Page No - NABL India Web viewDehydrates Fruits And Vegetable Proudcts [Onion Seasoning Powder]...

Laboratory Vimta Labs Ltd., Life Sciences Facility, Plot No. 5, Alexandria Knowledge Park, Genome Valley, Shameerpet, Hyderabad, Telangana

Accreditation Standard ISO/IEC 17025: 2005

Discipline Chemical Testing Issue Date 31.03.2015

Certificate Number T-0047 Valid Until 30.03.2017

Last Amended on - of 177

S.No. Product / Material of Test

Specific Test Performed Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

I. DRUGS & PHARMACEUTICALS1. Pharmaceutical Formulations

Ibuprofen Tablets DissolutionAssay

IP 2014 (by titration) 50 % to 120 %90 % to 110 %

Metronidazole Tablets

DissolutionAssay

IP/BP 2014 (by titration) 50 % to 120 %90 % to 110 %

Paracetamol Tablets

Assay IP/BP 2014 (by UV-Vis Spectrophotometry)

90 % to 110 %

Isoniazid Tablets DissolutionAssay

BP 2014 (by titration) 50 % to 120 %90 % to 110 %

Paracetamol Syrup 4 – Aminophenol Assay

IP/BP 2014 (by HPLC) Limit Test90 % to 110 %

Sodium Chloride Assay IP/BP 2014 (by titrimetry) 90 % to 110 %

Dextrose Injection Assay IP/BP 2014 (by optical rotation) 90 % to 110 %2. Hormones

LevonorgestrelNorgestrel

Assay IP 2014 90 % to 110 %

EthinylEstradiolTablets

Assay IP 2014 90 % to 110 %

3. General Tests

Anita RaniConvenor

N. Venkateswaran Program Manager









Pharmaceuticals and Formulation Chemicals

Description IP 2014/ BP 2014/ USP-37 As per the Monograph’sSpecification


Solubility IP 2014/ BP 2014/ USP 37 As per the Monograph’sspecification

pH IP 2014/ BP 2014/ USP 37 1.0 to 13.0

General Identification reactions

Chemical reactions

IP 2010/ BP 2014/USP 37/EP 7.7 (By UV-Visible, IR)

Qualitative

Limit test for chloride IP 2014 Clause. 3.10/BP 2014 Appendix VII/USP 37 Chapter <221>/EP 7.7 Method 2.4.4

Qualitative

Limit test for Iron IP 2014 Clause. 3.10/BP 2014 Appendix VII / USP 37 Chapter <241>/EP 7.7 Method 2.4.9)

Qualitative

Limit test for Lead IP 2014 Clause. 3.14/ BP 2014 Appendix VII/ USP 37 Chapter <251>/ EP 7.7 Method 2.4.10

Qualitative

Determination of sulphated Ash

IP 2014 Clause.3.22/ BP 2014Appendix IXA/USP 37 Chapter

0 to 20 %

Anita RaniConvenor










<561>/ EP7.7 Method 2.4.14

Determination of water content

IP 2014 Clause. 3.24/ BP 2014Appendix IXC/ USP 37 Chapter<921>/ EP 7.7 Method 2.5.12

0.01 % to 10 %


Determination of Ash IP2014(Clause 3.38) /BP 2014 (Appendix XI J) / USP 37 Chapter <561>/(chapter <561> ) / EP7.7 Method 2.4.16

0.01 % to 20 %

Clarity and Colour ofSolution

IP 2014 Clause. 6.1,6.2 /BP 2014 Appendix IV A& IVB2/EP 7.7 Method 2.2.1&2.2.2

Qualitative

Disintegration test for tablets IP 2014 Clause. 7.1/ BP 2014Appendix XIIA/ USP 37Chapter<701>/ EP 7.7 Method 2.9.1

1 min to 180 min

Dissolution test for tablets Dissolution test for capsules

IP 2014 Clause. 7.3/ BP 2014Appendix XIID/ USP 37 Chapter<711>/ EP 7.7Method 2.9.3

50 % to 120 %

Loss on drying IP 2014 Clause.8.6/ BP 2014Appendix IXD/ USP 37

0.1 % to 30 %

Anita RaniConvenor










Chapter<731>/ EP 7.7 Method 2.2.32

Loss on Ignition IP 2014 Clause. 8.7/ USP 37Chapter<281>

0.01 % to 30 %

Optical Rotation and Sp. Optical rotation.

IP 2014 Clause.8.9/ BP2014Appendix VF/ USP 37Chapter <781>/ EP 7.7Method 2.2.7

89 o to 999.99 o


Refractive index IP 2014 Clause.8.13/BP 2014 Appendix VE/USP 37 Chapter <831>/EP 7.7 Method 2.2.6

1.3330 to 1.6500

Weight per ml IP 2014 Clause. 8.15 /BP 2014Appendix VG/ USP 37 Chapter<841>

0.9 to 1.3

Weight per tablet IP 2014 Page No.2.5.3/ BP2014Appendix XII G/ USP37 Chapter<905>/ EP7.7Method 2.9.5

0.005 g to 1.5 g

Residual solvents(Organic Volatile Impurities)

USP 37 chapter <467> (by GC) Acetonitrile ≤ 400 ppm

4. Injectables particulate matter IP 2014 Pack size >100 ml;

Anita RaniConvenor










Products 10 micron≤ 25/mlPack size >100 ml;25 micron≤ 3/mlPack size >100 ml;10 micron≤ 6000/containerPack size >100 ml;25 micron≤ 600/containerPack size >100 ml;10 micron≤ 6000/containerPack size >100 ml;25 micron≤ 600/container

5. Blood BagsChemical

Oxidizable constituents ISO 3826 (part 1): 2003 & IP 2014

0.1 ml to 5 ml

Ammonia Qualitative

Blood BagsChemical

Chloride ions Qualitative

Heavy metals Qualitative

Acidity or Alkalinity Qualitative

Residue on evaporation 0.1 mg to 10 mg

Opalescence Qualitative

Coloration Qualitative

UV absorbance Qualitative

Anita RaniConvenor










Description Qualitative

pH 1 to 13

Total citrates 90.0 % to 110.0 %

Total Sodium 90.0 % to 110.0 %

Sodium DihydrogenPhosphate Monohydrate

90.0 % to 115.0 %

Adenine 90.0 % to 115.0 %

Dextrose 90.0 % to 100.0 %

Loss on Ignition 0.0001 - 2.0000mg/g

II. FOODS & AGRICULTURAL PRODUCTS1. Meat And Meat

ProductsHeavy metals

Lead IS 14988 (Part 1): 2001 AOAC 972.23/AOAC 999.11-2000

0.5 mg/kg to 50 mg/kg

Tin AOAC (18th Edition) 985.16 0.5 mg/kg to 50 mg/kg

Metal contaminants

Anita RaniConvenor










Copper SOP No:06/03 2014.04.16Issue no. 8.0


Arsenic SOP No:06/03 2014.04.16Issue no. 8.0

0.01 mg/kg to 0.1 mg/kg

Zinc SOP No:06/03 2014.04.16Issue no. 8.0


Cadmium SOP No:06/03 2014.04.16Issue no. 8.0


Mercury SOP No:06/03 2014.04.16Issue no. 8.0


Chromium SOP No:06/03 2014.04.16Issue no. 8.0


Nickel SOP No:06/03 2014.04.16Issue no. 8.0


2. Dry Fruits Extraneous Veg Matter IS 4333 (Part 1): 1996 0.1 % to 10.0 %

Insect Fragments IS 4333 (Part 1): 1996 0.1 % to 5 %

Rodent Hair&Excreta IS 6261 (Part 1): 1971 0.1 % to 5 %

Anita RaniConvenor










Added Colour SOP No:06/43: 2013.1.14 1 mg/kg to 100 mg/kg

Acidity of Extraced fats as expressed as oleic acid

IS 1011: 2002 0.1 % to 15 %

Metal contaminants

Lead SOP No:06/03 2014.04.16Issue no. 8.0






Tin SOP No:06/03 2014.04.16Issue no. 8.0






Dry Fruits Mercury SOP No:06/03 2014.04.16Issue no. 8.0


Anita RaniConvenor














3. Nuts & Rasins Extraneous Veg Matter IS 4333 (Part 1): 1996 0.1 % to 10.0 %

Insect Fragments IS 4333 (Part 1): 1996 0.1 % to 5 %

Rodent Hair & Excreta IS 6261 (Part 1): 1971 0.1 % to 5 %

Added Colour SOP No:06/43:2013.01.14 1 mg/kg to 100 mg/kg

Acidity of Extraced fats as expressed as oleic acid

IS 1011: 2002 Annexure B

0.1 % to 2.0 %

Metal contaminants







Tin SOP No:06/03 2014.04.16 0.04 mg/kg to 0.8 mg/kg

Anita RaniConvenor










Issue no. 8.0

Nuts & Rasins Zinc SOP No:06/03 2014.04.16Issue no. 8.0










4. Cereals & Pulses Moisture (Loss in Weight determined as specified)

AOAC (19th Edition)925.09 & 925.10

0.1 % to 20.0 %

Argemone Seeds IS 4333 (Part 1): 1996 0.1 % to 3 %

Khesari Dal IS 4333 (Part 1): 1996 0.1 % to 2 %

Insect damaged byweevilled grain

IS 4333 (Part 1): 1996 0.1 % to 5 %

Other Edible grain IS 4333 (Part 1): 1996 0.1 % to 10 %

Insect IS 4333 (Part 1): 1996 0.1 % to 10 %

Anita RaniConvenor










Rodent hair & Excreta IS 6261: 1971 0.1 % to 5 %

Cereals & Pulses Metal contaminants















Chromium SOP No:06/03 2014.04.16 0.5 mg/kg to 50 mg/kg

Anita RaniConvenor










Issue no. 8.0



5. Salt & Spices Extraneous matter IS 2322: 2010 0.1 % to 10 %

Insect IS 2322: 2010 0.1 % to 20 %

Salt & Spices Rodent Hair & excreta IS 6261: 1971 0.1 % to 5 %

Moisture and Volatile matter at 103°C

AOAC (19th Edition) 986.21 0.1 % to 30 %

Total ash AOAC (19th Edition) 941.12 0.10 % to 15 %

Ash insoluble in Dil HCL AOAC (19th Edition) 941.12 0.1 to 3.0

Solubility in cold Water on dry Wt basis

IS 3633:2003 0.10 % to 30 %

Total Nitrogen on dry basis AOAC (19th Edition)920.173 0.1 % to 30 %

Crude Fibre on dry basis IS 10226 (Part 1): 2010 0.1 % to 50 %

Added colour SOP No:06/43:2013.01.14 Issue No. 1.0

1 mg/kg to 100 mg/kg

Volatile oil content (v/w) IS 1797: 1985 0.1 % to 20 %

Anita RaniConvenor










AOAC (19th Edition) 962.17

Tendrils ,Moother Cloves IS 4404: 2010 0.1 % to 10 %

Khokar Cloves IS 4404: 2010 0.1 % to 10 %

Headless cloves IS 4404: 2010 0.1 % to 10 %

Insect Fragments IS 4404: 2010 0.1 % to 10 %

Insect damaged cloves IS 4404: 2010 0.1 % to 10 %

Damaged /discoloured cloves IS 4404: 2010 0.1 % to 10 %

Salt & Spices Insect damaged matter IS 4404: 2010 0.1 % to 10 %

Rodent Contamination IS 6261: 1971 0.1 % to 5 %

Lead SOP No:06/03:2014.04.16Issue no. 8.0


Copper SOP No:06/03:2014.04.16Issue no. 8.0


Arsenic SOP No:06/03:2014.04.16Issue no. 8.0


Tin SOP No:06/03:2014.04.16Issue no. 8.0

0.04 mg/kg -0.8 mg/kg

Anita RaniConvenor










Zinc SOP No:06/03:2014.04.16Issue no. 8.0


Cadmium SOP No:06/03:2014.04.16Issue no. 8.0


Mercury SOP No:06/03:2014.04.16Issue no. 8.0


Chromium SOP No:06/03:2014.04.16Issue no. 8.0


Nickel SOP No:06/03:2014.04.16Issue no. 8.0


6. Fruit Drinks:(Mango Fruit Drink ,Concentrated Fruit/ Vegetable Juice (Juice Concentrate)

Chemical Parameters

Total soluble solids IS 13815: 2010 /ISO 2173: 1978 0.1-90%

Acidity (as citric acid) AOAC(19th Edition) 950.15, 42.15, IS 13844:2003

0.1 % to 10 %

Colour added non permitted & synthetic colour poncea 4R

SOP No:06/43:2013.01.14 1-100%

Metal contaminants

Anita RaniConvenor










Lead SOP No:06/03:2014.04.16Issue no. 8.0




Arsenic SOP No:06/03:2014.04.16Issue no. 8.0



0.04 mg/kg -0.8 mg/kg







Fruit Drinks:(Mango Fruit Drink ,Concentrated Fruit/ Vegetable Juice (Juice Concentrate)





Anita RaniConvenor










7. Bakery Products(Food Aid Biscuits)

Acid insoluble ash in Dil HCL(on dry basis)

IS 1011: 2002 0.01 % to 0.5 %

Acidity of extracted fat (as Oleic Acid)

IS 1011: 2002 0.1 % to 5 %

Added coloring matter SOP No:06/43:2013.01.14 Issue No. 1.0

1 % to 100 %

Salt (as Sodium Chloride) IS 7874 (Part 2): 1975 (RA 2004) 0.1 % to 15 %

Artificial sweetners(singly) SOP No: 06/44:2015.04.15 Issue No. 2.0

0.1 % to 20 %

Asparatame SOP No: 06/44:2013.01.08Issue No. 1.0


Acesulphane -K SOP No: 06/44:2013.01.08Issue No. 1.0


Metal contaminants





Bakery Products(Food Aid Biscuits)



Tin SOP No:06/03 2014.04.16 0.04 mg/kg to 0.8 mg/kg

Anita RaniConvenor










Issue no. 8.0











8. Fruit &Vegetable Product

Moisture content AOAC (19th Edition) 934.06 0.1% to 90%

Ash insoluble in Dil HCL AOAC (19th Edition) 900.02 0.1 % to 2 %

Added coloring matter SOP No:06/43:2013.01.14Issue no.1.0

0.1 to 50 mg/kg

Sulphur Dioxide AOAC (19th Edition) 990.28 0.1 mg/kg to 250 mg/kg

Metal contaminants



Anita RaniConvenor










Fruit &Vegetable Product

















Physical parametersRodent contamination IS:6261:1971 0.1-5%

Total soluble solids(TSS) IS:13815:2010/ISO:2173:1978

1- 100%

Anita RaniConvenor










Acidity as Citric acid/Acetic acid/Lactic acid/L-Tartaric acid/Malic acid

IS:13844:2003 0.1-30%


Added Nutritive Sweeteners SOP NO:06/44:2015.04.15 Issue No 2.0

50-500 mg/kg

Moisture IS:10623:2012IS: 3508: 1966

0.1-100%

Hydrocyanic acid AOAC 19th edtn(920.144) Qualitative

Acid insoluble ash(HCL) IS 13846:2009 0.01-1.5%

Total Sugars IS 3881: 1993 1-70%

Sulphur Dioxide content AOAC, 19th edition, 990.28 1-200 mg/kg

pH IS 14328: 1995 1-14

Extraneous matter IS 4333(Part-1):1996 1-7 %

Damaged Matter IS 1797:1985 1.5 - 5%

Ascorbic acid IS 5838:1970 0.01-1000 mg/100g

Colours SOP No:06/43:2013.01.14 Issue No. 1.0

1-100 mg/kg

Total Ash IS 14466:1997 /IS1656:2007 0.1-15%

Anita RaniConvenor










Mineral Impurities IS:13816:2009ISO 762:2003

0.1-1%

Lead SOP NO:06/03:2014.04.16 Issue No. 8.0

0.5-50 mg/kg


Copper SOP NO:06/03:2014.04.16 Issue No. 8.0

0.5-50 mg/kg

Arsenic SOP NO:06/03:2014.04.16 Issue No. 8.0

0.01-0.1 mg/kg

Tin SOP NO:06/03:2014.04.16 Issue No. 8.0

0.04-0.8 mg/kg

Zinc SOP NO:06/03:2014.04.16 Issue No. 8.0

0.5-50 mg/kg

Cadmium SOP NO:06/03:2014.04.16 Issue No. 8.0

0.5-50 mg/kg

Mercury SOP NO:06/03:2014.04.16 Issue No. 8.0

0.04-0.8 mg/kg

Chromium SOP NO:06/03:2014.04.16 Issue No. 8.0

0.5-50 mg/kg

Nickel SOP NO:06/03:2014.04.16 Issue 0.5-50 mg/kg

Anita RaniConvenor










No. 8.0

9. Beverages [Instant Coffee and Indian Black Tea

Moisture (on dry basis) IS 3633: 2003 0.1 % to 15 %

Total Ash soluble in boiling water

IS 3633: 2003 0.1 % to 70 %

Ash insoluble in HCL IS 3633: 2003 0.1 % to 2.0 %

Caffeine content (on dry basis)

AOAC (19th Edition) 925.16IS 3309: 1992

0.1 % to 25 %

Beverages [Instant Coffee and Indian Black Tea

Solubility in cold water at 16 + 2oC

IS 3309: 1992 Qualitative

Solubility in hot water at 50 + 2oC


Extract obtained by boiling dry tea (dried at constant weight at 1000C)

IS3633: 2003 32 % to 70 %

Alakalinity of water soluble ash expressed as KOH (m/m)

IS 3633: 2003 0.10 % to 4 %

Crude Fibre (determined on tea dried to a constant weight at 100oC)

IS 10226 (Part 1): 1982 0.10 % to 20 %

Rodent Hair & excreta DGHS Manual ,Lab manual no 3, 0.1 % to 10 %

Anita RaniConvenor










2005

Insect fragmants IS 3633: 2003 0.1 % to 5 %

Total catechins IS 15344: 2003 0.10 % to 25 %

Total ash IS 3633: 2003 0.1 % to 10 %

Iron filling IS 3633: 2003 0.1 ppm to 150 ppm

Protein IS 7219: 1976 0.1 % to 30 %

Fat AOAC (19th Edition) 996.06 0.1 % to 5 %

Carbohydrate as sugar DGHS manual, Lab manual No. 4,2005

0.1 % to 10 %


Energy By calculation 0.1 Kcal to 120 Kcal

Sugars DGHS manual, Lab manual No. 4,2005

0.1 % to 10 %

Vitamin C IS 5838: 1970 (0.1 mg to 40 mg)/100 g

Polyphenol JAOAC/ISO 14502(Part 1): 2005 0.1 % to 20 %

Metal contaminants

Tin SOP NO:06/03:2014.04.16Issue no.8.0


Anita RaniConvenor










Zinc SOP NO:06/03:2014.04.16Issue no.8.0


Cadmium SOP NO:06/03:2014.04.16Issue no.8.0


Chromium SOP NO:06/03:2014.04.16Issue no.8.0


Nickel SOP NO:06/03:2014.04.16Issue no.8.0


Mercury SOP NO:06/29:2014.04.15Issue no.3.0


Copper SOP NO:06/29:2014.04.15Issue no.3.0



Lead SOP NO:06/29:2014.04.15Issue no.3.0


Arsenic SOP NO:06/29:2014.04.15Issue no.3.0


10. Non Alcholic Beverages

Caffeine IS 3309: 1992 1 mg/kg to 200 mg/kg

Benzoic acid SOP NO:06/44:2013.01.08Issue no.1.0


Anita RaniConvenor










Artificial sweeteners (Singly)

Aspartime SOP NO:06/44:2013.01.08Issue no.1.0


Acesuphamate- K SOP NO:06/44:2013.01.08Issue no.1.0


Sucrolose Jpn. J. Food Chem. Safety, Vol 19(1), 2012


Sacharine sodium DGHS Manual ,Lab Manual No. 8, 2005 (By HPLC)


Heavy metals

Lead SOP NO:06/11:2012.04.16Issue No. 7.0


Copper SOP NO:06/11:2012.04.16Issue No. 7.0


Non Alcholic Beverages

Arsenic SOP NO:06/11:2012.04.16Issue No. 7.0


Zinc SOP NO:06/11:2012.04.16Issue No. 7.0


Anita RaniConvenor










Metal Contaminants

Tin SOP No. 06/03:2014.04.16Issue No. 8.0


Cadmium SOP No. 06/03:2014.04.16Issue No. 8.0


Mercury SOP No. 06/03:2014.04.16Issue No. 8.0


Chromium SOP No. 06/03:2014.04.16Issue No. 8.0


Nickel SOP No. 06/03:2014.04.16Issue No. 8.0


11. Carbonated Beverages/ Sweetened Carbonated Beverages

Carbonated Beverages/

Caffeine SOP NO:06/01:2014.04.15SOP NO:06/44:2013.01.18Issue no.6.0


Benzoic acid SOP NO:06/44:2013.01.18Issue no.6.0


Sorbic acid SOP NO:06/44:2013.01.18Issue no.6.0


Artificial sweeteners (Single)

