Muhammad Shahid Anwar - IMMT
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Research Muhammad Shahid Anwar Ph.D. (Physics.) Contact address: Colloids and Material Chemistry Department & TEM Lab CSIR-Institute of Mineral and Material Technology (IMMT) Formerly RRL, Acharya Vihar Bhubaneswar-751013, Odisha. INDIA. Email: [email protected] [email protected] https://sites.google.com/site/shahidanwr/ Telephone: +91-674-2379149(O) Publications Conferences Invited Talks Honors/Awards EXPERIENCE: Scientist-C: (March 2011 – Continuing) Colloids and Material Chemistry Department CSIR- IMMT, Bhubaneswar, India. Scientist-C: (Feb 2008 – March 2011), Central Instrumentation Facility (CIF) Division, CSIR- CECRI Karaikudi, Tamil Nadu India. Research Group Collaborations Photos
Transcript of Muhammad Shahid Anwar - IMMT
Department & TEM Lab CSIR-Institute of Mineral and Material
Technology (IMMT) Formerly RRL, Acharya Vihar Bhubaneswar-751013,
Odisha. INDIA.
Email: [email protected] [email protected] https://sites.google.com/site/shahidanwr/ Telephone: +91-674-2379149(O)
Department CSIR- IMMT, Bhubaneswar, India.
Scientist-C: (Feb 2008 – March 2011), Central Instrumentation Facility (CIF)
Division, CSIR- CECRI Karaikudi, Tamil Nadu India.
Research Group
Multiferroics Materials.
Thermoelectric materials.
Metallic Thin film, Hard coating, etc.
Electron microscopy:
Resolved the existing controversies of space-group in SrCaTiO3 ceramics, at different Ca
concentration level. Initially various space groups e.g. Pnma (Pbnm), I4/mcm, Imma, P21/m,
Cmcm were reported. On the basis of XRD, Electron microscopic and TEM simulation data above
listed space groups has been tested thoroughly and finally Pnma space group has been assigned
along with a new feasible space group P21212 as a minor phase. Phase coexistence studies are
under progress.
Relaxor Ferroelectrics:
A new lead free ferroelectric relaxor ceramics has been found in Hf doped BaTIO3 (i.e. BaTi1-
xHfxO3) ceramics. Crossover from normal to relaxor behaviour has been characterized and
shown as an efficient candidate for industrial usage. Established novel technique to characterize
relaxors.
Multiferroics: Synthesis of pure and doped BiFeO3, composite materials e.g. BiFeO3: LaFeO3,
BiFeO3:NiFe2O4 etc. for fundamental science and functional device applications.
Proton conductor: Development of BaCeO3 and BaZrO3 based Proton conductors material for
intermediate temperature operation.
Area of Interest: Current research activities are focused on thermoelectric materials,
Proton conducting fuel cell (PCFC), Metallic Thin film & Hard coating, etc.
Publications
Journals:
1. Relaxor ferroelectric behavior of “A” site deficient Bismuth doped Barium Titanate ceramic: T.
Badapanda & V. Senthil & D. K. Rana & S. Panigrahi & S. Anwar. J Electroceram 29 (2), 117 (2012)
2. Meso-Structured Silica-Nafion Hybrid Membranes for Direct Methanol Fuel Cells: A. K. Sahu, S.
Meenakshi, S. D. Bhat, A. Shahid, P. Sridhar, S. Pitchumani, and A. K. Shukla, Journal of the
Electrochemical Society, 159 (11) F1-F9 (2012)
3. Hydrolysis of SnCl2 on Polyaniline: Formation of Conducting PAni-SnO2 Composite with Enhanced
Electrochemical Properties: C R. K. Rao, M. Vijayan, Shahid Anwar, D. Jeyakumar, Journal of
Applied Polymer Science, Vol. 124, 4819–4826 (2012)
