P and S fertilizer reaction products in the seed-row as revealed by XANES

spectroscopyGourango Kar*, Jeff Schoenau, AdamGillespie, and Derek Peak

Department of Soil Science, University of Saskatchewan Canada.

Introduction

2

Sulfur (S) and phosphorus (P) are an essential nutrients for crop production

S and P fertilizers are commonly applied together in bands for crop production in Western Canada

Forms and AvailabilityAvailability depends on Species formed after application Soluble (solution) sulfate and phosphate

immediately available for root uptake Some fertilizers require transformation to

these forms

Understand the fate of applied S andP!

Will help to most beneficially use S and Pcontaining fertilizers

3

Traditional Approaches to Study of S and P Fertilizer Fate

Examining plant availability of the S and P

Through plant nutrient uptake and yieldresponse

Measuring content of total or available formsin soil before and after plant growth

4Photo courtesy T. King

Research Justification

There has been little recent work tofollow the fate and transformation(speciation) of applied S and Pfertilizers in prairie soils in the weeksfollowing application

XANES spectroscopy is under-utilizedas a tool to reveal chemical speciationin agricultural soils

5

Traditional wet chemical analyses methods- May not be able to identify particular S and P species in soil, artifacts created

6

XANES spectroscopy can distinguish different oxidation states of an element

Offers unique ability to followtransformation of fertilizers todifferent forms of varying plantavailability over time.

2.14 2.15 2.16 2.17 2.18

(b)

variscite

Fe(III)PO4

HCO3-NaOH

Energy (keV)

Why XANES

Objective

7

To develop and employ a synchrotrontechnique to assess the fate of differentfertilizer S forms and P added in theseed-row

www.maptown.com/.../canada-topo-maps.html

Black Chernozem MelfortBrown ChernozemCentral Butte

Saskatchewan, Canada

Field Study Sites

8

http://www.maptown.com/.../canada-topo-maps.html

Experiment Details Research design: RCBD Treatment: Urea, ammonium sulfate, calcium

sulfate, elemental S, and monoammoniumphosphate

Application rate: 20 kg S and P2O5 ha-1 in seed-row

Soil sample collection: from the seed-row 1, 4and 8 weeks after seeding canola.

9Photo courtesy T.KingU of S

Analytical Techniques

Wet chemical analysis: CaCl2 extractable available sulfate Available P by modified Kelowna method

XAS spectroscopic techniques: S and P K-edge XANES

Data analysis: Gaussian curve fitting Linear combination fitting

10

11

ResultsAvailable soil sulfate concentration in theseed-row after 1, 4 and 8 weeks of crop growth

Black Chernozem

0

100

200

300

400

Control AS Gypsum ES

Central Butte site

Week 1Week 4Week 8

SO4-

2 -S

(mg

kg-1

soil)

Brown Chernozem

Chart1

ControlControlControlControlControlControlControl13.47512.90718496689.464356.60541949216.60541949219.7606908789.7606908785.6833742625.683374262

ASASASASASASAS119.93513.23305084755.71761446.729629073446.72962907344.43170644614.43170644610.96725949640.9672594964

GypsumGypsumGypsumGypsumGypsumGypsumGypsum429.30539.092778187212.5280299.558731889399.558731889312.435318303212.43531830323.24600399863.2460039986

ESESESESESESES18.27513.01764922627.86956158.28018317038.28018317039.66077529.66077523.38286637753.3828663775

Week 1

Week 4

Week 8

Melfort site

2013 Field PLANT Data HASAN

Total NTotal PTotal S

SitePlotSiteCropTreatmentBlockSerial #Total BiomassBagTotal BiomassTotal BiomassTotal BiomassGrain BiomassGrain BiomassGrain BiomassStraw BiomassStraw BiomassStraw BiomassStrawStrawStrawStrawGrainGrainGrainGrainTN UptakeStrawStrawStrawStrawGrainGrainGrainGrainTP UptakeP RecoveryStrawStrawStrawStrawGrainGrainGrainGrainTS UptakeS RecoverySas Template

and Bag (g)(g)(g)(g/m2)(kg/ha)(g)(g/m2)(kg/ha)(g)(g/m2)(kg/ha)Total NN UptakeTotal NN UptakeGrain+StrawTotal PP UptakeTotal PP UptakeGrain+StrawS UptakeS UptakeGrain+StrawSITEP RecoveryS Recovery

1.0 metre row length harvest. 25.4 cm seed row spacing.1M row lengthug/mlug/gkg/kgkg/haug/mlug/gkg/kgkg/hakg/haug/mlug/gkg/kgkg/haug/mlug/gkg/kgkg/hakg/ha%% Sug/gkg/kgkg/ha% Sug/gkg/kgkg/hakg/ha%Central Butte (CB) = 1SiteSiteCropBlockTreatmentGrain BioTotal BioP UptakeS UptakeSiteCropBlockTreatmentP RecSiteCropBlockTreatmentS Rec

=75ml/0.2500g=300Melfort Herzberg (MH) = 2t/hat/hakg/hakg/ha%%

CB10111110350168182716.57165.483.03326.893268.9098.97389.653896.4610.33683101.040.0031010412.0888.19426458.200.026586.4998.570.7536043015226.08129044120.00022608130.8811.3423402.600.003411.1212.000.151631516.30.00151635.910.208820880.0020886.8312.73Melfort Armstrong (MA) = 3CB11113.277.1712.0012.73111843.97111379.75

Wheat19111219298149149585.75857.563.89251.542515.3584.89334.213342.1312.92043876.120.0038761212.95100.1130033.000.030075.5488.500.7887638603236.62915808820.00023662920.7912.3753712.500.00379.3410.130.174691746.90.00174695.840.264962649.60.00264966.6612.50Wheat11212.525.8610.1312.50112849.62112341.67

(1-48)25111325404162242951.59515.089.27351.463514.57152.41600.046000.399.39122817.360.0028173616.9182.37824713.400.024786.86103.761.1337181985340.11545955880.00034011552.0415.7534725.900.004716.6118.650.151421514.20.00151429.090.246532465.30.00246538.6617.75(1-48)11313.519.5118.6517.75113857.571133-5.09

