PHASE II ENVIRONMENTAL SUBSURFACE INVESTIGATION

PHASE II ENVIRONMENTAL SUBSURFACE INVESTIGATION

Prepared by:

EEA

55 Hilton Avenue, Garden City, New York 11510 Environmental Consultants To Industry And Government Since 1979

www.eeaconsultants.com

Prepared for:

MADISON REALTY CAPITAL 825 THIRD AVENUE, 37TH FLOOR

NEW YORK, NEW YORK 10022

55 ECKFORD STREET BROOKLYN, NEW YORK

Project No. 11734

DECEMBER 2011

Inc.


FOR PROPERTY LOCATED AT

55 ECKFORD STREET

BROOKLYN, NEW YORK

_____________________________________________________________________________

TABLE OF CONTENTS

Page

EXECUTIVE SUMMARY........................................................................ 1

I. INTRODUCTION .............................................................................. 5

II. SCOPE OF WORK PERFORMED ................................................ 6

a. Health and Safety Plan .................................................................. 6 b. Subsurface Utility Locations, Permits and Bonding................. 6

c. Investigative Work Summary ....................................................... 6

III. RESULTS OF LABORATORY ANALYSES ............................... 7

IV. FINDINGS ........................................................................................... 7

V. CONCLUSIONS ................................................................................. 9 VI. RECOMMENDATIONS ................................................................... 9

VII. SAMPLING METHODOLOGY...................................................... 10

a. Soil Sampling.................................................................................. 10 b. Quality Assurance and Quality Control Plan ........................... 10

VIII. QUALIFICATIONS ........................................................................... 10 IX. DISCLAIMER .................................................................................... 11

X. REFERENCES.................................................................................... 11

FIGURES: Figure 1: Site Location Plan Figure 1: Site and Sampling Plan

TABLES: Table 1: Soil Analytical Results: VOCs – B-1 through B-4

Table 2: Soil Analytical Results: VOCs – B-5 11’-12’, B-5 13’-15’, B-6 Table 3: Soil Analytical Results: VOCs – B-1 through B-4 Table 4: Soil Analytical Results: VOCs – B-5 11’-12’, B-5 13’-15’, B-6

Table 5: Soil Analytical Results: METALS Table 6: Groundwater Analytical Results: VOCs

Table 7: Groundwater Analytical Results: Metals (Filtered/Unfiltered)

APPENDIX: A. Site Photographs B. Chain-of-Custody Record C. Laboratory Analytical Report

D. Soil Boring Log Report

55 Eckford Street, Brooklyn, New York – Phase II - DRAFT 1 of 11


FOR PROPERTY LOCATED AT

55 ECKFORD STREET

BROOKLYN, NEW YORK _______________________________________________________________________________

Executive Summary

EEA, Inc. performed a Phase II Environmental Subsurface Investigation at 55 Eckford Street in the Brooklyn, New York to address Recognized Environmental Conditions (RECs) noted during EEA’s Phase I Environmental Site Assessment (ESA #11306) of the same property

(dated November 2011). The subject property contained a partially completed development consisting of a six-story building structure of support beams and flooring. The location of the subject property is shown on Figure 1.

The following two (2) Recognized Environmental Conditions (RECs) were noted during EEA’s 2011 Phase I site inspection and were addressed as part of this Phase II Environmental Subsurface Investigation:

Former On-site Hazardous Waste Generation

From approximately 1942-2007, the subject property was occupied by an electroplating facility which is listed as a USEPA Hazardous Waste Generator (USEPA Facility Id:

NYD001236017) associated with the storage, generation and/or use of the following hazardous wastes: solid waste that exhibits the characteristics of corrosivity and reactivity, Mercury, wastewater treatment sludges from electroplating operations, Spent cyanide plating bath solutions from electroplating operations, Zinc cyanide, Arsenic, Spent non-halogenated solvents,

and plating bath residues from the bottom of plating baths.

In addition, a lacquer spray finishing facility was also formerly present on the subject property during the same time period. This former spray facility was also likely associated with

the generation, storage and/or use of solvents used during spraying operations. It should also be noted that the subject property was identified in the NYSDEC Chemical Bulk Storage (CBS) database for the following: a “closed”, 500 gallon aboveground tank containing sodium hypochlorite.

Adjacent Hazardous Waste Generation From approximately 1965-present, the adjacent/contiguous property to the north, Carter

Spray Finishing, is/was occupied by a metal finishing facility, which is listed as a USEPA Hazardous Waste Generator associated with the storage, generation and/or use of hazardous wastes such as spent halogenated and non-halogenated solvents. In addition, this same property was identified on the Chemical Bulk Storage (CBS) database for the following: two (2) “closed”

275 gallon aboveground tanks containing trichloroethene.


Findings Soil Conditions

Based upon visual, olfactory and PID screening analysis, borings B-1 and B-3 through B-

6, contained strong solvent odors, grey staining and PID readings ranging from 129-1085 ppm, at or in close proximity to the groundwater interface.

According to analytical laboratory results, the VOC sec-Butylbenzene, was detected at

levels exceeding NYSDEC CP-51 guidelines in soil obtained from boring B-4. In addition, the following SVOCs were detected at levels above NYSDEC CP-51 and Brownfield Part 375

Restricted Use Residential Guidelines in sample B-5 11’-12’: Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Chrysene. Finally, several Metals were detected at levels above NYSDEC guidelines in all soil samples collected including: Arsenic, Lead, Mercury and Selenium.

It should be noted that VOC and SVOC analytical results of soil samples obtained from

borings B-1 and B-3 through B-6, depict raised laboratory report limits due to interference caused by the presence of target and non-target list compounds in each sample. Furthermore,

soil samples collected for laboratory analysis from borings B-1 and B-4 contained the highest reporting limits in addition to the highest PID readings observed during the Phase II Investigation. Lastly, many of these raised reporting limits are above NYSDEC CP-51 guidelines and indicate the presence of unknown contaminants present in soil.

Groundwater Conditions The table below represents VOC compounds detected in groundwater samples at concentrations above NYSDEC TOGs 1.1.1 Guidelines:

VOC Samples above TOGS 1.1.1 Guidelines

2-Isopropyltoluene B-1GW, B-4GW, B-6GW

Isopropylbenzene B-1GW, B-4GW

Sec-Butylbenzene B-1GW, B-4GW

Tert-Butylbenzene B-1GW, B-4GW, B-6GW n-Butylbenzene B-4GW

The table below represents metals detected in unfiltered groundwater samples at concentrations above NYSDEC TOGs 1.1.1 Guidelines:

Metal Samples above TOGs Guidelines

Arsenic B-1GW, B-2GW, B-4GW, B-6GW

Barium B-1GW, B-2GW, B-4GW, B-6GW

Chromium B-1GW, B-2GW, B-4GW, B-6GW

Lead B-1GW, B-2GW, B-4GW, B-6GW

Mercury B-1GW Selenium B-1GW, B-2GW, B-4GW, B-6GW


The table below represents metals detected in filtered groundwater samples at concentrations above NYSDEC TOGs 1.1.1 Guidelines:

Metal Samples above TOGs Guidelines Arsenic B-2GW and B-4GW

Lead B-1GW, B-2GW and B-4GW

Selenium B-1GW, B-2GW, B-4GW, B-6GW

As depicted in tables above, six (6) metals were detected in unfiltered groundwater

samples, and three (3) metals in filtered groundwater samples, at concentrations exceeding their respective NYSDEC TOGS 1.1.1 GQS. Barium, Chromium and Mercury were not detected in filtered groundwater samples; furthermore, the high levels of Barium, Chromium and Mercury in unfiltered samples are the result of the affinity of these metals to adhere to suspended soil

particles present in groundwater. However, it should be noted that filtered groundwater sample results show that Arsenic, Lead and Selenium are present in the groundwater at levels above NYSDEC Guidelines revealing that metals have dissolved in and contaminated on-site groundwater.

Conclusions Based upon analysis of laboratory and field data, the subject property soils are

contaminated with VOCs and SVOCs and groundwater is contaminated with VOCs. The presence of these VOCs and SVOCs are due to releases from the lacquer spray facility once present on the subject property. Furthermore, the following four (4) VOCs detected at levels above guidelines in groundwater are typically used as coating agents or thinners in lacquer

applying applications: sec-Butylbenzene, 2-isopropyltoluene, Isopropylbenzene, and tert-Butylbenzene.

Based upon analysis of laboratory and field data, the subject property soils and

groundwater are contaminated with Metals. These contaminants are due to releases from the electroplating facility once present on the subject property. Furthermore, such metals as Mercury and Arsenic were listed as past hazardous wastes produced at the subject property and were detected above regulatory guidelines in soil and unfiltered groundwater (arsenic also found

above guidelines in filtered groundwater).

Recommendations REPORTING REQUIREMENTS

Results of this Phase II Investigation depict the presence of contaminants due to past releases/spills from the electroplating and lacquer spraying facility once present on the subject property. Federal and State law require that appropriate government agencies be notified of any spilled/contaminated materials found on a property upon their discovery. EEA recommends that

this report is forwarded to the NYSDEC for review and comment prior to any further investigation or remedial action.


The NYSDEC considers each property investigation findings on a case-by-case basis in consideration of the history and surrounding neighborhood property use and its location to sensitive human, wildlife and environmental interests. Industrial and commercial pr operties may be treated

differently than residential or environmentally sensitive areas.

*The NYSDEC will likely require additional testing and remediation of this property.

If there are any questions regarding the findings of this report please contact us.

PROJECT MANAGER:

Sean Martin Sean Martin

Project Geologist

Phase II Environmental Subsurface Investigations REVIEWER:

Nicholas Recchia Nicholas J. Recchia, P.G. Vice President

Senior Hydrogeologist


I. INTRODUCTION

EEA, Inc. performed a Phase II Environmental Subsurface Investigation at 55 Eckford

Street in the Brooklyn, New York to address Recognized Environmental Conditions (RECs) noted during EEA’s Phase I Environmental Site Assessment (ESA #11306) of the same property (dated November 2011). The subject property contained a partially completed development consisting of a six-story building structure of support beams and flooring. The location of the

subject property is shown on Figure 1. The following two (2) Recognized Environmental Conditions (RECs) were noted during

EEA’s 2011 Phase I site inspection and were addressed as part of this Phase II Environmental

Subsurface Investigation: Former On-site Hazardous Waste Generation

From approximately 1942-2007, the subject property was occupied by an electroplating facility which is listed as a USEPA Hazardous Waste Generator (USEPA Facility Id: NYD001236017) associated with the storage, generation and/or use of the following hazardous wastes: solid waste that exhibits the characteristics of corrosivity and reactivity, Mercury,

wastewater treatment sludges from electroplating operations, Spent cyanide plating bath solutions from electroplating operations, Zinc cyanide, Arsenic, Spent non-halogenated solvents, and plating bath residues from the bottom of plating baths.

In addition, a lacquer spray finishing facility was also formerly present on the subject property during the same time period. This former spray facility was also likely associated with the generation, storage and/or use of solvents used during spraying operations. It should also be noted that the subject property was identified in the NYSDEC Chemical Bulk Storage (CBS)

database for the following: a “closed”, 500 gallon aboveground tank containing sodium hypochlorite. Adjacent Hazardous Waste Generation

From approximately 1965-present, the adjacent/contiguous property to the north, Carter Spray Finishing, is/was occupied by a metal finishing facility, which is listed as a USEPA Hazardous Waste Generator associated with the storage, generation and/or use of hazardous

wastes such as spent halogenated and non-halogenated solvents. In addition, this same property was identified on the Chemical Bulk Storage (CBS) database for the following: two (2) “closed” 275 gallon aboveground tanks containing trichloroethene.

EEA, Inc. performed this Phase II Environmental Subsurface Investigation to determine the soil and groundwater quality at the subject property and address the aforementioned RECs identified in EEA’s 2011 Phase I ESA. EEA initiated field activities on December 3, 2011 and completed the field investigation by this date. The photographs of the work performed are

presented in the Appendix A to this report. This report summarizes the work performed, the results of the investigation, and the recommendations.


II. SCOPE OF WORK PERFORMED

a. Health and Safety P lan

EEA uses a company Generic Health and Safety P lan for all investigative work relating

to performing Phase II Environmental Subsurface Investigations. The HASP assigns responsibilities, establishes personal protection standards, recommends operating procedures,

and provides for contingencies that may arise during performance of the assessment at the site. The protocols in the HASP apply to all personnel involved in the work activities including EEA, all outside subcontractors, client, or regulatory agencies present during the performance of the work. In addition, the following safety equipment is maintained on-site for responding to

potential emergency situations: portable eyewash, ABC fire extinguisher, and first aid kit. Telephone numbers of emergency response units in the area are also posted where all those working at the site can easily see them. All personnel working at the site will also be required to receive training in respirator fitting, emergency procedures, equipment decontamination and

specific task procedures. All personnel involved with the collection of soil or water will have successfully completed the 40-hour OSHA Hazardous Materials Training Program.

b. Subsurface Utility Location, Permits and Bonding

EEA notified DigNet New York under the New York State Regulation Code 753 prior to

initiating the work to identify the location of underground utilities in the vicinity of the proposed boring locations. Any permits for soil boring were obtained from the local agencies. In addition,

any license and permit bonding required was secured for the work. c. Investigation Work Summary

On December 3, 2011, EEA conducted a Phase II Subsurface Investigation at the subject property. Six (6) borings were advanced on the subject property, using a Geoprobe Model 54LT rig, in order to determine if former electroplating and lacquer spraying operations at the subject property impacted property soils and groundwater.

All borings were advanced until groundwater was encountered, which ranged between 7-13 feet below grade, depending on surface elevation. Soil samples were collected from 0-4 foot depth intervals from each boring and were screened using visual, olfactory and PID screening

techniques. The soil sample exhibiting the highest PID reading was selected for laboratory analysis. Temporary screened PVC piping was inserted into all six (6) borings on-site and with the

intent to collect groundwater. However, borings B-3 and B-5 did not produce enough water to sample due to silty soils encountered at these locations. Therefore, only four (4) groundwater samples were collected (B-1GW, B-2GW, B-4GW and B-6GW). It should be noted that in soil boring B-3, the soil sample yielding the highest PID reading was collected near the groundwater

interface (9’–11’ below grade). In regards to soil boring B-5, the soil sample yielding the highest PID reading was collected at approximately 11’ below grade, which was above the groundwater


interface; however, an additional soil sample was collected from this boring at the groundwater interface (approximately 13’ below grade) since a groundwater sample could not be collected.

III. RESULTS OF LABORATORY ANALYSES EcoTest Laboratories, Inc., (NYSDOH #10320) prepared the results of soil samples,

which were analyzed for contaminants using USEPA methods 8260 VOCs, 8270 SVOC BN only and RCRA Metals. Tables 1 to 5 represent a comparison of the soil sampling results, obtained from on-site borings, as compared to NYSDEC CP-51 guidelines and NYSDEC Part 375 Restricted Use Residential Guidelines.

EcoTest Laboratories, Inc., also prepared the results of groundwater samples, which were

analyzed for contaminants using USEPA methods 8260 VOCs, and RCRA Metals (Filtered/ Unfiltered). Tables 6 and 7 represent a comparison of the groundwater sampling results

obtained from on-site borings, as compared to NYSDEC TOGS 1.1.1 guidelines. The chain-of-custody records, as well as the analytical laboratory data sheets, are

presented in the Appendix B and C to this report, respectively.

IV. FINDINGS

Soil Conditions

As previously mentioned, six (6) borings (B-1 through B-6) were advanced on-site until groundwater depth. Based upon visual, olfactory and PID screening analysis, borings B-1 and

B-3 through B-6, contained strong solvent odors, grey staining and elevated PID readings at or in close proximity to the groundwater interface. The table below depicts the highest PID readings encountered in each soil sample and corresponding information (i.e., depth of reading, boring location, water table depth).

Boring Highest PID reading Depth of reading (ft) Groundwater Depth (ft) B-1 1085 12 12

B-2 0.0 NA* 12

B-3 129 8 8

B-4 1030 11 7

B-5 389 10 13

B-6 400 13 13 *NA = Not Applicable

According to analytical laboratory results, the VOC sec-Butylbenzene, was detected at

levels exceeding NYSDEC CP-51 guidelines in soil obtained from boring B-4. In addition, the following SVOCs were detected at levels above NYSDEC CP-51 and Brownfield Part 375

Restricted Use Residential Guidelines in sample B-5 11’-12’: Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Chrysene.


It should be noted that VOC and SVOC analytical results of soil samples obtained from borings B-1 and B-3 through B-6, depict raised laboratory report limits due to interference caused by the presence of target and non-target list compounds in each sample. Furthermore,

soil samples collected for laboratory analysis from borings B-1 and B-4 contained the highest reporting limits in addition to the highest PID readings observed during the Phase II Investigation. Lastly, many of these raised reporting limits are above NYSDEC CP -51 guidelines and indicate the presence of unknown contaminants present in soil.

The table below depicts metals detected in soil samples at concentrations above

NYSDEC Guidelines:

Metal Samples above CP-51 Samples above Residential Use Arsenic B-1, B-2, B-3, B-6 B-2, B-3, and B-6

Lead B-1 through B-6 B-1, B-2, B-3, B-5 13’-15’, B-6

Mercury B-1 through B-6 B-1, B-3 and B-4

Selenium B-1 and B-3 None

Groundwater Conditions

The table below depicts VOC compounds detected in groundwater samples at concentrations above NYSDEC TOGs 1.1.1 Guidelines:

VOC Samples above TOGS 1.1.1 Guidelines

2-Isopropyltoluene B-1GW, B-4GW, B-6GW

Isopropylbenzene B-1GW, B-4GW

Sec-Butylbenzene B-1GW, B-4GW

Tert-Butylbenzene B-1GW, B-4GW, B-6GW

n-Butylbenzene B-4GW

The table below depicts metals detected in unfiltered groundwater samples at concentrations above NYSDEC TOGs 1.1.1 Guidelines:


Arsenic B-1GW, B-2GW, B-4GW, B-6GW

Barium B-1GW, B-2GW, B-4GW, B-6GW

Chromium B-1GW, B-2GW, B-4GW, B-6GW

Lead B-1GW, B-2GW, B-4GW, B-6GW

Mercury B-1GW


The table below depicts metals detected in filtered groundwater samples at concentrations above NYSDEC TOGs 1.1.1 Guidelines:


Arsenic B-2GW and B-4GW

Lead B-1GW, B-2GW and B-4GW



As depicted in tables above, six (6) metals were detected in unfiltered groundwater samples, and three (3) metals in filtered groundwater samples, at concentrations exceeding their respective NYSDEC TOGS 1.1.1 GQS. Barium, Chromium and Mercury were not detected in

filtered groundwater samples; furthermore, the high levels of Barium, Chromium and Mercury in unfiltered samples are the result of the affinity of these metals to adhere to suspended soil particles present in groundwater. However, it should be noted that filtered groundwater sample results show that Arsenic, Lead and Selenium are present in the groundwater at levels above

NYSDEC Guidelines revealing that metals have dissolved in and contaminated on-site groundwater.

V. CONCLUSIONS Based upon analysis of laboratory and field data, the subject property soils are

contaminated with VOCs and SVOCs and groundwater is contaminated with VOCs. The

presence of these VOCs and SVOCs are due to releases from the lacquer spray facility once present on the subject property. Furthermore, the following four (4) VOCs detected at levels above guidelines in groundwater are typically used as coating agents or thinners in lacquer applying applications: sec-Butylbenzene, 2-isopropyltoluene, Isopropylbenzene, and tert-

Butylbenzene. Based upon analysis of laboratory and field data, the subject property soils and

groundwater are contaminated with Metals. These contaminants are due to releases from the

electroplating facility once present on the subject property. Furthermore, such metals as Mercury and Arsenic were listed as past hazardous wastes produced at the subject property and were detected above regulatory guidelines in soil and unfiltered groundwater (arsenic also found above guidelines in filtered groundwater).

VI. RECOMMENDATIONS

Results of this Phase II Investigation depict the presence of contaminants due to past releases/spills from the electroplating and lacquer spraying facility once present on the subject property. Federal and State law require that appropriate government agencies be notified of any spilled/contaminated materials found on a property upon their discovery. EEA recommends that

this report is forwarded to the NYSDEC for review and comment prior to any further investigation or remedial action.