Anita RaniConvenor










Sweetened Carbonated Beverages

Aspartime SOP NO:06/44:2013.01.18Issue no.6.0


Acesuphamate-K SOP NO:06/44:2013.01.18Issue no.6.0


Sucrolose Jpn. J. Food Chem. Safety,Vol.19(1),2012


Sacharine sodium DGHS Manual ,Lab Manual No. 8,2005(By HPLC)


Heavy metals

Lead SOP NO:06/11:2014.04.16Issue no.7.0

0.005 mg/l to 0.5 mg/l

Copper SOP NO:06/11:2014.04.16Issue no.7.0

0.005 mg/l to 0.5 mg/l

Arsenic SOP NO:06/11:2014.04.16Issue no.7.0

0.005 mg/l to 0.5 mg/l

Zinc SOP NO:06/11:2014.04.16Issue no.7.0

0.005 mg/l to 0.5 mg/l

Cadmium SOP NO:06/11:2014.04.16Issue no.7.0

0.005 mg/l to 0.5 mg/l

Tin SOP NO:06/11:2014.04.16 0.005 mg/l to 0.5 mg/l

Anita RaniConvenor










Issue no.7.0

Carbonated Beverages/ Sweetened Carbonated Beverages

Chromium SOP NO:06/11:2014.04.16Issue no.7.0

0.005 mg/l to 0.5 mg/l

Nickel SOP NO:06/11:2014.04.16Issue no.7.0

0.005 mg/l to 0.5 mg/l

Selenium SOP NO:06/11:2014.04.16Issue no.7.0

0.005 mg/l to 0.5 mg/l

Iron SOP NO:06/11:2014.04.16Issue no.7.0

0.025 mg/l to 0.5 g/mL

Mercury SOP NO:06/11:2014.04.16Issue no.7.0


Brix AOAC (19th Edition) 44.1.04(932.14)

0.1 % to 100 %

Carbonation IS 2346: 1992 0.5 % to 15 %

Sugars IS 6287: 1985 0.10 % to 20 %

Hypercine SOP NO:06/33:2013.05.06Issue no.1.0

0.20 to 4.00 mg/l

Saffrole SOP NO:06/37:2013.05.06Issue no.1.0

1.0 mg/l to 20 mg/l

Anita RaniConvenor










Agaric acid SOP NO:06/32:2013.05.06Issue no.1.0

1 mg/l to 100 mg/l

Hydrocyanic acid AOAC (19th Edition) 920.144 Qualitative

Carbonated Beverages/ Sweetened Carbonated Beverages

Sunset yellow SOP NO: 06/43:2013.01.14Issue no. 1.0

1.0 mg/l to 100 mg/l

Ponceau 4R SOP NO: 06/43:2013.01.14Issue no. 1.0


Tartrazine SOP NO: 06/43:2013.01.14Issue no. 1.0


Acidity as citric acid DGHS manual lab manual No. 5,2005

0.1 % to 20 %

Copperoxy chloride as copper

SOP No. 06/11:2004.04.16Issue no 7.0

0.005 mg/l to 0.5 mg/l

Inorganic bromide EPA 300.1 0.5 ppm to 100 ppm

Appearance SM-PR 905 NA

Taste & flavour SM-PR-400 NA

Phosohoric ES 259: 2001 0.1 ppm to 600 ppm

12. Sweetening Agents

Anita RaniConvenor










[Honey] Specific gravity IS 4941: 1994 0.8 g/ml to 2.0 g/ml

Moisture IS 4941: 1994 0.1 % to 20 %

Total reducing Sugars IS 4941: 1994 0.1 % to 90 %

Sucrose IS 4941: 1994 0.1 % to 80 %

Fructose-glucose ratio IS 4941: 1994 0.1 % to 3.0 %

Sweetening Agents [Honey]

Ash IS 4941: 1994 0.1 % to 0.5 %

Acidity IS 4941: 1994 0.1 % to 1.0 %

Fieh's test IS 4941: 1994 Qualitative

Hydroxy methyl furfural, mg/kg

IS 4941: 1994 0.1+150 mg/kg

Metal contaminants

Lead SOP no:06/03:2014.04.16Issue No. 8.0


Copper SOP no:06/03:2014.04.16Issue No. 8.0


Arsenic SOP no:06/03:2014.04.16Issue No. 8.0


Anita RaniConvenor










Tin SOP no:06/03:2014.04.16Issue No. 8.0


Zinc SOP no:06/03:2014.04.16Issue No. 8.0


Cadmium SOP no:06/03:2014.04.16Issue No. 8.0


Mercury SOP no:06/03:2014.04.16Issue No. 8.0


Chromium SOP no:06/03:2014.04.16Issue No. 8.0


Sweetening Agents [Honey]

Nickel SOP no:06/03:2014.04.16Issue No. 8.0


13. Dehydrates Fruits And Vegetable Proudcts [Onion Seasoning Powder]

Moisture AOAC (19th Edition) 934.06 0.1 % to 10 %

Total ash IS 1797: 1985 (RA 2001) 0.1 % to 5 %

Ash insoluble in dil HCl IS 5403: 1999IS 13846: 1993

0.1 % to 2 %

Sulfur dioxide (except onion seasoning powder)

AOAC (19th Edition) 990.28 0.1 mg/kg to 300 mg/kg

Heavy Metals

Anita RaniConvenor










Lead SOP NO:06/03:2012.04.16Issue no. 8.0


Arsenic SOP NO:06/03:2012.04.16Issue no. 8.0


Metal contaminants







Dehydrates Fruits And Vegetable Proudcts [Onion Seasoning Powder]









Anita RaniConvenor










14. Sweets and Confectinery(Sugar Boiled Confectionery,Lozenges,Chewing Gum And Bubble Gum,Chocolate,Ice Lollies Or Edible Ice Jelly Candy Drops /Fox Blackurrant Tin)

Ash Sulphated(On salt free basis)

AOAC (19th Edition)900.02 0.1 % to 1 %

Ash insoluble in diluted HCl IS 6287: 1985 0.01 % to 1 %

Total Protein IS 6287: 1985 0.1 % to 20 %

Total Fat content IS 1163: 1992 0.1 % to 40 %

Moisture IS 6287: 1985 0.1 % to 10 %

Reducing sugars IS 6287: 1985 0.1 % to 40 %

Added sweetners SOP No: 06/44:2015.04.15 Issue No. 2.0


Milk fat IS 1163: 1992 IS 548 (Part 1): 1964

0.1 % to 5 %

Cocoa Solids IS 1163: 1992 0.1 % to 40 %

Milk Solids IS 1163: 1992 0.1 % to 30 %

Sweets and Confectinery(Sugar Boiled Confectionery,Lozenges,Chewing Gum And Bubble Gum,Chocolate,Ice Lollies Or

Total Sugars expressed as Sucrose

IS 6287: 1985 0.1 % to 60 %

Preservatives(Sorbic acid and its Sodium,calcium&potassium salts as sorbic acid,Benzoic acid and its Sodium,calcium & potassium

SOP NO:06/44:2013.01.18Issue no. 1.0


Anita RaniConvenor










Edible Ice Jelly Candy Drops /Fox Blackurrant Tin)

salts.

Lead SOP NO:06/03:2014.04.16Issue no. 8.0


Copper SOP NO:06/03:2014.04.16Issue no. 8.0


Arsenic SOP NO:06/03:2014.04.16Issue no. 8.0


Tin SOP NO:06/03:2014.04.16Issue no. 8.0


Zinc SOP NO:06/03:2014.04.16Issue no. 8.0


Cadmium SOP NO:06/03:2014.04.16Issue no. 8.0


Mercury SOP NO:06/03:2014.04.16Issue no. 8.0


Chromium SOP NO:06/03:2014.04.16Issue no. 8.0


Sweets and Confectinery(Sugar Boiled Confectionery,

Nickel SOP NO:06/03:2014.04.16Issue no. 8.0


Sulphur Dioxide IS 15279: 2003 0.1 mg/kg to 300 mg/kg

Anita RaniConvenor










Lozenges,Chewing Gum And Bubble Gum,Chocolate,Ice Lollies Or Edible Ice Jelly Candy Drops /Fox Blackurrant Tin)

Added colour (permitted) SOP NO:06/43:2013.01.14Issue no.1.0


15. Sweetening Agents Including Honey (Sugar, Misri, Honey, Gur or Jaggery, Golden Syrup

Freedom from foreign matter IS 4941: 1994 Clause. 5.2 Qualitative

Moisture IS 4941: 1994 0.1 % to 20 %

Ash insoluble in diluted HCl IS 4941: 1994 0.01 % to 0.5 %

Conductivity ash IS 1151: 2003 0.1 % to 1 %

Total ash IS 4941: 1994 0.1 % to 1 %

Colour IS 1151: 2003 1 to 50

Specific gravity at 27°C IS 4941: 1994 0.80 g/mL to 2.0 g/mL

Reducing sugars IS 4941: 1994 0.1 % to 50 %

Fructose-Glucose ratio IS 4941: 1994 0.1 % to 3 %

Acidity(Expressed as formic acid)

IS 4941: 1994 0.1 % to 1.0 %

Sweetening Agents Fiehe's test IS 4941: 1994 Qualitative

Anita RaniConvenor










Including Honey (Sugar, Misri, Honey, Gur or Jaggery, Golden Syrup

Hydroxy methyl furfural IS 4941: 1994 0.1 mg/kg to 180 mg/kg

Glucose IS 4941: 1994 0.1 % to 3 %

Flavour IS 4941: 1994 Clause. 5.1 Qualitative

Arsenic SOP No: 06/03:2012.04.02Issue no 8.0


Lead SOP No: 06/03:2012.04.02Issue no 8.0


Chromium SOP No: 06/03:2012.04.02Issue no. 8.0


Aspertame SOP No: 06/44:2013.1.08Issue no. 8.0


Acesulfame-K SOP No: 06/44:2013.01.18Issue no. 8.0


Metal contaminants

Copper SOP No: 06/03:2014.04.16Issue no. 8.0


Tin SOP No: 06/03:2014.04.16Issue no. 8.0


Anita RaniConvenor










Zinc SOP No: 06/03:2014.04.16Issue no. 8.0


Sweetening Agents Including Honey (Sugar,Misri, Honey, Gur or Jaggery, Golden Syrup

Cadmium SOP No: 06/03:2014.04.16Issue no. 8.0


Mercury SOP No: 06/03:2014.04.16Issue no. 8.0


Nickel SOP No: 06/03:2014.04.16Issue no. 8.0


16. Salt, Spices, Condiments and Related Products(Caraway,Cardamom,Chillies and Capsicum,Cinnamon,Cassia,Cloves,Coriander,Cumin,Fennel,Fenugrrek,Ginger,Mace,Mustard,Nutmeg,Pepper Black,Poppy,Saffron,Turmeric,Curry Powder,Mixed Masala, Aniseed, Ajowan, Dried Mango Slices,

Extraneous matter IS 1797: 1985 0.1 % to 5 %

Moisture IS 1797: 1985 0.1 % to 30 %

Total ash IS 1797: 1985 0.10 % to 15 %

Ash insoluble in diluted HCl IS 1797: 1985 0.1 % to 30 %Volatile oil content IS 1797: 1985 0.1 % to 20 %

Insect damaged matter IS 2322: 2010 0.1 % to 1 %

Empty and Malformed capsules by count

IS 1907: 1994IS 13446: 2009

0.1 % to 2 %

Immature and shrivelled capsules

IS 1907: 1994IS 13446: 2009

0.1 % to 1 %

Unripe and marked fruits IS 2322: 2010 0.1 % to 1 %

Anita RaniConvenor










Dried Mango Powder,Pepper White, Garlic, Celery,Dehydrated Onion, Asafoetida, Edible Common SaltSalt, Spices, Condiments and Related Products(Caraway,Cardamom,Chillies and Capsicum,Cinnamon,Cassia,Cloves,Coriander,Cumin,Fennel,Fenugrrek,Ginger,Mace,Mustard,Nutmeg,Pepper Black,Poppy,Saffron,Turmeric,Curry Powder,Mixed Masala, Aniseed, Ajowan, Dried Mango Slices,Dried Mango Powder,Pepper White, Garlic,

Broken fruits,seed& fragments

IS 2322: 2010 0.1 % to 1 %

Crude fiber IS 1797: 1985 1.0 % to 50 %

Split Fruits IS 13446: 2009 0.1 % to 1 %

Damaged/ Discoloured fruits IS 13446: 2009 0.1 % to 1 %

Non volatile ether extract IS 1797: 1985 0.1 % to 30 %

Defective seeds IS 13446: 2009 0.1 % to 1 %

Edible seeds other than fennel

IS 13446: 2009 0.1 % to 1 %

Cold water soluble extract IS 1797: 1985 0.1 % to 25 %

Water soluble ash IS 1797: 1985 0.10 % to 20 %

Light Berries IS 1797: 1985 0.1 % to 1 %

Pinheads or broken berries IS 1797: 1985 0.1 % to 1 %

Bulk Density IS 4333 (Part 3): 2002IS 1797:1985

0.8 % to 3 %

Total Nitrogen on dry basis IS 7219: 1973 0.1 % to 30 %

Defective Rhizomes IS 3576: 2010 Qualitative

Anita RaniConvenor










Celery,Dehydrated Onion, Asafoetida, Edible Common Salt

Test for Lead Chromate (Turmeric Powder)


Colouring powder expressed as curcuminoid content on dry basis (Turmeric Powder)

IS 3576: 2010


Total Starch IS 3576: 1994/DGHS manual,Lab Manual no.10,2005

0.1% to 70%

Salt,Spices, Condiments and Related Products(Caraway,Cardamom,Chillies and Capsicum,Cinnamon,Cassia,Cloves,Coriander,Cumin,Fennel,Fenugrrek,Ginger,Mace,Mustard,Nutmeg,Pepper Black,Poppy,Saffron,Turmeric,Curry Powder,Mixed Masala, Aniseed, Ajowan, Dried Mango

Lead SOP No: 06/03:2014.04.16 0.5 mg/kg to 50 mg/kg

Acidity as anhydrous tartaric acid

IS 13844: 2003 0.1 % to 5 %

Sodium Chloride content IS 7874 (Part 2): 1975 0.1 % to 15 %

Metal contaminants

Copper SOP No.:06/03:2014.04.16Issue No. 8.0


Arsenic SOP No.:06/03:2014.04.16Issue No. 8.0


Tin SOP No.:06/03:2014.04.16Issue No. 8.0


Zinc SOP No.:06/03:2014.04.16 0.5 mg/kg to 50 mg/kg

Anita RaniConvenor










Slices,Dried Mango Powder, Pepper White, Garlic, Celery, Dehydrated Onion, Asafoetida, Edible Common Salt

Issue No. 8.0

Cadmium SOP No.:06/03:2014.04.16Issue No. 8.0


Mercury SOP No.:06/03:2014.04.16Issue No. 8.0


Chromium SOP No.:06/03:2014.04.16Issue No. 8.0


Nickel SOP No.:06/03:2014.04.16Issue No. 8.0


17. Biscuits & Bread Moisture IS 1011:2002/IS 12711: 1989

0.1 % to 10 %

Acid insoluble ash IS 1011:2002/IS 12711: 1989

0.1 % to 1.0 %

Acidity of extracted fat(as oleic acid), percent by mass, Max

IS 1011:2002/IS 12711: 1989

0.1 % to 5 %

Alcoholic acidity IS 12711: 1989 0.1 % to 1.5 %

Free / Total gossepol SOP NO:06/45: 2014.11.25 Issue No. 1.0


Anita RaniConvenor










Metal contaminants

Lead SOP No: 06/03:2014.04.16Issue no.8.0


Copper SOP No: 06/03:2014.04.16Issue no.8.0


Arsenic SOP No: 06/03:2014.04.16Issue no.8.0


Tin SOP No: 06/03:2014.04.16Issue no.8.0


Zinc SOP No: 06/03:2014.04.16Issue no.8.0


Cadmium SOP No: 06/03:2014.04.16Issue no.8.0


Biscuits & Bread Mercury SOP No: 06/03:2014.04.16Issue no.8.0


Chromium SOP No: 06/03:2014.04.16Issue no.8.0


Nickel SOP No: 06/03:2014.04.16Issue no.8.0


18. Nutritional Value for Processed Food

Moisture IS 1011: 2002925.09,926.07,926.08,950.46

0.1 % to 10 %

Anita RaniConvenor










Acid insoluble ash in biscuit IS 1011: 2002 0.1 % to 10 %

Acidity of extracted fat(as oleic acid),percent by mass,max,in biscuit

IS 1011: 2002 0.1 % to 5 %

Total ash AOAC (19th Edition) 945.45 0.10 % to 15 %

Protein IS 7219: 1973 0.1 % to 40 %

Fat

Milk powder IS 11721: 2013 0.1 % to 30 %

Meat products AOAC (19th Edition) 976.21 0.1 % to 30 %

Biscuit IS 1011: 2002 0.1 % to 25 %

Chocolates IS 1163: 1992 0.1 % to 40 %

Fish products AOAC(19th Edition) 948.16 0.1 % to 25 %

Nutritional Value for Processed Food

Flour AOAC(19th Edition) 9420.85 0.1 % to 5 %

Cheese AOAC(19th Edition) 920.152 0.1 % to 20 %

Macronic food AOAC(19th Edition) 925.12 0.1 % to 10 %

Bread AOAC(19th Edition) 935.38 0.1 % to 2 %

Anita RaniConvenor










Ice-cream AOAC(19th Edition) 952.06 0.1 % to 15 %

Carbohydrate By calculation 1 % to 99 %

Energy By calculation 1 Kcal to 500 Kcal

Calories from fat AOAC(19th Edition) 983.23 0.1 % to 3 %

Crude fiber AOAC(19th Edition) 962.09 0.1 % to 17 %

Sugars IS 5982: 2003/DGHS manual; lab manual no. 4: 2005

0.1 % to 100 %

Sucrose IS 5982: 2003 0.1 % to 100 %

Fatty acid profile Sop No. 06/04: 2014.02.15,Issue No. 7

0.1 % to 100 %

Dietary fiber AOAC(19th Edition) 2001.03 0.1 % to 45 %

Sugar profile(glucose, fructose, sucrose)

AOAC(19th Edition) 977.20 0.01 % to 98 %

Amino acid profile JAOCS((2010)87: 127-132,DO1 10.1007/s 11746-009-1484-2)

0.1 % to 50 %


Fat soluble vitamins (A,D3,E)