45111445325145180707.67076.483.80329.923299.2195.94377.723777.1713.76524129.560.0041295615.6092.66627799.800.027891.72107.321.0948295956328.44887867650.00032844891.2412.7393821.700.003812.6113.850.191519150.0019157.230.229862298.60.00229867.5814.82CROP11413.307.0813.8514.821148-38.21114310.14

12112112376168208818.98189.083.39328.313283.07124.61490.594905.9112.17163651.480.0036514817.9190.59627178.800.027289.23107.140.7844399449235.33198345590.0002353321.1511.823546.000.003511.6412.800.137031370.30.00137036.720.223612236.10.00223617.3414.06Wheat = 111123.288.1912.8014.06111932.7711142.73

13112213354145209821.98218.584.39332.243322.44124.36489.614896.0611.76723530.160.0035301617.2893.57328071.900.028193.27110.550.80962875242.8886250.00024288861.1912.2733681.900.003712.2313.420.181218120.0018128.870.266912669.10.00266918.8717.74Canola = 211223.328.2213.4217.741129167.71112485.58

33112333327133194762.57624.886.51340.593405.91107.16421.894218.9012.91083873.240.0038732416.3484.28725286.100.025386.12102.461.3129786765393.89360294120.00039389361.6616.0134803.900.004816.3618.020.169911699.10.00169917.170.230442304.40.00230447.8515.02Peas = 311323.417.6218.0215.021139-39.15113464.66

42112442288115173681.86817.768.05267.912679.13105.12413.864138.5811.93643580.920.0035809214.8288.60926582.700.026671.2286.041.7895860294536.87580882350.00053687582.2211.373411.000.00349.1411.360.155915590.0015596.450.223182231.80.00223185.9812.4311422.686.8211.3612.43114919.1811446.20

711317341168173681.16811.073.41289.022890.1699.59392.093920.8714.37964313.880.0043138816.91102.2730681.000.030788.67105.590.8654667463259.64002389710.000259641.0212.4633738.900.003710.8111.820.346163461.60.003461613.570.246924690.0024697.1420.7179.7511132.896.8111.8220.7111110-6.44111519.32

14113214317114203797.47974.479.47312.873128.74123.08484.574845.6710.44963134.880.0031348815.1985.83625750.800.025880.5795.760.7528940074225.86820220590.00022586821.0910.8353250.500.003310.1711.260.184151841.50.00184158.920.247624760.0024767.7516.6741.67Wheat: Samples 1-4811233.137.9711.2616.6711210-19.75112527.00

29113329354141213838.68386.289.71353.193531.89123.30485.434854.3312.1143634.20.003634217.6479.29823789.400.023884.02101.660.9839349265295.18047794120.00029518051.4310.693207.000.003211.3312.760.203322033.20.00203329.870.208720870.0020877.3717.24-5.09Caniola: Samples 49-9611333.538.3912.7617.241131021.501135-0.43

46113446280107173680.46803.966.79262.952629.53106.03417.444174.4115.30724592.160.0045921619.1795.00528501.500.028574.9594.121.6889018382506.67055147060.00050667062.1213.4854045.500.004010.6412.750.221852218.50.00221859.260.249862498.60.00249866.5715.8310.14Peas: Samples 97-14411432.636.8012.7515.8311410-25.8211451.14

811418303168135531.55315.053.43210.352103.5481.57321.143211.4218.09845429.520.0054295217.4496.22728868.100.028960.7378.161.438434375431.53031250.00043153031.3913.4574037.100.00408.499.880.244182441.80.00244187.840.245542455.40.00245545.1713.012.7311142.105.319.8813.0111111-3.4511160.25

15114215352146206809.98099.273.89290.912909.06131.83519.025190.1620.74326222.960.0062229632.3093.92428177.200.028281.97114.271.6141433824484.24301470590.0004842432.5111.1463343.800.00339.7312.240.252412524.10.002524113.100.273652736.50.00273657.9621.0685.5811242.918.1012.2421.061121150.751126-43.33

351143354271402871131.511315.0100.59396.023960.24186.81735.477354.7221.19926359.760.0063597646.7792.31527694.500.0277109.68156.452.3530268382705.90805147060.00070590815.1916.3814914.300.004919.4624.650.190251902.50.001902513.990.258162581.60.002581610.2224.2264.66RCBD Design11343.9611.3124.6524.2211311-14.191136-57.87

41114441298120178699.66995.768.54269.842698.43109.15429.724297.2415.63724691.160.0046911620.1687.87726363.100.026471.1491.301.8262549632547.87648897060.00054787652.3513.0483914.400.003910.5612.920.217942179.40.00217949.370.224992249.90.00224996.0715.446.20Blocks; 1, 2, 3, 411442.707.0012.9215.441141142.09114635.32

511515336168168661.46614.270.80278.742787.4097.20382.683826.7712.48123744.360.0037443614.3395.04228512.600.028579.4893.800.6667086949200.01260845590.00020001260.7711.5093452.700.00359.6210.390.216152161.50.00216158.270.229412294.10.00229416.3914.6719.3211152.796.6110.3914.6711112107.001117-31.63

23115223329119210826.18261.085.86338.033380.31123.97488.074880.718.58722576.160.0025761612.5785.30425591.200.025686.5199.080.4884426287146.53278860290.00014653280.7212.8543856.200.003913.0413.750.147514750.0014757.200.236782367.80.00236788.0015.2027.0011253.388.2613.7515.20112120.7711271.77

27115327337127210828.08279.587.29343.663436.61123.01484.294842.9111.49363448.080.0034480816.7087.11226133.600.026189.81106.510.6731368566201.94105698530.00020194110.9817.0635118.900.005117.5918.570.204552045.50.00204559.910.226992269.90.00226997.8017.71-0.4311353.448.2818.5717.711131233.391137-38.40

43115443306113193761.37613.489.75353.353533.46103.63407.994079.9212.47883743.640.0037436415.2786.71926015.700.026091.93107.201.3238106618397.14319852940.00039714321.6212.7053811.500.003813.4715.090.186021860.20.00186027.590.207762077.60.00207767.3414.931.1411453.537.6115.0914.931141271.161147-30.94