The NYSDEC considers each property investigation findings on a case-by-case basis in

consideration of the history and surrounding neighborhood property use and its location to sensitive human, wildlife and environmental interests. Industrial and commercial properties may be treated differently than residential or environmentally sensitive areas.

*The NYSDEC will likely require additional testing and remediation of this property.


VII. SAMPLING METHODOLOGY

a. Soil Sampling

Soil samples were collected with a Geoprobe drill rig, were visually inspected and field screened using a portable Photo ionization detector (MiniRae 3000 10.6 ev lamp) for evidence of impacted soils. The selected soil/groundwater sample was placed in a laboratory pre-cleaned sample

jar which was then placed in a cooler and chilled to a temperature of 4 degrees C in accordance with standard operating procedures. A Chain of Custody form was completed at the time of sampling.

b. Quality Assurance and Quality Control QA/QC Plan

EEA implements a QA/QC Plan to ensure sample integrity and avoid contamination and/or cross-contamination of samples. All sampling equipment is cleaned before each sample is collected. The following procedures are followed in the decontamination process:

Step 1: Steam clean equipment. Step 2: Scrub with a bristle brush using a non-phosphate detergent (such as Alconox).

Step 3: Rinse with hot tap water. Step 4: Rinse twice with deionized water. Step 5: Air dry. Step 6 Nitric Acid (5%) solution rinse (if sampling for metals)

Step 7: Rinse twice with deionized water. Step 8: Air dry

VIII. QUALIFICATIONS

EEA, Inc. is an environmental consulting firm that has undertaken environmental pollution investigations, development feasibility studies, and environmental site assessment

studies since 1979. These site evaluation studies have been prepared for major lenders, public corporations, businesses, developers and governmental agencies. Approximately 4,000 parcels have been evaluated in the metropolitan New York-New Jersey area during the past twenty years, ranging from Phase I Environmental Site Assessments to comprehensive subsurface

hazardous material investigations and testing programs. EEA also prepares bid specifications for remedial cleanup actions and supervises site cleanup.

EEA’s principals and senior managers for the hazardous waste investigations each have

over 20 years experience in environmental consulting, with established credentials in the field. Individual qualifications of EEA personnel, including specific credentials of persons involved in the preparation of this report can be provided upon request.


IX. DISCLAIMER This report is for use by Madison Realty Capital and its successors and/or assigns and is

only to be used as a guide in determining the potential for contamination by toxic or hazardous materials on the subject property at the time of the site visit. This Phase II Environmental Subsurface Investigation was undertaken in accordance with generally accepted protocols, including ASTM Standards Related to the Phase II Environmental Site Assessment Process.

This Phase II Investigation is based principally on the review of historic and regulatory records (made available within a reasonable time period), relating to past occupants and usage of the subject property, as well as activities at nearby sites, and upon a visual assessment of the subject property, and makes no determinations with respect to portions of the subject property and its

structures which were not inspected. Our professional services have been performed using that degree of care and skill ordinarily exercised under similar circumstances by reputable qualified professionals practicing in this or similar situations. The interpretation of the field data is based on good judgment and experience. However, no matter how qualified the professional or

detailed the investigation, subsurface conditions cannot always be predicted beyond the points of actual sampling and testing. No other warranty, expressed or implied, is made to the professional advice included in this report.

Any and all liability on the part of EEA, Inc. shall be limited solely to EEA’s professiona l liability insurance (errors and omissions coverage of one million dollars). EEA, Inc. shall have no liability for any other damages, whether consequential, compensatory, punitive, or special, arising out of, incidental to, or as a result of, this assessment. EEA, Inc. assumes no liability for

the use of this report by any person or entity other than the institution and/or entities or persons for whom it has been prepared.

X. REFERENCES 1. NYSDEC Bureau of Spill Prevention & Response Sampling Guidelines and Protocols, March

1991.

2. DER-10 Technical Guidance for Site Investigation and Remediation, Date Issued May 3,

2010.

3. EEA’s Phase I Environmental Site Assessment ESA 11306 dated November 2011.

FIGURES

Subject Property Location USGS Topographic Map (Brooklyn Quad) Figure 1

55-63 Eckford Street Brooklyn, New York

B-1/B-1GW

B-2/B-2GW

B-5 B-6/B-6GW

B-4/B-4GW

ECK

FOR

D

S

TREE

T

B-3

Former Electro-plating Facility

Former Lacquer Spraying Facility

B-1/B-1GW - Soil Boring/ Groundwater Sample Location

Legend

Property Boundary

EEA, Inc.

55 Hilton Avenue

Garden City, New York

(516) 746-4400

Property Located at:

55 Eckford Street,

Brooklyn, NY 11222

SAMPLE COLLECTION

LOCATIONS

Figure 2

TABLES

Sample Identification S-1 S-2 S-3 S-4Boring Number B-1 B-2 B-3 B-4Sample Depth 12-14 feet 11-13 feet 9-11 feet 11-12 feetSample Date 12/3/2011 12/3/2011 12/3/2011 12/3/2011

Sample Matrix Soil Soil Soil SoilUnits ug/kg ug/kg ug/kg ug/kg

1,1,1,2-Tetrachloroethane <1800 <5.7 <300 <1500 NS NS1,1,1-Trichloroethane <1800 <5.7 <300 <1500 680 100,0001,1,2,2-Tetrachloroethane <1800 <5.7 <300 <1500 NS NS1,1,2-Trichloroethane <1800 <5.7 <300 <1500 NS NS1,1-Dichloroethane <1800 <5.7 <300 <1500 270 19,0001,1-Dichloroethene <1800 <5.7 <300 <1500 330 100,0001,1-Dichloropropene <1800 <5.7 <300 <1500 NS NS1,2,3-Trichlorobenzene <1800 <5.7 <300 <1500 NS NS1,2,3-Trichloropropane <1800 <5.7 <300 <1500 NS NS1,2,4-Trichlorobenzene <1800 <5.7 <300 <1500 3,600 NS1,2,4-Trimethylbenzene <1800 <5.7 <300 <1500 NS NS1,2-Dibromo-3-chloropropane <1800 <5.7 <300 <1500 NS NS1,2-Dichlorobenzene <1800 <5.7 <300 <1500 1,100 1,1001,2-Dichloroethane <1800 <5.7 <300 <1500 20 23001,2-Dichloropropane <1800 <5.7 <300 <1500 NS NS1,3,5-Trimethylbenzene <1800 <5.7 <300 <1500 8,400 NS1,3-Dichlorobenzene <1800 <5.7 <300 <1500 2,400 NS1,3-Dichloropropane <1800 <5.7 <300 <1500 NS NS1,4-Dichlorobenzene <1800 <5.7 <300 <1500 1,800 9,8002,2-Dichloropropane <1800 <5.7 <300 <1500 NS NS2-Chlorotoluene <1800 <5.7 <300 <1500 NS NS2-Hexanone <9100 <29 <1500 <7400 NS NS2-Isopropyltoluene <1800 <5.7 550 10000 NS NS4-Chlorotoluene <1800 <5.7 <300 <1500 NS NS4-Methyl-2-Pentanone (MIBK) <9100 <29 <1500 <7400 NS NSAcetone <9100 <29 <1500 <7400 50 100,000Acrylonitrile <3600 <11 <610 <3000 NS NSBenzene <1800 <5 7 <300 <1500 60 2900

Table 1Soil Samples Volatile Organic Analytical Results

55 Eckford Street, Brooklyn, New York

NYSDEC CP-51 Cleanup

Guidelines

NYSDEC Brownfield’s Part

375-6.8(a) Restricted Use Resdential Soil Cleanup Objectives

Volatile Organic Compounds (µg/kg) - EPA Method 8260

Benzene <1800 <5.7 <300 <1500 60 2900Bromobenzene <1800 <5.7 <300 <1500 NS NSBromochloromethane <1800 <5.7 <300 <1500 NS NSBromodichloromethane <1800 <5.7 <300 <1500 NS NSBromoform <1800 <5.7 <300 <1500 NS NSBromomethane <1800 <5.7 <300 <1500 NS NSCarbon Disulfide <1800 <5.7 <300 <1500 NS 100,000Carbon Tetrachloride <1800 <5.7 <300 <1500 760 1,400Chlorobenzene <1800 <5.7 <300 <1500 1,100 100,000Chloroethane <1800 <5.7 <300 <1500 NS NSChloroform <1800 <5.7 <300 <1500 370 100,000Chloromethane <1800 <5.7 <300 <1500 NS NScis-1,2-Dichloroethene <1800 <5.7 <300 <1500 250 59,000cis-1,3-Dichloropropene <1800 <5.7 <300 <1500 NS NSDibromochloromethane <1800 <5.7 <300 <1500 NS NSDibromoethane <1800 <5.7 <300 <1500 NS NSDibromomethane <1800 <5.7 <300 <1500 NS NSDichlorodifluoromethane <1800 <5.7 <300 <1500 NS NSEthylbenzene <1800 <5.7 <300 <1500 1,000 30,000Hexachlorobutadiene <1800 <5.7 <300 <1500 330 NSIsopropylbenzene <1800 <5.7 <300 <1500 NS NSm&p-Xylene <1800 <5.7 <300 <1500 NS NS


Sample Matrix Soil Soil Soil SoilUnits ug/kg ug/kg ug/kg ug/kg

Methyl Ethyl Ketone <9100 <29 <1500 <7400 120 100,000Methyl t-Butyl Ether (MTBE) <3600 <11 <610 <3000 930 62,000Methylene Chloride <1800 <29 <300 <1500 50 51,000Naphthalene <1800 <5.7 <300 <1500 NS NSn-Butylbenzene <1800 <5.7 <300 5500 NS NSn-Propylbenzene <1800 <5.7 <300 <1500 3,900 100,000o-Xylene <1800 <5.7 <300 <1500 NS NSp-Isopropyltoluene <1800 <5.7 <300 <1500 NS NSsec-Butylbenzene 5500 <5.7 730 20000 11,000 100,000Styrene <1800 <5.7 <300 <1500 NS NStert-Butylbenzene 2300 <5.7 <300 4500 5,900 100,000Tetrachloroethene <1800 <5.7 <300 <1500 1,300 5,500Tetrahydrofuran (THF) <3600 <11 <610 <3000 NS NSToluene <1800 <5.7 <300 <1500 700 100,000Total Xylenes <1800 <5.7 <300 <1500 260 100,000trans-1,2-Dichloroethene <1800 <5.7 <300 <1500 190 100,000trans-1,3-Dichloropropene <1800 <5.7 <300 <1500 NS NStrans-1,4-dichloro-2-butene <3600 <11 <610 <3000 NS NSTrichloroethene <1800 <5.7 <300 <1500 470 100,000Trichlorofluoromethane <1800 <5.7 <300 <1500 NS NSTrichlorotrifluoroethane <1800 <5.7 <300 <1500 NS NSVinyl Chloride <1800 <5.7 <300 <1500 20 210

ug/kg…micrograms per kilogramBold values indicate concentrations exceeding laboratory method detection limits.

Shaded values indicate concentrations above NYSDEC Brownfield Unresticted Use Guidelines.

NS : No Standard

Table 1 (Cont'd)Soil Samples Volatile Organic Analytical Results



Guidelines




Sample Identification S-5 S-6 S-7Boring Number B-5 B-5 B-6Sample Depth 11-12 feet 13-15 feet 13-15 feetSample Date 12/3/2011 12/3/2011 12/3/2011

Sample Matrix Soil Soil SoilUnits ug/kg ug/kg ug/kg

1,1,1,2-Tetrachloroethane <290 <340 <310 NS NS1,1,1-Trichloroethane <290 <340 <310 680 100,0001,1,2,2-Tetrachloroethane <290 <340 <310 NS NS1,1,2-Trichloroethane <290 <340 <310 NS NS1,1-Dichloroethane <290 <340 <310 270 19,0001,1-Dichloroethene <290 <340 <310 330 100,0001,1-Dichloropropene <290 <340 <310 NS NS1,2,3-Trichlorobenzene <290 <340 <310 NS NS1,2,3-Trichloropropane <290 <340 <310 NS NS1,2,4-Trichlorobenzene <290 <340 <310 3,600 NS1,2,4-Trimethylbenzene <290 <340 <310 NS NS1,2-Dibromo-3-chloropropane <290 <340 <310 NS NS1,2-Dichlorobenzene <290 <340 <310 1,100 1,1001,2-Dichloroethane <290 <340 <310 20 23001,2-Dichloropropane <290 <340 <310 NS NS1,3,5-Trimethylbenzene <290 <340 <310 8,400 NS1,3-Dichlorobenzene <290 <340 <310 2,400 NS1,3-Dichloropropane <290 <340 <310 NS NS1,4-Dichlorobenzene <290 <340 <310 1,800 9,8002,2-Dichloropropane <290 <340 <310 NS NS2-Chlorotoluene <290 <340 <310 NS NS2-Hexanone <1500 <1700 <1600 NS NS2-Isopropyltoluene 1400 2200 790 NS NS4-Chlorotoluene <290 <340 <310 NS NS4 M th l 2 P t (MIBK) <1500 <1700 <1600 NS NS

Table 2 Soil Samples Volatile Organic Analytical Results



Guidelines




4-Methyl-2-Pentanone (MIBK) <1500 <1700 <1600 NS NSAcetone <1500 <1700 <1600 50 100,000Acrylonitrile <580 <680 <630 NS NSBenzene <290 <340 <310 60 2900Bromobenzene <290 <340 <310 NS NSBromochloromethane <290 <340 <310 NS NSBromodichloromethane <290 <340 <310 NS NSBromoform <290 <340 <310 NS NSBromomethane <290 <340 <310 NS NSCarbon Disulfide <290 <340 <310 NS 100,000Carbon Tetrachloride <290 <340 <310 760 1,400Chlorobenzene <290 <340 <310 1,100 100,000Chloroethane <290 <340 <310 NS NSChloroform <290 <340 <310 370 100,000Chloromethane <290 <340 <310 NS NScis-1,2-Dichloroethene <290 <340 <310 250 59,000cis-1,3-Dichloropropene <290 <340 <310 NS NSDibromochloromethane <290 <340 <310 NS NSDibromoethane <290 <340 <310 NS NSDibromomethane <290 <340 <310 NS NSDichlorodifluoromethane <290 <340 <310 NS NSEthylbenzene <290 <340 <310 1,000 30,000Hexachlorobutadiene <290 <340 <310 330 NSIsopropylbenzene <290 <340 <310 NS NSm&p-Xylene <290 <340 <310 NS NS


Sample Matrix Soil Soil SoilUnits ug/kg ug/kg ug/kg

Methyl Ethyl Ketone <1500 <1700 <1600 120 100,000Methyl t-Butyl Ether (MTBE) <580 <680 <630 930 62,000Methylene Chloride <290 <340 <310 50 51,000Naphthalene <290 <340 <310 NS NSn-Butylbenzene 370 910 <310 NS NSn-Propylbenzene <290 <340 <310 3,900 100,000o-Xylene <290 <340 <310 NS NSp-Isopropyltoluene <290 <340 <310 NS NSsec-Butylbenzene 1300 2800 350 11,000 100,000Styrene <290 <340 <310 NS NStert-Butylbenzene 560 1500 780 5,900 100,000Tetrachloroethene <290 <340 <310 1,300 5,500Tetrahydrofuran (THF) <580 <680 <630 NS NSToluene <290 <340 <310 700 100,000Total Xylenes <290 <340 <310 260 100,000trans-1,2-Dichloroethene <290 <340 <310 190 100,000trans-1,3-Dichloropropene <290 <340 <310 NS NStrans-1,4-dichloro-2-butene <580 <680 <630 NS NSTrichloroethene <290 <340 <310 470 100,000Trichlorofluoromethane <290 <340 <310 NS NSTrichlorotrifluoroethane <290 <340 <310 NS NSVinyl Chloride <290 <340 <310 20 210

Table 2 (Cont'd)Soil Samples Volatile Organic Analytical Results



Guidelines




NS : No Standardug/kg…micrograms per kilogramBold values indicate concentrations exceeding laboratory method detection limits.


Sample Matrix Soil Soil Soil Soil

Units ug/kg ug/kg ug/kg ug/kg

1,2 Dichlorobenzene(sv) <1700 <260 <280 <1400 NG NG



2,4-Dinitrotoluene <1700 <260 <280 <1400 NG NG

2,6-Dinitrotoluene <1700 <260 <280 <1400 NG NG

2-Chloronaphthalene <1700 <260 <280 <1400 NG NG

2-Methylnaphthalene <1700 <260 <280 <1400 NG NG

2-Nitroaniline <7000 <1100 <1200 <5700 NG NG

3,3'-Dichlorobenzidine <9600 <1500 <1600 <7800 NG NG


4-Bromophenyl phenyl ether <1700 <260 <280 <1400 NG NG

4-Chloroaniline <1700 <260 <280 <1400 NG NG

4-Chlorophenyl phenyl ether <1700 <260 <280 <1400 NG NG


Acenaphthene <1700 <260 <280 <1400 20,000 100,000Acenaphthylene <1700 <260 <280 <1400 100,000 100,000Anthracene <1700 <260 <280 <1400 100,000 100,000Azobenzene <1700 <260 <280 <1400 NG NG

Benzo(a)anthracene <1700 <260 510 <1400 1,000 1,000Benzidine <9600 <1500 <1600 <7800 NG NG

Table 3Soil Samples Semi-Volatile Organic Analytical Results



Guidelines


375-6.8(b) Residential Use Soil Cleanup Objectives

Semi-Volatile Organic Compounds (µg/kg) - EPA Method 8270

Benzo(a)pyrene <1700 <260 470 <1400 1,000 1,000Benzo(b)fluoranthene <1700 <260 570 <1400 1,000 1,000Benzo(ghi)perylene <1700 <260 300 <1400 100,000 100,000Benzo(k)fluoranthene <1700 <260 <280 <1400 800 1,000Benzoic acid <2400 <370 <400 <2000 NG NGBenzyl alcohol <1700 <260 <280 <1400 NG NGBenzyl butyl phthalate <1700 <260 <280 <1400 NG 100,000Bis(2-chloroethoxy)methane <1700 <260 <280 <1400 NG NGBis(2-chloroethyl)ether <1700 <260 <280 <1400 NG NGBis(2-chloroisopropyl)ether <1700 <260 <280 <1400 NG NGBis(2-ethylhexyl)phthalate <1700 <260 <280 <1400 NG NGChrysene <1700 <260 450 <1400 1,000 1,000Dibenzo(a,h)anthracene <1700 <260 <280 <1400 330 1,000Dibenzofuran <1700 <260 <280 <1400 NG NGDiethyl Phthalate <1700 <260 <280 <1400 NG NGDimethyl Phthalate <1700 <260 <280 <1400 NG NGDi-n-Butyl Phthalate <1700 <260 <280 <1400 NG NGDi-n-octyl Phthalate <1700 <260 <280 <1400 NG NGFluoranthene <1700 <260 1200 <1400 100,000 100,000Fluorene <1700 <260 <280 <1400 30,000 100,000Hexachlorobenzene <1700 <260 <280 <1400 NG 100,000Hexachlorobutadiene <1700 <260 <280 <1400 NG NG

Sample Identification S-1 S-2 S-3 S-4

Boring Number B-1 B-2 B-3 B-4

Sample Depth 12-14 feet 11-13 feet 9-11 feet 11-12 feet

Sample Date 12/3/2011 12/3/2011 12/3/2011 12/3/2011

Sample Matrix Soil Soil Soil Soil

Units ug/kg ug/kg ug/kg ug/kg

Hexachlorocyclopentadiene <1700 <260 <280 <1400 NG NGHexachloroethane <1700 <260 <280 <1400 NG NGIndeno(1,2,3-cd)pyrene <1700 <260 <280 <1400 500 500Isophorone <1700 <260 <280 4200 NG 500Naphthalene(sv) <1700 <260 <280 <1400 12,000 100,000Nitrobenzene <1700 <260 <280 <1400 NG NGN-Nitrosodimethylamine <1700 <260 <280 <1400 NG NGN-Nitrosodi-n-propylamine <1700 <260 <280 <1400 NG NGN-Nitrosodiphenylamine <1700 <260 <280 <1400 NG NGPhenanthrene <1700 <260 680 <1400 100,000 100,000Pyrene <1700 <260 1200 <1400 100,000 100,000

ug/kg…micrograms per kilogram

Note: The MS and MSD sample results are displayed; however, these results were not compared to NYSDEC guildeines.

