anxietyThomas Haydenp 2611

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BIO SPHERE

Proteomics of the uncultured endosymbiont of Riftia pachyptilaJennifer Griffithsp 2612

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MATERIAL WORLD

A novel response materializesThomas Haydenp 2613

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FEATURES

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Analytical Chemistry (ACS Publications)

Chemical Analysis of Single Mammalian Cells with MicrofluidicsAlexander K. Price, Christopher T. Culbertsonpp 2614 - 2621

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The Hunt for Counterfeit MedicineRajendrani Mukhopadhyaypp 2622 - 2627

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BIO SPHERE

Directly counting proteins in a cellRajendrani Mukhopadhyayp 2628

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ACCELERATED ARTICLES

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Analytical Chemistry (ACS Publications)

Detection of Urinary Drug Metabolite (Xenometabolome) Signatures in Molecular Epidemiology Studies via Statistical Total Correlation (NMR) SpectroscopyElaine Holmes, Ruey Leng Loo, Olivier Cloarec, Muireann Coen, Huiru Tang, Elaine Maibaum, Stephen Bruce, Queenie Chan, Paul Elliott, Jeremiah Stamler, Ian D. Wilson, John C. Lindon, and Jeremy K. Nicholsonpp 2629 - 2640; (Accelerated Article) DOI: 10.1021/ac062305n

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Can Breath Isoprene Be Measured by Ozone Chemiluminescence?Shin-Ichi Ohira, Jianzhong Li, William A. Lonneman, Purnendu K. Dasgupta, and Kei Todapp 2641 - 2649; (Accelerated Article) DOI: 10.1021/ac062334y

Abstract Full: HTML / PDF (199K) Supporting Info

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Analytical Chemistry (ACS Publications)

Identification of Oxidation Products of Squalene in Solution and in Latent Fingerprints by ESI-MS and LC/APCI-MSKatrina A Mountfort, Hugo Bronstein, Nia Archer, and Sue M Jickellspp 2650 - 2657; (Accelerated Article) DOI: 10.1021/ac0623944

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Raman Chemical Imaging Spectroscopy Reagentless Detection and Identification of Pathogens: Signature Development and EvaluationKathryn S. Kalasinsky, Ted Hadfield, April A. Shea, Victor F. Kalasinsky, Matthew P. Nelson, Jason Neiss, Amy J. Drauch, G. Steven Vanni, and Patrick J. Treadopp 2658 - 2673; (Accelerated Article) DOI: 10.1021/ac0700575

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Analytical Chemistry (ACS Publications)

Gas-Phase Pyridylamination of Saccharides: Development and ApplicationsShin-ichi Nakakita, Wataru Sumiyoshi, Nobumitsu Miyanishi, Shunji Natsuka, Sumihiro Hase, and Jun Hirabayashipp 2674 - 2679; (Accelerated Article) DOI: 10.1021/ac0700878

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PERSPECTIVES

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Direct Immobilization of Protein G Variants with Various Numbers of Cysteine Residues on a Gold SurfaceJeong Min Lee, Hyun Kyu Park, Yongwon Jung, Jin Kyeong Kim, Sun Ok Jung, and Bong Hyun Chungpp 2680 - 2687; (Perspective) DOI: 10.1021/ac0619231

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ARTICLES

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Analytical Chemistry (ACS Publications)

Design and Characterization of a High-Power Laser-Induced Acoustic Desorption Probe Coupled with a Fourier Transform Ion Cyclotron Resonance Mass SpectrometerRyan C. Shea, Steven C. Habicht, Weldon E. Vaughn, and Hilkka I. Kenttämaapp 2688 - 2694; (Article) DOI: 10.1021/ac061597p

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Electrochemically Addressable Functionalization and Parallel Readout of a DNA Biosensor ArrayLifang Niu and Wolfgang Knollpp 2695 - 2702; (Article) DOI: 10.1021/ac061678l

