N/A Matrix: Derivative Certificate Harvest/Lot ID: 012WP of ...
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report is an Kaycha Labs certification. The results relate only to the material or product analyzed. Test results are confidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batch material may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter, ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) and Limit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured by an analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholds for human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty of measurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for the pass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310. Jorge Segredo Lab Director State License # n/a ISO Accreditation # 97164 ___________________ Signature 05/29/2020 ___________________ Signed On 4131 SW 47th AVENUE SUITE 1408 Kaycha Labs Grounded N/A Matrix: Derivative Certificate of Analysis Sample:DA00526006-001 Harvest/Lot ID: 012WP Seed to Sale #N/A Batch Date :N/A Batch#: 012WP-A Sample Size Received: 15 ml Retail Product Size: 30 Ordered : 05/21/20 Sampled : 05/21/20 Completed: 05/29/20 Expires: 05/29/21 Sampling Method: SOP Client Method May 29, 2020 | Tonic CBD 2566 Pennsylvania Ave Sayre PA, 18840 PASSED Page 1 of 3 PRODUCT IMAGE SAFETY RESULTS MISC. Pesticides NOT TESTED Heavy Metals NOT TESTED Microbials PASSED Mycotoxins NOT TESTED Residuals Solvents PASSED Filth NOT TESTED Water Activity NOT TESTED Moisture NOT TESTED Terpenes NOT TESTED CANNABINOID RESULTS Total THC 0.203% Total CBD 5.144% Total Cannabinoids 5.852% CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA 0.372% ND 0.096% 0.011% ND 0.019% ND 0.049% 5.102% 0.203% ND 3.720 mg/g ND 0.960 mg/g 0.110 mg/g ND 0.190 mg/g ND 0.490 mg/g 51.020 mg/g 2.029 mg/g ND LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001 % % % % % % % % % % % Cannabinoid Profile Test Analyzed by Weight Extraction date : Extracted By : 450 3.0555g 05/26/20 09:05:40 965 Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 05/27/20 10:02:51 Analytical Batch -DA012653POT Instrument Used : DA-LC-003 Batch Date : 05/26/20 08:27:22 Reagent Dilution Consums. ID 032320.27 400 280678841 052620.R19 914C4-914AK 052620.R18 929C6-929H Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Transcript of N/A Matrix: Derivative Certificate Harvest/Lot ID: 012WP of ...
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
05/29/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsGrounded
N/AMatrix: Derivative
Certificateof Analysis
Sample:DA00526006-001Harvest/Lot ID: 012WP
Seed to Sale #N/ABatch Date :N/A
Batch#: 012WP-ASample Size Received: 15 ml
Retail Product Size: 30Ordered : 05/21/20Sampled : 05/21/20
Completed: 05/29/20 Expires: 05/29/21Sampling Method: SOP Client Method
May 29, 2020 | Tonic CBD2566 Pennsylvania Ave SayrePA, 18840
PASSEDPage 1 of 3
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesNOT TESTED
Heavy MetalsNOT TESTED
MicrobialsPASSED
MycotoxinsNOT TESTED
ResidualsSolventsPASSED
FilthNOT TESTED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesNOT TESTED
CANNABINOID RESULTS
Total THC
0.203%Total CBD
5.144%Total Cannabinoids
5.852%
CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA
0.372% ND 0.096% 0.011% ND 0.019% ND 0.049% 5.102% 0.203% ND
3.720mg/g ND
0.960mg/g
0.110mg/g ND
0.190mg/g ND
0.490mg/g
51.020mg/g
2.029mg/g ND
LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :450 3.0555g 05/26/20 09:05:40 965
Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 05/27/20 10:02:51Analytical Batch -DA012653POT Instrument Used : DA-LC-003 Batch Date : 05/26/20 08:27:22
Reagent Dilution Consums. ID
032320.27 400 280678841052620.R19 914C4-914AK052620.R18 929C6-929HFull spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
05/29/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsGrounded
N/AMatrix : Derivative
Certificate of Analysis PASSEDTonic CBD
2566 Pennsylvania Ave SayrePA, 18840Telephone: (516)313-6443Email: [email protected]
Sample : DA00526006-001Harvest/LOT ID: 012WPBatch# : 012WP-ASampled : 05/21/20Ordered : 05/21/20
Sample Size Received : 15 mlCompleted : 05/29/20Expires: 05/29/21Sample Method : SOP Client Method
Page 2 of 3
Residual Solvents PASSED
Solvent LOD Units ActionLevel(PPM)
Pass/Fail Result
1,1-DICHLOROETHENE 0.8 ppm 8 PASS ND
1,2-DICHLOROETHANE 0.2 ppm 2 PASS ND
2-PROPANOL 50 ppm 500 PASS ND
ACETONE 75 ppm 750 PASS ND
ACETONITRILE 6 ppm 60 PASS ND
BENZENE 0.1 ppm 1 PASS ND
BUTANES (N-BUTANE) 500 ppm 5000 PASS ND
CHLOROFORM 0.2 ppm 2 PASS ND
DICHLOROMETHANE 12.5 ppm 125 PASS ND
ETHANOL 500 ppm PASS ND
ETHYL ACETATE 40 ppm 400 PASS ND
ETHYL ETHER 50 ppm 500 PASS ND
ETHYLENE OXIDE 0.5 ppm 5 PASS ND
HEPTANE 500 ppm 5000 PASS ND
METHANOL 25 ppm 250 PASS ND
N-HEXANE 25 ppm 250 PASS ND
PENTANES (N-PENTANE) 75 ppm 750 PASS ND
PROPANE 500 ppm 5000 PASS ND
TOLUENE 15 ppm 150 PASS ND
TOTAL XYLENES 15 ppm 150 PASS ND
TRICHLOROETHYLENE 2.5 ppm 25 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By850 0.0204g 05/28/20 04:05:53 850
Analysis Method -SOP.T.40.032Analytical Batch -DA012745SOL Reviewed On - 05/29/20 14:31:33Instrument Used : DA-GCMS-002Batch Date : 05/28/20 16:43:30
Reagent Dilution Consums. ID
1 00279984161291-124154107
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.30.032 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
05/29/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsGrounded
N/AMatrix : Derivative
Certificate of Analysis PASSEDTonic CBD
2566 Pennsylvania Ave SayrePA, 18840Telephone: (516)313-6443Email: [email protected]
Sample : DA00526006-001Harvest/LOT ID: 012WPBatch# : 012WP-ASampled : 05/21/20Ordered : 05/21/20
Sample Size Received : 15 mlCompleted : 05/29/20Expires: 05/29/21Sample Method : SOP Client Method
Page 3 of 3
Microbials PASSED
Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.
Analysis Method -SOP.T.40.043 / SOP.T.40.045Analytical Batch -DA012657MIC | Reviewed On - 05/27/20 17:19:24Instrument Used : PathogenDX PCR_Array Scanner DA-111,PathogenDX PCR_DA-171Batch Date : 05/26/20 09:22:26
Analyzed by Weight Extraction date Extracted By513 1.0766g 05/26/20 09:05:23 1082
Reagent Dilution Consums. ID
050520.09 181019-274
101519.12 SG298A
032720.137 181207119C
022120.85 918C4-918J
032720.168 914C4-914AK
032720.180 929C6-929H
022120.46 50AX26219
Reagent Consums. ID032720.107032720.74032720.215032720.24
25219065190611634
Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR)method consisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as acrude lysate which avoids purification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli,Salmonella, Aspergillus fumigatus, Aspergillus flavus, Aspergillus niger, or Aspergillus terreus isdetected in 1g of a sample, the sample fails the microbiological-impurity testing.
