Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for...
Transcript of Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for...
Preparation of Polymer Samples for MicrospectroscopyPreparation of Polymer Samples for MicrospectroscopyKristen WileySenior Cleanroom Microscopists, McCrone AssociatesAugust 27, 2015
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The McCrone GroupThe McCrone Group
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Hooke College of Applied SciencesHooke College of Applied Sciences
Light Microscopy Microspectroscopy
Electron Microscopy Sample Preparation
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MATERIALS ANALYSIS
McCrone AssociatesMcCrone Associates
ISO 14644 Class 5 Cleanroom
Polymers Polymers Different Forms
Wikipedia.com
Preparing Polymer Samples for FTIRPreparing Polymer Samples for FTIR
Rubber Stoppers Plastic Shavings
MethodsMethods
Selection of the appropriate sampling method is critical to achieving good results!
• Are made from a large cover glass Micro Cover GlassesMicro Cover Glasses
Micro Cover GlassesMicro Cover Glasses
• Are made from a glass slideGlass WedgeGlass Wedge
Glass WedgeGlass Wedge
1mm
Micro ToolsMicro ToolsSmall particles require small tools
• Tungsten needle
• Carbide scribe
• Curved forceps
• KBr holder
Micro KBr CrystalsMicro KBr Crystals• Purchased as 1” x 1” x 4mm crystal
Results??? To Be Continued:Results??? To Be Continued:
Are There Any Questions??Are There Any Questions??
Kristen Wiley and Heidi TaleskySenior Cleanroom Microscopists
[email protected] • [email protected] •(630) 887‐7100
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