PowerPoint Presentation...Optimization of supply component irradiation: • Electron to X-ray...

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Lifetime study of electronic devices for extreme radiation conditions Andrea Šagátová 1,2 , Marko Fülöp 1 , Martin Magyar 3 , Vladimír Nečas 2 , Bohumír Zaťko 4 , Peter Hybler 1 , Michal Rafaj 3 1 University Centre of Electron Accelerators, Slovak Medical University in Bratislava, Ku kyselke 497, 911 06 Trenčín, Slovak Republic 2 Institute of Nuclear and Physical Engineering, Slovak University of Technology, Ilkovičova 3, 812 19, Bratislava, Slovak Republic 3 RMC Ltd., Trenčianska ulica 863/66, 018 51 Nová Dubnica, Slovak Republic 4 Institute of Electrical Engineering, Slovak Academy of Sciences, Dúbravská cesta 9, 841 04 Bratislava, Slovak Republic CERN accelerator component Engine for precise positioning of dipole magnets in Super LHC accelerator in CERN Made in ZTS VVÚ KOŠICE Ltd., SK Tested by PC controlled tester at ZTS VVÚ KOŠICE Ltd. SK Background Methodology Linear electron accelerator UELR 5-1S Producer NIIEFA, St. Petersburg Maximum beam power 1 kW Electron energy (3.6 - 6.2) MeV Beam repetition rate 5, 10, 20, 40, 120 or 240 Hz Converted X-rays up to 6.2 MeV Beam scanning width: 40 cm, 45 cm, 50 cm Beam diameter at window 11 mm Conveyor velocity: 0.1 mm/s - 100 mm/s Three modes of irradiation: I. the static scientific irradiation II. the in-line routine irradiation on conveyor III. the rotational irradiation LINEAR ELECTRON ACCELERATOR UELR 5-1S ACCELERATOR IN CROSS-SECTION VIEW OF THE BUILDING Radiation technology development and its applications bring new requirements on related electronic devices. The study of radiation effect on electronic devices is important for increasing their lifetime and the reliability of the whole technology, when used in radiation harsh environment like space, large accelerators, nuclear reactors etc. We have studied the effect of the X-rays and the high energy electrons on lifetime of devices used in radiation extreme conditions: the CERN accelerator component (by electrons) the semiconductor devices for the first Slovak satellite (by X- rays) the semiconductor detectors for radiation imaging and dosimetry (by electrons ) Method of lifetime study 1. Monte Carlo simulations of irradiation geometry and tested device together with dose-depth distribution in it 2. Irradiation of phantom of tested device 3. Irradiation of tested device 4. Electrical and /or mechanical functional tests of irradiated device in collaboration with: Slovak University of Technology in Bratislava, SK, ZTS VVÚ KOŠICE Ltd., SK 5. Proposal of measures for longer device operational life in real radiation fields Radiation sensitive wires Radiation sensitive connectors Simulation of operating radiation environment: Stray radiation fields are created at high-energy particle accelerators by the intentional interaction of the accelerated beam with targets, beam dumps, collimators and by unintentional beam losses on structural components of the machine. At electron accelerators (UCEA), the most important secondary radiation is bremsstrahlung photons and high-energy electrons produced in electromagnetic cascades. At proton accelerators (CERN), interaction of the beam with materials generates a hadron cascade containing neutrons, charged hadrons, muons, photons and electrons. Dominant are neutrons. Simulation of secondary particles of 250 MeV protons at various depths of concrete shield impinging on an iron target thicker than the proton range (A) and neutron energy distributions in iron after various concrete thicknesses penetration (B): A B Absorbed dose distributions in supply components irradiated at CERN proton accelerator and by X-rays of 5 MeV linac are similar within relative deviation of 20% according to MC simulation. Optimization of supply component irradiation: Electron to X-ray conversion efficiency only 15-17 % 2 MGy: 200 h X -ray or 20 h electron irradiation e - and X-rays: similar radiation damage, electron range in material has to be considered (only for low density components). Suggestion for making supply component more radiation resistant : Shielding of supply component by 8 cm thick polyethylene (CH 2 ) with 3% B will decrease the absorbed dose by 12%. Irradiation Partial dose [kGy] Total dose [kGy] Type of radiation Functional test result 1. 250 250 X-rays Functional 2. 500* 750 electrons Functional 3. 500* 1250 electrons Functional 4. 