N/A Matrix : Derivative Certificate Harvest/Lot ID: J27V01 ...
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report is an Kaycha Labs certification. The results relate only to the material or product analyzed. Test results are confidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batch material may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter, ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) and Limit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured by an analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholds for human safety for consumption and/or inhalation Jorge Segredo Lab Director State License # n/a ISO Accreditation # 97164 ___________________ Signature 11/12/2019 ___________________ Signed On Kaycha Labs 1500mg CBD Oil N/A Matrix : Derivative Certificate of Analysis SAMPLE:DA91107003-002 Harvest/Lot ID: J27V01 Seed to Sale #N/A Batch#: J27V02 Sample Size: 30 ml Ordered : 11/06/19 Sampled : 11/06/19 Completed: 11/12/19 Expires: 11/12/20 Sampling Method: SOP Client Method Nov 12, 2019 | Green Roads 5150 SW 48TH WAY DAVIE FL, USA 33314 PASSED PRODUCT IMAGE SAFETY RESULTS MISC. Pesticides PASSED Heavy Metals PASSED Microbials PASSED Mycotoxins PASSED Residuals Solvents PASSED Filth NOT TESTED Water Activity NOT TESTED Moisture NOT TESTED Terpenes TESTED CANNABINOID RESULTS Total THC 0.000% Total CBD 4.136% ND ND 4.136 % ND ND 0.011 % ND ND ND ND ND ND ND 41.360 mg/g ND ND 0.110 mg/g ND ND ND ND ND D9-THC THCA CBD CBDA CBN CBDV D8-THC THCV CBG CBGA CBC Cannabinoid Profile Test Analyst Weight Sample Prep : Extracted By : 450 3.1966g 2019-11-07 08:11:49 965 Analysis Method -SOP.T.40.020, SOP.T.30.050 Analytical Batch -DA007765 Reagent Dilution Consums. ID 110519.R03 400 76124-662 110519.R04 SFN-BX-1025 849C4-849AK 840C6-840H Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Transcript of N/A Matrix : Derivative Certificate Harvest/Lot ID: J27V01 ...
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
11/12/2019
___________________Signed On
Kaycha Labs1500mg CBD Oil
N/AMatrix : Derivative
Certificateof Analysis
SAMPLE:DA91107003-002Harvest/Lot ID: J27V01
Seed to Sale #N/ABatch#: J27V02
Sample Size: 30 mlOrdered : 11/06/19Sampled : 11/06/19
Completed: 11/12/19 Expires: 11/12/20Sampling Method: SOP Client Method
Nov 12, 2019 | Green Roads5150 SW 48TH WAY DAVIEFL, USA 33314
PASSED
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthNOT TESTED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesTESTED
CANNABINOID RESULTS
Total THC
0.000%Total CBD
4.136%
ND ND 4.136 % ND ND 0.011 % ND ND ND ND ND
ND ND41.360mg/g ND ND
0.110mg/g ND ND ND ND ND
D9-THC THCA CBD CBDA CBN CBDV D8-THC THCV CBG CBGA CBC
Cannabinoid Profile TestAnalyst Weight Sample Prep : Extracted By :450 3.1966g 2019-11-07 08:11:49 965
Analysis Method -SOP.T.40.020, SOP.T.30.050Analytical Batch -DA007765
Reagent Dilution Consums. ID
110519.R03 400 76124-662110519.R04 SFN-BX-1025
849C4-849AK840C6-840H
Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep andShimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
11/12/2019
___________________Signed On
Kaycha Labs1500mg CBD Oil
N/AMatrix : Derivative
Certificate of Analysis PASSED
Green Roads
5150 SW 48TH WAY DAVIEFL, USA 33314Telephone: (844) 747-3367Email:[email protected]
Sample : DA91107003-002,Harvest/LOT ID: J27V01,
Batch# : J27V02Sample Size : 30 mlOrdered : 11/06/19
Sampled : 11/06/19Completed : 11/12/19 Expires : 11/12/20Sample Method : SOP Client Method
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Terpenes TESTED
Terpenes TEST RESULT (%)
ALPHA-CEDRENE NDALPHA-HUMULENE NDALPHA-PINENE NDALPHA-TERPINENE NDBETA-MYRCENE 0.020BETA-PINENE NDBORNEOL NDCAMPHENE NDCAMPHOR NDCARYOPHYLLENE OXIDE NDCEDROL NDALPHA-BISABOLOL NDISOPULEGOL NDCIS-NEROLIDOL ND3-CARENE NDFENCHYL ALCOHOL NDHEXAHYDROTHYMOL NDEUCALYPTOL NDISOBORNEOL NDFARNESENE NDFENCHONE NDGAMMA-TERPINENE NDGERANIOL NDGERANYL ACETATE NDGUAIOL NDLIMONENE NDLINALOOL NDNEROL NDOCIMENE NDALPHA-PHELLANDRENE NDPULEGONE NDSABINENE NDSABINENE HYDRATE ND
Terpenes TEST RESULT (%)
TERPINEOL ND
TERPINOLENE ND
TRANS-CARYOPHYLLENE ND
TRANS-NEROLIDOL ND
VALENCENE ND
Terpenes TESTED
Analyst Weight Sample Prep : Extracted By :585 1.0979g 2019-11-08 04:11:27 585
Analysis Method -SOP.T.40.090Analytical Batch -DA007763
Reagent Dilution Consums. ID
10
Terpenoid profile screening is performed using GC-MS with Liquid Injection (Gas Chromatography –Mass Spectrometer) which can screen 38 terpenes using Method SOP.T.40.091 Terpenoid AnalysisVia GC/MS.