SOP No:06/27, 2014.02.25, Issue No.4.0

1 ppm to 100 ppm

Anita RaniConvenor










Sulphated ash DGHS manual, lab manual No. 4: 2005

0.1 % to 2 %

Metal contaminants

Lead SOP No:06/03: 2014.04.16Issue No. 8.0


Copper SOP No:06/03: 2014.04.16Issue No. 8.0


Arsenic SOP No:06/03: 2014.04.16Issue No. 8.0


Tin SOP No:06/03: 2014.04.16Issue No. 8.0


Zinc SOP No:06/03: 2014.04.16Issue No. 8.0


Cadmium SOP No:06/03: 2014.04.16Issue No. 8.0


Mercury SOP No:06/03: 2014.04.16Issue No. 8.0


Chromium SOP No:06/03: 2014.04.16Issue No. 8.0


Anita RaniConvenor











Nickel SOP No:06/03: 2014.04.16Issue No. 8.0


19. Ayurvedic / Herbal Products

Metal contaminants

Lead SOP No:06/30: 2014.04.15Issue No. 3.0


Copper SOP No:06/30: 2014.04.15Issue No. 3.0


Arsenic SOP No:06/30: 2014.04.15Issue No. 3.0


Tin SOP No:06/30: 2014.04.15Issue No. 3.0


Zinc SOP No:06/30: 2014.04.15Issue No. 3.0


Cadmium SOP No:06/30: 2014.04.15Issue No. 3.0


Mercury SOP No:06/30: 2014.04.15Issue No. 3.0


Chromium SOP No:06/30: 2014.04.15Issue No. 3.0


Anita RaniConvenor










Nickel SOP No:06/30: 2014.04.15Issue No. 3.0


20. Dairy Products Moisture IS:16072: 2012 0.01 % to 5.0 %

A)Total fat IS:12758:2005IS:3509: 1966IS: 11762:2013

0.01 % to 50 %

Milk solids not fat AOAC 19th edition , 990.21 1 % to 20 %

Milk fat IS:1163:1992 0.01 % to 10 %

Ash insoluble in Dil HCl,% W

IS 14433:2007 0.01 % to 10 %

Milk protein IS:1656:2007 0.01 % to 50 %

Total ash IS1656:2007 0.01 % to 10 %

Solubility IS:12759:1989IS14433:2007, IS:15757:2007

0.1 % to 98 %

Solubility Index IS:12759:1989IS:1656:2007IS 14433:2007, IS:15757:2007

0.1 ml to 4 ml

Vitamin-A SOP No. 06/27:2014.02.15 Issue No.4.0

0.1 to 10000 IU/100gm

Anita RaniConvenor










Cholecalciferol SOP No. 06/27:2014.02.15 Issue No.4.0


Vitamin-C IS:5838:1970IS:1656:2007IS 14433:2007, IS:15757:2007


Dairy Products Thiamine SOP No. 06/38:2014: 2014.11.25 Issue No.:1.0


Riboflavin SOP No. 06/38:2014: 2014.11.25 Issue No.:1.0


Niacin SOP No. 06/38:2014: 2014.11.25 Issue No.:1.0


Pyridoxin SOP No. 06/38:2014: 2014.11.25 Issue No.:1.0


Folic acid SOP No. 06/38:2014: 2014.11.25 Issue No.:1.0


Pantothenic acid SOP No. 06/38: 2014.11.25 Issue No.:1.0


Sodium SOP No. 06/39:2015.04.15 Issue No. 2.0


Anita RaniConvenor










Potassium SOP No. 06/39:2015.04.15 Issue No. 2.0


Chloride IS 11763:2005 0.1 mg/kg to 1000 mg/kg

Phosphorus AOAC, 19th ed., 995.11 0.05 mg/kg to 100 mg/kg

Lead SOP NO:06/08:2014.04.16 Issue No. 3.0




Dairy Products Tin SOP NO:06/08:2014.04.16 Issue No. 3.0








Nickel SOP NO:06/08:2014.04.16 Issue No. 3.0


Magnesium SOP NO:06/08:2014.04.16 Issue No. 3.0


Anita RaniConvenor










Iron SOP NO:06/08:2014.04.16 Issue No. 3.0


Iodine SOP NO:06/08:2014.04.16Issue No. 3.0






Manganese SOP NO:06/08:2014.04.16 Issue No. 3.0


Dairy Products Selenium SOP NO:06/08:2014.04.16 Issue No. 3.0


Crude fibre IS 10226 (Part 1): 1982 0.1 % to 20 %

Titrable acidity IS 1165:2002IS 11766:1986

0.1 % to 10 %

Sugar(Sucrose) IS 1166:1986 0.1 % to 50 %

pH IS 14328:1995 1 to 14

Lactose content IS 1479 (Part 2):1961 1 % to 50 %

Anita RaniConvenor










21. Fats, Oils and Fat Emulsions

Butro-refractive meter reading or Refractive Index at 40°c

IS 548 (Part 1 & Part 2): 1964 (RA 1976)

1.33298 to 1.56999

Iodine value IS 548 (Part 1 & Part 2): 1964 (RA 1976)

10 to 150

Saponification value IS 548 (Part 1): 1964 100 to 300

Un saponifacation matter IS 548 (Part 1): 1964 0.01 % to 1.5 %

Acid Value IS 548 (Part 1): 1964 0.01 to 10

Flash Point-Polensky Marten closed cup mehod

IS 1448 (Part 20): 1988 50 °C to 400 °C

Peroxide value IS 548 (Part 2): 1976 0.1 to 10Meq O2/Kg

BTT Test IS 548 (Part 2): 1976 37 °C to 50 °C

Toal Fatty Acid SOP No.:06/04; 2014.02.15, Issue No.:7.0

0.1 % to 100 %

Fats, Oils and Fat Emulsions

Moisture & Volatile Matter IS:548(part-1:1964) 0.01 % to 10 %

Free fatty acid IS:548(part-1:1964) 0.01 % to 10 %

Linolenic acid SOP NO:06/04:2014.02.15 Issue No. 7.0

1 % to 70 %

Residual Nickel SOP NO:06/03:2014.04.16 Issue No. 8.0


Anita RaniConvenor










Lead SOP NO:06/03:2014.04.16Issue No. 8.0
















Fats, Oils and Fat Emulsions

Colour in a 5 1/4- in cell on the lovibond Scale

IS 548 (Part 1): 1964 Cl. 13 5 to 50

Hexane IS 4277 :2014 Annex B 10-1500 mg/kg

Anita RaniConvenor










Aflatoxins IS 4277:2014 Annex A Quantitative test by ELISA

Phosphorous IS 4276 :2014 Annex C 0.05 mg/kg to 100mg/kg

Insoluble Bromide (poly bromide) Test

IS 4276 :2014 Annex D Qualitative Test

Specific gravity at 30/30 °C IS 548 (Part 1): 1964 Cl. 11 0.1 mg/L to 1 mg/L

Oryzanol content Annex C of IS 3448 :2014 1 % to 2 %

Admixure of other oils IS 548 (Part 2): 1976 Cl. 9, 10, 11, 14, 15 & 16

Qualitative Test

Natural essential oil (as allylisothicyanate)

IS 548 (Part 1): 1964 Cl. 17 0.1 % to 0.60 %

Cloud Point, °C IS 1448: 2012 Cl. 10 0.1 °C to 10 °C

22. Sugar Color ICUMSA GS 2/3-9-1994, ICUMSA 2-10-1998

0.1 to 100 ICUMSA

Extraneous Matter IS 5982: 2003 0.1 % to 1 %

Sulphur dioxide content IS 15279: 2003 1 mg/kg to 200 mg/kg

Colouring matter IS 15279: 2003 1 % to 100 %

Moisture IS 15279: 2003 0.01 % to 10 %Sugar Conductivity of Ash IS 15279: 2003 0.1 moh/cm2 to 1 moh/cm2

Anita RaniConvenor










Total Sugars as Sucrose IS 15279: 2003 0.10 % to 90 %

Metal contaminants Lead SOP NO:06/03:2014.04.16

Issue No. 8.00.5 mg/kg to 50 mg/kg

















Anita RaniConvenor










23. All Fish and fish Products

Ash insolule in dil Hcl (on dry basis)

IS 14950 : 2001 0.1 % to 1 %

All Fish and fish Products

Acidity of extracated fat (as oleic acid)

Annex B, IS 1011: 2002 0.1 % to 10 %

Mercury AOAC 19th Edn 2005; Chapter-09, 9.02.23; 977.15/AOAC 19th Edn 977.15


Cadium AOAC 19th Edn 2005; Chapter-09, 9.01.09; 999.11


Metal ContaminantsLead SOP NO:06/03:2014.04.16

Issue No. 8.00.5 mg/kg to 50 mg/kg









Chromium SOP NO:06/03:2014.04.16 0.5 mg/kg to 50 mg/kg

Anita RaniConvenor










Issue No. 8.0



23. Residues in Food Products

a. Eggproducts/ Poultry/ Meat/ Marine Products/Honey & Milk

Antibiotic residues& MiscellaneousNitrofurans: Furazolidone, Furaltadone, Nitrofurantoine &Nitrofurazone,Furylfuramide,Nifuratel,Nifuroxime,Nifurprazine

SOP No. 15/30G 2014.06.06 Issue No. 5.0Based on Journal of Chromatography B, 691, 1999, 87-94

1.0 µg/kg to 200.0 µg/kg(each residue)

Metabolite of Nitro furans

AOZ (Metabolite of Furazolidone)

SOP No. 15/30G 2014.06.06 Issue No. 5.0Based on Journal of Chromatography B, 691, 1999, 87-94


AMOZ (Metabolite of Furaltadone)AHD (Metabolite of Nitrofurantoine)

Anita RaniConvenor










SEM (Metabolite of Nitrofurazone)

Eggproducts/ Poultry/ Meat/ Marine Products/Honey & Milk

SulfonamidesSulfadiazine,Sulfathiazole,Sulfamerazine,Sulfamethiazole,Sulfadimidine/Sulfamethazine,Sulfachloropyridazine,Sulfamethoxazole, Sulfadimethoxine,Sulfadoxine,Sulfamethoxypyridazine,Sulfaguanidine,Sulfanilamide,Sulfaacetamide,Sulfisoxazole,Sulfaquinoxaline,Trimethoprim, Sulfobromomethazine, Sulfaethoxypyridazine, Sulfapyrazine, Sulfadinethoxine, Sulfaethoxazole, Sulphadiazine

SOP No. 15/30B SOP No. 15/30G 2014.06.05 Issue No. 5.0 Based on J. Chrom. B, 774, 2002, 39-52


Tetracyclines: Tetracycline,Oxy-tetracycline,

SOP No. 15/30C 2014.05.28 Issue No. 4.0Based on J. Agr. Food Chem., 48,

5.0 µg/kg to 200.0 µg/kg(For each individual residue)

Anita RaniConvenor










Chloro-tetracycline,Doxy cyclin,4 –Epi-tetracycline,4-Epi-Oxytetracycline,4-Epi-chlorotetracycline

2000,6

Chloramphenicol SOP No. 15/30F 2014.05.24 Issue No. 4.0Based on USFDA Lab Inf Bull. 4303, Vol. 19(4), 2003

0.1 µg/kg to 5 µg/kg

Malachite and Leuco Malachite Green (For marine products only)

Method Validation No: VLS-TAL/ML-LMG-R/001 Based on USFDA ORA LIB no. 4363

0.2 µg/kg to 20.0 µg/kg


Fluoroquinolones Ciprofloxacin, Enrofloxacin,Sarafloxacin, Difloxacin,Flumequin,Nalidixic acid,Oxolinic acid,Norfloxacin, Piromidic acid, Pipemidic acid, Rosoxacin, Enoxacin, Lomefloxacin, Nadifloxacin,

Method Validation No: VLS-TAL/FLQ-R/01

10 µg/kg to 100 µg/kg (For each residue)

Anita RaniConvenor










Ofloxacin, Pefloxacin, Rufloxacin, Balofloxacin, Gatifloxacin, Grepafloxacin,Levofloxacin,Monifloxacin,Pazufloxacin,Sparfloxacin,Temafloxacin,Tosufloxacin,Besifloxacin,Clinafloxacin, Gemifloxacin, Trovafloxacin, Prulifloxacin,


Glycopeptides : Vancomycin, Teicoplanin,Telavancin,Bleomycin, Ramoplanin,Decaplanin

Method Validation No: VLS-TAL/GLY-R/01

0.01 mg/kg to 0.2 mg/kg(For each residue)

OthersStreptomycinSpectinomycin,

SOP No.15/30D: 2014.09.20 Issue No.4.0Based on J. Mark E. P. Hows.,

10.0 µg/kg to 500 µg/kg(For each residue)

Anita RaniConvenor










Josamycin,Lincomycin, Colistin,Neomycin, ,

Veterinary Lab Agency, UK

Nitroimidazoles: Nitroimidazole,Dimetridazole, Metronidazole, Benzimidazole,Probenzimidazole,Flubendazole, Amprolium,Ronidazole, Ipronidazoles, Clenbuterol, Diethyl Istibestrol

Method Validation No: VLS-TAL/NIM-R/001

10.0 µg/kg to 200 µg/kg(For each individual residue)

Egg products/Poultry/ Meat/ Marine Products/Honey

Macrolides : Tylosin, Erithromycin,Azithromycin, Clarithromycin, Dirithromycin, Roxithromycin,

SOP No.15/30D 2014.09.20 Issue No.4.0Method Validation No: VLS-TAL/MCL-R/001

10.0 µg/kg to 500 µg/kg(For each individual residue)


Steroids: Trenbolone, 19-Nortestosterone, Testosterone, Estradiol 17-Beta

Method Validation No: VLS-TAL/STE-R/001

1.0 µg/kg to 200.0 µg/kg(For each residue)

Anita RaniConvenor










Egg products/Poultry/ Meat/ Marine Products/

alpha -BHC, b-BHC, Lindane, d-BHC, Heptachlor, Aldrin, Hepta-chlorepoxide, Endosulphan I, 2,4-DDE,4,4-DDE, Dieldrin, Endrin, EndosulfanII, 2,4-DDD,4,4-DDD, Endrin aldehyde, Endosulphan sulphate, 2,4-DDT,4,4-DDT, Methoxychlor, chlorthalanil, Dicofol, Endrin Ketone ,Sulfotep,Chlorpyriphos,Disulfoton,Famphur, Thionazin, Phorate, Parathion Ethyl, Parathion Methyl,

SOP No.15/04 & 15/05;Based on AOAC (19th Edition), Based on DGHS-Manual of methods of PR analysis of Food Commodities

0.001 mg/kg to 0.2 mg/kg(For each individual residue

Anita RaniConvenor










Honey OOO- Trimethyl Phosphorothionate, Dimethoate, Quinalphos Permethrin,Deltamethrin,Cypermethrin,Cyfluthrin,Fenvalerate,Fluvalinate,Cyhalothrin,Boscalid,Lasalocid,Cyromazine,Vinclozoline,Chlorobenzilate,Hexachlorbenzene,Coumaphos,Malathion,Phosalone,Carbofuran,Propoxur,Carbaryl,Cymiazol,Amitraz,Bromopropylate,Chinomethionate.Fenitrothion,chlorfenvinphos,2,4-D,Ethion,

Anita RaniConvenor











Monocrotophos,Trichlorfen,Carbendazim,Benomyl,3-Hydroxy carbofuran,Edifenphos, Fenthion and its oxygen sulfone & suloxides, Pirimphos methyl, Phoarate Sulfone, Phoarate Sulfoxide

PCBsMono-chlorobiphenyl, Dichlorobiphenyl, Trichlorobiphenyl, Tetrachloro-biphenyl, Penta-chlorobiphenyl, Hexa-chlorobiphenyl,Hepta-chlorobiphenyl andOctachlorobiphenyl

SOP No.15/05 Based on AOAC 19th Edition DGHS-manual of methods of PR analysis of Food commodities

0.001 mg/kg to 0.2 mg/kg(For each individual residue)

Dioxins like PCBs- HRGC/HRMS3,3’-4,4’-tetrachlorobiphenyl (PCB 77), 3,4,4’,5-tetrachlorobiphenyl (PCB 81), 2,3,3’,4,4’-pentachlorobiphenyl

EPA 1668 (Rev.B) (2008)VLS-TAL/dl-PCB-R/001

0.06 ng/kg to 100 ng/kg(For each individual residue)

Anita RaniConvenor











(PCB 105), 2,3,4,4’,5-pentachlorobiphenyl (PCB 114), 2,3’,4,4’,5-pentachlorobiphenyl (PCB 118), 2’,3,4,4,5’-pentachlorobiphenyl (PCB 123), 3,3’,4,4’,5-pentachlorobiphenyl (PCB 126), 2,3,3’,4,4’,5-hexachlorobiphenyl (PCB 156), 2,3,3’,4,4’,5’-hexachlorobiphenyl (PCB 157), 2,3’,4,4’,5, 5’-hexachlorobiphenyl (PCB 167) 3,3’,4,4’,5,5’-hexachlorobiphenyl (PCB 169),2,2’,3,3’,4,4’,5-heptachlorobiphenyl (PCB 170), 2,2’,3,4,4’,5,5’-heptachlorobiphenyl (PCB 180),

Anita RaniConvenor










2,3,3’,4,4’,5,5’-heptachlorobiphenyl (PCB 189)Dioxins & Furans : Polychlorinated dibenzodioxin and polychlorinated dibenzodifuran (PCDD/P CDF)

EPA 1613 Rev.B (Oct 1998)VLS-TAL/Dx-R/001

0.03 ng/kg to 6.25 ng/kg

b. Alcoholic Drinks, & Fruit Beverages,Soft Drinks

Polychlorinated biphenyl (PCBs) Mono-chlorobiphenyl, Dichlorobiphenyl, Trichlorobiphenyl, tetrachloro-biphenyl, penta-chlorobiphenyl, Hexa-chlorobiphenyl, Hepta-chlorobiphenyl and octachlorobiphenyl

Method Validation No: VLS-TAL/PCB/Fruit Juices-R/001 Based on PAM, USFDA APHA 6431 / IS 13428: 2005 Based on AOAC Method (19th edition)

0.01 mg/l to 0.2 mg/l(For each residue)

Alpha-HCH,Beta-HCH, Lindane,Delta-HCH,2,4-DDE,4,4-DDE,2,4-DDD,4,4-DDD,2,4-DDT,4,4-DDT,

Method Validation No: VLS-TAL/PRSD-R/001 Based on AOAC Method No.2007.09

0.5 µg/l to 5.0 µg/l(For each individual residue)

Anita RaniConvenor










Alcoholic Drinks, & Fruit Beverages,Soft Drinks

Aldrin,Dieldrin,Alpha-endosulfan,Beta endosulfan,Endosulfan sulfate,Malathion,Malaoxon,Chlorpyrifos,Ethion,Methylparathion,Monocrotophos,Ethephon, Chloral hydrate, Dieldrin, Chlordane,Dichlorovos, Dicofol, Dimethoate,

Fenitrothion,Parathion,Paroxon,Methylparaxon,Phosphamidon,Pyrethrins,Chlorobenzilate,2,4-D,Formothion,monocrotophos,Paraquat dichloride,Phosalone,

Method Validation No: VLS-TAL/PRSD-R/001 Based on AOAC Method No.2007.09

0.01 to 0.2 mg/l(For each individual residue)

Anita RaniConvenor










Trichlorfon,Thiometon,carbendizim,Benomyl,Captan,Carbofuran,Dithiocarabamates,Phoarate(its sulfone, sulfoxide), Ethphon,Tridemorph


Aflatoxins Based on AOAC Method Chap 49.2.17

0.1 µg/l to 20.0 µg/l

Methyl mercury as Hg SOP No. 15/62: 0.05 mg/l to 2.5 mg/l

PCBs- HRGC/HRMS3,3’-4,4’-tetrachlorobiphenyl (PCB 77), 3,4,4’,5-tetrachlorobiphenyl (PCB 81), 2,3,3’,4,4’-pentachlorobiphenyl (PCB 105),

EPA 1668 Rev.B (2008) 0.2 mg/l to 5.0 mg/l(For each individual residue)

Anita RaniConvenor











2,3,4,4’,5-pentachlorobiphenyl (PCB 114), 2,3’,4,4’,5-pentachlorobiphenyl (PCB 118), 2’,3,4,4,5’-pentachlorobiphenyl (PCB 123), 3,3’,4,4’,5-pentachlorobiphenyl (PCB 126), 2,3,3’,4,4’,5-hexachlorobiphenyl (PCB 156), 2,3,3’,4,4’,5’-hexachlorobiphenyl (PCB 157), 2,3’,4,4’,5, 5’-hexachlorobiphenyl (PCB 167), 3,3’,4,4’,5,5’-hexachlorobiphenyl (PCB 169), 2,2’,3,3’,4,4’,5-heptachlorobiphenyl (PCB 170), 2,2’,3,4,4’,5,5’-heptachlorobiphenyl (PCB 180),

Anita RaniConvenor










2,3,3’,4,4’,5,5’-heptachlorobiphenyl (PCB 189) Polychlorinated dibenzodioxin and polychlorinated dibenzodifuran (PCDD/PCDF)

EPA 1613 Rev. B (1994) 0.06 mg/l to 10 mg/l

c. Food and Agricultural Products (Processed and Raw) Fruit, Vegetables & Fruit JuicesIncluding Grapes

Food and Agricultural Products (Processed and Raw) Fruit,

Polychlorinated dibenzodioxin and polychlorinated dibenzodifuran (PCDD/PCDF)

EPA 1613 Rev. B (1994) 0.01 µg/kg to 5.0 µg/kg

Mevinphos, Omethoate, Monocrotophos,Dimethoate,Methylparathion,Heptachlor, Fenitrothion,Diazinon, Malathion,Fenthion, Chlorpyrifos,Pyrithion, Methidathion,Fenamiphos,Heptachlor epoxide, Endosulfan-I,

SOP 15/25-D 2014.05.17 Issue No. 6.0 Based on DGHS-Manual of methods of PR analysis of Food Commodities, AOAC method (19th

Edition )Standard operating procedure for the analysis of agrochemical residue(annexure 9 of the residue monitoring plan of APEDA)grapesMethod Validation No: VLS-TAL/PR/GRP/001


Anita RaniConvenor










Vegetables & Fruit JuicesIncluding Grapes

Endosulfan Sulfate, Dieldrin, Endosulfan-II, p,p’-DDT, Dicofol,Bifenthrin, Lambda cyhalothrin, Permethrin,Cyfluthrin, Cypermethrin,Fenvalerate,Deltamethrin,2-phenyl phenol, Acrinathrin,Aldicarb (incl., Aldicarb sulfoxide, Aldoxycarb),Amitraz,Abamectin,Azinphos-methyl,Benalaxyl, Bifenthrin,Boscalid,Bromacil, Bromophos, Bromopropylate,Bromuconazol,Buprimat,Chlorobenzilat, Dichlorvos, Dimethoate (incl., Omethoate)

Food and Organochlorine SOP 15/25-D 2014.05.17 0.005 mg/kg to 0.2 mg/kg

Anita RaniConvenor










Agricultural Products (Processed and Raw) Fruit, Vegetables & Fruit JuicesIncluding Grapes

Compounds:Aldrin, Chlordane (cis & trans), Chlorothalonil, DDT (all isomers), Endrin, HCH isomers,4-bromo-2-chlorophenol, Dicofol, Lindane, Dialdrin, Endosulfan (all isomers)

Issue No. 6.0 Based on DGHS-Manual of methods of PR analysis of Food Commodities, AOAC method (19th


(For each individual residue)

OrganoPhosphorus Compounds:4-bromo-2-chlorophenol (metabolite of Profenophos), Acephate, Chlorfenvinphos, Edifenphos, Ethion, Etrimfos, Fenitrothion Fenthion (fenthion and its oxygen analogue, their sulfoxides and sulfone expressed as parent),



0.01 mg/kg to 0.2 mg/kg (For each individual residue)

Anita RaniConvenor










Food and Agricultural Products (Processed and Raw) Fruit, Vegetables & Fruit JuicesIncluding Grapes

Glufosinate-ammonium (sum of glufosinate, its salts, MPP and NAG expressed as glufosinate equivalents) Glyphosate (and the metabolite aminomethylphosphonic acid), Iprobenphos, Chlorpyrifos, Chlorpyrifos methyl Diazinon,Methaimidaphos, Acephate

Malathion (sum of malathion and malaxon, expressed as malathion), Methamidophos, Monocrotophos, Omerthoate (refer to Dimethoate), Oxydemeton – methyl (sum of oxydemeton methyl and demeton – S- methylsulfone expressed as oxydemeton methyl), parathion methyl (sum of parathion methyl and Paraxon methyl expressed as Parathion methyl), Phenthoate, Phorate (sum of Phorate, its oxygen analogue



Anita RaniConvenor










and their sulfones expressed as phorate), Phosalone, Phosphamidon, Pirimiphos-methyl, Profenophos, Propetamphos, Quinalphos, Temephos, Thiometon , Triazophos.