750* 2000 electrons Functional Beam repetition rate 10 Hz, scanning width 40 cm, steady mode Results: After 250 kGy – connector mechanically destroyed After 750 kGy – significant color change of plastic parts After 2 MGy – engine still functional UCEA SMU Conclusions The CERN accelerator component, the engine for dipole precise positioning, tested up to 2 MGy of electrons, only its plastic were mechanically destroyed. The commercial semiconductor devices for skCUBE satellite power unit from various manufacturers were tested up to a dose of 1300 Gy of X-rays, representing the dose obtained by satellite on its orbit during about 3 years. The semiconductor detectors were irradiated up to 120 kGy of electrons preserving the functionality with initial improvement of energy resolution followed by its degradation. Trenčín UCEA ,Trenčín, SK IRRADIATING ROOM Semiconductor devices for skCUBE Semiconductor detectors of radiation SkCUBE, the first Slovak satellite: made by Slovak Organization for Space Activities ready for launch in 2017 Circular Earth’s orbit with 500 km altitude with an inclination angle of 98 gives estimated ionizing dose exposure of 400 Gy/year (40 kRad/y) Mission duration from 1 to 2 years Commercial semiconductor devices for the skCUBE power supply unit were chosen according to their radiation hardness evaluated by X-ray irradiation 7.1.2016: presentation of final skCUBE . SkCUBE with power source board. -6 -4 -2 0 2 4 9.6 9.7 9.8 9.9 10.0 10.1 10.2 10.3 -10 -5 0 5 10 fz = 10Hz, fs= 0.25Hz, dr=40cm, rtg. to 5 MeV, h = 98cm, t=1380s ionizing chamber 104,5nC = 5Gy, dose-rate = 0.722814 rad/s dose(Gy) y(cm) x (cm) 9.650 9.734 9.818 9.901 9.985 10.07 10.15 10.24 10.32 Irradiation: By continuous spectrum of X-rays up to 5 MeV Beam repetition rate 10 Hz, scanning width 40 cm, steady mode Doses obtained in 13 steps Electronic devices for satellite power supply mounted on PCB ( Printed Circuit Board) with ionizing chamber on the right. Results: Two kinds of degradation with increasing applied dose: the output voltage of device degraded and the input current preserved with applied dose (voltage references) the functionality of device is preserved, but the input current dramatically increases (battery chargers) Homogeneity of irradiating field. 0 200 400 600 800 1000 1200 1.248 1.249 1.250 1.251 1.252 1.253 Output voltage (V) Dose (Gy) Sample REF3312Al: 1 2 0 200 400 600 800 1000 1200 1.24 1.26 1.28 1.30 1.32 1.34 Output voltage (V) Dose (Gy) Sample ADR1581A: 1 2 0 200 400 600 800 1000 0 500 1000 1500 2000 2500 3000 3500 Input current at 2 V (A) Dose (Gy) SPV1040 sample: 1 2 3 4 0.6 0.8 1.0 1.2 1.4 Starting input voltage (V) The output voltage of references as a function of accumulative dose. The input current of battery chargers as a function of accumulative dose. 0 20 40 60 80 100 120 50 55 60 65 70 75 Rev. voltage 200 V 241 Am - - 59.5 keV 4A - 20 kGy/h CCE (%) Dose (kGy) 20 40 60 80 100 0 500 1000 1500 2000 2500 3000 3500 Channel Counts per channel Channel Dose: 0 kGy 2 kGy 24 kGy 40 kGy 86 kGy 120 kGy Detector 4A2, Rev. voltage 200 V, t = 100 s, 241 Am - - 59.5 keV dose rate 20 kGy/h 20 40 60 80 100 1 10 100 1000 10000 Counts per channel 0 20 40 60 80 100 120 15 20 25 30 35 40 Rev. voltage 200 V 241 Am - - 59.5 keV 4A - 20 kGy/h FWHM (%) Dose (kGy) GaAs detectors of ionizing radiation Made by Slovak Academy of Sciences in Bratislava, SK Working in single photon counting mode Prepared from 230 µm thick semi-insulating GaAs. Top Schottky contact: circle: 1 mm, Ti/Pt/Au (10/35/90 nm) , Back ohmic contact: full-back-side, Ni/AuGe/Au (30/50/90 nm) Developed for digital imaging with X-ray tube and particle tracking in space and accelerators Irradiation: By 5 MeV electrons, Beam repetition rate 10 Hz, scanning width 40 cm, steady mode, Doses obtained in 12 steps 28.4. 22.5. 5.6. 2.7. 18.8. 26.8.13.11.9.12. 19.1. 17.3. 27.4. 12.1. 0 20 40 60 80 100 120 2015 4 1 Dose (kGy) date 2 2014 Accumulative dose applied to detectors: 9.12.9.12.9.12. 12.12. 12.12. 15.1.16.1.20.1.27.1.29.1.29.1. 4.2. 27.2. 6.3. 0 200 400 600 800 1000 1200 1400 2015 50 10 Dose (Gy) date 25 2014 Accumulative dose applied to electronic devices for skCUBE: SI GaAs DETECTORS for digital radiation imaging Detector charge collection efficiency (CCE) systematically decreases with applied dose. Gradual degradation of relative energy resolution (FWHM) with accumulative dose in the range of doses of 24 up to 120 kGy. . Detector ability to measure spectra after radiation degradation. 0 2 4 6 8 10 12 14 16 0 1 2 3 4 5 6 Dose (kGy) Material depth (mm) GaAs Si 5 MeV electrons Dose-depth distribution in Si and GaAs -20 -15 -10 -5 0 5 10 15 20 0 50 100 150 200 250 300 350 Dose (kGy) Distance from the beam centre (cm) distance from acc. window: y=10 cm y=20 cm y=30 cm y=40 cm y=55 cm y=96 cm Dose distribution perpendicular to beam scan Results: Irradiation

