Sample ID: DICO 1 COHP Date Analyzed: 06/25/03 19:45 Lab ... · SW305OB/601OB METALS BY ICP Client...
Transcript of Sample ID: DICO 1 COHP Date Analyzed: 06/25/03 19:45 Lab ... · SW305OB/601OB METALS BY ICP Client...
SU3050B/6010BHETALS BY ICP
SDMSDocID 164946
Client : ECOLOGY AND ENVIRONMENTProject : oico SIGNAL HILLSDG NO. : 03F116Sample ID: DICO 1 COHPLab Samp IDs F1U-01Lab File ID: 107F02Q013Ext Btch 10: IPF044SCallb. Raf.: I07FQ2Q008
PARAMETERS
AntimonyBariumBeryllium
Cadmium •chromiumCobaltCopperMolybdenumNickelSilverVanadiumZinc
KL: Reporting Limit
Date Collected; 06/20/03Date Racoived: 06/20/03Date Extracted: 06/24/03 15:15Date Analyzed: 06/25/03 19:45Dilution factor: 1Matrix : SOIL% Moisture ; 5.2Instrument IB : ENAXTI07
RESULTS(mg/kg)
RL(mg/lcg)
ND132.33J
-777J18.3S.06Z4.4
ND10.7
ND22.9
163
10.5,05,05,05.11.1111
5.27,11.11
2.111.05
MDL(mg/ko)
2.22.131.124.382.648.729.498.778.58
.662
.462
.304
V
20 'd 200S
SW3050B/6010BMETALS BY TRACE ICP
ClientProjectSOG MO.
: DICO SIGNAL HILL: 03F116
Sample ID: DICO 1 COWLab Samp 10: F116-01Lab File ID: I31F020013Ext Btch ID: IPF044SCalib. Ref.: I31F020008
ENVIRONMENTHtLU
Date Collected;Date Received:Date Extracted;Date Analyzed:Dilution Factor:Matrix :% MoistureInstrument ID :
06/20/0306/20/0306/24/03 15:1506/25/03 20:291SOIL5.2EHAXTI31
PARAMETERS
ArsenicLeadSeleniumThallium
RL: Reporting Limit
RESULTS
(rngAg)RL
(ma/kg)
3.6178,1
NOND
1.051.051.0S1.05
MDL(mg/leg)
.222
.164
.301,32Z
ZT'd I£:6 £002 L
SW305OB/601OBMETALS BY ICP
ClientProjectSDG NO.Sample 10Lab Samp IDLab file IDExt Btch IDCalib. Ref.
ECOLOGY AND ENVIRONMENTDtCO SIGNAL HILL03F116DtCO 2 COMPF116-02I07F02QQ14IPF044SI07F02000S
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted; 06/24/03 15:15Date Analyzed: 06/25/03 19:50Dilution Factor: 1Matrix : SOIL% Moisture : n.einstrument ID : EMAXTI07
PARAMETERS
AntimonyBariimBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSIiverVanadiumZinc
BL: Reporting Limit
RESULTS(nig/kg)
RL(mg/lca)
2.36J150.308J.976J16
6.2733NO
17.8ND22163
11.3.13.13.13.27Z.Z72.275.672.272.272.271.13
WDL(ma/kg)
2.38.141.134.41,696.783.535.837.624.712.497.327
WTd £002 L
SW3050B/6010BMETALS 8V TRACE ICO
Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project ; DICO SI6HAL HILL Data Received: 06/20/03SDG NO. : 03F116 Date Extracted: 06/24/03 15:15Sample ID: 01 CO Z CQMPLab Samp 10: F 116- 02Lab File ID: I51F020014Ext Btch ID: IPF044SCelib. Ref.-. I31F020008
PARAMETERS
ArsenicL«adSeleniumThallium
Date Analysed; 06/25/03 20:35Dilution Factor: 1Matrix : SOIL% Moisture : 11.8Instrument ID : EMAXTI31
RESULTS RL KDL(ma/kg) Cmg/kg)
4.67 1.135V. 1 1.15
ND 1.13.764J 1.13
C ing/ kg)
.239
.107
.323
.346
RL: Reporting Limit
£Td 12:6 £002 L I"f
SU30508/60108METALS BY ICP
client : ECOLOGY AND ENVIRONMENTProject : oico SIGNAL HILL506 NO. ; 03F116Sample ID: DICO 6 COMPLab samp ID: F116-03Lab File ID: I07F020015Ext Btch ID: IPF044SCalib. Ref.: IQ7F020008
Date Collected: 06/20/03Date Received: 04/20/03Date Extracted: 06/24/03 15:15Date Analyzed: 06/25/03 19:54Dilution Factor; 1Matrix : SOIL% Moisture : 4.7Instrument ID : EMAXT107
PARAMETERS
AntimonyBariumBeryl Ii urnCadmiumchromiumcobaltCopperMolybdenumNickelS1iverVanadiumZinc
RL: Reporting Limit
RESULTS(ma/kg)
RL<ntg/kg)
MDL
4.25J594.269J.9J
34.864.345.711618.3ND
36.6276
10.51.051.0S1.052.1a.i2.1
5.2S2.12.12.11.05
2.21.13.124.38.644-7Z5.499-77«.577.659.46.302
SO'd £002 L
SW3050B/60108METALS BY TRACE ICP
Client : ECDLOGT AND ENVIRONMENT <>»<•, couched:Project : oico SIGNAL HILL Date Received: 06/20/03SDC NO. i 03F116 Date Extracted: 06/24/03 15:15Sample ID: DICO 6 COM? Date Analyzed: 06/25/03 20:40Lab Samp 10: F116-03 Dilution Factor: 1Lab File ID: l31fOS0015 Matrix : SOILExt Btch ID: IPF044S % Moisture : 4.rCalib. Ref.: I31F020008 instrument ID : EMAXTI31
RESULTS RL MDLPARAMETERS (rnsAg) Cmfl/kg)
Araenie 7.21 1.05 .221Lead 214 1.05 .183Sslenlum ND 1.05 .299Thallium ND 1.05 .32
RL: Reporting Limit
12:6 200S L
SW3050B/6010BMETALS BY ICP
Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : OICO SIGNAL HILL Date Received: 06/20/03SPG NO. ; 03M16 Date Extracted: 06/24/03 15:15Sample ID: DICQ 7 COOP Date Analyzed: 06/25/03 19:59Lab sun? ID: F116-OA Dilution Factor: 1Lab File ID: I07F020016 Matrix : SOILExt Btch ID: IPF044S % Moisture : 3.5Ctlib. Ref,; I07F02000B Instrument ID : EMAXTI07
RESULTS RL MDLPARAMETERS <mg/kg> (mg/k9> (mj/kg)
Antimony 2.7U 10.4 2.18Barium 298 1.04 .128Dcr/llitm .277J 1.Q4 .122cadmium 1.93 1.04 .375Chronriun 27.5 2.07 .636Cobalt 6.13 2.07 .716Copper 43.1 2.07 .489Molybdenum NO 5.18 .765Nickel 38 2.07 .57Silver ND 2.07 .651Vanadium 41.3 2.07 .4542inc 303 1.04 .298
RL: Reporting Limit
90'd Z£:6 £002 L
SW305QB/6010BMETALS BY TRACE ICP
Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : D1CO SIGNAL HILL Date Received: 06/20/03SDG NO. ; 03F116 Date Extracted: 06/24/03 15:15Sample ID: DICO 7 COMP Date Analyzed; 06/2S/03 20:46Lab Samp ID: F116-Q4 Dilution Factor; 1Lab File ID: 131F020016 Matrix : SOILExt Btch ID; IPFD44S 5C Moisture : 3.5Calib. Ref.: I31F020008 Instrument ID : EMAXT131
PARAMETERS
ArsenicLeadSeleniumThallium
RESULTS(mg/ks)
7.11282NDND
RL MDL(mg/kg) (ma/kg)
1.041.041,0*1.04
.218.18
.2!>S
.316
RL: Report ins L i m i t
ST'd 12:6 £003 L
SU3050B/60108METALS BY ICP
client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLSPG NO. ; 03F116Sample ID; DICO 3 COMPLab Samp ID: F116-05Lab File ID: I07F020017Ext etch ID: IPFD44SCalib. Ref.: I07F02000B
Date collected; 06/20/03Date Received: 06/20/03Date Extracted; 06/24/03 15:15Date Analyzed; 06/25/03 20:04Dilution Factor: 1Matrix : SOIL% Moisture : 2.5Instrument ID : EMAXTI07
PARAMETERSRESULTSCms/tea)
RL(ma/kg)
AntimonyBariumBerylliumCadmiunChromiumCobaltCopperMolybdenumNickelSiIverVanadiumZinc
RL: Reporting Limit
ND171-257J.732J21.74.9125.8ND
13.9ND
24.2113
10.303030305
2.052.055.13Z.052.05£.051.93
MDL(ma/lea)
2.16.127.121.371.63.709.484.757,564.644.449.295
ZO'd 82:6 2002 L
5W3050E/6010B
METALS BY TRACE ICP
Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project ; DICO SIGNAL HILL Date Received: 06/20/03SOG NO. : 03F116 Date Extracted: Qe/24/03 15i1SSample ID: DICO 3 COMP Date Analyzed: 06/25/03 20:51Lab Samp ID: F116-03 Dilution Factor: 1Lab File ID: I31FOJQ017 Matrix : SOILExt Btcr, ID; IPF044S % Moisture : 2.5Calfb. Kef.; I31F02000* Instrument ID : EHAXTJ31
RESULTS RL WDLPARAMETERS (mg/kfl) (mg/ita) (mg/fcgj
Arsenic 4.98 1.03 .£16Lead 12? 1.03 .179Seleniun ND 1.03 .292Thallium ND 1.03 .313
RL: Reporting Limit
9T'd I£:6 2002 L
SW3050B/6010B
METALS BY ICF1
Client ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLSDG NO. :Sample ID:Lab Samp ID:Lab File ID:Ext Btch ID:callb, Ref,:
03F116DICO 4 COMPF116-06107F020018IPF044SI07F020008
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/24/03 15:15Date Analyzed: 06/25/03 20:08Dilution Factor: 1Matrix : SOILX Moisture ; 2.9Instrument ID : EMAXTI07
PARAMETERS
AntimonyBariumBerylliumCadmiumChromiumcobaltCopperMolybdenumNickelSiIvcrVanadiumZinc
RL: Reportins Limit
RESULTStmg/kg)
8.45J2090.312J3.03
767.Z1
13810.4
47ND
41.5577
RL
10.31.03
030306
2.062.065.152.062.062.061.03
MDL(mg/kg)
2.17.128.122.373.632.712.486.76
.566
.647
.451.297
80'd 82:6 2002 L IT
SW3050B/6010BMETALS BY TRACE ICP
Client : ECOLOGY MO ENVIRONMENTProject : DICO SIGNAL HILLSDG NO. ; 03F116Sample ID i DICO 4 COHPLab Samp ID: f 116-06Lab File ID: I31F020018Ext Btch ID; IPF044SCalib. Ref.: 131F02000S
Date Collected: 06/20/D3Bate Reeaivod: 06/20/03Date Extracted: 06/24/03Date Analyzed: 06/25/03Dilution Factor: 1Matrix : SOIL% Moisture : 2.9Instrument ID : EIHAXTI31
15:1520:57
RESULTS RL HDLPARAMETERS (rag/kg) (ma/kg) (mg/kg)
Arsenic 17.8 1.03 .217Load 1000 1.03 .179Selenium ND 1.03 .293Thallium ND 1.03 .314