NS : No Standard

Table 3 (Cont'd)Soil Samples Semi-Volatile Organic Analytical Results



Guidelines





Sample Matrix Soil Soil Soil

Units ug/kg ug/kg ug/kg

1,2 Dichlorobenzene(sv) <1300 <310 <290 NG NG



2,4-Dinitrotoluene <1300 <310 <290 NG NG

2,6-Dinitrotoluene <1300 <310 <290 NG NG

2-Chloronaphthalene <1300 <310 <290 NG NG

2-Methylnaphthalene <1300 <310 <290 NG NG

2-Nitroaniline <5500 <1300 <1200 NG NG

3,3'-Dichlorobenzidine <7600 <1800 <1700 NG NG


4-Bromophenyl phenyl ether <1300 <310 <290 NG NG

4-Chloroaniline <1300 <310 <290 NG NG

4-Chlorophenyl phenyl ether <1300 <310 <290 NG NG


Acenaphthene 1400 <310 <290 20,000 100,000Acenaphthylene <1300 <310 <290 100,000 100,000Anthracene <1300 <310 <290 100,000 100,000Azobenzene <1300 <310 <290 NG NG

Benzo(a)anthracene 2100 600 340 1,000 1,000Benzidine <7600 <1800 <1700 NG NG

Benzo(a)pyrene 1400 630 <290 1,000 1,000Benzo(b)fluoranthene 1800 720 350 1,000 1,000

Table 4Soil Samples Semi-Volatile Organic Analytical Results



Guidelines




Benzo(ghi)perylene <1300 450 <290 100,000 100,000Benzo(k)fluoranthene <1300 <310 <290 800 1,000Benzoic acid <1900 <450 <410 NG NGBenzyl alcohol <1300 <310 <290 NG NG

Benzyl butyl phthalate <1300 <310 <290 NG 100,000

Bis(2-chloroethoxy)methane <1300 <310 <290 NG NGBis(2-chloroethyl)ether <1300 <310 <290 NG NGBis(2-chloroisopropyl)ether <1300 <310 <290 NG NGBis(2-ethylhexyl)phthalate <1300 <310 320 NG NGChrysene 1700 530 300 1,000 1,000Dibenzo(a,h)anthracene <1300 <310 <290 330 1,000Dibenzofuran <1300 <310 <290 NG NGDiethyl Phthalate <1300 <310 <290 NG NGDimethyl Phthalate <1300 <310 <290 NG NGDi-n-Butyl Phthalate <1300 <310 <290 NG NGDi-n-octyl Phthalate <1300 <310 <290 NG NGFluoranthene 7000 1800 940 100,000 100,000Fluorene <1300 <310 <290 30,000 100,000Hexachlorobenzene <1300 <310 <290 NG 100,000Hexachlorobutadiene <1300 <310 <290 NG NG

Sample Identification S-5 S-6 S-7

Boring Number B-5 B-5 B-6

Sample Depth 11-12 feet 13-15 feet 13-15 feet

Sample Date 12/3/2011 12/3/2011 12/3/2011

Sample Matrix Soil Soil Soil

Units ug/kg ug/kg ug/kg

Hexachlorocyclopentadiene <1300 <310 <290 NG NGHexachloroethane <1300 <310 <290 NG NGIndeno(1,2,3-cd)pyrene <1300 320 <290 500 500Isophorone <1300 <310 <290 NG 500Naphthalene(sv) <1300 <310 <290 12,000 100,000Nitrobenzene <1300 <310 <290 NG NGN-Nitrosodimethylamine <1300 <310 <290 NG NGN-Nitrosodi-n-propylamine <1300 <310 <290 NG NGN-Nitrosodiphenylamine <1300 <310 <290 NG NGPhenanthrene 6200 1100 370 100,000 100,000Pyrene 5900 1800 900 100,000 100,000

ug/kg…micrograms per kilogram


NS : No Standard

Table 4 (Cont'd)Soil Samples Semi-Volatile Organic Analytical Results



Guidelines




Sample Identification S-1 S-2 S-3 S-4 S-5 S-6 S-7Boring Number B-1 12-14ft B-2 11-13ft B-3 9-11ft B-4 10-12ft B-5 11-12ft B-5 13-15ft B-6 13-15ft

Sample Date 12/3/2011 12/3/2011 12/3/2011 12/3/2011 12/3/2011 12/3/2011 12/3/2011

Sample Matrix Soil Soil Soil Soil Soil Soil Soil

Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Arsenic as As 14.7 86.3 63.3 5.65 12.2 7.54 53.9 13 16

Barium as Ba 271 188 233 50.9 51.3 68.1 212 350 350

Cadmium as Cd 1.26 2.05 1.95 0.62 2.47 0.9 1.25 2.5 2.5

Chromium as Cr 12.7 113 37.5 16.7 25.7 16.2 13.3 30 36

Lead as Pb 401 895 590 76.3 172 1080 547 63 400

Mercury as Hg 2.15 0.19 1.77 0.9 0.53 0.23 0.23 0.18 0.81

Selenium as Se 9.7 3.4 4.3 <1.6 3 <1.8 3.9 3.9 36

Silver as Ag <0.45 <0.4 <0.42 <0.4 <0.37 <0.44 <0.45 2 36


375-6.8(b) Residential Use

Soil Cleanup Objectives

Metals (TAL) (mg/kg)

Table 5Soil Samples Inorganic Analytical Results


NYSDEC CP-51 Guidelines

g

m/kg…miligram per kilogram

Bold values indicate concentrations exceeding laboratory method detection limits.Shaded values indicate concentrations above NYSDEC CP-51 Guidelines.Shaded values indicate concentrations above NYSDEC CP-51 and Brownfield Residential Use Guidelines.


NS : No Standard

Groundwater Samples Organic Analytical Results

Sample Identification S-1 S-2 S-3 S-4Boring Number B-1GW B-2GW B-4 GW B-6 GW

Sample Date 12/3/2011 12/3/2011 12/3/2011 12/5/2011Sample Matrix Water Water Water Water

Units ug/L ug/L ug/L ug/L

1,1,1,2-Tetrachloroethane <2 <1 <5 <2 51,1,1-Trichloroethane <2 <1 <5 <2 51,1,2,2-Tetrachloroethane <1 <0.5 <2.5 <1 51,1,2-Trichloroethane <2 <1 <5 <2 11,1-Dichloroethane <2 <1 <5 <2 51,1-Dichloroethene <2 <1 <5 <2 51,1-Dichloropropene <2 <1 <5 <2 51,2,3-Trichlorobenzene <2 <1 <5 <2 51,2,3-Trichloropropane <2 <1 <5 <2 0.041,2,4-Trichlorobenzene <2 <1 <5 <2 51,2,4-Trimethylbenzene <2 <1 <5 <2 51,2-Dibromo-3-chloropropane <2 <1 <5 <2 0.041,2-Dichlorobenzene <2 <1 <5 <2 31,2-Dichloroethane <2 <1 <5 <2 51,2-Dichloropropane <2 <1 <5 <2 11,3,5-Trimethylbenzene <2 <1 <5 <2 51,3-Dichlorobenzene <2 <1 <5 <2 31,3-Dichloropropane <2 <1 <5 <2 51,4-Dichlorobenzene <2 <1 <5 <2 32,2-Dichloropropane <2 <1 <5 <2 52-Chlorotoluene <2 <1 <5 <2 52-Hexanone <10 <5 <25 <10 502-Isopropyltoluene 50 <1 65 14 54-Chlorotoluene <2 <1 <5 <2 54-Methyl-2-Pentanone (MIBK) <10 <5 <25 <10 NSAcetone <50 <25 <130 <50 50Acrylonitrile <10 <5 <25 <10 0.07Benzene <2 <1 <5 <2 1Bromobenzene <2 <1 <5 <2 5Bromochloromethane <2 <1 <5 <2 5

Table 6


NYSDEC TOGS 1.1.1 Groundwater Quality

Standards

Volatile Organic Compounds (µg/L) - EPA Method 8260

Bromochloromethane <2 <1 <5 <2 5Bromodichloromethane <1 <0.5 <2.5 <1 50Bromoform <2 <1 <5 <2 NSBromomethane <2 <1 <5 <2 5Carbon Disulfide <10 <5 <25 <10 NSCarbon Tetrachloride <2 <1 <5 <2 5Chlorobenzene <2 <1 <5 <2 5Chloroethane <2 <1 <5 <2 5Chloroform <2 <1 <5 <2 7Chloromethane <2 <1 <5 <2 NScis-1,2-Dichloroethene <2 <1 <5 <2 NScis-1,3-Dichloropropene <1 <0.5 <2.5 <1 0.4Dibromochloromethane <1 <0.5 <2.5 <1 NSDibromoethane <2 <1 <5 <2 NSDibromomethane <2 <1 <5 <2 5Dichlorodifluoromethane <2 <1 <5 <2 5Ethylbenzene <2 <1 <5 <2 5Hexachlorobutadiene <0.8 <0.4 <2 <0.8 5Isopropylbenzene 35 <1 6.8 <2 5m&p-Xylene <2 <1 <5 <2 5

Groundwater Samples Organic Analytical Results

Sample Identification S-1 S-2 S-3 S-4Boring Number B-1GW B-2GW B-4 GW B-6 GW

Sample Date 12/3/2011 12/3/2011 12/3/2011 12/5/2011Sample Matrix Water Water Water Water

Units ug/L ug/L ug/L ug/L

Methyl Ethyl Ketone <10 <5 <25 <10 50Methyl t-Butyl Ether (MTBE) <2 <1 <5 <2 NSMethylene Chloride <2 <1 <5 <2 5Naphthalene <2 <1 <5 <2 5n-Butylbenzene <2 <1 34 <2 5n-Propylbenzene 3 <1 <5 <2 5o-Xylene <2 <1 <5 <2 5p-Isopropyltoluene <2 3.1 <5 <2 5sec-Butylbenzene 130 1.2 110 4 5Styrene <2 <1 <5 <2 5tert-Butylbenzene 37 <1 33 14 5Tetrachloroethene <2 <1 <5 <2 5Tetrahydrofuran (THF) <10 <5 <25 <10 NSToluene <2 <1 <5 <2 5Total Xylenes <2 <1 <5 <2 5trans-1,2-Dichloroethene <2 <1 <5 <2 NStrans-1,3-Dichloropropene <1 <0.5 <2.5 <1 NStrans-1,4-dichloro-2-butene <10 <5 <25 <10 5Trichloroethene <2 <1 <5 <2 5Trichlorofluoromethane <2 <1 <5 <2 5Trichlorotrifluoroethane <2 <1 <5 <2 NSVinyl Chloride <2 <1 <5 <2 2

ug/L…micrograms per literBold values indicate concentrations exceeding laboratory method detection limits.

NS : No Standard

Shaded values indicate concentrations above NYSDEC TOGS 1.1.1 Guidelines.

Table 6 Cont'd


NYSDEC TOGS 1.1.1 Groundwater Quality

Standards

Volatile Organic Compounds (µg/L) - EPA Method 8260

Sample Identification S-5 S-6 S-7 S-8

Sample Location B-1GW B-2GW B-4 GW B-6 GW

Sample Date 12/3/2011 12/3/2011 12/3/2011 12/3/2011

Sample Matrix Water Water Water Water

Arsenic as As 1.09 39.7 2.59 0.479 0.025Barium as Ba 4.19 4.3 9.05 2.09 1Cadmium as Cd 0.001 <0.01 0.034 0.012 0.005Chromium as Cr 0.581 1.43 1.41 0.16 0.05Lead as Pb 19.7 13.5 25.4 3.4 0.025Mercury as Hg 0.0057 <0.0008 <0.0008 <0.0008 0.0007Selenium as Se 0.117 0.796 0.336 0.121 0.01Silver as Ag <0.001 <0.001 0.01 <0.01 0.05

Arsenic as As 0.022 2.36 0.12 0.014 0.025Barium as Ba 0.302 0.1 0.121 0.088 1Cadmium as Cd <0.001 <0.001 <0.001 0.001 0.005Chromium as Cr 0.011 0.009 0.006 <0.001 0.05Lead as Pb 0.294 0.061 0.065 0.009 0.025Mercury as Hg <0.0008 <0.0008 <0.0008 <0.0008 0.0007

Metals(TAL) mg/L - Unfiltered

NYSDEC TOGS 1.1.1

Groundwater Quaility Standard

Table 7Water Samples Inorganic Analytical Results


Metals(TAL) mg/L - Filtered

Selenium as Se 0.02 0.022 0.011 0.011 0.01Silver as Ag <0.001 <0.001 <0.001 <0.001 0.05mg/L…miligrams per literShaded values represent concentration exceeding the GQSBold values represent concentration exceeding the laboratory method detection limits

Shaded values indicate concentrations above NYSDEC TOGS 1.1.1 Guidelines.

APPENDICES

APPENDIX A

PHOTOGRAPHS

PHOTOGRAPHS 55 Eckford Street, Brooklyn, New York

Fig 1. View of Subject Property located at 55 Eckford Street, Brooklyn, NY.

Fig 2. View of boring B-1 advanced on the subject property.

Fig 3. View of soil sample collected for laboratory analysis at B-1.


Fig 5. View of soil sample collected from boring B-4.


Fig 3. View of soil sample collected from soil boring B-5.

APPENDIX B

CHAIN-OF-CUSTODY

APPENDIX C

LABORATORY REPORTS

Sample Information Custody Information

Matrix:Location Code:

Rush Request:

P.O.#:

Collected by:Received by:

Analyzed by:

SOIL

EEA | B

12/03/11

LB

see "By" below

SM

Laboratory Data

B-1 12-14 FT

Phoenix ID: BB07251

12/05/11

9:45

16:00

Parameter Result RL Units Date By Reference

FOR: Attn: Mr. Sean MartinEEA, Inc.55 Hilton AveGarden City, NY 11530

Analysis ReportDecember 13, 2011

Time

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBB07251

Client ID:

Project ID: 55 ECKFORD ST.

< 0.45Silver 0.45 12/06/11 LK 6010/200.7mg/Kg14.7Arsenic 0.91 12/06/11 LK 6010/200.7mg/Kg271Barium 0.45 12/06/11 LK 6010/200.7mg/Kg1.26Cadmium 0.45 12/06/11 LK 6010/200.7mg/Kg12.7Chromium 0.45 12/06/11 LK 6010/200.7mg/Kg2.15Mercury 0.11 12/06/11 RS SW-7471mg/Kg401Lead 4.5 12/07/11 LK 6010/200.7mg/Kg9.7Selenium 1.8 12/06/11 LK 6010/200.7mg/KgCompletedTotal Metals Digest 12/05/11 AG SW846 - 3050

69Percent Solid 12/05/11 JL E160.3%CompletedSoil Extraction for SVOA 12/05/11 BB/R SW3545

CompletedMercury Digestion 12/06/11 SW7471

VolatilesND1,1,1,2-Tetrachloroethane 1800 12/08/11 R/J SW8260ug/KgND1,1,1-Trichloroethane 1800 12/08/11 R/J SW8260ug/KgND1,1,2,2-Tetrachloroethane 1800 12/08/11 R/J SW8260ug/KgND1,1,2-Trichloroethane 1800 12/08/11 R/J SW8260ug/KgND1,1-Dichloroethane 1800 12/08/11 R/J SW8260ug/KgND1,1-Dichloroethene 1800 12/08/11 R/J SW8260ug/KgND1,1-Dichloropropene 1800 12/08/11 R/J SW8260ug/KgND1,2,3-Trichlorobenzene 1800 12/08/11 R/J SW8260ug/KgND1,2,3-Trichloropropane 1800 12/08/11 R/J SW8260ug/KgND1,2,4-Trichlorobenzene 1800 12/08/11 R/J SW8260ug/KgND1,2,4-Trimethylbenzene 1800 12/08/11 R/J SW8260ug/KgND1,2-Dibromo-3-chloropropane 1800 12/08/11 R/J SW8260ug/KgND1,2-Dichlorobenzene 1800 12/08/11 R/J SW8260ug/KgND1,2-Dichloroethane 1800 12/08/11 R/J SW8260ug/Kg

Page 1 of 43 Ver 1

B-1 12-14 FT

Phoenix I.D.: BB07251

Parameter Result RL Units Date By ReferenceTime

Client ID:55 ECKFORD ST.Project ID:

ND1,2-Dichloropropane 1800 12/08/11 R/J SW8260ug/KgND1,3,5-Trimethylbenzene 1800 12/08/11 R/J SW8260ug/KgND1,3-Dichlorobenzene 1800 12/08/11 R/J SW8260ug/KgND1,3-Dichloropropane 1800 12/08/11 R/J SW8260ug/KgND1,4-Dichlorobenzene 1800 12/08/11 R/J SW8260ug/KgND2,2-Dichloropropane 1800 12/08/11 R/J SW8260ug/KgND2-Chlorotoluene 1800 12/08/11 R/J SW8260ug/KgND2-Hexanone 9100 12/08/11 R/J SW8260ug/KgND2-Isopropyltoluene 1800 12/08/11 R/J SW8260ug/KgND4-Chlorotoluene 1800 12/08/11 R/J SW8260ug/KgND4-Methyl-2-pentanone 9100 12/08/11 R/J SW8260ug/KgNDAcetone 9100 12/08/11 R/J SW8260ug/KgNDAcrylonitrile 3600 12/08/11 R/J SW8260ug/KgNDBenzene 1800 12/08/11 R/J SW8260ug/KgNDBromobenzene 1800 12/08/11 R/J SW8260ug/KgNDBromochloromethane 1800 12/08/11 R/J SW8260ug/KgNDBromodichloromethane 1800 12/08/11 R/J SW8260ug/KgNDBromoform 1800 12/08/11 R/J SW8260ug/KgNDBromomethane 1800 12/08/11 R/J SW8260ug/KgNDCarbon Disulfide 1800 12/08/11 R/J SW8260ug/KgNDCarbon tetrachloride 1800 12/08/11 R/J SW8260ug/KgNDChlorobenzene 1800 12/08/11 R/J SW8260ug/KgNDChloroethane 1800 12/08/11 R/J SW8260ug/KgNDChloroform 1800 12/08/11 R/J SW8260ug/KgNDChloromethane 1800 12/08/11 R/J SW8260ug/KgNDcis-1,2-Dichloroethene 1800 12/08/11 R/J SW8260ug/KgNDcis-1,3-Dichloropropene 1800 12/08/11 R/J SW8260ug/KgNDDibromochloromethane 1800 12/08/11 R/J SW8260ug/KgNDDibromoethane 1800 12/08/11 R/J SW8260ug/KgNDDibromomethane 1800 12/08/11 R/J SW8260ug/KgNDDichlorodifluoromethane 1800 12/08/11 R/J SW8260ug/KgNDEthylbenzene 1800 12/08/11 R/J SW8260ug/KgNDHexachlorobutadiene 1800 12/08/11 R/J SW8260ug/KgNDIsopropylbenzene 1800 12/08/11 R/J SW8260ug/KgNDm&p-Xylene 1800 12/08/11 R/J SW8260ug/KgNDMethyl Ethyl Ketone 9100 12/08/11 R/J SW8260ug/KgNDMethyl t-butyl ether (MTBE) 3600 12/08/11 R/J SW8260ug/KgNDMethylene chloride 1800 12/08/11 R/J SW8260ug/KgNDNaphthalene 1800 12/08/11 R/J SW8260ug/KgNDn-Butylbenzene 1800 12/08/11 R/J SW8260ug/KgNDn-Propylbenzene 1800 12/08/11 R/J SW8260ug/KgNDo-Xylene 1800 12/08/11 R/J SW8260ug/KgNDp-Isopropyltoluene 1800 12/08/11 R/J SW8260ug/Kg5500sec-Butylbenzene 1800 12/08/11 R/J SW8260ug/KgNDStyrene 1800 12/08/11 R/J SW8260ug/Kg2300tert-Butylbenzene 1800 12/08/11 R/J SW8260ug/KgNDTetrachloroethene 1800 12/08/11 R/J SW8260ug/KgNDTetrahydrofuran (THF) 3600 12/08/11 R/J SW8260ug/KgNDToluene 1800 12/08/11 R/J SW8260ug/KgNDTotal Xylenes 1800 12/08/11 R/J SW8260ug/Kg

