M.Tech (Chemical) PDE - UPES

UNIVERSITY OF PETROLEUM & ENERGY STUDIES


M. TECH. CHEMICAL ENGINEERING (with specialization in PROCESS DESIGN ENGINEERING)

(VERSION 1.0)

w.e.f. 2017

_________________________________________________________________________________________

UPES Campus Tel: + 91-135-2261090/91 “Energy Acres” Fax: + 91-135-2694204 P.O Bidholi via Prem Nagar, Bidholi URL: www.upes.ac.in Dehradun – 248007 (Uttarakhand)


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@ UPES


M.TECH. CHEMICAL ENGINEERING (with specialization in

PROCESS DESIGN ENGINEERING) w.e.f 2017

SEMESTER I SEMESTER II

Subject Code Subject Credits


CHPD 7001 Transport Phenomena 3 CHPD 7008 Process Design and Flow Sheeting 3

CHPD 7002 Chemical Engineering Computing 3 CHPD 7009

Process Modeling and Simulation 3

CHPD 7003 Advanced Thermodynamics 3 CHPD 7010

Mass Transfer Equipment Design and Separation Processes 3

CHPD 7004 Chemical Reactor Engineering and Design 3 CHPD 7011

Principles of Chemical Process Safety 3

CHPD 7005 Fluid Flow and Heat Transfer Equipment Design 3

Elective 1 from among a basket of available courses given below 3

CHPD 7006 Petroleum Refining, Petrochemicals and Polymers 3

Elective 2 from among a basket of available courses given below 3

(ELECTIVES) Available basket

CHPD 7012 Systems Analysis and Optimization 3

LSCM 8001 Project Management and Contract Administration 3

CHPD 7013 Advanced Process Control 3

+ +

CHPD 7113 Advanced Process Control Lab 1

CHPD 7014 Biochemical Engineering 3

CHPD 7015 Gasification Technology 3

CHPD 7016 Polymer Engineering 3

CHPD 7017 Plant Utility Equipment and Systems 3

CHPD 7020 Catalysis and Catalytic Materials 3

PRACTICAL PRACTICAL

CHPD 7102 Chemical Engineering Computing Lab 1 Elective Lab (if applicable) 1

TOTAL 19 TOTAL 18/19 SEMESTER III

SEMESTER IV



DIST 8102 Dissertation I

17

DIST 8103 Dissertation II

17 (including two seminars) (including two seminars)

Summer CORE COURSES (6 weeks) Credits

CHPD 8001 Plant Simulation 5

TOTAL 22 TOTAL 17

Total Credits 76/77


Program Outcomes:

1. Scholarship of Knowledge - Acquire in-depth knowledge of specific discipline and global perspective, with an ability to discriminate, evaluate, analyze and synthesize existing and new knowledge, and integration of the same for enhancement of knowledge pool.

2. Critical Thinking - Analyze complex engineering problems critically, apply independent judgement for synthesizing information to make intellectual and/or creative advances for conducting research in a wider theoretical, practical and policy context.

3. Problem Solving - Think laterally and originally, conceptualize and solve engineering problems, evaluate a wide range of potential solutions for those problems and arrive at feasible, optimal solutions after considering public health and safety, cultural, societal and environmental factors in the core areas of expertise.

4. Research Skill - Extract information through literature survey and experiments, apply appropriate research methodologies, techniques and tools, design, conduct experiments, analyze and interpret data, contribute individually/in group(s) to the development of scientific/technological knowledge in one or more domains of engineering.

5. Usage of modern tools - Create, select, learn and apply appropriate techniques, resources, and modern engineering and IT tools, including prediction and modelling, to complex engineering activities with an understanding of the limitations.

6. Collaborative and Multidisciplinary work – Demonstrate collaboration to foster multidisciplinary scientific research, also demonstrate decision-making abilities to achieve common goals.

7. Project Management and Finance - Demonstrate knowledge and understanding to manage projects efficiently in respective disciplines and multidisciplinary environments after consideration of economical and financial factors.

8. Communication - Communicate with the engineering community and with society, regarding complex engineering activities confidently and effectively and give and receive clear instructions.

9. Life-long Learning - Recognize the need for, and have the preparation and ability to engage in life-long learning independently, with a high level of enthusiasm and commitment to improve knowledge and competence continuously.

10. Ethical Practices and Social Responsibility - Acquire professional and intellectual integrity, professional code of conduct, ethics of research and scholarship, consideration of the impact of research outcomes on professional practices and an understanding of responsibility to contribute to the community for sustainable development of society.

11. Independent and Reflective Learning - Observe and examine critically the outcomes of one’s actions and make corrective measures subsequently, and learn from mistakes without depending on external feedback.

Program Specific Outcomes:

PSO1. Apply the concepts and skills of Chemical Engineering to provide focused and practical solutions to advanced problems of Process Design Engineering

PSO2. Analyze the solutions obtained for feasibility, reliability, economics and safety using experimental and computational tools.


Course Objectives

1. To help the students to understand the fundamentals of momentum transfer. 2. To enable students to apply momentum transfer concepts to solve real-life problems. 3. To give the students a perspective to appreciate the use of heat and mass transfer in solving

day to day activities 4. To enable students to apply the concepts in design industrial or fundamental research in

transport problems

Course Outcomes On completion of this course, the students will be able to CO1. Apply the concepts of transport phenomena to solve problems in momentum transfer

and can write codes to solve fundamental chemical engineering problems using MATLAB CO2. Apply the concepts of transport phenomena to solve problems in heat transfer also

simulate chemical engineering operations CO3. Apply the concepts of transport phenomena to solve problems in mass transfer

Catalog Description While momentum, heat, and mass transfer developed independently as branches of classical physics long ago, their unified study has found its place as one of the fundamental engineering sciences. This development, in turn, less than half a century old, continues to grow and to find applications in new fields such as biotechnology, microelectronics, nanotechnology, and polymer science. The essence of this subject is the careful and compact statement of the conservation principles, along with the flux expressions, with emphasis on the similarities and differences among the three transport processes considered. Often, specialization to the boundary conditions and the physical properties in a specific problem can provide useful insight with minimal effort. Course Content