RL; Reporting Limit
ZT'd 12:6 2002 L IT
SU3050B/6010BMETALS BY ICP
Client ; ECOLOGY AMD ENVIRONMENTProject :
SDG NO. :Sample ID;Lab Samp ID:Lab File ID;Ext Btch ID;
DICO SIGNAL HILL
03F116DICO 5 COUPF116-07107F020019IPF044S
CaUb. Ref.! 107FOZOOQ8
Data Collected: 06/20/03Date R«c«iv*d: 06/20/03
Date Extracted: 06/24/03 15:15Date Analyzed; 06/25/03 20:13Dilution Factor: 1Matrix : SOIL% Moisture : 2.4instrument ID ; EMAXTICT
PARAMETERS
AntimonyBariumBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSi LverVanadiumZinc
RL: Reporting Limit
RESULTS(mg/kg)
RLCmg/kfl)
26.61190.521J2.3154.8B.16
8911.937.5
ND43.5337
10.202020205OS
0512050505
1.02
MDL(mg/kg)
2.15.127.121.371.629.roe.484.756.564.643.449.295
60'd 82:6 2002 L IT
SU3050S/6010BMETALS BY TRACE ICP
Cltsnt ; ECOLB6T A.NP ENVIRONMENTProject : DICO SIGNAL HILLSDG NO. : 03F116Sample ID: DICO 5 COUPLab Samp ID: F116-07Lab File ID: I31FQ20019Ex* Bteh ID: 1PFO&4SCalib. Ref.: I51F02000B
Data Collected: 06/20/03Rccoiv.d:
extracted: 06/24/03 15:15Analyzed; 06/25/03 21:03
1SOIL2.4
DateDateDilution Factor:MatrixX MoistureInstrument ID : EMAXT131
RESULTS RLPARAMETERS
ArsenicLeadSeleniumThallium
RL: Reporting Limit
8.6264NDND
1.021.021.021.02
MDL(mo/kg)
.216
.178
.292
.313
8I'd 12:6 2002 L IT
SWSOSQB/6010BMETALS BY ICP
Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : DICO S16MAL MILL Date Received: 06/20/03SDC NO. : 03F116 Date Extracted: 06/24/03 15:15Sample ID; DICO #6 Date Analyzed: 06/25/03 20:27Lab Samp ID: F116-08 Dilution Factor: 1Lab File ID: IQ7FQ200Z2 Matrix : SOILExt Btch ID: IPF044S X Moiatura : 4.7Co Lib. Ref.: I07F020020 Instrument ID : EMAXT107
RESULTS RL MDLPARAMETERS (mg/kg) (mg/kg) (mg/kg)
Antimony ND 10.5 2.21Barium 39.9 1.05 .13Beryllium NO 1.05 .124Cadmium ND 1.05 .38Chromium 5.18 2.1 .644Cobalt 3.4S 2.1 .725Copper 2Q.1 2.1 .495Molybdenum ND 5.2S .774Nickel 4.82 2.1 .577Silver ND 2.1 .659Vanadium 11.7 2.1 .46Zinc 129 1.05 .302
RL: Reporting Limit
01'd 82:6 2002 L IT
SW3050B/6010SMETALS BY TRACE ICP
client ; ECOLOGY AND ENVIRONMENTProject C DICQ SIGNAL HILLSDC NO. : 03F116
S«mpl» ID: OICO #8
Lab Samp ID: F116-OBLab File ID: 131F020022Ext Btch ID: IPF044SCalib. Ref.: I31F020020
Date Collected: 06/20/03Dat* Received: 06/20/03Date Extracted; 06/24/03 15:15Date Analyzed: 06/25/03 21:19Dilution Factor: 1Matrix : SOIL% Moisture : 6.7Instrument ID
-===tt««tt;;5==mi:s==
PARAMETERS
ArsenicLa«dSeleniumThallium
RL; Reporting Limit
RESULTS(mg/kg)
RL(mg/kg)
2.5411.4NDND
1.051.051.051.05
MDL(mg/kg)
.221
.183
.zw.32
61 'd 12 = 6 £002 L IT
Clientproject :SDG NO. :Sample ID:Lab Samp ID:Lab File ID:Ext Btch ID:Calib. Ref.:
ECOLOGY ANDDICO SISNAL03F116DICO 49 COMPF116-09I07F020023IPF044SI07F020020
SU3050B/6010BMETALS BY ICP
ENVIRONMENTHILL
Date collected:Date Received;Date Extracted:Date Analyzed:Dilution factor:Matrix :% Moisture :Instrument 10 :
06/20/0306/EO/0306/24/03 15:1506/25/03 20:311SOIL4.2EMAXTI07
PARAMETERS
AntimonyBariumBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSiIvervanadiumZinc
RESULTSting/kg)
RL(tns/ka)
ND112-25J.597J13.24.5535
-908JS.61
ND
19.6215
10.40404040909
2.095.222.092.092.091.04
MDL(mg/kg)
2.2.129.123.378.641.721.493.77.574.656.457.301
RL: Reporting Limit
ird 82:6 2002 L IT
SW305OB/601 OB
METALS BY TRACE ICP
==s ======•
Client !Project :SOG NO. :Sample ID;Lab Samp ID:Lab File ID:Ext etch ID:Calib. Ref.:
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO *9 COM?F116-09131F020023IPF044SI31F020020
Pate Collected:Date Received:Date Extracted:Date Analyzed:Dilution Factor!Matrix :% Moisture :Instrument 10 :
06/20/0306/20/0306/24/03 15:1506/25/03 21:251SOIL4.2EMAXTI31
PARAMETERS
ArsenicLeadSeleniumTrtallium
RL; Reporting Limit
RESULTS(mg/kg)
RL(mg/kg)
3.1449.5
NDND
1.041.041.041.04
MDL(mg/kg)
.22.182.297.318
02'd 22:6 2002 L IT
SW305OB/601 OBMETALS BY ICP
Client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLSDG NO. : 03F116Sample ID; DICO #10 COMPLab Samp ID: F116-1DLib File ID: 107F020024Ext Btch ID: IPF044SCaltb. Ref.: I07FOEOOEO
Date Collected; 06/20/03Date Received! 06/20/03Date Extracted: 06/24/03 15:15Date Analyzed: 06/25/03 20:36Dilution Factor; 1Matrix : SOILX Moisture ; 19.0Instrument ID : EMAXTI07
PARAMETERS
AntimonyBariumBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSiIverVanadiumZinc
RL: Reporting Limit
RESULTS(ing/kg)
RL(mg/kg}
NO212
.4B4J1.12J24.96.5037.4
ND14.8
ND30.5
310
12.31.231.231.232.472.472.476.172.472.472.471.23
MDL(mg/lcg)
2.6,153.146.447.758.653.583.911.679.775.541.356
20 'd 62:6 2002 L IT
SU30SOB/6010B
METALS BY TRACE ICP
Client :Project ;SOS NO. ;Sample ID;Lab Samp ID;Lab File ID:Ext Btch ID:Calib. Ref.:«==m»K=__£
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO #10 COMPF116-10I31F020024IPF044S131F02002D
Date Collected:Date Received:Date Extracted:Date Analyzed:Dilution Factor:Matrix :X Hoi a tare :Instrument ID :
06/20/0306/20/0306/24/0306/25/031SOIL19,0EMAXT131
15:1521:30
PARAMETERS
ArsenicLeadSeleniumThallium
RL: Reporting Limit
RESULTS(mg/kg)
RL(mg/kg)
4.9184.9
NDND
1.231.231.251.23
(mg/kg)
.26.215.352.377
12'd 22:6 2002 L IT
SW3050B/6010BMETALS 8Y ICP
=3BB=========»«==========HK===~======3-==="====S===="=
Client ; ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILL
SDG NO. : 03F116SampU ID: DICO *11Lab Samp ID: F116-12Lab File ID: I07F020030Ext Btch ID: IPF044SCalib. Ref.: I07F020020
Date Collected: 06/20/03Data Received: 06/20/03Data Extracted: 06/24/03 15:15Date Analyzed: 06/25/03 21:09Dilution Factor; 1Matrix : SOILX Moisture : 19.2Instrument ID : EMAXTI07
PARAMETERS
RESULTS(mg/kg)
RL(mg/kg)
AntimonyB«r i urnBerylliumcadmiumChromiumCobaltcopperMolybdenumNickelSilverVanadi urnZinc
RL: Reporting Limit
3.17J364.342J2.4922.49.9348.6£.53.123.4
ND23.5235
12.41.241.241.242.48Z.4B2.4B6.192.482.482.481.24
HDL(mg/kg)
2.6.153.146.448.76.653.564.913,681.777.542.356
SO'd 62:6 2002 L IT
SW3050B/6010BMETALS BY TRACE ICP
Client ;project :SDG NO. :Sample ID:Lab Samp ID:Lab File ID:Ext Btch ID1.Colib. Ref.:
PARAMETERS
AraenieLeadSeleniumThallium
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO #11F116-12I31F020030IPF044SI31F020020
Date Collectad:Data Received:Date Extracted:Date Analyzed:Dilution Factor;Matrix :X Moisture :Instrument 10
06/20/0306/20/0306/24/03 15:1506/25/03 22:041SOIL19.2EMAXTI31
RESULTS(ma/kg)
8.58769
NDND
RL(mg/kg)
1.241.241.24
HDL(mg/kg)
.26.215.353.378
Reporting Limit
22'd 22:6 2002 L IT
SW3050B/6010BMETALS BY ICP
Client ECOLOGY AND ENVIRONMENTProject DICO SIGNAL HILLSDG NO. 03F116Sample ID DICO #12lab Samp ID F116-11Lab File ID: I07F020029Ext Btch ID; IPF044S
Date Collected: 06/20/03Dote Rocctvcd: OA/BO/03
Date Extraetodi 06/24/03 15:15Date Analyzed:Dilution Factor:Matrix :% Moisture :
Calib. Ref.: I07F020020 Instrument ID
06/25/03 21:031SOIL6.6EMAXT107
PARAMETERSRESULTS(mg/kg)
RL(mg/kg)
AntimonyBariumB cry I HunCadniumChromiumCobaltCopperMolybdenumNickelSILverVanadiumZinc
RL: Reporting Limit
2.46J262.758J1.0736.514.946.8
ND27.2
ND60.9142
10.71.071.071.072.142.142.145.352.142.142.141.07
MDL
(mg/kg)
2.25.133.126.388.657.74.505.79.589.672.469.508
WTd 62:6 2002 L IT
SU3Q50B/6010BMETALS BY TKACE ICP
Client : ECOLOGY AND ENVIRONMENT Date Collected; 06/20/03Project : DICO SISNAL HILL Date Received: 06/20/03SDC NO. : 03F116 Date Extracted: 06/24/03 15:15Sample ID: DICO #12Lab Samp ID; F116-11Lab File ID: I31F020029Ext 9tch ID: IPFQ44SCalib. Ref.: I31F020020
PARAMETERS
ArsenicLeadSeleniumThallium
Date Analyzed:Dilution Factor:Matrix :X Moisture :Instrument ID :
RESULTS RL(mg/kg) (mg/kg)
11 1.0729.4 1.07
ND 1.07.46J 1.07
06/25/02 21:501SOIL6.6EHAXTI31
MDL(mg/kg)
.225
.186
.305
.327
RL: Reporting Limit
22'd 22:6 2002 L \r\£
SW3050B/6010BMETALS BY ICP
ClientProjectSDG NO.sample ID: DICO #15Lab Samp ID:Lab File ID:Ext Btch 10:Cslib. Ref,!
