Percobaan IV_Destilasi Larutan Biner

LA?}RAN ?RAl<TtKu/\ KtwrrR FIS}<A

Ois-tilar Larulan Biner

fi/omo r Lahraloriurn

Nll4

)ldnt

: K-[? -U0^f, l0o vl37 377:{

t 2 Ail lotz-.'' f4eretga Rraurr'

hgoPfioPrun KIMIA fisrlcA

JuRusnru KnrttA.

FAttuutns MATFIAlrT,kfi DAhl I LmU PF NlaETl{tuA\,

0l\JrvElts|TAS Rl4V

&rnNenruPo12.

4l#tt

fo{ta',i Larutan Birrer

AbArac'l

Drsti\a{ion ts 3 Lcnique og cfranical sepralion lffitd on

dyF** in Siting 'pirt,.

ln tttu ar4iwrrl, chewical

rrra.{"iat ulod{ &htalrd ruar mixeJ oS glutal aceltc aci,l

' tdi{h aqudttt' csnen{rat-.ovr of 6ahc aad reuvlel dts'lila{ton,

ms?'vrej m eaoh aAduJ I nrL, lo nr-, Anl 2o mL Aqfudei,

llne mued {axen I nL brS,r;, lq€al,r,s Cd, hlilale (0), and

Tat,dv fB). Each d&A aq$M+ arifom Gdvlton of

Scalic aad cor',unlraliw' '[h" wlve c,x,cen{nhans op aelic

adJ hral resul'l R ) c ) D- thts elfiild lnne754

Corrca,ka{ion -lhat kehc Ac\J htu tavLl ts tubre lwe.

P,qLasan

k{r|ali alar,n bpntr pmisahon hrvria

Wk,daan tifir ddit" . hAa gabaan inr mid

y-dng didafi las,- adaltu nmryran ssdy d9rynn

0ir- lre:nsrlru; wrn u*al hasil d^hltu' Lry-

hnp ponanhahan I rur, /o nL , dian co mL aquadei. Camyxr*t

diarnlrt I rnu sehlw fzzrnanrltan Cc), da];1y CD) , dan

t2"sidu CR). sehap pniathlnn Oquad' I wwnilkan

fujvrarBan W.lra('i dwn Aelral, i;ildi korc"nfrarr' asdh

e;Ya4 VMrg ddapNtan R 7 c > D. tni merNnful,an FrtryUTtukotvnlrAl,: tnhi,gg, a{dm anlar yanT dihasrtVan bbih'rrurni '

I. fie frrlose of 6,prttwt+l. Ur&rslan| dailafiorr prncipal

l. (hhnlru dalas lhceserty (r a Chari lqu Mwr.nCorrrpr{ion. boiting P'n{ aF firnarg Soly/ion2n Wcoba24Tujran Wcoba\n

l- l.tovighami ?nnsip. d"t'httst2. Mrrlen[vn 661x- dab ganq &prl.wan ,uyilvk s,m]yt, u,tani,rUVa' da+a- lala yang

_

am/gra;1v

Laporan Praktikum Kimia Fisika I

ri-(rtit AJl" dari larulm biner

II. Latar &takang feorf PtahaqDstrlat; per{arna katr' ditqnukan oleh krrnr auran

Yunoni Sekrtar 'bad

*nhna rn'sehr- yang

dtpiru {rruteqo oth tinggrnga prmin{aan(ksrhpa, r*g).

kt lasi sr&rtaana dav drs{.lasi brasa alalah tekn tk

iebihpmisahan krnrd rrntvt merrti2ahkan fuq alavicomnnan qanq rrPmttrki Hhdaan f*it< didih ,/ar

Dttital; a{au Psnuulinqan adalah &rt{u rnelode

kmisahan hhan hm6 Wr[asrVan gh]aan kecepalan

?{au kemudahan fiajuap fvotatital) lxhan ilav dtdeginisr]an

FirnfE uS&p Mlanrkan

Pa"rbagqan Dahlartl. W*aEarvan Wwrfi {r, qi dva, gailv,

0 Dtstilal lontrn,ub. hhlas; botrh

x. Berdasarkan bis trkanan lprlrs\nga fur@l hq^, gEiirr:'d . DstrUEi a'l.rnoge.is

b B{rlasi \lakun r

c. Dsh\x; IBvanan

Ba&sarLan lomprren pergosnnTS Ierbl d,n, Witu:a- bhlal sisbrv binerb. h{rlar; sistr

Bx&sarkan sistervl 1i dra, ya,l,u'

0. l'rngte-sQ" di

b n'?uHi -sl:{,, dislilalion [Larfit a , cnog).