Page 2 of 43 Ver 1

B-1 12-14 FT




NDtrans-1,2-Dichloroethene 1800 12/08/11 R/J SW8260ug/KgNDtrans-1,3-Dichloropropene 1800 12/08/11 R/J SW8260ug/KgNDtrans-1,4-dichloro-2-butene 3600 12/08/11 R/J SW8260ug/KgNDTrichloroethene 1800 12/08/11 R/J SW8260ug/KgNDTrichlorofluoromethane 1800 12/08/11 R/J SW8260ug/KgNDTrichlorotrifluoroethane 1800 12/08/11 R/J SW8260ug/KgNDVinyl chloride 1800 12/08/11 R/J SW8260ug/Kg

QA/QC Surrogates106% 1,2-dichlorobenzene-d4 12/08/11 R/J 70 - 130 %%

116% Bromofluorobenzene 12/08/11 R/J 70 - 130 %%

94% Dibromofluoromethane 12/08/11 R/J 70 - 130 %%

100% Toluene-d8 12/08/11 R/J 70 - 130 %%

SemivolatilesND1,2-Dichlorobenzene 1700 12/06/11 D/P SW8270ug/KgND1,3-Dichlorobenzene 1700 12/06/11 D/P SW8270ug/KgND1,4-Dichlorobenzene 1700 12/06/11 D/P SW8270ug/KgND2,4-Dinitrotoluene 1700 12/06/11 D/P SW8270ug/KgND2,6-Dinitrotoluene 1700 12/06/11 D/P SW8270ug/KgND2-Chloronaphthalene 1700 12/06/11 D/P SW8270ug/KgND2-Methylnaphthalene 1700 12/06/11 D/P SW8270ug/KgND2-Nitroaniline 7000 12/06/11 D/P SW8270ug/KgND3,3'-Dichlorobenzidine 9600 12/06/11 D/P SW8270ug/KgND3-Nitroaniline 7000 12/06/11 D/P SW8270ug/KgND4-Bromophenyl phenyl ether 1700 12/06/11 D/P SW8270ug/KgND4-Chloroaniline 1700 12/06/11 D/P SW8270ug/KgND4-Chlorophenyl phenyl ether 1700 12/06/11 D/P SW8270ug/KgND4-Nitroaniline 7000 12/06/11 D/P SW8270ug/KgNDAcenaphthene 1700 12/06/11 D/P SW8270ug/KgNDAcenaphthylene 1700 12/06/11 D/P SW8270ug/KgNDAnthracene 1700 12/06/11 D/P SW8270ug/KgNDAzobenzene 1700 12/06/11 D/P SW8270ug/KgNDBenz(a)anthracene 1700 12/06/11 D/P SW8270ug/KgNDBenzidine 9600 12/06/11 D/P SW8270ug/KgNDBenzo(a)pyrene 1700 12/06/11 D/P SW8270ug/KgNDBenzo(b)fluoranthene 1700 12/06/11 D/P SW8270ug/KgNDBenzo(ghi)perylene 1700 12/06/11 D/P SW8270ug/KgNDBenzo(k)fluoranthene 1700 12/06/11 D/P SW8270ug/KgNDBenzoic acid 2400 12/06/11 D/P SW8270ug/KgNDBenzyl alcohol 1700 12/06/11 D/P SW8270ug/KgNDBenzyl butyl phthalate 1700 12/06/11 D/P SW8270ug/KgNDBis(2-chloroethoxy)methane 1700 12/06/11 D/P SW8270ug/KgNDBis(2-chloroethyl)ether 1700 12/06/11 D/P SW8270ug/KgNDBis(2-chloroisopropyl)ether 1700 12/06/11 D/P SW8270ug/KgNDBis(2-ethylhexyl)phthalate 1700 12/06/11 D/P SW8270ug/KgNDChrysene 1700 12/06/11 D/P SW8270ug/KgNDDibenz(a,h)anthracene 1700 12/06/11 D/P SW8270ug/KgNDDibenzofuran 1700 12/06/11 D/P SW8270ug/KgNDDiethyl phthalate 1700 12/06/11 D/P SW8270ug/KgNDDimethylphthalate 1700 12/06/11 D/P SW8270ug/Kg

Page 3 of 43 Ver 1

B-1 12-14 FT




NDDi-n-butylphthalate 1700 12/06/11 D/P SW8270ug/KgNDDi-n-octylphthalate 1700 12/06/11 D/P SW8270ug/KgNDFluoranthene 1700 12/06/11 D/P SW8270ug/KgNDFluorene 1700 12/06/11 D/P SW8270ug/KgNDHexachlorobenzene 1700 12/06/11 D/P SW8270ug/KgNDHexachlorobutadiene 1700 12/06/11 D/P SW8270ug/KgNDHexachlorocyclopentadiene 1700 12/06/11 D/P SW8270ug/KgNDHexachloroethane 1700 12/06/11 D/P SW8270ug/KgNDIndeno(1,2,3-cd)pyrene 1700 12/06/11 D/P SW8270ug/KgNDIsophorone 1700 12/06/11 D/P SW8270ug/KgNDNaphthalene 1700 12/06/11 D/P SW8270ug/KgNDNitrobenzene 1700 12/06/11 D/P SW8270ug/KgNDN-Nitrosodimethylamine 1700 12/06/11 D/P SW8270ug/KgNDN-Nitrosodi-n-propylamine 1700 12/06/11 D/P SW8270ug/KgNDN-Nitrosodiphenylamine 1700 12/06/11 D/P SW8270ug/KgNDPhenanthrene 1700 12/06/11 D/P SW8270ug/KgNDPyrene 1700 12/06/11 D/P SW8270ug/Kg

QA/QC Surrogates74% 2-Fluorobiphenyl 12/06/11 D/P 30 - 130 %%

63% Nitrobenzene-d5 12/06/11 D/P 30 - 130 %%

93% Terphenyl-d14 12/06/11 D/P 30 - 130 %%

Comments:

ND=Not detected BDL=Below Detection Level RL=Reporting Level

* Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for thesemivolatile analysis.

Elevated reporting limits for volatiles due to the presence of target and non-target compounds.

Phyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

December 13, 2011

This report must not be reproduced except in full as defined by the attached chain of custody.

Page 4 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

SOIL

EEA | B

12/03/11

LB

see "By" below

SM

Laboratory Data

B-2 11-13 FT

Phoenix ID: BB07252

12/05/11

10:38

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


< 0.40Silver 0.40 12/06/11 LK 6010/200.7mg/Kg86.3Arsenic 0.81 12/06/11 LK 6010/200.7mg/Kg188Barium 0.40 12/06/11 LK 6010/200.7mg/Kg2.05Cadmium 0.40 12/06/11 LK 6010/200.7mg/Kg113Chromium 0.40 12/06/11 LK 6010/200.7mg/Kg0.19Mercury 0.07 12/06/11 RS SW-7471mg/Kg895Lead 4.0 12/07/11 LK 6010/200.7mg/Kg3.4Selenium 1.6 12/06/11 LK 6010/200.7mg/KgCompletedTotal Metals Digest 12/05/11 AG SW846 - 3050



VolatilesND1,1,1,2-Tetrachloroethane 5.7 12/10/11 H/J SW8260ug/KgND1,1,1-Trichloroethane 5.7 12/10/11 H/J SW8260ug/KgND1,1,2,2-Tetrachloroethane 5.7 12/10/11 H/J SW8260ug/KgND1,1,2-Trichloroethane 5.7 12/10/11 H/J SW8260ug/KgND1,1-Dichloroethane 5.7 12/10/11 H/J SW8260ug/KgND1,1-Dichloroethene 5.7 12/10/11 H/J SW8260ug/KgND1,1-Dichloropropene 5.7 12/10/11 H/J SW8260ug/KgND1,2,3-Trichlorobenzene 5.7 12/10/11 H/J SW8260ug/KgND1,2,3-Trichloropropane 5.7 12/10/11 H/J SW8260ug/KgND1,2,4-Trichlorobenzene 5.7 12/10/11 H/J SW8260ug/KgND1,2,4-Trimethylbenzene 5.7 12/10/11 H/J SW8260ug/KgND1,2-Dibromo-3-chloropropane 5.7 12/10/11 H/J SW8260ug/KgND1,2-Dichlorobenzene 5.7 12/10/11 H/J SW8260ug/KgND1,2-Dichloroethane 5.7 12/10/11 H/J SW8260ug/Kg

Page 5 of 43 Ver 1

B-2 11-13 FT




ND1,2-Dichloropropane 5.7 12/10/11 H/J SW8260ug/KgND1,3,5-Trimethylbenzene 5.7 12/10/11 H/J SW8260ug/KgND1,3-Dichlorobenzene 5.7 12/10/11 H/J SW8260ug/KgND1,3-Dichloropropane 5.7 12/10/11 H/J SW8260ug/KgND1,4-Dichlorobenzene 5.7 12/10/11 H/J SW8260ug/KgND2,2-Dichloropropane 5.7 12/10/11 H/J SW8260ug/KgND2-Chlorotoluene 5.7 12/10/11 H/J SW8260ug/KgND2-Hexanone 29 12/10/11 H/J SW8260ug/KgND2-Isopropyltoluene 5.7 12/10/11 H/J SW8260ug/KgND4-Chlorotoluene 5.7 12/10/11 H/J SW8260ug/KgND4-Methyl-2-pentanone 29 12/10/11 H/J SW8260ug/KgNDAcetone 29 12/10/11 H/J SW8260ug/KgNDAcrylonitrile 11 12/10/11 H/J SW8260ug/KgNDBenzene 5.7 12/10/11 H/J SW8260ug/KgNDBromobenzene 5.7 12/10/11 H/J SW8260ug/KgNDBromochloromethane 5.7 12/10/11 H/J SW8260ug/KgNDBromodichloromethane 5.7 12/10/11 H/J SW8260ug/KgNDBromoform 5.7 12/10/11 H/J SW8260ug/KgNDBromomethane 5.7 12/10/11 H/J SW8260ug/KgNDCarbon Disulfide 5.7 12/10/11 H/J SW8260ug/KgNDCarbon tetrachloride 5.7 12/10/11 H/J SW8260ug/KgNDChlorobenzene 5.7 12/10/11 H/J SW8260ug/KgNDChloroethane 5.7 12/10/11 H/J SW8260ug/KgNDChloroform 5.7 12/10/11 H/J SW8260ug/KgNDChloromethane 5.7 12/10/11 H/J SW8260ug/KgNDcis-1,2-Dichloroethene 5.7 12/10/11 H/J SW8260ug/KgNDcis-1,3-Dichloropropene 5.7 12/10/11 H/J SW8260ug/KgNDDibromochloromethane 5.7 12/10/11 H/J SW8260ug/KgNDDibromoethane 5.7 12/10/11 H/J SW8260ug/KgNDDibromomethane 5.7 12/10/11 H/J SW8260ug/KgNDDichlorodifluoromethane 5.7 12/10/11 H/J SW8260ug/KgNDEthylbenzene 5.7 12/10/11 H/J SW8260ug/KgNDHexachlorobutadiene 5.7 12/10/11 H/J SW8260ug/KgNDIsopropylbenzene 5.7 12/10/11 H/J SW8260ug/KgNDm&p-Xylene 5.7 12/10/11 H/J SW8260ug/KgNDMethyl Ethyl Ketone 29 12/10/11 H/J SW8260ug/KgNDMethyl t-butyl ether (MTBE) 11 12/10/11 H/J SW8260ug/KgNDMethylene chloride 29 12/10/11 H/J SW8260ug/KgNDNaphthalene 5.7 12/10/11 H/J SW8260ug/KgNDn-Butylbenzene 5.7 12/10/11 H/J SW8260ug/KgNDn-Propylbenzene 5.7 12/10/11 H/J SW8260ug/KgNDo-Xylene 5.7 12/10/11 H/J SW8260ug/KgNDp-Isopropyltoluene 5.7 12/10/11 H/J SW8260ug/KgNDsec-Butylbenzene 5.7 12/10/11 H/J SW8260ug/KgNDStyrene 5.7 12/10/11 H/J SW8260ug/KgNDtert-Butylbenzene 5.7 12/10/11 H/J SW8260ug/KgNDTetrachloroethene 5.7 12/10/11 H/J SW8260ug/KgNDTetrahydrofuran (THF) 11 12/10/11 H/J SW8260ug/KgNDToluene 5.7 12/10/11 H/J SW8260ug/KgNDTotal Xylenes 5.7 12/10/11 H/J SW8260ug/Kg

Page 6 of 43 Ver 1

B-2 11-13 FT




NDtrans-1,2-Dichloroethene 5.7 12/10/11 H/J SW8260ug/KgNDtrans-1,3-Dichloropropene 5.7 12/10/11 H/J SW8260ug/KgNDtrans-1,4-dichloro-2-butene 11 12/10/11 H/J SW8260ug/KgNDTrichloroethene 5.7 12/10/11 H/J SW8260ug/KgNDTrichlorofluoromethane 5.7 12/10/11 H/J SW8260ug/KgNDTrichlorotrifluoroethane 5.7 12/10/11 H/J SW8260ug/KgNDVinyl chloride 5.7 12/10/11 H/J SW8260ug/Kg

QA/QC Surrogates101% 1,2-dichlorobenzene-d4 12/10/11 H/J 70 - 130 %%

89% Bromofluorobenzene 12/10/11 H/J 70 - 130 %%

90% Dibromofluoromethane 12/10/11 H/J 70 - 130 %%

100% Toluene-d8 12/10/11 H/J 70 - 130 %%

SemivolatilesND1,2-Dichlorobenzene 260 12/05/11 DD SW8270ug/KgND1,3-Dichlorobenzene 260 12/05/11 DD SW8270ug/KgND1,4-Dichlorobenzene 260 12/05/11 DD SW8270ug/KgND2,4-Dinitrotoluene 260 12/05/11 DD SW8270ug/KgND2,6-Dinitrotoluene 260 12/05/11 DD SW8270ug/KgND2-Chloronaphthalene 260 12/05/11 DD SW8270ug/KgND2-Methylnaphthalene 260 12/05/11 DD SW8270ug/KgND2-Nitroaniline 1100 12/05/11 DD SW8270ug/KgND3,3'-Dichlorobenzidine 1500 12/05/11 DD SW8270ug/KgND3-Nitroaniline 1100 12/05/11 DD SW8270ug/KgND4-Bromophenyl phenyl ether 260 12/05/11 DD SW8270ug/KgND4-Chloroaniline 260 12/05/11 DD SW8270ug/KgND4-Chlorophenyl phenyl ether 260 12/05/11 DD SW8270ug/KgND4-Nitroaniline 1100 12/05/11 DD SW8270ug/KgNDAcenaphthene 260 12/05/11 DD SW8270ug/KgNDAcenaphthylene 260 12/05/11 DD SW8270ug/KgNDAnthracene 260 12/05/11 DD SW8270ug/KgNDAzobenzene 260 12/05/11 DD SW8270ug/KgNDBenz(a)anthracene 260 12/05/11 DD SW8270ug/KgNDBenzidine 1500 12/05/11 DD SW8270ug/KgNDBenzo(a)pyrene 260 12/05/11 DD SW8270ug/KgNDBenzo(b)fluoranthene 260 12/05/11 DD SW8270ug/KgNDBenzo(ghi)perylene 260 12/05/11 DD SW8270ug/KgNDBenzo(k)fluoranthene 260 12/05/11 DD SW8270ug/KgNDBenzoic acid 370 12/05/11 DD SW8270ug/KgNDBenzyl alcohol 260 12/05/11 DD SW8270ug/KgNDBenzyl butyl phthalate 260 12/05/11 DD SW8270ug/KgNDBis(2-chloroethoxy)methane 260 12/05/11 DD SW8270ug/KgNDBis(2-chloroethyl)ether 260 12/05/11 DD SW8270ug/KgNDBis(2-chloroisopropyl)ether 260 12/05/11 DD SW8270ug/KgNDBis(2-ethylhexyl)phthalate 260 12/05/11 DD SW8270ug/KgNDChrysene 260 12/05/11 DD SW8270ug/KgNDDibenz(a,h)anthracene 260 12/05/11 DD SW8270ug/KgNDDibenzofuran 260 12/05/11 DD SW8270ug/KgNDDiethyl phthalate 260 12/05/11 DD SW8270ug/KgNDDimethylphthalate 260 12/05/11 DD SW8270ug/Kg

Page 7 of 43 Ver 1

B-2 11-13 FT




NDDi-n-butylphthalate 260 12/05/11 DD SW8270ug/KgNDDi-n-octylphthalate 260 12/05/11 DD SW8270ug/KgNDFluoranthene 260 12/05/11 DD SW8270ug/KgNDFluorene 260 12/05/11 DD SW8270ug/KgNDHexachlorobenzene 260 12/05/11 DD SW8270ug/KgNDHexachlorobutadiene 260 12/05/11 DD SW8270ug/KgNDHexachlorocyclopentadiene 260 12/05/11 DD SW8270ug/KgNDHexachloroethane 260 12/05/11 DD SW8270ug/KgNDIndeno(1,2,3-cd)pyrene 260 12/05/11 DD SW8270ug/KgNDIsophorone 260 12/05/11 DD SW8270ug/KgNDNaphthalene 260 12/05/11 DD SW8270ug/KgNDNitrobenzene 260 12/05/11 DD SW8270ug/KgNDN-Nitrosodimethylamine 260 12/05/11 DD SW8270ug/KgNDN-Nitrosodi-n-propylamine 260 12/05/11 DD SW8270ug/KgNDN-Nitrosodiphenylamine 260 12/05/11 DD SW8270ug/KgNDPhenanthrene 260 12/05/11 DD SW8270ug/KgNDPyrene 260 12/05/11 DD SW8270ug/Kg

QA/QC Surrogates67% 2-Fluorobiphenyl 12/05/11 DD 30 - 130 %%

71% Nitrobenzene-d5 12/05/11 DD 30 - 130 %%

93% Terphenyl-d14 12/05/11 DD 30 - 130 %%

Comments:




December 13, 2011


Page 8 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

SOIL

EEA | B

12/03/11

LB

see "By" below

SM

Laboratory Data

B-3 9-11 FT

Phoenix ID: BB07253

12/05/11

11:02

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


< 0.42Silver 0.42 12/06/11 LK 6010/200.7mg/Kg63.3Arsenic 0.85 12/06/11 LK 6010/200.7mg/Kg233Barium 0.42 12/06/11 LK 6010/200.7mg/Kg1.95Cadmium 0.42 12/06/11 LK 6010/200.7mg/Kg37.5Chromium 0.42 12/06/11 LK 6010/200.7mg/Kg1.77Mercury 0.09 12/06/11 RS SW-7471mg/Kg590Lead 4.2 12/06/11 EK 6010/200.7mg/Kg4.3Selenium 1.7 12/06/11 LK 6010/200.7mg/KgCompletedTotal Metals Digest 12/05/11 AG SW846 - 3050



VolatilesND1,1,1,2-Tetrachloroethane 300 12/10/11 H/J SW8260ug/KgND1,1,1-Trichloroethane 300 12/10/11 H/J SW8260ug/KgND1,1,2,2-Tetrachloroethane 300 12/10/11 H/J SW8260ug/KgND1,1,2-Trichloroethane 300 12/10/11 H/J SW8260ug/KgND1,1-Dichloroethane 300 12/10/11 H/J SW8260ug/KgND1,1-Dichloroethene 300 12/10/11 H/J SW8260ug/KgND1,1-Dichloropropene 300 12/10/11 H/J SW8260ug/KgND1,2,3-Trichlorobenzene 300 12/10/11 H/J SW8260ug/KgND1,2,3-Trichloropropane 300 12/10/11 H/J SW8260ug/KgND1,2,4-Trichlorobenzene 300 12/10/11 H/J SW8260ug/KgND1,2,4-Trimethylbenzene 300 12/10/11 H/J SW8260ug/KgND1,2-Dibromo-3-chloropropane 300 12/10/11 H/J SW8260ug/KgND1,2-Dichlorobenzene 300 12/10/11 H/J SW8260ug/KgND1,2-Dichloroethane 300 12/10/11 H/J SW8260ug/Kg