111611334168166653.56535.472.03283.582835.8393.97369.963699.6112.28923686.760.0036867613.6479.28823786.400.023867.4581.090.8223075246.692250.00024669220.9116.1674850.100.004913.7514.670.203120310.0020317.510.184941849.40.00184945.2412.760.2511162.846.5414.6712.761218-23.60111843.29

22116222283168115452.84527.640.33158.781587.8074.67293.982939.7610.70763212.280.003212289.4481.16624349.800.024338.6648.111.4616077206438.48231617650.00043848231.2914.3734311.900.00436.858.140.160881608.80.00160884.730.216721670.0021673.448.17-43.3311261.594.538.148.171228-6.55112848.18

30116330270115155611.76116.961.08240.472404.7294.29371.223712.2014.30884292.640.0042926415.9494.78528435.500.028468.3884.310.8007234375240.217031250.0002402170.8916.9395081.700.005112.2213.110.174011740.10.00174016.460.228882288.80.00228885.5011.96-57.8711362.406.1213.1111.961238-5.921138-3.86

40116440376149227894.98949.296.53380.043800.39130.78514.885148.8212.60843782.520.0037825219.4890.15227045.600.0270102.78122.261.7232623162516.97869485290.00051697872.6613.1133933.900.003914.9517.610.194481944.80.001944810.010.219322193.20.00219328.3418.3535.3211463.808.9517.6118.3512482.091148-12.07

911719305168137539.45393.756.07220.752207.4880.93318.623186.2211.97123591.360.0035913611.4489.17126751.300.026859.0570.501.3295818015398.87454044120.00039887451.2712.0853625.500.00368.009.270.139131391.30.00139134.430.232722327.20.00232725.149.57-31.6311172.215.399.279.571219-11.76111972.11

18117218280125155610.76107.167.81266.972669.6987.31343.743437.4011.9643589.20.003589212.3493.58728076.100.028174.9587.290.5797598162173.92794485290.00017392790.6013.0423912.600.003910.4511.040.184861848.60.00184866.350.236942369.40.00236946.3312.681.7711272.676.1111.0412.68122917.751129170.59

28117328281115166654.96548.867.49265.712657.0998.85389.173891.7315.16324548.960.0045489617.7090.03927011.700.027071.7789.480.7730397243231.91191727940.00023191190.9013.273981.000.004010.5811.480.198011980.10.00198017.710.233512335.10.00233516.2013.91-38.4011372.666.5511.4813.911239-63.59113993.27

47117447291151140550.05500.057.49226.342263.3982.21323.663236.6115.27364582.080.0045820814.8397.79829339.400.029366.4181.240.9707944853291.23834558820.00029123830.9413.1173935.100.00398.919.850.192719270.0019276.240.242362423.60.00242365.4911.72-30.9411472.265.509.8511.72124944.70114928.33

611816388168220866.18661.490.29355.473554.72129.71510.675106.6912.0843625.20.003625218.5191.09827329.400.027397.15115.660.672275625201.68268750.00020168271.0314.2454273.500.004315.1916.2243.970.196719670.00196710.040.234842348.40.00234848.3518.3943.2911183.558.6616.2218.391211016.8511110-29.04

241182244031092941155.611555.991.08358.583585.83202.44797.017970.0814.93044479.120.0044791235.7092.30127690.300.027799.29134.991.0853294118325.59882352940.00032559882.6012.6723801.600.003813.6316.2349.620.191351913.50.001913515.250.203782037.80.00203787.3122.5648.1811283.5911.5616.2322.5612210-10.6911210-7.36

32118332336143193759.07590.285.66337.243372.44107.13421.774217.728.6222586.60.002586610.9180.30424091.200.024181.2592.161.1793545956353.80637867650.00035380641.4916.8275048.100.005017.0218.5257.570.162461624.60.00162466.850.230672306.70.00230677.7814.63-3.8611383.377.5918.5214.6312310-4.4211310-15.24

38118438258127131515.75157.150.04197.011970.0880.95318.703187.0112.1083632.40.003632411.5889.09826729.400.026752.6664.241.1567139706347.01419117650.00034701421.1113.2413972.300.00407.838.93-38.210.196111961.10.00196116.250.252482524.80.00252484.9711.22-12.0711481.975.168.9311.2212410127.981141043.28

11119111382168214842.58425.288.98350.313503.15125.02492.204922.0514.92684478.040.0044780422.0495.74228722.600.0287100.62122.660.8405176654252.15529963240.00025215531.2411.3363400.800.003411.9113.1532.770.249562495.60.002495612.280.256672566.70.00256678.9921.2772.1111193.508.4313.1521.2712111-44.251111156.91

171192175181453731469.114691.3160.33631.226312.20212.83837.918379.1311.94123582.360.0035823630.0287.7126313.000.0263166.09196.110.5766611581172.99834742650.00017299831.4514.5554366.500.004427.5629.01167.710.241552415.50.002415520.240.230642306.40.002306414.5634.80170.5911296.3114.6929.0134.801221133.941121110.58

26119326380168212834.68346.589.63352.873528.74122.37481.774817.7214.79724439.160.0044391621.3988.71126613.300.026693.91115.301.1191571691335.74715073530.00033574721.6218.0625418.600.005419.1220.74-39.150.316613166.10.003166115.250.257622576.20.00257629.0924.3493.2711393.538.3520.7424.3412311-43.4211311-15.64

44119444279114165650.96509.462.83247.362473.62102.51403.584035.8322.66086798.240.0067982427.4494.14428243.200.028269.8697.302.2337862132670.13586397060.00067013592.7016.3464903.800.004912.1314.8319.180.226552265.50.00226559.140.247452474.50.00247456.1215.2628.3311492.476.5114.8315.2612411136.651141141.56

4111014320168152598.45984.367.30264.962649.6184.70333.463334.6512.27963683.880.0036838812.2886.53225959.600.026068.7881.070.8850619853265.51859558820.00026551860.8911.1463343.800.00338.869.75-6.440.170311703.10.00170315.680.206842068.40.00206845.4811.16-29.04111102.655.989.7511.161211240.7711112110.38

211110221366168198779.57795.378.89310.593105.91119.11468.944689.379.12842738.520.0027385212.8491.40427421.200.027485.1798.010.301715183890.51455514710.00009051460.4212.1823654.600.003711.3511.78-19.750.196819680.0019689.230.250322503.20.00250327.7717.00-7.36112103.117.8011.7817.001221246.1311212-53.67