4. Low temperature stabilized rutile phase TiO2 films grown by sputtering: Swati S. Pradhan, S.K.
Pradhan, V. Bhavanasi, Sambita Sahoo, S.N. Sarangi, S. Anwar, P.K. Barhai, Thin Solid Films, Vol
520, Issue 6, 2012, Pages 1809-1813
5. A Comparative Study of Electrochemical Capacitive Behavior of NiFe2O4 Synthesized by different
Routes: Shahid Anwar, K. Sudalai Muthu, V. Ganesh and N. Lakshminarasimhan Journal of The
Electrochemical Society, 158 (9) 1-6 (2011)
6. Directed Synthesis of MC-PEDOT Composite Catalyst-Supports for Durable PEFCs: K. K. Tintula A. K.
Sahu, A. Shahid, S. Pitchumani, P. Sridhar and A. K. Shukla, Journal of The Electrochemical Society,
158 (6) B622-B631 (2011)
7. Effect of swift heavy ion irradiation in W/Co multilayer structures: S. Bagchi, Shahid Anwar and N.P.
Lalla Nuclear Inst. and Methods in Physics Research, B Volume: 268 Pages: 1601-1606 (2010)
8. Mesoporous Carbon and Poly (3, 4-ethylenedioxythiophene) Composite as Catalyst support for
Polymer Electrolyte Fuel Cells: Journal of Electrochemical Society. 157, B1679 (2010).
9. Structural and magnetic study of swift heavy ion irradiated W/Fe multilayer structure: S. Bagchi, S.
Jani, Shahid Anwar, N. Lakshmi and N.P. Lalla, Journal of Magnetism and Magnetic Materials
322, 3851 (2010).
10. Thermally Stimulated Depolarization Current Studies of Relaxation in L-Asparagine Monohydrate: D
Jain, L. S. Sharath Chandra, S. Bharadwaj, S. Anwar, V. Ganesan, N. P. Lalla, A. M. Awasthi , R. Nath
IEEE Transactions on Dielectrics and Electrical Insulation, Vol. 17, Issue 4, pp. 1128-1134,
August 2010.
11. Effect of swift heavy ion irradiation in Fe/W multilayer structures: S. Bagchi, Shahid Anwar and N.P.
Lalla Applied Surface Science (2009) 256. 541-546
12. Occurrence of a new superlattice phase across the antiferroelectric phase transition in Sr1-xCaxTiO3
(x=0.30, 0.40): Shahid Anwar and N. P. Lalla: Journal of Phys: Cond. Mat. (2008) 20, 325231
13. Effect of oxygenation on the structural and dielectric properties of Sr1-xCaxTiO3 with
0.20≤x≤0.40: Shahid Anwar and N. P. Lalla: Applied Physics Letter (2008) 92, 212901.
14. Electron microscopic studies of antiferroelectric phase in Sr0.60Ca0.40TiO3 ceramic: Shahid Anwar
and N. P. Lalla: Journal of Solid State chem. (2008) 181, 997
Lalla: Solid State Science (2008), 10 (3) 307.
16. Space group analysis of Sr1-xCaxTiO3 ceramics for x= 0.20, 0.27 & 0.30 through Electron diffraction:
Shahid Anwar and N. P. Lalla: Journal of Phys: Cond. Mat. (2007) 19, 436210.
17. Locating the normal to relaxor phase boundary in Ba(Ti1−xHfx)O3 ceramics: Shahid Anwar, P.R.
Sagdeo and N. P. Lalla: Mat. Res. Bull. (2008) 43, 1761.
18. Study of the relaxor behavior in BaTi1-xHfxO3 (0.20≤x≤0.30) ceramic: Shahid Anwar, P.R. Sagdeo and
N. P. Lalla: Solid State Science (2007) 9, 1054.
19. Crossover from classical to Relaxor ferroelectric in Ba(Ti1-xHfx)O3 ceramic: Shahid Anwar, P.R.
Sagdeo and N. P. Lalla: Journal of Phys: Cond. Mat. (2006) 16, 8445.
20. Ferroelectric Relaxor behavior in Hafnium doped Barium-Titanate ceramic: Shahid Anwar, P.R.
Sagdeo and N. P. Lalla: Solid State Comm. (2006) 138 331.