Unit I: 8 lecture hours Constitutive Equations: Newton’s Law of Viscosity, Non-Newtonian Fluids, Shell Momentum Balances and Velocity Distributions in Laminar Flow, Flow of non-Newtonian Fluids. Fourier’s Law of Heat Conduction in Simple Laminar Flow. Unit II: 14 lecture hours Equation of Continuity and Navier-Stokes (NS) Equation, Flow through Conduits and Flow over Submerged Objects, Boundary Layer Theory, Basics of Turbulence and Turbulent Flows, Reynold’s Averaged NS Equations, Prandtl’s Mixing Length, Universal Distribution Law, Turbulent Flow in Pipes Multiphase Flow, Gas-Liquid Flows, Gas-Solid Flows, Ergun Equation. Unit III: 14 lecture hours

CHPD 7001 Transport Phenomena L T P C

Version 1.0 3 0 0 3

Pre-requisites/Exposure Basic Engineering Mathematics, Fluid Mechanics, Thermodynamics, Heat Transfer and Mass Transfer

Co-requisites --


Applications of the Energy and Component Mass Balance Equations, Interphase Transport and Transfer Coefficients. Fick's Law of Binary Diffusion (Molecular Mass Transport), Temperature and Pressure Dependence of Diffusivities, Mass Transfer Theories, Concentration Distributions in Solids and in Laminar Flow. Unsteady state momentum, energy and mass transfer. Simultaneous momentum, heat and mass transfer Text Books R. B. Bird, W. E. Stewart and E. N. Lightfoot, Transport Phenomena, 2nd Ed., Wiley, New York, 2002.

Reference Books C. J. Geankoplis, Transport Processes and Separation Process Principles, 4th Ed., Prentice Hall, Upper Saddle River, NJ, 2003.

W. M. Deen, Analysis of Transport Phenomena, Oxford University Press, New York, 1998.

Modes of Evaluation: Quiz/Assignment/ presentation/ extempore/ Written Examination Examination Scheme:

Components Seminar/Review Paper Internal Assessment ESE Weightage (%) 20 30 50

Relationship between the Course Outcomes (COs) and Program Outcomes (POs)

Mapping between COs and POs

Course Outcomes (COs) Mapped Program Outcomes

CO1 Apply the concepts of transport phenomena to solve problems in momentum transfer and can write codes to solve fundamental chemical engineering problems using MATLAB

PO1, PO3, PO4, PO5

CO2 Apply the concepts of transport phenomena to solve problems in heat transfer also simulate chemical engineering operations

PO2, PO3, PO4, PO5

CO3 Apply the concepts of transport phenomena to solve problems in mass transfer

PO2, PO3, PO4, PO5


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Course Title PO1 PO2 PO3 PO4 PO5 PO6 PO7 PO8 PO9 PO10 PO11 PSO1 PSO2

CHPD 7001

Transport Phenomena 3 3 3 2 3 - - - - - - 2

1=weakly mapped 2= moderately mapped 3=strongly mapped


Course Objectives

5. To understand the solution techniques of linear and nonlinear algebraic equations using matrix algebra

6. To understand the solution techniques of numerically, interpolation, differentiation and integration problems.

7. To enable students to obtain and solve the sets of coupled, non-linear ordinary differential equations of the initial value kind (ODE-IVPs) and look at the stability and accuracy of integration algorithms.

Course Outcomes On completion of this course, the students will be able to

CO1. Explain and solve sets of coupled linear algebraic equations CO2. Explain and solve for the eigenvalues of matrices and interpret them in terms of

stability of systems CO3. Explain and solve sets of coupled non-linear algebraic equations CO4. Explain and solve sets of coupled, non-linear ordinary differential equations of the

initial value kind (ODE-IVPs) and look at the stability and accuracy of integration algorithms

CO5. Explain and solve sets of coupled, non-linear ordinary differential equations of the boundary value kind (ODE-BVPs)

CO6. Explain and solve sets of coupled, non-linear partial differential equations (parabolic, elliptic and hyperbolic)

Catalog Description Chemical engineering systems are formulated using algebraic, ordinary and partial differential equations. The understanding of solution techniques of these equations will enable students to design and develop chemical engineering systems. Students will learn about various solution methods available along with selection criterion, greater accuracy and lesser computation time. Students will be encouraged to actively take part in classroom teaching and all assignments. Course Content

Unit I: 3 lecture hours Linear Algebraic Equations, Gauss Elimination, Gauss-Seidel, SOR Methods Unit II: 2 lecture hours Eigenvalues, Eigenvectors, Stability of Systems, Fadeev-Leverrier Method

CHPD7002 Chemical Engineering Computing L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure UG level Mathematics and Chemical Engineering courses

Co-requisites --


Unit III: 4 lecture hours Solutions of Nonlinear Algebraic Equations: Successive Substitutions and Newton-Raphson; Multiplicity of Solutions; Singularity Theory Unit IV: 8 lecture hours Solutions of Ordinary Differential Equations-Initial Value Problems (ODE-IVPs): Stiffness; Explicit and Implicit Methods; Runge-Kutta Methods; Stability; Accuracy, Gear’s package for ODE-IVPs; DDASSL package for DAEs Unit V: 15 lecture hours Solutions of Ordinary-Differential Equations-Boundary Value Problems (ODE-BVPs): Finite Difference; Orthogonal Collocation; Orthogonal Collocation on Finite Elements; Galerkin Finite Elements; Shooting Methods Unit VI: 8 lecture hours Solutions of Partial Differential Equations: Finite Difference; Collocation; Finite Elements Text Books Gupta, Santosh K.; Numerical Methods for Engineers, New Age Intl. Publishers, New Delhi, 3rd (Indian) Ed., 2015; 3rd (NAS, UK) Ed., 2014. The 2nd Edition will be issued to you by the UPES Library. If you wish to purchase a personal copy, please buy the 3rd Indian edition)

Reference Books

Carnahan, B.; Luther, H. A. and Wilkes, J. O.; Applied Numerical Methods, Wiley, New York, 1969 (a bit outdated now – yet a classic when it first came out)

Finlayson, B. A.; Nonlinear Analysis in Chemical Engineering, McGraw Hill, New York, 1980 (a bit at an advanced level – errata is quite long), re-published by Bruce Alan Finlayson, Seattle, USA, 2003