ECOLOGY AND ENVIRONMENTOICO SIGNAL HILL
03F116
F116-13I07F020Q31IPF044SI07FOZ0020
Date Collected: 06/20/03Date Received: 06/20/0!Date Extracted: 06/24/03 15:15Dato Analyzed: 06/25/03 21:13Dilution Factor: 1Matrix ; SOILX Moisture : 19.2Instrument ID ; EMAXTiO?
PARAMETERS
AntimonyBariumBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSilverVanadium
Zinc
RL: Reporting Limit
RESULTS
(mg/kg)RL
(ma/kg)
ND358.336J2.8923,110.144.71.3J25ND24242
12.41.241.241.242.482.*e2.486.192.482.462.481.24
MDL(mg/kg)
2.6.153.146.448.76.855.584,913.681.777.542.356
90'd 02:6 2002 L IT
SU3050B/6010BMETALS BY TRACE ICP
Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : D1CQ SIGNAL HILL Date Received: 00/20/03SDG NO. : 03F116 Date Extracted: 06/24/03 15:15Sample ID; DICO #15 Date Analyzed: 06/25/03 22:09Lab Samp ID: F116-13 Dilution Factor: 1Lab File ID; 131*020031 Matrix : SOILExt Etch ID: IPFQ44S % Moisture : 19.2Calib. Ref.: I31F020D20 Instrument ID : EMAXTI31
RESULTS RL MDLPARAMETERS (ng/kg) (ma/kg) (mg/kg)
Arsenic 7.64 1,24 ,26Lead 701 1.24 .215Selenium ND 1,24 .353Thallium ND 1.24 .378
RL: Reporting Limit
t?2'd 22:6 2002 L IT
SU3050B/6010BMETALS BY ICP
Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : DICO SIGNAL HILL Date Received: 06/20/03
SDG NO. : 03F116 Date Extracted; 06/24/03 15:15sample ID: DICO #13 Date Analyzed; 06/25/03 21:27Lab Samp ID: F116-14 Dilution Factor: 1Lab File ID; 107F020034 Matrix : SOILExt Btch ID: IPF044S % Moisture ; NACalib. Ref.: 107F020032 Instrument ID ; EHAXT107
RESULTS RL MDLPARAMETERS (mg/kg) (ma/kg) (mg/kg)
Antimony ND 10 2.1Barium 2 1 .124Beryllium ND 1 .118Cadmium ND 1 .362Chromium ND 2 .614Cobalt ND £ .<A\Copper H.7 2 .472Molybdenum a.68j 5 .738Nickel MO 2 .55Silver ND 2 .628Vanadium ND 2 .438Zinc 107 1 .288
RL: Reporting Limit
02:6 2002 L IT
SW30SOB/6010BMETALS BY TRACE ICP
Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : DICO SIGKAL HILL Date Received: 06/20/03SDG NO. : 03F116 Date Extracted: 06/24/03 15:15Sample ID: DICO #13 Date Analyzed; 06/25/03 22:26Lab Samp ID: F116-14 Dilution Factor: 1Lab File ID: I31F020034 Matrix : SOILExt Btch ID: IPF044S % Moisture : NACalib. Ref.: 131F02003E Instrument ID : EMAXTI31
PARAMETERS
ArsenicLeadSeleniumThallium
RESULTS(mg/kg)
ND8.19
NDND
RL HDL(mg/kg) (mg/kg)
11l1
.21.174.285.305
RL: Reporting Limit
S2'd 22:6 2002 L IT
SW3050B/6Q108METALS BY ICP
ID:
ClfcntProjactSDG NO.SampleLab Samp ID:Lab File ID:Ext Btch ID:Calib. Ref.:
ECOLOGY AMD 6UVIftOHMENTDICO SIGNAL HILL03F116DICO #14F116-1SI07F020035IPF044SI07FOZ0032
Date Collected: 06/20/03Date Recaived: 06/20/03Date Extracted: 06/E4/03 15:15Date Analyzed; 06/25/03 21:31Dilution Factor: 1Matrix i SOIL54 Moisture : 29.1Instrument ID : EMAXTI07
PARAMETERS
AntimonyBariumBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSilverVanadiumZinc
RL-. Reporting Limit
RESULTS(mg/ks)
RL
25.68420.516J7,7348432.466870.6367ND2341530
14,11.411.411.412.822.822.827.052.62£.82Z.K1.41
MDL(mg/kg)
2.97.175.166.511.866.975.6661.04.776.886.618.406
80 "d 02:6 2002 Z IT
SU3050B/6010BMETALS BY TRACE ICP
s=s:==seE'ClientProjectSDG NO.SampleLab Samp ID: F116-15Lab File ID: I31F02003SExt Btch ID;Calib. «ef.:
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116OICO m
IPF044SI31F020032
Date Collected; 06/20/03Date Received: 06/20/03Date Extracted: 06/24/03 15:15
06/25/03 22:311SOIL29.1EMAXTI31
Date Analyzed:Dilution Factor:Matrix :% Moisture :Instrument ID :
PARAMETERS
ArsenicLeadselenium
RESULTS(mg/kg)
RL(mg/kg)
30.916401.962-41
1.411.411.411.41
HDL(mg/kg>
.297
.246
.402.43
RL: Reporting Limit
92'd 22:6 2002 L IT
SU3050B/6010BMETALS BY ICP
Client :Project :SDG NO. :sample ID:Lab Samp ID:Lab File ID:Ext Btch ID:celib. Ref.:
ECOLOGY ANDDICO SIGNAL03F116MBLK1S1PF044SBI07P020010IPF044S107F02000B
ENVIRONMENT Date collected:HILL Date Received:
Date Extracted:Date Analyzed:Dilution Factor:Matrix :% Moisture :Instrument ID :
WA06/24/0306/24/0306/25/031SOILNAEMAXTI07
15:1519:29
PARAMETERS
AntimonyBariumBerylliumcadmiumChromiumCobaltCopperMolybdenumNickelSilverVanadiumZinc
RL: Reporting Limit
RESULTSCrng/ka)
RL(mg/kg)
NDNDNDNDNDND
WNDNDNDNDND
1011122252221
MDL(mg/k9>
2.1.124.118.362.614.691.472.738.55.626.438.288
60'd 02:6 2002 L IT
SW3050B/6010BMETALS BY TRACE ICP
Client : ECOLOGY AND ENVIRONMENTProject : Dico SIGNAL HILLsee NO. t 03M16Sample ID: MBLK1SLab Samp ID: IPF044SBLab File IDt I31F020010Ext Btch ID: IPF044SCalib. Ref.; I31F0200D8
Date collected; NADate Received: 06/24/03Date Extracted: 06/84/03 15:15Date Analyzed: 06/25/03 20:12Dilution Factor:Matrix ;% Moisture :Instrument ID
1SOILNAEMAXT131
PARAMETERS
LeadSeleniumThallium
RL: Reporting Limit
RESULTS(mg/ks)
RL(ma/kg)
ND
.203JNDNO
MDL(mg/kg)
.21.174.285.305
22:6 2002 L IT
HETHOD 747JAHERCURY BY OHO VAPOR
CMO
a!