21. Strain induced coexistence of monoclinic and charge ordered phases in La1-xCaxMnO3 P.R. Sagdeo,
Shahid Anwar and N. P. Lalla: Physical Review B (2006) 76(1).
22. Powder X-ray diffraction and Reitveld Analysis of La1-xCaxMnO3 (0<x<1). P.R.Sagdeo, Shahid
Anwar and N. P. Lalla: Powder Diffraction (2006) 21 40.
23. The contribution of grain boundary and defects to the resistivity in the ferromagnetic state of
polycrystalline manganites. P.R. Sagdeo, Shahid Anwar, N. P. Lalla and S.I. Patil: J. Mag. and Mag.
Mat. (2006) 306, 60.
24. Electron diffraction evidence of charge-ordering at room-temperature in La1-xCaxMnO3
(0.55<x<0.67)P.R. Sagdeo, Shahid Anwar and N. P. Lalla: Solid State Comm. (2005) 137 158.
25. Unambiguous evidence for wurtzite phase in capped CdS quantum dots. S. K. Gautam, D. Pandey, S.N.
Upadhyay, Shahid Anwar and N.P. Lalla: Solid State Comm. (2008), 146 (9-10) 425
Conferences
1. “Evidence of thickness dependent stability of nanometer range of W/Ni multilayers against swift heavy ion irradiation” International Conference on ‘Advanced nanomaterials and Nanotechnology (ICANN-2009) at IIT-Guwahati
2. “Space group analysis and structural studies of Sr1-xCaxTiO3 through Convergent Beam Electron Diffraction technique” Madhya-Pradesh young science congress Bhopal (2009) -Oral Presentation
3. “Synthesis and characterization of nanostructured Ce0.8Y0.2O2-δ for SOFC” during Nov 22- 25 2009 in International conference on electrochemical power sources (ICEPS-2008) at thiruvanantpuram.
4. “Structural and dielectric studies on some perovskites based oxide ceramic” Proceedings of the 53rd DAE Solid State Physics Symposium (2008)-Oral Presentation
5. “Oxygenation effect on Sr1-xCaxTiO3 (0.20≤x≤0.40) perovskite ceramics” Proceedings of the 53rd DAE Solid State Physics Symposium (2008)
6. “Structural phase coexistence in Sr0.70Ca0.30TiO3 ceramic studied through electron diffraction.” Presented (Oral) at International conference (IUMRS-ICAM 2007) at Bangalore.
7. “Study of the relaxor behavior in Hafnium doped BaTiO3 ceramics (0.20≤x≤0.30)”. NCMRAT –2007, Aurangabad.
8. “Ferroelectric relaxor in BaTi0.75Hf0.25O3”. Proceedings of the DAE Solid Physics Symposium. (2006).
9. “Relaxor Behavior in hafnium doped barium titanate ceramic”. Proceedings of the DAE Solid Physics Symposium. 50, 819 (2005).
10. “Possibility of quick x-ray Reflectivity measurement using Energy Dispersive set-up”. Proceedings of the DAE Solid Physics Symposium. 49, 701 (2004).
Workshop:
1. 1 Month SERC School on “Condensed Matter and Materials Physics” at BHU during March 1 to 28 2006.
2. National DST Workshop on "Modern aspect in Electrochemical science and tedhonology", held at CSIR-CECRI karaikudi (15th -19th Sept., 2008).
Honors/Awards
Awards:
Awarded Madhya Pradesh Young scientist Award for physics in 2009 by MP council for science and Technology.
Recipient of National Scholarship CSIR-SRF during April 2007 - Feb 2008
Recipient of National Scholarship DST-JRF & SRF during Dec 2002-May 2006
Research Group
Scientists of CMC department & other departments of CSIR-IMMT and Project
Fellows/JRF/SRF of CMC department.
