N/A Matrix: Derivative Certificate · 2021. 1. 4. · pass/fail does not include the UM. The...

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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report is an Kaycha Labs certification. The results relate only to the material or product analyzed. Test results are confidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batch material may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter, ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) and Limit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured by an analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholds for human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty of measurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for the pass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310. Jeremy Campbell Lab Director State License # CMTL-0001 ISO Accreditation # 97164 ___________________ Signature 10/05/2020 ___________________ Signed On 2444 NE 1st Blvd Suite 700 Gainesville, FL, 32609, USA Kaycha Labs CBD Cooling Rub Peppermint N/A Matrix: Derivative Certificate of Analysis Sample:GA00723001-001 Harvest/Lot ID: CBD RUB 1000MG Seed to Sale #N/A Batch Date :N/A Batch#: CBD RUB 1000MG Sample Size Received: 60 ml Retail Product Size: 60 Ordered : 07/23/20 Sampled : 07/23/20 Completed: 08/03/20 Expires: 08/03/21 Sampling Method: SOP Client Method Aug 03, 2020 | Southern Sun 11613 SW 234th St Archer, FL, 32618, US PASSED Page 1 of 4 PRODUCT IMAGE SAFETY RESULTS MISC. Pesticides PASSED Heavy Metals PASSED Microbials PASSED Mycotoxins PASSED Residuals Solvents PASSED Filth PASSED Water Activity NOT TESTED Moisture NOT TESTED Terpenes NOT TESTED CANNABINOID RESULTS Total THC 0.039% THC/Container :23.682 mg Total CBD 1.492% CBD/Container :895.212 mg Total Cannabinoids 1.643% Total Cannabinoids/Container :986.088 mg CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA 0.052% ND 0.040% ND ND 0.018% ND ND 1.492% 0.039% ND 0.520 mg/g ND 0.400 mg/g ND ND 0.180 mg/g ND ND 14.920 mg/g 0.390 mg/g ND LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001 % % % % % % % % % % % Cannabinoid Profile Test Analyzed by Weight Extraction date : Extracted By : 508 3.0091g 07/24/20 09:07:10 650 Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 07/28/20 16:51:33 Batch Date : 07/24/20 08:43:01 Analytical Batch -GA014256POT Instrument Used : GA-HPLC-001 2030C Plus Running On : Reagent Dilution Consums. ID 042720.09 400 280670882 072020.R29 VAV-09-1020 Lot# 947.077 072120.R02 6970145500298 190624060 16466-042 Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L). Filth PASSED Analyzed By Weight Extraction date LOD(ppm) Extracted By 650 NA 07/23/20 650 Analysis Method -SOP.T.40.013 Batch Date : 07/23/20 16:32:25 Analytical Batch -GA014249FIL Reviewed On - 07/28/20 14:09:04 Instrument Used : GA-Filth/Foreign Material Microscope Running On : This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing waste and by-products. An SH-2B/T Stereo Microscope is use for inspection.

Transcript of N/A Matrix: Derivative Certificate · 2021. 1. 4. · pass/fail does not include the UM. The...

  • This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.

    Jeremy CampbellLab Director

    State License # CMTL-0001ISO Accreditation # 97164 ___________________

    Signature

    10/05/2020

    ___________________Signed On

    2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, USA

    Kaycha LabsCBD Cooling Rub Peppermint

    N/AMatrix: Derivative

    Certificateof Analysis

    Sample:GA00723001-001Harvest/Lot ID: CBD RUB 1000MG

    Seed to Sale #N/ABatch Date :N/A

    Batch#: CBD RUB 1000MGSample Size Received: 60 ml

    Retail Product Size: 60Ordered : 07/23/20Sampled : 07/23/20

    Completed: 08/03/20 Expires: 08/03/21Sampling Method: SOP Client Method

    Aug 03, 2020 | Southern Sun11613 SW 234th StArcher, FL, 32618, US

    PASSEDPage 1 of 4

    PRODUCT IMAGE SAFETY RESULTS MISC.

