Multi-residue Method for Pesticides Residue Analysis in Grapes by
PROFICIENCY TESTING PROGRAMS PESTICIDES … · Pesticides in vegetables & fruits (dithiocarbamates)...
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Transcript of PROFICIENCY TESTING PROGRAMS PESTICIDES … · Pesticides in vegetables & fruits (dithiocarbamates)...
Pesticides in fruits and citrus fruits
Pesticides in cereals
Pesticides in vegetables
Pesticides in fats
Pesticides in vegetables (bromides, nitrates)
Pesticides in wines
Pesticides in honeys
Pesticides in vegetables & fruits (dithiocarbamates)
Pesticides in Dairy Products
Multi-residue screening of pesticides in Food
A = PTS accredited by COFRAC
1 / 11FiCir01-Pesticides-GB
Révision l du 27/09/2016
A19a
A19b
A19c
A19d
A19e
A19f
A19g
A19h
A19j
A66
PROFICIENCY TESTING PROGRAMS
PESTICIDES RESIDUES
Document valide au 04/10/2016
• Proficiency testing scheme created in 1990
• This PTS is accredited by COFRAC
• 68 participants worldwide
• 6 rounds per annual series
• For more details on the samples, please refer to the schedule.
2 / 11
19a- PESTICIDES IN FRUITS AND CITRUS FRUITS
NA => Non accredited parameter
*This list of parameters could be modified according to the nature of the product. The information mentioned in thatform could be modified during annual series after decisions from the Committee, technical group or Chairperson.
Fruits and GrapeAcetamipride Diphenylamine MetrafenoneAzoxystrobine Etephon MyclobutanilBifenthrine Fenhexamid OmethoateBoscalide Fenitrothion Parathion methylButoxyde de pyperonyl Fludioxonil PhosaloneCarbendazime Glufosinate PhosmetCarbofuran Kresoxym methyl PyraclostrobineCyhalothrine-lambda Lindane PyrimethanilCyprodinyl Mandipropamide PyrimicarbeDeltamethrine Mepanipyrim TebufenozideDimethoate Metalaxyl-m Thiaclopride
Additional Molecules – only on GrapeAcrinathrine Etoxazole PenconazoleBenalaxyl Fenamidone PermethrineBuprofezine Fenbuconazole ProcymidoneChlorpyriphos ethyl Flusilazole ProquinazideChlorpyriphos methyl Fosetyl aluminium / Phosphorous acid (ethyl phosphite) SpiroxamineCyazofamide Hexytiazox TebuconazoleCyflufenamide Iprodione TebufenpyradCyproconazole Iprovalicarb TriadimenolDimetomorphe Oxadixyl Vinclozoline
Citrus fruits
Bifenthrine Hexytiazox Orthophenylphenol
Buprofezine Imazalil Phosalone
Carbendazime Iprodione Phosmet
Chlorpyriphos ethyl Lindane Procymidone
Cyflufenamide Malathion Pyrimicarbe
Deltamethrine Omethoate Thiabendazole
Dimethoate
1 unknown molecule per round
MAIN PARAMETERS *
Lemon Orange Apple
Strawberry Peach Grape
MATRICES
FiCir01-Pesticides-GB
Révision l du 27/09/2016
Document valide au 04/10/2016
• Proficiency testing scheme created in 1990
• This PTS is accredited by COFRAC
• 57 participants worldwide
• For more details on the samples, please refer to the schedule.
3 / 11
19B- PESTICIDES IN CEREALS
Common wheat Corn
Feed Flour
MATRICES
2,4-D
Ampa Imidacloprid
Azoxystrobine Lindane
Bifenthrine Malathion
Boscalide Mepiquat
Butoxyde de pyperonyl Metalaxyl-m
Chlormequat Pendimetaline
Chlorpyriphos ethyl Permethrine
Chlorpyriphos methyl Profenophos
Cyhalothrine-lambda Propyconazole
Cypermethrine Pyrimicarbe
Deltamethrine Pyrimiphos methyl
Diflufenican Tebuconazole
Fenitrothion Thiametoxam
Glyphosate Triazophos
1 unknown molecule per round
MAIN PARAMETERS *
NA => Non accredited parameter
*This list of parameters could be modified according to the nature of the product. The information mentioned in thatform could be modified during annual series after decisions from the Committee, technical group or Chairperson.
FiCir01-Pesticides-GB
Révision l du 27/09/2016
Document valide au 04/10/2016
4 / 11
19C- PESTICIDES IN VEGETABLES
• Proficiency testing scheme created in 1990
• This PTS is accredited by COFRAC
• 57 participants worldwide
• 4 rounds per annual series
• For more details on the samples, please refer to the schedule.