Others:Fenoxycarb,Fenpropathrin,Fenpropimorph, Fenthion (incl. -sulfoxide, -oxon, -oxon-sulfoxide, -oxon-sulfone), Fluazifop, Fluazinam, Flucythrinate




Fludioxonil, Fluquinconazol, Formothion, Heptenophos, Hexythiazox, Imazalil, Iprovalicarb, Kresoxim-methyl, Lufenuron, Mecarbam, Mepanipyrim, Mepronil,


Edition )Standard operating procedure for the analysis of agrochemical residue(annexure 9 of the residue monitoring plan of APEDA)grapesMethod Validation No: VLS-

0.01 to 0.2 mg/kg(For each Residue)

Anita RaniConvenor











Metazachlor, Methidation, Methiocarb (incl. -sulfoxid, -sulfon), Methoxychlor, Methoxyfenozid,Metribuzin, Mevinphos, Nuarimol, Oxadixyl,Oxamyl,Pendimethalin, Pentachloranisol, Phenthoat, Phosmet, Piperonylbutoxide, Pirimicarb (incl. Desmethly-),Pirimiphos-ethyl, Pirimiphos-methyl, Prochloraz, Procymidon, Profluralin, Propamocarb, Propoxur,Propyzamid, Prothiofos, Pymetrozin, Pyraclostrobin, Pyrazophos, Pyridaben, Pyridaphenthion, Pyrifenox, Chlorpropham,

TAL/PR/GRP/001

Anita RaniConvenor











Chlorthal-dimethyl,Chlozolinat,Clofentezin,Cyproconazol,Cyprodinil,Curomazin,Chlorfenvinphos, Ethoprophos

Pyrimethanil, Pyriproxyfen, Quinoxyfen, Quintozen, Rotenon, Spirodiclofen, Spiromesifen, Spiroxamine, Tau-Fluvalinate, Tebufenozide, Tebufenpyrad, Tecnazene, TeflubenzuronTefluthrin, Terbuthylazin, Tetraconazol, Tetradifon, Thiabendazole, Tolclofos-methyl, Tolylfluanid, Trichlorfon, Trifloxystrobin, Triflumizole, Trifluralin, Triforine,




Anita RaniConvenor











Tridemorph, VinclozolinMalaoxon, Demeton-S-methyl (incl., Oxydemeton-methyl,Demeton-S-methyl-sulfon),Dichlobenil, Dichlofenthion,Dichlofluanid,Dichloran,Diethofencarb,Diflubenzuran,Diniconazol,Diphenyl amine, Disulfoton, (incl., sulfoxide, sulfone), Ditalimfos, Chlorpyrifos- Methyl, Dichlorvos,Epoxyconazole,Epoxyquin,Ethoxyquin,Etridiazol,Famoxadone,Fenamidone, Fenazaquin, Fenbuconazole, Fenhexamid

Fruit, Vegetables & Fruit Juices

Allethrin, Bioallethrin,

SOP 15/25-D 2014.05.17 Issue No. 6.0

0.01 mg/kg to 0.2 mg/kg (For each individual

Anita RaniConvenor










Including Grapes

Fruit, Vegetables & Fruit JuicesIncluding Grapes

Ethofenprox, Trans-fluthrin, Atrazine, Flufenzina, Simazine, Metalaxyl, Metalaxyl-M, Benalaxyl-M, Oxycarboxin, Propanil, Bendiocarb, Benfuracarb, Benomyl, Carbaryl, Carbofuran, Carbosulfan, Dazomet, Fenobucarb, Indoxacarb, Methomyl, Thiodicarb, Thiobencarb, Fenarimol, Bitertanol, Difenoconazole, Flusilazole, HexaconazoleMyclobutanil, Paclobutrazol, Penconazole, Propiconazole, Tebuconazole, Triadimefon,

Based on DGHS-Manual of methods of PR analysis of Food Commodities, AOAC method (19th


residue)

Anita RaniConvenor










Iprodione, Captafol, Captan, Carbendazim, Thiophanate-methyl, Dithiocarbamates, Acetamiprid, Clothianidin, Imidacloprid, Thiamethoxim, Dinocap, Cymoxanil, Dimethomorph, Diafenthiuron, Diuron, Iodosulfuron-methyl, Isoproturon, Linuron, Pencycuron, Flufenoxuron


Azoxystrobin,Fenpyroxymate, Oxyfluorofen,

SOP 15/25-D 2014.05.17 Issue No. 6.0 Based on DGHS-Manual of


Anita RaniConvenor










Alachlor, Butachlor, Carboxin, Flufenacet, Metalochlor, Novaluron, 1-Napthylacetic acid, 6-Benzyl adenine, Azadiractin, Bifenazate, Buprofezin, Cartap hydrochloride, Chlormequat chloride, Homobrassilide, Diquat, Dithianon, Dodine, Emamectin benzoate, Ethephon, Flubendiamide, Forchlorfenuron, Fosetyl-Al, Gibberillic acid, Iso prothioalane, Mandipropamide, Mepiquat chloride, Milbemectin, Oxadiazon, Paraquat, Propargite, Spinosad, Tricyclazole,

methods of PR analysis of Food Commodities, AOAC method (19th


Anita RaniConvenor











Uracil, Dithion, Propineb, Pyrethrins, Chlorobenzilate, Dichlorotrichlorfon, Ethylene, bis-Dithiocarbamates, 2,4-D

Fipronil SOP 15/25-D 2014.05.17 Issue No. 6.0 Based on DGHS-Manual of methods of PR analysis of Food Commodities, AOAC method (19th

Edition )Standard operating procedure for the analysis of agrochemical residue(annexure 9 of the residue monitoring plan of APEDA) grapes Method Validation No: VLS-TAL/PR/GRP/001


d. Tobacco Organochlorine Pesticides: Alpha-BHC, Beta-BHC, Delta -BHC, chlordane, Heptachlor, Aldrin,

OP No.15/19A, 2014.12.20 Issue No. 4.0 & SOP No.15/19B, 2014.12.20, Issue No. 4.0

Based on AOAC 19th Ed.:2012, Based On Pesticide Analytical Manual;


Anita RaniConvenor










Tobacco

p,p" -DDE, Dieldrin, p,p-DDD, Endosulphan sulphate, p,p’-DDT, Dicofol, Ethion, captafol, phosalone, chloropyrifos, Endosulfan I, Endosulfan II Lindane(gamma-BHC), endosulfan sulphate, o,p-DDE, o,p-DDT, o,p-DDD, Chlordane, Aldicarb,Aldicarb Sulfone, Aldicarb Sulfoxide.

Synthetic pyrethroidsLambda cyhalothrin, cyfluthrin, cypermethrin, Deltamethrin, Fenvalerate, Permethrin, Alphamethrin,

SOP No.15/19 A, 2014.12.20 Issue No. 4.0 & SOP No.15/19B, 2014.12.20, Issue No. 4.0Based On Pesticide Analytical Manual;


Anita RaniConvenor










Tobacco

Organo Phophorous Pesticides: fenpropathrin. Acephate, Diazinon, Dichlorvos, Dimethoate, fenitrothion, malathion, monocrotophos, parathion-ethyl, parathion-methyl, phosphamidon, Atrazine, metalaxyl, carbofuran, carbaryl, thiram, fenthion Fosetyl aluminium, Baygon, Simazine and Aldicarb, 2,4-D

SOP No.15/19 A, 2014.12.20 Issue No. 4.0 & SOP No.15/19B, 2014.12.20, Issue No. 4.0Based on AOAC 19th Ed.,:2012Based On Pesticide Analytical Manual;


e. Food Grains, Dry Products and Soil

Organochlorine pesticidesalpha-BHC, Beta-BHC, Delta-BHC(HCHs) chlordane,

SOP No.15/02 A, 2015.04.08 Issue No.:4.0 & SOP No.15/02 B 2015.04.08 Issue No.:4.0 Based on DGHS:2005-Manual of methods of


Anita RaniConvenor










Food Grains, Dry Products and Soil

Heptachlor, Aldrin, p,p'-DDE, Dieldrin, p,p'-DDT p,p'-DDD, Endosulphan sulphate, Endosulfan I, Endosulfan II, Lindane(Gamma-BHC),Endosulfan sulphate, o,p-DDE, o,p-DDD, o,p-DDT, Heptachlor Epoxide,Methoxychlor,Endrin,Endrin Ketone,Endrin Aldehyde, Chlorienvinphos, Paraquat dichloride,trichlorfon

PR analysis of Food Commodities, Based on AOAC 19th Ed.,:2012Based On Pesticide Analytical Manual;

Synthetic pyrethroidsLambda cyhalothrin, cyfluthrin, cypermethrin, Deltamethrin, Fenvalerate, permethrin.Others:

SOP No.15/02 A, 2015.04.08 Issue No.:4.0 & SOP No.15/02 B 2015.04.08 Issue No.:4.0 Based on DGHS:2005-Manual of methods of PR analysis of Food Commodities, Based on AOAC 19th Ed.,:2012Based On Pesticide Analytical


Anita RaniConvenor










Dicofol, Ethion, Captafol, Phosalone, chloropyrifos

Manual;

Food Grains, Dry Products and Soil

Organophosphorous Pesticide:Acephate,Diazinon,Dichlorovos,Dimethoate,Fenitrothion,Malathion,Monocrotophos,Parathion, ethyl Parathion, methyl,Phosphamidon, Atrazine,Metalaxyl,Carbofuran,Carbaryl,Thiram,Fenthion,Fosetyl aluminium,Propoxur (Baygon),Simazine,Aldicarb,O,O,O-trimethyl

SOP No.15/02 A, 2015.04.08 Issue No.:4.0 & SOP No.15/02 B 2015.04.08 Issue No.:4.0 Based on DGHS:2005-Manual of methods of PR analysis of Food Commodities, Based on AOAC 19th Ed.,:2012Based On Pesticide Analytical Manual;


Anita RaniConvenor










phosphorothinate,Disulfoton, Sulfotep, Phorate,Famphur,Thionazin,Thiometon,Carbendazin,Benomyl, Pyrethrin,Dithiocarbamates, Phenthoate,Phoarate, Pirimiphos methyl,Oxydemeton methyl, 2,4-D

f. Food Grains/Rice/Chillies /Cereals & Pulses/Ground Nuts/Wheat,Barley & Rye

Aflatoxin-B1, B2, G1 and G2Ochratoxin A

Mycotoxins:Deoxynivalenol, T-2 toxin , HT-2 toxin, Zeralanone, Fumonosins B1, B2,

SOP No. 15/39 , 2014.10.21, Issue No. 4.0;Based on AOAC 19th Ed.,:2000 chap.49/In house validated method Chap.49.2.17


Anita RaniConvenor










DyesSudan-I, II, III & IV

Sudan Red-BSudan Orange-GSudan Red-GSudan Red -7BPara RedDimethyl yellowRhodamine-B

SOP No.15/38 , 2014.09.20, Issue No. 4.0;Based on Journal of Chrom. 1042, 2004, 123-130;


Melamine SOP No.15/54 , 2013.05.08, Issue No. 3.0; Based on LI-00.176-4


Cyanuric acid SOP No.15/54 , 2013.05.08, Issue No. 3.0; Based on LI-00.176-4


Food Grains/Rice/Chillies/ Cereals & Pulses/ Ground Nuts/Wheat,Barley & Rye

Aldrin, Dieldrin, Carbaryl, Chlordane,Diazinon, Dichlorvos, Dicofol,Dimethoate,Endosulfan & its isomers,Fenitrothion, Heptachlor,

Method Validation No: VLS-TAL/PR- Food Grains/001;DGHS-Manual of methods of PR analysis of Food Commodities, AOAC method 19th edition USEPA 8141A,5151.1Standard operating procedure for the analysis of agrochemical residue(annexure 9 of the residue monitoring plan of APEDA)grapes

0.01 µg/kg to 0.2 mg/kg(For each individual residue)

Anita RaniConvenor










Food Grains/Rice/

HCH Isomers,Malathion, Phosphomidon residues and its desethyl derivative,Pyrethrins, Chlorfenviphos, Chlorpyriphos, 2,4-D,Ethion,Monocrotophos,Trichlorfon, Thiometon and its sulfoxide&Sulfone,Carbendazim,Benomyl,Carbofuran,3-HydroxyCarbofuran,Cypermethrin,Deltamethrin,Edifenophos,Fenthion and its oxygen sulfone & sulfoxide,Dithiocarbomates,Phenthoate,Phorate and its oxygen analogue & their sulfoxides & its sulfones, Simazine, Pirimiphos methyl, Alachlor,

Anita RaniConvenor










Chillies/ Cereals & Pulses/ Ground Nuts/Wheat,Barley & Rye

Biternol, Cartap Hydrochloride,Ethephon,Metalaxyl,Methylchloro phenoxy acetic acid,Oxadiazon,Oxydemeton methyl,Triazophos,Iprodione,Tridemorph,Propiconazole,Sulfosulfuron,Trifluraline,Etoxy Sulfosulfuron,Glyphosate,Oxyflurofen, Carbosulfan,Tricyclazole, Aflatoxins

Imidacloprid,Butachlor,Chlorimuron ethyl,Dichlofop methyl,Fenazaquin,Pendimethalin,Pretilachlor, Metasulfuron methyl,

Method Validation No: VLS-TAL/PR- Food Grains/001;DGHS-Manual of methods of PR analysis of Food Commodities, AOAC method (19th Edition) USEPA 8141A,5151.1Standard operating procedure for the analysis of agrochemical

Anita RaniConvenor










Food Grains/Rice/Chillies/ Cereals & Pulses/ Ground Nuts/Wheat,Barley & Rye

Methabenzthiazuron,Cyhalofop –butyl,Triallate,Thiamethoxam,Fenobucarb,Anilophos,Fenoxy prop p ethyl,Clodinafop propanyl,Kitazin,Isoprothiolane,Triadimefon,Ethofenprox,Benfucarb,Flufenacet,Buprofezin,Carpropamid,Oxadiargyl,Pyrazo ethyl,Clomazone,Tebuconazole,Thiachlroprid,Glufosinate ammonium,Propargite, Aldicarb Aldicarb sulfone, Aldicarb Sulfoxide, Chlorobenzilate, Paraquat dichloride, Coumaphos, Fenchlorphos,

residue Annexure 9 of the residue monitoring plan of APEDA)grapes

Anita RaniConvenor










Methylparaxon, Endrin, Aldehyde, Endrin Ketone

g. Milk and Its Products

Milk and Its Products

Aldrin,Dieldrin,Chlordane, DDT Isomers,Fenitrothion,Heptachlor,HCH Isomers, Chlorfenviphos,Chlorpyriphos, 2,4,-D, Ethion,Monocrotophos,

Based on DGHS-Manual of methods of PR analysis of Food Commodities, 2011 (S.No:7-44)/AOAC (19th Edition) 970.52: 2005VLS/TAL/MILK/PR-001

0.01 mg/l to 0.2 mg/l (For each individual residue)

Paraquat dichlorate, Trichlorfon,Thiometon and its sulfoxide, its sulfone, Carbendazim,Benomyl,Thenthoate, Carbofuran ,3-Hydroxy Carbofuran,Cypermethrin,Edifenphos,Fenthion,its oxygen sulfone, and its Oxygen sulfoxide,Fenvalerate,Phenthoate,

Based on DGHS-Manual of methods of PR analysis of Food Commodities, 2011 (S.No:7-44)/AOAC (19th Edition) 970.52: 2005,

0.01 mg/l to 0.2 mg/l(For each individual residue)

Anita RaniConvenor










Phorate and its oxygen analogue & their sulfoxides & its sulfones,Pirimiphos methyl, Cyanuric acid

Aflatoxin M1, DGHS-Manual of methods of PR analysis of Food Commodities


Melamine Method Validation No: VLS-TAL/MILK PR-R/001

0.05 mg/l to 5.0 mg/l

h. Apple juice and its ingredients in other beverages

Patulin VLS-TAL/PATULIN/MVR/001 0.01 µg/l to 0.2 µg/l

i. Seeds, Oils, Fats & Related Products

Dioxin like PCBs3,3’-4,4’-tetrachlorobiphenyl (PCB 77), 3,4,4’,5-tetrachlorobiphenyl (PCB 81), 2,3,3’,4,4’-pentachlorobiphenyl (PCB 105), 2,3,4,4’,5-pentachlorobiphenyl (PCB 114), 2,3’,4,4’,5-pentachlorobiphenyl (PCB 118),

EPA 1668 method (2008)

VLS-TAL/dl-PCB-R/001Based on AOAC (19th Edition)/USFDA/DGHS-manual of methods of PR analysis of food commodities,2011(S.No: 7-44)

0.01 ng/kg to 0.2 ng/kg(For each individual residue)

Anita RaniConvenor










Seeds, Oils, Fats & Related Products

2’,3,4,4,5’-pentachlorobiphenyl (PCB 123), 3,3’,4,4’,5-pentachlorobiphenyl (PCB 126), 2,3,3’,4,4’,5-hexachlorobiphenyl (PCB 156), 2,3,3’,4,4’,5’-hexachlorobiphenyl (PCB 157), 2,3’,4,4’,5, 5’-hexachlorobip3,3’,4,4’,5,5’-hexachlorobiphenyl (PCB 169),2,2’,3,3’,4,4’,5-heptachlorobiphenyl (PCB 170), 2,2’,3,4,4’,5,5’-heptachlorobiphenyl (PCB 180),2,3,3’,4,4’,5,5’-heptachlorobiphenyl (PCB 189)

Polychlorinated dibenzodioxin and polychlorinated dibenzodifuran

EPA 1613 method (1994) VLS-TAL/Dx-R/001

0.01 ng/kg to 0.2 ng/kg

Anita RaniConvenor










(PCDD/PCDF)