Total 0.021
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
11/12/2019
___________________Signed On
Kaycha Labs1500mg CBD Oil
N/AMatrix : Derivative
Certificate of Analysis PASSED
Green Roads
5150 SW 48TH WAY DAVIEFL, USA 33314Telephone: (844) 747-3367Email:[email protected]
Sample : DA91107003-002,Harvest/LOT ID: J27V01,
Batch# : J27V02Sample Size : 30 mlOrdered : 11/06/19
Sampled : 11/06/19Completed : 11/12/19 Expires : 11/12/20Sample Method : SOP Client Method
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Pesticides PASSED
Pesticides LOQ Action Level Units ResultCHLORDANE 0.010 0.1 ppm NDCAPTAN 0.100 3 ppm NDBOSCALID 0.010 3000 PPM NDDIMETHOATE 0.010 0.1 ppm NDABAMECTIN B1A 0.020 0.3 ppm NDCIS-PERMETHRIN 0.050 1 ppm NDSPINETORAM 0.010 PPM NDACEPHATE 0.010 3 ppm NDDIMETHOMORPH 0.005 3 ppm NDETHOPROPHOS 0.010 0.1 ppm NDACEQUINOCYL 0.050 2 ppm NDACETAMIPRID 0.010 3 ppm NDETOFENPROX 0.010 0.1 ppm NDALDICARB 0.020 0.1 ppm NDETOXAZOLE 0.010 1.5 ppm NDAZOXYSTROBIN 0.010 3 ppm NDFENHEXAMID 0.010 3 ppm NDBIFENAZATE 0.010 3 ppm NDFENOXYCARB 0.010 0.1 ppm NDFENPYROXIMATE 0.010 2 ppm NDBIFENTHRIN 0.010 0.5 ppm NDCARBARYL 0.010 0.5 ppm NDFIPRONIL 0.020 0.1 ppm NDFLONICAMID 0.010 2 ppm NDCARBOFURAN 0.010 0.1 ppm NDCHLORANTRANILIPROLE 0.010 3 ppm NDFLUDIOXONIL 0.010 3 ppm NDHEXYTHIAZOX 0.010 2 ppm NDCHLORFENAPYR 0.010 0.1 ppm NDIMAZALIL 0.010 0.1 ppm NDCHLORPYRIFOS 0.010 0.1 ppm NDIMIDACLOPRID 0.010 3 ppm NDCLOFENTEZINE 0.010 0.5 ppm NDKRESOXIM-METHYL 0.010 1 ppm NDCOUMAPHOS 0.005 0.1 ppm NDMALATHION 0.010 2 ppm NDCYPERMETHRIN 0.020 1 ppm NDDAMINOZIDE 0.020 0.1 ppm NDMETALAXYL 0.010 3 ppm ND
Pesticides LOQ Action Level Units ResultDICHLORVOS 0.050 0.1 ppm NDMETHIOCARB 0.010 0.1 ppm NDMETHOMYL 0.010 0.1 ppm NDDIAZANON 0.010 0.2 ppm NDMEVINPHOS 0.010 0.1 ppm NDMYCLOBUTANIL 0.010 3 ppm NDNALED 0.010 0.5 ppm NDOXAMYL 0.010 0.5 ppm NDPACLOBUTRAZOL 0.010 0.1 ppm NDTRANS-PERMETHRIN 0.050 1 ppm NDPHOSMET 0.010 0.2 ppm NDPIPERONYL BUTOXIDE 0.010 3 ppm NDPRALLETHRIN 0.050 0.4 ppm NDPROPICONAZOLE 0.010 1 ppm NDPROPOXUR 0.010 0.1 ppm NDPYRETHRIN I 0.010 1 ppm NDPYRIDABEN 0.010 3 ppm NDSPINOSAD (SPINOSYN A) 0.010 3 ppm NDSPINOSAD (SPINOSYN D) 0.010 3 ppm NDSPIROMESIFEN 0.010 3 ppm NDSPIROTETRAMAT 0.020 3 ppm NDSPIROXAMINE 0.010 0.1 ppm NDTEBUCONAZOLE 0.010 1 ppm NDTHIACLOPRID 0.010 0.1 ppm NDTHIAMETHOXAM 0.010 1 ppm NDTRIFLOXYSTROBIN 0.010 3 ppm ND
Pesticides PASSED
Analyst Weight Sample Prep : Extracted By :585 1.0465g 2019-11-07 12:11:10 1082
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch - DA007784
Reagent Dilution Consums. ID
SOP.T.30.065, SOP.T.40.065
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
11/12/2019