Lapidus, L. and Seinfeld, J. H.; Numerical Solutions of ODEs, Academic Press, New York, 1971

Davis, M. E.; Numerical Methods and Modelling for ChE, Wiley, New York, 1984 (short, yet good presentation), re-published by Dover Publications, 2013

Chapra, S. C. and Canale, R.; Numerical Methods for Engineers, 7th Ed., 2014 (softcover edition available) Modes of Evaluation: Quiz/Assignment/ presentation/ extempore/ Written Examination Examination Scheme:





Course Outcomes (COs) Mapped

Programme Outcomes

CO1 Explain and solve sets of coupled linear algebraic equations PO1, PO3,

CO2 Explain and solve for the eigenvalues of matrices and interpret them in terms of stability of systems PO1, PO3

CO3 Explain and solve sets of coupled non-linear algebraic equations

PO2, PO3

CO4

Explain and solve sets of coupled, non-linear ordinary differential equations of the initial value kind (ODE-IVPs) and look at the stability and accuracy of integration algorithms

PO2, PO3, PO5

CO5 Explain and solve sets of coupled, non-linear ordinary differential equations of the boundary value kind (ODE-BVPs)

PO2, PO3, PO5

CO6 Explain and solve sets of coupled, non-linear partial differential equations (parabolic, elliptic and hyperbolic)

PO2, PO3, PO5


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CHPD7002 Chemical Engineering Computing

2 3 3 3 2 3



Model Question Paper

Name:

Enrolment No:

Course: CHPD7002 – Chemical Engineering Computing Programme: M. Tech (CE+PD) Semester: I Time: 03 hrs. Max. Marks:100 Instructions:

1. Show all intermediate steps of your answers (and not just the final answers) for marks 2. Please answer the questions in the sequence: 1, 2, 3. You can do this by assigning, a priori, a few pages to each

question, in the correct sequence. You may then answer the questions in whatever sequence you wish to, all parts in one place.

3. No student is allowed to leave the exam hall in the first hour of the exam

SECTION A ( attempt all questions)

1. Consider the following non-linear ODE-BVP

23

25 3 0

0 : 0; 1: ( 1) 3

d y dyy

dx dxdy

x x y xdx

;

Using the OC for the non-symmetric case, and with N + 2 = 4:

(a) What are the numerical values of x2 and x3 (03)

(b) Give the simplified OC equation for x1 = 0 (take ALL the constants and the non-linear

terms to the right hand side) (08)

(c) Give the simplified OC equation for point 2 (keep the Bij and Aij terms separate) (08)

Continued . . .

(d) Give the simplified OC equation for point 3 (keep the Bij and Aij terms separate) (08)

(e) Fill up the following matrix form of these equations in the question paper itself

(keeping the numerical values of the Bij and Aij terms separate in the first equation

below and the combined numerical values in the second equation)

(08)

[30] CO6, CO7


NOTE that there are only three rows (and not four) in the equation given below.

2. We wish to study the stability of the Hermite explicit ODE-IVP algorithm (with q – 1 = 3; α1 = ―4, α2 = 5, β1 = 4, β2 = 2, all other αi, βi zero; Table 5.1 of the text).

(a) Obtain expressions for all the roots, μi, of the characteristic equation for this algorithm (use first principles) (10)

(b) Obtain the values of all the μis for values of hλ given in the Table below. Fill these

up in the Table. Also, fill up the corresponding values of exp(hλ). (10)

[35] CO5


hλ μ1 μ2 μ3 (if present),

etc. exp(hλ)

0.0 ─ 0.5 ─ 1.0 ─ 2.0 + 1.0

(c) Identify which of these μi is the principal root of the characteristic equation. (05)

(d) Discuss the stability of this algorithm if both h and λ are real (h positive and λ negative). (10)

3. Consider the three-variable non-linear algebraic equations in the final matrix equation in Q. 1 (on page 2). We wish to use the multi-variable Newton-Raphson technique to reduce these into linear algebraic equations in the three variables, y1, y2 and y3.

(a) Write down the second of these equations in the form, F2(y1, y2, y3) = 0. Then simplify this using the Newton-Raphson technique to obtain the 3-variable linear algebraic equation. (15)

(b) Now, write down the third of these equations in the form, F3(y1, y2, y3) = 0, and obtain the 3-variable linear algebraic equation. (10)

(c) Finally, write down the first of these equations in the form, F1(y1, y2, y3) = 0, and obtain the corresponding 3-variable linear algebraic equation (Hint: You may be able to do this part fast). (05)

Hint: Write the simplified equations in terms of the iteration numbers, k + 1 and k.

You do not need to go any further for the examination.

(d) Fill up these equations in the matrix equation given on the next page (page 4) in the question paper itself (05)

[35]

CO1, CO2, CO3, CO4


Course Objectives

1. To dwell with all laws of Thermodynamics and exhaustive discussions on the thermodynamics of Solutions and Petroleum fractions.

Course Outcomes On completion of this course, the students will be able to CO1.Learn about the basic premises on which the laws of thermodynamics rest. CO2.Analyze various thermodynamic problems and solve them.

Catalog Description Studies of Advance thermodynamics is necessary and sufficient. Course Content

Unit I: 8 lecture hours Review Basic concepts of Thermodynamics Zeroth, First, Second & Third laws. Reversible & Irreversible Processes. Enthalpy, Entropy, PVT behavior & Equations of State. Unit II: 8 lecture hours Thermodynamic Properties Fundamental Equations. Gibbs Free Energy-Maxwell Relations. Phase Equilibrium. Clausius Clapeyron Equation, Vapor–liquid equilibrium calculations. Triple Points. Unit III: 7 lecture hours Phase Equilibrium Chemical potential, Gibbs Free Energy, Gibbs-Duhem Equations, Fugacity and fugacity-coefficient for pure gases and gas mixtures. Generalized correlations for fugacity coefficients. Excess properties. Unit IV: 8 lecture hours Equilibrium in Solutions Chemical Reaction Equilibrium, Review equilibrium constants, Effects of temperature , pressure and composition on equilibrium constant, Phase rule and Duhem’s theorem for reacting systems. Introduction to Statistical Thermodynamics. Unit V: 5 lecture hours Hydrocarbon Thermodynamics Pseudo-components of petroleum fractions. Phase Equilibrium, EFV–TBP-ASTM assay at super atmospheric pressures. Text Books

CHPD 7003 Advance Thermodynamics L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure Thermodynamics

Co-requisites --


1. Thermodynamics, an Engineering Approach; Cengel and Boles; McGrawHill, 7e Pulication.

Reference Books 1. Introduction to Chemical Engineering Thermodynamics, Gopinath Halder,




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CHPD7003 Process Optimization 3 3 3

3



Programme Outcomes

CO1 Understanding the basics of Process Optimization PO10

CO2 Application of the optimization theory in chemical engineering problem. PO10

CO3

PO12

CO4 PO12


Course Objectives

1. To apply basics of engineering (UG level) to understand the reaction kinetics. 2. To able to apply conservation laws on reactor volume to get design equations of different

reactors. 3. Use of modern software for solving reactor design equations.