Polychlorinated biphenyl (PCBs) Mono-chlorobiphenyl, Dichlorobiphenyl, Trichlorobiphenyl, Tetrachloro-biphenyl, Penta-chlorobiphenyl, Hexa-chlorobiphenyl, Hepta-chlorobiphenyl and Octachlorobiphenyl Carbaryl, Endosulfan & its Isomers,Chlorpyriphos, Ethion, Monocrotophos, Paraquat,Trichlorfon, Acephate, Methamidophos, Carbendazim,Benomyl, Carbofuran,3hydoxy carbofuran,Cypermethrin,Deltamethrin,Fenvalerate, Phenothate, Phorate,

VLS-TAL/dl-PCB-R/001Based on AOAC 19th edition/USFDA/DGHS-manual of methods of PR analysis of food commodities,2011(S.No: 7-44)


Anita RaniConvenor











Phorate sulfone,Phorate Sulfoxide,Alachlor,Diuron,Chlormequat chloride, Diflubenzuron,Fluchloralin, Methomyl, Triazophos, Profenophos, Fenpropathrin, Iprodione, Myclobutanil, Metolachlor,Oxyfluorfen, Imidacloprid, Metribuzin,Lambda Cyhalothrin, Pendimethalin, Fluvalinate, Imazethapyr, Spinosad, Thiodicarb,Acetamiprid,Indoxacarb, Metiram, Novaluron,Clomazone,Thiacloprid, Aldicarb sulfone,

0.01 mg/ kg to 0.2 mg/kg(For each individual residue)

Anita RaniConvenor










Aldicarb Sulfoxide,Aldicarb

j. Pesticide Residues in Raw Materials in Medicinal Products

Pesticide Residues in Raw Materials in Medicinal

α-HexachlorocyclohexaneHexochlorobenzeneβ-HexachlorocyclohexaneLindaneδ-Hexachlorocyclohexaneє-HexachlorocyclohexaneAldrinAlachlorChlordane (sum of cis- and trans- isomers and oxychlordane)Heptachlor (sum of heptachlor and heptachlor epoxide)o, p’-DDEChlorfenvinphosα –EndosulfanDieldrinp, p’-DDEo, p’-DDDEndrinβ -Endosulfano, p’-DDTDichlorvosFonofosDiazinonParathion-Methyl

Based on USP 34 (2011) Chapter<561>,USP 37

0.01 mg/ kg to 0.2mg/kg(For each individual residue)

Anita RaniConvenor










Products Chlorpyrifos-MethylPirimiphos-MethylMalathionParathionChlorpyrifosMethidathionEthionAzinphos-MethylPhosalonecis-Permethrintrans-PermethrinCypermethrin ( and isomers)FenvalerateDeltamethrinFenitrothionBromopropylateDithiocarbamates (as CS2)Quintozene (Sum of quintozene, pentachloroanilene, methyl pentachlorophenyl sulfide),Piperonyl butoxide

0.01 µg / kg to 0.2 µg/kg(For each individual residue)

k. Sugar & Sugar Based Confectionery Products

Organochlorine pesticidesAldrin, Chlordane (cis & trans), chlorothalonil, DDT (all isomers), Endrin, HCH isomers,

SOP No.15/27 A, 2014.05.30, Issue No.8.0 & SOP No.15/27B 2014.05.27, Issue No.7.0Based on USP 34 (2011) Chapter<561> USEPA 508,525.2; IS 14543-1988

0.1 µg / kg to 2.0 µg / kg(For each individual residue)

Anita RaniConvenor










Sugar & Sugar Based Confectionery Products

4-bromo-2-chlorophenol, Dicofol, Lindane, Dieldrin, Endosulfan (all isomers)

Organophosphorus pesticides: O,O,O-trimethyl hosphorothinate,Disulfoton, Sulfotep, Phorate,Famphur,Thionazin,Thiometon,Carbendazin,Benomyl, Pyrethrin,Phenthoate,Phoarate, Pirimiphos methyl,Oxydemeton methyl

SOP No.15/27 A, 2014.05.30, Issue No.8.0 & SOP No.15/27B 2014.05.27, Issue No.7.0Based on USP 34 (2011) Chapter<561> USEPA 508,525.2; IS 14543-1988


OthersPhorate Sulfone,EndosulfanI, EndosulfanII, Lindane(gamma- BHC), Dicofol,

SOP No.15/27 A, 2014.05.30, Issue No.8.0 & SOP No.15/27B 2014.05.27, Issue No.7.0Based on USP 34 (2011) Chapter<561> USEPA 508,525.2;


Anita RaniConvenor











cypermethrin, Deltamethrin, Fenvalerate, permethrin. Acephate, Diazinon, Dichlorvos, Dimethoate, fenitrothion, fenthion, fosetyl aluminium, malathion, metalaxyl, methyl parathion, monocrotophos,Parathion, phosphomidon, Aldicarb, carbaryl, carbofuran, propoxur, Dithiocarbamates, Atrazine, Simazine, Diuron, formothion, Imidacloprid, phorate, Quinalphos, Fipronil,

IS 14543-1988

Anita RaniConvenor











oxamyl, MEMC(Methoxy ethyl mercury oxide), Alachlor, MCPA, paraquat dichloride, 2,4-D, Metribuzin, Azinophos-methyl, Etroprophos, propiconazole.Heptachlor, , Heptachlor Epoxide,Methoxychlor,Endrin, Endrin Ketone,Endrin Aldehyde, Chlorienvinphos, Paraquat dichloride,trichlorfonCaptafol, phosalone, Ethion, chloropyrifos, Endosulfan Sulphate, Methyl Paraoxon,Butachlor, Malaoxon,Isoproturon, Phorate Sulfoxide,

Anita RaniConvenor










l. Coffee ,Tea &Tea Products

Coffee ,Tea &Tea Products

Organochlorine Pesticides: Alpha-BHC, Beta-BHC, Delta -BHC, chlordane,o,p-DDE Heptachlor,Aldrin, p,p -DDE, Trifluralin,Dieldrin, p,p- DDD, Endosulphan sulphate, p,p-DDT, Dicofol, Ethion, captafol, phosalone, EndosulfanI, Endosulfan II, o,p-DDT,o,p-DDD Lindane(gamma-BHC), Endosulfan sulphate,Bromopropylate,

SOP No.15/26 A, 2015.02.15 Issue No. 5.0 & SOP No.15/26 B, 2015.02.15 Issue No. 5.0SOP No. 15/03 A, 2014.06.02 issue No. 5.0 & SOP No. 15/03 B, 2014.06.06 issue No. 5.0Based on AOAC 19th Ed.: 2012 USFDA/ DGHS-Manual of methods of PR analysis of Food Commodities, 2011 (S.No:7-44)

0.01 to 0.2 mg/kg(For each individual residue)

Synthetic pyrethroidsLambda cyhalothrin, cyfluthrin, cypermethrin, Deltamethrin,

SOP No.15/26 A, 2015.02.15 Issue No. 5.0 & SOP No.15/26 B, 2015.02.15 Issue No. 5.0SOP SOP No. 15/03 A, 2014.06.02 issue No. 5.0 & SOP

0.01 to 0.2 mg/kg(For each individual residue)

Anita RaniConvenor










Fenvalerate, permethrin, Alphamethrin, Bifenthrin,Ethofenprox,

No. 15/03 B, 2014.06.06 issue No. 5.0Based on AOAC 19th edn.:2012 / USFDA/ DGHS: 2005-Manual of methods of PR analysis of Food Commodities, 2011 (S.No:7-44)

Coffee ,Tea &Tea Products

Organo Phophorous Pesticides: Fenpropathrin. Acephate, Diazinon, Dichlorvos, Dimethoate, Malathion, Monocrotophos, Parathion-ethyl, Parathion-methyl,Phosphamidon, Atrazine, Metalaxyl, Carbofuran, Carbaryl, Thiram , Fenitrothion,Chlorpyriphos methyl, Profenophos, GlyphosateCartap,Glufosinate Ammonium, Tetradifon ,Quinalphos,Methamidophos,Thiamethoxam,

SOP No.15/26 A, 2015.02.15 Issue No. 5.0 & SOP No.15/26 B, 2015.02.15 Issue No. 5.0SOP No. 15/03 A, 2014.06.02 issue No. 5.0 & SOP No. 15/03 B, 2014.06.06 issue No. 5.0Based on AOAC 19th edn.:2012/ USFDA/ DGHS:2005-Manual of methods of PR analysis of Food Commodities, 2011 (S.No:7-44);


Anita RaniConvenor










Fenazaquin,Pirimiphos methyl,Phorate, S-421,Hexaconazole,Triazophos,Methidathion,Fenthion,Propargite,Triadimefon.Malathi on,Oxydemeton methyl,Fenitrothion,Imidacloprid,2,4-D,Paraquat,Malathion,Oxydemeton methyl, Clothianidan, Fenproximate, EthephonAflatoxin B1,B2, G1, G2 Ochratoxin

AOAC Method (Based on QuEChERS method)


m. Kraft Paper Anthraquinone, PCP AOAC Method (Based on QuEChERS method)

0.01 to 0.2 mg/Kg(each residue)

n. Guar gum Dioxin & Furans –Polychlorinated dibenzodioxin and Furan polichlrinated dibenzodifuran (PCDD/PCDF)

USEPA 1613 Rev.B (1994) 0.01 ng/kg to 100 ng/kg

Anita RaniConvenor










Guar gum

Dioxins like PCBs- HRGC/HRMS3,3’4,4’-tetrachlorobiphenyl (PCB 77), 3,4,4’,5-tetrachlorobiphenyl (PCB 81),2,3,3’,4,4’-pentachlorobiphenyl (PCB 105), 2,3,4,4’,5-pentachlorobiphenyl (PCB 114), 2,3’,4,4’,5-pentachlorobiphenyl (PCB 118), 2’,3,4,4,5’-pentachlorobiphenyl (PCB 123), 3,3’,4,4’,5-pentachlorobiphenyl (PCB 126), 2,3,3’,4,4’,5-hexachlorobiphenyl (PCB 156), 2,3,3’,4,4’,5’-hexachlorobiphenyl (PCB 157), 2,3’,4,4’,5, 5’-hexachlorobiphenyl (PCB 167),

EPA 1668 Rev. B (2008) 0.05 ng/kg to 10.0 ng/kg(For each individual residue)

Anita RaniConvenor










3,3’,4,4’,5,5’-hexachlorobiphenyl (PCB 169), 2,2’,3,3’,4,4’,5-heptachlorobiphenyl (PCB 170), 2,2’,3,4,4’,5,5’-heptachlorobiphenyl (PCB 180), 2,3,3’,4,4’,5,5’-heptachlorobiphenyl (PC B 189)

Pentachlorophenol SOP 15/47 0.001 mg/kg to 100 mg/kg

III. WATER1. Water & Waste

Water

Water & Waste

Pesticide residues:Alpha-BHC, Beta-BHC, Gamma-BHCDelta-BHC, Aldrin, Dieldrin, Endosulfan-I, Endosulfan-II, Endosulfan SulfateO,p’-DDE, P,p’-DDE, O,p’-DDD, P,p’-DDD,

SOP No.15/31A 2014.05.13 Issue No. 5.0 & SOP No.15/31B 2014.05.13 Issue No. 5.0 Based on IS: 14543-2004, IS: 13428 -2005, USEPA, Based on AOAC 19th Ed.:2012, APHA 22nd ed:2012, Pesticide analytical manual, USFDA

0.01 µg/l to 0.2 µg/l (For each individual residue)

Anita RaniConvenor










Water O,p’-DDT, P,p’-DDT

MonocrotophosAlachlorButachlorIsoproturonAtrazineMalathionEthionChlorpyrifosMethyl ParathionPhorate2,4-DMalaoxonMethyl ParaoxonPhorate Sulfone, Phorate Sulfoxide

SOP No.15/31A 2014.05.13 Issue No. 5.0 & SOP No.15/31B 2014.05.13 Issue No. 5.0 Based on IS: 14543-2004, IS: 13428 -2005, USEPA, Based on AOAC 19th Edition:2012,APHA22nded:2012, Pesticide analytical manual, USFDA


Polychlorinated biphenyls (PCBs):Mono-chlorobiphenyl, Dichlorobiphenyl, Trichlorobiphenyl, Tetrachloro-biphenyl, Penta-chlorobiphenyl, Hexa-chlorobiphenyl, Hepta-chlorobiphenyl and Octachlorobiphenyl

APHA 22nd ed.:2012IS: 13428-2005 SOP No.15/31A 2014.05.13 Issue No. 5.0 & SOP No.15/31B 2014.05.13 Issue No. 5.0Pesticide Analytical Manual,USFDA


Anita RaniConvenor










Water & Waste Water

PCBs- HRGC/HRMS3,3’-4,4’-tetrachlorobiphenyl (PCB 77), 3,4,4’,5-tetrachlorobiphenyl (PCB 81), 2,3,3’,4,4’-pentachlorobiphenyl (PCB 105), 2,3,4,4’,5-pentachlorobiphenyl (PCB 114), 2,3’,4,4’,5-pentachlorobiphenyl (PCB 118), 2’,3,4,4,5’-pentachlorobiphenyl (PCB 123), 3,3’,4,4’,5-pentachlorobiphenyl (PCB 126), 2,3,3’,4,4’,5-hexachlorobiphenyl (PCB 156), 2,3,3’,4,4’,5’-hexachlorobiphenyl (PCB 157), 2,3’,4,4’,5, 5’-hexachlorobiphenyl (PCB 167),

EPA 1668 Rev B (2008)

VLS-TAL/dl-PCB-R/001

0.3 µg/l to 100 µg/l (For each individual residue)

Anita RaniConvenor










Water & Waste Water

3,3’,4,4’,5,5’-hexachlorobiphenyl (PCB 169), 2,2’,3,3’,4,4’,5-heptachlorobiphenyl (PCB 170), 2,2’,3,4,4’,5,5’-heptachlorobiphenyl (PCB 180), 2,3,3’,4,4’,5,5’-heptachlorobiphenyl (PCB 189)

Polychlorinated dibenzodioxin and polychlorinated dibenzodifuran (PCDD/PCDF)

EPA 1613 Rev.B (1994)VLS-TAL/Dx-R/001

0.01 mg/l to 5.0 mg/l

Volatile Organic Compounds (BenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformn-butylbenzeneSec-butylbenzeneTert-butylbenzeneCarbon tetrachlorideChlorobenzene

EPA –8260 B (1996)/ APHA (22nd Edition)EPA 524.2

0.0003 mg/l to 0.2 mg/l(For each individual residue)

Anita RaniConvenor










Chloroform2-chlorotoluene4-chlorotolueneDibromochloromethane1,2-dibromo-3-Chloropropane1,2-dibromoethaneDibromomethane1,2-dichlorobenzene1,3-dichlorobenzenerobenzene1,1-dichloroethane1,2-dichloroethane1,1-dichloroetheneCis-1,2-dichloroetheneTrans-1,2-dichloroethene1,2-dichloropropane1,3-dichloropropane2,2-dichloropropane1,1-dichloropropeneCis-1,3- dichloropropeneTrans-1,3- dichloropropeneEthylbenzeneHexachlorobutadieneIsopropylbenzenep-isopropyltolueneDichloromethaneNaphthalenePropylbenzeneStyrene

Water & Waste Water

Anita RaniConvenor










1,1,1,2-tetrachloroethane1,1,2,2-tetrachloroethaneTetrachloroethene Toluene1,2,3-trichlorobenzene1,2,4- trichlorobenzene1,1,1-trichloroethane1,1,2-trichloroethaneTrichloroethene1,2,3-trichloropropane1,2,4-trimethylbenzene1,3,5-trimethylbenzeneo-XyleneM&P-XyleneBromomethaneChloroethaneChloromethaneDichlorodifluoromethaneTrichlorofluoromethaneVinyl chloride)

Water & Waste Water

AcenaphthaneAcenaphthyleneAnthracene, Benz(a)anthraceneBenzo(a)pyrene, Benzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluoranthene

EPA- 8310 APHA (22nd Edition)

0.01µg/l to 0.2µg/l (For each individual residue)

Anita RaniConvenor










Chrysene, Dibenz(a,h)anthraceneFluoranthene, Fluorene, PyreneIndeno(1,2,3-cd)pyrene, NaphthalenePhenanthrene

AldicarbAldicarb SulfoxideAldicarb SulfoneCarbofuranChlorotoluron

Method Validation No: VLS-TAL/WATER/P-R/001(Based on EPA Method:525.2,531.2.532,528,515.4,552..2,555,508)LC-MS/MS

0.03 µg/l to 0.2 µg/l(For each individual residue)

Water & Waste Water

DimethoateOxamylPendimethalinPyriproxyfenSimazineTerbuthylazineMolinateMetolachlor2,4,6 Trichlorophenol2,4,DBDalaponDichloroprop

Anita RaniConvenor










DinosebMCPA, CyanazineMecopropPicloram

Fenoprop2,4,5-T (Trichlorophenoxy acetic acid)Pentachlorophenol

Method Validation No: VLS-TAL/WATER/P-R/001(Based on EPA Method:525.2,531.2.532,528,515.4,552..2,555,508)LC-MS/MS

0.03 µg/l to 0.2µg/l(For each individual residue)

EndrinHeptachlorHeptachlorepoxideTranschlordaneCis ChlordaneTrifluralinHexachlorobenzeneMethoxychlor

Method Validation No: VLS-TAL/WATER/P-R/001(Based on EPA Method:525.2, 505.5)(GC-MS/MS)


Water & Waste Water

Diquat Method Validation No: VLS-TAL/WATER/P-R/004(Based on EPA Method:549.2, 548.1)(LC-MS/MS)

0.01 µg/l to 0.2µg/l

Endothall Hydrate Method Validation No: VLS-TAL/WATER/P-R/004(Base

50.0 µg/l to 250 µg/l

Anita RaniConvenor










d on EPA Method 547,(LC-MS/MS)

Edetic acid Method Validation No: VLS-TAL/WATER/P-R/004

Di(2-ethylhexyl)phthalateDi(2-ethylhexyl)adipateHexachlorocyclopentadieneChloralhydrateDichloroacetonitrile Dibromoacetonitrile

Method Validation No: VLS-TAL/WATER/P-R/005(Based on EPA Method:525.2, 551.1,552.2)(GC-MS/MS)


Haloacetic acidsMonochloro acetate(Monochloro acetic acid)Dichloro acetate(Dichloro acetic acid)Trichloro acetate(Trichloro acetic acid)

Method Validation No: VLS-TAL/WATER/P-R/002(Based on EPA Method:552.2)(GC-MS/MS)


Acrylamide Method Validation No: VLS-TAL/WATER/P-R/001 (LC-MS/MS)

0.03 µg/l to 0.2µg/l

Epichlorohydrin EPA524.2/GC-MS/MS 0.40 µg/l to 25 µg/l

Glyphosate VLS-TAL/water/PR/003 0.1µg/l to 5.0µg/lWater & Waste Water

Formaldehyde EPA8315A/GC-MS/MS 5.0 µg/l to 100 µg/l

Toxaphene EPA505/GC-MS/MS 0.03 µg/l to 0.2 µg/l

Anita RaniConvenor










1,4,-Dioxine Method Validation No: VLS-TAL/WATER/P-R/006 GC-MS/MS

10.0 µg/l to 200 µg/l µg/l

Nitrilotriacetic acid Method Validation No: VLS-TAL/WATER/P-R/006 GC-MS/MS

100.0 µg/l to 500.0µg/l µg/l

Cyanogen Chloride Method Validation No: VLS/TAL/Coke-R/001

10 µg/kg to 200 µg/kg

2. All Waters Other than Effluents Water

Color (Pt-Co) IS 3025 (Part 4): 1983APHA 2120 C 22nd edition

1 to 50 Pt-Co Units

Odour IS 3025 (Part 5): 1983APHA 2150 22nd edition

Qualitative

Total dissolved solids IS 3025 (Part 16): 1984APHA 2540 C 22nd edition

1 mg/L to 50 mg/L50 mg/L to 100 mg/L100 mg/L to 500 mg/L>500 mg/L

Turbidity IS 3025 (Part 10): 1984APHA 2130 B 22nd edition

0.1 NTU to 1 NTU1 NTU to 10 NTU

pH IS 3025 (Part 11): 19834500 B 22nd edition

1 to 13

Conductivity IS 3025(Part 14): 1984, APHA 2510 B 22nd edition

0.01 µS/cmto 1000 µS/cm>1000 µS/cm

Anita RaniConvenor










All Waters Other than Effluents Water

Mineral oil IS:3025(Part-39) - 1991,APHA 5520 (B&C) 22nd edition

4 mg/L100 mg/L

Residual free chlorine IS:3025(Part-26,1.2)-1986 APHA 4500 Cl G 22nd edition

0.1 mg/L to 10 mg/L10 mg/L to 500 mg/L>500 mg/L

Chloride USEPA-300.1-2(1997) by IC 0.1 mg/L to 10 mg/L10 mg/L to 500 mg/L>500 mg/L