Acetamipride GlufosinateAzoxystrobine Hydrazine maleiqueBoscalide ImidaclopridButoxyde de pyperonyl IprodioneCarbofuran LindaneChlorates LinuronChlorprophame Metalaxyl-mChlorpyriphos ethyl MetoxuronCyhalothrine-lambda OxadixylCyprodinyl PhosmetDeltamethrine ProcymidoneEtephon PropyzamideFludioxonil PyrimethanilFlutolanil Pyrimicarbe
Fosetyl aluminium / acide phosphoreux (ethyl phosphite)
TebufenozideVinclozoline
1 unknown molecule per round
Carrot Cabbage
Green beans Lettuce
MATRICES
MAIN PARAMETERS *
NA => Non accredited parameter
*This list of parameters could be modified according to the nature of the product. The information mentioned in thatform could be modified during annual series after decisions from the Committee, technical group or Chairperson.
FiCir01-Pesticides-GB
Révision l du 27/09/2016
Document valide au 04/10/2016
5 / 11
19D- PESTICIDES IN FATS
• Proficiency testing scheme created in 1990
• This PTS is accredited by COFRAC
• 41 participants worldwide
• 4 rounds per annual series
• For more details on the samples, please refer to the schedule.
Acetamipride Glufosinate
Azoxystrobine Hydrazine maleique
Boscalide Imidacloprid
Butoxyde de pyperonyl Iprodione
Carbofuran Lindane
Chlorates Linuron
Chlorprophame Metalaxyl-m
Chlorpyriphos ethyl Metoxuron
Cyhalothrine-lambda Oxadixyl
Cyprodinyl Phosmet
Deltamethrine Procymidone
Etephon Propyzamide
Fludioxonil Pyrimethanil
Flutolanil Pyrimicarbe
Fosetyl aluminium / acide phosphoreux (ethyl phosphite)
Tebufenozide
Vinclozoline
1 unknown molecule per round
MAIN PARAMETERS *
Cheese Refined green olives
Refined olive oil Soyabean
MATRICES
NA => Non accredited parameter
*This list of parameters could be modified according to the nature of the product. The information mentioned in thatform could be modified during annual series after decisions from the Committee, technical group or Chairperson.
FiCir01-Pesticides-GB
Révision l du 27/09/2016
Document valide au 04/10/2016
6 / 11
19E- PESTICIDES IN VEGETABLES: NITRATES ET BROMIDES
• Proficiency testing scheme created in 1990
• This PTS is accredited by COFRAC
• 55 participants worldwide
• 3 rounds per annual series
• For more details on the samples, please refer to the schedule..
NA => Non accredited parameter
*This list of parameters could be modified according to the nature of the product. The information mentioned in thatform could be modified during annual series after decisions from the Committee, technical group or Chairperson.
Lettuce Spinach
Nitrates Bromides
MATRICES
MAIN PARAMETERS *
FiCir01-Pesticides-GB
Révision l du 27/09/2016
Document valide au 04/10/2016
Lettuce Spinach
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19F- PESTICIDES IN WINES
• Proficiency testing scheme created in 1990
• This PTS is accredited by COFRAC
• 53 participants worldwide
• 4 rounds per annual series
• For more details on the samples, please refer to the schedule.
NA => Non accredited parameter
*This list of parameters could be modified according to the nature of the product. The information mentioned in thatform could be modified during annual series after decisions from the Committee, technical group or Chairperson.
MATRICES
MAIN PARAMETERS *
• Azoxystrobin• Benalaxyl• Boscalide• Carbendazim• Chlorpyriphos-ethyl• Chlorpyriphos-methyl• Cyazofamide• Cyproconazol• Cyprodinil• Dimethomorph• Fenamidone• Fenbuconazol• Fenhexamide
• Fenitrothion• Fludioxonil• Flusilazol• Fosetyl aluminium• Iprodione• Iprovalicarb• Kresoxim-methyl• Mandipropamid• Mepanipyrime• Metalaxil-M• Metrafenone• Myclobutanil• Penconazol
• Procymidone• Pyraclostrobin• Pyrimethanil• Spiroxamine• Tebuconazol• Tebufenozide• Tebufenpyrade• Vinclozolin
•1 unknown molecule per round
FiCir01-Pesticides-GB
Révision l du 27/09/2016
Document valide au 04/10/2016
8 / 11
19G- PESTICIDES IN HONEYS
• Proficiency testing scheme created in 1990
• This PTS is accredited by COFRAC
• 31 participants worldwide
• 4 rounds per annual series
• For more details on the samples, please refer to the schedule.
NA => Non accredited parameter
*This list of parameters could be modified according to the nature of the product. The information mentioned in thatform could be modified during annual series after decisions from the Committee, technical group or Chairperson.
