<£/.3/2

P£fl PUERTO RfCQ INC.

RIAL P A R K / B O X 2521'HUVACAu F.i~ ' 1 O MiCU :

,1k. Wi££iom J. LibAizziVine.ctoAEmeAg&ncy & Remedial Re^ponie Uiv-iiionU.S. EnviAwimentat1 Ptiote.cti.onRegion II26 FedeAoNew yo^fe N.y. 1027S

72, 7 9 S 5

Pea/i ^k. li.bnJ.zz-i'*

Thii> tzttzsiMvich 7, 79*5.

Re: LetteA doted 3-7-S5, Request&OA Information undeA 42 U.S.C.9604 and 42 U.S.C. 6927

Cteefe, Humacao, P.R.

the. -information ne.qu.eAtejd. on you*. tctteA

PCR PueAto Rico, Inc. {PKD090578014) ber;an opeAata?nA -en 7977 attke. Humacao InduAt/ual PaAk.

s—x.

I. any fiazaAdou-4 -6u.6<5iance4 and/oA. hazoAdou*which youA company nauXed, handte.d on. generated eve/t.diAchaAge.d into the. fAontQAa CAe.uk OA tAibutaAy tocate.d•in Hwmacao, P.R. ? 1^ ine an&i/oeA iA yeA, p£eaie provide.the. date. (A) on whic/t ^heie AubAtanceA weAe. duchatged

C^ieefe.

PCR PueAto Rico, Inc. ha6 not d-c6cnatged ant/ hazoAdouAOA non hazoAdouA> ^abitance* into F^onte^a

II. We/te ant/ w/vccn nwuy nawe contained hazoAdou*and/at hazoAdou& uxuteA and which may have.

been di&chaAoe,d into the. Cteefe, hauie.d, handled OAge.neAate,d by youA company? 1$ &o, identify the. natuAe.0(J them.

PCR PueAto Rico, Inc. had not di&chaAged any -te^e eitnetcontaining hazaAdouA oft non-hazaAdou& Aubitancei intoPAonteAa C^eefe.

III. P£ea&e identify tne nature and quantity ofi aJUi hazaAdouA

oto

T tLRPHO^E : (809)35^: 1520 TELEX 3B59JOI

PCR PUERTO RICO, INC.PAGE 2

-6ub-6.tanc.e4 and/on, wa&teA diAchoAged Jinto the. Cteefe.To -ide.nti^y a chemical on otheA hazaAdouA Aubttancz,<inctu.de. the. name,, compoA<ition and -it* 40uA.ce and/OAoAig-in. I(J applicable., 'ide.nti^y the. manufacturingpft.oc.eAi, 'in which the. hazadouA 4ub4.fttnce uxu> ge.neAate.dand -inctu.de. a copy o& all chemical analyAeA

Ai Atatid, -in the, pAe.v-iouA two anAweAA, PCR PueAto P^ico,Inc. ha& not di&chaAQe.d any MUteA -into FtionteAa

1 1/. PleMe. i.de.Yiti^ij wheAe. alZ watte, mateAiati, ge,neAate.d atyouA {ac^itity weAe. dAApot>e.d o£. Vnovtde. the. Locationand type. o& du>pot>al ^acULitij (e.g. tand^lit, tAe.atme.ntplant] and the. -idcnti cation o£ att tAanApoAteAA 06 edto haul the. uxu>teA -including name., addAeA*,, te£e.phone.ncmbeA and any otheA appAopAiate.

PCR PaeAto Rxtco, Inc. ha* ge.neAate.d the. ^ottow-ing

Slake. Lime. W.O.S. ORAi-E WA 91^9

ThL& AtAzam which -i& -in a ttudge. ^oAm ha& beentAan(>poAte.d out o£ the. plantAsite. by the.

1. CoAAeAa* TAucking - PRV000692566Uta GAande. Box. 950San Juan, P.R. 00902( £ 0 9 ) 72S-54S6

2. Mhtand Chw-ical Co. - PRV000706291P.O. Box. 1026Bayamon, P.R. 00621(509) 788-2400

The. dLtspo&al ^acx6C-ctte,5 wheAe. th<ib waAtc. ha& been.6en£ to aAe.:

SCA SeAv-icU - SCV0703759S5Rt. 1 P.O. BOX 55Pi.newood, S.C. 29125(S03) 452-5003

Chem.ca£ Wa&te. Management, Inc.. ALV000622464Eme££e FacMtyAlabama Highway 17 at Mile.

163Alabama 35459

(205) 652-9721

U)M00

PCR PUERTO RICO, INC.PAGE 3

Wat>te. CliloAo^oAjn N.0.S. ORAI-A UW

T^ci toaA^e IOOA tAanApoAte.d out o^ the. plant&ite. by:

1. Mhland Chemical Co. - PRV0007"6291P.O. Box 7026Eayamon, P.R. 006 2 1(S09) 788-2400

Thib wa&te. wo* di&poAe.d at:

Chemical Wcu>t& Ma.nagwe.nt, Inc.. - ALVOQOt>22464Emzlle. TaciLityAlabama. Highway 17 at

Ma^fee/i 763., Alabama 35459

( 2 0 5 ) 652-9721

Ptcce-4-sed

JkLb AtfLQMn goei to the, Hwnacao lnditi>t>iial PaAkt/ieatm&nt

Ms.. La-ten C.ManagingHumacao InduA&uaJt56 fang* CouAtSantux.ce., P.R. 00971

E08 C-AG-0007WPPES PR0022217

V. Plea&e. i.ndi.cate. the. amount oft each type. oAubAtance. &LanAposite.d to any tA.eatme.nt plant, fon.Liqiu-d wa&tu youA. anAweA. should be. -in teAm* of,volume., ^OA. AoLid waAte., in teAm& o£ weight.

7. Slake. Lime. W.O.S. ORM-E NA97S9

Quantity1980 223, 990" £64 . ^T 9 « J 45,240 lb&. %1982 36,000 Ib*. °1983 25,3/0 £fa4. 01984 24,000 £64. o

2. Wa6ie ChtoAofaAm H.O.S. OKM-A Un1888 0CO

T9I?

3.

2,000 gallons e.vi>Ay ux>n.king day

PCR PUERTO RICO, INCPAGE 4

I/I. Please. submit 01 ide.ntifaij all doc.ume.ntt> which delate. tothe. diApoAal, i>tona.ge. on. tfie.atmo.nt ofa hazan.douA Aub&tancuat the. CAe.e.k, at youA faacititieA on at a. tA.eatme.nt plant.To ide-ntifay a doc.iume.n-t, ductu.be, the. natuAz ofa the. doc.ume.nt(e.g., invoice., in\>e.nto>uj faonm, etc.), bnA.e.falij deAcAi.be.the. n.eJLe.\iant information c.ontai.ne.d theAeJ-n identify byname, and job title, the. peAAon Mho pne.pan.e.d the., doc.ume.nt, andi^ the, doc.iane.nt <it> not fieadiJli] available., ide.ntA.faij wheAe. itiA &tofie.d on. maintai.ne.d on. why it iA no longeA available..