341110334339143196771.37713.477.44304.883048.82118.48466.464664.579.05522716.560.0027165612.6777.19323157.900.023270.6083.281.3535542279406.06626838240.00040606631.8920.5826174.600.006218.8320.7221.500.150971509.70.00150977.040.211572115.70.00211576.4513.49-15.24113103.057.7120.7213.4912312-1.1911312-35.14

391110439339142197774.37742.982.82326.063260.63113.85448.234482.2810.57923173.760.0031737614.2392.38427715.200.027790.37104.590.7171484559215.14453676470.00021514450.9611.7993539.700.003511.5412.51-25.820.193611936.10.00193618.680.247852478.50.00247858.0816.7643.28114103.267.7412.5116.761241247.561141247.73

2111112376168208818.98189.088.94350.163501.57119.06468.744687.4012.56163768.480.0037684817.6692.52527757.500.027897.19114.860.7096459743212.89379227940.00021289381.0012.6843805.200.003813.3214.32-3.450.236912369.10.002369111.100.247032470.30.00247038.6519.7556.91111113.508.1914.3219.75131869.921213-42.98

161111216373143230903.99039.4103.44407.244072.44126.16496.694966.938.70722612.160.0026121612.9783.82525147.500.0251102.41115.390.283069963284.92098897060.0000849210.4210.4683140.400.003112.7913.2150.750.195951959.50.00195959.730.222582225.80.00222589.0618.8010.58112114.079.0413.2118.801328-7.351223245.45

311111331306135171672.06719.771.61281.932819.2999.07390.043900.3911.55723467.160.0034671613.5276.78923036.700.023064.9578.470.8673490257260.20470772060.00026020471.0112.6253787.500.003810.6811.69-14.190.192231922.30.00192237.500.211232112.30.00211235.9613.45-15.64113112.826.7211.6913.451338-8.3512338.40

481111448346140206810.98109.483.72329.613296.06122.26481.344813.3913.52524057.560.0040575619.5386.02825808.400.025885.07104.600.9932575368297.97726102940.00029797731.4320.6176185.100.006220.3921.8242.090.198291982.90.00198299.540.213692136.90.00213697.0416.5941.56114113.308.1121.8216.591348-34.111243-98.29

31112134611682931153.511535.4124.11488.624886.22168.89664.926649.2111.18283354.840.0033548422.3194.5128353.000.0284138.54160.850.5499540993164.98622977940.00016498621.1012.8783863.400.003918.8819.97107.000.229082290.80.002290815.230.201992019.90.00201999.8725.10110.38111124.8911.5419.9725.10131915.1412140.53

201112220321168153602.46023.666.86263.232632.2886.14339.133391.3410.93683281.040.0032810411.1388.06326418.900.026469.5480.670.9169897059275.09691176470.00027509690.9312.93870.000.003910.1911.120.770.185761857.60.00185766.300.230692306.90.00230696.0712.37-53.67112122.636.0211.1212.371329-32.921224143.91

361112336327127200786.57865.082.03322.953229.53117.74463.544635.439.46322838.960.0028389613.1673.37422012.200.022071.0984.252.0531051471615.93154411760.00061593152.8612.3493704.700.003711.9614.8233.390.100221002.20.00100224.650.212322123.20.00212326.8611.50-35.14113123.237.8614.8211.501339-5.8312349.60

371112437337127210825.48253.990.97358.153581.50118.68467.244672.4413.83844151.520.0041515219.4091.83927551.700.027698.68118.071.1164047794334.92143382350.00033492141.5614.3334299.900.004315.4016.9671.160.191641916.40.00191648.950.230352303.50.00230358.2517.2047.73114123.588.2516.9617.201349-111.331244-106.66

CB58121158302168134527.65275.642.08165.671656.6991.92361.893618.905.28841586.520.001586525.7486.81326043.900.026043.1548.890.263572389779.07171691180.00007907170.2919.0055701.500.00579.459.730.444684446.80.004446816.090.36195370373619.5370370370.0036195376.0022.09CB12111.665.289.7322.09131108.231215-53.36

Canola6712126723916871279.52795.320.1879.45794.4950.82200.082000.7911.5683470.40.00347046.94100.6930207.000.030224.0030.940.9188542279275.65626838240.00027565630.5519.0485714.400.00574.545.090.433543350.0043358.670.44881481484488.14814814810.00448814813.5712.24Canola12210.792.805.0912.241321036.971225125.63

49-9673121373311168143563.05629.941.83164.691646.85101.17398.313983.078.19842459.520.002459529.80113.5934077.000.034156.1265.920.17146551.43950.00005143950.2020.8116243.300.006210.2810.490.391343913.40.003913415.590.47185185194718.51851851850.00471851857.7723.3649-9612311.655.6310.4923.3613310-39.7412357.26

93121493392168224881.98818.978.29308.233082.28145.71573.665736.616.39121917.360.0019173611.00106.1131833.000.031898.12109.120.0130.0000030.0219.8655959.500.006018.3718.390.353563535.60.003535620.280.582215822.10.005822117.9538.2312413.088.8218.3938.2313410-23.171245-186.45

60122160270168102401.64015.730.70120.871208.6671.30280.712807.094.91521474.560.001474564.1489.66426899.200.026932.5136.650.368616011110.58480330880.00011058480.3120.5566166.800.00627.457.760.434324343.20.004343212.190.39142592593914.25925925930.00391425934.7316.9212121.214.027.7616.9213111-45.90121682.01

61122261332168164645.76456.751.50202.762027.56112.50442.914429.138.31122493.360.0024933611.04121.7436522.000.036574.0585.090.241792996372.53789889710.00007253790.3219.1615748.300.005711.6611.980.357573575.70.003575715.840.54888888895488.88888888890.005488888911.1326.9712222.036.4611.9826.971321113.301226145.02

81122381358168190748.07480.367.85267.132671.26122.15480.914809.066.78242034.720.002034729.79101.6930507.000.030581.4991.280.136784889741.03546691180.00004103550.2016.8655059.500.005113.5213.710.465434654.30.004654322.380.479714797.10.004797112.8135.2012322.677.4813.7135.20133115.3112360.90