Page 9 of 43 Ver 1

B-3 9-11 FT




ND1,2-Dichloropropane 300 12/10/11 H/J SW8260ug/KgND1,3,5-Trimethylbenzene 300 12/10/11 H/J SW8260ug/KgND1,3-Dichlorobenzene 300 12/10/11 H/J SW8260ug/KgND1,3-Dichloropropane 300 12/10/11 H/J SW8260ug/KgND1,4-Dichlorobenzene 300 12/10/11 H/J SW8260ug/KgND2,2-Dichloropropane 300 12/10/11 H/J SW8260ug/KgND2-Chlorotoluene 300 12/10/11 H/J SW8260ug/KgND2-Hexanone 1500 12/10/11 H/J SW8260ug/Kg5502-Isopropyltoluene 300 12/10/11 H/J SW8260ug/KgND4-Chlorotoluene 300 12/10/11 H/J SW8260ug/KgND4-Methyl-2-pentanone 1500 12/10/11 H/J SW8260ug/KgNDAcetone 1500 12/10/11 H/J SW8260ug/KgNDAcrylonitrile 610 12/10/11 H/J SW8260ug/KgNDBenzene 300 12/10/11 H/J SW8260ug/KgNDBromobenzene 300 12/10/11 H/J SW8260ug/KgNDBromochloromethane 300 12/10/11 H/J SW8260ug/KgNDBromodichloromethane 300 12/10/11 H/J SW8260ug/KgNDBromoform 300 12/10/11 H/J SW8260ug/KgNDBromomethane 300 12/10/11 H/J SW8260ug/KgNDCarbon Disulfide 300 12/10/11 H/J SW8260ug/KgNDCarbon tetrachloride 300 12/10/11 H/J SW8260ug/KgNDChlorobenzene 300 12/10/11 H/J SW8260ug/KgNDChloroethane 300 12/10/11 H/J SW8260ug/KgNDChloroform 300 12/10/11 H/J SW8260ug/KgNDChloromethane 300 12/10/11 H/J SW8260ug/KgNDcis-1,2-Dichloroethene 300 12/10/11 H/J SW8260ug/KgNDcis-1,3-Dichloropropene 300 12/10/11 H/J SW8260ug/KgNDDibromochloromethane 300 12/10/11 H/J SW8260ug/KgNDDibromoethane 300 12/10/11 H/J SW8260ug/KgNDDibromomethane 300 12/10/11 H/J SW8260ug/KgNDDichlorodifluoromethane 300 12/10/11 H/J SW8260ug/KgNDEthylbenzene 300 12/10/11 H/J SW8260ug/KgNDHexachlorobutadiene 300 12/10/11 H/J SW8260ug/KgNDIsopropylbenzene 300 12/10/11 H/J SW8260ug/KgNDm&p-Xylene 300 12/10/11 H/J SW8260ug/KgNDMethyl Ethyl Ketone 1500 12/10/11 H/J SW8260ug/KgNDMethyl t-butyl ether (MTBE) 610 12/10/11 H/J SW8260ug/KgNDMethylene chloride 300 12/10/11 H/J SW8260ug/KgNDNaphthalene 300 12/10/11 H/J SW8260ug/KgNDn-Butylbenzene 300 12/10/11 H/J SW8260ug/KgNDn-Propylbenzene 300 12/10/11 H/J SW8260ug/KgNDo-Xylene 300 12/10/11 H/J SW8260ug/KgNDp-Isopropyltoluene 300 12/10/11 H/J SW8260ug/Kg730sec-Butylbenzene 300 12/10/11 H/J SW8260ug/KgNDStyrene 300 12/10/11 H/J SW8260ug/KgNDtert-Butylbenzene 300 12/10/11 H/J SW8260ug/KgNDTetrachloroethene 300 12/10/11 H/J SW8260ug/KgNDTetrahydrofuran (THF) 610 12/10/11 H/J SW8260ug/KgNDToluene 300 12/10/11 H/J SW8260ug/KgNDTotal Xylenes 300 12/10/11 H/J SW8260ug/Kg

Page 10 of 43 Ver 1

B-3 9-11 FT




NDtrans-1,2-Dichloroethene 300 12/10/11 H/J SW8260ug/KgNDtrans-1,3-Dichloropropene 300 12/10/11 H/J SW8260ug/KgNDtrans-1,4-dichloro-2-butene 610 12/10/11 H/J SW8260ug/KgNDTrichloroethene 300 12/10/11 H/J SW8260ug/KgNDTrichlorofluoromethane 300 12/10/11 H/J SW8260ug/KgNDTrichlorotrifluoroethane 300 12/10/11 H/J SW8260ug/KgNDVinyl chloride 300 12/10/11 H/J SW8260ug/Kg

QA/QC Surrogates108% 1,2-dichlorobenzene-d4 12/10/11 H/J 70 - 130 %%

121% Bromofluorobenzene 12/10/11 H/J 70 - 130 %%

89% Dibromofluoromethane 12/10/11 H/J 70 - 130 %%

101% Toluene-d8 12/10/11 H/J 70 - 130 %%

SemivolatilesND1,2-Dichlorobenzene 280 12/05/11 DD SW8270ug/KgND1,3-Dichlorobenzene 280 12/05/11 DD SW8270ug/KgND1,4-Dichlorobenzene 280 12/05/11 DD SW8270ug/KgND2,4-Dinitrotoluene 280 12/05/11 DD SW8270ug/KgND2,6-Dinitrotoluene 280 12/05/11 DD SW8270ug/KgND2-Chloronaphthalene 280 12/05/11 DD SW8270ug/KgND2-Methylnaphthalene 280 12/05/11 DD SW8270ug/KgND2-Nitroaniline 1200 12/05/11 DD SW8270ug/KgND3,3'-Dichlorobenzidine 1600 12/05/11 DD SW8270ug/KgND3-Nitroaniline 1200 12/05/11 DD SW8270ug/KgND4-Bromophenyl phenyl ether 280 12/05/11 DD SW8270ug/KgND4-Chloroaniline 280 12/05/11 DD SW8270ug/KgND4-Chlorophenyl phenyl ether 280 12/05/11 DD SW8270ug/KgND4-Nitroaniline 1200 12/05/11 DD SW8270ug/KgNDAcenaphthene 280 12/05/11 DD SW8270ug/KgNDAcenaphthylene 280 12/05/11 DD SW8270ug/KgNDAnthracene 280 12/05/11 DD SW8270ug/KgNDAzobenzene 280 12/05/11 DD SW8270ug/Kg510Benz(a)anthracene 280 12/05/11 DD SW8270ug/KgNDBenzidine 1600 12/05/11 DD SW8270ug/Kg470Benzo(a)pyrene 280 12/05/11 DD SW8270ug/Kg570Benzo(b)fluoranthene 280 12/05/11 DD SW8270ug/Kg300Benzo(ghi)perylene 280 12/05/11 DD SW8270ug/KgNDBenzo(k)fluoranthene 280 12/05/11 DD SW8270ug/KgNDBenzoic acid 400 12/05/11 DD SW8270ug/KgNDBenzyl alcohol 280 12/05/11 DD SW8270ug/KgNDBenzyl butyl phthalate 280 12/05/11 DD SW8270ug/KgNDBis(2-chloroethoxy)methane 280 12/05/11 DD SW8270ug/KgNDBis(2-chloroethyl)ether 280 12/05/11 DD SW8270ug/KgNDBis(2-chloroisopropyl)ether 280 12/05/11 DD SW8270ug/KgNDBis(2-ethylhexyl)phthalate 280 12/05/11 DD SW8270ug/Kg450Chrysene 280 12/05/11 DD SW8270ug/KgNDDibenz(a,h)anthracene 280 12/05/11 DD SW8270ug/KgNDDibenzofuran 280 12/05/11 DD SW8270ug/KgNDDiethyl phthalate 280 12/05/11 DD SW8270ug/KgNDDimethylphthalate 280 12/05/11 DD SW8270ug/Kg

Page 11 of 43 Ver 1

B-3 9-11 FT




NDDi-n-butylphthalate 280 12/05/11 DD SW8270ug/KgNDDi-n-octylphthalate 280 12/05/11 DD SW8270ug/Kg1200Fluoranthene 280 12/05/11 DD SW8270ug/KgNDFluorene 280 12/05/11 DD SW8270ug/KgNDHexachlorobenzene 280 12/05/11 DD SW8270ug/KgNDHexachlorobutadiene 280 12/05/11 DD SW8270ug/KgNDHexachlorocyclopentadiene 280 12/05/11 DD SW8270ug/KgNDHexachloroethane 280 12/05/11 DD SW8270ug/KgNDIndeno(1,2,3-cd)pyrene 280 12/05/11 DD SW8270ug/KgNDIsophorone 280 12/05/11 DD SW8270ug/KgNDNaphthalene 280 12/05/11 DD SW8270ug/KgNDNitrobenzene 280 12/05/11 DD SW8270ug/KgNDN-Nitrosodimethylamine 280 12/05/11 DD SW8270ug/KgNDN-Nitrosodi-n-propylamine 280 12/05/11 DD SW8270ug/KgNDN-Nitrosodiphenylamine 280 12/05/11 DD SW8270ug/Kg680Phenanthrene 280 12/05/11 DD SW8270ug/Kg1200Pyrene 280 12/05/11 DD SW8270ug/Kg



109% Terphenyl-d14 12/05/11 DD 30 - 130 %%

Comments:





December 13, 2011


Page 12 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

SOIL

EEA | B

12/03/11

LB

see "By" below

SM

Laboratory Data

B-4 10-12 FT

Phoenix ID: BB07254

12/05/11

11:45

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


< 0.40Silver 0.40 12/06/11 LK 6010/200.7mg/Kg5.65Arsenic 0.79 12/06/11 LK 6010/200.7mg/Kg50.9Barium 0.40 12/06/11 LK 6010/200.7mg/Kg0.62Cadmium 0.40 12/06/11 LK 6010/200.7mg/Kg16.7Chromium 0.40 12/06/11 LK 6010/200.7mg/Kg0.90Mercury 0.10 12/06/11 RS SW-7471mg/Kg76.3Lead 0.40 12/06/11 LK 6010/200.7mg/Kg< 1.6Selenium 1.6 12/06/11 LK 6010/200.7mg/KgCompletedTotal Metals Digest 12/05/11 AG SW846 - 3050




Page 13 of 43 Ver 1

B-4 10-12 FT




ND1,2-Dichloropropane 1500 12/08/11 R/J SW8260ug/KgND1,3,5-Trimethylbenzene 1500 12/08/11 R/J SW8260ug/KgND1,3-Dichlorobenzene 1500 12/08/11 R/J SW8260ug/KgND1,3-Dichloropropane 1500 12/08/11 R/J SW8260ug/KgND1,4-Dichlorobenzene 1500 12/08/11 R/J SW8260ug/KgND2,2-Dichloropropane 1500 12/08/11 R/J SW8260ug/KgND2-Chlorotoluene 1500 12/08/11 R/J SW8260ug/KgND2-Hexanone 7400 12/08/11 R/J SW8260ug/Kg100002-Isopropyltoluene 1500 12/08/11 R/J SW8260ug/KgND4-Chlorotoluene 1500 12/08/11 R/J SW8260ug/KgND4-Methyl-2-pentanone 7400 12/08/11 R/J SW8260ug/KgNDAcetone 7400 12/08/11 R/J SW8260ug/KgNDAcrylonitrile 3000 12/08/11 R/J SW8260ug/KgNDBenzene 1500 12/08/11 R/J SW8260ug/KgNDBromobenzene 1500 12/08/11 R/J SW8260ug/KgNDBromochloromethane 1500 12/08/11 R/J SW8260ug/KgNDBromodichloromethane 1500 12/08/11 R/J SW8260ug/KgNDBromoform 1500 12/08/11 R/J SW8260ug/KgNDBromomethane 1500 12/08/11 R/J SW8260ug/KgNDCarbon Disulfide 1500 12/08/11 R/J SW8260ug/KgNDCarbon tetrachloride 1500 12/08/11 R/J SW8260ug/KgNDChlorobenzene 1500 12/08/11 R/J SW8260ug/KgNDChloroethane 1500 12/08/11 R/J SW8260ug/KgNDChloroform 1500 12/08/11 R/J SW8260ug/KgNDChloromethane 1500 12/08/11 R/J SW8260ug/KgNDcis-1,2-Dichloroethene 1500 12/08/11 R/J SW8260ug/KgNDcis-1,3-Dichloropropene 1500 12/08/11 R/J SW8260ug/KgNDDibromochloromethane 1500 12/08/11 R/J SW8260ug/KgNDDibromoethane 1500 12/08/11 R/J SW8260ug/KgNDDibromomethane 1500 12/08/11 R/J SW8260ug/KgNDDichlorodifluoromethane 1500 12/08/11 R/J SW8260ug/KgNDEthylbenzene 1500 12/08/11 R/J SW8260ug/KgNDHexachlorobutadiene 1500 12/08/11 R/J SW8260ug/KgNDIsopropylbenzene 1500 12/08/11 R/J SW8260ug/KgNDm&p-Xylene 1500 12/08/11 R/J SW8260ug/KgNDMethyl Ethyl Ketone 7400 12/08/11 R/J SW8260ug/KgNDMethyl t-butyl ether (MTBE) 3000 12/08/11 R/J SW8260ug/KgNDMethylene chloride 1500 12/08/11 R/J SW8260ug/KgNDNaphthalene 1500 12/08/11 R/J SW8260ug/Kg5500n-Butylbenzene 1500 12/08/11 R/J SW8260ug/KgNDn-Propylbenzene 1500 12/08/11 R/J SW8260ug/KgNDo-Xylene 1500 12/08/11 R/J SW8260ug/KgNDp-Isopropyltoluene 1500 12/08/11 R/J SW8260ug/Kg20000sec-Butylbenzene 1500 12/08/11 R/J SW8260ug/KgNDStyrene 1500 12/08/11 R/J SW8260ug/Kg4500tert-Butylbenzene 1500 12/08/11 R/J SW8260ug/KgNDTetrachloroethene 1500 12/08/11 R/J SW8260ug/KgNDTetrahydrofuran (THF) 3000 12/08/11 R/J SW8260ug/KgNDToluene 1500 12/08/11 R/J SW8260ug/KgNDTotal Xylenes 1500 12/08/11 R/J SW8260ug/Kg

Page 14 of 43 Ver 1

B-4 10-12 FT








101% Toluene-d8 12/08/11 R/J 70 - 130 %%

SemivolatilesND1,2-Dichlorobenzene 1400 12/06/11 D/P SW8270ug/KgND1,3-Dichlorobenzene 1400 12/06/11 D/P SW8270ug/KgND1,4-Dichlorobenzene 1400 12/06/11 D/P SW8270ug/KgND2,4-Dinitrotoluene 1400 12/06/11 D/P SW8270ug/KgND2,6-Dinitrotoluene 1400 12/06/11 D/P SW8270ug/KgND2-Chloronaphthalene 1400 12/06/11 D/P SW8270ug/KgND2-Methylnaphthalene 1400 12/06/11 D/P SW8270ug/KgND2-Nitroaniline 5700 12/06/11 D/P SW8270ug/KgND3,3'-Dichlorobenzidine 7800 12/06/11 D/P SW8270ug/KgND3-Nitroaniline 5700 12/06/11 D/P SW8270ug/KgND4-Bromophenyl phenyl ether 1400 12/06/11 D/P SW8270ug/KgND4-Chloroaniline 1400 12/06/11 D/P SW8270ug/KgND4-Chlorophenyl phenyl ether 1400 12/06/11 D/P SW8270ug/KgND4-Nitroaniline 5700 12/06/11 D/P SW8270ug/KgNDAcenaphthene 1400 12/06/11 D/P SW8270ug/KgNDAcenaphthylene 1400 12/06/11 D/P SW8270ug/KgNDAnthracene 1400 12/06/11 D/P SW8270ug/KgNDAzobenzene 1400 12/06/11 D/P SW8270ug/KgNDBenz(a)anthracene 1400 12/06/11 D/P SW8270ug/KgNDBenzidine 7800 12/06/11 D/P SW8270ug/KgNDBenzo(a)pyrene 1400 12/06/11 D/P SW8270ug/KgNDBenzo(b)fluoranthene 1400 12/06/11 D/P SW8270ug/KgNDBenzo(ghi)perylene 1400 12/06/11 D/P SW8270ug/KgNDBenzo(k)fluoranthene 1400 12/06/11 D/P SW8270ug/KgNDBenzoic acid 2000 12/06/11 D/P SW8270ug/KgNDBenzyl alcohol 1400 12/06/11 D/P SW8270ug/KgNDBenzyl butyl phthalate 1400 12/06/11 D/P SW8270ug/KgNDBis(2-chloroethoxy)methane 1400 12/06/11 D/P SW8270ug/KgNDBis(2-chloroethyl)ether 1400 12/06/11 D/P SW8270ug/KgNDBis(2-chloroisopropyl)ether 1400 12/06/11 D/P SW8270ug/KgNDBis(2-ethylhexyl)phthalate 1400 12/06/11 D/P SW8270ug/KgNDChrysene 1400 12/06/11 D/P SW8270ug/KgNDDibenz(a,h)anthracene 1400 12/06/11 D/P SW8270ug/KgNDDibenzofuran 1400 12/06/11 D/P SW8270ug/KgNDDiethyl phthalate 1400 12/06/11 D/P SW8270ug/KgNDDimethylphthalate 1400 12/06/11 D/P SW8270ug/Kg

Page 15 of 43 Ver 1

B-4 10-12 FT




NDDi-n-butylphthalate 1400 12/06/11 D/P SW8270ug/KgNDDi-n-octylphthalate 1400 12/06/11 D/P SW8270ug/KgNDFluoranthene 1400 12/06/11 D/P SW8270ug/KgNDFluorene 1400 12/06/11 D/P SW8270ug/KgNDHexachlorobenzene 1400 12/06/11 D/P SW8270ug/KgNDHexachlorobutadiene 1400 12/06/11 D/P SW8270ug/KgNDHexachlorocyclopentadiene 1400 12/06/11 D/P SW8270ug/KgNDHexachloroethane 1400 12/06/11 D/P SW8270ug/KgNDIndeno(1,2,3-cd)pyrene 1400 12/06/11 D/P SW8270ug/Kg4200Isophorone 1400 12/06/11 D/P SW8270ug/KgNDNaphthalene 1400 12/06/11 D/P SW8270ug/KgNDNitrobenzene 1400 12/06/11 D/P SW8270ug/KgNDN-Nitrosodimethylamine 1400 12/06/11 D/P SW8270ug/KgNDN-Nitrosodi-n-propylamine 1400 12/06/11 D/P SW8270ug/KgNDN-Nitrosodiphenylamine 1400 12/06/11 D/P SW8270ug/KgNDPhenanthrene 1400 12/06/11 D/P SW8270ug/KgNDPyrene 1400 12/06/11 D/P SW8270ug/Kg



101% Terphenyl-d14 12/06/11 D/P 30 - 130 %%

Comments:






December 13, 2011


Page 16 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

SOIL

EEA | B

12/03/11

LB

see "By" below

SM

Laboratory Data

B-5 11-12 FT

Phoenix ID: BB07255

12/05/11

12:00

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


< 0.37Silver 0.37 12/06/11 LK 6010/200.7mg/Kg12.2Arsenic 0.75 12/06/11 LK 6010/200.7mg/Kg51.3Barium 0.37 12/06/11 LK 6010/200.7mg/Kg2.47Cadmium 0.37 12/06/11 LK 6010/200.7mg/Kg25.7Chromium 0.37 12/06/11 LK 6010/200.7mg/Kg0.53Mercury 0.09 12/06/11 RS SW-7471mg/Kg172Lead 0.37 12/06/11 LK 6010/200.7mg/Kg3.0Selenium 1.5 12/06/11 LK 6010/200.7mg/KgCompletedTotal Metals Digest 12/05/11 AG SW846 - 3050