]. Slake. Lime.

3.

Manifaut HombeASouth CaAotinaSouth CarolinaSouth Can.oli.naSo'jth CarolinaSouth CaAolinaSouth CaAolinaSouth CaAolinaSouth Can.olU.Yia

Alabama CWMAAlabama CWMAAlabama CWMAAlabama CWMA

204920572052205420552056

2 0 7 2 766072

£ 7 2 2 081243S126SS12S6

Mabama CWMA / 455 29

2. Woi-te Chlon.ofaonm

Alabama CWMA &1244

?noc.eA&e.d WateAPlant n.e.c.ondt>

(PueAto Rico 7)(PueAto Rico 2}(PueAto Rico 3)

(PueAto Rico 4}(PueAto Rico 5}(PueAto Rico 7}(PueAto Rico g)(PueAto Rico 9}

(PueAto Rico 6}

additional i.nfaomnati.on i* needed, plua&e. le£ uut> fenoco.

A.Plant ManageA

oo

N>O

c-. EPA - SJU

fADO UBRE ASOC. _>o'o£ PUERTO RICO / OFICINA DEL GOb-MNADOR

• AG-CI-idn

Sr. Lorenzo G. Jergens MAY 8 A 1978GerenteHumacao Industrial Park56 Kings Count PentSanturce, Puerto Rico 00911

Asunto: C-AG-0007 & NPDES PR0022217Humacao Industrial Park . ^Humacao, Puerto Rico

Estimado senor Jergens:

Me refiero a su solicitud para la autorizaci6n de construcci6ndel sistema de disposici6n de aguas servidas sin descargas consis-tente en una planta de lodos activados, filtro de arena y lagunasde evaporaci6n para el proyecto de epigrafe.

Luego de someterse la documentaci6n necesaria, realizarse laevaluaci6n correspondiente y certificarse el disefio de las lagunas,se autoriza la construcci6n del mencionado sistema en cuanto acontaminaci6n de agua se refiere, sujeto a las siguientes condicior.es:

„ 1- La carga hidraulica no deberS sobrepasar de 15,000 GPD.

2- La carga orgSnica no deberS sobrepasar de 37.53 libras deDB05/DIA.

3- No se realizarSn cambios en el disefio del sistema sin laprevia autorizaci6n de esta Junta.

4- La autorizaci6n de construcci6n no podra" ser transferida aninguna otra persona o entidad.

5- La autorizaci6n de construcci6n veneer^ el 15 de noviembre de 1!De no haberse comenzado la construcci6n del sistema para esafecha y de persistir el peticionario en llevar a cabo la cons-truccifin, deberS solicitar una autorizaci6n nuevamente. Lasnormas del disefio aplicables a la fecha de la nueva solicitudse utilizarSn en la re-evaluaci6n del sistema.

6- El sistema de disposici6n de aguas usadas no podra1 tenerdescargas de acuerdo a la certificaci6n del Ing. Carmelo Hemancsometida a esta Junta (Affidavit ndmero 518 del 28 de abril de :del Lie. Jos€ A. Cepeda Rodriguez). Cualquier descarga o

002 0321

Sr. Lorenzo G. JergensPSgina 2

desborde de este sistema (excepto aquellos eventos consi-derados actos de Dios) constituirS una violaci6n a estaautorizaci6n.

7- Segdn especificado por el proponente en carta fechada el'*' 24 de febrero de 1978, el influente al sistema en cuesti6n

por parte de cada entidad que se acometa a dicho sistemano sobrepasara1 las limitaciones establecidas voluntariamentepor la Humacao Industrial Park y que se especlfican en laTabla I. (Copia adjunta) .

Deseamos indicarle, ademSs, lo siguiente:

1- El sistema de tratamiento en cuesti6n es de caractor provi-sional, ya que se descontinuarS su us.o tan pronto esteoperacional el sistema regional para la recolecci6n, trata-miento y disposici6n de aguas usadas de la Autoridad deAcueductos y Alcantarillados que servirS el Srea.

2- Es necesario obtcner de osta Junta una auto.rizaci6h paraoperar un sistema para el control de la contaminacio'n delas aguas antes de iniciar la operaci6n del sistema en

^^ . cuesti6n. Sera" necesario someter a esta Junta un AfidSvit! de exenci6n de descarga (Affidavit of exemption) que provee

la Agencia Federal para la Protecci6n del Ambiente (EPA)para sistemas que no tengan descargas a cuerpos de agua.Dicho afidSvit deberS someterse conjuntamente con la soli-citud de autorizaci6n de operaci6n. Copia del mismo seadjunta. No se otorgara autorizaci6n de operaci6n, sinose somete el referido afidavit debidamente cumplimentado.

3- Esta Junta se reserva el derecho de intervenir en elfuture respecto a otros aspectos ambientales de esteproyecto.

Luego de finalizada la construcci6n del sistema en cuesti6ny tan pronto se estime que las instalaciones estSn preparadas parauna rigurosa inspecci6n de verificaci6n de cumplimiento, agradece-remos solicite a esta Junta una solicitud de autorizaci6n deoperaci6n. De esta forma se adelantaria al mfiMor gradfcjposible elinicio del trSmite de la autorizaci6n de operaci6n.

V la. i/ff 13»o

S

Pedro A. Marrero Pedro A. Gela^ertDirector Asociado Director Ejecutivopara Agua y Aire

.South Carolina Departs**! of Health and Eavlrowiaiitat ControlSolid Matte Nanate*«at Dlvldoa2*0a tall Street, ColunaU. SC »2I1

(Ml) TSI-SMI "

snipping No. 5199

INTERIMHAZARDOUS

Manifest

MANIFEST_ _ / _ _ / _ / _ _ _ -(rear noath^ day

Instructions for co«pletlnrthis farm on reverse *IJ«. '

(I) CeneritarPCR, Inc.

(2) Traniaertar No. 1Brvson

1.0. Cod* s<Htre*l A44rea*P 0 Box' 166

FT108 White1; Oak Lane

Phone Muaberlaica Jndt I •usUtaxL

(904)376-8216-(803)796-6408

Date Shippedor i

-»M80 / Q8

/ 08_/_2L___d.i/ 2(I_Z3i/Traaifartar (to. t

r*v.<S| ?l?l Services Rt. l.:;p'!0 Box 55 / 0 8 /

'•" • MJLi11) DOT Propai

Slake Lime

»THa*ar4Clw*

None

(S) Quaatltf

39,000 1

(4) Hast a Co4aS| Ilasar4o«a Waste

QharecMf^ftlcCs

lgltltaoetorro»iie

OReactlva*DTo*Ie • • - ;

initablaDCorro»U«

Tonlc,

Q CorrosiveDReactlva^i

ile.i ;IIMJ,,.B. Special'IU^Iia|"jailn.ctio;.-.-.. p. --'-. »i i

Ccatfalor |tf* Count

Contalaar Type Nunbar

70 x 55 galloidrums

(7) TSDP I tea) Check

Container Nuaibar

70

(|| Quant Iby ttcl:(pound•

Eawrgeiicy Response lafornatloa:la event al aa everiency, phone the Generator at:

1904 iIsi event or a sp376-8246illf li

OayarUtent at (W) TU-SISI.South Caroliaa, call tha „None -

: l-vl;.-. I:' " 1

B, Cpaaiaatft

This U ta_tertUy that tha tbove-aaaed aatarlals are properly classlfted,'de«cribed, packaied. aarke4 sn4 Iabele4, aa4 ire !• proper condltloa, fortra»spo/<ftj)M accof^npX jl •Bfncable^ai-latlosiB of tha V-S- D9T. fM.t,P. f.S.C. aad |hf ^.C, O.H-8.C.