CN
cn
to0
R^~, (i— >
Client : ECOLOGY AND EHVIROWEHrProject : DICO SISMAL HCLLBatch No. : 03F116
SAMPLE ID
teuisLCS1SLC01SDICO #10 COHPASDICO #10 COHPDICO #10 COflPDLDICO #10 COWHSDICO #10 COHPHSODICO 1 COHPDICO 2 COHPDICO € COHPDICO 7 COHPDICO 3 CO*DICO 5 CONPDICO #8DICO ft) CWPDICO #12DICO #11DICO #15DICO #13OICO 4 COHPDICO *14
EHAXSAHPLE ID
HGF030SBHGF030SLHGF030SCF116-1DAF116-10FU6-10TF116-10MF116-10SF116-01F116-OZF116-03F116-04F116-05F116-07F116-D8FU6-09F116-11F116-12Fllfi-13F116-14F116-D6F116-16
RESULTS(ng/ltg>
NO.847.848.574.173
HO1.271.21.542.314.451.836.3231.68
NO-0919J
.25.782.943
.043ZJ2.39.1
DUF
111315a1111111
5LC
noisr
NANANA
19.819.019.019.019.05.2
11.84.73-52.52.44.74.26.619.219.2
RA2.9
29.1
Rl(eg/leg)
.1
.1
.1.123.123.617.123.123.105.113.105.104.103.102.105.104.107.124.124
.1.5151.41
MDL(•gflcgl
.013
.033
.033.0407.0407.204
.0407
.0407
.0348
.0374
.0346
.0342
.0338
.0338
.0346
.0344
.0353
.owe
.040B.033.17
.465
AnalysisDATETIHE
06/26/0311:1606/26/0311:2105/26/0311:2305/26/0311:2505/26/0311:2806/26/0311:3005/26/0311:32(6/26/0311:3405/26/0311:3705/26/0311:3905/26/0311:4605/26/0311:4845/26/0311:5006/26/0311:55(6/26/8311:57(6/26/0311:5906/26/0312:0206/26/0312:05(16/26/0312:0706/26/0312:1406/26/0312:1806/26/0312:23
ExtractionDATETIHE LFJD
06/25/0316:00 H47FD2001006/25/0316:00 H47F020D1106/25/0316:00 H47F020D1205/25/0316:03 N47F02001305/25/0316:00 M7F02001406/25/0316:00 H47F02D01506/25/G316:C» H47F02001606/25/0316: CD H47F02001705/25/0316:00 H47F02001806/25/0316:00 N47F02001905/25/0316:00 H47F020022OS/25/0316: CQ H47F020D2306/25/0316:00 H47F0200E406/25/0316:00 H47F0200Z606/25/0316:00 H47F02002705/25/0316:00 HWOZOOM05/25/0316: CO N47f 02002906/25/0316:10 H47F02903005/25/0316 :KJ H47F02Q03106/25/0316:00 HtTFOZOOM06/25/0316:00 H47F020U3506/25/0316:00 H47F020D37
CAL REF
H47FDZC008N(7F02000BNW0200DBH47F020BOBH47FOZOD08N47F02BDD8N47F020003M47F0200DBm7F02000BH47F020DOSW7F029D2CN47F020020Hi7f02D020W.7F020tJ20H47F020D20N47F024D20H47FOHOOZON47f02M20H47F020920H47F020D32m7F020D32H47F020032
Matrix : SOILInstrument ID : TIM7
me BATCH
«Sf030SHGF030SHSF030SHGF0395HGFQ30SHOF030SHGf030SHCJTJ30SKGF030SMGT030SKSF030SUGF03DSHCF03DSHGF030SHGf03D5HSFC30SHSF030SUGF030S(ttF03!TSHGF030SHCF030SHGFC33S
CollectionDATITIHE
NAHAHA
06/20/0306/20/0306/20/0366/20/0306/20/0306/20/0306/20/0306/20/0306/20/0306/20/0306/20/0305/20/0306/20/0306/20/0306/20/0306/20/0305/20/0306/20/0306/20/03
ReceivedOATETIHE
06/25/8306/25/0305/25/0306/20/0306/20/0306/20/0306/20/0306/20/0305/20/0306/20/0306/20/0306/20/0306/20/0306/20/0306/20/0366/20/0306/20/03OS/20/0306/20/0305/20/0305/20/03C6/20/03
RL: Reporting Limit
*'*«* ^ '"-"''-
METHOD M8015TOTAL PETROLEUM HYDROCARBONS BT EXTRACTION
Client : ECOLOGT AND ENVIRONMENT Date Collected: 06/20/03»roject : DICO SIGNAL HILL Date Received: 06/20/03Batch No. : 03F116 Date Extracted: 06/23/03 17:50sample ID: DICO 1 COHP Date Analysed-. 06/26/03 07:32tab Samp ID: F116-01 Dilution Factor; 1Lab File 10: TF24066A Meui* -. SOILExt Btch ID: DSF020S % Moisture : 5.2Calib. ftef.: TF2406&A Instrument ID : GCT050
RESULTS RL MDL'ARAHETERS (ma/kg) (mg/lcg) (mg/xs)
)I£SEI. ND 11 2.1^lOTOR OIL 380 53 2.1
SURROGATE PARAMETERS X RECOVERY QC LIMIT
SROMOBENZENE 114 4S-165MEXACOSANE 133 27-176
RL ! Reporting LimitSUSftl : BromobenzeneSURR2 : Hexacosane
£002 8
METHOD H8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
=i;.~< : ECOLOGY AMD EWVlROHMgNT"reject : DICO SIGNAL HILL3atch No. : 03F116Sample ID: DICO 2 CQMP.ab Samp 10: F116-OZtab File ID: TF24067Aext Btch IDs 03F020SCBlib. Ref.; TF24064A
Bfife Collected:Date Rsceivea;Data Extracted:Date Analyzed:Dilution Factor:Matru ;% Moisture ;Instrument ID :
06/20/0306/20/0306/23/03 17:5006/26/03 06 ;H1SOIL11.8GCT050
PARAMETERS
OIESEL
RESULTS(ma/kg)
RL
OIL
SURROGATE PARAMETERS
3ROMOBENZEKEHEXACQSANE
RL : Reporting LimitSUR.R1 ; BromooenzencSURR2 ; Hexacoaenc
NO440
RECOVERY
115143
1157
QC LIMIT
45-16527-176
MDL
(mg/k9)
2.3
"d £2:8 £002 8
METHOD M8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
: ECOLOGY AND ENVIRONMENT: DICO SIGNAL HILL: 03F116
ID; DICO 3 COMP10: F116-OSTID: TF24089AID: DSF020S
Calib. Ref.: TF24080A
ClientProjectBatch No.S atrip Le16D SampLab FilcExt etch
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 17:50Date Analyzed: 06/26/03 23:32Dilution Factor: SOMatrix ; sou% Moisture : 2.5Instrument ID : GCT050
PARAMETERS
OIESELMOTOR OIL
SURROGATE PARAMETERS
SROMOBENZcNEHEXACOSANE
RESULTS(mg/kg)
RLCms/kg)
ND16000
55 RE COVERT
DODO
510£600
oc LIMIT
45-16527-176
MDL(rag/kg)
100100
•aSUUR1SURR2
30
Reporting L i m i t
BromobenieneHexacosane
Diluted out
'd 172:8 200S 8
METHOD MB015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
:l lent
aatcn No.Sample ID:Lab Samp ID;Lab F i l e ID:
ECOLOGY AND
DICO SIGNAL HILL03F116DICO t COMPF116-06TTF24090A
Date Collected: 06/20/03Date Received: 06/20/03
Ext BtCti ID: DSF020SCalib. Ref.: TF24080A
Date Extracted;Date Analyzed:Dilution Factor:Matrix !S Moisture !Instrument ID i
06/23/03 17:5006/27/03 00; 13100SOIL2.9QCT050
PARAMETERS
DIESELMOTOR OIL
SURROGATE PARAMETERS
3ROMOBEN2EME
HEXACOSANE
RL : Reporting LimitSURR1 s BromobenzeneSURR2 : Hexacosane
30 ; Diluted out
RESULTS(mg/kg)
RL(mg/kg)
MDL
ND28000
RECOVERY
DODO
10005100
QC LIMIT
45-16527-176
210210
0£'d £002 8
M6THOO M6015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
ClientProjectBatch NoSampletab samp-ab File£xt Btch
:= ; : = 3 V » » ~ -: ECOLOGY AND ENVIRONMENT: Oico SIGNAL HILL: 03F116
ID: DICO 5 COHPID: F116-07TID: TP24091AID: DSF020S
:aUb. Ref,: TF24060A
PARAMETERS
DIESELMOTOR OIL
SURROGATE PARAMETERS
aROMOBENZENE^EKACOSANE
Rl ; Reporting LimitSURR1 : BromobenzeneSURR2 : Hexacosane
==:;Sa=»Date collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 17:50Date Analyzed: 06/27/03 00:55Dilution Factor: 100Matrix ; SOIL% Moisture : 2.4Instrument ID : GCT050
RESULTS(ms/Vg)
RL(ms/k9)
MDL
ND34000
% RECOVERY
DODO
10005100
QC LIMIT
&5-16SE7-176
200200
00 : Diluted out
T£'d £002 8
(10015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
Client :Project :
Batch No. :Sample ID:•-ab Samp ID: F116-03T-ab file 10: TF24068A:xt Btch ID: OSFOZOSCallb, Ref,: TF2«80A
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO 6 COMP
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted; 06/Z3/W 17:50Date Analyzed; 06/26/03 22:50Dilution Factor: 3Matrix ; SOILX Moisture : 4.7Instrument ID : GCTOSO
PARAMETERS
DIESELMOTOR OIL
SURROGATE PARAMETERS
3ROMOBENZENEHEXACOSANE
RESULTS(ing/Kg)
NP
3100 '
% RECOVERY
126337*
RL
(ing/Kg)MDL
160
OC LIMIT
45-16527-176
6.36.3
U '. Reporting Limit3URR1 : BromobenieneSUSRZ : Hexacosana
" : out of QC limits due to matrix interference
£00^ 8
METHOD M8015TOTAL PETROLEUM HYDROCARBONS BT tMRACTiON
Client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLBatch No. i 03M14Sample ID: DICO 7 COMPLab Samp ID: F116-04 .uab Fi l e ID: TF24069ASxt Btch ID: DSF020SCalib. Ref.! TF24064A
D8te Collected; 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 17:50Date Analyzed: 06/26/03 09:37Dilution Factor: 1Matrix ; SOILX Moisture : 3.5Instrument ID : CCT050
PARAMETERS
DIESEL
MOTOR OIL
SURROGATE PARAMETERS
3ROMOBENZENE
-itXACOSANE
<L : Reporting LimitSURR1 : BromobenzeneSURR2 : Htxacosane
RESULTS(mg/kg)
RL(mg/kg)
ND1500
% RECOVERY
119173
1052
QC LIMIT
45-16527-176
MDLcms/kg)
2.12.1
82'd £002 8
METHOD M8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : DICO SIGNAL HILL Date Received; 06/20/03Batch No- : 03F116 Date Extracted: 06/23/03 17:50Sample ID; DICO #8 0»te Analysed: 06/27/03 01:36v.ab Samp ID: F116-08T Dilution Fsetor: 100.ab File ID: TF24092A Matrix : SOIL••xt Btch ID: OSF020S H Moisture ; 4.7:shb. Ref.s TF24080A Instrument 10 : GCT050
PARAMETERS
DIESELMOTOR OIL
RESULTS RL MCu(mg/kg) (mg/kg) (mg/l<9)
ND 1000 21031DOO S200 210
SURROGATE PARAMETERS
3RON08ENZENE4EXACOSAH6
^L : Reporting LimitSURR1 : Bromo&enieneSURRE ; Mexacossne
30 t Diluted out
RECOVERY
DODO
CC LIMIT
45-16527-176
£2:8 £002 8
METHOD M8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
ClientProjectBatch No.SampleLab SampLab FileExt Btch
10:ID;ID;
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO <P? COMPF116-09TTF2409SA
ID: DSF020SCalib. Ref.: TF24093A