90122490357134223878.08779.572.28284.572845.67150.72593.395933.865.39761619.280.001619289.6192.7727831.000.027879.2088.810.071928821721.57864650740.00002157860.1318.8785663.400.005716.1216.240.386463864.60.003864622.930.397193971.90.003971911.3034.2312422.858.7816.2434.2313411-32.741246-271.37

55123155290168122480.34803.135.94141.501414.9686.06338.823388.194.44121332.360.001332364.5192.14927644.700.027639.1243.630.175202922852.56087683820.00005256090.1818.6815604.300.00567.938.110.358093580.90.003580912.130.39991666673999.16666666670.00399916675.6617.79-42.9812131.414.808.1117.79131127.95121732.26

62123262392168224881.98818.964.97255.792557.87159.03626.106261.029.33722801.160.0028011617.54111.1533345.000.033385.29102.830.3837186397115.11559191180.00011511560.7221.0186305.400.006316.1316.850.403234032.30.004032325.250.45106481484510.64814814810.004510648111.5436.78245.4512232.568.8216.8536.7813212-8.44122738.54

77123377325168157618.16181.139.38155.041550.39117.62463.074630.7111.4783443.40.003443415.95122.5436762.000.036857.0072.940.7434382169223.03146507350.00022303151.0322.1396641.700.006610.3011.330.420074200.70.004200719.450.555255520.0055528.6128.068.4012331.556.1811.3328.0613312-7.8012372.90

94123494343168175689.06889.859.44234.022340.16115.56454.964549.619.11282733.840.0027338412.44108.8532655.000.032776.4288.860.4533363419136.00090257350.00013600090.6219.2915787.300.005813.5414.160.351323513.20.003513215.980.530525305.20.005305212.4228.40-98.2912432.346.8914.1628.40134128.921247-137.42

56124156287168119468.54685.033.91133.501335.0485.09335.003350.0010.07643022.920.0030229210.1399.91729975.100.030040.0250.140.67559625202.6788750.00020267890.6819.4245827.200.00587.788.460.460446040.00460415.420.50327777785032.77777777780.00503277786.7222.140.5312141.344.698.4622.142118-34.041218-48.18

63124263320168152598.45984.344.55175.391753.94107.45423.034230.3111.20923362.760.0033627614.23121.0336309.000.036363.6877.910.3675860846110.27582536760.00011027580.4718.9785693.400.00579.9910.450.403374033.70.004033717.060.54539814815453.98148148150.00545398159.5726.63143.91CB Canola Trt 7 GRAIN N&P12241.755.9810.4526.632128-69.301228153.75

83124383335168167657.56574.842.45167.131671.26124.55490.354903.5413.54924064.760.0040647619.93129.0838724.000.038764.7284.650.6061472426181.84417279410.00018184420.8920.2126063.600.006110.1311.030.387738770.00387719.010.581655816.50.00581659.7228.739.6096.92729078.1019.29712341.676.5711.0328.732138-85.851238-141.61

89124489329168161633.96338.639.55155.711557.09121.45478.154781.5010.23363070.080.0030700814.68116.534950.000.035054.4269.100.287482665486.24479963240.00008624480.4120.9276278.100.00639.7810.190.360823608.20.003608217.250.662086620.80.006620810.3127.56-106.66104.5531365.0019.43312441.566.3410.1927.56214840.83124819.43

5312515326416896378.03779.528.93113.901138.9867.07264.062640.558.06522419.560.002419566.39105.0131503.000.031535.8842.270.4143589522124.30768566180.00012430770.3319.4025820.600.00586.636.960.443564435.60.004435611.710.44258333334425.83333333330.00442583335.0416.75-53.36108.0732421.0019.84112151.143.786.9616.752119-44.95121963.70

71125271305168137539.45393.744.23174.131741.3492.77365.243652.366.6920070.0020077.33105.1431542.000.031554.9362.260.178701121353.61033639710.00005361030.2019.765928.000.005910.3210.520.466714667.10.004667117.050.44541666674454.16666666670.00445416677.7624.80125.63103.182333333330954.719.523666666712251.745.3910.5224.80212926.96122987.28

75125375331168163641.76417.355.95220.282202.76107.05421.464214.578.12522437.560.0024375610.27117.0835124.000.035177.3787.640.0130.0000030.0118.4275528.100.005512.1812.190.395739570.00395716.680.48785185194878.51851851850.004878518510.7527.427.2612352.206.4212.1927.42213997.391239-218.04

91125491262143119468.54685.034.50135.831358.2784.50332.683326.7710.59363178.080.0031780810.57111.1333339.000.033345.2855.860.268189301580.45679044120.00008045680.2720.046012.000.00608.178.430.382043820.40.003820412.710.506035060.30.00506036.8719.58-186.4512451.364.698.4319.58214914.371249-39.61

49126149389168221870.18700.866.34261.182611.81154.66608.906088.987.44242232.720.0022327213.59106.1231836.000.031883.1596.740.06069729618.20918878680.00001820920.1120.696207.000.006216.2116.320.317343173.40.003173419.320.41990740744199.07407407410.004199074110.9730.2982.0112162.618.7016.3230.292111026.051211035.91

70126270320168152598.45984.350.39198.391983.86101.61400.044000.399.1227360.00273610.9599.24529773.500.029859.0770.010.5742639154172.27917463240.00017227920.6921.6486494.400.006512.8813.570.462344623.40.004623418.500.41563888894156.38888888890.00415638898.2526.74145.0212261.985.9813.5726.74212101.2912210-57.23

78126378317168149586.65866.145.24178.111781.10103.76408.504085.046.89762069.280.002069288.45101.6230486.000.030554.3062.750.213265808863.97974264710.00006397970.2617.8515355.300.00549.549.800.390783907.80.003907815.960.443364433.60.00443367.9023.860.9012361.785.879.8023.8621310-59.2512310-95.64

8812648823216864252.02519.732.53128.071280.7131.47123.901238.987.0382111.40.00211142.62101.1730351.000.030438.8741.490.315397224394.61916727940.00009461920.1220.616183.000.00627.928.040.422014220.10.00422015.230.457764577.60.00457765.8611.09-271.3712461.282.528.0411.092141064.621241081.39