A _' RudnlnH Prii»fo».-l>aff M»^a^». 8-2Q-8Q______•:V**>JUL*. ^frCL.wSfi

DataI hereby certify that I aa>by *a for aitlaiata delivery

Traaspa'tar Raj. 2i

tfcaritai r«D«a»aa»«*J»a «t tk« »»« «atta|») a-4 aw«jffltf d««cri»ifd t« thl* N«filff«| aata baaa accept^^ - - ^ 8.20-80our

JSOJu1 hereby cartbee* •ccep

Itad representative of^thj TSDf Ideatl^ifd above aa4 that the naste(s) and s«<ntlty 4a»crlbe4 la this Haalfest hare

' A=—————DUE

-if*

ezeo 200 OHJ

>«Ce<>«Jd Hai

>/{»OP Nil' Phoafcs (

Cartllaa Pepertoeat of HealthlJd Hem Naaageaeat blvltloa

Nil Street. Columbia. SC(Ml) VSI-SM1 '•

oad Bnvlroojwatal Control INTERIMHAZARDOUS NA3TE MANIFEST

____/__ / __/__year •ontlT" I»r

Instructions for cea

itano rj'-.s I.'.C. •'

'%?•»•»%»•' '•'• ••••:R, inc.Brysontransporter No. t

si Services(|| tOT Propai

Slake Lime

i

(2) DOT1 > ItasardClass

None

In oeont of an energencr,

1 904 i 376-8246In ovenl of i spill in Son

' ptpartntat at (••]) 711

I.D. CodeIflfln*** 1 fte^f^l

. i • • ..

\(S) Qnantltr

37,950 1

it) Haste Code

Address ' ^-ii

P. 0. Box 1466

108 White Oak Lane3t%fC 2?072

L *kt. i,Plr^pwpr

Charac

py'ijjjH c^

o«is"Wi>•••>..'t •<

OCorrosUoM 'O Reactive !";

OToxIc ' "

DCorroslfa ••'OMeectlvf.jiDToxIc ''l ,Hl'^tr1 ' '

|X tt

!i*te

i

iaiialtable'i |>[Q Corrosive,' . 1?D Reactive .'.-' j

n: D. Special Head lingphono the Cone rn tor at: <

.thscar.ll.., call th. NQnfi

OT

1 ||

i ' 1

Phone NtnherLmi fade. JLtmtetJ ______

(904) 376-8246

(803) 796-6408i

-(a) GfMrptor tit* COM!

Contelaer Type

69 X 55 99!drums

'• • ' :

Niaaber

T-4

cttons: '

Pate Shippedor Accf Bted. ___________

80 / 08 /21M«* . -,, •«*•». *v

8 0 / 0 8 / 2 1year •"•It f«I

1 1VttBa* feOMlfc dial V

fib / 08 /21¥•• T aVOHth llttr

()) TSDP It en Check

Container Tjrpo

&WS

WMber

tf

(11 Qnaatltrhf Nel|M(pounds)

*

B. Coaa iatit

/jlQ^^^O

$00£ if<&l/'*2& ^~•~^

This ie tojaoftlfy that the abovo-naned oaterlels are propertr clasilfled. described, packaged, narked aad labeled, and are In proper condition fortrBnspoprat^&Jcco^iyjA^t amicable r^ulatlona of tha U.S. HOT, the sic. P.3.C. and the S.C. D.II.B.C. r

Ronald HcNeal. Asst. Warehouse Foreman. p.?]-Rn '" .me and Title '——————————————————————————————wt«>f .

1 hereof eartlff that I aai aa authorised representative of th,e trapipoflfr^ ^ 1 ^ 4 " ^ ^ ^ ^ ^ -

tkf^ the «raata(e| and o^tantttf described la this Manifest bete boon accepted1 wn\1e Wages ' «» !««-

I berebf certlfjr that Ibeen accettfceVlbr *e founVaa

rlxed repre»eatatlvo of the TSUF Idaatlfled fbova a*d that the waftota) ead qttiUtltr deicrlbed In thlt Na^lfaet have, I r - ——

3)

1 ?k

»

£5

8U

±.

1 to-

ss

*isca *.e

I<••I

fcj

Jle!

J

Ik, U

cs9J!CO|

i </i ac

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oic •C

C I

ITJC I

oil :e >* »-C )•I1

00:

aarUon

;£

e\py-£!• c>-r-

ocaDPSCA Se

5*13

X.O

.cr*--

jti•#J

•a«#J

MSv

• *

•

id

Mifc"825

fer

COcoinVI

X E

CO t-

vo TJ• •»-•e w u

*•'->

o*.w

ii-'ew

ui.<

o*'tM

«'

" ni

_ k u

»«

b. k

W—

« - to

U—

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=

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• • rfe k

a K

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« ••

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OW e>)i»e a M

MO

a e-

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t-^.p

it >--.—u

an~ •

231513 ^D^3^3^3 3O

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CMOOOOl

iJ301^M•o

£-~,v_-5S!,r.

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L*'•-.;-r^T.- .,,--v

ootoK)

tn

jootli Cara t \ p a r t n r n t o f H e a l t hSol id »»Jto /xcmcnt lilvlslon Hnni ion i>ocu«Cdlir.nii H u l l S t r ee t , ColunMa, SC 29201I'hoiie: (»OJ) 7 S R - S 6 I I

Nnme(1) Venerator

.P.f"! R Pnerfn R'f'*'1* T(2* Transporter Ho. I

PRMSA.Transporter No. Z• Bryson

1J) JfiHf Services •(I) DOT Propei

ShlpplntNone

Slaked Lime

l':»9TJCMCy RCJpIn event of

1.809)

(2) DOTIl i tardClass (I

None 3'

pti50 I n f o r m a t i o n :an emergency, ph

852-4520In event oF a sp i l l lit South

Department at (101) 751-5

, HAZARDOUS WAS-I-E MANIFEST y e n r .^^.Sj r- r ' t o -p i r tm, . 'i t h i s l :orm on reverse 5l \ lc ,

l .n. Code 'dumber S.JOUKlJ — ._... _.

\i

.' ' '•

) Quantity

4,000 Ibs

•

(4) Naste Code

541-2102.