    PesticidesPASSED

    Heavy MetalsPASSED

    MicrobialsPASSED

    MycotoxinsPASSED

    ResidualsSolventsPASSED

    FilthPASSED

    Water ActivityNOT TESTED

    MoistureNOT TESTED

    TerpenesNOT TESTED

    CANNABINOID RESULTS

    Total THC

    0.039%THC/Container :23.682 mg

    Total CBD

    1.492%CBD/Container :895.212 mg

    Total Cannabinoids

    1.643%Total Cannabinoids/Container:986.088 mg

    CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA

    0.052% ND 0.040% ND ND 0.018% ND ND 1.492% 0.039% ND

    0.520mg/g ND

    0.400mg/g ND ND

    0.180mg/g ND ND

    14.920mg/g

    0.390mg/g ND

    LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001

    % % % % % % % % % % %

    Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :508 3.0091g 07/24/20 09:07:10 650

    Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 07/28/20 16:51:33 Batch Date : 07/24/20 08:43:01Analytical Batch -GA014256POT Instrument Used : GA-HPLC-001 2030C Plus Running On :

    Reagent Dilution Consums. ID

    042720.09 400 280670882072020.R29 VAV-09-1020 Lot# 947.077072120.R02 6970145500298

    19062406016466-042

    Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).

    Filth PASSEDAnalyzed By Weight Extraction date LOD(ppm) Extracted By650 NA 07/23/20 650

    Analysis Method -SOP.T.40.013 Batch Date : 07/23/20 16:32:25Analytical Batch -GA014249FIL Reviewed On - 07/28/20 14:09:04Instrument Used : GA-Filth/Foreign Material MicroscopeRunning On :

    This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.

  • This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.

    Jeremy CampbellLab Director

    State License # CMTL-0001ISO Accreditation # 97164 ___________________

    Signature

    10/05/2020

    ___________________Signed On

    2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, USA

    Kaycha LabsCBD Cooling Rub Peppermint

    N/AMatrix : Derivative

    Certificate of Analysis PASSEDSouthern Sun

    11613 SW 234th StArcher, FL, 32618, USTelephone: (954) 336-1166Email: [email protected]

    Sample : GA00723001-001Harvest/LOT ID: CBD RUB 1000MGBatch# : CBD RUB1000MGSampled : 07/23/20Ordered : 07/23/20

    Sample Size Received : 60 mlCompleted : 08/03/20Expires: 08/03/21Sample Method : SOP Client Method

    Page 2 of 4

    Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.3 NDACEPHATE 0.01 ppm 3 NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDBIFENAZATE 0.01 ppm 3 NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 3 NDCHLORMEQUAT CHLORIDE 0.05 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.5 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZANON 0.01 ppm 0.2 NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDDIMETHOMORPH 0.02 ppm 3 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 1.5 NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 2 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 2 NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 3 NDKRESOXIM-METHYL 0.01 ppm 1 NDMALATHION 0.02 ppm 2 NDMETALAXYL 0.01 ppm 3 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 3 NDNALED 0.025 ppm 0.5 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL BUTOXIDE 0.1 ppm 3 NDPRALLETHRIN 0.01 ppm 0.4 ND

    Pesticides LOD Units Action Level ResultPROPICONAZOLE 0.01 ppm 1 NDPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.05 ppm 1 NDPYRIDABEN 0.02 ppm 3 NDSPINETORAM 0.02 PPM 3 NDSPIROMESIFEN 0.01 ppm 3 NDSPIROTETRAMAT 0.01 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)

    0 PPM 20 ND

    TOTAL PERMETHRIN 0.01 ppm 1 NDTOTAL SPINOSAD 0.01 ppm 3 NDTRIFLOXYSTROBIN 0.01 ppm 3 NDCHLORDANE * 0.01 PPM 0.1 NDPENTACHLORONITROBENZENE(PCNB) *

    0.01 PPM 0.2 ND

    PARATHION-METHYL * 0.01 PPM 0.1 NDCAPTAN * 0.025 PPM 3 NDCHLORFENAPYR * 0.01 PPM 0.1 NDCYFLUTHRIN * 0.01 PPM 1 NDCYPERMETHRIN * 0.01 PPM 1 ND

    Pesticides PASSED

    Analyzed by Weight Extraction date Extracted By635 , 1541 0.9950g 07/27/20 02:07:49 635 , 1541Analysis Method - SOP.T.30.065, SOP.T.40.065 ,SOP.T.30.065, SOP.T40.070Analytical Batch - GA014315PES , GA014391VOL Reviewed On- 07/28/20 14:09:04Instrument Used : GA-LCMS-001 Pes , GA-GCMS-003 Triple Quad PestRunning On :Batch Date : 07/27/20 14:02:46

    Reagent Dilution Consums. ID072320.R12 10 280670882070620.R17 6970145500298071320.R01 VAV-09-1020 (947.077) / ALK-09-1412 (9291.179)

    P734631 / P7411895

    Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrations forregulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060 Sample Preparation forPesticides Analysis via LCMSMS and SOP.T40.065 Procedure for Pesticide Quantification Using LCMS). * VolatilePesticide screening is performed using GC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.