Date coUectea; 06/80/osDate Received: 06/20/03Date Extracted: 06/23/03 17:50Date Analyzed: 06/27/03 03:41Dilution Factor: 5Matrix : SOILX Moisture : 4.2Instrument ID : GCTOSO
RESULTS(mg/ksl
ND7300
V, RECOVERY
PARAMETERS
31S5ELVICTOR OIL
SURROGATE PARAMETERS
SROMOBENZENEHEXACOSANE
3L : Reporting LimitSURR1 ; 8 rouwbenzoneSURR2 : Hexacoeane
: Out of OC limits due to matrix interference
RL(mo/kg)
52260
QC LIMIT
45-16527-176
MDL(mg/Kg)
1010
££'d 52:8 £002 8
METHOD M6015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
Client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLSatcn NO. : 03F116Sample ID: 51 CO 1*10 COMPLab Samp ID: F116-10Lab File ID: TF24075AExt Btch ID: OSF020SCalib. Ref.: TF24064A
Date Collected; 06/20/03Date Received; 06/20/03Date Extracted: 06/23/03 17:50Date Analyzed: 06/26/03 13:48Dilution Factor: 1Matrix : SOILX Moisture : 1°-0Instrument ID : GCT050
'ARAHETERS
3TESELMOTOR OIL
SURROGATE PARAMETERS
8ROMQ6ENZENEHEXACOSANE
RESULTS(ms/kg>
RL(mg/kg)
NDZ100
RECOVERY
244*
126Z
QC LIMIT
45-16527-176
MDL(mg/ks)
2,52.S
RL : Reporting LimitSURR1 : BrotnobenieneSURR2 : Hexacosane
• : Out Ot QC limits due to matrix interference
I7£'d £002 8
METHOD M8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/05 17:50Date Analyzed: 06/29/03 11:06Dilution Factor: 10Matrix ; SOILX Moisture : 19.2Instrument ID : GCT050
clientProjectBatch No.SampleLab SampLab FileExt BtchCalib. Re
; ECOLOGY AND ENVIRONMENT; DICO SIGNAL HILL: 03F116
ID: DICO *nID: F116-12TID: TFZ7062AID: DSF020Sif.: TF27060A
PARAMETERS
DIESELMOTOR OIL
SURROGATE PARAMETERS
BROMOBENZENE
HEXACOSANE
RL : Reporting LimitSURR1 : BromobenreneSURR2 : Hexacosane
RESULTS(mg/kg)
RL(mg/kg)
450015000
X RECOVERY
00DO
120620
QC LIMIT
45-16527-176
HDL(ng/kg)
2525
00 : Diluted out
9£'d S2:8 £002 8
METHOD H8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
-s===ca*===s:
Client :'roject :•Jatch No. :Sample 10:_ab Samp ID:uab File 10:Fxt BtCh 10:Calib. Ref.;
PARAMETERS
3USELMOTOR OIL
ECOLOGY ANDDICO SIGNAL03F116DICO #12H16-11TF26082AD5F020STF24080A
ENVIRONMENT Date Collected:HILL Date Received:
Date Extracted;Date Analyzed:Di lution Factor;Matrix ;X Moisture :instrument ID :
RESULTS RL(mg/kg) (mg/kg)
ND 112ZQ 54
06/20/0306/20/0306/23/03 17:5006/26/03 18:411SOU6.6CCTD50
MOL(mg/kg)
2,12.1
SURROGATE PARAMETERS
6R0140BEN&ENEHEXACQSAHE
% RECOVERY
115115
OC LIMIT
45-16527-176
RLSURR1SURR2
Reporting LimitBromobenzeneHexacosane
S2:8 £002 8
METHOD M8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
clientProjectCatch No.Simple IDLab Samp IDLab File IDEXt Btch IDCalib. Ref.
PARAMETERS
DIESELMOTOR OIL
; ECOLOGY AND: DICO SIGNAL'. 03F116: DICO #13: F116-14T: TF24096A: DSFOE1S: Tf£40«3A
ENVIRONMENT Date Collected: 06/20/03HILL Date Received: 06/20/03
Date Extracted: 06/24/03 16:30Date Analyzed: 06/27/03 04:23Dilution Factor: 1000Matrix : SOIL% Moisture : NAInstrument ID : GCT050
RESULTS RL MDL(ma/kg) (mg/kg) (mgAg)
24000 10000 20006BOOOO 50000 2000
SURROGATE PARAMETERS
BROM08EHZENE
UCXACOSANE
RL ; Reporting LimitSURR1 : BromobenzeneSURR2 ; Hexacosane
RECOVERY
00DO
QC LIMIT
27-176
00 ; 0i Luted out
8£'d S2:8 £002 8
METHOD M8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
clientProjectBatch No.SampleLab ScirpLftb FileExt BtchCalib. Ref.:
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO #14F116-15TTC0200SAOSF020STS02003A
Date collected; oo/go/03pate Received: 06/20/03Date Extracted: 06/23/03 17:30Date Analyzed: 07/02/03 17:09Dilution Factor: 1000Matrix ; SOILX Moisture : 29.1Instrument ID : GCTD50
RESULTSPARAMETERS
RL
(ma/kg)
MOTOR OIL
SURROGATE PARAMETERS
BROM08ENZENEHEXACOSANE
RL : Reporting LimitSURR1 : BroroobcnicneSURR2 : Hexacosane
DO : Diluted out
ND58000
RECOVERY
DODO
1400071000
OC LIMIT
4S-16527-176
HDL(ms/ks)
28002800
6£'d S2:8 £002 8
.rtaBuswda fcw_
METHOD H801STOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
clUnt : ECOLOGY AMD ENVIRONMENTProject : DICO S1QNAL HILLBatch No. : 03F116Sample ID: DICO 015Lab Samp ID: F116-13Tlefa File ID: TF2706/AEXt BtCh ID: OSF020SCalib, ftef.; TF27060A
Date Collectedi 06/20/03Date Received; 06/20/03Date Extracted: 06/23/03Date Analyzed: 06/29/03Dilution Factor: 10Matrix : SOIL% Moisture : 19.2Instrument ID : GCT05Q
17:5014:35
PARAMETERS
DIESELMOTOR OIL
SURROGATE PARAMETERS
8ROHOBENZENEHEXACOSANE
RL • Reporting LimitSURR1 : SromobenzeneSURR2 : HORocoaane
RESULTS(mg/ks)
RL
780019000
X RECOVERY
DO00
120620
QC LIMIT
45-16527-176
MOL(me/kg)
2525
DO : Diluted out
92:8 £002 8
METHOD HS015
TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
Date Collected: NADate Received; 06/23/03»at« Extracted! 06/23/03 17:50Date Analyzed: 06/23/03 18:16Dilution Factor: 1Matrix : SOILX Moisture : NAInstrument ID : GCT050
Client :5roject :Satch No. :Sample ID;
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116MBLK1S
Cab Samp ID; DSF020SBlab File ID: TF23004AExt Bteh ID: DSF020SCalib. Re* ! TF23002A
PARAMETERSRESULTS
(mg/k8)RL
(mg/kg)
1DTOR OIL
SURROGATE PARAMETERS
3ROMOBEN2ENEHEXACOSANE
RL : Reporting LimitSURR1 : QromobenxcneSURR2 : HexecosaneParameter H-C RangeOiesel C10-C24
Oil C16-C34
NOND
RECOVERY
10787
1050
QC LIMIT
45-16527-176
MDL(mg/kg)
22
017 'd 92:8 £002 8
EHAX QUALITY CONTROL DATALCS/LCD ANALYSIS
CLIENT: ECOLOGY AND ENVIRONMENTPROJECT: DICO SIGNAL HILL3ATCH NO.: 03F116METHOD: METHOD M8015
MATRIX:DILUTION FACTORSAMPLE ID:uAB SAMP ID;-AS fILE ID:JATE EXTRACTED:JATE ANALYZED:'SEP. BATCH;CALIB. REF:
ACCESSION:
SOIL1H8LK1SDSF020SBTF23004A
DSF020SLTF23005A
06/23/0317:50 06/23/0317:50
1
DSF020SCTFZ3006A06/23/03 \f; 50
06/23/0316:16 06/23/0318:56 06/23/0319]39DSF020STF23002A
DSF020S DSFQ20STFZ3002A
MOISTURE; NA
BATE COLLECTED: MA
DATE RECEIVED: 06/23/03
PARAMETER
Diesel
BLNK RSLT(mg/kg)
SPIKE AMT<mg/kg)
BS(itK
RSLT)Aa>
BS% REC
SPIKE AMT(mg/ks)
BSD RSLT(mg/ki>
BSDX REC
RPD QCC
LIMIT MAX RPD
ND 500 464 93 500 478 96 3 50-160 50
SURROGATE PARAMETER
Bromobenzenenexacoaane
SPIKE AMT(mg/kg j
10025
BS RSLT(mg/kgj
12023
BS% REC
12092
SPIKE AMT(mg/kg>
10025
BSD RSLT
12122.9
BSD'4 REC
12192
QC LIMI'
50-15030-160
92:8 £002 8
METHOD MB015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION
Client :Project ;Batch NO. ;Sample ID;Lab Samp ID:..ab File ID:£xt fitch ID:Calib. Ref.:
PARAMETERS
DIESELMOTOR OIL
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL
03F116
MBLK2S
DSF021SB
TF24060ADSF021STF24054A
Date Collected:Dote Rec«wod:Date Extracted:Date Analyzed:Dilution Factor;Matrix :X Moisture •Instrument ID :
RESULTS RL(mg/kg) (mg/kg)
ND 10ND 50
NA06/24/0306/24/0306/26/031SOILMAGCT050
(
16:3003:23
MDlms/ks )
22
SURROGATE PARAMETERS
JKQM08ENZENEItXACOSANE
*L : Reporting LimitSURR1 : Bromobenzenc5URR2 : Hexacosaneparameter H-C RangeOiesel C10-C24Motor Oil C18-C34
X RECOVERY
119101
8C LIMIT
45-16527-176
217'd 92:8 £002 8
EHAX QUALITY CONTROL DATALCS/LCD ANALYSIS
CLIENT: ECOLOGY AND ENVIRONMENTPROJECT: DICO SIGNAL HILLBATCH NO.: 03F116METHOD: METHOD
MATRIX:DILUTION FACTOR:SAMPLE ID:LAB SAMP ID:LAB FILE ID:DATE EXTRACTED:DATE ANALYZED:POEP. BATCH:CALIB. REF:
ACCESSION:
PARAMETER
Oicael
SOIL1HBIK2SDSF021SBTF2406QA06/E4/0316:3006/26/0303:23DSF021STF24054A
1
DSF021SLTF24061A06/24/0316:3006/26/0304:04DSF021STF24054A
1
DSF021SCTF24062A06/24/03\4:3006/26/0304:46DSF021STF24054A
BLNK RSLT SPIKE AMTCmaAg)
BS RSLT
% MOISTURE: NA
DATE COLLECTED: NADATE RECEIVED: 06/24/03
BSREC
SPIKE AMT(me/kg)
BSD RSLT(mg/kg:
BSDX REC
RPD QC LIMIT( X )
MAX RPO< X )
500 504 101 500 472 94 50-140 SO
SURROGATE PARAMETER
8romobenzeneHexacosane
SPIKE AMT BS RSLT(mg/kg) (n>s/k9>
10025
11326.8
BS SPIKE AMT BSD RSLT% REC (mg/kg) <tng/kg>
113107
10025
11225. B
BSD% REC
112103
QC LIMIT( X )
50-15030-160
£17'd 92:8 £002 8 \r\£
EMAX QUALITY CONTROL DATAHS/MSD ANALYSIS
CLIENT:PROJECT:BATCH NO.:METHOD:
MATRIX;DILUTION FACTOR;SAMPLE ID:LAB SAMP ID:LAB FILE ID!DATE EXTRACTED:DATE ANALYZED;PREP. BATCH:CALIB. REP:
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116METHOD H8015
SOIL101 CO #10 COMPF116-10TF24075A06/23/0317:5006/26/0313:48DSF020STF24064A
1
F116-10MTFZ4077A06/23/0317:5006/26/0315:11DSF020STC26064A
1
F116-10STF24078A06/23/0317:5006/26/0315:53BSF020STF24064A
X MOISTURE: 19.0
DATE COLLECTED; 06/20/03BATE RECEIVED! 06/20/03
ACCESSION;