1. Dr. Niranjan Pd. Lalla, UGC-DAE-Consortium for scientific research, Indore,
India
3. Dr. Tanmaya Badapanda, CV Raman College, Bhubaneswar, India.
4. Dr. K Sarvanan B, Kongunadu Arts and Science College Coimbatore, India.
5. Dr. Kallol Das, St. Aloysius College, Jabalpur, India.
Invited Talks
Invited Talks
“Structural and dielectric studies on some perovskites based oxide ceramic” BARC Mumbai Dec-2008
“Space group analysis and structural studies of Sr1-xCaxTiO3 through Convergent Beam Electron Diffraction technique” MPCST Bhopal (28Feb 2009)
“X-ray diffraction technique in material science” Algappa Engineering college Bhubaneswar May 2009.
“Basic of Transmission Electron Microscope (TEM) and its Applications. CSIR-CECRI Karaikudi, 19th Jan 2011.
Projects
IMMT)
Email: [email protected] [email protected] https://sites.google.com/site/shahidanwr/ Telephone: +91-674-2379149(O)
Department CSIR- IMMT, Bhubaneswar, India.
Scientist-C: (Feb 2008 – March 2011), Central Instrumentation Facility (CIF)
Division, CSIR- CECRI Karaikudi, Tamil Nadu India.
Research Group
Multiferroics Materials.
Thermoelectric materials.
Metallic Thin film, Hard coating, etc.
Electron microscopy:
Resolved the existing controversies of space-group in SrCaTiO3 ceramics, at different Ca
concentration level. Initially various space groups e.g. Pnma (Pbnm), I4/mcm, Imma, P21/m,
Cmcm were reported. On the basis of XRD, Electron microscopic and TEM simulation data above
listed space groups has been tested thoroughly and finally Pnma space group has been assigned
along with a new feasible space group P21212 as a minor phase. Phase coexistence studies are
under progress.
Relaxor Ferroelectrics:
A new lead free ferroelectric relaxor ceramics has been found in Hf doped BaTIO3 (i.e. BaTi1-
xHfxO3) ceramics. Crossover from normal to relaxor behaviour has been characterized and
shown as an efficient candidate for industrial usage. Established novel technique to characterize
relaxors.
Multiferroics: Synthesis of pure and doped BiFeO3, composite materials e.g. BiFeO3: LaFeO3,
BiFeO3:NiFe2O4 etc. for fundamental science and functional device applications.
Proton conductor: Development of BaCeO3 and BaZrO3 based Proton conductors material for
intermediate temperature operation.
Area of Interest: Current research activities are focused on thermoelectric materials,
Proton conducting fuel cell (PCFC), Metallic Thin film & Hard coating, etc.
Publications
Journals:
1. Relaxor ferroelectric behavior of “A” site deficient Bismuth doped Barium Titanate ceramic: T.
Badapanda & V. Senthil & D. K. Rana & S. Panigrahi & S. Anwar. J Electroceram 29 (2), 117 (2012)
2. Meso-Structured Silica-Nafion Hybrid Membranes for Direct Methanol Fuel Cells: A. K. Sahu, S.
Meenakshi, S. D. Bhat, A. Shahid, P. Sridhar, S. Pitchumani, and A. K. Shukla, Journal of the
Electrochemical Society, 159 (11) F1-F9 (2012)
3. Hydrolysis of SnCl2 on Polyaniline: Formation of Conducting PAni-SnO2 Composite with Enhanced
Electrochemical Properties: C R. K. Rao, M. Vijayan, Shahid Anwar, D. Jeyakumar, Journal of
Applied Polymer Science, Vol. 124, 4819–4826 (2012)
4. Low temperature stabilized rutile phase TiO2 films grown by sputtering: Swati S. Pradhan, S.K.
Pradhan, V. Bhavanasi, Sambita Sahoo, S.N. Sarangi, S. Anwar, P.K. Barhai, Thin Solid Films, Vol
520, Issue 6, 2012, Pages 1809-1813
5. A Comparative Study of Electrochemical Capacitive Behavior of NiFe2O4 Synthesized by different
Routes: Shahid Anwar, K. Sudalai Muthu, V. Ganesh and N. Lakshminarasimhan Journal of The
Electrochemical Society, 158 (9) 1-6 (2011)
6. Directed Synthesis of MC-PEDOT Composite Catalyst-Supports for Durable PEFCs: K. K. Tintula A. K.
Sahu, A. Shahid, S. Pitchumani, P. Sridhar and A. K. Shukla, Journal of The Electrochemical Society,
158 (6) B622-B631 (2011)
7. Effect of swift heavy ion irradiation in W/Co multilayer structures: S. Bagchi, Shahid Anwar and N.P.
Lalla Nuclear Inst. and Methods in Physics Research, B Volume: 268 Pages: 1601-1606 (2010)
8. Mesoporous Carbon and Poly (3, 4-ethylenedioxythiophene) Composite as Catalyst support for
Polymer Electrolyte Fuel Cells: Journal of Electrochemical Society. 157, B1679 (2010).