Transcript of PowerPoint Presentation...Optimization of supply component irradiation: • Electron to X-ray...

Page 1: PowerPoint Presentation...Optimization of supply component irradiation: • Electron to X-ray conversion efficiency only 15-17 % • 2 MGy: 200 h X -ray or 20 h electron irradiation

Lifetime study of electronic devices for extreme radiation conditions

Andrea Šagátová1,2, Marko Fülöp1, Martin Magyar3, Vladimír Nečas2, Bohumír Zaťko4, Peter Hybler1, Michal Rafaj3

1 University Centre of Electron Accelerators, Slovak Medical University in Bratislava, Ku kyselke 497, 911 06 Trenčín, Slovak Republic

2 Institute of Nuclear and Physical Engineering, Slovak University of Technology, Ilkovičova 3, 812 19, Bratislava, Slovak Republic 3 RMC Ltd., Trenčianska ulica 863/66, 018 51 Nová Dubnica, Slovak Republic

4 Institute of Electrical Engineering, Slovak Academy of Sciences, Dúbravská cesta 9, 841 04 Bratislava, Slovak Republic

CERN accelerator component • Engine for precise positioning of dipole magnets in Super

LHC accelerator in CERN • Made in ZTS VVÚ KOŠICE Ltd., SK • Tested by PC controlled tester at ZTS VVÚ KOŠICE Ltd. SK

Background

Methodology

Linear electron accelerator UELR 5-1S Producer NIIEFA, St. Petersburg Maximum beam power 1 kW Electron energy (3.6 - 6.2) MeV Beam repetition rate 5, 10, 20, 40, 120 or 240 Hz Converted X-rays up to 6.2 MeV Beam scanning width: 40 cm, 45 cm, 50 cm Beam diameter at window 11 mm Conveyor velocity: 0.1 mm/s - 100 mm/s

Three modes of irradiation: I. the static scientific irradiation

II. the in-line routine irradiation on conveyor III. the rotational irradiation

LINEAR ELECTRON ACCELERATOR UELR 5-1S

ACCELERATOR IN CROSS-SECTION VIEW OF THE BUILDING

• Radiation technology development and its applications bring new requirements on related electronic devices.

• The study of radiation effect on electronic devices is important for increasing their lifetime and the reliability of the whole technology, when used in radiation harsh environment like space, large accelerators, nuclear reactors etc.