PARAMETER
Diesel
SMPL RSLT(mg/kg)
SPUE AMT(ma/kg)
MS RSLT(mg/kg) %
MSREC
SPIKE AMT(rag/kg)
MSD RSLTCms/ kg)
USDX REC
RPD( X )
QC LIMITX >
MAX RPO( X )
617 365 617 364 59 45-154 50
SURROGATE PARAMETER
BromobenseneHexacoaanc
SPIKE AMT(mg/kg)
12330.9
MS RSLT(mg/kg)
15770.7
MS SPIKE AMT MSD RSLT% REC (mg/kg) (mg/kg)
127229*
12330.9
15566.6
MSD% REC
125222*
OC LIMIT( X )
45-16527-176
Out of QC limits due to matrix interference
1717'd 92:8 £002 8
• A. . 3 -JO-*.*»*
SH3550B/S082
PCBs
ECOLOGY AND ENVIRONMENTOICO SIGNAL HILL
03F116
DICO 1 COMPF116-01WF 23071A
ClUntProjectBatch No.Sample IDLab Samp IDLab File IDExt Oteh ID: 60F019S
CaUb. Ref.: WF23QS4A
Date Collected:Date Received:Date Extracted:Date Analyzed:Dilution Factor:Matrix :X Moisture ;Instrument ID :
06/20/0306/20/0306/23/0306/24/031SOIL
5.2QCTQ16
18:3020:32
PARAMETERS
PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEDECACHLOROBIPHENYL
RESULTS(ug/kg)
ND|(ND)ND|(ND)NDJ(ND)NDJ(ND)NO|(NO)ND|(ND>
620£|(630E)
% RECOVERY
102|(82)93|(81)
RL(U9/kg)
53535353535355
MDl(U9/k
18181818181818
9)
18181818181818
QC LIMIT
54-14536-176
RL: Reporting LimitLeft of | is related to first column( > included the raported column* Out sida of QC Limit
Right of | related to second column
20'd 61:8 £002 8
SW3550B/8D82PCBs
Client ; ECOLOGY AND ENVIRONMENT
Project : DICO SIGNAL HILLBatch NO. : 03F116Sample ID; DICO 1 COHPDLLab Samp ID: H16-01TLab File IDi WF23100AEXt fitch ID: 60F019SCalfb. Rcf.i UF23099A
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 11:01Dilution Factor; 5Matrix : SOIL% Moisture : 5.2Instrument ID : GCT016
PARAMETERS
PCB-1016
PCB-12Z1
PCS-1232PCB-1242PCB-124B
PCB-1254PCS-1260
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENE
DECACHLOROB1PHENYL
RESULTS(ug/kg>
NDNDNDNONDND
(ND)(ND)(ND)(ND)(ND)(ND)
?20|(690)
% RECOVERY
85 | (77)
RL; Report ins LimitLeft of | is related to first column( ) included the reported colunn• Out aide of QC Limit
RL(ug/kg)
260
sw260260260260260
QC LIMIT
54-14336-176
MDL(us/kg)
686688
888888
88188881888818888188
Right of I related to second column
£0'd 61:8 £002 8
frl*4t- \v^
SU3550B/8082PCBs
Client : ECOLOGY AND ENVIRONMENT
Project : DICO SIGNAL HILLBatch No, : 03F116Sample ID: ptco 2 COUPLab Samp ID: F116-02Lab File ID: WF23072AExt Btch ID: 60F019SCalib. Ref.: UF230S4A
Date Collected; 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03Date Ana Iyled: 06/24/03Dilution Factor: 5Matrix : SOILX Moisture : 11.8Instrument ID : QCT016
18:3020:57
PARAMETERS
PCS-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEOECACHLOROBIPHENYL
RESULTS(US/kg)
NDNDNDND
(ND)(ND)(ND)(ND)
ND|(ND)ND|(ND>
1000|(7?0)
% RECOVERY
99|(84)97|(83>
RL: Reporting LimitLeft of | is related to first column( } included the reported column* out aide of QC limit
RLCug/kg)
280260280280280280280
MDL(ug/kg)
95 9595J959595
9595
95|959S|9S9SJ9S
QC LIHIT
54-14336-176
Right of 1 related to second column
170'd 02:8 £002 8
SW3550B/80S2PCBS
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 12:16Dilution Factor: 15Matrix : SOILX Notsrure ; 2.5Instrument ID ; ecrou
(KentProI actBatch NosampleLab samp IDLab File IDExt Btch ID
ID;
ECOLOGY AND ENVIRONMENT
DICQ SIGNAL HILL03F116DICO 3 COMPF116-05WF23103A60F019S
Calib. Ref.; WF23099A
PARAMETERS
PCB-1016PCB-1221PCB-1232PCB-1242PCS•1248PC8-1Z54PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-H-XYLENEDCCACHLOROBIPHENYL
RESULTS(us/kg)
NDNDNDNDNDND
(ND)(ND)(WO)(ND)(ND>(ND)
2500[C2200)
% RECOVERY
85|C67)711(47)
RL MOL(ug/kg) (ug/ks)
770770770770770770770
260(260260 j 260Z60|260Z6Q|260260)260260)260260)260
QC LIMIT
54-14336-176
RL: Reporting LimitLtft of | is related to first column ; Right of( ) included the reported column« Out side of QC Limit
[ related to second column
02:8 £0028
SU3S50S/S082PCBs
Client :Project :Batch No. :Sample ID:Lab Samp ID:Lsb File ID;Ext Btch 10:Calib. Ref.:
PARAMETERS
PCB-1016PCB-1221PCB-1232
PCS -1246PCB-1254PCB-1260
ECOLOGY ANDDICO SIGNAL03F116OICO 4 COUPF116-06HF23104A60F019SWFZ3099A
ENVIRONMENTHILL
RESULTS(ug/kg)
NDNDNDNDNDND
3700
(ND)<KD)(NO)(ND)(ND)(ND)(3400)
Date Collected:Date Received:Date Extracted:Date Analyzed:Oi lution Factor:Matrix :% Moisture :Instrument ID i
RL(ug/kg)
770770770770770770770
06/20/0306/20/0506/23/03 18:06/25/03 12:15SOIL2.96CT016
HDL(US/kg)
2601260260 | 260260 | 260260 | 260260 | 260Z60J260260 | 260
3042
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEDECACNLOROB1PHENYL
% RECOVERY
65|(53>146)(93)
RL: Reporting LimitLeft of | is related to first column ; Right of( ) included the reported column* Out side of QC Limit
QC LIMIT
S4-14S36-176
related to second column
80 'd 02:8 £002 8
CUent 5
Project
Batch No.SampleLab SartpLab FileExt 8tch
;*
ID:ID:ID:ID:
Calib. Ref.:
SW3550B/B082PCBs
ECOLOGY AND ENVIRONMENT
DICO SIGNAL HILL
03F116
OICO 5 COHP
F1 16-07UF23105A60FQ19SWF23099A
Date Collected:Date Received:Date Extracted:Date Analyzed:Dilution Factor:Matrix :% Hoisture :Instrument ID ;
06/20/0306/20/0306/ZS/0306/25/03250SOIL2.4CCT016
18:3013:07
RESULTSPARAMETERS
PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1E54PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENE
OeCACHLOROBlPHENYL
ND|(NP)NDJ(ND)
ND|(ND)ND|(ND)
NDJ(ND)
75000 | (62000)
% RECOVERY
DO | DODO j DO
RL; Reporting LimitLaft of | is related to first column ; Right of( ) included the reported column* Out side of QC Limft
RL HPL(us/kg) (ug/kg)
13000 4300|430013000 &IODJ430013000 43DO|430013000 4300|430015000 43001630013000 4300|430013000 43CO|4300
QC LIMIT
54-14336-176
related to second column
60'd 02:8 £002 8
SW355C9/8062PCBS
clientProjectBatch NoSampleLab samp ID;Lab Pile IDiExt Btch
: ECOLOGY AMD ENVIRONMENT; DICO SIGNAL HILL: 03F116
ID: DICO 6 COUPF11o-03UF23101A
ID; 6DF019SCalib. Ref.: UF2309QA
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 11:26Dilution Factor: 100Matrix : SOILX Moisture : 4,7Instrument ID : GCT016
PARAMETERS
PCB-1016PCS-1221PCB-1232PCB-1242PCS-1246PCS-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-H-XYLENEDECACHLOROBIPNENYL
RESULTS(ug/kg)
NDNDND
(ND)(ND)(NO)
ND|(ND)NDND
(ND)(ND)
35000|(27000)
% RECOVERY
115|(80)B9|(92>
RL: Reporting LimitLeft of | is related to first column( ) Included the reported column* Out side of QC Limit
RL(ug/ks)
MDL(ug/kg)
5200 1800|18005200 1800j18005200 1600j18005200 1800j18005200 1800j16005200 1BOO|18005200 1800j1800
QC LIMIT
54-14336-176
Right of | related to second column
SO'd 02:8 £002 8
A *. l_ „,.,
SW3550B/60B2PCBs
client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLBatch No. s Q3F116Sample ID; DICO 7 COHPLab San? ID: M16-04Lab File ID: UF23102AExt Bteh ID: 60F019SCalib. Ref.: UF23099A
PARAMETERS
Oate Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 11:51Dilution Factor: 100Matrix : SOIL2 Moisture : 3.5Instrument ID : CCT016
PCB-1016PCB-1221PCB-1232PCS-1242PCB-1248PCB-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-H-XYLENEDECACHLOROBIPHEKYL
RESULTS(ug/kg)
ND (ND)ND (ND)ND (ND)ND (ND?ND (ND)ND (NO)
33000 (26000)
RL(ug/Kg)
S200520052005200520052005200
MDL<U8/kg>
1700 | 17001700 17001700 17001700 17001700 17001700 17001700 1700
% RECOVERY
99|(87)100|(85)
RL: ReportfngLeft of | ia related to first column ; Right of( } included the reported colum* Out side of QC Limit
QC LIMIT
54-14336-176
related to second column
90'd 02:8 £0028
SU35SOB/8082PCBS
Client : ECOLOGY ANDProject : DICO SIGNALBatch No. : 03F116Sample ID: DICO «8Lab Samp ID: F116-OSLab File ID: WFZ3083AExt Btch ID: 60F019SCalib. Ref.: WF23078A
PARAMETERS
PCB-1016PCB-1221PCB-1232PCB-1242
PCB-1248PCB-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEDECACHLOROB1PHENYL
ENVIRONMENTHILL
RESULTS(us/kg)
NDl(ND)NDl(ND)NO (ND)ND (ND)ND (ND)ND (ND)
1704|(180J)
% RECOVERY
77 |(68)70|(58)
Date coUcctod;Date Received;Date Extracted:Date Analyzed:Di lution Factor:Matrix :% Moisture ;Instrument ID ;
RL(ug/kg)
260260260260260260260
ac LIMIT
54-14336-176
s»=£3Z=::=£
06/20/0306/20/0306/23/03 1806/25/03 015SOIL4.7GCT016
MDL(ug/kg)
88 1 8888 1 8888 8866 8088 88B8 &888 86
=3-
-.30:34
RL: Reporting LimitLeft of | is related to first column( ) included the reported* Out side of QC Limit
Right of I related to second column
OT'd 12:8 £002 8 inr;
>*«.