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Analytical Chemistry (ACS Publications)

Quantitative Hydrogen Analysis of Zircaloy-4 Using Low-Pressure Laser Plasma TechniqueKoo Hendrik Kurniawan, Marincan Pardede, Rinda Hedwig, Zener Sukra Lie, Tjung Jie Lie, Davy Putra Kurniawan, Muliadi Ramli, Ken-ichi Fukumoto, Hideaki Niki, Syahrun Nur Abdulmadjid, Nasrullah Idris, Tadashi Maruyama, Kiichiro Kagawa, and May On Tjiapp 2703 - 2707; (Article) DOI: 10.1021/ac061713o

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Hyphenation of Gas Chromatography to Microcoil 1H Nuclear Magnetic Resonance SpectroscopyMarc David Grynbaum, Diana Kreidler, Jens Rehbein, Armin Purea, Paul Schuler, Walter Schaal, Harri Czesla, Andrew Webb, Volker Schurig, and Klaus Albertpp 2708 - 2713; (Article) DOI: 10.1021/ac0617767

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Analytical Chemistry (ACS Publications)

18O Labeling Method for Identification and Quantification of Succinimide in ProteinsGang Xiao, Pavel V. Bondarenko, Jaby Jacob, Grace C. Chu, and Dirk Cheliuspp 2714 - 2721; (Article) DOI: 10.1021/ac0617870

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Interpretation of Reversible Addition-Fragmentation Chain-Transfer Polymerization Mechanism by MALDI-TOF-MSGuangchang Zhou and Issifu I. Harrunapp 2722 - 2727; (Article) DOI: 10.1021/ac061930p

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Distinguishing Individual Vibrational Fingerprints: Single-Molecule Surface-Enhanced Resonance Raman Scattering from One-to-One Binary Mixtures in Langmuir-Blodgett MonolayersPaul J. G. Goulet and Ricardo F. Arocapp 2728 - 2734; (Article) DOI: 10.1021/ac062059f

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Analytical Chemistry (ACS Publications)

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Probing Heterogeneous Electron Transfer at an Unbiased Conductor by Scanning Electrochemical Microscopy in the Feedback ModeHui Xiong, Jidong Guo, and Shigeru Amemiyapp 2735 - 2744; (Article) DOI: 10.1021/ac062089i

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In Vivo Analysis and Spatial Profiling of Phytochemicals in Herbal Tissue by Matrix-Assisted Laser Desorption/Ionization Mass SpectrometryKwan-Ming Ng, Zhitao Liang, Wei Lu, Ho-Wai Tang, Zhongzhen Zhao, Chi-Ming Che, and Yung-Chi Chengpp 2745 - 2755; (Article) DOI: 10.1021/ac062129i

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Analytical Chemistry (ACS Publications)

Using a Multijunction Microfluidic Device To Inject Substrate into an Array of Preformed Plugs without Cross-Contamination: Comparing Theory and ExperimentsLiang Li, James Q. Boedicker, and Rustem F. Ismagilovpp 2756 - 2761; (Article) DOI: 10.1021/ac062179n

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Method for Label-Free Detection of Femtogram Quantities of Biologics in Flowing Liquid SamplesDavid Maraldo, Kishan Rijal, Gossett Campbell, and Raj Mutharasanpp 2762 - 2770; (Article) DOI: 10.1021/ac0621726

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Optimized Threshold Selection for Single-Molecule Two-Color Fluorescence Coincidence SpectroscopyRichard W. Clarke, Angel Orte, and David Klenermanpp 2771 - 2777; (Article) DOI: 10.1021/ac062188w

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Analytical Chemistry (ACS Publications)

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Thin-Layer Chromatography/Desorption Electrospray Ionization Mass Spectrometry: Investigation of Goldenseal AlkaloidsGary J. Van Berkel, Bruce A. Tomkins, and Vilmos Kerteszpp 2778 - 2789; (Article) DOI: 10.1021/ac0622330