• We have studied the effect of the X-rays and the high energy electrons on lifetime of devices used in radiation extreme conditions: • the CERN accelerator component (by electrons) • the semiconductor devices for the first Slovak satellite (by X-

rays) • the semiconductor detectors for radiation imaging and

dosimetry (by electrons )

Method of lifetime study 1. Monte Carlo simulations of irradiation

geometry and tested device together with dose-depth distribution in it

2. Irradiation of phantom of tested device 3. Irradiation of tested device 4. Electrical and /or mechanical functional tests

of irradiated device in collaboration with: Slovak University of Technology in Bratislava, SK, ZTS VVÚ KOŠICE Ltd., SK

5. Proposal of measures for longer device operational life in real radiation fields

Radiation sensitive wires Radiation sensitive connectors

Simulation of operating radiation environment: Stray radiation fields are created at high-energy particle accelerators by the intentional interaction of the accelerated beam with targets, beam dumps, collimators and by unintentional beam losses on structural components of the machine. At electron accelerators (UCEA), the most important secondary radiation is bremsstrahlung photons and high-energy electrons produced in electromagnetic cascades. At proton accelerators (CERN), interaction of the beam with materials generates a hadron cascade containing neutrons, charged hadrons, muons, photons and electrons. Dominant are neutrons.

Simulation of secondary particles of 250 MeV protons at various depths of concrete shield impinging on an iron target thicker than the proton range (A) and neutron energy distributions in iron after various concrete thicknesses penetration (B):

A B

Absorbed dose distributions in supply components irradiated at CERN proton accelerator and by X-rays of 5 MeV linac are similar within relative deviation of 20% according to MC simulation. Optimization of supply component irradiation: • Electron to X-ray conversion efficiency only 15-17 % • 2 MGy: 200 h X -ray or 20 h electron irradiation • e- and X-rays: similar radiation damage, electron range in material has to be

considered (only for low density components).

Suggestion for making supply component more radiation resistant : Shielding of supply component by 8 cm thick polyethylene (CH2) with 3% B will decrease the absorbed dose by 12%.

Irradiation Partial dose [kGy]

Total dose [kGy]

Type of radiation

Functional test result

1. 250 250 X-rays Functional

2. 500* 750 electrons Functional

3. 500* 1250 electrons Functional

4. 750* 2000 electrons Functional

Beam repetition rate 10 Hz, scanning width 40 cm, steady mode

Results: • After 250 kGy – connector mechanically destroyed • After 750 kGy – significant color change of plastic parts • After 2 MGy – engine still functional

UCEA

SMU

I

Conclusions • The CERN accelerator component, the engine for dipole precise positioning,

tested up to 2 MGy of electrons, only its plastic were mechanically destroyed. • The commercial semiconductor devices for skCUBE satellite power unit from

various manufacturers were tested up to a dose of 1300 Gy of X-rays, representing the dose obtained by satellite on its orbit during about 3 years.

• The semiconductor detectors were irradiated up to 120 kGy of electrons preserving the functionality with initial improvement of energy resolution followed by its degradation.

Trenčín

UCEA ,Trenčín, SK

IRRADIATING ROOM

Semiconductor devices for skCUBE

Semiconductor detectors of radiation

SkCUBE, the first Slovak satellite: • made by Slovak Organization for Space Activities • ready for launch in 2017 • Circular Earth’s orbit with 500 km altitude with an

inclination angle of 98 gives estimated ionizing dose exposure of 400 Gy/year (40 kRad/y)

• Mission duration from 1 to 2 years • Commercial semiconductor devices for the skCUBE

power supply unit were chosen according to their radiation hardness evaluated by X-ray irradiation

7.1.2016: presentation of final skCUBE . SkCUBE with power source board.

-6

-4

-2

0

2

4

9.6

9.7

9.8

9.9

10.0

10.1

10.2

10.3

-10

-5

0

5

1 0

fz = 10Hz, fs= 0.25Hz, dr=40cm, rtg. to 5 MeV, h = 98cm, t=1380s

ionizing chamber 104,5nC = 5Gy, dose-rate = 0.722814 rad/s

do

se

(Gy)

y (cm)x (cm)

9.650

9.734

9.818

9.901

9.985

10.07

10.15

10.24

10.32

Irradiation: • By continuous spectrum of X-rays up to 5 MeV • Beam repetition rate 10 Hz, scanning width

40 cm, steady mode • Doses obtained in 13 steps

Electronic devices for satellite power supply mounted on PCB ( Printed Circuit

Board) with ionizing chamber on the right.