57127157324168156614.26141.749.00192.911929.13107.00421.264212.606.4021920.60.00192068.0996.92729078.100.029156.1064.190.273907169182.17215073530.00008217220.3519.2975789.100.005811.1711.510.409954099.50.004099517.270.41702777784170.27777777780.00417027788.0525.3132.2612171.936.1411.5125.312111134.5712111129.51

66127266274168106417.34173.232.34127.321273.2373.66290.002900.006.96122088.360.002088366.06103.182333333330954.70.031039.4145.470.4040241728121.20725183820.00012120730.3519.52366666675857.10.00597.467.810.375543755.40.003755410.890.40862962964086.29629629630.00408629635.2016.0938.5412271.274.177.8116.0921211168.931221163.91

76127376317168149586.65866.141.65163.981639.76107.35422.644226.387.11482134.440.002134449.02104.5531365.000.031451.4360.450.296725367689.01761029410.00008901760.3819.4335829.900.00589.569.940.409284092.80.004092817.300.46859259264685.92592592590.00468592597.6824.982.9012371.645.879.9424.982131163.0012311-241.01

95127495319168151594.55944.942.40166.931669.29108.60427.564275.5910.8663259.80.003259813.94108.0732421.000.032454.1268.060.3978090993119.34272977940.00011934270.5119.8415952.300.00609.9410.450.384893848.90.003848916.460.481014810.10.00481018.0324.49-137.4212471.675.9410.4524.49214114.571241183.10

5412815424716879311.03110.225.3999.96999.6153.61211.062110.635.92321776.960.001776963.7595.04428513.200.028528.5032.250.253131066275.93931985290.00007593930.1618.6345590.200.00565.595.75-23.600.387953879.50.00387958.190.39180555563918.05555555560.00391805563.9212.10-48.1812181.003.115.7512.102111256.7612112125.57

72128272379168211830.78307.164.88255.432554.33146.12575.285752.768.99762699.280.0026992815.53113.7234116.000.034187.14102.670.251452996375.43589889710.00007543590.4320.5676170.100.006215.7616.19-6.550.521285212.80.005212829.990.48362962964836.29629629630.004836296312.3542.34153.7512282.558.3116.1942.3421212-133.941221217.38

80128380302168134527.65275.643.07169.571695.6790.93357.993579.927.02482107.440.002107447.5497.67629302.800.029349.6957.230.7533468199226.00404595590.0002260040.8119.5195855.700.00599.9310.74-5.920.362433624.30.003624312.970.475424754.20.00475428.0621.04-141.6112381.705.2810.7421.0421312-27.7412312-127.54

86128486333128205807.18070.960.61238.622386.22144.39568.465684.659.98522995.560.0029955617.03113.1333939.000.033980.9998.010.250325404475.09762132350.00007509760.4319.4785843.400.005813.9414.372.090.399373993.70.003993722.700.564695646.90.005646913.4736.1819.4312482.398.0714.3736.1821412-10.601241226.61

59129159293168125492.14921.325.0498.58985.8399.96393.543935.4312.14163642.480.0036424814.33102.6930807.000.030830.3744.711.026375307.91250.00030791251.2120.5276158.100.00626.077.28-11.760.464294642.90.004642918.270.50932407415093.24074074070.00509324075.0223.2963.7012190.994.927.2823.292218-115.451313-27.63

65129265345168177696.96968.545.11177.601775.98131.89519.255192.5218.73565620.680.0056206829.19130.5339159.000.039269.5598.731.0576279412317.28838235290.00031728841.6519.8585957.400.006010.5812.2317.750.493814938.10.004938125.640.56607407415660.74074074070.005660740710.0535.6987.2812291.786.9712.2335.692228-89.6213233.58

7412937424916881318.93189.015.4860.94609.4565.52257.952579.5317.25245175.720.0051757213.35126.1837854.000.037923.0736.420.9927248162297.81744485290.00029781740.7721.326396.000.00643.904.67-63.590.372043720.40.00372049.600.62292592596229.25925925930.00622925933.8013.39-218.0412390.613.194.6713.39223880.66133341.69

92129492361168193759.87598.450.11197.281972.83142.89562.565625.5913.33083999.240.0039992422.50110.1533045.000.033065.1987.691.1485455882344.56367647060.00034456371.9421.4916447.300.006412.7214.6644.700.358143581.40.003581420.150.513295132.90.005132910.1330.27-39.6112491.977.6014.6630.2722485.491343-39.73

521210152287168119468.54685.038.04149.761497.6480.96318.743187.407.74482323.440.002323447.41101.830540.000.030545.7453.140.3753282904112.59848713240.00011259850.3618.4385531.400.00558.288.6416.850.448124481.20.004481214.280.4160370374160.37037037040.00416037046.2320.5135.91121101.504.698.6420.512219-99.571314-18.02

691210269298168130511.85118.141.71164.211642.1388.29347.603475.986.5161954.80.00195486.79101.7130513.000.030550.1156.900.099379025729.81370772060.00002981370.1018.9715691.300.00579.359.45-10.690.409674096.70.004096714.240.42649074074264.90740740740.00426490747.0021.24-57.23122101.645.129.4521.242229128.2113241.86

821210382322168154606.36063.051.36202.202022.05102.64404.094040.947.59962279.880.002279889.21105.0431512.000.031563.7272.930.252101139775.63034191180.00007563030.3118.8635658.900.005711.4411.75-4.420.378783787.80.003787815.310.510751070.00510710.3325.63-95.64123102.026.0611.7525.632239-43.161334107.29

8712104874271712561007.910078.796.65380.513805.12159.35627.366273.627.92842378.520.0023785214.92109.2832784.000.0328124.75139.670.104759503731.42785110290.00003142790.2018.4265527.800.005521.0321.23127.980.394033940.30.003940324.720.463954639.50.004639517.6542.3781.39124103.8110.0821.2342.372249201.42134448.02

501211150350168182716.57165.451.85204.132041.34130.15512.405124.0213.01163903.480.0039034820.00117.4635238.000.035271.9391.930.5270382353158.11147058820.00015811150.8118.1055431.500.005411.0911.90-44.250.388513885.10.003885119.910.4882129634882.12962962960.00488212969.9729.87129.51121112.047.1711.9029.87221106.161315-17.26

