Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar,...

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Recent Progress and Perspectives in Solid State Photomultipliers Yu. Musienko University of Notre Dame (Notre Dame) And Institute for Nuclear Research RAS (Moscow) Yu. Musienko, Detector Seminar, CERN, 30.06.2017 1

Transcript of Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar,...

Page 1: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Recent Progress and Perspectives in Solid State Photomultipliers

Yu. Musienko

University of Notre Dame (Notre Dame)

And

Institute for Nuclear Research RAS (Moscow)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 1

Page 2: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Outline

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 2

• Introduction and brief history of SiPM/SSPM invention

• SiPM principles of operation and properties• SiPM parameters• Recent progress in SiPMs• SiPM radiation damage• Exotic SSPM structures• Applications of SiPMs in HEP• Summary and SiPM/SSPM perspectives

Page 3: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Introduction

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 3

Significant progress in understanding of physics of SiPM operation was achieved during last 3-5 years.As a result a breakthrough in SiPM understanding/development. SiPMswith reduced correlated noise (X-talk, afterpulsing), improved PDE, reduceddark noise were developed and produced.Here I will review current (June 2017) status of SiPM/SSPM development.A special attention is paid to new developments in the field of radiation-hardSiPMs. Possible perspectives of SiPM/SSPM development will be alsodiscussed.I would like to thank all the people whose slides (shown at PhotoDet-2012,NDIP-2014, PhotoDet-2015, VCI-2016, Elba-2015, 2nd SiPM Advancedworkshop-Geneva-2014, CPAD-2016 and RICH-2016, IEEE-NS/MIC-2016,INSTR-2017 conferences etc.) are used in this presentation.

Page 4: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Avalanche multiplication in Si

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 4

Applying high electric field in uniform p-njunction may cause an avalanchemultiplication of electrons and holes createdby absorbed light

Dependence of ionization coefficients of electrons and holes in Si on the electric

field at room temperature

Silicon is a good material for APD construction: high sensitivity in visible and UV range, significant difference between ionization coefficients for electrons and holes – smaller positive feedback and

smaller multiplication noise

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Silicon avalanche photodiodes operated below breakdown (CMS APDs)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 5

0.1

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ain

20

Advantages: high QE, gain up to 1000, area up to 2 cm2

Disadvantages: ENF(multiplication noise) and temperature coefficient increases with increasing gain

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APDs operated in Geiger mode

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 6

High gain operate APDs over breakdown Geiger mode APDs

Single pixel Geiger mode APDs developed a long time ago

( see for example: R.Haitz et al, J.Appl.Phys. (1963-1965))

Planar APD structure Passive quenching circuit

In G-M operation mode an APD bias voltage is set to few volts overbreakdown voltage. In high electric field free carrier undergoesavalanche multiplication produces very rapid current increase (fewtens of ps). Rise of the current drop of the voltage due to resistor inAPD biasing circuit current is reduced to a such level (“latchcurrent”) that statistical fluctuations may quench the avalanche.“Latch” current is ~20 mA. This sets a limit on the quenching resistorvalue (>100 kOhm for a few volts overvoltage). Finally voltage on APDis recovered to an initial value with time constant equal CAPD*R APD is ready for another free carrier …

Page 7: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Single cell Geiger mode APDs

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 7

Photon counting module (Perkin Elmer/Excelitas)

Dark count rate – 500 Hz (25 Hz -selected)

• Very high PDE (up to 70 %) of APDs operated in Geiger modebut:

• Single pixel devices are not capable of operating in multi-photon mode• Sensitive area is limited by dark count and dead time (few mm2 Geiger mode APD can operate only at low temperature, needs “active quenching”)

Solution: Multi-cell Geiger mode APD (SiPM)

Page 8: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Silicon photomultipliers (SiPMs)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 8

Simplified SiPM structure and principles of operation (briefly)