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Electrochemical Immunosensor Using p-Aminophenol Redox Cycling by Hydrazine Combined with a Low Background CurrentJagotamoy Das, Kyungmin Jo, Jae Wook Lee, and Haesik Yangpp 2790 - 2796; (Article) DOI: 10.1021/ac062291l

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Analytical Chemistry (ACS Publications)

Identification of a Single Tryptophan Residue as Critical for Binding Activity in a Humanized Monoclonal Antibody against Respiratory Syncytial VirusZiping Wei, Jinhua Feng, Hung-Yu Lin, Sombabu Mullapudi, Eric Bishop, Guillermo I. Tous, Jose Casas-Finet, Fadi Hakki, Robert Strouse, and Mark A. Schenermanpp 2797 - 2805; (Article) DOI: 10.1021/ac062311j

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Spin Coherence Transfer in Chemical Transformations Monitored by Remote Detection NMRM. Sabieh Anwar, Christian Hilty, Chester Chu, Louis-S. Bouchard, Kimberly L. Pierce, and Alexander Pinespp 2806 - 2811; (Article) DOI: 10.1021/ac062327+

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Chemometric Study of Maya Blue from the Voltammetry of Microparticles ApproachAntonio Doménech, María Teresa Doménech-Carbó, and María Luisa Vázquez de Agredos Pascualpp 2812 - 2821; (Article) DOI: 10.1021/ac0623686

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Analytical Chemistry (ACS Publications)

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Charge-Remote Metastable Ion Decomposition of Free Fatty Acids under FAB MS: Evidence for Biradical Ion StructuresHong Ji, Jeff Morré, Valery G. Voinov, Max L. Deinzer, and Douglas F. Barofskypp 2822 - 2826; (Article) DOI: 10.1021/ac0610356

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Bromate Determination in Water after Membrane Complexation and Total Reflection X-ray Fluorescence AnalysisVasilios S. Hatzistavros, Pavlos E. Koulouridakis, Ioanna I. Aretaki, and Nikolaos G. Kallithrakas-Kontospp 2827 - 2832; (Article) DOI: 10.1021/ac061231c

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Analytical Chemistry (ACS Publications)

Use of Liquid Chromatography Coupled to Quadrupole Time-of-Flight Mass Spectrometry To Investigate Pesticide Residues in FruitsSusana Grimalt, Óscar J. Pozo, Juan V. Sancho, and Félix Hernándezpp 2833 - 2843; (Article) DOI: 10.1021/ac061233x

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Bead-Based DNA Diagnostic Assay for Chlamydia Using Nanoparticle-Mediated Surface-Enhanced Resonance Raman Scattering Detection within a Lab-on-a-Chip FormatPaul B. Monaghan, Karen M. McCarney, Alastair Ricketts, Rachael E. Littleford, Frances Docherty, W. Ewen Smith, Duncan Graham, and Jonathan M. Cooperpp 2844 - 2849; (Article) DOI: 10.1021/ac061769i

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Analytical Chemistry (ACS Publications)

Enantiomer Separation of Amino Acids by Complexation with Chiral Reference Compounds and High-Field Asymmetric Waveform Ion Mobility Spectrometry: Preliminary Results and Possible LimitationsAxel Mie, Magnus Jörntén-Karlsson, Bengt-Olof Axelsson, Andrew Ray, and Curt T. Reimannpp 2850 - 2858; (Article) DOI: 10.1021/ac0618627

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Precolumn Isotope Dilution Analysis in nanoHPLC-ICPMS for Absolute Quantification of Sulfur-Containing PeptidesDirk Schaumlöffel, Pierre Giusti, Hugues Preud'Homme, Joanna Szpunar, and Ryszard obi skipp 2859 - 2868; (Article) DOI: 10.1021/ac061864r

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Analytical Chemistry (ACS Publications)