. Se\ain p*hqtan drr+,tagi di.alH, oblar referensi\ain^ runybu{)can matrin^ fi6an &shuar i,gairly,I- Dstilal xrht*tana

pePdn

3

1.


Jauh.

p. k{ita:i ka)csionali (a"hrtfa+)an &ftfnri e&rhano,lnrye &.s{ttasr

.or&tor iary lebth

hnpow yary

t-IbmlrKr' perkha n.l.Dshlaii '/zeotmp

teLanan tnggi.'f-Dshtgl l)"?

Untvk nvrwgil ,n zal /xry.adalcm oirz cbn {r{,r. didrhriya cv

Vfulvvn ?41 ssiF +rsebul nvnnfnizal calF svdah herura,', {rrokri da"r,' dlau mewelaml

[9ahi yrubatnn- YLaua zal rsebu] htrae- drytdimurnik2a secara duhta>i s a ah, daltlis,.br.{irgLnt, rnela,nW haws art' &)gan desJrlasr'

v6D.

l. Ds'trla:r \An,nl"lunisah Larr h^ fr-f. &*hnv a

atlatat, d"ganrend7; dari

ral die yangrulan Aary fi-lLilaLvtan derc1an

a- M"'[oJe I

Wnn caftLarulan Vnrgtanpa adtb)ana.


b- l4utoJ" ttda.i pn&nt tce bJana

xhnga l*ulan {a6eb,iluSlt Vang rnergalrr k ala5

1flA6m zal CSir 1lan1dr&{ila:iYa^ Mks +r{ir.

"

P, = flr p

nn7 =fl,p,+fl;?z-

Datarrr hal ini,P , Tevanen ty{a t

gatv larulx W kdri,dy, ' L3rn[xnn V Jun B rvrgtap,

rnak6 b4non dp ^ t?A) dinyalari seb4at .

fla= Pi -X^

dirran a, t


(wiJr-un Ii , aoot).

i rnolekol {at salents Lebth

aYsi fnoleLvl sehnts maVa

hykur RouL{, dan sabatit

fiolekvl -{ap S",tnis tBbit,

rnolek/t se)enis ftdks tB]' rnan fotar a?an bbirt Lzsa,chri p:rhrlvngan lil^rn RouL{ fliq Lab. }c*u nofi ioitl.

lll "'The Eqaprrwnts a'm] |'nakrralr /nn+ &an blnnfl.-fV egu)prrynts wd I AIat yang dtqunaLan

t. Ds{ilalicn flrsx / WW drshla:i -

J. gtrrnrg hr'/ &targ Yga'l'lt' flgnome{er f'tamorrv]*

1' Grcbns"r / Pond;,'*'

7. B',re{ 1o 6L6, WaWr glass / hetas ptala loo mL

7 , TpHe'Atp I 6p+ I'Vs

B' Prlenm"Ym Ji /hl^

ML

@las ukur 5 r,rnt^

Has vW( 9o rnL

p( Udure

13. sya{vla

Srto Jr'

t1. fint llaV /tfut hnr J5ornr-

6. Walerue thz t)"?.Iir:e rnaterial wd /

| , QYacial kelic

A. MOtt o'5 M

7. lgudnst /aryab4' {?.enottlatein


lV. The tlrerrre \,Uorks

k1pre lmttng, t.m] fiorn lhe dishlahon rr {aWn and mlvddit b alenrtup..(c,J

lo rnL oy gbfrll fcelic eqA rryd wilh I nL sp aqvacbsl

ln{o a *sftlahon gtask.

Con&rgr mour{rd, Stirring g{ones anJ 'fherm ovnel^'- lfW4eJ 610{ne ds{ibtron flask.