Address ' 1'hont M u m l i o r U n t c sl''rPcJ

(nrc i . tnJe £ n u m l i r r l o r A c c f l i t r d r

Carr, t f j Km. / b . y . , . 8 0 / 1 1 /Buzon 2521 Humacso, P.-R. pno~HS ?-/,«; 9 n f f * r ,u»nr~- ~~^-G.P.O. Box 5091 / /n r t r t * t n * i i f ^ f • - m-,m<?nn Tjian PP 809-703.-1A1A- V/Sr" " ~«oiilIT ._...__ .d.108 tvhite Oak Lane / /_T.exlngron, S.r.T • Hm-l tlhr-ftAnR . . . . . . . . YOD.T pon.lli oK C . 1 P.O. B o x 5 5 I IFlneWOOdr S.C. Jim-' "iZ-Snr , r e a r ni nlh i

(G) Genera to r lira Count (7) TSUr UCM ClieckS) I t a tn rdous Haste ( t) Q u n u t :

Charncterlstlc(s — : ————————— • — i —————— ————————————— i —————— l>y "c ',Conta ine r Type Number C o n t a i n e r Type Kunlier (pouix

grp.iil t n u t e , . \ 1 iUCnrroslve •* . .' '- 'i^tv/\ 1 *STv-<»\ai tcnct ive • 55 Gal. Steel 72 ;: -^^ivv ' ^vv ~~)~~) '/<""y//S!?!lL ' Drum c-Vvx^> ' ^ "j < '— UU.S.tCa—. —————— ———————— , ——————— — - ————— — : — i— J^ ——— £- ————— ——————— —— '—LJIg'" t a b l eQCorroslve , ' '•DReoct lve •g lOKlCl.litc.l , . . —————————— . —— —————— ————————————— —————— • ———————I jni t n b l cQCorroslveOi tenct lveUToxIcOl.lsted I

1). Special t l m i d l i u g Ins t ruc t ions : |]( connents:one- the Generator at! -•- •

Carol lnn, call the511.

This Is to ce r t lCy that the »bove-n««ed nnler l i i ls ire property c l a s s i f i e d , described, puck t j cd , marked md labeled, and are In proper condition fortransportation according to all appllcnble reflations of the U.S. DOT, the S.C. r.S.C. and the S.C. II. II. 11. C.

t hereby cer t lby us for ultl

Transporte

Transporte

fy l h a r l *« en authorized represen ta t ive of the transporter and that the v«ste(s) and quantity described In this Manifest have been acceptr•ete delivery to the TSOP Identified above.r Mo. li ^ ' • ^ * ————————————r Mo. «»'""*?'

1 herciir ««JftVJ^Mfat ' "•/*!/*been 'C<^d/J^^£#f

wme ' f" i l("

. fl'/ty^ZQ ' """ffl^^te*' jfa*^^- '„."}} I ; ' ' f ' ^utborlt««l r epres fHia i lve of the TSW I d e n t i f i e d ibove »nd>liat the ¥asYe(s) and q u a n t i t y described In t h i s Hnnl fes t h«veSjt.^itoriiM. «««l/«r disposal. ^ /$Cf^>i f A /^__ ' ^/l/r^'s /OC^ «i //<? /CO

,,, (/200

rf /icpirtnont of I'eilth ind Rnv l ronncnt i i uuniH'.vl*loit

•!'. S t r e e t , Colunlili. SC 29201

IN /JL.M

HAZARDOUS WASTE MANIFESTM n n l f e s t Hnctimnnt Nunlier • / "^^ —

~"ijil rurl luin for c»«i»trt I

.,.e ' . '' i G e n e r a t o rPCR PUERTO RICO. INC.

;• T r a n s p o r t e r No. 1SFA-LAJ& SERVICES

T r a n s p o r t e r No. 2 • • • •ITjyqOS"

^PA^RVTCFS\ ] 'JOT Proper

S h i p p i n g

Slaked Lime

• . ; :.

C l n s s

Corrosive

•

• • .. •• ;.

n e r R c n c y He sponge I n f o r n i t l oIn e v e n t of an -emergency ,

In e v e n t ol l sp i l l In SouDepar tment a t (&OJ) 7SI

f . n . Code.(mmbfjcJL

*/&&&

*ource1

d-^Otf^o

~3C0OOf)fJ<ZZ3/Z.J£'/)O 7O3Z3 '/*&

3) Q u i n t l t y

35,200 Lbs

(4) V e s t e Code •

i

541-2102

n :phone th* C e n e r i t o r i t :

th C»ro l ln« , e«ll the- S S J I .

AJ-r , , , - -

carr. ffj Km. .76 .9Buzon 2521 Humaran, P .R .G.P.O. Box 2409

_San .Tuan; P ^ P , nnq^f iL08 Whice Oak LaneLexingj:on, S.C.11T. 1 P.O. Box 55P 1 r> n. if\f*A Q f— x-u.uawaoci! — a.*.-.

S) t l a t K r d o u s M u t eC h n r n c t e r l s t l c ( 5

Q lp .n l t a b l eU tlnr ros 1 vcO n c n c 1 1 ve •atonicQl. luci l . . . -.L J l R n i l ao l eQ(!orros IveQ l l e n c t l v eg l o x l c

LI « tfl'X" i t a b l eQ C o r r o j IveQ H e a c t l v c

I'hone N u n h c rlor.cn_coilc_lL-nu

finq-flS?-6S?f

nn(?r1

1

809-781-6600803-796-6408

803-452-500?( 0 ) G e n e r a t o r t t e n Count

C o n t a i n e r Type

75 Gal. SteelDrum

Number

75

1 ) , S p e c i a l n . i n J l i i i | f I n s t r u c t i o n * :

C.

l l n t e Sh ipped

_81_yc«

-*%

: ——— —— So/

r ..,-"<

nti i . .._..—7>irr._

r '— T5UTUH—— ' —/ / -w?>"V/ .y e a r ««

(7) TSOF 1 It- C l i e c V

C o n t t l n o r Typ«

£)*»*Nunl ie r

ni l )

( f t ) Q i i n n l

(pom

^•'

H. Coxw'ents :

"ils I* to cert i fy that tlie itiove-nmev1 imterlatj ire proper ty c l a s s i f i e d , descr ibed. p a c V « _ . e d , marked ind labeled, and are In proper co*t'ltl*« Ul:rniiportn.tlon accord ln)| to nil eppllcable renulatlons of tlie U.S_. DOT, tlto S.C. P .S .C . and I lie S .C. II.II.I!.C.

i i TT <f Til Tc>iere!i)r c e r t i f y

u» forTr.nipornr

e r t i f y IhmN n»/iin ;»«lhorl ttd/Tcprt^tn 1 1 ve of tli« t ransporter and tlmt tlie vMte(i) ind mi«ntlty .Itscrll.oil In Dili Mtnlf.it Vi,« \t<« •<C«pt*'1

ultl»lt« tlallvcrV iff «'ie TS'jn/ldent/L/J/eJ «l>ov«. A , _,, _. J , ...rnr Mo. I; /->_X^7 /.v..../ /A?.^^ _______________ _ ^tsyt-'V^Zj/r//, j. 7*,^' ________ </jfc'.'»y ___

~~ ———————— — " —Tmniporter Ho. I:

hereby certU^tlint I •«• een *ccepV«>rJdp •• "for t

^r«n/snenmt I ve of tlio TSIM: l U e n t U ' c U lUove mid t l X t »lie

find/or tllspot.il.