Determining Chemical Activity of (Semi)volatile Compounds by Headspace Solid-Phase MicroextractionCharlotte N. Legind, Ulrich Karlson, Joel G. Burken, Fredrik Reichenberg, and Philipp Mayerpp 2869 - 2876; (Article) DOI: 10.1021/ac061880o

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Surface Studies of Aminoferrocene Derivatives on Gold: Electrochemical Sensors for Chemical Warfare AgentsMohammad A. K. Khan, Yi-Tao Long, Gabriele Schatte, and Heinz-Bernhard Kraatzpp 2877 - 2884; (Article) DOI: 10.1021/ac061981m

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Analysis of Freely Dissolved Alcohol Ethoxylate Homologues in Various Seawater Matrixes Using Solid-Phase MicroextractionSteven T. J. Droge, Theo L. Sinnige, and Joop L. M. Hermenspp 2885 - 2891; (Article) DOI: 10.1021/ac0620260

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Analytical Chemistry (ACS Publications)

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Potentiometric Sensor for Heparin Polyion: Transient Behavior and Response MechanismJan Langmaier, Eva Samcová, and Zden k Samecpp 2892 - 2900; (Article) DOI: 10.1021/ac062060e

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Electron Capture Dissociation of Oligosaccharides Ionized with Alkali, Alkaline Earth, and Transition MetalsJulie T. Adamson and Kristina Håkanssonpp 2901 - 2910; (Article) DOI: 10.1021/ac0621423

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Analytical Chemistry (ACS Publications)

Temperature-Programmed GC Using Silicon Microfabricated Columns with Integrated Heaters and Temperature SensorsShaelah Reidy, Don George, Masoud Agah, and Richard Sackspp 2911 - 2917; (Article) DOI: 10.1021/ac062148s

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Tools in Metabonomics: An Integrated Validation Approach for LC-MS Metabolic Profiling of Mercapturic Acids in Human UrineSilvia Wagner, Karoline Scholz, Maximilian Sieber, Marco Kellert, and Wolfgang Voelkelpp 2918 - 2926; (Article) DOI: 10.1021/ac062153w

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Halo Ion Trap Mass SpectrometerDaniel E. Austin, Miao Wang, Samuel E. Tolley, Jeffrey D. Maas, Aaron R. Hawkins, Alan L. Rockwood, H. Dennis Tolley, Edgar D. Lee, and Milton L. Leepp 2927 - 2932; (Article) DOI: 10.1021/ac062155g

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Analytical Chemistry (ACS Publications)

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Reusable Electrochemical Sensing Platform for Highly Sensitive Detection of Small Molecules Based on Structure-Switching Signaling AptamersZai-Sheng Wu, Meng-Meng Guo, Song-Bai Zhang, Chen-Rui Chen, Jian-Hui Jiang, Guo-Li Shen, and Ru-Qin Yupp 2933 - 2939; (Article) DOI: 10.1021/ac0622936

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Analytical Methodology for TEX86 Paleothermometry by High-Performance Liquid Chromatography/Atmospheric Pressure Chemical Ionization-Mass SpectrometryStefan Schouten, Carme Huguet, Ellen C. Hopmans, Michiel V. M. Kienhuis, and Jaap S. Sinninghe Damstépp 2940 - 2944; (Article) DOI: 10.1021/ac062339v

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Analytical Chemistry (ACS Publications)

Shape-Selective Extraction of PCBs and Dioxins from Fish and Fish Oil Using In-Cell Carbon Fractionation Pressurized Liquid ExtractionP. Haglund, S. Sporring, K. Wiberg, and E. Björklundpp 2945 - 2951; (Article) DOI: 10.1021/ac0624501

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TECHNICAL NOTES

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Scanning Electrochemical Microscopy: Approach Curves for Sphere-Cap Scanning Electrochemical Microscopy TipsGeorgina Lindsey, Stuart Abercrombie, Guy Denuault, Salvatore Daniele, and Eddy De Faveripp 2952 - 2956; (Technical Note) DOI: 10.1021/ac061427c