Page 17 of 43 Ver 1

B-5 11-12 FT





Page 18 of 43 Ver 1

B-5 11-12 FT








99% Toluene-d8 12/08/11 R/J 70 - 130 %%

SemivolatilesND1,2-Dichlorobenzene 1300 12/06/11 D/P SW8270ug/KgND1,3-Dichlorobenzene 1300 12/06/11 D/P SW8270ug/KgND1,4-Dichlorobenzene 1300 12/06/11 D/P SW8270ug/KgND2,4-Dinitrotoluene 1300 12/06/11 D/P SW8270ug/KgND2,6-Dinitrotoluene 1300 12/06/11 D/P SW8270ug/KgND2-Chloronaphthalene 1300 12/06/11 D/P SW8270ug/KgND2-Methylnaphthalene 1300 12/06/11 D/P SW8270ug/KgND2-Nitroaniline 5500 12/06/11 D/P SW8270ug/KgND3,3'-Dichlorobenzidine 7600 12/06/11 D/P SW8270ug/KgND3-Nitroaniline 5500 12/06/11 D/P SW8270ug/KgND4-Bromophenyl phenyl ether 1300 12/06/11 D/P SW8270ug/KgND4-Chloroaniline 1300 12/06/11 D/P SW8270ug/KgND4-Chlorophenyl phenyl ether 1300 12/06/11 D/P SW8270ug/KgND4-Nitroaniline 5500 12/06/11 D/P SW8270ug/Kg1400Acenaphthene 1300 12/06/11 D/P SW8270ug/KgNDAcenaphthylene 1300 12/06/11 D/P SW8270ug/KgNDAnthracene 1300 12/06/11 D/P SW8270ug/KgNDAzobenzene 1300 12/06/11 D/P SW8270ug/Kg2100Benz(a)anthracene 1300 12/06/11 D/P SW8270ug/KgNDBenzidine 7600 12/06/11 D/P SW8270ug/Kg1400Benzo(a)pyrene 1300 12/06/11 D/P SW8270ug/Kg1800Benzo(b)fluoranthene 1300 12/06/11 D/P SW8270ug/KgNDBenzo(ghi)perylene 1300 12/06/11 D/P SW8270ug/KgNDBenzo(k)fluoranthene 1300 12/06/11 D/P SW8270ug/KgNDBenzoic acid 1900 12/06/11 D/P SW8270ug/KgNDBenzyl alcohol 1300 12/06/11 D/P SW8270ug/KgNDBenzyl butyl phthalate 1300 12/06/11 D/P SW8270ug/KgNDBis(2-chloroethoxy)methane 1300 12/06/11 D/P SW8270ug/KgNDBis(2-chloroethyl)ether 1300 12/06/11 D/P SW8270ug/KgNDBis(2-chloroisopropyl)ether 1300 12/06/11 D/P SW8270ug/KgNDBis(2-ethylhexyl)phthalate 1300 12/06/11 D/P SW8270ug/Kg1700Chrysene 1300 12/06/11 D/P SW8270ug/KgNDDibenz(a,h)anthracene 1300 12/06/11 D/P SW8270ug/KgNDDibenzofuran 1300 12/06/11 D/P SW8270ug/KgNDDiethyl phthalate 1300 12/06/11 D/P SW8270ug/KgNDDimethylphthalate 1300 12/06/11 D/P SW8270ug/Kg

Page 19 of 43 Ver 1

B-5 11-12 FT




NDDi-n-butylphthalate 1300 12/06/11 D/P SW8270ug/KgNDDi-n-octylphthalate 1300 12/06/11 D/P SW8270ug/Kg7000Fluoranthene 1300 12/06/11 D/P SW8270ug/KgNDFluorene 1300 12/06/11 D/P SW8270ug/KgNDHexachlorobenzene 1300 12/06/11 D/P SW8270ug/KgNDHexachlorobutadiene 1300 12/06/11 D/P SW8270ug/KgNDHexachlorocyclopentadiene 1300 12/06/11 D/P SW8270ug/KgNDHexachloroethane 1300 12/06/11 D/P SW8270ug/KgNDIndeno(1,2,3-cd)pyrene 1300 12/06/11 D/P SW8270ug/KgNDIsophorone 1300 12/06/11 D/P SW8270ug/KgNDNaphthalene 1300 12/06/11 D/P SW8270ug/KgNDNitrobenzene 1300 12/06/11 D/P SW8270ug/KgNDN-Nitrosodimethylamine 1300 12/06/11 D/P SW8270ug/KgNDN-Nitrosodi-n-propylamine 1300 12/06/11 D/P SW8270ug/KgNDN-Nitrosodiphenylamine 1300 12/06/11 D/P SW8270ug/Kg6200Phenanthrene 1300 12/06/11 D/P SW8270ug/Kg5900Pyrene 1300 12/06/11 D/P SW8270ug/Kg



113% Terphenyl-d14 12/06/11 D/P 30 - 130 %%

Comments:






December 13, 2011


Page 20 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

SOIL

EEA | B

12/03/11

LB

see "By" below

SM

Laboratory Data

B-5 13-15 FT

Phoenix ID: BB07256

12/05/11

12:10

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


< 0.44Silver 0.44 12/06/11 LK 6010/200.7mg/Kg7.54Arsenic 0.89 12/06/11 LK 6010/200.7mg/Kg68.1Barium 0.44 12/06/11 LK 6010/200.7mg/Kg0.90Cadmium 0.44 12/06/11 LK 6010/200.7mg/Kg16.2Chromium 0.44 12/06/11 LK 6010/200.7mg/Kg0.23Mercury 0.10 12/06/11 RS SW-7471mg/Kg1080Lead 4.4 12/07/11 LK 6010/200.7mg/Kg< 1.8Selenium 1.8 12/06/11 LK 6010/200.7mg/KgCompletedTotal Metals Digest 12/05/11 AG SW846 - 3050




Page 21 of 43 Ver 1

B-5 13-15 FT





Page 22 of 43 Ver 1

B-5 13-15 FT








102% Toluene-d8 12/08/11 R/J 70 - 130 %%

SemivolatilesND1,2-Dichlorobenzene 310 12/05/11 DD SW8270ug/KgND1,3-Dichlorobenzene 310 12/05/11 DD SW8270ug/KgND1,4-Dichlorobenzene 310 12/05/11 DD SW8270ug/KgND2,4-Dinitrotoluene 310 12/05/11 DD SW8270ug/KgND2,6-Dinitrotoluene 310 12/05/11 DD SW8270ug/KgND2-Chloronaphthalene 310 12/05/11 DD SW8270ug/KgND2-Methylnaphthalene 310 12/05/11 DD SW8270ug/KgND2-Nitroaniline 1300 12/05/11 DD SW8270ug/KgND3,3'-Dichlorobenzidine 1800 12/05/11 DD SW8270ug/KgND3-Nitroaniline 1300 12/05/11 DD SW8270ug/KgND4-Bromophenyl phenyl ether 310 12/05/11 DD SW8270ug/KgND4-Chloroaniline 310 12/05/11 DD SW8270ug/KgND4-Chlorophenyl phenyl ether 310 12/05/11 DD SW8270ug/KgND4-Nitroaniline 1300 12/05/11 DD SW8270ug/KgNDAcenaphthene 310 12/05/11 DD SW8270ug/KgNDAcenaphthylene 310 12/05/11 DD SW8270ug/KgNDAnthracene 310 12/05/11 DD SW8270ug/KgNDAzobenzene 310 12/05/11 DD SW8270ug/Kg600Benz(a)anthracene 310 12/05/11 DD SW8270ug/KgNDBenzidine 1800 12/05/11 DD SW8270ug/Kg630Benzo(a)pyrene 310 12/05/11 DD SW8270ug/Kg720Benzo(b)fluoranthene 310 12/05/11 DD SW8270ug/Kg450Benzo(ghi)perylene 310 12/05/11 DD SW8270ug/KgNDBenzo(k)fluoranthene 310 12/05/11 DD SW8270ug/KgNDBenzoic acid 450 12/05/11 DD SW8270ug/KgNDBenzyl alcohol 310 12/05/11 DD SW8270ug/KgNDBenzyl butyl phthalate 310 12/05/11 DD SW8270ug/KgNDBis(2-chloroethoxy)methane 310 12/05/11 DD SW8270ug/KgNDBis(2-chloroethyl)ether 310 12/05/11 DD SW8270ug/KgNDBis(2-chloroisopropyl)ether 310 12/05/11 DD SW8270ug/KgNDBis(2-ethylhexyl)phthalate 310 12/05/11 DD SW8270ug/Kg530Chrysene 310 12/05/11 DD SW8270ug/KgNDDibenz(a,h)anthracene 310 12/05/11 DD SW8270ug/KgNDDibenzofuran 310 12/05/11 DD SW8270ug/KgNDDiethyl phthalate 310 12/05/11 DD SW8270ug/KgNDDimethylphthalate 310 12/05/11 DD SW8270ug/Kg

Page 23 of 43 Ver 1

B-5 13-15 FT




NDDi-n-butylphthalate 310 12/05/11 DD SW8270ug/KgNDDi-n-octylphthalate 310 12/05/11 DD SW8270ug/Kg1800Fluoranthene 310 12/05/11 DD SW8270ug/KgNDFluorene 310 12/05/11 DD SW8270ug/KgNDHexachlorobenzene 310 12/05/11 DD SW8270ug/KgNDHexachlorobutadiene 310 12/05/11 DD SW8270ug/KgNDHexachlorocyclopentadiene 310 12/05/11 DD SW8270ug/KgNDHexachloroethane 310 12/05/11 DD SW8270ug/Kg320Indeno(1,2,3-cd)pyrene 310 12/05/11 DD SW8270ug/KgNDIsophorone 310 12/05/11 DD SW8270ug/KgNDNaphthalene 310 12/05/11 DD SW8270ug/KgNDNitrobenzene 310 12/05/11 DD SW8270ug/KgNDN-Nitrosodimethylamine 310 12/05/11 DD SW8270ug/KgNDN-Nitrosodi-n-propylamine 310 12/05/11 DD SW8270ug/KgNDN-Nitrosodiphenylamine 310 12/05/11 DD SW8270ug/Kg1100Phenanthrene 310 12/05/11 DD SW8270ug/Kg1800Pyrene 310 12/05/11 DD SW8270ug/Kg



111% Terphenyl-d14 12/05/11 DD 30 - 130 %%

Comments:





December 13, 2011


Page 24 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

SOIL

EEA | B

12/03/11

LB

see "By" below

SM

Laboratory Data

B-6 13-15 FT

Phoenix ID: BB07257

12/05/11

13:15

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


< 0.45Silver 0.45 12/06/11 LK 6010/200.7mg/Kg53.9Arsenic 0.89 12/06/11 LK 6010/200.7mg/Kg212Barium 0.45 12/06/11 LK 6010/200.7mg/Kg1.25Cadmium 0.45 12/06/11 LK 6010/200.7mg/Kg13.3Chromium 0.45 12/06/11 LK 6010/200.7mg/Kg0.23Mercury 0.09 12/06/11 RS SW-7471mg/Kg547Lead 4.5 12/07/11 LK 6010/200.7mg/Kg3.9Selenium 1.8 12/06/11 LK 6010/200.7mg/KgCompletedTotal Metals Digest 12/05/11 AG SW846 - 3050




Page 25 of 43 Ver 1

B-6 13-15 FT




ND1,2-Dichloropropane 310 12/08/11 R/J SW8260ug/KgND1,3,5-Trimethylbenzene 310 12/08/11 R/J SW8260ug/KgND1,3-Dichlorobenzene 310 12/08/11 R/J SW8260ug/KgND1,3-Dichloropropane 310 12/08/11 R/J SW8260ug/KgND1,4-Dichlorobenzene 310 12/08/11 R/J SW8260ug/KgND2,2-Dichloropropane 310 12/08/11 R/J SW8260ug/KgND2-Chlorotoluene 310 12/08/11 R/J SW8260ug/KgND2-Hexanone 1600 12/08/11 R/J SW8260ug/Kg7902-Isopropyltoluene 310 12/08/11 R/J SW8260ug/KgND4-Chlorotoluene 310 12/08/11 R/J SW8260ug/KgND4-Methyl-2-pentanone 1600 12/08/11 R/J SW8260ug/KgNDAcetone 1600 12/08/11 R/J SW8260ug/KgNDAcrylonitrile 630 12/08/11 R/J SW8260ug/KgNDBenzene 310 12/08/11 R/J SW8260ug/KgNDBromobenzene 310 12/08/11 R/J SW8260ug/KgNDBromochloromethane 310 12/08/11 R/J SW8260ug/KgNDBromodichloromethane 310 12/08/11 R/J SW8260ug/KgNDBromoform 310 12/08/11 R/J SW8260ug/KgNDBromomethane 310 12/08/11 R/J SW8260ug/KgNDCarbon Disulfide 310 12/08/11 R/J SW8260ug/KgNDCarbon tetrachloride 310 12/08/11 R/J SW8260ug/KgNDChlorobenzene 310 12/08/11 R/J SW8260ug/KgNDChloroethane 310 12/08/11 R/J SW8260ug/KgNDChloroform 310 12/08/11 R/J SW8260ug/KgNDChloromethane 310 12/08/11 R/J SW8260ug/KgNDcis-1,2-Dichloroethene 310 12/08/11 R/J SW8260ug/KgNDcis-1,3-Dichloropropene 310 12/08/11 R/J SW8260ug/KgNDDibromochloromethane 310 12/08/11 R/J SW8260ug/KgNDDibromoethane 310 12/08/11 R/J SW8260ug/KgNDDibromomethane 310 12/08/11 R/J SW8260ug/KgNDDichlorodifluoromethane 310 12/08/11 R/J SW8260ug/KgNDEthylbenzene 310 12/08/11 R/J SW8260ug/KgNDHexachlorobutadiene 310 12/08/11 R/J SW8260ug/KgNDIsopropylbenzene 310 12/08/11 R/J SW8260ug/KgNDm&p-Xylene 310 12/08/11 R/J SW8260ug/KgNDMethyl Ethyl Ketone 1600 12/08/11 R/J SW8260ug/KgNDMethyl t-butyl ether (MTBE) 630 12/08/11 R/J SW8260ug/KgNDMethylene chloride 310 12/08/11 R/J SW8260ug/KgNDNaphthalene 310 12/08/11 R/J SW8260ug/KgNDn-Butylbenzene 310 12/08/11 R/J SW8260ug/KgNDn-Propylbenzene 310 12/08/11 R/J SW8260ug/KgNDo-Xylene 310 12/08/11 R/J SW8260ug/KgNDp-Isopropyltoluene 310 12/08/11 R/J SW8260ug/Kg350sec-Butylbenzene 310 12/08/11 R/J SW8260ug/KgNDStyrene 310 12/08/11 R/J SW8260ug/Kg780tert-Butylbenzene 310 12/08/11 R/J SW8260ug/KgNDTetrachloroethene 310 12/08/11 R/J SW8260ug/KgNDTetrahydrofuran (THF) 630 12/08/11 R/J SW8260ug/KgNDToluene 310 12/08/11 R/J SW8260ug/KgNDTotal Xylenes 310 12/08/11 R/J SW8260ug/Kg

Page 26 of 43 Ver 1

B-6 13-15 FT








101% Toluene-d8 12/08/11 R/J 70 - 130 %%

SemivolatilesND1,2-Dichlorobenzene 290 12/05/11 DD SW8270ug/KgND1,3-Dichlorobenzene 290 12/05/11 DD SW8270ug/KgND1,4-Dichlorobenzene 290 12/05/11 DD SW8270ug/KgND2,4-Dinitrotoluene 290 12/05/11 DD SW8270ug/KgND2,6-Dinitrotoluene 290 12/05/11 DD SW8270ug/KgND2-Chloronaphthalene 290 12/05/11 DD SW8270ug/KgND2-Methylnaphthalene 290 12/05/11 DD SW8270ug/KgND2-Nitroaniline 1200 12/05/11 DD SW8270ug/KgND3,3'-Dichlorobenzidine 1700 12/05/11 DD SW8270ug/KgND3-Nitroaniline 1200 12/05/11 DD SW8270ug/KgND4-Bromophenyl phenyl ether 290 12/05/11 DD SW8270ug/KgND4-Chloroaniline 290 12/05/11 DD SW8270ug/KgND4-Chlorophenyl phenyl ether 290 12/05/11 DD SW8270ug/KgND4-Nitroaniline 1200 12/05/11 DD SW8270ug/KgNDAcenaphthene 290 12/05/11 DD SW8270ug/KgNDAcenaphthylene 290 12/05/11 DD SW8270ug/KgNDAnthracene 290 12/05/11 DD SW8270ug/KgNDAzobenzene 290 12/05/11 DD SW8270ug/Kg340Benz(a)anthracene 290 12/05/11 DD SW8270ug/KgNDBenzidine 1700 12/05/11 DD SW8270ug/KgNDBenzo(a)pyrene 290 12/05/11 DD SW8270ug/Kg350Benzo(b)fluoranthene 290 12/05/11 DD SW8270ug/KgNDBenzo(ghi)perylene 290 12/05/11 DD SW8270ug/KgNDBenzo(k)fluoranthene 290 12/05/11 DD SW8270ug/KgNDBenzoic acid 410 12/05/11 DD SW8270ug/KgNDBenzyl alcohol 290 12/05/11 DD SW8270ug/KgNDBenzyl butyl phthalate 290 12/05/11 DD SW8270ug/KgNDBis(2-chloroethoxy)methane 290 12/05/11 DD SW8270ug/KgNDBis(2-chloroethyl)ether 290 12/05/11 DD SW8270ug/KgNDBis(2-chloroisopropyl)ether 290 12/05/11 DD SW8270ug/Kg320Bis(2-ethylhexyl)phthalate 290 12/05/11 DD SW8270ug/Kg300Chrysene 290 12/05/11 DD SW8270ug/KgNDDibenz(a,h)anthracene 290 12/05/11 DD SW8270ug/KgNDDibenzofuran 290 12/05/11 DD SW8270ug/KgNDDiethyl phthalate 290 12/05/11 DD SW8270ug/KgNDDimethylphthalate 290 12/05/11 DD SW8270ug/Kg

Page 27 of 43 Ver 1

B-6 13-15 FT




NDDi-n-butylphthalate 290 12/05/11 DD SW8270ug/KgNDDi-n-octylphthalate 290 12/05/11 DD SW8270ug/Kg940Fluoranthene 290 12/05/11 DD SW8270ug/KgNDFluorene 290 12/05/11 DD SW8270ug/KgNDHexachlorobenzene 290 12/05/11 DD SW8270ug/KgNDHexachlorobutadiene 290 12/05/11 DD SW8270ug/KgNDHexachlorocyclopentadiene 290 12/05/11 DD SW8270ug/KgNDHexachloroethane 290 12/05/11 DD SW8270ug/KgNDIndeno(1,2,3-cd)pyrene 290 12/05/11 DD SW8270ug/KgNDIsophorone 290 12/05/11 DD SW8270ug/KgNDNaphthalene 290 12/05/11 DD SW8270ug/KgNDNitrobenzene 290 12/05/11 DD SW8270ug/KgNDN-Nitrosodimethylamine 290 12/05/11 DD SW8270ug/KgNDN-Nitrosodi-n-propylamine 290 12/05/11 DD SW8270ug/KgNDN-Nitrosodiphenylamine 290 12/05/11 DD SW8270ug/Kg370Phenanthrene 290 12/05/11 DD SW8270ug/Kg900Pyrene 290 12/05/11 DD SW8270ug/Kg



111% Terphenyl-d14 12/05/11 DD 30 - 130 %%

Comments:





December 13, 2011


Page 28 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

GROUND WATER

EEA | B GW

12/03/11

LB

see "By" below

SM

Laboratory Data

B-1GW

Phoenix ID: BB07258

12/05/11

9:55

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


< 0.001Silver 0.001 12/06/11 LK 6010/200.7mg/L1.09Arsenic 0.004 12/06/11 LK 6010/200.7mg/L4.19Barium 0.002 12/06/11 LK 6010/200.7mg/L0.001Cadmium 0.001 12/06/11 LK 6010/200.7mg/L0.581Chromium 0.001 12/06/11 LK 6010/200.7mg/L< 0.001Silver (Dissolved) 0.001 12/06/11 LK 6010/200.7mg/L0.022Arsenic (Dissolved) 0.004 12/06/11 LK 6010/200.7mg/L0.302Barium (Dissolved) 0.002 12/06/11 LK 6010/200.7mg/L< 0.001Cadmium (Dissolved) 0.001 12/06/11 LK 6010/200.7mg/L0.011Chromium (Dissolved) 0.001 12/06/11 LK 6010/200.7mg/L< 0.0008Mercury (Dissolved) 0.0008 12/06/11 RS 7470/E245.1mg/L0.294Lead (Dissolved) 0.002 12/06/11 LK 6010/200.7mg/L0.020Selenium (Dissolved) 0.011 12/06/11 LK 6010/200.7mg/L0.0057Mercury 0.0008 12/06/11 RS 7470/E245.1mg/L19.7Lead 0.020 12/06/11 EK 6010/200.7mg/L0.117Selenium 0.010 12/08/11 EK 6010/200.7mg/LCompletedDissolved Metals Preparation 12/05/11 AG SW846-3005