9. Structural and magnetic study of swift heavy ion irradiated W/Fe multilayer structure: S. Bagchi, S.
Jani, Shahid Anwar, N. Lakshmi and N.P. Lalla, Journal of Magnetism and Magnetic Materials
322, 3851 (2010).
10. Thermally Stimulated Depolarization Current Studies of Relaxation in L-Asparagine Monohydrate: D
Jain, L. S. Sharath Chandra, S. Bharadwaj, S. Anwar, V. Ganesan, N. P. Lalla, A. M. Awasthi , R. Nath
IEEE Transactions on Dielectrics and Electrical Insulation, Vol. 17, Issue 4, pp. 1128-1134,
August 2010.
11. Effect of swift heavy ion irradiation in Fe/W multilayer structures: S. Bagchi, Shahid Anwar and N.P.
Lalla Applied Surface Science (2009) 256. 541-546
12. Occurrence of a new superlattice phase across the antiferroelectric phase transition in Sr1-xCaxTiO3
(x=0.30, 0.40): Shahid Anwar and N. P. Lalla: Journal of Phys: Cond. Mat. (2008) 20, 325231
13. Effect of oxygenation on the structural and dielectric properties of Sr1-xCaxTiO3 with
0.20≤x≤0.40: Shahid Anwar and N. P. Lalla: Applied Physics Letter (2008) 92, 212901.
14. Electron microscopic studies of antiferroelectric phase in Sr0.60Ca0.40TiO3 ceramic: Shahid Anwar
and N. P. Lalla: Journal of Solid State chem. (2008) 181, 997
Lalla: Solid State Science (2008), 10 (3) 307.
16. Space group analysis of Sr1-xCaxTiO3 ceramics for x= 0.20, 0.27 & 0.30 through Electron diffraction:
Shahid Anwar and N. P. Lalla: Journal of Phys: Cond. Mat. (2007) 19, 436210.
17. Locating the normal to relaxor phase boundary in Ba(Ti1−xHfx)O3 ceramics: Shahid Anwar, P.R.
Sagdeo and N. P. Lalla: Mat. Res. Bull. (2008) 43, 1761.
18. Study of the relaxor behavior in BaTi1-xHfxO3 (0.20≤x≤0.30) ceramic: Shahid Anwar, P.R. Sagdeo and
N. P. Lalla: Solid State Science (2007) 9, 1054.
19. Crossover from classical to Relaxor ferroelectric in Ba(Ti1-xHfx)O3 ceramic: Shahid Anwar, P.R.
Sagdeo and N. P. Lalla: Journal of Phys: Cond. Mat. (2006) 16, 8445.
20. Ferroelectric Relaxor behavior in Hafnium doped Barium-Titanate ceramic: Shahid Anwar, P.R.
Sagdeo and N. P. Lalla: Solid State Comm. (2006) 138 331.
21. Strain induced coexistence of monoclinic and charge ordered phases in La1-xCaxMnO3 P.R. Sagdeo,
Shahid Anwar and N. P. Lalla: Physical Review B (2006) 76(1).
22. Powder X-ray diffraction and Reitveld Analysis of La1-xCaxMnO3 (0<x<1). P.R.Sagdeo, Shahid
Anwar and N. P. Lalla: Powder Diffraction (2006) 21 40.
23. The contribution of grain boundary and defects to the resistivity in the ferromagnetic state of
polycrystalline manganites. P.R. Sagdeo, Shahid Anwar, N. P. Lalla and S.I. Patil: J. Mag. and Mag.