•Tiynuref

f>ii'"c T c

and q u a n t i t y descr ibed In l'.*t li»>Ht»l ">•«••

P5Tf

/ / )

82EO 200 OHd

1 -...IMIIIinaMc|iailiucmnl lUalitiamll iiviruiiitKtiuKunuulS<4t<l awl Haraidmu Waste Management Division2MM Bull Mr«l, Columbia. SC 292(11Phi«K:lMl))7SI-5AXIiiitngfncy * IMiJays: (»!)) 75» S53I

), JbUv;*' 'DoCWnclil Numrirr

HAZARDOUS WASTE MANIFEST

C

Name

(I) OneiPCR

(2) Iran*..SEA.

Trans3RYS

atorPUERTO RICO,,purler No. 1LAND. SJffiVJCJBJSporter No 201?

I It. ( iMk Address

CST. HWAY.t»3 KM. 76.9INC. PRD090578014 HUMACAO, P.R. 00661

R.P.O. BOX 2409SAN THAN P T TJ, nnenfi

108 WHITE OAK LANEsrnOnnR9?T17 iwrvr.Traa n r fQf\Ty

SERVICES SCD079375985 ^rEAo5D?*S?8^ 5^9125

(1) Cknerator Hem Count

Number

67

K meritItCllCl

Container Type

30 GALLONSTEEL DRUM

ifc_

(2) IX) T Proper ShippingName'Ha/ard Class/

DOT Idenlirkatiiin Number

SLAKED LIME/CORROSIVE,NA 9189

O) TotalQuantity

2,010

<4) Weigh!(pounds)

26,800

Phone Number(area code * number)

(B091

(803)

(803)

R 52-4 520

781-6600

796-6408—

452-5003

O) Wade Code

541-2102

ncy Response Information: D. Special Handling loslroctiom:1 event of an emergency, phone the <>eneralor at:$09 ) S52-4520

i event of a spiB in South Caiotku,lU ike Depjictmeiit at («OJ) 7JI 5331

•**This is to cafmigf hauhc above -nalWaSujfrtab are proaeth; clauiried, described, packaged, marked and labeled, and are in proper condition•»jtr *\4r»vK itMfr wtftTmJi »Llrmw nuc Bp F ^

Hale Shippedor Accepted

83 '12 ' n i

1

*k *»

1JW •••»> *•»

i 1I*M «Mk «•»

i ffix mi** <•>

16) TSDF Hen Check

Number Container Typeby Weight(pounds)

E. Comments:

for transportation according to all attplkabk refutations of the U.S.

O I hereby certify thai I am an wrthorixcd Kpresenlalive of tl

Transporter No. I: .___:_____

TraMportcr No. 2:

and thai the «ssle(s) and quantity described in this ManMed have beea accepted by us for allMUte delivery to Ike TSDF ideolified above.

II I hereby ceilify that I am an authorised reprcieniaiivc of the TSUF identiried above and that the «a*1c<i) and quantity in this Manifest have been accepted by me for treatment, storage, and/or disposal.

6 Z £ 0 200 OH«3 Instruction* »w comnfetine tl>« F«rm on reverte tide.

«i\I

\.

f).

C.

F.

0.

H.

Solid -nd Ha Is Waste Management DivisionWC UStrev olumbia. SC 29201'him.:. (803)758.5681 *emergency A Holidays: (803) 758-5531

Name

(1) GeneratorpfTR Piierfn Riro,

I.D. Code

Inc. l(2) Transporter No. 1 ^ ~"'~

Transporter No. 2 "" ^-— "*"M-:r~

(3) TSDFSr.A Services

(1) Generator Item Count

imber

63

Container Type

55 Gal. Steel

(2) DOT Proper Shipp.!Name/Hazard Class/

DOT Identification Num

---—" ——/^ Slaked Lime /Coi^ NA 9189

>x^ — — •—^*»«»M» 1 III

Emergency Response Information:in evegt^ an -ng&Jtgff* Genera.or at:In event of « spill in South Carolina,call the Department at (803) 758-5531

This is KDOT. U

/thereby

I ncrcw]

tf

i certify that the above-named materials are properly cy€>A>S«S.C. PJCaA the.S.C-IlUlt£

M^jflMtt*.

certify ihrf 1 am an au

mwir *f /

Ihorind representative of tha t

a* ^~

„,„ —thoeked representative of the 1

"\ ......... . ~V- 'HAZARDOUS W^i-E MANIFEST -,- ~nAn<i

JN* lUlfc*

— . , _,, __, _»,. . |__r

^^

Phone Number Dale ShippedAddress (area code A number) or AcceptedCan960GPOSan

-. 03 Km. 76.9 PO Box »? • m ; 30Punta Santiago, PR 0074: (809) 852-4520 ff > t ,U —— ' —— SBox 2409 ^ . ^)

108 White Oak Lane (^ , ___ . ^Lexlneton, S.C. (803) 796-6408 , - . ' ' - « « . ' _rRT.Pine

"' (3) Total. Quantityoer

"N•roslve 3J465.00

D. Special Handling

1 PO Box 55 gr\2. i -^ | | "f•woods. S.C. (803) 452-5003 —••>*•- ^^ ' i,

(4) Weight (5)WMteCode (6) TSDF Item Check ^$3?(pounds) ———— i ——— - — ""• • fL.~J.iNumber Container Type (pounds)

,1.5.0 <^^T~^ ^ 0^^, A|I20M(

Instructions: E. Comments:^ I . • • , 1C^-fJC/OS^.C4 ( ^A*/t3'L_

lassified, described, packaged, marked and labeled, and are in proper condition for transportation according to aO applicable regulations of the U -

' Pedro A. Martinpz, Plant- Manager 3 fjn 782-.«_„_ .__• Tfak *^ I^MnT

ramporter and that the wa«te(s) and quantity described la ink Manifest have been accepted by us for ultimate delivery to the TSDF Identified above.

I/ • ,- sr ^ */ ^& /X^5g54ts3*fe-- S~tSyfY~J»&

MM ~

MMM

— ^^ o»> v

D«t

fSDF identified above and that the wasted) and quantity In this Manifest have been accepted by me for treatment, storage, and/or disposal.

^jC-/r ^J&l-S'Cgrl - s£s&&* fiPc^A. , ^~~/"4-Q2~

0££0 ZOO OHJ InMroeAnia for completing tMa Form cm reverse side.

ALABAMAHAZARDOUS WASTI MAN|ft$T

CWMAN281220

Wam MmMMMlK.Em«H« Facility

Inc.

Box 2521Hmvy^ytjP.O. BOX 1026

P.R.854 South OD ception St.