Fluoride

USEPA-300.1-2(1997) by IC 0.1 mg/L to 10 mg/L>10 mg/L

IS 3025 (Part 60,1.2): 2008 APHA 4500 F- D 22nd edition

0.1 mg/L to 1.4 mg/L>1.4 mg/L

APHA 4500 F- C 22nd edition 0.1 mg/L to 1.4 mg/L>1.4 mg/L

Alkalinity (p & m) IS 3025 (Part 23): 1986,APHA 2320 B 22nd edition

1 mg/L to 100 mg/L100 mg/L to 500 mg/L>500 mg/L

Total hardness IS 3025 (Part 21,2 & 3): 2009APHA 2340 B&C 22nd edition

1.0 mg/L to 100 mg/L

Phenolic compounds IS 3025 (Part 43): 1992APHA 5530 C 22nd edition

0.001 mg/L to 1.0 mg/L>1 mg/L

Anita RaniConvenor










Silica IS 3025 (Part 35, 3) : 1988APHA 4500-Si C 22nd edition



Nitrate

IS:3025(Part-34, 3.3) -1988 0.1 mg/L to 1 mg/L1 mg/L to 10 mg/L>10 mg/L

USEPA-300.1-2(1997) by IC 0.1 mg/L to 1 mg/L1 mg/L to 10 mg/L

APHA 4500 NO3- B&C 22nd

edition0.1 mg/L to 1 mg/L1.0 mg/L to 10 mg/L

Nitrite

IS: 3025(Part-34, 4)-1988/APHA 4500 NO2

- B22nd edition


USEPA-300.1-2(1997) by IC 0.1 mg/L to 1 mg/L1 mg/L to 10 mg/L>10 mg/L

Sulphates

IS:3025(Part-24, 4)-1986/APHA 4500 SO4

2- E 22nd edition0.1 mg/L to 1 mg/L1 mg/L to 10 mg/L>10 mg/L

USEPA-300.1-2(1997) by IC 0.1 mg/L to 1 mg/L >20 mg/L

Sulphide IS:3025(Part-29, 3)-1986 0.01 mg/L to 10 mg/L

Anita RaniConvenor










APHA 4500 S2- D 22nd edition 10 mg/L to 100 mg/L

Bromide USEPA – 300.1-2 (1997) by IC 0.01 mg/L to 10 mg/L

Bromate USEPA – 300.1-2 (1997) by IC 0.01 mg/L to 10 mg/L

Chlorite USEPA – 300.1-2 (1997) by IC 0.01 mg/L to 10 mg/L


Chlorate USEPA – 300.1-2 (1997) by IC 0.01 mg/L to 1 mg/L1 mg/L to 20 mg/L

Cyanide

IS 3025 (Part 27, 3): 1986 0.05 mg/L to 0.1 mg/L0.1 mg/L to 1.0 mg/L1.0 mg/L to 10 mg/L

APHA 4500-CN-, E & F 0.05 mg/L to 0.1 mg/L0.1 mg/L to 1.0 mg/L1.0 mg/L to 10 mg/L

Calcium IS 3025 (Part 40, a): 1991APHA 3500 Ca B

0.1 mg/L to 1 mg/L1 mg/L to 10 mg/L> 10 mg/L

Sodium IS 3025 (Part 45, a ): 1993 0.1 mg/L to 1 mg/L> 1 mg/L

Anionic surface active agents (MBAS)

IS 13428: 2005 0.01 mg/L to 2 mg/L2 mg/L to 10 mg/L

Antimony APHA 3113 B & 3125 22nd edition 0.001 mg/L to 0.1 mg/L

Anita RaniConvenor










> 0.1 mg/L

IS:15303:2003/Annex C of IS 13428:2005

0.005 mg/L to 0.1 mg/L>0.1 mg/L

Copper APHA 3111 B 22nd edition 0.01 mg/L to 0.1 mg/L> 0.1 mg/L

APHA 3125 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

IS:3025 Part 2:2004 0.02 mg/L to 5 mg/L>0.01mg/L


Iron APHA 3111 22nd edition 0.04 to 1.0> 1.0 mg/L


IS 3025 part 2:2004 0.05 mg/L to 1.0 mg/L>1.0mg/L

Manganese APHA 3125 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

IS 3025 Part 2:2004 0.05 mg/L to 1.0 mg/L>0.01 mg/L

Arsenic APHA 3113 B 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

APHA 3114 C 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

Anita RaniConvenor










APHA 3125 22nd edition

0.001 mg/L to 0.1 mg/L> 0.1 mg/L

IS 3025 (Part 37): 1988 0.05 mg/L to 0.1 mg/L>0.05 mg/L

Mercury APHA 3112 B 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

EPA 200.8-13 (1994) 0.0005 mg/L to 0.05 mg/L

IS 3025 (Part 48): 1994 0.001 mg/L to 0.1 mg/L>0.001 mg/L

Cadmium APHA 3113 B 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L


IS 3025 (Part 41): 1992 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

Chromium APHA 3125 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

APHA 3111 D 22nd edition 0.04 mg/L to 5.0 mg/L> 5.0 mg/L

IS :3025 Part 2:2004 0.01 mg/L to 0.1 mg/L>0.1 mg/L

Zinc APHA 3111 B 22nd edition 0.01 mg/L to 0.1 mg/L> 0.1 mg/L

Anita RaniConvenor











IS:3025 Part 2:2004 0.01 mg/L to 2.0 mg/L> 0.01 mg/L

Selenium APHA 3113 B 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

APHA 3114 C 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L


IS:15303:2003 0.01 mg/L to 1.0 mg/L>1.0 mg/L

Boron APHA 3125 22nd edition 0.005 mg/L to 0.1 mg/L> 0.1 mg/L


IS 13428: 2005 Annexure H 0.2 mg/L to 1.0 mg/L> 0.2 mg/L

Borate IS:3025 (Part 2): 2004 0.2 mg/L to 1.0 mg/L> 0.2 mg/L

Aluminium APHA 3125 22nd edition 0.005 mg/L to 0.1 mg/L> 0.1 mg/L

IS 3025 (Part 55):2003 20 mg/L to 300 mg/L> 0.03 mg/L

Anita RaniConvenor










Lead APHA 3111 B 22nd edition 0.04 mg/L to 1 mg/L>1.0 mg/L

APHA 3113 B 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L


IS:3025 -Part 47:1994 1.0 mg/L to 10.0 mg/L> 0.01 mg/L

Cobalt APHA 3125 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

Molybdenum APHA 3125 22nd edition

0.001 mg/L to 0.1 mg/L> 0.1 mg/L

Nickel APHA 3125 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

APHA 3111 B 22nd edition, Annexure L of IS: 13428:2005

0.01 mg/L to 1 mg/L>1.0 mg/L


Silver APHA 3125 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

APHA 3111 B 22nd edition, Annexure J of IS: 13428:2005

0.01 mg/L to 1 mg/L>1.0 mg/L

Barium APHA 3125 22nd edition 0.001 to 0.1 mg/L

Anita RaniConvenor










> 0.1 mg/L

APHA 3111 B 22nd edition, Annexure F of IS: 3025 Part2:2004

0.01 mg/L to 1 mg/L>1.0 mg/L

Beryllium APHA 3125 22nd edition 0.0005 mg/L to 0.05 mg/L> 0.1 mg/L

Uranium APHA 3125 22nd edition 0.0005 mg/L to 0.05 mg/L> 0.1 mg/L

Thalium APHA 3125 22nd edition 0.001 mg/L to 0.1 mg/L> 0.1 mg/L

Mono chloramine IS:3025(Part-26,1.2)-1986APHA 4500 Cl G 22nd edition

0.05 mg/L & 1 mg/L1 mg/L to 10 mg/L

TOC(Total Organic Carbon) APHA 5310 B 22nd editionEP/USP-31

0.1 mg/L to 1.0 mg/L1 mg/L to10 mg/L

Total suspended solids IS 3025 (Part 16): 1984 1.0 mg/L to 20000 mg/L

Total Solids IS 3025 (Part 16): 1984APHA 2540B 22nd edition

1.0 mg/L to 20000 mg/L

Dissolved oxygen IS 3025 (Part 38): 1989 1 mg/L to 9 mg/L

Ammonia IS 3025 (Part 34): 1988 0.1 mg/L to 0.6 mg/LAll Waters Other than Effluents Water

COD APHA 5220B 22nd edition 5 mg/L to 250 mg/L

BOD IS 3025 (Part 44): 1993 5 mg/L to 300 mg/L

Anita RaniConvenor










Phosphate as PO4 IS 3025 (Part 31): 1988 1.0 mg/L to 20 mg/L

Magnesium IS 3025 (Part 46): 1994 0.1 mg/L to 30 mg/L

IV. AIR, GASES & ATMOSPHERE

1. Ambient Air Monitoring/ Fugitive Emission Monitoring

Total suspended particulate matter (TSPM)

IS 5182(Part 4): 1999 (RA 2005)Methods of air sampling and Analysis (second Edition)APHA INTERSOCIETY COMMITTEE – 501

5 µg/m3 to 5 mg/m3

P.M.10 ( Particulate Matter < 10 µm) / Respirable suspended particulate matter

IS 5182 (Part 23): 2006 (RA 2012) 5µg/m3 to 5mg/m3

P.M.2.5 USEPA Quality Assurance Guidance Document Volume 2(Part 2): 2012

1µg/m3 to 5mg/m3

Sulphur dioxide ( as So2) IS 5182 (Part 2): 2001 (RA 2012)Method of air sampling and analysis (second Edition ), APHA INTERSOCIETY COMMITTEE – 704

4 µg/m3 to 1000 µg/m3

Nitrogen oxides(as NO2) IS 5182(Part 6): 2006 (RA 2012) Method of air sampling and analysis (second Edition ), APHA INTERSOCIETY

10 µg/m3 to 1000µg/m3

Anita RaniConvenor










COMMITTEE – 408 Ambient Air Monitoring/ Fugitive Emission Monitoring

Ozone (as O3) IS 5182 (Part 9): 1974 (RA 2012) Methods of Air Sampling and Analysis (Second Edition) APHA INTERSOCIETY COMMITTEE-820

2.0 µg /m3 to 1.0mg/ m3

Mercaptans ASTM D-2913 2 µg/m3 to 200 µg/m3

Chlorine IS 5182 (Part 19): 1982 (RA 2014) 145 µg/m3 to 2900 µg/m3

Ammonia Method of air sampling and Analysis (second Edition) APHA INTERSOCIETY COMMITTEE- 401

20 µg/m3 to 700 µg/m3

Carbon Monoxide IS 5182(Part 10) 1999(RA 2014)

50 µg/m3 to 10 mg/m3

Hydrogen Sulphide IS 5182 (Part 7): 1973 (RA 2014) Method of air Sampling and Analysis (Second Edition) APHA INTERSOCIETY COMMITTEE-701

1 µg/m3 to 100 µg/m3

Benzo (a) pyrene IS 5182 (Part 12): 2004 (RA 2014) USEPA Method (TO-13)

0.1 µg/m3 to 10 µg/m3

Benzene (C6 H6) IS 5182 (Part 11): 2006 1.0 µg/m3 to 10 µg/m3

Aluminum as Al USEPA Method –IO 3.4 0.1 µg/m3 to 100 µg/m3

Anita RaniConvenor










Antimony as Sb

Barium as BaCadmium as Cd

Ambient Air Monitoring/ Fugitive Emission Monitoring

Lead as Pb

Manganese as Mn

Zinc as Zn

Nickel as Ni USEPA Method- IO 3.4 1 µg/m3 to 100 µg/m3

Arsenic as Ni

Mercury as As

Iron as Fe

Total Chromium

Volatile Organic Compounds

USEPA Method to 17 0.1 µg/m3 to 1.0 µg/m3

Benzene BromobenzeneBromochloromethane BromodichloromethaneBromoformn-butylbenzene

Anita RaniConvenor










sec-butylbenzenetert-butylbenzenecarbon tetrachloridechlorobenzenechloroform2-chlorotoluene4- chlorotolueneDibromochloromethane 1,2-dibromo-3Chloropropane


1,2-dibromoethaneDibromomethane1,2-dichlorobenzene1,3- dichlorobenzene1,4- dichlorobenzene1,1-dichloroethane1,2-dichloroethane1,1-dichloroetheneCis-1,2-dichloroetheneTrans-1,2- dichloroethene1,2-dichloropropane1,3- dichloropropane2,2- dichloropropane1,1- dichloropropaneCis-1,3- dichloropropaneTrans-1,3- dichloropropaneEthylbenzeneHexachlorobutadieneIsopropylbenzene

p-isopropyltoluene

Anita RaniConvenor











dichloromethane naphthalenepropylbenzenestyrene1,1,1,2-tetrachloroethane1,1,1,2-tetrachloroethaneTetrachloroethaneToluene1,2,3-trichlororbenzene1,2,4-trichlorobenzenw1,1,1-trichloroethane1,1,2-trichloroethaneTrichloroethene1,2,3-trichloropropropane1,2,4-1,1,1,2-tetrachloroethane1,3,5-1,1,1,2-tetrachloroethane

o-Xylene, Xylene, p-Xylene, Bromomethane, Chlorethane, Dichlorodifluoromethane, Trichlorfluoromethane, Vinyl chloride

2. Stack Emission Monitoring/ Gaseous Pollutants

Particulate matter IS 11255 (Part 1): 1985 (RA 2014) USEPA Method -1,2,3,4,5

5 mg/Nm3 to 100 mg/Nm3

Moisture USEPA Method 4 1 % to 50 %

Anita RaniConvenor










Sulphur dioxide(as SO2) IS 11255 (Part 2): 1985 (RA 2014) Flue Gas Analyzer USEPA Method 6

3 mg/Nm3 to 80000mg/Nm3

Nitrogen oxides (NOx) Flue Gas Analyzer/ USEPA Method-7


CO USEPA Method 10 1 ppm to 10000 ppm

CO2 USEPA Method 3A 0.1 % to 20 %

O2 USEPA Method 3A 0.1 % to 20 %

Total hydrocarbons (as CH4) USEPA Method 3C 5 ppm to 5000 ppm

Mercaptans ASTM D 2913 2 µg/Nm3 to 200 µg/Nm3

Stack Emission Monitoring/ Gaseous Pollutants

Ammonia Method of air sampling and Analysis (second Method ) APHA INTERSOCIETY COMMITTEE 401


Hydrogen Chloride USEPA 26 A 0.01 mg/Nm3 to 100 mg/Nm3

Hydrogen Fluoride USEPA 26 A 0.01 mg/Nm3 to 100 mg/Nm3

Hydrogen Cyanide USEPA Method 33 0.01 mg/Nm3 to 100 µg/Nm3

Anita RaniConvenor










Hydrogen Sulphide USEPA Method 11 8 mg/Nm3 to 740mg/Nm3

Aluminum as AlAntimony as SbCadmium as CdChromium as CrCobalt as CoCopper as Cu

USEPA Method 29 0.1µg/m3 – 100 µg/m3

Dioxin - Polychlorinated dibenzodioxin and Furan-polychlorinated dibenzodifuran (PCDD/PCDF)

USEPA 8290 (page.no.1-71)/ 1613 (page.no.1-86) by using high resolution gas chromatography /high resolution mass spectrometer

0.001 µg/m3 to 10 µg/m3

(as per WHO TEF)

Mercury as HgLead as Pb

Manganese as Mn Stack Emission Monitoring/ Gaseous Pollutants

Nickel as Ni

Zinc as Zn

Arsenic as As

Barium as Ba

Anita RaniConvenor










Selenium as Se

Polynuclear Aromatic Hydrocarbons

Acenaphthene CARB Method 429 0.01 to 10 µg/m3

AcenaphthyleneAnthraceneBenz(a) AnthraceneBenzo(a)pyrineBenz(b) fluorantheneBenzo(q,h,i)peryleneBenzo(k)FluorantheneChryseneDibenz(a,h)AnthraceneFluorantheneFluoreneIndeno(1,2,3-cd)PyrineNaphthalenePhenanthrenePyreneCarbazole


Volatile Organic CompoundsBenzene ,Bromobenzene, Bromochloromethane,

USEPA Method-0031-1996& 8260B-1996

0.01 – 10 µg/m3

Anita RaniConvenor










Stack Emission

Bromodichloromethane, Bromoform,n-Butylbenzene, sec-Butylbenzene tert-Butylbenzene ,Carbon tetrachloride, Chlorobenzene ,Chloroform,2-Chlorotoluene, 4-Chlorotoluene, Dibromochloromethane1,2-Dibromo-3-chloropropane, 1,2-Dibromoethane Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, cis-1,2-Dichloroethene, trans-1,2-Dichloroethene, 1,2-Dichloropropane, 1,3-Dichloropropane, 2,2-Dichloropropane, 1,1-Dichloropropene, cis-1,3-Dichloropropene,trans-1,3-Dichloropropene, Ethylbenzene,

Anita RaniConvenor










Monitoring/ Gaseous Pollutants

Hexachlorobutadiene, Isopropylbenzene, p-Isopropyltoluene, Dichloromethane,Naphthalene,Propylbenzene,Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, 1,2,3-Trichlororbenzene,1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, 1,2,3-Trichloropropane, 1,2,4-Trimethylbenzene, 1,3,5-Trimethylbenzene, o-Xylene,

m-Xylene,p-Xylene Bromomethane, Chloroethane, Chloromethane, DichlorodifluoromethaneTrichlorofluoromethane, Vinyl chloride,

USEPA Method-0031-1996 & 8260B -1996

0.01 µg/m3 to 10 µg/m3

Anita RaniConvenor











Polychlorinated Biphenyls2-Chlorobiphenyl2,3-Dichlorobiphenyl2,2’,3,3’,4,4’4’,6-Heptachlorobiphenyl2,2’,4,4’,5,6’-Hexachlorobiphenyl2,2’,3’,3’,4,5’,6,6’-Octachlorobiphenyl2,2’,3’,4,6-Pentachlorobiphenyl2,2’,4,4’-Tetrachlorobiphenyl2,4,5-Trichlorobiphenyl

CARB Method-428-1990 0.01 µg/m3 to 10 µg/m3

Dioxins - Polychlorinated dibenzo-p-dioxins and Furans-polychlorinated dibenzofurans (PCDD and PCDF)2,3,7,8-TCDF1,2,3,7,8-PeCDF2,3,4,7,8-PeCDF1,2,3,4,7,8-HxCDF1,2,3,6,7,8-HxCDF2,3,4,6,7,8-HxCDF1,2,3,7,8,9-HxCDF1,2,3,4,6,7,8-HpCDF1,2,3,4,7,8,9-HpCDFOCDF2,3,7,8-TCDD

USEPA 8290-1994/ 1613-1994by using high resolution gas chromatography /high resolution mass spectrometer

0.001 to 10 µg/m3

(as per WHO TEF)

Anita RaniConvenor










1,2,3,7,8-PeCDD1,2,3,4,7,8-HxCDD1,2,3,6,7,8-HxCDD1,2,3,7,8,9-HxCDD1,2,3,4,6,7,8-HpCDDOCDD


Semi Volatile Organic CompoundsAcenaphtheneAcenaphthyleneAnthraceneAzobenzeneBenzo (a) anthraceneBenzo (a) pyrineBenzo (b) fluorantheneBenzo (G,H,I)peryleneBenzo (k) FluorantheneBenzyl butyl phthalate

USEPA Method 8270D-1998 0.01 to 10 µg/m3

Bis(2-chloroethoxy) methaneBis (2-chloroethyl) etherBis(2-chloroisopropyl) etherBis(2-ethylhexyl) phthalateCarbazoleChryseneDi-n-butyl phthalateDi-n-octyl phthalateDibenz (a,h) anthraceneDibenzofuran

Anita RaniConvenor











Diethyl phthalateDimethyl PhthalateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethaneIndeno (1,2,3,-CD) PyreneIsophoroneN-Nitrosodi –n-PropylamineN-NitrosodimethylamineNaphthaleneNitrobenzenePentachlorophenolPhenanthrenePhenolPyrene1,2-Dichlorobenzene1,2,4-Trichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene2-Chloronaphthalene2-Methyl-4,6-dinitrophenol2-methylnaphthalene2-Methylphenol2-Nitroaniline2-Nitrophenol2,4-Dichlorophenol2,4-Dimethylphenol