641211264383168215846.58464.667.20264.572645.67147.80581.895818.906.26041878.120.0018781210.9396.68929006.700.029076.7487.670.254027812576.208343750.00007620830.4420.8196245.700.006216.5216.9733.940.399583995.80.003995823.250.38198148153819.81481481480.003819814810.1133.3663.91122112.658.4616.9733.3622210-1.901325-28.42

79121137924216874291.32913.422.8690.00900.0051.14201.342013.3911.57763473.280.003473286.99100.6930207.000.030227.1934.180.6334935662190.04806985290.00019004810.3818.7985639.400.00565.085.46-43.420.353135310.0035317.110.442954429.50.00442953.9911.10-241.01123110.902.915.4611.1022310-45.09133551.87

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511212151370168202795.37952.863.15248.622486.22138.85546.655466.546.4081922.40.001922410.5195.21228563.600.028671.0281.520.4267447059128.02341176470.00012802340.7019.9655989.500.006014.8915.5940.770.381713817.10.003817120.870.34645370373464.5370370370.0034645378.6129.48125.57121122.497.9515.5929.4822111-193.8713167.91

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851212485363147216850.48503.960.04236.382363.78155.96614.026140.168.70122610.360.0026103616.03118.1935457.000.035583.8199.840.291460312587.438093750.00008743810.5420.6816204.300.006214.6715.2047.560.386753867.50.003867523.750.556245562.40.005562413.1536.9026.6198.02329406.9011.15124122.368.5015.2036.9022411156.671346-12.38

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97-14412123132657741686062385.823858.3302.841192.2811922.83303.161193.5411935.4323.1386941.40.006941482.85108.6332589.000.0326388.55471.401.7636529.080.000529086.3110.2543076.200.003136.6842.990.069976699.760.000699768.350.150391503.90.001503917.9326.2897-144233111.9223.8642.9926.283133-141.86

14123142854851683171248.012480.3147.43580.435804.33169.57667.606675.9830.7579227.10.009227161.60105.7531725.000.0317184.14245.742.1949658.470.000658474.4010.5843175.200.003218.4322.830.074498744.980.000744984.970.16512121651.2120.0016512129.5814.5623415.8012.4822.8314.56314397.74

1082321252400168232913.49133.9105.92417.014170.08126.08496.384963.7822.9986899.40.006899434.25114.8234446.000.0344143.64177.892.1352640.560.000640563.1812.4533735.900.003715.5818.760.0820772727820.77272727270.00082077274.070.171861718.60.00171867.1711.2423124.179.1318.7611.24311471.82

1092322253414168246968.59685.0134.41529.175291.73111.59439.334393.3120.5386161.40.006161427.07107.9632388.000.0324171.39198.461.5846475.380.000475382.0910.6283188.400.003216.8718.960.0492336364492.33636363640.00049233642.160.137841378.40.00137847.299.4623225.299.6918.969.46312436.47

12923232734541682861126.011259.8117.06460.874608.66168.94665.126651.1824.5297358.70.007358748.94122.4836744.000.0367169.34218.281.4416432.480.000432482.8812.683804.000.003817.5320.410.072442724.420.000724424.820.18217441821.7440.0018217448.4013.2123324.6111.2620.4113.213134-57.94

13823242825411683731468.514685.0156.48616.066160.63216.52852.448524.4125.877400.0077465.98112.4233726.000.0337207.77273.751.5782473.460.000473464.0412.5423762.600.003823.1827.220.075408754.080.000754086.430.15850081585.0080.0015850089.7616.1923426.1614.6927.2216.193144-15.28

10323312474561682881133.911338.6132.94523.395233.86155.06610.476104.7233.49910049.70.010049761.35123.3737011.000.0370193.71255.062.2932687.960.000687964.2012.233669.000.003719.2023.400.0754854545754.85454545450.00075485454.610.190891908.90.00190899.9914.6011.7023135.2311.3423.4014.603115-12.21

1102332254322168154606.36063.080.38316.463164.5773.62289.842898.4326.1977859.10.007859122.78108.5832574.000.0326103.08125.861.7497524.910.000524911.5210.3683110.400.00319.8411.360.0793309091793.30909090910.00079330912.300.183591835.90.00183595.818.11-7.2623233.166.0611.368.113125-68.44

12523332696731685051988.219881.9261.721030.3910303.94243.28957.809577.9530.6559196.50.009196588.08107.2932187.000.0322331.65419.742.1596647.880.000647886.2110.6883206.400.003233.0439.240.101210120.0010129.690.182981829.80.001829818.8528.554.04233310.3019.8839.2428.553135-147.92

14223342866281684601811.018110.2208.86822.288222.83251.14988.749887.4028.1584450.00844583.50115.2134563.000.0346284.21367.701.7261517.830.000517835.1210.8073242.100.003226.6631.780.072845728.450.000728457.200.17904241790.4240.00179042414.7221.9273.6723438.2218.1131.7821.92314513.38

10423412484741683061204.712047.2154.23607.206072.05151.77597.525975.2017.7353190.00531931.78119.7435922.000.0359218.12249.900.94874284.6220.0002846221.7011.183354.000.003420.3722.070.0725890909725.89090909090.00072589094.340.216952169.50.002169513.1717.5140.8223146.0712.0522.0717.513116-46.28

1112342255404168236929.19291.3108.37426.654266.54127.63502.485024.8042.20912662.70.012662763.63120.0336009.000.0360153.63217.263.1418942.540.000942544.7411.733519.000.003515.0119.750.11525454551152.54545454540.00115254555.790.20520500.002058.7514.5457.0223244.279.2919.7514.54312638.53

13123432754531682851122.011220.5137.15539.965399.61147.85582.095820.8728.6148584.20.008584249.97114.9434482.000.0345186.19236.162.087626.10.00062613.6410.5063151.800.003217.0220.660.115121151.20.00115126.700.227342273.40.002273412.2818.98-13.0523345.4011.2220.6618.983136-98.58

13723442815201683521385.813858.3181.05712.807127.95170.95673.036730.3125.9497784.70.007784752.39108.3532505.000.0325231.69284.091.5851475.530.000475533.209.52962858.880.002920.3823.580.075813758.130.000758135.100.18096481809.6480.00180964812.9018.0034.4423447.1313.8623.5818.00314670.12