Al electrode

Rquench

n+/p junctions

p-Si substrate

SiO2+Si3N4p-epi layer

300µ

2-4µ

(EDIT-2011, CERN)

Vbias> VBD

GM-APD

Rq

substrate

Al electrode

Vout

Q Q

Qtot = 2Q

• SiPM is an array of small cells (SPADs) connected in parallel on a common substrate and operated in Geiger mode

• Each cell has its own quenching resistor (from 100kΩ to several MΩ)

• Common bias is applied to all cells (~10-20% over breakdown voltage)

• Cells fire independently

• The output signal is a sum of signals produced by individual cells

For small light pulses (Ng<<Npixels) SiPM works as an analog photon detector

Page 9: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

The very first SSPM design (MRS APD, 1989)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 9

The very first metall-resitor-smiconductor APD (MRS APD) were proposed in 1989 by A. Gasanov, V.

Golovin, Z. Sadygov, N. Yusipov (Russian patent #1702831, from 10/11/1989 ). APDs up to 5x5 mm2

were produced by MELZ factory (Moscow).

Few % photon detection efficiency for red light was measured with 0.5x0.5 mm2 APD. Good pixel-to-pixel uniformity. Small geometrical efficiency. Very low QE for green and blue light.

LED pulse spectrum(A. Akindinov et al., NIM387 (1997) 231)

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Key elements of typical SiPM cell

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 10

(slide taken from presentation of G. Collazuol at PhotoDst-2012)

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SiPM equivalent circuit (small signal model) and pulse shape

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 11

(slide taken from presentation of G. Collazuol at PhotoDst-2012)

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Pulse shape vs. T

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 12

Fast and slow components behave differently with temperature:• Fast - doesn’t depend• Slow – time constant increases with T due to Rq increaseFor HPK SiPM with polysilicon quenching resistor the slow time constant increases ~8 times when temperature drops from 300 K to 77 K

(H. Otono et. al, PD-07)

Page 13: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Photon detection efficiency & Geometric factor

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 13

Cells should be electrically independent “dead” space between SiPM cells reduces its PDE. It is especially important for the small cell pitch SiPMs

(Yu.Musienko, CTA SiPM Workshop, Geneva, 2014)

PDE (l, U,T) = QE(l)*Gf*Pb(l,V,T)

Page 14: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Optical cross-talk between cells (direct cross-talk)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 14

Cellls are not optically independent! Light is produced inside firing cell due to hot-carrier luminescence process:105 carriers produces ~3 photons with anwavelength less than 1 mm.Optical cross-talk causes adjacent pixels to be fired increases gain fluctuations increases noiseand excess noise factor !

(R. Mirzoyan, NDIP08, Aix-les-Bains)

N.Otte, SNIC-2006

Avalanche luminescence

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Optical crosstalk and Single electron spectra

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 15

When V-Vb>>1 V typical single pixel signal resolution is better than 10% (FWHM)). However an optical cross-talk results in more than one pixel fired by single photoelectron. This results in deterioration of SiPMs SES and …

SES MEPhI/PULSAR APD, U=57.5V, T=-28 C

1

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1000

10000

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ADC ch.

Co

un

ts

(Y. Musienko, NDIP-05, Beaune)

Amplitude spectra of SiPM measured with very low light intensity (<<1 photon/pulse) and electronics threshold ~0.5 pe.

Page 16: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

SiPMs: Optical cross-talk - II

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 16

Other effects of cell luminescence:- External cross-talk

(light can be reflected from optical interface to another SiPM cell)

- Delayed pulses from light absorbed in non-depleted region (look like after-pulses)

Page 17: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

After-pulses

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 17

Carriers trapped during the avalanche discharging and then released trigger a new

avalanche during a period of several 100 ns after the breakdown after-pulses

-0.35

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Vo

lta

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)

Events with after-pulse measured on a single cell.