AM t dnp or tndca{or ?p anl {i'lrat"J tL wlh Mayll er rt

{d. drst'lat" r{ capcrly up +o

rr.orJrJ a{ exac{lq I tnu tD,)

Aldtt I 'drops of tnit turln [/ao[t otj N ,

, I mL op llx d'tshYdlion is hy"n (

r drry op lndrca{or pp bAJaotl 05 N '

l,tltuh %rne5o Acdvirc

SKP

J dala

drJ it for il)eA agrn&{ lo ard ao rnL,Cr, Rz , C^, D.. XnJ

9 k na k*Ja

lo rnt dmn eplat qlual

V< &lam tah, &Urar;urlctn M^, I mt aqv'#*ls

Konf',so. diruag , Hv *k &la.n tah Jshr i . ' '


gdutn Frnanosan, I mL dari tabu &lh'las,' d;a,rrbit

dimauran VE dahrn erlenrrralrr Cc,).&an

rndrta{or pn di{arnbahyan ve Cr dan dili.lraE,'

Mott o', N3 {tlqdu,,orn

P*nanalan Jimut6i, dalihldtata+ sN [am+ 1 mL

di.hrnpung hiry9a I rnL, suhvllD, )

? te{.:

dutqan

ln&uat". pp ditarnbahYan

A/aOU Ol tv

W. 0t /,an dr h{rusi

Pqnr'gffn dil,B'^litan , I rnv da'i lahr &shles,' diarnbrt fn

?{e\a tnJivoior ?V d."tambar,ran ke Rr dan diti{,ar,'

aqnks lo dan co mL" VlaVe

C., 0n den R3

L'rrqUal'r #ry sart10

&p*v,IaLwavt unlrr

&{aptanbahanQ, 0^, R.,

V. Eb dan llatit Prrqama{v WVaa,a Puna*hhan f ,^r^ qudu, 9tN lol"c

Ct, UaOH {ergaLar'

D, Mou {<PtaiR, , Naoll ta ptcsf

b. Pet'rardoahan lo rntcL, MoH {crpaY?iq, [JaDLl {aPLf ''R1, M0tt tnpata,'

c. P*rambahan ?o rnl-

C7, lw)rrq lrr[ahi

Jdr I MflB, B rnL

h,l mtAlWleS, guhv lDo"c

,r,g rnL

c)i nrL

lt,7 p L

aq\frM, &hv /oo o

c

4tT lxL

A3 rhl5,4 rn l-


Vl- P.rhiluryan

p= N-V-&= h5. ot75.7!

I

= T gram

l, ltcnqrr{osi Asam

a. Rnamhhan

CtVI

Dr. v,1

Rr' V'

t

b Psnambahan

c, V'

I

AeIaI

I rnL

tJr = Vl A/,'

Nr = 1g,l'O$Nr = l{,05' V

N,Nr -- l.9,0'o'5Nr = 6AoNNr:VrN*f,Jr= 75,1 .0,5

Nr ' 17,r, N

Io rnL

Nr ' \[, Nt:-

Nr . lJ' 9-0,5

Nr' 0,{5 N

Nt = VL Vr-

Nr ' 9,1' 0,5

N, = y',7J N

;.J, = V2 Nz

Nr : l3J' aiNt.. (0,85 N

D, Vr

I

R. V,

t

c. p**plnhan co rnr-

C7 V Nr " V1' NJ1

t Nt= 4,7-0,5

Nr'239w


q v:N,= VrNe,| ' Nr -- ?,1 '0,1

Nr= lllN?t. VN,=V'Nr

t 'lur : f,fl' 09

N,:CloN

e- kat \arutan

f asrn ase,l8{ ' l,o6 lgtta Pd?attrbhsn I mLq'

'='!'oll '''10,b grfin

b.Pnanbahan lo rnL

Cr- m = f-v=t,ob.l&= 19,90 g(M

c- Pmarnbahan ao rqt-

ca m=f-v= l'06' )5-- 3j,t 96(rl

^' BrA Aam Asetal

e. ?nrnm]rfrhan I muc1

'= l)*u. ,nir,

= 1,06 gr/nv

Dl. m= f -v Rr

=l,ob-9

> Er4 grarn

rtr= f V 7t=1,*.11

= /8101 grlm

m=f -V V7

=1,06.31= 36,0{ grtm

re: f-v= Eo6-&

= $,,10 qr?n

rn= f-v: l,o6 - ll,

_- l6,gt, gr?n''