PROGRAM SPECIFIC OUTCOMES for M. Tech Chemical (Spl. in Process Design Engineering) PSO1. Apply the concepts and skills of Chemical Engineering to provide focused and practical solutions to advanced problems of Process Design Engineering PSO2. Analyse the solutions obtained for feasibility, reliability, economics and safety using experimental and computational tools. Course Outcomes On completion of this course, the students will be able to CO4. Understand fundamentals of kinetics including definitions of rate and forms of rate expressions

and relationships between moles, concentration, extent of reaction and conversion. CO5. Able to develop the overall rate expressions by analysing reactor data including integral and

differential analysis in constant- and variable-volume systems. CO6. Formulate set of consistent material/energy balance equations to describe operation of batch, and

continuous (CSTR, PFR) reactor system with single and multiple reactions. CO7. Determine operating parameters (size, flowrates, conversion, etc.) for isothermal operation of

ideal batch, CSTR and plug flow reactors to achieve desired conversions. CO5. Use of various software (polymath, MATLAB) for solution and analysis of design equations of different reactors.

Catalog Description Chemical reaction engineering (CRE) is the branch of engineering that encompasses the selection, design, and operation of chemical reactors. Because of the diversity of chemical reactor applications, the wide spectrum of operating conditions, and the multitude of factors that affect reactor operations, CRE encompasses many diverse concepts, principles, and methods that cannot be covered adequately in a single volume. A chemical reactor is an equipment unit in a chemical process (plant) where chemical transformations (reactions) take place to generate a desirable product at a specified production rate, using a given chemistry. The reactor configuration and its operating conditions are selected to achieve certain objectives such as maximizing the profit of the process, and minimizing the generation of pollutants, while satisfying several design and operating constraints (safety, controllability, availability of raw materials, etc.). The study of this subject enables students to use novel methodologies as well as software for design and analysis of chemical reactors. Course Content

CHPD7004 Chemical Reactor Engineering & Design L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure Engineering knowledge gained during UG.

Co-requisites --


Unit I: 8 lecture hours Introduction to reaction engineering, reaction kinetics, analysis of batch reactor data by using integral method, differential methods, half-life method, initial rate method, etc. Numerical exercise based on real life problems. Assignment-I Unit II: 8 lecture hours Introduction to reactor design, Material as well as energy balances, types and characteristics of different reactors, Design of ideal reactors (Isothermal), Numerical exercise based on real life problems. Test-1, Quiz-1, Unit III: 10 lecture hours Design and real world problems exercise of non-isothermal reactors. Assignment-2 Unit IV 10 lecture hours Introduction to catalysis, design of heterogeneous reactions, Fluid particle reaction kinetics. Test-2, Quiz-2, Text Books

1. J.B. Rawlings and J.G. Ekerdt, Chemical Reactor Analysis and Design Fundamentals, Second Printing, Nob Hill Publishing, 2004.

2. Octave Levenspiel, “Chemical Reaction Engineering” 3rd Edition, John Wiley & Sons Pte Ltd.

Reference Books 1. H. Scott Fogler, “Elements of Chemical Reaction Engineering” 3rd Edition, Prentice Hall

of India.



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CHPD7004

Chemical Reactor Engineering & Design

3 3 3

3


Name:

Enrolment No:

Course: CHPD7004 – Chemical Reactor Engineering and Design Programme: M.Tech. (CE+PD) Semester: I (2017-18) Time: 03 hrs. Max. Marks:100 Instructions: Attempt ALL four questions from Section A (60 marks) any Two Questions from Section B (each carrying 20 marks).

Section A ( attempt any two)

1. The rates of reaction at concentrations 0.15 mol/l and 0.05 mol/l are 0.0027 and 0.0003

mol/(l.min). What is order of reaction with respect to the reactant? [15]

CO1, CO2

2. A specific enzyme E acts as a catalyst in the fermentation of substrate A (the reactant). At

given Enzyme concentration in the aqueous feed stream of 25 l/min. Find the volume of

PFR required to achieve 95% conversion of reactant A (CA0=2 mol/l). The kinetics and

stoichiometry of the reaction are given by, min))./((5.01

10.0, lmol

C

CrRA

A

AA

[15] CO2


3. What are the different non ideal flow patterns? Explain about E and C curves with their

relations. [15]

CO2, CO3

4. Liquid reactant A produces R and S by the following reactions in parallel,

AS

AR

CrSA

CrRA

2,

4.0, 2

A feed of aqueous A with CA0=40 mol/m3 enters MFR to produce R and S, and a mixture

of A, R and S leaves the reactor. Find CR, CS and τ for 90% conversion.

[15] CO2, CO4

SECTION B (Attempt any Two Questions) 4. The desired liquid phase reaction [ )(, 3.05.1

1 BAR CCkrRBA ] is accompanied by the

undesired [ )(, 8.15.01 BAR CCkrSBA ] reaction. What contacting schemes (reactor types

and Temperature/concentration condition) would you use to these reactions to minimize

the concentration of undesired product?

[20]

CO3, CO4

5. One gaseous feed stream, containing A with C’A0=0.01 mol/l, at a rate of 1 l/min and

second gaseous stream, containing B with C’B0=0.02 mol/l, at a rate of 3 l/min enter a

MFR (Volume=1 l) and react in it to form a number of product R,S,T…. Analysis of the

exit stream of 6 l/min shows CAf=0.0005 mol/l and CRf=0.001 mol/l. The flow rates and

concentrations are measured at uniform T and P conditions of reactor. Estimate the rate of

reaction of A and rate of formation of R in the reactor.