y = 0.0067x2 - 0.4218x + 6.639

y = 0.0068x2 - 0.4259x + 6.705

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Tint = 100ns

After-pulse probability vs bias

(C. Piemonte: June 13th, 2007, Perugia)

Solution: “cleaner” technology, smaller gain, blocking layer to stop delayed pulses from Si bulk after-pulsing reduced to < 2%

Page 18: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

X-talk reduction

Yu. Musienko, INSTR-17, Novosibirsk 18

(KETEK – Photodet-2015 (Troitsk))

(HPK: Koei Yamamoto, 2nd SiPMAdvanced Workshop, March 2014)

Metal filledtrench

< 1 µm

The way to reduce X-talk: trench filled with non-transparent material (tungsten)

Extremely low X-talk value of 0.05% was measured for the Hamamatsu HD-1015CN SiPM

(Yu.Musienko , INSTR-2017)

Page 19: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Afterpulsing and delayed X-talk reduction

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 19

25µm 30µm 35µm 40µm

(G. Zappalà, VCI-2016)

(HPK: Koei Yamamoto, 2nd SiPMAdvanced Workshop, March 2014)

After-pulsing and delayed X-talk were reduced from 30% to <1.5% at high overvoltage (FBK NUV SiPM)

Page 20: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

SiPMs: PDE increase

Yu. Musienko, Detector Seminar, CERN, 30.06.201720

Small X-talk and after-pulsing allow SiPM operation at high over-voltages. As a result maximum PDE increased from 20 ÷ 30% to 50 ÷ 60 % (SiPMs with 43÷50 mm cell pitch).

VBD: 25.5 V

(KETEK – Photodet-2015 (Troitsk))

(SensL MicroFJ-SMA-3035-E46, CERN APD Lab)

(T.Kirn, VCI-2016)

SiPM array for LHCb Scintillating Fibre Tracker

Page 21: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

PDE increase: SiPMs with very thin trenches

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 21

NUV-HD

SiPM

Trench< 2 µm

High-field region

Poly stripresistor

Metal

High-field region

Cell 2Cell 1

~ 4.5 µm

NUV-

SiPM

Cell 2 Cell 3Cell 1

NUV High-Density (HD) technology:

Lower dead border region → Higher Fill Factor

Trenches between cells → Lower Cross-Talk

(G. Zappalà(FBK), VCI-2016)

Cherenkov light spectrum in Earth’s atmosphere

NUV-HD 30µm Cell Pitch PDE, 10V OV

30 mm cell pitch SiPMs: GF=77% PDE>50 % !!

Page 22: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Dark noise reduction

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 22

25µm 30µm 35µm 40µm(G. Zappalà(FBK), VCI-2016)

(HPK: Koei Yamamoto, 2nd SiPMAdvanced Workshop, March 2014)

J.Merphy(SensL) 2nd SiPMAdvanced Workshop, March 2014)

Gettering? Dark Count ~30kHz/mm2 was measured atdVB=2÷3 V at roomtemperature with SiPMs fromseveral producers. Now itbecomes a standard!!

Page 23: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Dark noise at low temperature

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 23

Standard field

Low-field

> 7 orders of magnitude !

A 10x10 cm2 SiPM array would have a total DCR < 100 Hz!

Dark noise can be significantly reduced by lowering SiPM temperature. However, tunnelling is a limiting factor for SiPM dark noise reduction at low T.

A low-electric field NUV-HD version has been developed by FBK to reduce the tunnelling component of the DCR.

(G. Zappalà(FBK), VCI-2016)

Tunnelling component

Page 24: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Further GF increase: Metal Film Quenching Resistor

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 24

(HPK: Koei Yamamoto, 2nd SiPMAdvanced Workshop, March 2014)

Polysilicon quenching resistors occupy some of the cell’s sensitive area. They are non-transparent for UV/blue/green light. The loss of sensitivity can be significant (especially for small cells). Solution

proposed by Hamamatsu transparent MFQ resistors

Another advantages of MFQ resistors are better uniformity and relatively small temperature coefficient smaller cell recovery time

change with temperature

Page 25: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

SiPMs with Metal Quenching Resistor: PDE increase

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 25

Polysilicon resistorsMQ resistors

MPPCs developed by HPK for the CMS HCAL Upgrade project

PDE(515 nm)>30% for 15 mm cell pitch MQR MPPCs. It was improved by a factor of >3 in comparison to the 15 mm cell pitch MPPCs with polysilicon quenching resistors.