34S49

P.O. Bpx 55 Z TEmelle, Alabamfc 35459

~$0f—

9721206/692)6000

PA K> COM

Pi Rl Pi Oi 9( Ol 5l 71 8! d

A|L|D{0|0|0|6|2|2|4|(

•/ASTI IMPOtMATION

NO TVH OOaumON/CLASSTOTAL UNIT

EFAID No.

C W M AWASTI CODE WEIG

130 Gal.drum

WASTE SLAKE LIMB N.O.S.Corrosive Material GAL EDQ2i

ASH-61-053 '«$55 Gal.

2 drumWASTE SLAKE LIME N.O.SCORROSIVE MATERIAL

/<>)110 i i ASH-61-053 8(

' 'MMOINCY INtOtMATIOMtMMMMCY MOLt MSfOHft — Utt> «il4HW ; OfNUATO* —X

NtfreucnoMfc 9721US COAST OUAftO 1 -«0O-414-4»02

CUTIPICATION«!••<« I U, «• !•

•* Tr*M9MtaHM. MM U.S.

PLANT MANAGER 1-31-84OoW

TRANSPORTER NO. Thto

/A'&?' . 0*»« C•*!»-Data

TRANSPORTER NO. 3 TJtto

Dot.

IMfOiMATIOMCWMA

WASTE COM UNJT MOCCSSCOtX TRENCH UVCL QUAD COMMENTS

'H •

ooto

oCOCO

V>«A«T At

'VIRONMBltTAfc 'QUALITY \RDKAZARDOUS WASTE MANltkST

OOCUMiHT Up,EM

t

L» J J .' J J •' .' .' 'F m ii if w 10 • «t

P. R i i i ITM€ FMST MANIFEST OOCUMUIT MO. II

tfffiyiiTfiirnmi [i • mrrmrrrTwi nr rrnmnmi WTTT T-impr r tt-TiTTTnr n mrvronmnjtynrf i—

U.I EM mt thi Cenvhomwrith «t P.R !>• •»» dMcrik* APM Mrt CMHigMd M ttw TraMfMrt* MMA T)Me<Mi«dau«wMU.indhuivriidNnMu4*M.lc«f^|lty|tlMlM«M«MnMifid»«nautlNk«(<^av

TRANSPORTER «X IVEHICU10. NO.

QATESHIPW)ift li <n ij

U ' J»T^

.. tEM AT THIS PHtfOMTMN

DATE RECEIVED

" ii* niv ^n

I «liKi4 th* nnltnti •( ttin «J»pm«nl"FRO 002 0332

•~ ALABAMAHAZARDOUS WASTE MANIRST

CWMAN281243

MPMMATIOMfctiiaW Jn^tf^

GENERATORrCK LJC.

fcSHLftfJP .CHEMICAL COMPANY iTRANSPORTER NO. 2SL'IAHAIL. 'INC.TRANSPORTER NO. 3

\

Cherpical Waste Management, Inc.Emelle Facility

' * - ADDRESSP.O. BOX 9COPunta bantaa.qo, p.R. 00741P.O. BOX 1026

^Baysuon* Puerto Rico OOG21 •854 SO7IU COfcCtl'ilpN ST.Mabile, Alaban'a 3-1 "34 y

P.O. Box 55Emelle, Alabama 35459

•HpNl— ~46tt\ _ !ii!i!

J52-4^M'f Tc!8u9

788-2400 ,205

433-2651JUN

S721205/652-85M

CR. "^ ^W]»a»|&0l^|5|7U|0|]

* I | t l j0 |0 |0 |7 |0 |6 |2 |£

A|L|D|pl7J7|8|9|5|l|:Q j"^

i ? 1 1 1 I 1 1 1 1

A|L|D|0|0|0|6|2|2|4|€

WASTE IMTOtMATIONCO

NO.

7

NTA1NER

TYPE

55 GftL.

DESCRIPTION/CLASS

KAbTE SLAKE LIME N.O.S.CXi IOGIVE MA 1760

—.£ /.-?-^~- rM *'••>• •' '••'

TOTAtQUAN.

rWff

UNIT

^al.

EPAHoiW«tt

TtanB

[ardOMSDNo.

1

1|

1,

|

C W M AWASTE CODE

ASH-61-053

»»

WEIQ

'MH

IMERGINCY INFORMATION

IMUtOINCY NOt.: OtSTOMR — (101)iNmucnoMt

«MnUTOR US COAST QUARO 1400-4144M39721

1%fe b ^ *M iM •&_» A* _^~_—• i^v w •• wfnvy vOTT fHV w^^v

ER NO. 2 Title Data

•^ TRANSPORTER NO. 3 Tltto DataTW» to ta MrtMy

7 , '; /X O C /<A. ' //

£? D&br ^—- - TW« Datah

DISPOSAL INFORMATIONCWMA

WASTE CODE QUANTITY

7UNIT

r^

?

PROCESS COOE

^ T-tf-fW-rvT-M

LOCATIONTRENCH

V 1%

LEVEL

?"

QUAD COMMENTS ^

xr J N

GU

OJ

:cLCOMMONWEALTH OP PUERTO . CO,, ENVIRONMENTAL QUALITY BOARDHAZARDOUS WASTE MANIFEST « - <» » »

i x ».-.- S. • ,DOCUMENT NO.

OltOWmGlkSVPDOPUT

THE FIRST MANIFEST DOCUMENT NO. IS.THAN TWO

THIS FORM IS NOEQB/EPA

WASTE TYPEUS DOT

HAZARD CUSSPROPER US DOTSHIPPING NAME

GEN EPA (Of

Ml limped wtttt or m«tria«y

TRANSPORTER NO. 2VEHICLE10 NO. I I I I I I ( I

»ftQpT «QIPI j P1 WC||It WCATWN Of ANY Otf FER^NCtS BETWEEN MANIFEST AND SHIPMENT OR USTWG OF REASONS' ' '

&-__l XPL fy* »

ffii?KANOUNG

[HOB

KCUVU

trfftttMtMMUtOwltatM* iMt'*• -•- . , i »« -. - .-Tf* -• . . - , „ > ^^^^uiaf • p. «uo

j^PHUltt->.? iv

10/«nFKO 002 0334

ALABAMA . :. ?6-T 2-7 CWMAHAZARDOUS'WASTE MANIFEST N281265

IQJHTIHCATIOMUAA.UT• r WPIf

GENERATOR

PCJi TJ*J.TRANSPORTER NO. 1

r^r'AMi: nnsMTfaT. m. .jJYTRANSPORTER NO. 2

'.-•liU/TT.,, IfljC.TRANSPORTER NO. 3

MVOSiftChemical Wast* Manaoemant, Inc.