  • This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.

    Jeremy CampbellLab Director

    State License # CMTL-0001ISO Accreditation # 97164 ___________________

    Signature

    10/05/2020

    ___________________Signed On

    2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, USA

    Kaycha LabsCBD Cooling Rub Peppermint

    N/AMatrix : Derivative

    Certificate of Analysis PASSEDSouthern Sun

    11613 SW 234th StArcher, FL, 32618, USTelephone: (954) 336-1166Email: [email protected]

    Sample : GA00723001-001Harvest/LOT ID: CBD RUB 1000MGBatch# : CBD RUB1000MGSampled : 07/23/20Ordered : 07/23/20

    Sample Size Received : 60 mlCompleted : 08/03/20Expires: 08/03/21Sample Method : SOP Client Method

    Page 3 of 4

    Residual Solvents PASSED

    Solvent LOD Units ActionLevel(PPM)

    Pass/Fail Result

    1,1-DICHLOROETHENE 0.8 ppm 8 PASS ND

    1,2-DICHLOROETHANE 0.2 ppm 2 PASS ND

    2-PROPANOL 50 ppm 500 PASS ND

    ACETONE 75 ppm 750 PASS ND

    ACETONITRILE 6 ppm 60 PASS ND

    BENZENE 0.1 ppm 1 PASS ND

    BUTANES (N-BUTANE) 500 ppm 5000 PASS ND

    CHLOROFORM 0.2 ppm 2 PASS ND

    DICHLOROMETHANE 12.5 ppm 125 PASS ND

    ETHANOL 500 ppm PASS ND

    ETHYL ACETATE 40 ppm 400 PASS ND

    ETHYL ETHER 50 ppm 500 PASS ND

    ETHYLENE OXIDE 0.5 ppm 5 PASS ND

    HEPTANE 500 ppm 5000 PASS ND

    METHANOL 25 ppm 250 PASS ND

    N-HEXANE 25 ppm 250 PASS ND

    PENTANES (N-PENTANE) 75 ppm 750 PASS ND

    PROPANE 500 ppm 5000 PASS ND

    TOLUENE 15 ppm 150 PASS ND

    TOTAL XYLENES 15 ppm 150 PASS ND

    TRICHLOROETHYLENE 2.5 ppm 25 PASS ND

    Residual Solvents PASSED

    Analyzed by Weight Extraction date Extracted By508 .0239g 07/27/20 01:07:20 508

    Analysis Method -SOP.T.40.032Analytical Batch -GA014302SOL Reviewed On - 07/29/20 14:54:38Instrument Used : GA-GCMS-001 Headspace SolventRunning On :Batch Date : 07/27/20 12:29:02

    Reagent Dilution Consums. ID

    24154107164282-100279984

    Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.40.032 Residual Solvents Analysis via GC-MS).

  • This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.

    Jeremy CampbellLab Director

    State License # CMTL-0001ISO Accreditation # 97164 ___________________

    Signature

    10/05/2020

    ___________________Signed On

    2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, USA

    Kaycha LabsCBD Cooling Rub Peppermint

    N/AMatrix : Derivative

    Certificate of Analysis PASSEDSouthern Sun

    11613 SW 234th StArcher, FL, 32618, USTelephone: (954) 336-1166Email: [email protected]

    Sample : GA00723001-001Harvest/LOT ID: CBD RUB 1000MGBatch# : CBD RUB1000MGSampled : 07/23/20Ordered : 07/23/20

    Sample Size Received : 60 mlCompleted : 08/03/20Expires: 08/03/21Sample Method : SOP Client Method

    Page 4 of 4

    Microbials PASSED

    Analyte LOD ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.

    Analysis Method -SOP.T.40.043 / SOP.T.40.044Analytical Batch -GA014214MIC Batch Date : 07/23/20Instrument Used : GA-093 PathogenDx ScannerRunning On :

    Analyzed by Weight Extraction date Extracted By1748 0.9422g 07/27/20 1748

    Dilution10Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) methodconsisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoidspurification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus,Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails themicrobiological-impurity testing.

    Mycotoxins PASSED

    Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A+ 0.002 ppm ND 0.02

    Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -GA014316MYC | Reviewed On - 07/29/20 09:44:43Instrument Used : GA-LCMS-001 MYCRunning On :Batch Date : 07/27/20 14:03:17

    Analyzed by Weight Extraction date Extracted By635 0.9950g 07/27/20 02:07:58 635

    Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be