Page 26: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Linearity and dynamic range (small signal model)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 26

Linearity of SiPM is determined by its total number of pixels

(B. Dolgoshein, TRD05, Bari)

In the case of uniform illumination:

This equation is correct for lightpulses which are shorter thanpixel recovery time , and for an“ideal” SiPM (no cross-talk andno after-pulsing). For slow lightpulses SiPM dynamic rangeincreases by a factor of:t(emission)/t(cell recovery)

Page 27: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Over saturation behaviour of SiPMs at high photon exposure

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 27

Over saturation behaviour of SiPMs at high photon exposure was observed by L. Gruber et al. Several types ofsilicon photomultipliers were exposed to short pulsed laser light (~30ps FWHM) with its intensity varying fromsingle photon to well above the number of microcells of the device. A significant deviation of the output ofSiPMs from the expected behaviour was observed at very high photon exposure.

Page 28: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

The future of SiPMs: UHD SiPMs

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 28

During last 3 years very high geometric factors (up to 80%) were achieved with smallcell pitch SiPMs or (Ultra High Density SiPMs). Small cells have many advantages: lowgain smaller X-talk, after-pulsing, recovery time; larger dynamic range, possibility tooperate SiPMs at high over-voltages, better resistance to radiation: smaller darkcurrents of irradiated SiPMs, smaller power dissipation, reduced blocking effects. Smallcells potentially should provide better timing resolution (smaller avalanchedevelopment time)

Previous development: linear array of MAPDs (18x1 mm2 , 15 000 cells/mm2 ) produced by Zecotek for the CMSHCAL Upgrade project.

Page 29: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Large dynamic range SiPMs for the CMS HE HCAL Upgrade

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 29

PD

E(51

5 n

m)

[%]

SiPM, T=23.2 C 45

40 HPK-array-10003-ch5

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8-ch. SiPM array for the CMS HE HCAL Upgrade project: Ø2.8 mm SiPMs, 15 mm cell pitch

05

1015202530354045

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PD

E [%

]

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dVB=4.0 V

Glass widow with special filter was designed by HPK to cut off UV light which can be produced by muons and hadrons in plastic fibers

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plit

ud

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V]

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Yu. Musienko, PD-15

SiPM laser response

Recovery time 7-8 ns

1400 SiPM arrays have beendelivered to CERN during this year

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FBK UHD2 SiPMs

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 30

RGB-UHDL < 1um

RGB-HD

RGB

(Alberto Gola – PhotoDet 2015, Troitsk)

L (um) Fill Factor

0.75 57.1%

1 48.8%

1.25 40.3%

1.5 32.6%

Fill Factor vs. trench widthCell sensitive area vs. trench width

Finished 10 mm cell pitch SiPM

Page 31: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

UHD2 SiPM parameters

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 31

3.4 ns

Laser response Recovery time

(Alberto Gola – PhotoDet-2015 , Troitsk)

12.5 um cellOV = 5.7 V

7.5 um cellOV = 4.6 V

L = 0.75 umT = 24 °C

Page 32: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

SiPM timing

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 32

SiPM cell size small, avalanche development time ~ tens of picoseconds. This promises very good time resolution. Single-photon time resolution for 3 SiPM area, measured at different biases for 425 nm light. Larger area SiPMs have slower signal rise-time. Factors limiting SPTR are signal rise-time, signal electron resolution and correlated noise (X-talk and delayed pulses). The latest is especially important for multi-photon events. The result which is shown here is among the best measured so far.