___________________Signed On
Kaycha Labs1500mg CBD Oil
N/AMatrix : Derivative
Certificate of Analysis PASSED
Green Roads
5150 SW 48TH WAY DAVIEFL, USA 33314Telephone: (844) 747-3367Email:[email protected]
Sample : DA91107003-002,Harvest/LOT ID: J27V01,
Batch# : J27V02Sample Size : 30 mlOrdered : 11/06/19
Sampled : 11/06/19Completed : 11/12/19 Expires : 11/12/20Sample Method : SOP Client Method
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Residual Solvents PASSED
SOLVENT ACTION LEVEL(PPM)
PASS/FAIL RESULT
PROPANE 2100 PASS ND
BUTANES (N-BUTANE) 2000 PASS ND
ETHYLENE OXIDE 5 PASS ND
METHANOL 250 PASS ND
ETHANOL 5000 PASS ND
PENTANES (N-PENTANE) 750 PASS ND
ETHYL ETHER 500 PASS ND
ACETONE 750 PASS ND
2-PROPANOL 500 PASS ND
ACETONITRILE 60 PASS ND
DICHLOROMETHANE 125 PASS ND
N-HEXANE 250 PASS ND
ETHYL ACETATE 400 PASS ND
BENZENE 1 PASS ND
HEPTANE 500 PASS ND
TOLUENE 150 PASS ND
CHLOROFORM 2 PASS ND
1,2-DICHLOROETHANE 2 PASS ND
TRICHLOROETHYLENE 25 PASS ND
1,1-DICHLOROETHENE 8 PASS ND
TOTAL XYLENES 150 PASS ND
Residual Solvents PASSED
Analyst Weight Sample Prep : Extracted By :850 0.0274g 2019-11-07 04:11:19 850
Analysis Method -SOP.T.40.032Analytical Batch -DA007806
Reagent Dilution Consums. ID
1
Residual solvents screening is performed using GC-MS which can detect below single digit ppmconcentrations. Currently we analyze for 34 Residual solvents. (Method: SOP.T.30.042 ResidualSolvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
11/12/2019
___________________Signed On
Kaycha Labs1500mg CBD Oil
N/AMatrix : Derivative
Certificate of Analysis PASSED
Green Roads
5150 SW 48TH WAY DAVIEFL, USA 33314Telephone: (844) 747-3367Email:[email protected]
Sample : DA91107003-002,Harvest/LOT ID: J27V01,
Batch# : J27V02Sample Size : 30 mlOrdered : 11/06/19
Sampled : 11/06/19Completed : 11/12/19 Expires : 11/12/20Sample Method : SOP Client Method
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Mycotoxins PASSED
Analyte Result Action LevelAFLATOXIN G2 NDAFLATOXIN G1 NDAFLATOXIN B2 NDAFLATOXIN B1 NDOCHRATOXIN A+ ND 0.02TOTAL AFLATOXINS 0.000 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA007785
Microbials PASSED
Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.
Heavy Metals PASSED
Reagent Dilution Consums. ID
50
Metal Result Action Level
ARSENIC ND 1.5CADMIUM ND 0.5LEAD ND 0.5MERCURY ND 3
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA007766
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma– Mass Spectrometer) which can screen down to below single digit ppbconcentrations for regulated heavy metals using Method SOP.T.30.052 SamplePreparation for Heavy Metals Analysis via ICP-MS and SOP.T.40.050 HeavyMetals Analysis via ICP-MS.