USEPA Method 8270D-1998 0.01 – 10 µg/m3

Anita RaniConvenor










2,4-Dinitrophenol2,4-Dinitrotoluene2,4,5-Trichlorophenol2,4,6-Trichlorophenol2,6 – Dinitrotoluene

3-Nitroaniline4-Bromophenylphenyl Ether4-Chloro-3-Methylphenol4-Chloroaniline4-Chlorophenyl ether4-Methylphenol4-Nitroaniline4-Nitrophenol

3. Noise Pollution Monitoring

L10, L50, L90, Ldn, Ld, Ln& Leq IS 9989 – 1981 (Reaffirmed 2001) 10 dB(A) to 130 dB(A)

V. POLLUTION & ENVIRONMENT

1. Solid Waste Volatile Organic Compounds (BenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformn-butylbenzeneSec-butylbenzeneTert-butylbenzeneCarbon tetrachloride

EPA 8260 B/ APHA (21th Edition)EPA 524.2

1.0 mg/kg to 10 mg/kg(For each individual residue)

Anita RaniConvenor










ChlorobenzeneChloroform2-chlorotoluene4-chlorotolueneDibromochloromethane1,2-dibromo-3-chloropropane1,2-dibromoethaneDibromomethane1,2-dichlorobenzene1,3-dichlorobenzene1,4-dichlorobenzene1,1-dichloroethane1,2-dichloroethane1,1-dichloroetheneCis-1,2-dichloroetheneTrans-1,2-dichloroethene1,2-dichloropropane1,3-dichloropropane2,2-dichloropropane1,1-dichloropropeneCis-1,3- dichloropropeneTrans-1,3- dichloropropeneEthylbenzeneHexachlorobutadieneIsopropylbenzenep-isopropyltolueneDichloromethaneNaphthalenePropylbenzeneStyrene

Solid Waste

Anita RaniConvenor










1,1,1,2-tetrachloroethane1,1,2,2-tetrachloroethaneTetrachloroethene Toluene1,2,3-trichlorobenzene1,2,4- trichlorobenzene1,1,1-trichloroethane1,1,2-trichloroethaneTrichloroethene1,2,3-trichloropropane1,2,4-trimethylbenzene1,3,5-trimethylbenzeneo-XyleneM&P-XyleneBromomethaneChloroethaneChloromethaneDichlorodifluoromethaneTrichlorofluoromethaneVinyl chloride)

2. ETP Biosolid/ Spent Carbon

PCDD/PCDF EPA 1613 Rev B (1994) 0.025 pg/g to 50.0 pg/g

Benzene, Carbon Tetrachloride,Chlordane, Chlorobenzene,Chloroform,

Method Validation No: VLS-TAL/TCLP-R/001 (Based on EPA 1311)


Anita RaniConvenor










ETP Biosolid/ Spent Carbon

2,4-D,1,4-Dichlorobenzene,1,2-Dichloroethane,1,1-Dichloroethylene,2,4-Dinitro Toulene,Endrin,Heptachlor,Hexachlorobenzene,Trichlorophenol,2,4,6-Trichlorophenol,Vinyl Chloride,2,4,5-TP,Hexachlorobutadiene,Hexachloroethane,Lindane,Methoxychlor,Methyl ethyl ketone,Nitrobenzene,Phenol,PCBs,Pyridine,Tetrachloroethylene,Toxaphene,Trichloroethylene,Pentachlorophenol,o-Cresol,m-Cresol,p-Cresol

Polynuclear Aromatic EPA-8310 0.1 mg/kg to 2.0 mg/kg

Anita RaniConvenor










Hydrocarbons(Acenaphthene,Acenaphthylene,anthracene,benz(a)anthracene,benzo(a)pyrene,benzo(b)flouroanthene,benzo(g,h,i)perylene,benzo(k)fluoranthene chrysene,dibenz(a,h)anthracene fluoranthene,fluorene indeno(1,2,3-cd)pyreneNaphthalene,phenanthrene,pyrene)

APHA (21st Edition)

3. Liquid Effluents/ Waste water/ Trade Effluents/ Sewage Effluents

pH APHA-22nd ed.(4500-H+-B)2012 / Portable on-site testing kit

1 to 13

Conductivity APHA-22nd ed.( (2510-B) (Page.no-54)-2012/ Portable on-site testing kit

10 µs/cm to 90000 µs/cm

Dissolved oxygen Wrinkler’s method, APHA-22nd ed.(4500-O-C) / Portable on-site testing kit

1 mg/L to 9 mg/L

Color Pt-Co APHA-22nd ed. (2120-C) -2012 1unit-500 units

Anita RaniConvenor










Liquid Effluents/ Waste water/ Trade Effluents/ Sewage Effluents

Temperature APHA-22nd ed. (2550-B)-2012 0 to 50 °C

Total Residual Chlorine APHA-22nd ed. (4500-Cl) -2012 0.1 mg/L to 2.0 mg/L

Arsenic as As APHA-22nded. 3120 B -2012 0.01 mg/L to 10 mg/L

Mercury as Hg USEPA 200.8 -1994 0.001 mg/L to 1.0 mg/L

Lead as Pb APHA-22nded. 3120 B -2012 0.01 mg/L to 10 mg/L

Cadmium as Cd APHA-22nded. 3120 B -2012 0.01 mg/L to 10 mg/L

Copper as Cu APHA-22nded. 3120 B -2012 0.01 mg/L to 10 mg/L

Total Chromium APHA-22nded. 3120 B-2012 0.01 mg/L to 10 mg/L

Zinc APHA-22nded 3120 B -2012 0.01 mg/L to 10 mg/L

Selenium as Se APHA-22nded. 3120 B -2012 0.01 mg/L to 10 mg/L

Nickel as Ni APHA-22nded. 3120 B -2012 0.01 mg/L to 10 mg/L

Boron as B APHA-22nded. 3120 B -2012 0.01 mg/L to 10 mg/L

Percent Sodium APHA-22nded. (3500 (Na-C &D, Ca-C&D, Mg-C&D, K-C&D) 2012

0.1 % to 95 %

Residual Sodium Carbonate APHA-22nded. (2340-C, 2320-B)- 2012

0.1 % to 95 %

Anita RaniConvenor










Fluoride APHA-22nded.(4500-F B,C,D) – 2012

0.1 mg/L to 19 mg/L


Chloride APHA-22nded.(4500–Cl B) – 2012 >1.0 mg/L

Phenolic Compounds APHA-22nded.(5530 Phenol-C)APHA-22nded.(5530 Phenol-D) – 2012

0.001 mg/L to 0.1 mg/L

Manganese APHA-22nded.(3120 B/3125B) – 2012


Vanadium APHA-22nded.(3120 B) – 2012 0.01 mg/L to 10 mg/L

Cobalt APHA-22nded.(3120 B/3125B) – 2012


Suspended Solids APHA-22nd ed. (2540-D) - 2012 1.0 mg/L to 20000 mg/L

Dissolved solids APHA-22nd ed. (2540-C) – 2012

Volatile Solids APHA-22nd ed. (2540-E) – 2012

Total Solids APHA-22nd ed. (2540-B) – 2012

Total Fixed Solids APHA-22nd ed. (2540-E) – 2012

Turbidity APHA-22nd ed. (2130-B) – 2012 >1 NTU

Anita RaniConvenor










Oil and Grease APHA-22nd ed. (5520 B & C) – 2012

1.0 to 50000 mg/L

Total Kjeldahl Nitrogen APHA-22nd ed. 4500-Norg-B – 2012

1.0 -10000 mg/L

Free Ammonia APHA-22nd ed. (4500-NH3,F) - 2012

0.1 -0.6 mg/l


Nitrate Nitrogen APHA-22nd ed.(4500- NO3,B,E) - 2012

0.1 -11 mg/l

Ammonical Nitrogen APHA-22nd ed.(4500-NH3,B,C) – 2012

> 1 mg/l

Phosphorus as P APHA – 22nd ed. (4500-P,C) – 2012

0.1 to 1.0 mg/L

Phosphate as PO4 APHA – 22nd ed. (4500-P,D) – 2012

1.0 to 20 mg/L

Kjeldahl Nitrogen APHA-22nd ed.(4500-NH3,B,C) – 2012

>1.0 mg/L

Iron APHA-22nded.(3120 B/3125B) – 2012


Total Petroleum Hydrocarbon (n-Hexane extractable Matter)

ASTM D-7678-11 0.001 % to 10 %

Anita RaniConvenor










Hexavalent Chromium APHA – 22nd ed. (3500-Cr B) – 2012

0.02 mg/L to 2.0 mg/L

Sulphates as SO4 APHA – 22nd ed. (4500-SO42- D,

E) – 2012 IS 3025 (Part 24)0.5 mg/L to 40 mg/L10 mg/L to 10000 mg/L

Sulfide APHA – 22nd ed. (4500-S2- D,F) - 2012

0.1 mg/L to 20 mg/L5.0 mg/L to 100 mg/L

Nitrite as NO2 APHA – 22nd ed. (4500-NO2- B) –

20120.005 mg/L to 0.2 mg/L


Cyanide APHA-22nd ed. (4500-CN ,B,C,D) – 2012

1 mg/L to 10 mg/L

Chloride APHA-22nd ed.(4500-Cl-B) - 2012 10 mg/L to 1000 mg/L

Fluoride APHA-22nd ed. (4500-F-C) - 2012 1 mg/L to 1900 mg/L

APHA-22nd ed. 4500-F-D) – 2012 0.1 mg/L to 1.4 mg/L

Potassium APHA-22nd ed. -(3500-K-C&D) – 2012

0.1 mg/L to 1000 mg/L

Calcium APHA-22nded. (3500-Ca-C&D) – 2012

1 mg/L to 1000 mg/L

Magnesium APHA-22nd ed. -(3500-Mg-C&D) – 2012

1 mg/L to 1000 mg/L

Anita RaniConvenor










Alkalinity APHA-22nd ed. -(2320-B) – 2012 10 mg/L to 1000 mg/L

Hardness APHA-22nd ed. -(2340-C) - 2012 10 mg/L to 1000 mg/L

Biochemical Oxygen Demand 3 day at 27 °C

IS:3025(Part-44)-2000 3 mg/L to 1000 mg/L

Biochemical Oxygen Demand 5 day at 20 °C

APHA-22nd ed. -(5210-B) - 2012 3 mg/L to 1000 mg/L

Chemical Oxygen Demand APHA-22nd ed. (5220-B) - 2012 5 mg/L to 50000 mg/L

4. Solids/Solid Wastes /Soils/ Scale, Hazardous Solid Waste, Toxic Waste

pH ASTM D- 4980-89 1 to 13

Total Nitrogen ASTM E-778-08 5 mg/kg to 1000 mg/kg

Electrical Conductivity ASTM D-5334-14/ USEPA Method 9100-1986

1 µs/cm to 10000 µs/cm

Total Sulphur ASTM E-775-87(2008) e1 5 mg/kg to 1000 mg/kg

Available Nitrogen Soil Chemical Analysis by M.L Jackson (soil) Page No.181-191


Ammonical Nitrogen Soil Chemical Analysis by M.L 10 mg/kg to 1000 mg/kg

Anita RaniConvenor










Jackson (soil)Page No.189-191

Available Phosphorus Soil Chemical Analysis by M.L Jackson (soil)Page No.151-157


Total Phosphorus USEPA 3050 B-1996 10 mg/kg to 1000 mg/kg

Exchangeable Sodium, Potassium, Calcium, Magnesium

Soil Chemical Analysis by M.L Jackson (soil)Page No. 83 – 109


Water Extractable Chlorides, Sulphates

ASTM C -871-11e1, ASTM D – 516-11 (1-6)


Total Nitrogen Soil Chemical Analysis by M.L Jackson (soil) , Page No. 183-197, USEPA– 440-1997


Solids/Solid Wastes /Soils/ Scale, Hazardous Solid Waste, Toxic Waste

Arsenic as As USEPA 3050 B-1996/ 3060 A-1996/7196 A-1992/ ASTM D-5198-09


Mercury as Hg

Selenium as SeAluminum as AlAntimony as SbBarium as Ba

Anita RaniConvenor










Lead as PbCadmium as CdCopper as CuNickel as NiChromium- Cr3+

Zinc as ZnVanadium, Cr6+

Beriyllium as BeCobalt as CoThallium as TlTin as SnVolatile Organic Compounds

EPA –8260 B-1996 0.1 mg/kg to 100 mg/kg


Benzene ,Bromobenzene, Bromochloromethane, Bromodichloromethane, Bromoform,n-Butylbenzene, sec-Butylbenzene tert-Butylbenzene ,Carbon tetrachloride, Chlorobenzene ,Chloroform,2-Chlorotoluene, 4-Chlorotoluene, Dibromochloromethane1,2-Dibromo-3-

Anita RaniConvenor










Solids/Solid Wastes /Soils/ Scale, Hazardous Solid

chloropropane, 1,2-Dibromoethane Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, cis-1,2-Dichloroethene, trans-1,2-Dichloroethene, 1,2-Dichloropropane, 1,3-Dichloropropane, 2,2-Dichloropropane, 1,1-Dichloropropene, cis-1,3-Dichloropropene,trans-1,3-Dichloropropene, Ethylbenzene, Hexachlorobutadiene, Isopropylbenzene, p-Isopropyltoluene, Dichloromethane,Naphthalene,Propylbenzene,Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, 1,2,3-Trichlororbenzene,

Anita RaniConvenor










Waste, Toxic Waste

1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, 1,2,3-Trichloropropane, 1,2,4-Trimethylbenzene, 1,3,5-Trimethylbenzene, o-Xylene,m-Xylene,p-Xylene Bromomethane, Chloroethane, Chloromethane, DichlorodifluoromethaneTrichlorofluoromethane, Vinyl chloride,Semi Volatile Organic Compounds AcenaphtheneAcenaphthyleneAnthraceneAzobenzeneBenzo (a) anthraceneBenzo (a) pyrineBenzo (b) fluorantheneBenzo (G,H,I)peryleneBenzo (k) FluorantheneBenzyl butyl phthalateBis(2-chloroethoxy) methaneBis (2-chloroethyl) ether

USEPA 8270 D-1998 0.1 ppm to 100 ppm

Anita RaniConvenor











Bis(2-chloroisopropyl) etherBis(2-ethylhexyl) phthalateCarbazoleChryseneDi-n-butyl phthalateDi-n-octyl phthalateDibenz (a,h) anthraceneDibenzofuranDiethyl phthalateDimethyl PhthalateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethaneIndeno (1,2,3,-CD) PyreneIsophoroneN-Nitrosodi –n-PropylamineN-NitrosodimethylamineNaphthaleneNitrobenzenePentachlorophenolPhenanthrenePhenolPyrene1,2-Dichlorobenzene1,2,4-Trichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene

Anita RaniConvenor











2-Chloronaphthalene2-Methyl-4,6-dinitrophenol2-methylnaphthalene2-Methylphenol2-Nitroaniline2-Nitrophenol2,4-Dichlorophenol2,4-Dimethylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,4,5-Trichlorophenol2,4,6-Trichlorophenol2,6 – Dinitrotoluene3-Nitroaniline4-Bromophenylphenyl Ether4-Chloro-3-Methylphenol4-Chloroaniline4-Chlorophenyl ether4-Methylphenol4-Nitroaniline4-NitrophenolPolynuclear Aromatic Hydrocarbons

EPA- 8310-1986 0.1 ppm to 10.0 ppm

Poly Chlorinated Biphenyls :Mono-chlorobiphenyl, Dichlorobiphenyl, Trichlorobiphenyl, tetrachloro-biphenyl, penta-chlorobiphenyl, Hexa-

USEPA 8082 -1996 0.1 mg/kg to 10.0 mg/kg

Anita RaniConvenor










chlorobiphenyl, Hepta-chlorobiphenyl and octachlorobiphenyl

Toxicity Characteristic Leachate Procedure (TCLP)

USEPA 1311 -1992

Arsenic as As 0.01 mg/L to 20 mg/L


Mercury as Hg 0.001 mg/L to 5 mg/L

Selenium as Se 0.01 mg/L to 20 mg/LSilver as Ag 0.01 mg/L to 20 mg/LChromium as Cr 0.01 mg/L to 20 mg/LBarium as Ba 0.01 mg/L to 20 mg/LLead as Pb 0.01 mg/L to 20 mg/LCadmium as Cd 0.01 mg/L to 20 mg/LOrganic CompoundsBenzene 0.001 mg/kg to 0.2 mg/kgCarbon Tetrachloride 0.001 mg/kg to 0.2 mg/kgChloroform 0.001 mg/kg to 0.2 mg/kgHexachlorobenzene 0.001 mg/kg to 0.2 mg/kgLindane 0.001 mg/kg to 0.2 mg/kgPyridine 0.001 mg/kg to 0.2 mg/kgMethyl ethyl ketone 0.001 mg/kg to 0.2 mg/kg

Grass Calorific Value ASTM E 711-87(1996) 200 kcal/kg to 10000 kcal/kg

Anita RaniConvenor










Moisture ASTM E871-82(2013) 0.1% to 90 %

Ash ASTM E872-82(2013) / ASTM E 830-87(1996)

0.1 % to 95 %

Volatile Matter ASTM E 897-88(1998) 0.1 % to 95 %

Total Petroleum Hydrocarbon (n-Hexane extractable Matter)

USEPA 9071 B -1998 0.001 % to 10 %


Total Potassium USEPA 3050 B -1996 & USEPA 6020 A -1998


Fluoride USEPA 9056 -1994 5 mg/kg to 1.0 %

Total Organic Carbon USEPA 415.1 0.01 % to 10 %

VI. INDUSTRIAL AND FINE CHEMICALS

1. Calcium Chloride Description IS 1314: 1984 (RA 2010) NA

Assay IS 1314: 1984 (RA 2010)& AWWA B550: 2010

1 % to 100 %

Fluoride EPA-300.1 1 mg/kg to 100 mg/kg

Arsenic SOP No:01/11 , 2014.05.15 0.1 mg/l to 100 mg/l

Anita RaniConvenor










Issue No.6.0 NSF 60Lead SOP No: 26/03

2014/07/21Issue No.3.0 NSF 60

0.015 mg/l

Chlorides IS 1314: 1984 (RA 2010) 0.01 % to 5 %

Total heavy metals SOP No: 26/03, 2014/07/21Issue No.3.0


Identification FCC, Pg. No: 165 NA

Magnesium and Alkali salts IS 1314: 1984 (RA 2010) & FCC 0.01 to 3.0

pH of a 5%Solution at 25°C IS 1314: 1984 (RA 2010) & FCC 4.5 to 11.0

Calcium Chloride Water insoluble matter IS 1314: 1984 (RA 2010)& AWWA B550: 2010

0.01 % to 10 %

Bromide EPA-300.1 1 mg/kg to 100 mg/kg

2. Sodium Chloride Description IS 4408: 1979 (RA 2010) NA

Assay IS 4408: 1979 (RA 2010) & AWWA B200: 2012

1 % to 100 %

Calcium and Magnesium AWWA B200: 12pg no8-10

0.001 % to 10 %

Anita RaniConvenor










Moisture IS 4408: 1979 (RA 2003)AWWA B200: 2012

0.01 % to 100 %

Matter insoluble in water other than NaCl

IS 253: 2014 (RA 2009) 0.1 % to 50%

Sulphates IS 253: 2014USP, pg. No:4653

0.01 % to 10 %

Water insoluble matter IS 253: 2014 0.01 % to 10 %

Arsenic SOP No: 26/20, 2013.10.28Issue No.1.0 EN 973


Lead SOP No: 26/20, 2013.10.28Issue No.1.0 EN 973


Cadmium SOP No: 26/20, 2013.10.28Issue No.1.0 EN 973


Sodium Chloride Chromium SOP No: 26/20, 2013.10.28Issue No.1.0 EN 973


Mercury SOP No:01/35, 2014.10.08Issue No.2.0 EN 973


Antimony SOP No: 26/20, 2013.10.28Issue No.1.0 EN 973


Anita RaniConvenor










Selenium SOP No: 01/11, 2014.05.15Issue No.6.0 & EN 973


Nickel SOP No: 26/20, 2013.10.28Issue No.1.0 EN 973


Iron SOP No: 26/20, 2013.10.28Issue No.1.0 EN 973


Copper SOP No: 26/20, 2013.10.28Issue No.1.0 EN 973


Anti-caking agent FCC: 1023 0.1 % to 1%

Antimony NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.006 mg/l

Arsenic NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.010 mg/l

Barium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

2.0 mg/l

Beryllium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.004 mg/l

Sodium Chloride Cadmium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.005mg/l