Page 33: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

SiPM time resolution - II

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 33

Page 34: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Vacuum ultra violet (VUV) SiPMs

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 34

Another important development: SiPMs sensitive to VUV light (<150 nm) were recently developed by HPK for detection LAr (T=-186 °C) scintillation light (l = 128 nm).

(NIM A833 (2016) 239–244)

The PDE(128 nm) wasmeasured ~8% for 50mm pitch SiPMs and~13% for 100 mm pitchSiPM at dVB=3 V

Am-241, E=5.5 MeV

Page 35: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Radiation induced damage in Silicon

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 35

Two types of radiation damage are produced by radiation in Si detectors:Bulk damage:• Incoming particle transfers a certain amount of energy

to atom• If the energy transferred to the atom is large than the

binding energy of a silicon atom (~190 eV) then the atom can be displaced, moving it to an interstitial site and leaving a vacancy single point or cluster defects

• Number of defects is proportional to the Non Ionizing Energy Loss (NIEL)

Surface damage:• Low energy X-rays can produce surface damage

affecting the SiO2/Si3N4 layer• Ionizing particles can produce charging up effects

affecting the internal fields inside the device

Page 36: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

SiPM: radiation hardness

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 36

In SiPMs radiation may cause:

• Fatal SiPMs damage (SiPMscan’t be used after certainabsorbed dose)• Dark current and dark countincrease (silicon …)• Change of the gain and PDE vs.voltage dependence (SiPM cell“blocking” effects due to highinduced dark carriersgeneration-recombination rate)• Breakdown voltage, PDE, Gainchange due to donor/acceptorconcentration change

SiPMs with high cell density and fast recovery time can operate up to 3*1012 neutrons/cm2 (gain change is< 25%).

Relative response to LED pulse vs. exposure to neutrons (Eeq~1 MeV) for different SiPMs

Page 37: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Dark current vs. exposure to neutrons (Eeq~1 MeV) for different SiPMs

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 37

High energy neutrons/protons produce silicon defects which cause an increase in dark count and leakage current in SiPMs:

Id~a*F*V*M*k,

a – dark current damage constant [A/cm];F – particle flux [1/cm2];V – silicon active volume [cm3]M – SiPM gaink – NIEL coefficient

aSi ~4*10-17 A*cm after 80 min annealing at T=60 °C (measured at T=20 °C) Damage produced by 40 neutrons (1 MeV) in 1 mm thick Si 1 dark count/sec at 20 °C

V~S*Gf*deff, S - areaGf - geometric factordeff - effective thickness

Thickness of the epi-layer for most of SiPMs is in the

range of 1-2 mm, however deff ~ 4 ÷ 50 mm for different SiPMs. High electric field effects (such as phonon assisted tunneling and field enhanced generation (Pool-Frenkel effect) play significant role in the origin of SiPM’s dark noise.

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Dependence of the SiPM dark current on the temperature (after irradiation)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 38

SiPM dark currents at low voltage (5V) behavesimilar with temperature to that of the PIN diode.However we observed significant difference of thisdependence for differenet SiPM types when theyoperate over breakdown! General trend is thatSiPMs with high VB value have faster dark currentreduction with the temperature.

(Yu.Musienko, NDIP-2014)

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Dependence of the SiPM dark current on the temperature (before/after irradiation)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 39

Interesting observation: dependence of the SiPM dark current on the temperature before and after irradiation is quite different:• For irradiated HE MPPC, Id reduction: ~1.88 times/10 °C• For non-irradiated HE MPPC, Id reduction: ~2.4 times/10 °C (like it should be for silicon

diodes!)

Page 40: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

SiPM irradiated up to 2.2*1014 n /cm2

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 40

Can SiPM survive very high neutron fluences expected at high luminosity LHC? Yes they can! FBK SiPM(1 mm2, 12 mm cell pitch was irradiated with 62 MeV protons up to 2.2*1014 n /cm2 (1 MeV equivalent).