Results: Two kinds of degradation with increasing applied dose: • the output voltage of device degraded

and the input current preserved with applied dose (voltage references)

• the functionality of device is preserved, but the input current dramatically increases (battery chargers)

Homogeneity of irradiating field.

0 200 400 600 800 1000 12001.248

1.249

1.250

1.251

1.252

1.253

Ou

tpu

t vo

lta

ge

(V

)

Dose (Gy)

Sample REF3312Al:

1

2

0 200 400 600 800 1000 1200

1.24

1.26

1.28

1.30

1.32

1.34

Outp

ut voltage (

V)

Dose (Gy)

Sample ADR1581A:

1

2

0 200 400 600 800 10000

500

1000

1500

2000

2500

3000

3500

Inp

ut

cu

rre

nt

at 2

V (

A)

Dose (Gy)

SPV1040 sample:

1

2

3

4

0.6

0.8

1.0

1.2

1.4

Sta

rtin

g in

pu

t vo

lta

ge

(V

)

The output voltage of references as a function of accumulative dose.

The input current of battery chargers as a function of accumulative dose.

0 20 40 60 80 100 120

50

55

60

65

70

75

Rev. voltage 200 V241Am - - 59.5 keV

4A - 20 kGy/h

CC

E (

%)

Dose (kGy)20 40 60 80 1000

500

1000

1500

2000

2500

3000

3500

Channel

Co

un

ts p

er

ch

an

ne

l

Channel

Dose:

0 kGy

2 kGy

24 kGy

40 kGy

86 kGy

120 kGy

Detector 4A2, Rev. voltage 200 V, t = 100 s, 241

Am - - 59.5 keV

dose rate 20 kGy/h

20 40 60 80 1001

10

100

1000

10000

Co

un

ts p

er

ch

an

ne

l

0 20 40 60 80 100 12015

20

25

30

35

40

Rev. voltage 200 V241Am - - 59.5 keV

4A - 20 kGy/h

FW

HM

(%

)

Dose (kGy)

GaAs detectors of ionizing radiation • Made by Slovak Academy of Sciences in

Bratislava, SK • Working in single photon counting mode • Prepared from 230 µm thick semi-insulating

GaAs. Top Schottky contact: circle: 1 mm, Ti/Pt/Au (10/35/90 nm) , Back ohmic contact: full-back-side, Ni/AuGe/Au (30/50/90 nm)

• Developed for digital imaging with X-ray tube and particle tracking in space and accelerators

Irradiation: By 5 MeV electrons, Beam repetition rate 10 Hz, scanning width 40 cm, steady mode, Doses obtained in 12 steps

28.4. 22.5. 5.6. 2.7. 18.8. 26.8.13.11.9.12. 19.1. 17.3. 27.4. 12.1.

0

20

40

60

80

100

120

2015

41

Dose (

kG

y)

date

2

2014

Accumulative dose applied to detectors:

9.12.9.12.9.12.12.12.12.12.15.1.16.1.20.1.27.1.29.1.29.1. 4.2. 27.2. 6.3.

0

200

400

600

800

1000

1200

1400

2015

5010

Dose (

Gy)

date

25

2014

Accumulative dose applied to electronic devices for skCUBE:

SI GaAs DETECTORS for digital radiation imaging

Detector charge collection efficiency (CCE) systematically decreases with applied dose.

Gradual degradation of relative energy resolution (FWHM) with accumulative dose in the range of doses of 24 up to 120 kGy.

.

Detector ability to measure spectra after radiation degradation.

0 2 4 6 8 10 12 14 160

1

2

3

4

5

6

Dose (

kG

y)

Material depth (mm)

GaAs

Si

5 MeV electrons

Dose-depth distribution in Si and GaAs

-20 -15 -10 -5 0 5 10 15 200

50

100

150

200

250

300

350

Dose (

kG

y)

Distance from the beam centre (cm)

distance from

acc. window:

y=10 cm

y=20 cm

y=30 cm

y=40 cm

y=55 cm

y=96 cm

Dose distribution perpendicular to beam scan

Results:

Irradiation