1012351245398168230905.59055.194.93373.743737.40135.07531.775317.7239.97119910.01199163.76125.8337749.000.0377141.08204.853.3811014.30.00101435.3913.2633978.900.004014.8720.260.0983428571983.42857142860.00098342865.230.191951919.50.00191957.1712.40-10.2523153.749.0620.2612.403117-37.65

11923522634401682721070.910708.7114.83452.094520.87157.17618.786187.8040.73712221.10.012221175.62120.4336129.000.0361163.33238.963.83451150.350.001150357.1212.9593887.700.003917.5824.690.121261212.60.00121267.500.201832018.30.00201839.1216.6377.9223254.5210.7124.6916.63312741.27

12323532676491684811893.718937.0242.88956.229562.20238.12937.489374.8026.5979770.00797774.78102.9130873.000.0309295.21370.002.3711711.330.000711336.679.25432776.290.002826.5533.220.078847788.470.000788477.390.178171781.70.001781717.0424.43-3.3123359.5618.9433.2224.433137-182.24

13923542837141475672232.322322.8268.841058.4310584.25298.161173.8611738.5827.1681480.00814895.65113.1233936.000.0339359.19454.831.7224516.720.000516726.0710.8923267.600.003334.5940.650.081047810.470.000810479.510.16400881640.0880.00164008817.3626.87123.15234510.5822.3240.6526.873147-37.45

972361241378168210826.88267.7103.52407.564075.59106.48419.214192.1325.1597547.70.007547731.64112.4833744.000.0337137.53169.171.8915567.450.000567452.3812.5283758.400.003815.3217.700.0839533333839.53333333330.00083953333.520.194991949.90.00194997.9511.47-19.6223164.088.2717.7011.473118-1.31

11823622625341683661440.914409.4139.62549.695496.85226.38891.268912.6036.70211010.60.011010698.13124.7237416.000.0374205.67303.803.1644949.320.000949328.4613.1543946.200.003921.6930.150.093612936.120.000936128.340.183531835.30.001835310.0918.4395.9623265.5014.4130.1518.43312830.26

12623632707701686022370.123700.8299.581179.4511794.49302.421190.6311906.3028.0818424.30.0084243100.30105.7531725.000.0317374.18474.482.0123603.690.000603697.199.8432952.900.003034.8342.020.105261052.60.001052612.530.189061890.60.001890622.3034.8315.27233611.7923.7042.0234.83313849.18

13623642806141684461755.917559.1202.41796.897968.90243.59959.029590.1623.5627068.60.007068667.79108.8232646.000.0326260.15327.941.3655409.650.000409653.9310.2183065.400.003124.4328.360.060848608.480.000608485.840.18993961899.3960.00189939615.1420.9764.1423467.9717.5628.3620.97314813.41

10523712494291682611027.610275.6111.48438.904388.98149.52588.665886.6141.96612589.80.012589874.11118.4935547.000.0355156.01230.134.53391360.170.001360178.0114.1234236.900.004218.6026.600.0733609091733.60909090910.00073360914.320.155391553.90.00155396.8211.14-22.9023174.3910.2826.6011.143119-34.46

11423722585361683681448.814488.2108.00425.204251.97260.001023.6210236.2226.5997979.70.007979781.68114.2934287.000.0343145.79227.472.3153694.590.000694597.1111.4863445.800.003414.6521.760.125991259.90.001259912.900.156521565.20.00156526.6619.55107.1623274.2514.4921.7619.553129-22.01

12423732686191684511775.617755.9213.27839.658396.46237.73935.949359.4524.8397451.70.007451769.74112.3133693.000.0337282.90352.651.6129483.870.000483874.5310.3983119.400.003126.1930.720.061279612.790.000612795.740.145351453.50.001453512.2017.94-14.9023378.4017.7630.7217.94313940.75

14323742874381682701063.010629.9129.04508.035080.31140.96554.965549.6138.10711432.10.011432163.44114.334290.000.0343174.20237.653.0046901.380.000901385.0012.2633678.900.003718.6923.690.082744827.440.000827444.590.15466681546.6680.0015466687.8612.45-21.0823475.0810.6323.6912.45314943.11

10223812464941683261283.512834.6147.93582.405824.02178.07701.067010.6340.05312015.90.012015984.24118.6335589.000.0356207.27291.513.0009900.270.000900276.3111.9013570.300.003620.7927.1037.020.0942636364942.63636363640.00094263646.610.177621776.20.001776210.3416.9557.1223185.8212.8327.1016.953111023.34

12023822646091684411736.217362.2208.19819.658196.46232.81916.579165.7524.9677490.10.007490168.65114.734410.000.0344282.04350.692.2472674.160.000674166.1812.423726.000.003730.5436.72253.550.081112811.120.000811127.430.161231612.30.001612313.2220.65111.9323288.2017.3636.7220.6531210-12.81

12823832726771685092003.920039.4260.601025.9810259.84248.40977.959779.5327.3478204.10.008204180.23111.6233486.000.0335343.56423.791.7792533.760.000533765.2210.7553226.500.003233.1038.32-9.210.086491864.910.000864918.460.17632081763.2080.00176320818.0926.55133.35233810.2620.0438.3226.5531310-13.99

13423842785401683721464.614645.7173.75684.066840.55198.25780.517805.1236.36410909.20.010909285.15105.6631698.000.0317216.83301.982.8394851.820.000851826.6510.2563076.800.003121.0527.70-40.840.046324463.240.000463243.620.16379281637.9280.00163792811.2014.82-13.7323486.8414.6527.7014.8231410-3.17

10723912514281682601023.610236.2103.65408.074080.71156.35615.556155.5135.25810577.40.010577465.11184.5155353.000.0554225.88290.993.19300.000935.7216.5324959.600.005020.2425.9638.970.12352727271235.27272727270.00123527277.600.239052390.50.00239059.7517.3661.1823194.0810.2425.9617.363111158.14

1132392257299168131515.75157.561.09240.512405.1269.91275.242752.3630.1999059.70.009059724.94124.2237266.000.037389.63114.562.1157634.710.000634711.7511.1143334.200.00338.029.77-99.840.113241132.40.00113243.120.180271802.70.00180274.347.45-20.0523292.415.169.777.4531