SUJ550B/8082PCBe
ClientProjectBatch No,Sample ID:Lab Samp IDLib Ftle ID: UF23004AExt Btch ID: 60F019SCalib. Ref.: WF23076A
ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO W) COWF116-09
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 02:00Dilution Factor: 5Matrix : SOIL% Moisture : 4.2Instrument ID ; CCT016
RESULTSPARAMETERS
PCB-1016PCB-1221PCB-1232PCB-1242PCS-1248PCB-1254PCB-1260
SURROGATE PARAMETERS
T6TRACHLORO-M-XYIENEDECACHLOROB1PHENYL
NDNDHDNDND
(ND)(MO)(ND)(ND)(ND)
NO ItNO)1900EJO600E)
% RECOVERY
102|(80)781(64)
RL: Reporting LimitLeft of 1 1s related to first column ,- Rijht of( ) included the reported eel urn* Out side of QC Limit
RL(us/kg)
260Z60Z60260260260260
MDL(us/kg)
87er8787876787
87678747678787
OC LIMIT
54-14336-176
related to second column
12:8 £002 8
SW3550B/8082PCBs
ClientProjectBatch No.Sample IDLab Samp 10Lab File 20Ext Btch IDCalib. Ref.s==3SB==:«==
: ECOLOGY AND ENVIRONMENT; DICO SIGNAL HILL: 03F116: DICO #9 COMPDL: F116-09T: UF23106A: 60F019S: WF23099A=53KC=»=artE=v=s*CC=»==tflC=w=~R
Datv C<jll«etedtDate Received:Date Extracted:Date Analyzed:Dilution Factor:Matrix :% Moisture :Instrument ID :
06/20/0306/20/0306/23/0306/25/0315SOIL4.2CCT016
18:3013:32
PARAMETERS
PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEOECACHLOR08IPHEMYL
RESULTS(ug/kg)
NDNDNDNDNDND
(ND)(ND)(ND)(NO)(ND)(ND)
2300|(1900)
X RECOVERY
1051(75)831 (71)
RL; Reporting LimitLeft of ] is related to first column ,- Right of( ) included the reported col urn* Out side of ac Limit
RL(ug/kg)
7807BO780780780780780
MDL(ug/Kg)
260(260260 260260260260260
260260260260
260 1 260
QC LIMIT
54-14336-176
related to second column
'd 12:8 £002 8
SU3550B/60B2PCBs
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/05 18:30Date Analyzed: 06/25/03 02:25Dilution Factor: 5Matrix : SOIL55 Moisture : 19.0Instrument ID : QCT016
CUentProjectBatch No.SampleLab Samp ID:Lab File ID:
: ECOLOGY AND ENVIRONMENT; DICO SIGNAL HILL: 03F116
ID: DtCO #10 COMPF116-10WFZ3085A
Ext Bteh ID: 60F019SCalib. Ref.: UF230raA
PARAMETERS
PCB-1016PC8-1221PC6-1232PCB-U42PCB-1248PCB-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEDECACHLOROB1PHEHYL
RL; Reporting LimitLeft of | is related to first colum( ) included the reported column* Out side of QC Limit
RESULTS(us/kg)
ND|(ND)NDJ(ND)NDJ(ND)NDJ(ND)NDl(ND)NO UNO
9400E|(12000E)
X RECOVERY
104 |(89)81) (69)
nr ; Right of |
RL(ug/kg)
210310310310310310310
QC LIMIT
5VH336-176
MDL(ug/kg)
100)100100)100100J100100|100100)100100)100100)100
related to second colutm
21 'd 12:8 £002 8
SW3550B/8082PCB6
Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project ; DICO SIGNAL HILLBatch No. : 03F116Sanpl» 10: DICO 910 COMPDLLab Sanf ID: F116-10TLab File ID; WF2310TAExt Btch ID; 60F019SCaUb. Ref.: WF23099A
PARAMETERS
PCB-1016PCB-1221PCB-1232PCS -1242PCB-12&8PCB-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-H-XYLENEDECACHLOROBIPHENYL
RESULTS(ug/k3)
ND (ND)ND (ND)NDJ(ND)ND (ND)ND (ND)ND (ND)
25000 (20000)
X RECOVERY
103 | (84)99 (75)
Dote Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 13:57Dilution Factor; 100Matrix : SOILX Moisture i 19.0instrument ID : GCT016
RL MDL(ug/Xg) (ug/kg)
6200 2100(21006200 2 100 j 21 006200 2100 21006200 2100 21006200 2100 21006200 2100 21006200 2100 2100
QC LIMIT
54-14336-176
RL: Reporting LimitLeft of | is related to first column( ) included the reported column* Out side of ac Limit
Right of I related to second column
12:8 £0028 jnf
SW3550B/SOB2PCBs
Client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLBatch No. : 03F116Sample ID: DICO #11Lab Samp 10: F116-12Lab File ID: UF23112AExt Btch ID: 60F019SCalib. Ref.: UF25099A
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 16:03Dilution Factor: 500Matrix : SOILX Moisture : 19.2Instrument ID : &CT016
PARAMETERS
PCB-1016PCS-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEDECACHLORQBIPHENYL
RESULTS(ug/kg)
NDNDNOND
NDND
200000
(ND)(ND)(NO)(ND)(ND)(ND)(160000)
RECOVERY
DO [00DO | DO
RL: Reporting LimitLeft of | is related to first column( ) Included the reported column* Out side of QC Limit
ftL H&L(ug/kg) <ufl/k9>
31000 10000j1000031000 10000j1000031000 10000)1000031000 1000011000031000 10000)1000031000 10000)1000031000 10000(10000
QC LIMIT
54-14336-176
Right of | related to second column
9I'd 22:8 £002 8
5W53508/8082PCBS
...:*.* *• ._
CUent : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLBatch No. s 03F116
ID; DICO #12Lob Samp ID: F116-11Lab File ID: UF23108AExt Btch ID; 60F019SCaUb. Ref.: WF23099A
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted; 06/23/03 18:30Date Analyzed: 06/25/03 14:22Dilution Factor:Matrix% MoistureInstrument ID
20SOU6.6GCT016
PARAMETERS
PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PC8-1E60
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEOECACHLOROBIPHENYL
RESULTS(uo/kg)
NDNDNDNDNDND
(ND)(NO)(ND)(ND)(NO)(ND)(3500)
X RECOVERY
103|<85)I0a|(82)
RL: Reporting LimitLeft of | is related to first column< ) included the reported column* Out side of OD Limit
RL(ug/kg)
MDL
1100110011001100110011001100
OC LIMIT
54-145
36-176
560|360360360360360
360360360360
360 j 360360 | 360
Right of | related to second column
ST'd T2:8 2002 8 \r\£
SW3550B/8082PCBs
Client :Project ;Batch No. :Sample ID:Lab Samp ID:Lab File ID: UF23113AExt Btch ID! 60F0195Calib. Ref.: WF23099A
ECOLOGY AND ENVIRONMENTPICO SIGNAL HILL03F116DICO #15F116-13
Date Collected: 06/20/03Pat* ft««eived: 06/20/03
Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 16:29Dilution Factor: 500Matrix : SOILX Moieturc : 19.2Instrument ID : GCT016
PARAMETERS
PCB-1016PCB-1221PCS -1232
PCS -1248PCB-12S4PCB-126Q
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEDECACHLOROB1PHENYL
RESULTSCuo/kg)
NDNONDND
(ND)(ND)(ND)(ND)
NO|(ND)NDJ(NO)
190000|(150000)
% RECOVERY
DQ|00DO | DO
RL: Reporting limitLeft of j is related to first column( ) included the reported column* Out side of QC Limit
RL MDL(US/kg) (ug/kg)
31000 10000(1000031000 10000|1000031000 10000)1000031000 10000|1000031000 1000011000031000 1000031000 10000
QC LIMIT
1000010000
54-14336-176
Right of I related to second column
22:8 £0028
SW355OB/8082PCB5
Client : ECOLOGY ANDProject ; DICO SIGNALBatch No. : 03F116Sanple ID: DICO #13Lab Samp ID: F116-14Lab File ID: WF23095AExt Btch ID: 60F019SCalib. Ref.: UF2307BA
PARAMETERS
PCB-TOlePCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEDECACHLOROBIPHENYL
RL: Reporting LimitLeft of ) is related to f( ) included the reported* Out side of QC Limit
ENVIRONMENTHILL
RESULTS(ug/kg)
ND|(ND)NDJ(ND)ND (ND)ND (ND)ND (HD)ND (NO)ND|(ND)
% RECOVERY
117|(104)104 j (66)
Irst column ; Right ofcolum
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Plate Analyzed: 06/25/03 04:37Dilution Factor: 30Matrix : SLUDGE% Moisture : NAInstrument ID : GCT016
RL MDL(ug/kg) < us/kg)
1500 500 5001500 500 5001500 500 5001500 500 | 5001500 500)5001500 500(5001500 508 | 500
QC LIMIT
54-14336-176
| related to second column
81 'd 22:8 £002 8
PCB3
Client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILL
Batch No. : 03F116Sample ID: DICO #14Lab Samp ID; F116-15Lab File ID: WF23111AExt Btch ID: 60F019SCaltb. Ref.: WF23Q99A
Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 15:38Dilution Factor: 250Matrix : SOIL% Moisture ; 29.1Instrument ID : acTOio
RESULTSPARAMETERS (us/kg)
PCB-1016 ND|(ND)PCB-1221 ND|(NP)PCB-1232 NPJ(ND)PCB-12C2 ND|(ND)PCS-1248 360001(31000)
PCB-1254 NDJ(ND)
PCB-1260 6700JJC6600J)
SURROGATE PARAMETERS % RECOVERY
TETRACHLORO-M-XYLENE 00|DODECACHLOROBIPHENYL DOJDO
RLc Reporting LimitLoft of | is related to first column( ) included the reported eolunn* out side of QC Limit
Calib. Ref. file for PCB 1248: UG03007A
RL MDL(ug/kg) (us/kg)
16000 5500|590016000 59001590018000 5900J50QO18000 5900)590018000 5000)590018000 5900|590018000 5900)5900
QC LIMIT
54-14336-176
Right of | related to second column
61 'd 22:8 £002 8
(.-*.