MAIN PARAMETERS *
Repellents against bees and varroacides:• Acrinathrine• Brompropylate• Chlorfenvinphos• Coumaphos• Cymiazole• DEET (diethyl toluamide)• Deltamethrin• Flumethrine• Malathion• Piperonil butoxide• Tetradifon• Tau fluvalinate
Pesticides:• Bifenthrine• Boscalide• Carbendazim• Chlorpyrifos-ethyl• Cypermethrin• Lambda cyhalothrine• Permethrin• Thiaclopride
1 unknown molecule per round
Honey
MATRICES
FiCir01-Pesticides-GB
Révision l du 27/09/2016
Document valide au 04/10/2016
9 / 11
19H- PESTICIDES IN VEGETABLES & FRUITS (DITHIOCARBAMATES)
• Proficiency testing scheme created in 2014
• This PTS is accredited by COFRAC
• 31 participants worldwide
• 4 rounds per annual series
• For more details on the samples, please refer to the schedule.
NA => Non accredited parameter
*This list of parameters could be modified according to the nature of the product. The information mentioned in that form could be
modified during annual series after decisions from the Committee, technical group or Chairperson.
Apple Endive Lettuce
MATRICES
Dithiocarbamates
MAIN PARAMETERS *
FiCir01-Pesticides-GB
Révision l du 27/09/2016
Document valide au 04/10/2016
Cheese Milk in powder form
• Proficiency testing scheme created in 2016• PTS accredited by COFRAC• 2 rounds per annual series• For more details on the samples, please refer to the schedule.
19j- PESTICIDES IN DAIRY PRODUCTS
2,4-D Endosulfan sulfate
Azoxystrobine Endosulfans (sum)
Bifenthrine Fenitrothion
Butoxyde de pyperonyl Hexachlorobenzene
Chlorpyriphos Ethyl Lindane
Chlorpyriphos Methyl Malathion
Cyhalothrine-lambda Metalaxyl-M
Cypermethrine Parathion Methyl
DDT Pyrimicarbe
Deltamethrine Pyrimiphos Methyl
Endosulfan alpha Pyroproxifen
Endosulfan bêta
1 unknown molecule per round
MAIN PARAMETERS *
NA => Non accredited parameter
*This list of parameters could be modified according to the nature of the product. The information mentioned in thatform could be modified during annual series after decisions from the Committee, technical group or Chairperson.
MATRICES
FiCir01-Pesticides-GB
Révision l du 27/09/2016 10 / 11
Document valide au 04/10/2016
2,4-D Endosulfan alpha OrthophenylphenolAcetamipride Endosulfan bêta OxadixylAcrinathrine Endosulfan sulfate OxidiazonAMPA Endosulfans (somme) Parathion MethylAtrazine Etephon PenconazoleAzoxystrobine Ethion PendimetalineBifenthrine Etoxazole PermethrineBenalaxyl Fenamidone PhosaloneBendiocarb Fenbuconazole PhosmetBoscalide Fenhexamid ProchlorazBromopropylate Fenitrothion ProcymidoneBuprofezine Fenproprathrine ProfenophosButoxyde de pyperonyl Fludioxonil PropargiteCarbaryl Flumethrine PropyconazoleCarbendazime Flusilazole PropyzamideCarbofuran Flutolanil ProquinazideChlorates Flutriafol PyraclostrobineChlorfenvinphos HCH-alpha PyrimethanilChlorprophame HCH-beta PyrimicarbeChlorpyriphos Ethyl HCH-delta Pyrimiphos MethylChlorpyriphos Methyl Hexachlorobenzene PyroproxifenCoumaphos Hexytiazox QuintozeneCyazofamide Imidacloprid SpiroxamineCyflufenamide Imazalil Tau-fluvanilateCyhalothrine-lambda Iprodione TebuconazoleCymiazole Iprovalicarb TebufenozideCypermethrine Kresoxym methyl TebufenpyradCyproconazole Lindane TetraconazoleCyprodinyl Linuron TetradifonDDT Malathion ThiabendazoleDeltamethrine Mandipropamide ThiacloprideDiazinon Mepanipyrim ThiametoxamDicofol Metalaxyl-M TriadimenolDiethyl toluamide (DEET) Methidathion TriazophosDifenoconazole Metolachlor TrifloxystrobineDiflufenican Metoxuron TrifluralineDimethoate Metrafenone VinclozolineDimetomorphe Myclobutanil
Diphenylamine Omethoate
• Proficiency test created in 2013
• This PTS is accredited by COFRAC
• Between 15 and 28 participants in the world
• 1 to 4 rounds per year
•For more details on the samples, please refer to the schedule.
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66 - Multi-residue screening of pesticides
NA => Non accredited matrixNote : BIPEA reserves the right to cancel the round in case of less than 12 participants.
*This list of parameters could be modified according to the nature of the product. The information mentioned in thatform could be modified during annual series after decisions from the Committee, technical group or Chairperson.
MAIN PARAMETERS *
66a - Fruits 66c – Vegetables
66b - Cereals 66i – Essential oils
MATRICES
Spiking range: 0.020 to 0.200 mg/kgBetween10 and 25 moleculesto identifyand quantify in blind among the followings:
FiCir01-Pesticides-GB
Révision l du 27/09/2016
Document valide au 04/10/2016