Emelle Facility

ADDRESS

P.O. Box 960Punta S.^r-*-iatjo, P.R. U074 LP.O. BOX 1026WYfu'-riN, HIivfiL 1'ICU UUfI?1.054 iXXTEH CJUNCUVIOt.1 ST.•.nRTTJi;, AL?M •J'J'A '>^5-;lJ

r

P.O. Box 55Emelle, Alabama 35459

PMOrflE

C,;9bi>2-4520

8097tJ;-24ju

205i33-iL;-i

:.-7L' 1205/652-JJ5JJI

EPA ID CODE

pliJololglo 15 \i l&

f RlulolulobloltJLblQlvblcjhl-

1 1 I 1 1 ! 1AL|D|0|0|0|6I2|2

i)

o

1

4

l|

o|

|

6!WASTE INFORMATION

CONO.

faNTAINER

TV«

i>5 ''AL.

DESCRIPTION/CLASS

WASIESSLAKR LIME N.O . S . ^ <*'' ' " " ..

•*•

TOTALQUAN.

^""i"?'

UNIT

3al.

EPA HoiWest*

Tli orl i 'ira "

ordoutDNo.

'K/l1,,

1|

C W M AWASTE CODE

AJ*i-61-U53

WEIGH!

•4- (_.•*' t'

IMERGENCY INFORMATION

IMttOIMCY NO&: MSPOMR — OOI) 4U4BK; UNOUTOR —4 8 Ob > Kh2-4ii«J'J US COAST GUARD 1400-424-4M2gJCIAl INSTRUCTIONSt 9721

CERTIFICATION

Tfch fc

Dita

<~/ ' -&*•'"TflANSPORTCR NO.Eoe^TTRANSPORTER NO. 2 TUI* Dot*

Thto It toTRANSPORTER NO. 3

•f MTitle Data

Tith "5S §DISPOSAL INFOtMATION

CWMA• «, WASTE CODE

•i

-

QUANTITY UNIT

, _,

PAOCESS CODE

-

0

LOCATIONTRENCH LEVEL QUAD COMMENTS

, 0- •,, w

Ol

COMMONWEALTH OF PUERTO RICO' VI RON MENTAL QUALITY *RD

HAZARDOUS WASTi MANIFEST

DOCUMENT NO.

FIU WTO FOLLOWING AS APPROBATE - •

Of A TOTAL OF ——— THE FIRST MANIFEST DOCUMENT NO. IS.

MORE THAN TWOTHIS FOAM IS NO.

IffQAl NANQUN6 NfSTWCDCIMI WMHW COWA»|W fXEMFOOK (UIOENT1FICATION OF AOWDONAL WASTES HKLUOEO IN SHIPMENT Of A UNHAZARDOUS NATURE MHQt

• v -.-!••:—s^v.'.,-• - ^v ,v . ^v^ ; .

DOCUMENT NO PRO 002 0336

$•««?«• «/M«fer ••

PART A:

COMMONWEALTH OF PUERTO RICO1VIRONMENTAL QUALITY I ARD

HAZARDOUS WASTE MANIFEST

DOCUMENT NO. P. R.

i I I I I I I 1 I I IA L DO 7 7 8 9 5 1 2 i

OlSPOSAl (TSO| f ACUITYSITE AOOftESS

PHONE

iNU. 1 - 1 1 1 1 1 . 1 1 1 1 1P.O. BOM ii. ,HlHh MMbVftDDE THAN TWO TRANSPORTERS AAE TO BE UTIU2tO. fiIf MOW

THIS f o«" IS «fO

. flU OUT THE FOUOWING AS APPROBATE

o*AT<7T*40f ——— TMf 'IRfT MANIFFST DOCUMFNT Nn IS P R 1 ,1 1 1 'PROPER US DOTSHIPPIKG NAME

US DOTHAZARD ClASS

UNNUMBER FOAM

NETQUANTITY UMITS

CONTAINERS

NO. TYPE£PA

cHA2" EQB/tPA

WASTE TY

OMOELZMB-oeftG&pm- rI I i i

I 1 U L.UJ LJ

SPECIAL HANOUNG INSTRUCTIONS INCLUDING CONTAINER EXEMPTION (i.a. IDENTIFICATION OF ADDITIONAL WASH S INClUOtO IN SHIPMtNT UF A NONHAZAHOOUS NATUHF. WHICH00 NOT HAVf TO at MANtf ESTEOI

GENERATORTS CERTtf (CATION: Thia • lo certify (ho tha abova nomad maitrialt aia ptopwly dassiliad, dasuibad. m«l>ad and labelled aid ai«in piopar condition Iw iianspoitanon nccwiiinii10 lha •pplicoWa lagulaiwu ol Iho OopoiunoM of Tronaponolion. U.S. EPA and tha Communwedllh ol I* R Tha wasta daiaitaad above wara consigned to Iha Transporter namad TheTreatment. Storage or OoooeaJ ftutiti con and will accopt Iho ihipmanl ol hvardous waste, and has a valid permit to do so I certify that the loreyoing is true «ul correct to the best ot nivknowled

TUH AT THIS PlfirOHATION

FRO 002 0337

ALABAMAHAZARDOUS WASTE MANIFEST

CWMAN2 81286

/~N INNTIMCATIOM INFORMATIONMAAAff^ • iww

GENERATOR

I1""TRANSPORTER NO. 1

ASTMDK il'iijP^1-00 ———TJWNSTORTER NO. 2

-SF/il'jIW P-1^1 -----TRANSPORTER NO. 3

Chemical Waste Management, Inc.Emelle Facility

ADDRESS

P.O. POX 960Piini-j» S^ni-i^ijn, P . R .P.O. DOT 1026naynnnn, P.t.. fiflti^l854 South Conception St.Mr»h-i 1 i > f Al aliai , A

P.O. Box 55Emelle, Alabama 35459

PHONE809

^2-15-1')809

7^-2400205

433-26f.l

9721205/652-85fitt

Ef A ID CODE

P! tl lk)i9lol5l7l8lolll •

T>lRlD lo lo lo l7 lo l6 l " ' l9 l '

L\lLlolol7

M M

A|L|D|0|0

7l8l9l5l i l2h

M i l l

0 6|2|2|4|6|4

WASTI INfOtMATIONCONTAINER

NO.

/2-

TYPE

5.p^^ .

OESCRIFTION /CLASS

WASTE SLAKE LIME N.O.S.QRM-E NA 9189

OCT ^ 9 -

TOTALQUAN.

£60Aj3pro:<: \

UNIT

<Jl.

EPA HazardousWait* ID No.

frOfri1|111

C W M AWASTE COOC

Aai-61-053

WEIGHT

*,&&•Apjr.rox

IMERGENCY INFORMATION

IMOUMNCY N0«.: OOVOMR — (201) 4S1-J9M ; «O4UUTO« —( SO4.* ) 8^2-4520 _ yj COAST QUAJtO 1400-424.M02

CERTIFICATIONThb !• »• b •*• . <ncriti<t

Dip«ilBH«t •! Tf«iu»«rt»Mo«. ttw U.S. lirrii

/ 96*

TW* to ••

x. •t«

TRANSPORTER NO. 3•»

1/k

Tltta

0DISPOSAL INFC

CWMAWASTE CODE

&PMT

AMATtON

QUANTmr

/P

UNIT

rr

PROCESS CODE

v -7^^r'^/:x>/

TRENCH

v',,-/

T

LOCATICtiLEVEL

/ ..,,

'

IK*

1QUAD

Dot*

COMMENTS

^"•'Z OU>0000

fa. <omltt«{1t-p<tcri)rypev»Tit»r.) "

«M HAZARDOUSiSTEMANt

ttl

Form Approved OMB No. 2000-04O4 Expire* 73121. Generators US EPA |p No.

p » n ft <

Manifest

»;• t- >i-

Information in the shadedaraas is not required by Federal

/wrvtor 8 NMIW *INC.