(A.Heering et al., NIM A824 (2016) 111)

We found:- Increase of VB: ~0.5 V- Drop of the amplitude (~2 times)- Reduction of PDE (from 10% to 7.5 %)- Increase of the current (up to ~1mA at

dVB=1.5 V- ENC(50 ns gate, dVB=1.5V)~80 e, rmsThe main result is that SiPM survived this dose of irradiation and can be used as photon detector!

Page 41: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

X-ray damage

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 41

(E.Garutti et.al., 2014 JINST 9 C03021)

KETEK PM1125 (1.2 x 1.2 mm, 25 mm pixels)

Left: KETEK PM1125 I-V curves before irradiation (in red), compared with 3 kGy irradiation (blue) and 20MGy irradiation (green); measurements have been performed at 20 ◦C. Right: inter-pixel cross-talk measurements for the sensors before irradiation (in red), compared with 3 kGy irradiation (blue) and 20 MGy irradiation (green); no relevant changes in cross talk probability are measured.

• No significant change in breakdown voltage• Increased dark current below as well as above breakdown voltage• Slight decrease in gain

Page 42: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Position-Sensitive SiPMs: PS-SiPM RMD

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 42

RMD had designed a 5x5 mm2 position-sensitive solid-state photomultiplier (PS-SSPM) using a CMOS process that provides imaging capability on the micro-pixel level. The PS-SSPM has 11,664 micro-pixels total, with each having a micro-pixel pitch of 44.3 micron.

A basic schematics showing the design layout and pattern for PS-SSPM resistive network. Each square represents a micro-pixel. The network resistors are 246.5 Ohm each.

Anger logic:

A plot of the X–Y spatial resolution

(FWHM) as a function of the incident

beam spot light intensity. Spot size was ~30 micron.

An image of a 66 LYSO array having 0.5 mm pixels uniformly irradiated with 22Na.

Page 43: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

PS SiPM - NDL

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 43

Schematic cross-section of the PS-SiPMwith bulk quenching resistor

Top view of tetra-lateral type electrodes of the PS-SiPM with 4 anodes

The device takes advantages of the sheet N+ layer as the intrinsic continuous cap resistor for charge division, the same way adopted in PIN or APD PSD

Page 44: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

PS-SiPM – NDL (II)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 44

Reconstruction of nine positions of light spots from optical fiber tested in the central part of the device

The device, with an active area of 2.2 mm × 2.2 mm, demonstrated spatial resolution of 78–97 μm, gain of 1.4 × 105

and 46-ps time jitter of transmission delay for 210–230 photons.

IEEE TRANSACTIONS ON ELECTRON DEVICES, VOL. 61, NO. 9, SEPTEMBER 2014

Page 45: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

SiPMs with Bandpass Dichroic Filters

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 45

(M.Mazillo et al., to be published in Sensors)

PDE measured at 515 nm vs bias on n-on-p SiPM with and without BP filter

Optical microscopepicture of the STMicroSiPM (548 cells, 67.4%geometrical factor)

PDE spectral shape measured at 24 °C and dVB=3 V on n-on-p SiPM with and without BP filter

Green bandpath filterwith 5x5 mm area and1.1 mm thickness

Such a photo-sensor can be very used inapplications where protection of the detector fromunwanted light background (ambient light forexample) is required.

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SiC SSPM

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 46

(S.Dolinsky, GE, NDIP-2014)

Dark current vs. temperature

Potentially can be more radiation hard than silicon

Page 47: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

GaAs SSPM

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 47

Wide bandgap (1.42 eV): potentially can be more

radiation hard than silicon. Timing with GaAs SSPM can

be also better (high mobility of electrons and holes, fastavalanche development – direct semiconductor)

LightSpin Photomultiplier Chip™

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TSV technology (no bonding wire)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 48

TSV Technology:Further improved geometrical efficiency for arrays ,

(KETEK – Photodet-2015 (Troitsk))

(HPK: Koei Yamamoto, 2nd SiPMAdvanced Workshop, March 2014)

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Applications in HEP and astroparticleexperiments (some!)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 49

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SiPMs for T2K experiment (near detector)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 50

First large scale (~60 000) use of SiPMs in HEP experiments: scintillator detector with WLS fiber read out for T2K near detector.