SU355 OB/6082
cuent ECOLOGY ANDProject DICO SIGNALBatch NO. 03F116Sample ID MBLK1SLob Samp ID 60F019SBLab File ID UF23066AExt Btch ID 60F019SCalib. Ref. WF23054A
PCBS
ENVIRONMENTHILL
RESULTSPARAMETERS
PCB-1016KB-1Z21PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEDECACHLQROBIPHENYL
(ug/kg)
ND|(ND)NDJ(ND)NDNDNDNDND
?ND)(NO)(ND)(ND)(ND)
X RECOVERY
71|C60)95 | (75)
Date Collected: NADate Received: 06/23/03Date Extracted: 06/23/03 IBDate Analyzed: 06/24/03 18Dilution Factor: 1Matrix : SOILX Moisture : NAInstrument ID : CCT016
:30:26
RL MDL(U9/k9) (ug/ks)
SO 17|1750 17|1750 17 1750 17 1750 17 1750 17 1750 17 17
OC LIMIT
54-14336-176
RL: Reporting LimitLeft of [ is related to first column< ) included the reported column* Out aida of OC Limit
Right of | related to second col urn
02 'd 22:8 £002 8 \r\£
SW3550B/808ZPCBs
clientProjectBatch No.Sample IDLab Samp 10Lab File IDExt Btch IDCalib. Ref.
f-ARAnETCKS
PCB-1016PCB-1221PCB-1232PCB-1ZA2
PCB-1248PCS -1254PCB-1260
; ECOLOGY AND-. DICO SIGNAL; 03F116: MBLK2S: 60F020SB: WFZ3092A: 60F019S: MF2907SA
ENVIRONMENTHILL
RESULTS(ug/kg)
ND|(ND)ND|(ND)ND|(ND)NO (ND)ND|(ND)ND|(ND)NDJ(NO)
Date Collected:Bate Received;
Date Extracted:Date Analyzed;Dilution Factor;Matrix :% Moisture :Instrument ID :
RL(us/ks)
150015001500150015001SOD1500
NA06/23/0306/23/03 18:3006/25/03 05:2130SOILNAGCT016
MDL<uj/kB)
500|SOC500 | 500500(500500 500SOO 500500(500500 500
SURROGATE PARAMETERS
TETRACHLORO-M-XYLENEDECACHLOROBIPHENYL
X RECOVERY
117|(97)721(69)
QC LIMIT
54-14336-176
Rl: Reporting LimitLeft of | is related to ftrst colum( ) included the reported column* Out side of QC Limit
Right of I related to ascend column
£2:8 £002 8 \r\£
EHOC OUAUTY CflHTKOI. DATALCS/LCD ANALYSIS
CLIENT:
PROJECT:
CM BATCH NO.:
^ METHOD:
MATRIX:
£0 DILUTION FACTOR:
" SAMPLE ID:
LAB SWP ID:
LAB FILE ID:
0 DATE EXTRACTED:CN DATE ANM.YZEO:
Oo PREP- BATCH:CALIB. REF:
3•~> ACCESSION:
PARAMETER
PCS- 1016
PCB-1260
ECOIOGY AMD
DICO SIGNAL
03F116
EWmcHHEfiT
HILL
SW3550B/B082
SOUtMBLK1S
60F019SB
WF23066AOi/23/0318:
60F019S
WFZ3054A
X N3ISTUKE: KA1 1
60F019SL 60F019SC
MF25067A WF2306BA30 06/23/0318:30 06/23/0318:30 DATE COLLECTED: NA
26 06/24/0318:51 06/24/0319:16 DATE RECEIVED: 06/Z3/0360F019S 60r019s
VF23054A WFZJ054A
BLNK NSLT SPUE AW BS RSL1 BS SPIKE ANT
<«3/kg> (u9/k9) (m/M) % R£C (ug/kg)
NDJ(ND) 167 149|<117) 89|(70) 167
«D|(NO) 167 20S((t56) 123|(94) 167
BSD RSLT BSD RPD flC LIMIT MAX «fD
<ug/kg) XREC ( X ) ( % ) ( 5 ! )
150|t12D) 90iC7Z) 1|<3) 30-150 50
206 j< 156) 124|<94) 0|(0) 40-160 50
SPIKE AMI BS RsirSURROGATE PARAMETER
BS SPIKE ANT% REC
BSD RSI! BSD OC L I M I T
% REC ( % )
Oecach (orobiphenyl
13.3 11|(9.15) S$|<69) 13.3 11.2|<9.Z9) M|(70) 60-15013.3 13.6J(10.5) 10H|(78) 13.3 13.8|(10.6> 103(<79) 40-160
EHAX QUALITY COMTJtOL DATA
LCS/LCB ANALYSIS
CLIENT: ECOLOGY AMD EHVI ROHHEW
PROJECT: DICO SIGNAL HILL
^ BATCH »0.: 03F116
^ METHOD: SVB550B/80B2
KATRIX: SOIL
£0 DILUTION FACTOR: 30
" SAMPLE 10: NBLK25
LUB SAMP ID: 60FOZOSB
LAB FILE ID: WF23092A0 DATE EXTRACTED: 06/23/0318:50R DATE ANALYZED: 06/25/0305:21
CO PREP. BATCH: 60F019SCALIB. REF: UF23078A
^ ACCESSION:
PARAMETER
PCB-1016
PCB-1H60
30 30
60FC20St 60FOZOSC
06/Z5/031B:30 0£/2J/031506/25/03C$:4& 06/25/03066QF019S 60F019SUF3307flA HFZ307BA
BLNK R5LT SPIKE AH T(us/ks) m»/k9>
ND|(HD) 167NO j (NO) 167
SPIKE ANT BS RS1T
SURROGATE PARAMETER
letrach toro-ro- xyleneDecachlorobi phenyl
(Mg/kg) <ua/kg)
13.3 15.7|(1Z.7)13.3 9.62JC9.25)
X MOISTURE: HA
:30 DATE COLLECTED: MA:11 DATE REtZIYED: 05/23/03
B5 RSLT BS SPIKE ANT BSD RSLT BSD RPD(ug/kg) X REC 0«/kg> (na/kg) X REC C X )
1W|<149) 116|C«9) 167 176|(144> 10&|C8*5 9|(3)IB3|(154) 110|(92) 167 1W((156) 113JC9O 3|(13
KS SPIKE ANT BSO SSLT BSD QC LIMIT% K.L <ua/kg) (us/kg) % REC ( X )
11B|<96> 13.3 15.1) (12.8) 113) (94) 60-130
72|<69) 13.3 10.7}<a.OZ) 80] (60) 40-160
OC LIMIT HAX RPD
( X ) < * >
30- 150 50
40-160 50
EHAX QUALITY CONTROL DATA
Ht/NSD ANALYSIS
CLIENT: ECOLOGY AND ENVIRONMENTPROJECT: HI CO SIGNAL HI LI
^ BATCH NO.: 03FI16<N NETKQO: SU3550B/80B2
MATRIX: SOILK> DILUTION FACTOR: 5^ SAMPLE ID: DICO #10 CONP00 LAB SAMP ID: F1 16-10
LAB FILE 10: UP 23085 A0 DATE EXTRACTED: 06/23/0318:30£3 DATE ANALYZED: 06/25/0302:25oo PREP- BATCH: 60F019S
CALI8. REF: UFZ3078A
>~> ACCESSION:
PARAMETER
PCB-1016
PCB-12AO
5
F116-10NW23CS6A05/23/03 1fl:3fl05/25/0502:5060F019SMF23CrfiA
SMPL RSLT<ug/ks>
8100[(12000)
% MOISTURE: 19.05
F116-10SWFZ30B7A
06/23/0318:30 DATE COtLEcrEO: 06/20/0306/ZS/OJ03:15 OAfE RECEIVED: OA/20/C360F019SWF23078A
SPIKE AMI MS RSL1 HS SPIKE AMT(U3/kg> do/kg) X REC (us/kg)
1030 1370 1 (3020) 327* (C2W) 10301030 W80JC1420D) ia3*(C214») 1030
SPIKE AMI MS RSLT MS SPIKE AMI USD RSLT
SURROGATE PARAMETER (
Tetrachloro-m-xyleneDeoachl orobi ph wiyl
;u3/ks) <iug/kg) X REC < ug/kg) (ug/kg)
82.3 80.6|(66.3) 98|(81) B2.3 83.7|<69.6)82.3 46.1 1(63.5) 80|(7/) 82.3 70.5(<65.6)
USD RSLT KSt> RPO OC LIMIT MAX RPD
(us/kg) % REC < % ) c % ) < X )
33BOl<2690) 32B*|(Z61*) OJ(12) 2T-165 509810JO3500) 16tj(146> 2|<5) 36-176 50
HSO QC LIH1TX REC ( X )
102|<85) 54-14386|(80) 36-176
* : Outside of QC limits