[20] CO4, CO5

6. Consider the competitive (parallel) liquid phase reactions:

[ )0.1(),( 3.00.1BAR CCrDesiredRBA ]

[ )0.1(),( 8.15.0BAs CCrUndesiredSBA ]

Equal volumetric flow rates of A and B streams are fed to the reactor. Each stream

has initial concentration of 20 mol/l. Find concentration of R in the product stream

for XA=0.9, if flow reactor is a) PFR, b) MFR.

[20] CO3, CO4


Course Objectives The course will enable the students

To apply fundamental equations of fluid flow to solve complex problems To analyze different modes of heat transfer To design shell and tube heat exchangers To design heat exchanger networks To analyze methods for design of petroleum refinery furnaces

Course outcomes: At the end of the course, the students will be able to:

CO1. Apply fundamental equations of fluid flow to solve complex problems CO2. Analyze different modes of heat transfer CO3. Design shell and tube heat exchangers CO4. Design heat exchanger networks CO5 Analyze methods for design of petroleum refinery furnaces

Catalog Description This course deals with design of fluid flow and heat transfer equipment used in major process industries especially refineries. It covers the fundamentals on fluid mechanics and heat transfer. These fundamentals are used in the process design of equipment such as pumps, compressors, heat exchangers and refinery furnaces. Students are given industrial problems on design of above equipment. Standard methods are used for manual/preliminary design of equipment, particularly shell and tube heat exchangers viz. heaters, coolers, condensers and reboilers. The course also discusses pinch technology for the design of heat exchanger network from energy conservation point of view. Finally, a demo on how to use HTRI software for the design of shell and tube heat exchangers enhances the quality of the course. Course Content Unit 1- Fluid Mechanics and Machinery 7 Lectures

Review of fluid mechanics fundamentals, single and multi-phase (Ergun), characteristics of Centrifugal Pumps, Reciprocating Pumps, Gas Compressors, Selection and Specification of Fluid Moving Machinery.

Unit 2- Heat Transfer Fundamentals 7 Lectures

CHPD 7005 FLUID FLOW AND HEAT TRANSFER EQUIPMENT DESIGN

L T P C

Version 1.0 3 0 0 3

Pre-requisites/Exposure 1. Thermodynamics, Fluid Mechanics 2. Heat Transfer and Engineering Mathematics

Co-requisites


Review of Heat Conduction and Convection, Use of Energy Balance in Heat Transfer Equipment Design, Solution of Transient (Unsteady) Energy Balance Equation

Unit 3- Heat Exchanger Design 7 Lectures

Selection, Sizing and Design: Criteria for Selection of Type of Heat Exchanger, Heat Transfer Coefficient, Surface Area, Number of Passes, Pressure Drop in Tube and Shell Sides of Shell and Tube Exchangers, Design of Condensers and Reboilers, Compact Heat Exchangers for Cryogenic Applications, Air Fin Coolers

Unit 4-Heat Exchanger Specifications and Networks 7 Lectures

Specifications and Data Sheet, Materials of Construction, TEMA Classification. Design and Analysis for Energy Economy, Pinch Technology.

Unit 5- Design of Furnaces 7 Lectures

Introduction to radiative heat transfer, Types and Configuration of furnaces, Combustion and Efficiency

Calculations. Heat Transfer Calculation, Sizing Radiant and Convection Sections, Burner Specification,

Stack and Draft Calculations, Heat Loss and Refractory Thickness Calculations.

Unit 6 HTRI 5 Lectures

Introduction to HTRI, Heat Exchanger Design in HTRI (Lab) TEXT BOOK: 1. W. L. McCabe, J. C. Smith and P. Harriottt, Unit Operations of Chemical Engineering, 7th Ed., McGraw Hill, New York, 2005. 2.S. Thakore and B. Bhatt, Introduction to Process Engineering Design, Tata McGraw Hill, New Delhi, India, 2008. 3.R. K. Sinnott, Chemical Engineering Design (Coulson & Richardson's Chemical Engineering, Volume 6), 4th Ed., Elsevier, Oxford, UK, 2005. 4. D. Q. Kern, Process Heat Transfer, McGraw-Hill, New York, 1950. 5.Robert W. Serth, Process Heat Transfer: Principles and Application, Elsevier Science & Technology, 2007. REFERRENCE BOOKS: 1.V. Gupta and S. K. Gupta, Fluid Mechanics and its Applications, 2nd Ed., New Age Intl., New Delhi, 2011. 2. F. A. Holland and R. Bragg, Fluid Flow for Chemical Engineers, 2nd Ed., Butterworth Heinemann, Oxford, UK, 1995. 3. R. Darby, Chemical Engineering Fluid Mechanics, 2nd Ed., Dekker, New York, 2001. 4.B. Nesbitt, Handbook of Pumps and Pumping: Pumping Manual International, Elsevier, Oxford, UK, 2006. 5.Standards of the Tubular Exchangers Manufacturers Association, 8th ed., 1999

Modes of Evaluation: Quiz/Assignment/ Class Test Examination Scheme:


Components Seminar/Review Paper Internal Assessment ESE

Weightage (%) 20 30 50


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CHPD 7005

FLUID FLOW AND HEAT TRANSFER EQUIPMENT DESIGN

3 3 3 3



Course Outcomes (COs) Mapped Programme Outcomes

CO1 Apply fundamental equations of fluid flow to solve complex problems PO1, PO3

CO2 Analyze different modes of heat transfer PO1

CO3 Design shell and tube heat exchangers

PO1, PO3

CO4 Design heat exchanger networks PO1, PO2,

PO3

CO5 Analyze methods for design of petroleum refinery furnaces PO1, PO2,

PO3


Course Objectives The course will enable the students

To understand the complete downstream processing of crude oil To understand different refinery configurations and refining technologies To understand refinery economics, effluent treatment and polymers

Course outcomes: At the end of the course, the students will be able to:

CO1. Identify refineries with technologies and their complexities CO2. Analyse different types of crude oils CO3. Classify various processes in refinery and petrochemical industry CO4. Compare different configurations of refineries and their profitability CO5 Familiarize with important Polymers(Production route and applications)

Catalog Description Refining is a process of converting crude oil into useful products through various operations. This course focuses on understanding different refineries and complexities involved and also various technologies in crude processing. Students will learn the advantage of refinery integration with petrochemical plants, key petrochemical families, refinery economics, effluent treatment. Students will be encouraged to actively take part in subject discussion and presentations Course Content INTRODUCTION TO PETROLEUM AND PETROCHEMICALS 5 LECTURES

Growth and Development of Refining/Petrochemicals Industry in India, Refineries and

Petrochemical Units in India, Process Licensors.