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CMS HCAL Upgrade

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 51

(Yu.Musienko, PD-15, Troitsk) ~20 000 large area SiPMs will be used for the Phase I CMS HCAL upgrade

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Sci Fi tracker of LHCB experiment

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 52

(A. Malinin, INSTR-17, Novosibirsk)

6 layers of 2.5 m long, 250 mm dia.scintillating fibres will be read out by 128 channel SiPM arrays

Page 53: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

KLOE-2 experiment (Frascati)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 53

(Danilo Domenici, INSTR-17, Novosibirsk)

SiPMs will be used to read out LYSO crystals and W/Sci tiles with WLS fibers

Page 54: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Baby-MIND experiment

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 54

(Yu. Kudenko, INSTR-17, Novosibirsk)

Neutrino magnetized detector Baby-MIND - NP05 project in framework of CERN Neutrino Platform

A spectrometer to measure muon momentum

and charge identification.

Baby-MIND has 18 active modules

Active elements – scintillator detectors

with WLS/SiPM readout

Each module: 95 horizontal bars

and 16 vertical bars

Horizontal bar: 2900(L)x30(W)x7(t) mm3

Vertical bar: 1950(L)x210(W)x7(t) mm3

In total 1800 horiz and 250 vert sci bars

and 3-cm thick 33 magnetized iron plates

Scintillator plane

Page 55: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Mu3e experiment (SciFi detector)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 55

(Simon Corrodi, INSTR-17, Novosibirsk)

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Mu2e experiment (calorimeter)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 56

(David Hitlin, INSTR-17, Novosibirsk)

The Mu2e calorimetercontains 1348 CsJcrystals read out by2696 14x20 mm2 UVextended SiPMs

Page 57: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

MEGII experiment (PSI)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 57

(Paolo W. Cattaneo, INSTR-17, Novosibirsk)

SiPMs will replace PMTs in MEGII gamma detector

Page 58: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

NICA MPD ECAL (Dubna)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 58

(I. Tyapkin INSTR-17, Novosibirsk)

Large dynamic range SiPMswill be used to read out Shashlyk type calorimeter

Page 59: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

SiPM camera for CTA

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 59

(N. Otte, NDIP-14, Tours)

Use of SiPMs in MSCT camera will allow a factor of 2 gain in sensitivity and operation at full moon

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SiPM producers/developers

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 60

(G. Collazuol, PhotoDet 2012)

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Summary

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 61

Significant progress in development of SiPMs/SSPMs over last 3 years by several developers:

• High PDE: ~50-60% for blue-green light

• SiPMs with good sensitivity (PDE>10%) for VUV light have been developed

• Dark count at room temperature was reduced: ~30 kHz/mm2

• Low optical cross-talk: <1-5% for high OV

• Fast timing: SPTR~75 ps (FWHM)

• Large dynamic range: >10 000 pixels/mm2 (with high PDE>30%)

• Very fast cell recovery time: ~4 ns

• Large area: 6x6 mm2 and more

• TSV technology was introduced to build very compact SiPM arrays

• Position-sensitive SiPMs with good position resolution: <100 mm

• SiPMs demonstrated their rad. tolerance up to 2.2*1014 n/cm2

• SiC, GaAs, InGaP SSPMs were successfully developed

• SiPM is the main topic of all photodetector/instrumentation conferences!

• Explosion of SiPM/SSPM applications!

• . . .