Mat. (2006) 306, 60.
24. Electron diffraction evidence of charge-ordering at room-temperature in La1-xCaxMnO3
(0.55<x<0.67)P.R. Sagdeo, Shahid Anwar and N. P. Lalla: Solid State Comm. (2005) 137 158.
25. Unambiguous evidence for wurtzite phase in capped CdS quantum dots. S. K. Gautam, D. Pandey, S.N.
Upadhyay, Shahid Anwar and N.P. Lalla: Solid State Comm. (2008), 146 (9-10) 425
Conferences
1. “Evidence of thickness dependent stability of nanometer range of W/Ni multilayers against swift heavy ion irradiation” International Conference on ‘Advanced nanomaterials and Nanotechnology (ICANN-2009) at IIT-Guwahati
2. “Space group analysis and structural studies of Sr1-xCaxTiO3 through Convergent Beam Electron Diffraction technique” Madhya-Pradesh young science congress Bhopal (2009) -Oral Presentation
3. “Synthesis and characterization of nanostructured Ce0.8Y0.2O2-δ for SOFC” during Nov 22- 25 2009 in International conference on electrochemical power sources (ICEPS-2008) at thiruvanantpuram.
4. “Structural and dielectric studies on some perovskites based oxide ceramic” Proceedings of the 53rd DAE Solid State Physics Symposium (2008)-Oral Presentation
5. “Oxygenation effect on Sr1-xCaxTiO3 (0.20≤x≤0.40) perovskite ceramics” Proceedings of the 53rd DAE Solid State Physics Symposium (2008)
6. “Structural phase coexistence in Sr0.70Ca0.30TiO3 ceramic studied through electron diffraction.” Presented (Oral) at International conference (IUMRS-ICAM 2007) at Bangalore.
7. “Study of the relaxor behavior in Hafnium doped BaTiO3 ceramics (0.20≤x≤0.30)”. NCMRAT –2007, Aurangabad.
8. “Ferroelectric relaxor in BaTi0.75Hf0.25O3”. Proceedings of the DAE Solid Physics Symposium. (2006).
9. “Relaxor Behavior in hafnium doped barium titanate ceramic”. Proceedings of the DAE Solid Physics Symposium. 50, 819 (2005).
10. “Possibility of quick x-ray Reflectivity measurement using Energy Dispersive set-up”. Proceedings of the DAE Solid Physics Symposium. 49, 701 (2004).
Workshop:
1. 1 Month SERC School on “Condensed Matter and Materials Physics” at BHU during March 1 to 28 2006.
2. National DST Workshop on "Modern aspect in Electrochemical science and tedhonology", held at CSIR-CECRI karaikudi (15th -19th Sept., 2008).
Honors/Awards
Awards:
Awarded Madhya Pradesh Young scientist Award for physics in 2009 by MP council for science and Technology.
Recipient of National Scholarship CSIR-SRF during April 2007 - Feb 2008
Recipient of National Scholarship DST-JRF & SRF during Dec 2002-May 2006
Research Group
Scientists of CMC department & other departments of CSIR-IMMT and Project
Fellows/JRF/SRF of CMC department.
1. Dr. Niranjan Pd. Lalla, UGC-DAE-Consortium for scientific research, Indore,
India
3. Dr. Tanmaya Badapanda, CV Raman College, Bhubaneswar, India.
4. Dr. K Sarvanan B, Kongunadu Arts and Science College Coimbatore, India.
5. Dr. Kallol Das, St. Aloysius College, Jabalpur, India.
Invited Talks
Invited Talks
“Structural and dielectric studies on some perovskites based oxide ceramic” BARC Mumbai Dec-2008
“Space group analysis and structural studies of Sr1-xCaxTiO3 through Convergent Beam Electron Diffraction technique” MPCST Bhopal (28Feb 2009)
“X-ray diffraction technique in material science” Algappa Engineering college Bhubaneswar May 2009.
“Basic of Transmission Electron Microscope (TEM) and its Applications. CSIR-CECRI Karaikudi, 19th Jan 2011.
Projects
IMMT)