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Analytical Chemistry (ACS Publications)

Improvements in Complex Mixture Analysis by NMR: DQF-COSY iDOSYJacob M. Newman and Alexej Jerschowpp 2957 - 2960; (Technical Note) DOI: 10.1021/ac061760g

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A Method To Reduce Gradient Delay Time of NanoLCHongji Liu, Jeffrey W. Finch, and John C. Geblerpp 2961 - 2964; (Technical Note) DOI: 10.1021/ac061942a

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Lattice-Boltzmann Simulations of Three-Dimensional Fluid Flow on a Desktop ComputerJeffrey D. Brewsterpp 2965 - 2971; (Technical Note) DOI: 10.1021/ac062178v

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Analytical Chemistry (ACS Publications)

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Method for Determination of Association and Dissociation Rate Constants of Reversible Bimolecular Reactions by Isothermal Titration CalorimetersTsuyoshi Egawa, Antonio Tsuneshige, Makoto Suematsu, and Takashi Yonetanipp 2972 - 2978; (Technical Note) DOI: 10.1021/ac062183z

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Surface Plasmon Resonance Imaging Using a High Numerical Aperture Microscope ObjectiveBo Huang, Fang Yu, and Richard N. Zarepp 2979 - 2983; (Technical Note) DOI: 10.1021/ac062284x

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Analytical Chemistry (ACS Publications)

Noninvasive Acoustic Cell Trapping in a Microfluidic Perfusion System for Online BioassaysMikael Evander, Linda Johansson, Tobias Lilliehorn, Jure Piskur, Magnus Lindvall, Stefan Johansson, Monica Almqvist, Thomas Laurell, and Johan Nilssonpp 2984 - 2991; (Technical Note) DOI: 10.1021/ac061576v

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Measuring Evaporation Rates of Metal Compounds from Solid SamplesChristian Ludwig, Jörg Wochele, and Urs Jörimannpp 2992 - 2996; (Technical Note) DOI: 10.1021/ac0622173

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Enhancing Sensitivity in Headspace-Mass Spectrometric Determination of BTEX in Drinking WaterAntonio Serrano, Mercedes Gallego, and Manuel Silvapp 2997 - 3002; (Technical Note) DOI: 10.1021/ac070044r

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Analytical Chemistry (ACS Publications)

CORRESPONDENCE

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Acoustic Recognition of Counterions in Ion-Exchange ResinsShungo Hirawa, Takashi Masudo, and Tetsuo Okadapp 3003 - 3007; (Small Correspondence) DOI: 10.1021/ac062030b

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Mechanism of Generation of Volatile Hydrides of Trace Elements by Aqueous Tetrahydroborate(III). Mass Spectrometric Studies on Reaction Products and IntermediatesAlessandro D'Ulivo, Zoltán Mester, Juris Meija, and Ralph E. Sturgeonpp 3008 - 3015; (Small Correspondence) DOI: 10.1021/ac061962c

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Analytical Performances of Aptamer-Based Sensing for Thrombin DetectionAlessandra Bini, Maria Minunni, Sara Tombelli, Sonia Centi, and Marco Mascinipp 3016 - 3019; (Small Correspondence) DOI: 10.1021/ac070096g

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CORRECTION

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Determination and Modeling of Peptide pKa by Capillary Zone ElectrophoresisRaphaël Plasson and Hervé Cottetpp 3020 - 3020; (Addition/Correction) DOI: 10.1021/ac062219n

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Temperature Profiles and Heat Dissipation in Capillary ElectrophoresisC.J. Evenhuis, R.M. Guijt, M. Macka, P.J. Marriott, and P.R. Haddadpp 3021 - 3021; (Addition/Correction) DOI: 10.1021/ac070216k

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Citation Management

Analytical Chemistry (ACS Publications)

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Analytical Chemistry (ACS Publications)

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