P.O. Box 960Piirtte fHrtlffa1 _ _

24. Transporter _J_ Company NamaSEARAIL TMT*

26. Transporter __ Company Name

?09) 852-452026. US EPA ID Number1A L D Q 7 727. US EPA 10 Numbar

28 US DOT Description (Including Proptr Shipping N»mo. Hazard Clast. and ID Numbar) R.W»«t« No.

b.

d.

32. Spacial Handling Instructions and Additional Information

33. Transporter. AcfcnowladQamant of Receipt of MaterialsPrintad/T] D. BOS

34. Transporter ___ Acknowledgement of Receipt of MaterialsPrinted/Typed Nama Signature

oo

OU)

Date

DateO.Y

t I

39. Discrepancy Indication Space

EPA Form 8700-22A (3-M)

IN C

ASE

OF

EMER

GEN

CY

OF

SP

IU IM

MED

IATE

LY C

ALL

TH

E E

NVI

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722-

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II

i

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1

(Continuation Sheet) PR DO 9 0 5 7 ft 0 1 J 00001

P. 0. Box 960Punta Santiago, PR 00741

KTrvnevortar J Company Nama i5. us ERA 10 Number

Sea-rail. Tnp. ————————————— tV1 " n ift All* fa V|L- — i<; 'i '•> .76. Tranaponar company Name) 27. us EPA ID Number

. i 1 . . . . . . . .

28. US DOT Daacriptlon (Including Pnpmr Snipping Warn*. Hmrd C/«««. em/ /£> Number.

CWM Profile Number

b.

CWM Profile Numberc.

CWM Profile Number

d.

CWM Profile Number

CWM Profile Number

f.

CWM Profile Number

B-

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COMMONWEALTH OF PUERTO RICOENVIRONMENTAL QUALITY BOARD

HAZARDOUS WASTE MANIFESTDOCUMENT NO.

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TKATMfNT.PttPOtAi (Tttl Fiipi AppRttif MORE THAI) TWp TMM«P»I Aft TQ f ||I|JW m OUT THE FWtOWIB AS APPMPIATE

FORM IS NO.————————— OF A TOTAL OF ——— THE FIHST MANIFEST DOCUMENT NO. IS. P . R I 1

ISPKIAl HANOUNO WSTBUCDONS WOUPIN6 COTAMEII EXEMPTION (it. IDENTIFICATION OF ADDITIONAL WASTES MCIUOEO IN SHIPMENT OF A (UNHAZARDOUS NATURE VUCHDO NOT HAVE TO * 4MMFE8TEO)

IfKMTOJrSCEmtFII TIOItniiithttM lluttwiif ft! Ktt vfbciMi ngulatiMi •» DM 0«pirtm« al Tnasportltion. US. EPA mo* *• Conunammldi of P.R Thi witu dMtribfd ibovo wtra tomignad ta thi Trwportw mnad. Tka

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FRO 002 0342

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law.3. Generator s NamePCR INC.P.O. Box 960

MM Mailing Address

>.R. ,00741 (809) 852-4520! US EPA 10 NumberP R D 0 0 0 7 0 6 2 9 .

». Transporter 1 Company NameASHLRNp CHEKTCAL

8 US EPA ID Number

l P R D 0 0 0 7 2 b 8 1 C 37. Transporter 2 Company Name

KAVTKR\R nf! PR.____Designated Facility Name and Site AddressCHEMICAL WASTE MANAGEMENT. INC.Emelle FacilityAlabama Highway 17 at Mile Marker 163Emelle, Alabama 3S459

10. US EPA ID Number

| A . L . P . O . P . O . 6 . 2 . 2 . 4 . 6 . 4

11. US DOT Description (Including Proper Shipping Name. Hazard Class, and ID Number)

•• WASTE SLAKE LIME N.O.S.OK4-E NA-9189

CWM Profile Number AT,h-Gl-053b.

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16.Special Handling Intuuctioni and Additional Information

18. OENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately describedabove by proper shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition fortransport by highway according to applicable international and natiooa^overnmentaLraimlations.

Printed/Typed NamePEDRO A. MARTINEZ

Month Day Year11 I 19 I 84

PRO 002 0343

manifest except as noted in

17> Transporter 1 wtedgoment of Receipt of Materials /

1». TfanaportyT^Acknowtsdgofnent or Roccipt of Materials

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20. Facility Owner or Operator Certification of receipt of* 9+

• ALABAMAHAZARDOUS WASTE MANIFEST

CWMAN2 81244

IMMTinCATIOM INFOtMATlOMNAMI

GENERATOR

f ANSPORTER NO. 1

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Chemical Waste Management, Inc.Emelle Facility

ADDRESS

P.O. i'ox SCOflBTl'il fr11'1- Irt' Cjf -> '-- JJ741P.O. tCX 1026

CS4 South CUtj .tiCii L.C.

P.O. Box 55Emelle, Alabama 35459

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EMERGENCY INFORMATION

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DISTOSAL INFORMATIONCWMA

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PART A:

COMMONWEALTH OF PUERlO RICOENVIRONMENTAL QUALITY BOARD

HAZARDOUS WASTE MANIFEST

DOCUMENT NO. P. R.

TREATMENT. STORAGE ORDISPOSAL (TSD) FACILITY

IF MORE THAN TWO TRANSPORTERS ARE TO BE UTILIZED, FILL OUT THE FOLLOWING AS APPROPIATE*

THIS FORM !S NO.——————————— OF A TOTAL OF ——— THE FIRST MANIFEST DOCUMENT NO. IS. p. a i i iPROPER US DOTSHIPPING NAME

US DOTHAZARD OASS

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TRANSPORTER NO. ( SIGNATURE•Jtorttf ttM conttnt* el 0*1

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TRANSPORTER NO. 2 S6NATURE 7<ty» k«tt of my km***))* th* conttnts of thtinippmmi I hiv« iccopti4 lor tramport eonlomu with th« ottcription on this mini!wt."

TRANSPORTER NO. 2VEHICLEID NO._______

I I I I I I I IDATE RECEIVED

BIVTRANSPORTER NO. 2 H6NATIME1 (01% Jh« I kwo not innpor»4 with or mtttriUty•iKHtf tbo contMtt of thit «Xpei«t"

fKE4TMiNT STORAGE M DtSMSAJ. FACJUTY WOCATION OR ANY DIFFEICNCES BETWEEN MANIFEST AND SHIPMENT OR LISTING OF REASONS HANOUNGHOD

FRO 002 0345