Chromium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.1 mg/l

Anita RaniConvenor










Copper NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

1.3 mg/l

Lead NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.015 mg/l

Mercury NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.002 mg/l

Selenium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.05 mg/l

Thallium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.002 mg/l

Bromide NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

10.0 mg/l

3. Soda Ash Description IS 6135: 1981 (RA 2010) NA

Assay IS 6135: 1981 (RA 2010) 1 % to 100 %

Matter insoluble in water IS 6135: 1981 (RA 2010) 0.01 % to 10 %

Sulphates IS 6135: 1981 (RA 2010) 0.01 % to 10 %

Chlorides IS 6135: 1981 (RA 2010) 0.01 % to 5 %

Soda Ash Arsenic SOP No: 26/201,2013.10.28 0.1 mg/kg to 100 mg/kg

Anita RaniConvenor










Issue No. 1.0 EN 987

Lead SOP No: 26/201,2013.10.28Issue No. 1.0 EN 987


Cadmium SOP No: 26/201,2013.10.28Issue No. 1.0 EN 987


Chromium SOP No: 26/201,2013.10.28Issue No. 1.0 EN 987


Mercury SOP No: 01/35,2014.10.08Issue No.2.0


Nickel SOP No: 26/201,2013.10.28Issue No. 1.0 EN 987


Iron SOP No: 26/201,2013.10.28Issue No. 1.0 EN 987


Antimony NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.006 mg/l

Arsenic NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.010 mg/l

Barium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

2.0 mg/l

Beryllium NSF 60, SOP No. 01/11 0.004 mg/l

Anita RaniConvenor










2014.05.15 Issue No.6.0

Soda Ash Cadmium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.005 mg/l

Chromium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.1 mg/l

Copper NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

1.3 mg/l

Lead NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.015 mg/l

Mercury NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.002 mg/l

Selenium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.05 mg/l

Thallium NSF 60 SOP No. 01/11,2014.05.15Issue No.6.0

0.002 mg/l

4. Ferrous Sulphate Description IS 262: 1982 (RA 2010) NA

Assay IS 262: 1982 (RA 2010) 1 % to 100 %

Free Sulfuric acid AWWA B-402: 2012 0.1 % to 10 %

Anita RaniConvenor










Insoluble matter IS 262: 1982 (RA 2010) & AWWA B-402: 2012

0.01 % to 10 %

Manganese SOP No: 26/23 2013/10/28Issue No.1.0 & EN-889


Ferrous Sulphate Titanium SOP No: 26/23 2013/10/28Issue No.1.0 & EN-889


Arsenic SOP No:01/11 2014.05.15Issue No.6.0 & EN-889


Lead SOP No: 26/23, 2013/10/28Issue No.1.0 & EN-889


Cadmium SOP No: 26/23, 2013/10/28Issue No.1.0 & EN-889


Chromium SOP No: 26/232013/10/28Issue No.1.0 & EN-889


Mercury SOP No:01/11 2014.05.15Issue No.6.0 & EN-889


Antimony SOP No:01/11, 2014.05.15Issue No.6.0 & EN-889


Selenium SOP No: 26/23, 2013/10/28Issue No.1.0 & EN-889


Anita RaniConvenor










Nickel SOP No: 26/23, 2013/10/28Issue No.1.0 & EN-889


Antimony NSF 60, SOP No:01/112014.05.15 Issue No.6.0

0.006 mg/l

Arsenic NSF 60, SOP No:01/112014.05.15 Issue No.6.0

0.010 mg/l

Ferrous Sulphate Barium NSF 60, SOP No:01/112014.05.15 Issue No.6.0

2.0 mg/l

Beryllium NSF 60, SOP No:01/112014.05.15 Issue No.6.0

0.004 mg/l

Cadmium NSF 60, SOP No:01/112014.05.15 Issue No.6.0

0.005 mg/l

Chromium NSF 60, SOP No:01/112014.05.15 Issue No.6.0

0.1 mg/l

Copper NSF 60, SOP No:01/112014.05.15 Issue No.6.0

1.3 mg/l

Lead NSF 60, SOP No:01/112014.05.15 Issue No.6.0

0.015 mg/l

Mercury NSF 60, SOP No:01/11 0.002 mg/l

Anita RaniConvenor










2014.05.15 Issue No.6.0

Selenium NSF 60, SOP No:01/112014.05.15 Issue No.6.0

0.05 mg/l

Thallium NSF 60, SOP No:01/112014.05.15 Issue No.6.0

0.002 mg/l

5. Lime Description IS 1540 (Part 1): 1989(RA 2010)

NA

Assay IS 1540 (Part 1): 1980(RA 2010)FCC: 171

1 % to 100 %

Lime Magnesium IS 1540 (Part 2): 1990(RA 2010)

0.1 % to 10 %

Iron oxide IS 1540 (Part 2): 1990 (RA 2010) & EN-12518

0.01 % to 10 %

Alumina as Al203 IS 1540 (Part 2): 1990(RA 2010) &-12518

0.01 % to 10 %

Dead burnt lime (as CaO) IS 1540 (Part 1): 1980(RA 2010)

0.1 % to 10 %

Carbon Dioxide IS 1540 (Part 2): 1990(RA 2010)

0.1 % to 10 %

Anita RaniConvenor










Acid insoluble ash FCC, Pg. No: 172 0.01 % to 10 %

Free water ASTM C-471 0.05 % to 10 %

Arsenic SOP No:01/35, 2014.10.08Issue No.2.0 & EN-12518


Lead SOP No: 26/20, 2013/10/28Issue No 1.0 & EN-12518


Cadmium SOP No: 26/20,2013/10/28,Issue No.1.0 & EN-12518


Chromium SOP No: 26/20,2013/10/28Issue No.1.0 & EN-12518


Mercury SOP No:01/35,2014.10.08Issue No.2.0 & EN-12518


Lime Nickel SOP No: 26/20,2013/10/28,Issue No.1.0 & EN-12518


Iron SOP No: 26/20,2013/10/28,Issue No.1.0& EN-12518


Antimony SOP No:01/35,2014.10.08Issue No.2.0&EN-12518


Selenium SOP No:01/35,2014.10.08Issue No.2.0&EN-12518


Anita RaniConvenor










Barium SOP No: 26/20,2013/10/28,Issue No.1.0& EN-12518


Manganese SOP No: 26/20,2013/10/28,Issue No.1.0&EN-12518


Sulphates IS 1540(Part 1): 1990 (RA 2010)

0.01 % to 10 %

Moisture IS 1540 (Part 2): 1990(RA 2010)

0.01 % to 100 %

Fluoride EPA-300.1 1 mg/kg to 100 mg/kg

Antimony NSF 60,SOP No.01/112014.05.15 Issue No. 6.0

0.006 mg/l

Arsenic NSF 60,SOP NO.01/112014.05.15 Issue No.6.0

0.010 mg/l

Barium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

2.0 mg/l

Lime Beryllium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.004 mg/l

cadmium NSF 60, SOP No,01/112014.05.15 Issue No.6.0

0.005 mg/l

Chromium NSF 60, SOP No.01/11 0.1 mg/l

Anita RaniConvenor










2014.05.15 Issue No.6.0

Copper NSF 60, SOP No.01/112014.05.15 Issue No.6.0

1.3 mg/l

Lead NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.015 mg/l

Mercury NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.002 mg/l

Selenium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.05 mg/l

thallium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.002 mg/l

6. Calcium Hypochlorite

Description IS 1065: 1989 (RA 2010) NA

Assay IS 1065: 1989 (RA 2010)AWWA B-300-10, pg no:6

1 % to 100 %

Arsenic SOP No:01/35,2014/10/08,Issue No.2.0 EN 900


Lead SOP No:01/35,2014/10/08,Issue No.2.0 EN 900


Calcium Hypochlorite

Cadmium SOP No:01/35,2014/10/08,Issue No.2.0 EN 900


Chromium SOP No:01/35,2014/10/08, 0.1 mg/kg to 100 mg/kg

Anita RaniConvenor










Issue No.2.0 EN 900

Mercury SOP No:01/35,2014/10/08,Issue No.2.0 EN 900


Nickel SOP No:01/35,2014/10/08,Issue No.2.0 EN 900


Iron SOP No:01/35,2014/10/08,Issue No.2.0 EN 900


Antimony SOP No:01/35,2014/10/08,Issue No.2.0 EN 900


Selenium SOP No:01/35,2014/10/08,Issue No.2.0 EN 900


Manganese SOP No:01/35,2014/10/08,Issue No.2.0 EN 900


Bromate ion EPA 300.1 1.0 mg/kg to 100 mg/kg

Chlorite ion EPA 300.1 1.0 mg/kg to 100 mg/kg

pH at 10g/l & 45g/l sol EN 900: 2007 10 to 14

Stability, Lossof chlorine on the basis of initial available chlorine

IS 1065: 1989 (RA 2010) 0.1 % to 10 %

Moisture IS 1065 : 1989 (RA 2010) 0.01 % to 100 %

Anita RaniConvenor











Insoluble in water EN 900: 2007, pg.No:8 0.01 % to 10 %

Antimony NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.006 mg/l

Arsenic NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.010 mg/l


2.0 mg/l

Beryllium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.004mg/l

Cadmium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.005 mg/l

Chromium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.1 mg/l

Copper NSF 60, SOP No.01/112014.05.15 Issue No.6.0

1.3 mg/l

Lead NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.015 mg/l

Mercury NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.002 mg/l

Selenium NSF 60, SOP No.01/11 0.05 mg/l

Anita RaniConvenor










2014.05.15 Issue No.6.0

Thallium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.002 mg/l


Bromate NSF 60 0.01 mg/l

Chlorate NSF 60 1.0 mg/l

7. Sodium Hydroxide Description IS 252: 2013 NA

Assay IS 252: 2013 & AWWA B 501: 2013

1 % to 100 %

Alkali (Na2O) AWWA B-501: 2014 1 % to 80 %

Sodium carbonate IS 252: 2013 FCC, Pg.No: 1036 & ASTM E 291


Chlorides IS 252: 2003 10 mg/kg to 100 mg/kg

Sulphates IS 252: 2003 10 mg/kg to 100 mg/kg

Matter insoluble in water IS 252: 2003 0.01 % to 10 %

Iron SOP No: 26/20, 2013/10/28,Issue No.1.0 & ASTM E291


Mercury SOP No.01/35,2014.10.08Issue No.2.0& EN-896


Anita RaniConvenor










Nickel SOP No.01/35,2014.10.08Issue No.1.0&EN-896


Total heavy metals SOP No.01/35,2014.10.08Issue No.1.0&EN-896


Sodium Hydroxide Arsenic SOP No.01/35,2014.10.08Issue No.1.0&EN-896


Lead SOP No.01/35,2014.10.08Issue No.1.0&EN-896


Cadmium SOP No.01/35,2014.10.08Issue No.1.0 & EN-896


Antimony NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.006 mg/l

Arsenic NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.010 mg/l


2.0 mg/l

Beryllium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.004 mg/l

Anita RaniConvenor










Cadmium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.005 mg/l

Chromium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.1 mg/l

copper NSF 60, SOP No.01/112014.05.15 Issue No.6.0

1.3 mg/l

lead NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.015 mg/l

Sodium Hydroxide mercury NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.002 mg/l

selenium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.05 mg/l

thallium NSF 60, SOP No.01/112014.05.15 Issue No.6.0

0.002 mg/l

8. Phosphoric Acid Description IS 10508: 1983 (RA 2007) NA

Assay IS 10508: 1983 (RA 2007) 1 % to 100 %

Total heavy metals SOP No: 26/03, 2014/07/21Issue No. 3.


Alkali phosphates USP, Pg.No: 1891 NA

Anita RaniConvenor










Chlorides IS 798: 1986 (RA 2010) 10 mg/kg to 100 mg/kg

Phosphorous and Hypo Phosphorous

BP, Pg. No: 1726 NA

Sulphates IS 798: 1986 (RA 2003) 0.001 % to 10 %

Arsenic SOP No:01/35, 2014.10.08Issue No. 2.0 IS10508:1983 (RA 2007)


Lead SOP No:01/35, 2014.10.08Issue No. 2.0 IS10508:1983 (RA 2007)


Iron SOP No: 26/20, 2013/10/28Issue No. 1.0


Phosphoric Acid Fluoride EPA -300.1 1 mg/kg to 100 mg/kg

Antimony NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

0.006 mg/L

Arsenic NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

0.010 mg/L

Barium NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

2.0 mg/L

Beryllium NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

0.004 mg/L

Anita RaniConvenor










Cadmium NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

0.005 mg/L

Chromium NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

0.1 mg/L

Copper NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

1.3 mg/L

Lead NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

0.015 mg/L

Mercury NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

0.002 mg/L

Selenium NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

0.05 mg/L

Thallium NSF 60 2013, SOP No. 01/11 2014.05.15 Issue No. 6.0

0.002 mg/L

9. Powder Activated Carbon

Iodine number IS 2752: 1995 (RA 2010) 100 mg/g to 2000 mg/g

Moisture IS 877: 1989 (RA 2010) 0.01 % to 100 %

pH IS 8366/ ASTM-D3838 2 to 8

Water soluble material IS 877: 1989 (RA 2010) 0.01 % to 10 %

Anita RaniConvenor










Apparent density ASTM D 2854 0.05 g/ml to 5 g/ml

Total Ash IS 877: 1989 (RA 2010) 0.01 % to 100 %

Total Sulphide EPA376.2 50 ug/kg to 100 ug/kg

Zinc EN 12902: 2004, Pg no: 26


Water extractable Substances

Antimony EN12902:2004, Pg no:21SOP No: 01/11,2014/05/15 Issue No. 6.0

1.0 ug/kg to 100 ug/kg

Arsenic EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


Cadmium EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


Chromium EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


Powder Activated Carbon

Cyanide EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0

50 ug/kg to 500 ug/kg

Anita RaniConvenor










Lead EN12902:2004, Pg no:21SOP No. 01/11 2014.05.15 Issue No. 6.0


Mercury EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


Nickel EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


Selenium EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


10. Granular Activated Carbon(Water Treatment, Pesticide Removal)

Antimony EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


Arsenic EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


Cadmium EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


Chromium EN12902:2004, Pg no:20 1 ug/kg to 100 ug/kg

Anita RaniConvenor










SOP No. 01/11, 2014.05.15 Issue No. 6.0

Granular Activated Carbon(Water Treatment, Pesticide Removal)

Cyanide EN12902:2004, Pg no:20SOP No. 01/11, 2014.05.15 Issue No. 6.0


Lead EN12902:2004, Pg no:20SOP No. 01/11, 2014.05.15 Issue No. 6.0


Selenium EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


Nickel EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


Mercury EN12902:2004, Pg no:21SOP No. 01/11, 2014.05.15 Issue No. 6.0


11. Proximate AnalysisUltimate Analysis

Moisture IS 1350 (Part 1): 1984(RA 2008)

0.01 % to 100 %

Ash IS 1350 (Part 1): 1984(RA 2008)

0.01 % to 100 %

Volatile matter IS 1350 (Part 1): 1984(RA 2008)

0.01 % to 100 %

Anita RaniConvenor










Fixed carbon IS 1350 (Part 1): 1984 (RA 2008)

0.01 % to 100 %

Carbon SOP No:26/02, 2014/07/31 Issue No. 3.0, IS 1350 Part 4: 1974

0.004% to 100 %

Proximate AnalysisUltimate Analysis

Hydrogen SOP No:26/02, 2014/07/31 Issue No. 3.0 , IS 1350 Part 4: 1974

0.002% to 100 %

Nitrogen SOP No:26/02, 2014/07/31 Issue No. 3.0, IS 1350 Part 4: 1974

0.001 % to 100 %

Sulphur SOP No:26/02, 2014/07/31 Issue No. 3.0, , IS 1350 Part 3:1969

0.005 % to 100 %

Mineral matter IS 1350 part-1:1984SOP No:26/02, 2014/07/31 Issue No. 3.0

0.5 % to 100 %

Gross calorific value IS 1350 (Part 2): 1975(RA 2010)

(200 kcal to 14000 kcal)/kg

12. Used Oil V & VI Colour ASTM D1500:Pg no:596

Qualitative

Water ASTM D95 pg no:81 0.10% to 100 %

Density IS1448 (Part 32): 1992 (RA 2008) 0.1g/cc to 1.0 g/cc

Anita RaniConvenor










Kinematic viscosity at 100 °C

ASTM D-445 pg no: 195 1.0 cSt to 450 cSt

Neutralisation No IS 1448 (Part 1): 1971(RA 2010)

(0.01 mg KOH to 100 mg KOH)/gm

Saponificationvalue

ASTM D-94: pg no:73 (0.01mg KOH to 100 mg KOH)/gm

Total Halogens ASTM D808 pg no: 297 0.01 % to 100 %

Lead ASTM D5185 pg no: 1085 0.1 mg/kg to 100 mg/kg

Used Oil V & VI Arsenic ASTM D5185 pg no: 1085 0.1 mg/kg to 100 mg/kg

Cadmium + Chromium +Nickel

ASTM D5185 pg no: 1085 0.1 mg/kg to 100 mg/kg

Sediments ASTM D1796 pg no:680 0.01 % to 100 %

13. Hydrochloric Acid Antimony NSF 60,SOP No. 01/112014.05.15 Issue No. 6.0

0.006 mg/l

Arsenic NSF 60,SOP No. 01/112014.05.15, Issue No. 6.0

0.010 mg/l

Barium NSF 60,SOP No. 01/112014.05.15, Issue No. 6.0

2.0 mg/l

Beryllium NSF 60,SOP No. 01/112014.05.15 Issue No. 6.0

0.004 mg/l

Anita RaniConvenor










Cadmium NSF 60,SOP No. 01/112014.05.15 Issue No. 6.0

0.005 mg/l

Chromium NSF 60,SOP No. 01/112014.05.15 Issue No. 6.0

0.1 mg/l

Copper NSF 60,SOP No. 01/112014.05.15 Issue No. 6.0

1.3 mg/l

Lead NSF 60,SOP No. 01/112014.05.15 Issue No. 6.0

0.015 mg/l

Mercury NSF 60,SOP No. 01/112014.05.15 Issue No. 6.0

0.002 mg/l

Selenium NSF 60,SOP No. 01/112014.05.15 Issue No. 6.0

0.05 mg/l

Hydrochloric Acid Thallium NSF 60,SOP No. 01/112014.05.15 Issue No. 6.0

0.002 mg/l

14. Carbonated ores Loss on ignition IS 1760 part 1:1991 (RA 2011) 50 % max

Silica IS 1760 part 21991 (RA 2011) 0.01 % to 20 %

Alumina IS 1760 part 3:1992 (RA 2001) 0.2 % to 2.0 %

Iron Oxide IS 1760 part 3:1992 (RA 2011) 0.2 % to 2.0 %

Calcium Oxide IS 1760 part 3:1992 (RA 2001) 0.5 % to 55 %

Anita RaniConvenor










Magnesium Oxide IS 1760 part 3:1992 (RA 2001) 0.2 % to 52 %

VII. PLASTICS AND RESINS

1. Plastic Bottles/Containers

Migration Test (Containers)Migration of colour 11 of IS 9845 : 1998 Qualitative

Overall migration 5 of IS 9845 : 1998 0.5 to 60 mg/L or 0.5 mg/dm2 to 10 mg/dm2

Migration Test (Caps)Migration of colours 11 of IS 9845 : 1998 Qualitative

Overall migration 8 of IS 9845 : 1998 0.5 to 60 mg/L or 0.5 to 10 mg/dm2

Amount of extraction 8 of IS 9845 : 1998 0.5 to 10.0 mg/dm2

2. Polyethylene Flexible Pouches

Overall migration IS 9845 : 1998 0.5 to 10 mg/dm2 0.5 to 60 mg/L

Max 10 mg/dm2 or 60 mg/L

Ink adhesion test for printed pouch

Annex H of IS 15606:2005 NA

Anita RaniConvenor










Product resistance test for printed pouch

Annex J of IS 15609:2005 NA

-X-X-X-X-X-X-X-X-X-X-X-X-X-X-

Anita RaniConvenor


Page No - NABL India Web viewDehydrates Fruits And Vegetable Proudcts [Onion Seasoning Powder]...

Documents

Transcript of Page No - NABL India Web viewDehydrates Fruits And Vegetable Proudcts [Onion Seasoning Powder]...