CRUDE OIL AND PETROLEUM PRODUCTS 5 LECTURES

Crude Oils and their Characteristics, Major Petroleum Products and their Specifications.

PETROLEUM REFINERY AND ITS UNITS 10 LECTURES

Various Process Units and Plants in a Refinery: Desalter, CDU, VDU, FCCU, Hydrocracking and

Hydrotreating, Delayed Coker, Bitumen Blowing, Light Ends Treatment, Isomerization, Hydrogen

Generation, Vis-Breaking, Lube Oil Refining, Oil Movement and Storage, Utilities, etc.,

Roles/Functions and Integration with one another, Feed and Product Blending.

REFINERY CONFIGURATIONS 5 LECTURES

CHPD 7006 Petroleum Refining,Petrochemicals and Polymers

L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure

1. Chemistry 2. Basic Engineering Knowledge

Co-requisites


Specialized Refinery Configuration for Optimizing Gas Recovery, Integrated Refinery and

Petrochemical Plants.

PETROCHEMICALS 5 LECTURES

Key Petrochemical Product Families, Industry Drivers: Cost of Production, Supply/Demand,

Profitability and Pricing/Costing, Key Petrochemical Production Processes.

EFFLUENT TREATMENT AND WASTE DISPOSAL 3 LECTURES

POLYMER ENGINEERING 3 LECTURES

Types of Polymers, Production Methods, Special Properties of Polymers, Process Flow Sheets.

TEXT BOOKS: I.D Mall, Petroleum Refining Technology, CBS Publishers James G.Speight, Chemistry & Technology of Petroleum D S Jones, Elements of Petroleum Processing, Wiley 1995 L. F. Hatch and S. Matar, From Hydrocarbons to Petrochemicals, Gulf, New York, 1981. R. A. Myers, Handbook of Petrochemicals Production Processes, McGraw Hill, New York, 2005. A. Kumar and R. K. Gupta, Fundamentals of Polymers, 2nd Ed., CRC Press, Boca Raton, FL, 2003 REFERRENCE BOOKS: Dr.Ram Prasad, Petroleum Refining Technology, Khanna Publishers I.D Mall, Petrochemial Process Technology, Laxmi Publications Shakun Srivastava, Anshu Srivastava, Polymer Science and Technology, S.K. Kataria & Sons Modes of Evaluation: Quiz/Assignment/ Class Test Examination Scheme:

Components Seminar /Review paper

Internal Assessment

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Course Title PO1 PO2 PO3 PO4 PO5 PO6 PO7 PO8 PO9 PO10 PO11 PSO1 PO11

CHPD 7006

PETROLEUM REFINING,PETROCHEMICALS AND POLYMERS

3 3 2 2 2 2 1



Course Outcomes (COs) Mapped Programme Outcomes

CO1 Identify refineries with technologies and their complexities PO1, PO2

CO2 Analyse different types of crude oils PO1,PO2,PO3,PO4

CO3 Classify various processes in refinery and petrochemical industry

PO1, PO2,PO3,PO4,PO5

CO4 Compare different configurations of refineries and their profitability

PO1,PO2, PO3,PO7

CO5 Familiarize with important polymers(Production route and applications) PO1, PO4


Course Objectives

8. To explain the fundamentals of process design 9. To explain the fundamental concepts of developing and reading PFD and P&ID 10. To enable students to prepare and simulate PFD using process simulators


CO1. Explain the fundamentals of process design

CO2. Explain the development of block flow diagram, process flow diagram (PFD) and piping and instrumentation diagram (P&ID).

CO3. Develop material and energy balance equations for a given process

CO4. Design of instrumentation loops.

CO5. Demonstrate the working of process simulators

Catalog Description Process design is important to commercialize the process from the concept. The steps involved in process design will help students how to proceed in engineering way from a basic concept to commercial plant. The PFDs and P&IDs developed during process are helpful to carry out material and energy balance, sizing and procurement of the equipment, plant construction etc. The understanding of process simulations will enable students to design and develop chemical engineering systems. Students will learn about process simulators available for PFD and P&ID simulations. Students will be encouraged to actively take part in classroom teaching and all assignments. Course Content

Unit I: 8 lecture hours

PROCESS DESIGN: Conceptual design, process synthesis and design alternatives,

Design under Uncertainty, safety considerations while designing, Plant location and plant

layout

CHPD7008 Process Design and Flowsheeting L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure Chemical Processes and Chemical Process Calculations

Co-requisites --


Unit II: 6 lecture hours

FLOW DIAGRAMS: Definition and objectives of FD, Purpose of Process Flow Diagram

(PFD), Piping & Instrumentation Diagram (P&ID), Information provided on PFD and P&ID,

Relevance of PFD and P&ID in plant design and engineering

Unit III: 4 lecture hours

DEVELOPMENT OF PFD: Features of Process Simulation Software, Contents of PFD,

Evolution of PFD from simulation results

Unit IV: 4 lecture hours

GENENRIC SYMBOLOGY AND NUMBERING SYSTEMS: Symbols: Equipment,

piping, valve, specialty items, control valves, other instrument hardware, Numbering, Tags and

Notations: Flow directions, origins of lines, special notes

Unit V: 10 lecture hours

UNDERSTANDING AND DEVELOPING P&ID: Guidelines on steps in evolving a P&ID,

Development of a simple basic P&ID, piping specification and line designation, Valves: Type

and application, Instruments: Development of control loops, need and location of measuring,

Depiction of DCS and RTU in P&ID, Incorporation of miscellaneous information in P&ID:

Slopes, elevations, Introduction to PDS: Software for making 2-D and 3-D layouts etc. CASE

STUDIES (Read a simple P&ID, Identity control loop details, Read and interpret a detailed

P&ID, Case studies specific to hydrocarbon industries)

Text Books

A. Chemical Engineering Design by Gavin Towler and Ray Sinnot, Elsevier.

B. Product and Process Design Principles By W D Sieder, J D Seader & D R Lewin, 2nd

Edtn., John Wiley & Sons, Inc.