CompletedTotal Metals Digestion 12/05/11 AG

CompletedFiltration 12/05/11 AG 0.45um Filter

CompletedDissolved Mercury Digestion 12/06/11 I/D SW7470

CompletedMercury Digestion 12/06/11 I/D 7471/245.1

VolatilesND1,1,1,2-Tetrachloroethane 2.0 12/07/11 R/T SW8260ug/LND1,1,1-Trichloroethane 2.0 12/07/11 R/T SW8260ug/LND1,1,2,2-Tetrachloroethane 1.0 12/07/11 R/T SW8260ug/LND1,1,2-Trichloroethane 2.0 12/07/11 R/T SW8260ug/LND1,1-Dichloroethane 2.0 12/07/11 R/T SW8260ug/L

Page 29 of 43 Ver 1

B-1GW




ND1,1-Dichloroethene 2.0 12/07/11 R/T SW8260ug/LND1,1-Dichloropropene 2.0 12/07/11 R/T SW8260ug/LND1,2,3-Trichlorobenzene 2.0 12/07/11 R/T SW8260ug/LND1,2,3-Trichloropropane 2.0 12/07/11 R/T SW8260ug/LND1,2,4-Trichlorobenzene 2.0 12/07/11 R/T SW8260ug/LND1,2,4-Trimethylbenzene 2.0 12/07/11 R/T SW8260ug/LND1,2-Dibromo-3-chloropropane 2.0 12/07/11 R/T SW8260ug/LND1,2-Dichlorobenzene 2.0 12/07/11 R/T SW8260ug/LND1,2-Dichloroethane 2.0 12/07/11 R/T SW8260ug/LND1,2-Dichloropropane 2.0 12/07/11 R/T SW8260ug/LND1,3,5-Trimethylbenzene 2.0 12/07/11 R/T SW8260ug/LND1,3-Dichlorobenzene 2.0 12/07/11 R/T SW8260ug/LND1,3-Dichloropropane 2.0 12/07/11 R/T SW8260ug/LND1,4-Dichlorobenzene 2.0 12/07/11 R/T SW8260ug/LND2,2-Dichloropropane 2.0 12/07/11 R/T SW8260ug/LND2-Chlorotoluene 2.0 12/07/11 R/T SW8260ug/LND2-Hexanone 10 12/07/11 R/T SW8260ug/L502-Isopropyltoluene 2.0 12/07/11 R/T SW8260ug/LND4-Chlorotoluene 2.0 12/07/11 R/T SW8260ug/LND4-Methyl-2-pentanone 10 12/07/11 R/T SW8260ug/LNDAcetone 50 12/07/11 R/T SW8260ug/LNDAcrylonitrile 10 12/07/11 R/T SW8260ug/LNDBenzene 2.0 12/07/11 R/T SW8260ug/LNDBromobenzene 2.0 12/07/11 R/T SW8260ug/LNDBromochloromethane 2.0 12/07/11 R/T SW8260ug/LNDBromodichloromethane 1.0 12/07/11 R/T SW8260ug/LNDBromoform 2.0 12/07/11 R/T SW8260ug/LNDBromomethane 2.0 12/07/11 R/T SW8260ug/LNDCarbon Disulfide 10 12/07/11 R/T SW8260ug/LNDCarbon tetrachloride 2.0 12/07/11 R/T SW8260ug/LNDChlorobenzene 2.0 12/07/11 R/T SW8260ug/LNDChloroethane 2.0 12/07/11 R/T SW8260ug/LNDChloroform 2.0 12/07/11 R/T SW8260ug/LNDChloromethane 2.0 12/07/11 R/T SW8260ug/LNDcis-1,2-Dichloroethene 2.0 12/07/11 R/T SW8260ug/LNDcis-1,3-Dichloropropene 1.0 12/07/11 R/T SW8260ug/LNDDibromochloromethane 1.0 12/07/11 R/T SW8260ug/LNDDibromoethane 2.0 12/07/11 R/T SW8260ug/LNDDibromomethane 2.0 12/07/11 R/T SW8260ug/LNDDichlorodifluoromethane 2.0 12/07/11 R/T SW8260ug/LNDEthylbenzene 2.0 12/07/11 R/T SW8260ug/LNDHexachlorobutadiene 0.80 12/07/11 R/T SW8260ug/L35Isopropylbenzene 2.0 12/07/11 R/T SW8260ug/LNDm&p-Xylene 2.0 12/07/11 R/T SW8260ug/LNDMethyl ethyl ketone 10 12/07/11 R/T SW8260ug/LNDMethyl t-butyl ether (MTBE) 2.0 12/07/11 R/T SW8260ug/LNDMethylene chloride 2.0 12/07/11 R/T SW8260ug/LNDNaphthalene 2.0 12/07/11 R/T SW8260ug/LNDn-Butylbenzene 2.0 12/07/11 R/T SW8260ug/L3.0n-Propylbenzene 2.0 12/07/11 R/T SW8260ug/L

Page 30 of 43 Ver 1

B-1GW




NDo-Xylene 2.0 12/07/11 R/T SW8260ug/LNDp-Isopropyltoluene 2.0 12/07/11 R/T SW8260ug/L130sec-Butylbenzene 5.0 12/07/11 R/T SW8260ug/LNDStyrene 2.0 12/07/11 R/T SW8260ug/L37tert-Butylbenzene 2.0 12/07/11 R/T SW8260ug/LNDTetrachloroethene 2.0 12/07/11 R/T SW8260ug/LNDTetrahydrofuran (THF) 10 12/07/11 R/T SW8260ug/LNDToluene 2.0 12/07/11 R/T SW8260ug/LNDTotal Xylenes 2.0 12/07/11 R/T SW8260ug/LNDtrans-1,2-Dichloroethene 2.0 12/07/11 R/T SW8260ug/LNDtrans-1,3-Dichloropropene 1.0 12/07/11 R/T SW8260ug/LNDtrans-1,4-dichloro-2-butene 10 12/07/11 R/T SW8260ug/LNDTrichloroethene 2.0 12/07/11 R/T SW8260ug/LNDTrichlorofluoromethane 2.0 12/07/11 R/T SW8260ug/LNDTrichlorotrifluoroethane 2.0 12/07/11 R/T SW8260ug/LNDVinyl chloride 2.0 12/07/11 R/T SW8260ug/L

QA/QC Surrogates128% 1,2-dichlorobenzene-d4 12/07/11 R/T 70 - 130 %%

129% Bromofluorobenzene 12/07/11 R/T 70 - 130 %%

92% Dibromofluoromethane 12/07/11 R/T 70 - 130 %%

99% Toluene-d8 12/07/11 R/T 70 - 130 %%

Comments:




December 13, 2011


Page 31 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

GROUND WATER

EEA | B GW

12/03/11

LB

see "By" below

SM

Laboratory Data

B-2GW

Phoenix ID: BB07259

12/05/11

10:40

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


< 0.001Silver 0.001 12/06/11 LK 6010/200.7mg/L39.7Arsenic 0.40 12/06/11 EK 6010/200.7mg/L4.30Barium 0.002 12/06/11 LK 6010/200.7mg/L< 0.010Cadmium 0.010 12/06/11 EK 6010/200.7mg/L1.43Chromium 0.001 12/06/11 LK 6010/200.7mg/L< 0.001Silver (Dissolved) 0.001 12/05/11 LK 6010/200.7mg/L2.36Arsenic (Dissolved) 0.043 12/06/11 EK 6010/200.7mg/L0.100Barium (Dissolved) 0.002 12/05/11 LK 6010/200.7mg/L< 0.001Cadmium (Dissolved) 0.001 12/05/11 LK 6010/200.7mg/L0.009Chromium (Dissolved) 0.001 12/05/11 LK 6010/200.7mg/L< 0.0008Mercury (Dissolved) 0.0008 12/06/11 RS 7470/E245.1mg/L0.061Lead (Dissolved) 0.002 12/05/11 LK 6010/200.7mg/L0.022Selenium (Dissolved) 0.011 12/05/11 LK 6010/200.7mg/L< 0.0008Mercury 0.0008 12/06/11 RS 7470/E245.1mg/L13.5Lead 0.020 12/06/11 EK 6010/200.7mg/L0.796Selenium 0.010 12/08/11 EK 6010/200.7mg/LCompletedDissolved Metals Preparation 12/05/11 AG SW846-3005






Page 32 of 43 Ver 1

B-2GW




ND1,1-Dichloroethene 1.0 12/07/11 R/T SW8260ug/LND1,1-Dichloropropene 1.0 12/07/11 R/T SW8260ug/LND1,2,3-Trichlorobenzene 1.0 12/07/11 R/T SW8260ug/LND1,2,3-Trichloropropane 1.0 12/07/11 R/T SW8260ug/LND1,2,4-Trichlorobenzene 1.0 12/07/11 R/T SW8260ug/LND1,2,4-Trimethylbenzene 1.0 12/07/11 R/T SW8260ug/LND1,2-Dibromo-3-chloropropane 1.0 12/07/11 R/T SW8260ug/LND1,2-Dichlorobenzene 1.0 12/07/11 R/T SW8260ug/LND1,2-Dichloroethane 1.0 12/07/11 R/T SW8260ug/LND1,2-Dichloropropane 1.0 12/07/11 R/T SW8260ug/LND1,3,5-Trimethylbenzene 1.0 12/07/11 R/T SW8260ug/LND1,3-Dichlorobenzene 1.0 12/07/11 R/T SW8260ug/LND1,3-Dichloropropane 1.0 12/07/11 R/T SW8260ug/LND1,4-Dichlorobenzene 1.0 12/07/11 R/T SW8260ug/LND2,2-Dichloropropane 1.0 12/07/11 R/T SW8260ug/LND2-Chlorotoluene 1.0 12/07/11 R/T SW8260ug/LND2-Hexanone 5.0 12/07/11 R/T SW8260ug/LND2-Isopropyltoluene 1.0 12/07/11 R/T SW8260ug/LND4-Chlorotoluene 1.0 12/07/11 R/T SW8260ug/LND4-Methyl-2-pentanone 5.0 12/07/11 R/T SW8260ug/LNDAcetone 25 12/07/11 R/T SW8260ug/LNDAcrylonitrile 5.0 12/07/11 R/T SW8260ug/LNDBenzene 1.0 12/07/11 R/T SW8260ug/LNDBromobenzene 1.0 12/07/11 R/T SW8260ug/LNDBromochloromethane 1.0 12/07/11 R/T SW8260ug/LNDBromodichloromethane 0.50 12/07/11 R/T SW8260ug/LNDBromoform 1.0 12/07/11 R/T SW8260ug/LNDBromomethane 1.0 12/07/11 R/T SW8260ug/LNDCarbon Disulfide 5.0 12/07/11 R/T SW8260ug/LNDCarbon tetrachloride 1.0 12/07/11 R/T SW8260ug/LNDChlorobenzene 1.0 12/07/11 R/T SW8260ug/LNDChloroethane 1.0 12/07/11 R/T SW8260ug/LNDChloroform 1.0 12/07/11 R/T SW8260ug/LNDChloromethane 1.0 12/07/11 R/T SW8260ug/LNDcis-1,2-Dichloroethene 1.0 12/07/11 R/T SW8260ug/LNDcis-1,3-Dichloropropene 0.50 12/07/11 R/T SW8260ug/LNDDibromochloromethane 0.50 12/07/11 R/T SW8260ug/LNDDibromoethane 1.0 12/07/11 R/T SW8260ug/LNDDibromomethane 1.0 12/07/11 R/T SW8260ug/LNDDichlorodifluoromethane 1.0 12/07/11 R/T SW8260ug/LNDEthylbenzene 1.0 12/07/11 R/T SW8260ug/LNDHexachlorobutadiene 0.40 12/07/11 R/T SW8260ug/LNDIsopropylbenzene 1.0 12/07/11 R/T SW8260ug/LNDm&p-Xylene 1.0 12/07/11 R/T SW8260ug/LNDMethyl ethyl ketone 5.0 12/07/11 R/T SW8260ug/LNDMethyl t-butyl ether (MTBE) 1.0 12/07/11 R/T SW8260ug/LNDMethylene chloride 1.0 12/07/11 R/T SW8260ug/LNDNaphthalene 1.0 12/07/11 R/T SW8260ug/LNDn-Butylbenzene 1.0 12/07/11 R/T SW8260ug/LNDn-Propylbenzene 1.0 12/07/11 R/T SW8260ug/L

Page 33 of 43 Ver 1

B-2GW




NDo-Xylene 1.0 12/07/11 R/T SW8260ug/L3.1p-Isopropyltoluene 1.0 12/07/11 R/T SW8260ug/L1.2sec-Butylbenzene 1.0 12/07/11 R/T SW8260ug/LNDStyrene 1.0 12/07/11 R/T SW8260ug/LNDtert-Butylbenzene 1.0 12/07/11 R/T SW8260ug/LNDTetrachloroethene 1.0 12/07/11 R/T SW8260ug/LNDTetrahydrofuran (THF) 5.0 12/07/11 R/T SW8260ug/LNDToluene 1.0 12/07/11 R/T SW8260ug/LNDTotal Xylenes 1.0 12/07/11 R/T SW8260ug/LNDtrans-1,2-Dichloroethene 1.0 12/07/11 R/T SW8260ug/LNDtrans-1,3-Dichloropropene 0.50 12/07/11 R/T SW8260ug/LNDtrans-1,4-dichloro-2-butene 5.0 12/07/11 R/T SW8260ug/LNDTrichloroethene 1.0 12/07/11 R/T SW8260ug/LNDTrichlorofluoromethane 1.0 12/07/11 R/T SW8260ug/LNDTrichlorotrifluoroethane 1.0 12/07/11 R/T SW8260ug/LNDVinyl chloride 1.0 12/07/11 R/T SW8260ug/L




104% Toluene-d8 12/07/11 R/T 70 - 130 %%

Comments:




December 13, 2011


Page 34 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

GROUND WATER

EEA | B GW

12/03/11

LB

see "By" below

SM

Laboratory Data

B-4GW

Phoenix ID: BB07260

12/05/11

11:50

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


0.010Silver 0.001 12/06/11 LK 6010/200.7mg/L2.59Arsenic 0.040 12/06/11 EK 6010/200.7mg/L9.05Barium 0.002 12/06/11 LK 6010/200.7mg/L0.034Cadmium 0.001 12/06/11 LK 6010/200.7mg/L1.41Chromium 0.001 12/06/11 LK 6010/200.7mg/L< 0.001Silver (Dissolved) 0.001 12/06/11 LK 6010/200.7mg/L0.120Arsenic (Dissolved) 0.004 12/06/11 LK 6010/200.7mg/L0.121Barium (Dissolved) 0.002 12/06/11 LK 6010/200.7mg/L< 0.001Cadmium (Dissolved) 0.001 12/06/11 LK 6010/200.7mg/L0.006Chromium (Dissolved) 0.001 12/06/11 LK 6010/200.7mg/L< 0.0008Mercury (Dissolved) 0.0008 12/06/11 RS 7470/E245.1mg/L0.065Lead (Dissolved) 0.002 12/06/11 LK 6010/200.7mg/L0.011Selenium (Dissolved) 0.011 12/06/11 LK 6010/200.7mg/L< 0.0008Mercury 0.0008 12/06/11 RS 7470/E245.1mg/L25.4Lead 0.20 12/06/11 EK 6010/200.7mg/L0.336Selenium 0.010 12/08/11 EK 6010/200.7mg/LCompletedDissolved Metals Preparation 12/05/11 AG SW846-3005






Page 35 of 43 Ver 1

B-4GW




ND1,1-Dichloroethene 5.0 12/08/11 R/T SW8260ug/LND1,1-Dichloropropene 5.0 12/08/11 R/T SW8260ug/LND1,2,3-Trichlorobenzene 5.0 12/08/11 R/T SW8260ug/LND1,2,3-Trichloropropane 5.0 12/08/11 R/T SW8260ug/LND1,2,4-Trichlorobenzene 5.0 12/08/11 R/T SW8260ug/LND1,2,4-Trimethylbenzene 5.0 12/08/11 R/T SW8260ug/LND1,2-Dibromo-3-chloropropane 5.0 12/08/11 R/T SW8260ug/LND1,2-Dichlorobenzene 5.0 12/08/11 R/T SW8260ug/LND1,2-Dichloroethane 5.0 12/08/11 R/T SW8260ug/LND1,2-Dichloropropane 5.0 12/08/11 R/T SW8260ug/LND1,3,5-Trimethylbenzene 5.0 12/08/11 R/T SW8260ug/LND1,3-Dichlorobenzene 5.0 12/08/11 R/T SW8260ug/LND1,3-Dichloropropane 5.0 12/08/11 R/T SW8260ug/LND1,4-Dichlorobenzene 5.0 12/08/11 R/T SW8260ug/LND2,2-Dichloropropane 5.0 12/08/11 R/T SW8260ug/LND2-Chlorotoluene 5.0 12/08/11 R/T SW8260ug/LND2-Hexanone 25 12/08/11 R/T SW8260ug/L652-Isopropyltoluene 5.0 12/08/11 R/T SW8260ug/LND4-Chlorotoluene 5.0 12/08/11 R/T SW8260ug/LND4-Methyl-2-pentanone 25 12/08/11 R/T SW8260ug/LNDAcetone 130 12/08/11 R/T SW8260ug/LNDAcrylonitrile 25 12/08/11 R/T SW8260ug/LNDBenzene 5.0 12/08/11 R/T SW8260ug/LNDBromobenzene 5.0 12/08/11 R/T SW8260ug/LNDBromochloromethane 5.0 12/08/11 R/T SW8260ug/LNDBromodichloromethane 2.5 12/08/11 R/T SW8260ug/LNDBromoform 5.0 12/08/11 R/T SW8260ug/LNDBromomethane 5.0 12/08/11 R/T SW8260ug/LNDCarbon Disulfide 25 12/08/11 R/T SW8260ug/LNDCarbon tetrachloride 5.0 12/08/11 R/T SW8260ug/LNDChlorobenzene 5.0 12/08/11 R/T SW8260ug/LNDChloroethane 5.0 12/08/11 R/T SW8260ug/LNDChloroform 5.0 12/08/11 R/T SW8260ug/LNDChloromethane 5.0 12/08/11 R/T SW8260ug/LNDcis-1,2-Dichloroethene 5.0 12/08/11 R/T SW8260ug/LNDcis-1,3-Dichloropropene 2.5 12/08/11 R/T SW8260ug/LNDDibromochloromethane 2.5 12/08/11 R/T SW8260ug/LNDDibromoethane 5.0 12/08/11 R/T SW8260ug/LNDDibromomethane 5.0 12/08/11 R/T SW8260ug/LNDDichlorodifluoromethane 5.0 12/08/11 R/T SW8260ug/LNDEthylbenzene 5.0 12/08/11 R/T SW8260ug/LNDHexachlorobutadiene 2.0 12/08/11 R/T SW8260ug/L6.8Isopropylbenzene 5.0 12/08/11 R/T SW8260ug/LNDm&p-Xylene 5.0 12/08/11 R/T SW8260ug/LNDMethyl ethyl ketone 25 12/08/11 R/T SW8260ug/LNDMethyl t-butyl ether (MTBE) 5.0 12/08/11 R/T SW8260ug/LNDMethylene chloride 5.0 12/08/11 R/T SW8260ug/LNDNaphthalene 5.0 12/08/11 R/T SW8260ug/L34n-Butylbenzene 5.0 12/08/11 R/T SW8260ug/LNDn-Propylbenzene 5.0 12/08/11 R/T SW8260ug/L

Page 36 of 43 Ver 1

B-4GW




NDo-Xylene 5.0 12/08/11 R/T SW8260ug/LNDp-Isopropyltoluene 5.0 12/08/11 R/T SW8260ug/L110sec-Butylbenzene 5.0 12/08/11 R/T SW8260ug/LNDStyrene 5.0 12/08/11 R/T SW8260ug/L33tert-Butylbenzene 5.0 12/08/11 R/T SW8260ug/LNDTetrachloroethene 5.0 12/08/11 R/T SW8260ug/LNDTetrahydrofuran (THF) 25 12/08/11 R/T SW8260ug/LNDToluene 5.0 12/08/11 R/T SW8260ug/LNDTotal Xylenes 5.0 12/08/11 R/T SW8260ug/LNDtrans-1,2-Dichloroethene 5.0 12/08/11 R/T SW8260ug/LNDtrans-1,3-Dichloropropene 2.5 12/08/11 R/T SW8260ug/LNDtrans-1,4-dichloro-2-butene 25 12/08/11 R/T SW8260ug/LNDTrichloroethene 5.0 12/08/11 R/T SW8260ug/LNDTrichlorofluoromethane 5.0 12/08/11 R/T SW8260ug/LNDTrichlorotrifluoroethane 5.0 12/08/11 R/T SW8260ug/LNDVinyl chloride 5.0 12/08/11 R/T SW8260ug/L