m '/-v=l,ob. 37

=t4,9,3 qfu\

6oI

= O'64V g(avl

D,' W : AJ- V - &-- 9'{0 ' o'ovl ' bo

I

= qrfl gram


Rr- W=N-V-&- wtil. otaol . g

I

> l, oi5 grarn

b. Pernrn\sohan lo nrLq t,u = N'V -Bc

, 6fr.otwl. 60

I

Da

' 0,907 gran

tn: N-V- 6.=4i17'o,aot -60

I

R'-

= o,lffi gram

l1g= l.t. V. E'c

" 6d5' o'ool ' 6ot

= o4ll gr8rn

c' l%nanr'bahtn pn yvrL

L7 w= l..r-V- &z h35- o,ool' 9e

I

D3

s OrHl grdfi

W: N.V.BC= l,l5' 0rol' 6o

I

Rg

= 0,0b9 gt8M

[4y = fu.V B?

= 0,171 gmnn

@t


Berat Rira. kra$!'ohn I rnL

q- War. = trJraux4 - Wasarvt Bse{al

= 10'6 -o'0q3= 9,717 gfarn

D, W&r' W uantat - [rJ 4nnn aula+

' 9,14' A561- 8,97i fitfil

Rl Weir = W\?nrten - lila$am ap{at

{ E,'{d - l,q3= J,491 grlrfi

b'Prnombohan kr mLct watr:

'Hf::; l* u*a,

= 18, 6is g$mD' \loir

: HIH- wasa^ aplar

= t7,Tj, grail

Ra \'uair ==Y,W;rrf'o' ageta+

= 16fi41 qrlm

c. ?aunbaW a,o /vrl

Cr, W atu = U) larrilan' Wosanapla+

= 371- o,t4l

= 36,999 qnnDi UJ arr : [,tJ tmda n - V)aw aPlOl

= 36,fr- o,obg

= 31,911 gnrn

Pf L,.J air -- hJ larularr- (rJasar fu?tal

= U,g[- oJT4

= j.l, $oL qwn


5. Mol Aarn Asdat

A. faramhhan I *tCr. n= ! Dr- r

tr\r-

_- 0,&43

b= 0, Oll mOl

b P.ffarnhhan lo rnL

% n=E Dr,ntnn

= 0ri0-7

6o

= 0,006q5 mo\

c.Pavnlrrrlan fln rylL

C-l n 4rMrO,l4l

0o

= Q0o4'15 nol

% n =y Ra.n' thr

= [,06!bo

--E Pr'iv\r

=Wl0

" 0r4M nol

= otD605 mol

=9nlrlr

6o

= e beJ rnol

=91Nlr

: 7,4t'l

,d

=0il2| yy1s1

Rt n= 3Ilnr

= y,rlg-l0

= 0t9t91 rno\ .

= gv Rr-

Vtr

= O$bA

h: 0,0fi1fl101

n= ttvtr

: lrD91.

Ao

= O,oUj rnol

9rMp

oAh6o

Rz

= 9,00135 yot -- Qaon5 rnot

6. Ytot Aira- PsnOsrbahan I mL

r o"$ 0,- n

Mr

= 9fl17ld

= 0'5fi I nnt

b, ?awnbatnn lo mLq- n -' 1- D1- rr

!nc

= N,6qt_r0

= lr 0385 rnot : o gg5g rnut


c-?awlbfihiln ?o rvrt

C3 ll=L h n=tl4r hr

= U,|roi. = 39,911

i$ l0-- ?t 05)j y$o\ : lrggf4 rnot

7. Ft8lcri Mol Asam AsstdXas"let 2-LfuAlL-

0oP\6I t n &c

a' Prnarnb*,an I mL

P1 n=AMc

= 1{,drA,0

:lt97VLnrl.

q. Xaeta{ =_Q7Aftd4+ =

D

Rr.