Reference Books


A. Chemical Engineering Design by R K Sinnott, 6th Edtn., Elsevier.

B. Plant Design and Economics for Chemical Engineers by M S Peters, K D

Timmerhaus & R E West, 5th Edtn., Mc-Graw Hill






Programme Outcomes

CO1 Explain the fundamentals of process design

PO1, PO3

CO2

Explain the development of block flow diagram, process flow diagram (PFD) and piping and instrumentation diagram (P&ID).

PO1, PO3, PO4

CO3

Develop material and energy balance equations for a given process

PO1, PO3

CO4

Design of instrumentation loops.

PO2, PO3

CO5

Demonstrate the working of process simulators

PO5


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CHPD7008

Process Design and Flow-sheeting

2 1 3 1 2 2 3




Name:

Enrolment No:

Course: CHPD7008 – Process Design and Flow-sheeting Programme: M. Tech (CE+PD) Semester: II Time: 03 hrs. Max. Marks:100 Instructions: 1. The question paper consists of two sections. 2. Answer the questions section wise in the answer booklet. 3. Attempt all the questions. 4. Assume suitable data wherever necessary.

SECTION A ( attempt all questions)

1. A process for making a single product involves reacting two liquids in a continuously agitated reactor and distilling the resulting mixture. Unused reactants are recovered as overhead and are recycled. The product is obtained in sufficiently pure form as bottoms from the distillation tower.

a) Prepare a qualitative flowsheet for the process, showing all pieces of equipment. b) With cross reference to the qualitative flowsheet, list each piece of equipment and tabulate for each the information needed concerning chemicals and the process, in order to design the equipment.

[15] CO2

2. What is flowsheet modelling? What are the types of process flowsheet simulation? Explain in details the steps involved in the simulation of process flowsheet. [15] CO5

3. a) Discuss the role of chemical engineer in process design. b) What do you mean by pilot plant? What is the importance of pilot plant in process

development? c) What are the various criterions for the good layout of new plant?

[15] CO1

4. a) What are the various design approaches towards the safe chemical plants? b) Draw a neat sketch of typical relief system installation for a pressure vessel.

[15] CO4

SECTION B ( attempt all questions)

5. a) Often, during the distillation of liquid mixtures, some non-condensable gases are dissolved in the feed to the tower. These non-condensable come out of solution when heated in the tower and may accumulate in the overhead reflux drum. In order to operate the column satisfactorily, these vapors must be periodically vented to a flare or stack. Sketch the P&ID representing the top portion of the tower, to show all the instrumentation needed for this control loop.

[20] CO2, CO4


b) A standard method for instrumenting a control valve is termed the “double block

and bleed,” which is illustrated in figure 1.

Figure 1: Double Block and Bleed Arrangement

Answer the following: i) What will be the opening/closing position of the various valves under normal

operating conditions? ii) Explain, carefully, the sequence of opening and closing valves required in order

to change out the valve stem on the control valve (valve b). iii) It has been suggested that the bypass valve (valve d) be replaced with another

gate valve to save money. Gate valves are cheap but essentially function as on-off valves. What do you recommend?

iv) What would be the consequence of eliminating the bypass valve (valve d)?

6. The figure 2 shows the main steps in a process for producing a polymer. From the following data, calculate the stream flows for a production rate of 10,000 kg/h. Reactor selectivity for polymer : 100% Slurry polymerization : 20 wt% monomer/water Conversion : 90% per pass Catalyst : 1 kg/1000 kg monomer Short stopping agent : 0.5 kg/1000 kg unreacted monomer Filter wash water approx. : 1 kg/1 kg polymer Recovery column yield : 98% (percentage recovered) Dryer feed : 5% water, Product specification : 0.5% H2O Polymer losses in filter and dryer: 1%

[20]

CO3


Figure 2: Process of producing polymer


Course Objectives

11. To help the students to understand the fundamentals of momentum transfer. 12. To enable students to apply momentum transfer concepts to solve real-life problems. 13. To give the students a perspective to appreciate the use of heat and mass transfer in solving

day to day activities 14. To enable students to apply the concepts in design industrial or fundamental research in

transport problems

Course Outcomes On completion of this course, the students will be able to CO8. Apply the concepts of transport phenomena to solve problems in momentum transfer

and can write codes to solve fundamental chemical engineering problems using MATLAB CO9. Apply the concepts of transport phenomena to solve problems in heat transfer also

simulate chemical engineering operations CO10. Apply the concepts of transport phenomena to solve problems in mass transfer

Catalog Description While momentum, heat, and mass transfer developed independently as branches of classical physics long ago, their unified study has found its place as one of the fundamental engineering sciences. This development, in turn, less than half a century old, continues to grow and to find applications in new fields such as biotechnology, microelectronics, nanotechnology, and polymer science. The essence of this subject is the careful and compact statement of the conservation principles, along with the flux expressions, with emphasis on the similarities and differences among the three transport processes considered. Often, specialization to the boundary conditions and the physical properties in a specific problem can provide useful insight with minimal effort. Course Content

Unit I: 5 lecture hours Introduction to Mathematical modelling - What is modelling? What is model? Transport phenomena based models, Empirical models, Steady state and dynamic models, Lumped and distributed parameter models Unit II: 14 lecture hours Development of analytical models - Conservative and constitutive equations, Strategy of process calculation, Degree of freedom analysis for a model, Thermodynamics and physical properties calculation facility, Unit III: 14 lecture hours Simultaneous equation solving approaches, Recycle calculations, Mathematical tools, Commercial simulators, Alternative modelling methods Text Books

CHPD 7009 Process Modeling and Simulation L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure Basic Engineering Mathematics, Fluid Mechanics,

Thermodynamics, Heat Transfer and Mass Transfer

Co-requisites --


1. L. Luyben William. Process Modelling, Simulation and Control for Chemical Engineers.

McGraw Hill, 2nd edition, 1996.