103% Toluene-d8 12/08/11 R/T 70 - 130 %%

Comments:





December 13, 2011


Page 37 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

GROUND WATER

EEA | B GW

12/03/11

LB

see "By" below

SM

Laboratory Data

B-6GW

Phoenix ID: BB07261

12/05/11

13:25

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


< 0.010Silver 0.010 12/06/11 EK 6010/200.7mg/L0.479Arsenic 0.004 12/06/11 LK 6010/200.7mg/L2.09Barium 0.002 12/06/11 LK 6010/200.7mg/L0.012Cadmium 0.001 12/06/11 LK 6010/200.7mg/L0.160Chromium 0.001 12/06/11 LK 6010/200.7mg/L< 0.001Silver (Dissolved) 0.001 12/06/11 LK 6010/200.7mg/L0.014Arsenic (Dissolved) 0.004 12/06/11 LK 6010/200.7mg/L0.088Barium (Dissolved) 0.002 12/06/11 LK 6010/200.7mg/L< 0.001Cadmium (Dissolved) 0.001 12/06/11 LK 6010/200.7mg/L< 0.001Chromium (Dissolved) 0.001 12/06/11 LK 6010/200.7mg/L< 0.0008Mercury (Dissolved) 0.0008 12/06/11 RS 7470/E245.1mg/L0.009Lead (Dissolved) 0.002 12/06/11 LK 6010/200.7mg/L< 0.011Selenium (Dissolved) 0.011 12/06/11 LK 6010/200.7mg/L< 0.0008Mercury 0.0008 12/06/11 RS 7470/E245.1mg/L3.40Lead 0.020 12/06/11 EK 6010/200.7mg/L0.121Selenium 0.010 12/08/11 EK 6010/200.7mg/LCompletedDissolved Metals Preparation 12/05/11 AG SW846-3005






Page 38 of 43 Ver 1

B-6GW




ND1,1-Dichloroethene 2.0 12/08/11 R/T SW8260ug/LND1,1-Dichloropropene 2.0 12/08/11 R/T SW8260ug/LND1,2,3-Trichlorobenzene 2.0 12/08/11 R/T SW8260ug/LND1,2,3-Trichloropropane 2.0 12/08/11 R/T SW8260ug/LND1,2,4-Trichlorobenzene 2.0 12/08/11 R/T SW8260ug/LND1,2,4-Trimethylbenzene 2.0 12/08/11 R/T SW8260ug/LND1,2-Dibromo-3-chloropropane 2.0 12/08/11 R/T SW8260ug/LND1,2-Dichlorobenzene 2.0 12/08/11 R/T SW8260ug/LND1,2-Dichloroethane 2.0 12/08/11 R/T SW8260ug/LND1,2-Dichloropropane 2.0 12/08/11 R/T SW8260ug/LND1,3,5-Trimethylbenzene 2.0 12/08/11 R/T SW8260ug/LND1,3-Dichlorobenzene 2.0 12/08/11 R/T SW8260ug/LND1,3-Dichloropropane 2.0 12/08/11 R/T SW8260ug/LND1,4-Dichlorobenzene 2.0 12/08/11 R/T SW8260ug/LND2,2-Dichloropropane 2.0 12/08/11 R/T SW8260ug/LND2-Chlorotoluene 2.0 12/08/11 R/T SW8260ug/LND2-Hexanone 10 12/08/11 R/T SW8260ug/L142-Isopropyltoluene 2.0 12/08/11 R/T SW8260ug/LND4-Chlorotoluene 2.0 12/08/11 R/T SW8260ug/LND4-Methyl-2-pentanone 10 12/08/11 R/T SW8260ug/LNDAcetone 50 12/08/11 R/T SW8260ug/LNDAcrylonitrile 10 12/08/11 R/T SW8260ug/LNDBenzene 2.0 12/08/11 R/T SW8260ug/LNDBromobenzene 2.0 12/08/11 R/T SW8260ug/LNDBromochloromethane 2.0 12/08/11 R/T SW8260ug/LNDBromodichloromethane 1.0 12/08/11 R/T SW8260ug/LNDBromoform 2.0 12/08/11 R/T SW8260ug/LNDBromomethane 2.0 12/08/11 R/T SW8260ug/LNDCarbon Disulfide 10 12/08/11 R/T SW8260ug/LNDCarbon tetrachloride 2.0 12/08/11 R/T SW8260ug/LNDChlorobenzene 2.0 12/08/11 R/T SW8260ug/LNDChloroethane 2.0 12/08/11 R/T SW8260ug/LNDChloroform 2.0 12/08/11 R/T SW8260ug/LNDChloromethane 2.0 12/08/11 R/T SW8260ug/LNDcis-1,2-Dichloroethene 2.0 12/08/11 R/T SW8260ug/LNDcis-1,3-Dichloropropene 1.0 12/08/11 R/T SW8260ug/LNDDibromochloromethane 1.0 12/08/11 R/T SW8260ug/LNDDibromoethane 2.0 12/08/11 R/T SW8260ug/LNDDibromomethane 2.0 12/08/11 R/T SW8260ug/LNDDichlorodifluoromethane 2.0 12/08/11 R/T SW8260ug/LNDEthylbenzene 2.0 12/08/11 R/T SW8260ug/LNDHexachlorobutadiene 0.80 12/08/11 R/T SW8260ug/LNDIsopropylbenzene 2.0 12/08/11 R/T SW8260ug/LNDm&p-Xylene 2.0 12/08/11 R/T SW8260ug/LNDMethyl ethyl ketone 10 12/08/11 R/T SW8260ug/LNDMethyl t-butyl ether (MTBE) 2.0 12/08/11 R/T SW8260ug/LNDMethylene chloride 2.0 12/08/11 R/T SW8260ug/LNDNaphthalene 2.0 12/08/11 R/T SW8260ug/LNDn-Butylbenzene 2.0 12/08/11 R/T SW8260ug/LNDn-Propylbenzene 2.0 12/08/11 R/T SW8260ug/L

Page 39 of 43 Ver 1

B-6GW




NDo-Xylene 2.0 12/08/11 R/T SW8260ug/LNDp-Isopropyltoluene 2.0 12/08/11 R/T SW8260ug/L4.0sec-Butylbenzene 2.0 12/08/11 R/T SW8260ug/LNDStyrene 2.0 12/08/11 R/T SW8260ug/L14tert-Butylbenzene 2.0 12/08/11 R/T SW8260ug/LNDTetrachloroethene 2.0 12/08/11 R/T SW8260ug/LNDTetrahydrofuran (THF) 10 12/08/11 R/T SW8260ug/LNDToluene 2.0 12/08/11 R/T SW8260ug/LNDTotal Xylenes 2.0 12/08/11 R/T SW8260ug/LNDtrans-1,2-Dichloroethene 2.0 12/08/11 R/T SW8260ug/LNDtrans-1,3-Dichloropropene 1.0 12/08/11 R/T SW8260ug/LNDtrans-1,4-dichloro-2-butene 10 12/08/11 R/T SW8260ug/LNDTrichloroethene 2.0 12/08/11 R/T SW8260ug/LNDTrichlorofluoromethane 2.0 12/08/11 R/T SW8260ug/LNDTrichlorotrifluoroethane 2.0 12/08/11 R/T SW8260ug/LNDVinyl chloride 2.0 12/08/11 R/T SW8260ug/L


189% Bromofluorobenzene 12/08/11 R/T 70 - 130 %% 3


101% Toluene-d8 12/08/11 R/T 70 - 130 %%

Comments:


Elevated reporting limits for volatiles due to the oily nature of the sample.



December 13, 2011

3 = This parameter exceeds laboratory specified limits.


Page 40 of 43 Ver 1



Rush Request:

P.O.#:


Analyzed by:

WATER

EEA | TRIP BLANK

12/03/11

LB

see "By" below

SM

Laboratory Data

TRIP BLANK

Phoenix ID: BB07361

12/05/11

0:00

16:00




Time

Date Time



SDG ID: GBB07251

Client ID:


VolatilesND1,1,1,2-Tetrachloroethane 1.0 12/06/11 H/T SW8260ug/LND1,1,1-Trichloroethane 1.0 12/06/11 H/T SW8260ug/LND1,1,2,2-Tetrachloroethane 0.50 12/06/11 H/T SW8260ug/LND1,1,2-Trichloroethane 1.0 12/06/11 H/T SW8260ug/LND1,1-Dichloroethane 1.0 12/06/11 H/T SW8260ug/LND1,1-Dichloroethene 1.0 12/06/11 H/T SW8260ug/LND1,1-Dichloropropene 1.0 12/06/11 H/T SW8260ug/LND1,2,3-Trichlorobenzene 1.0 12/06/11 H/T SW8260ug/LND1,2,3-Trichloropropane 1.0 12/06/11 H/T SW8260ug/LND1,2,4-Trichlorobenzene 1.0 12/06/11 H/T SW8260ug/LND1,2,4-Trimethylbenzene 1.0 12/06/11 H/T SW8260ug/LND1,2-Dibromo-3-chloropropane 1.0 12/06/11 H/T SW8260ug/LND1,2-Dichlorobenzene 1.0 12/06/11 H/T SW8260ug/LND1,2-Dichloroethane 1.0 12/06/11 H/T SW8260ug/LND1,2-Dichloropropane 1.0 12/06/11 H/T SW8260ug/LND1,3,5-Trimethylbenzene 1.0 12/06/11 H/T SW8260ug/LND1,3-Dichlorobenzene 1.0 12/06/11 H/T SW8260ug/LND1,3-Dichloropropane 1.0 12/06/11 H/T SW8260ug/LND1,4-Dichlorobenzene 1.0 12/06/11 H/T SW8260ug/LND2,2-Dichloropropane 1.0 12/06/11 H/T SW8260ug/LND2-Chlorotoluene 1.0 12/06/11 H/T SW8260ug/LND2-Hexanone 5.0 12/06/11 H/T SW8260ug/LND2-Isopropyltoluene 1.0 12/06/11 H/T SW8260ug/LND4-Chlorotoluene 1.0 12/06/11 H/T SW8260ug/LND4-Methyl-2-pentanone 5.0 12/06/11 H/T SW8260ug/LNDAcetone 25 12/06/11 H/T SW8260ug/L

Page 41 of 43 Ver 1

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NDAcrylonitrile 5.0 12/06/11 H/T SW8260ug/LNDBenzene 1.0 12/06/11 H/T SW8260ug/LNDBromobenzene 1.0 12/06/11 H/T SW8260ug/LNDBromochloromethane 1.0 12/06/11 H/T SW8260ug/LNDBromodichloromethane 0.50 12/06/11 H/T SW8260ug/LNDBromoform 1.0 12/06/11 H/T SW8260ug/LNDBromomethane 1.0 12/06/11 H/T SW8260ug/LNDCarbon Disulfide 5.0 12/06/11 H/T SW8260ug/LNDCarbon tetrachloride 1.0 12/06/11 H/T SW8260ug/LNDChlorobenzene 1.0 12/06/11 H/T SW8260ug/LNDChloroethane 1.0 12/06/11 H/T SW8260ug/LNDChloroform 1.0 12/06/11 H/T SW8260ug/LNDChloromethane 1.0 12/06/11 H/T SW8260ug/LNDcis-1,2-Dichloroethene 1.0 12/06/11 H/T SW8260ug/LNDcis-1,3-Dichloropropene 0.50 12/06/11 H/T SW8260ug/LNDDibromochloromethane 0.50 12/06/11 H/T SW8260ug/LNDDibromoethane 1.0 12/06/11 H/T SW8260ug/LNDDibromomethane 1.0 12/06/11 H/T SW8260ug/LNDDichlorodifluoromethane 1.0 12/06/11 H/T SW8260ug/LNDEthylbenzene 1.0 12/06/11 H/T SW8260ug/LNDHexachlorobutadiene 0.40 12/06/11 H/T SW8260ug/LNDIsopropylbenzene 1.0 12/06/11 H/T SW8260ug/LNDm&p-Xylene 1.0 12/06/11 H/T SW8260ug/LNDMethyl ethyl ketone 5.0 12/06/11 H/T SW8260ug/LNDMethyl t-butyl ether (MTBE) 1.0 12/06/11 H/T SW8260ug/LNDMethylene chloride 1.0 12/06/11 H/T SW8260ug/LNDNaphthalene 1.0 12/06/11 H/T SW8260ug/LNDn-Butylbenzene 1.0 12/06/11 H/T SW8260ug/LNDn-Propylbenzene 1.0 12/06/11 H/T SW8260ug/LNDo-Xylene 1.0 12/06/11 H/T SW8260ug/LNDp-Isopropyltoluene 1.0 12/06/11 H/T SW8260ug/LNDsec-Butylbenzene 1.0 12/06/11 H/T SW8260ug/LNDStyrene 1.0 12/06/11 H/T SW8260ug/LNDtert-Butylbenzene 1.0 12/06/11 H/T SW8260ug/LNDTetrachloroethene 1.0 12/06/11 H/T SW8260ug/LNDTetrahydrofuran (THF) 5.0 12/06/11 H/T SW8260ug/LNDToluene 1.0 12/06/11 H/T SW8260ug/LNDTotal Xylenes 1.0 12/06/11 H/T SW8260ug/LNDtrans-1,2-Dichloroethene 1.0 12/06/11 H/T SW8260ug/LNDtrans-1,3-Dichloropropene 0.50 12/06/11 H/T SW8260ug/LNDtrans-1,4-dichloro-2-butene 5.0 12/06/11 H/T SW8260ug/LNDTrichloroethene 1.0 12/06/11 H/T SW8260ug/LNDTrichlorofluoromethane 1.0 12/06/11 H/T SW8260ug/LNDTrichlorotrifluoroethane 1.0 12/06/11 H/T SW8260ug/LNDVinyl chloride 1.0 12/06/11 H/T SW8260ug/L

QA/QC Surrogates101% 1,2-dichlorobenzene-d4 12/06/11 H/T 70 - 130 %%

99% Bromofluorobenzene 12/06/11 H/T 70 - 130 %%

102% Dibromofluoromethane 12/06/11 H/T 70 - 130 %%

104% Toluene-d8 12/06/11 H/T 70 - 130 %%

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December 13, 2011


Page 43 of 43 Ver 1

APPENDIX D

SOIL BORING LOGS

EEA, INC. 55 HILTON AVENUE, GARDEN CITY, NEW YORK

SOIL BORING REPORT LOG DATE: 12/03/11 SHEET 1 OF 6

CLIENT: Silverstone Property Group LOCATION ID#

PROJECT LOCATION: 55 Eckford Street, Brooklyn, New York B – 1/GW-1 REMARKS: Sample taken in area of former electro-plating facility as depicted on Sanborn Atlas. PROJECT #11734

DRILLING CONTRACTOR: TSDT, INC. LOGGED BY SM DRILLER PR

EQUIPMENT SOIL SAMPLER HAMMER

WEIGHT/FALL Casing Type Monitor Well Specification DRILL RIG

DRILL METHOD

TYPE MACROCORE GEOPROBE LT 54

MACROCORE SIZE 2 inch O.D.

SURFACE ELEVATION: NA Surface Materials: Soil

WATER DEPTH (IN OPEN BOREHOLE): 12 feet DEPTH

(fbg) SAMPLE DEPTH OVA (ppm) MOISTURE STRATA SOIL – ROCK DESCRIPTION – CLASSIFICATION

0 S-1 0 - 4 0.0 Dry

Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material Stained grey, silty fine sand with fine gravel, very strong solvent odor. Groundwater @ ~12’ below grade (bg). End of Boring (EOB) @ 16’ bg. * *soil and groundwater sample collected for laboratory analysis

5 S-2 4 - 8 0.0 Dry

10 S-3 8 – 12 0.0 Dry

15 S-4 12 – 16** 1005 Moist/Wet 20




PROJECT LOCATION: 55 Eckford Street, Brooklyn, New York B – 2/GW-2 REMARKS: Sample taken in area of former electro-plating facility as depicted on Sanborn Atlas. PROJECT #11734




DRILL METHOD



SURFACE ELEVATION: NA Surface Materials: 4” asphalt

WATER DEPTH (IN OPEN BOREHOLE): 12 feet DEPTH


0 S-1 0 - 4 0.0 Dry

Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material – Brown/grey, silty fine sand with some gravel, no odors/staining Groundwater @ ~12’ below grade (bg). End of Boring (EOB) @ 16’ bg. * *soil and groundwater sample collected for laboratory analysis

5 S-2 4 - 8 0.0 Dry

10 S-3 8 – 12 0.0 Dry

15 S-4 12 – 16** 0.0 Moist/Wet 20




PROJECT LOCATION: 55 Eckford Street, Brooklyn, New York B – 3 REMARKS: Sample taken on in northwestern area of subject property PROJECT #11734




DRILL METHOD




WATER LEVEL (IN OPEN BOREHOLE): @ 8’ bg DEPTH


0 S-1 0 - 4 0.0 Dry

Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material - Stained grey, silty fine sand with fine gravel, strong solvent odor. Groundwater @ ~8’ below grade (bg). Note: grade elevation is lower at this boring than B-1 and B-2. End of Boring (EOB) @ 12’ bg. * soil sample collected for laboratory analysis; NOTE: PVC Well with screen was installed in this boring but due to siltyness of soil, well did not produce water

5 S-2 4 - 8 0.0 Dry

10 S-3* 8 – 12 129.0 Moist/Wet

15 20




PROJECT LOCATION: 55 Eckford Street, Brooklyn, New York B – 4/B-4GWREMARKS: Sample taken near former lacquer spraying facility as depicted on Sanborn PROJECT #11734




DRILL METHOD




WATER LEVEL (IN OPEN BOREHOLE): DEPTH


0 S-1 0 - 4 0.0 Dry

Fill Material – Brown, silty fine sand with brick, concrete and asphalt. 4’ – 7’ - Fill Material – Brown, silty fine sand with brick, concrete and asphalt. 7’ – 12’ - Fill Material - Stained grey, silty fine sand with fine gravel, very strong solvent odor especially at 11’ bg. Groundwater @ ~7’ below grade (bg). Note: grade elevation is lower at this boring than B-1 and B-2. End of Boring (EOB) @ 12’ bg. * *soil and groundwater sample collected for laboratory analysis

5 S-2 4 - 8 0.0 Dry/Moist

10 S-3** 8 – 12 1030 Moist/Wet




PROJECT LOCATION: 55 Eckford Street, Brooklyn, New York B – 5 REMARKS: Sample taken in area of lacquer spraying facility as depicted on Sanborn PROJECT #11734




DRILL METHOD




WATER LEVEL (IN OPEN BOREHOLE): 20 feet DEPTH


0 S-1 0 - 4 0.0 Dry

Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material – Brown, silty fine sand with brick, concrete and asphalt. 10’ – 12’ – Black silty sand and gravel, strong solvent odor Fill Material Stained grey, silty fine sand with fine gravel, solvent odor. Groundwater @ ~13’ below grade (bg). End of Boring (EOB) @ 16’ bg. * soil sample collected for laboratory analysis; NOTE: PVC Well with screen was installed in this boring but due to siltyness of soil, well did not produce water

5 S-2 4 - 8 0.0 Dry

10 S-3 8 – 12 389 Dry

15 S-4 12 – 16* 189 Moist/Wet




PROJECT LOCATION: 55 Eckford Street, Brooklyn, New York B – 6 REMARKS: Sample taken in area of 500 gallon UST. PROJECT #11734




DRILL METHOD



SURFACE ELEVATION: NA Surface Materials: Asphalt Parking Lot

WATER LEVEL (IN OPEN BOREHOLE): 20 feet DEPTH


0 S-1 0 - 4 0.0 Dry

Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material – Brown, silty fine sand with brick, concrete and asphalt. Fill Material Stained grey, silty fine sand with fine gravel, very strong solvent odor. Groundwater @ ~13’ below grade (bg). End of Boring (EOB) @ 16’ bg. * *soil and groundwater sample collected for laboratory analysis

5 S-2 4 - 8 0.0 Dry

10 S-3 8 – 12 0.0 Dry

15 S-4 12 – 16** 400 Moist/Wet

PHASE II ENVIRONMENTAL SUBSURFACE INVESTIGATION

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