= 0t OoA49

(o,Mr+l,oilt)ot oo fiS

o,ol4 = oto2j7

0r55tt

0,oo91 -- 0,OIB50t7dlo toYi

= ot do10t45ot

Ot0066 = ot0o6?I t 01195

o,oo175 - oroo40ot99oo5

o,oo685 .= Ot0o77ot qtaJS

b, P*nambaMn to rn L

C7 - Xalrlal

h. Xaselal 'l

c. ?"natu,loahan ?b rnLCt- Xae,lal = 0, otL)L : or@1V2 . = hrcDll

(o,oott, +?,611 t ,fr5 4X6$at. otOOU'

= o, @ll5 - = o,00o6

[0, m6 + t, go4) I ,9g9 55Xaslat = 0tbo29 = o,ooT9_=oroolr

Coitrl,g+l'%%) | g%,5


B. Fausi l'4Dl Air

Xarr=, h 6irfl $r { 0apbl

t. ?qrasrbahan t rnu

C\. xa\t - o,t4rl =

foflrt+q o H]

D'' Xatr = -PIAN-[or9$r+o'Pog1

fl{- Xtrr =]94!L = -0,4V,A = otgig3

b'4tto+t,061 6t45ot

b- F'ana*baharr lo ry1L

CL Xair= ttfi$J

c.

0P3a5+otoo^s)h, Xfir = OlM-

=

= ?,0537 ,-

(e,q$ro,ostg9\-- | t9A81

(o,oottl+1, 99${)

= | 'q|U(hnv6)

L oz85 -_ o,ffi301,04495o,gg53 = orjgSt0,99 oos

ot9t94 - = o,g1t6o,1cbl5

= e,oca9. = o,q989x t6165

=-L9904- = 0t9997l,9q55S

e l,g33E = or9gyjt t9765

Rr. Xar

kambdran

q' Xair

D'', X air

Rs Xair

9. GGftu frak-si mol vs luhul. F i Md vr S,frv Gn

Suhu ['c) Rafri P4o1 Ar Fnpsi Mol Ase{at

Iob

loo

loo

0 9740

0' 99\9ot i905

q 0?r7

0t o062

A t 00ll


Gegr I' Fnvlr U,lot ve S,rhu ('c\ Ctrwt707

106

105

to4suHU 103

102

101

100

99

y=-305,53x +4O4,47

R2 = 0,9578

-#fraksimolair

{-fraksi mol asetat

y=295,1x+99,019

R2 = 0195

guhu 9t) fraui t'tot Air fnni MD\ I-r{al

loL

loo

loo

0,9915

0$71o,%gA

0,Ot0,

o,@,8O r0006

IM t. DaYa Fahi He\ v! glhv htnt

6opr a . Rapli Mol vs Su hv C'r) brtila{

107

106

105

104

103trtu ,'0,101

100

99

98

0,4 0,6 0,8

FRAKSI MOL

y=401,5x+99,059

R2 = 0,9335

.+FRAKSI MOL ASETAT

+FRAKSIMOLAIR

y=-403,85x +5O2,75

R2 = o,9423

3. 2 f@i Mol us

lrtru uc Foui w\ Arf FraV,i l'4ol Asotat

loo

lou

lo

Q9191

aggtt0,9j05

u04ofot0017

O,0d,

fa?


to7106

105

104

suHu 103

to2101

100

99

y= 186,44x +99,222

R2 =O,974t

+FRAKSI MOL ASETAT

-I-FRAKSI MOL AIR

y= -188,25x +287,37

R2 =O,9727

GnFv t. fraln Hol V9 9fiu Coc) eJidt,

Vll. P*r,bahasarT

vlll. lcerimprbn

| . Dati\al adalan telnir. peryfisahan tirnid hdasar ka,tp<hJoan t'hr drJi r"

c. lluga hnrrnJrarr R)c)D3' ?vnakrn Aanpu Wnml[J'rn iltr tk6(w,Jrasi agam at'l*fivnvutt{' A@ yng lebivt Wn; lrdaya.t di resdv.


fiI\p t/wwar. Scie rre La b.

abs VA targqat t

Ap.il lolr.

@p'il w r,^trl Science 1tu. nm /ae+wrr;,A- nsds . p df .

llnuw Vada brgqal I Agil ;DIc .

Anontft. 7olo.

1r Lahr Krnrr? filika .J012. Paunlvn RaL4tutn hmrahs'La l. universitas ffi,

[,h'verr\as NWa YngpLa,la ' Yry*akarla '


Percobaan IV_Destilasi Larutan Biner

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