Page 62: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

SiPM/SSPM perspectives (3-5 years)

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 62

My point of view:

• Further work to reduce correlated noise (this is one of the limiting factors for many applications)

• Small cell pitch (5 mm), large dynamic range SIPMs

• DUV SiPMs with good sensitivity (PDE>30%) for VUV light

• Dark count at room temperature can be reduced: <10 kHz/mm2

• Development of SiPMs for fast timing: SPTR<50 ps (FWHM)

• Fast cell recovery time: 2-3 ns

• Large area: 10x10 mm2 and more

• PS SiPMs with position resolution: <50 mm for single photons

• SiPMs with rad. tolerance up to 5*1014 n/cm2

• Further development of SiC, GaAs, InGaP SSPMs.

• Price will go down (for large quantities) <10 CHF/cm2....

Page 63: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Thank you for your attention!

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 63

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Back-up

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 64

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Studies of SiPMs irradiated with 2E13 n/cm2

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 65

S10943-4732S10943-4733

S12572-010PS12572-015P

0

10

20

30

40

50

350400450500550600650700750800

PD

E [%

]

Wavelength [nm]

T=25 C

dVB=4.0 V

HE MPPC arrays (Ø2.8(3.3) mm SiPMs) and 3x3 mm2 MPPCs (SMD package)

Irradiation performed at Ljubljana reactor

Page 66: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

VB determination before after 2E13 n/cm2

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 66

(A. Heering et.al, IEEE-NSS/MIC 2016, N27-19)

Dark current vs. bias before/after irr.

SiPMs VB measured using 1/I*dI/dV max. technique.

VB is increased by 0.43 V

VB before/after irr.

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HPK SiPM after 2E13 n/cm2

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 67

LED (515 nm, 15 ns) pulse amplitude ~ 12 000 photons/pulse high enough to see signals from all SiPMs

Self-heating effects? SMD package!

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HPK S10943-4732 2.8 mm SiPM after 2E13 n/cm2 at reduced temperature

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 68

Average LED pulse amplitude ~2400 photons/pulse

• At T=-9.4 °C SiPM LED pulse response recovers to that of non-irradiated SiPM• From 24.9 °C to -23.5 °C: ~21 times Id reduction (~1.88 times/10 °C)• Maximum S/N improves >7 times due to dVB increase (IEEE-NSS/MIC 2016, N27-19)

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Irradiation with cold neutrons

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 69

(D.Durini et. all, NIM A835 (2016) 99-109 )

Thermal neutron study (T=23 °C) at FMR II reactor at Julich (En = 3.27 meV, up to 6E12 n/cm2)

SensL: 12x12 detector array ArrayC-30035-144P-PCB, 3x3 mm2, 35 mm cell pitch, VB+2.5 VHamamatsu: 8x8 MPPC array 12642–0808PB-50, 3x3 mm2 , 50 mm cell pitch, VB+2.4 V

Neutron dose dependent average dark currents measured respectively on 10 SiPM detectors from the SensL 12x12 SiPM Series-C detector board, and on 12 MPPC detectors from the Hamamatsu 8x8 MPPC array S12642–0808PB-50 detector board.

Thermal neutron capture can cause nuclear transmutations 30Si + n 31Si 31P + b-

Produces isolated defects with ~ 2-5 defects per absorbed neutron

Page 70: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Radiation hardness study of the Philips Digital Photon Counter with proton beam

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 70(M.Barnyakov et al., Elba-2015)

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Displacement damage function (NIEL) for protons, neutrons, pions and electrons vs. their energy

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 71

Page 72: Recent Progress and Perspectives in Solid State ......2017/06/30  · Musienko, Detector Seminar, CERN, 30.06.2017 23 Standard field Low-field > 7 orders of magnitude ! A 10x10

Fluence dependence of leakage current for silicon detectors

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 72

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Current related damage rate a as function of cumulated annealing time

Yu. Musienko, Detector Seminar, CERN, 30.06.2017 73

(M.Moll, PhD thesis)