Reference Books 1. C. J. Geankoplis, Transport Processes and Separation Process Principles, 4th Ed., Prentice Hall,

Upper Saddle River, NJ, 2003. 2. W. M. Deen, Analysis of Transport Phenomena, Oxford University Press, New York, 1998. 3. J. Beers Kenneth. Numerical methods for Chemical Engineers: Applications in MATLAB.

Cambridge University Press, 2005. 4. Richard G. Rice and Duong C. Do. Applied Mathematical Modelling for Chemical Engineers. 5. John Wiley and Sons, 1995. 6. B. V. Babu. Process plant simulation. Oxford University Press, 2004. 7. Wayne C. Bequette. Process Dynamics: Modelling, Analysis and Simulation. Prentice Hall 8. International, 1998. 9. Bruce A. Finlayson. Introduction to Chemical Engineering Computing. John Wiley and Sons, 10. 2006





Course Outcomes (COs) Mapped Program Outcomes

CO1 Apply the concepts of transport phenomena to solve problems in momentum transfer and can write codes to solve fundamental chemical engineering problems using MATLAB

PO1, PO3, PO4, PO5

CO2 Apply the concepts of transport phenomena to solve problems in heat transfer also simulate chemical engineering operations

PO2, PO3, PO4, PO5

CO3 Apply the concepts of transport phenomena to solve problems in mass transfer

PO2, PO3, PO4, PO5


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CHPD 7001

Transport Phenomena 3 3 3 2 3 - - - - - - -



Course Objectives

15. Exhaustive deliberations of fundamental principles responsible for mass transfer. 16. To dwell with the analysis of various mass transfer process and the design of the respective

equipmen.

Course Outcomes On completion of this course, the students will be able to CO1.Learn about the strong fundamental theories about the mass transfer process. CO2.Analyze the various mass transfer process and design the respective equipment.

Catalog Description Chemical Engineering Study is incomplete without studying Mass Transfer Processes. Course Content

Unit I: Introduction: 8 lecture hours Thumbnail sketch of the Separation Processes and of the Mass Transfer Processes used in practice. Deliberations on Thermodynamics of Phase Changes. Unit II: 8 lecture hours Elaborated Discourse on the Mass Transfer Equipment: Exhaustive Discussions on Preliminary Design aspect of the Major Mass Transfer Equipment. Discussion of available Design Software for the design of the same.

Unit III: 10 lecture hours Comprehensive analysis of the Mass transfer Theory: The analysis of the various modes of mass transfer from theoretical context. Unit IV: 10 lecture hours Detailed Designing of important Mass transfer apparatus. Deliberations on Individual Case studies for Mass Transfer equipment design. Text Books 1. Mass Transfer Operations: Treybal. Reference Books

1. 1. Chemical Process Design and Integration, Robin Smith, JWS.

CHPD7010 Mass Transfer Equp. Design & Sepn. Process. L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure Preliminary knowledge on Mass Transfer process/

Co-requisites --


1. Optimization of Chemical Processes, T.F. Edgar, D.M. Himmelblau, L.S. Lasdon,

Mcgraw Hill. Modes of Evaluation: Quiz/Assignment/ presentation/ extempore/ Written Examination Examination Scheme:



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CHPD7010

Mass Transfer Equp. Design & Sepn. Process.

3 3 3

3




Programme Outcomes

CO1 Understanding the basics of Process Optimization PO10

CO2 Application of the optimization theory in chemical engineering problem. PO10


Course Objectives

1. Analyse the important technical fundamentals of chemical process safety. 2. Understand different types of fires and explosions and designs to prevent them. 3. Able to recognize and eliminate potential hazards by active or passive measures of design.

PROGRAM SPECIFIC OUTCOMES for M. Tech Chemical (Spl. in Process Design Engineering) PSO1. Apply the concepts and skills of Chemical Engineering to provide focused and practical solutions to advanced problems of Process Design Engineering PSO2. Analyse the solutions obtained for feasibility, reliability, economics and safety using experimental and computational tools. Course Outcomes

CO1. Understand the important technical fundamentals of chemical process safety. CO2. Analyse source, toxic release and dispersion models. CO3. Understand different types of fires and explosions and designs to prevent them.

CO4. Design relief valves/scenarios and carry out relief sizing. CO5. Recognize safety signs, colour codes, use MSDS and specify PPE.

Catalog Description Complex processes, such as, at higher pressure, more reactive chemicals, and exotic chemistry. More complex processes require more complex safety technology. Many industrialists even believe that the development and application of safety technology is actually a constraint on the growth of the chemical industry. As chemical process technology becomes more complex, chemical engineers will need a more detailed and fundamental understanding of safety. H. H. Fawcett said, "To know is to survive and to ignore fundamentals is to court disaster." This book sets out the fundamentals of chemical process safety. Since 1950, significant technological advances have been made in chemical process safety. Today, safety is equal in importance to production and has developed into a scientific discipline that includes many highly technical and complex theories and practices.. Course Content

Unit I: 8 lecture hours Introduction- Environmental Concern and Safety, Accidental statistical methods, significant industrial hazards of history, Assignment-I , Unit II: 8 lecture hours Fires and Explosions, Design to Prevent Fires and Explosions, Fire extinguishers, fire alarm systems, Test-1,

CHPD7011 Principles of Chemical Process Safety L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure Knowledge of physics, chemistry, mathematics and transfer

processes

Co-requisites --


Quiz-1, Unit III: 10 lecture

hours Introduction Source Models, Laws and Regulations, Toxicology, Toxic Release and dispersion Models, Assignment-2 Unit IV 10 lecture hours Personnel Protective Equipment (PPE), Introduction to Reliefs and Relief Sizing,

Test-2, Quiz-2, Text Books

3. Chemical Process Safety: Fundamentals with Applications, Daniel A. Crowl and Joseph F. Louvar, Prentice Hall International, 1990 (T1).

Reference Books

A. Hydrocarbon Process Safety, J. C. Jones, Pennwell Books, 2003 (T2) B. Loss Prevention in the Process Industries, F. P. Lees, 1980 (R1) C. Emergency Response and Hazardous Chemical Management, Clyde B. Strong (R2) D. S. Mannan and F. P. Lees, Lees’Loss Prevention in the Process Industries, Elsevier,

Oxford, UK, 1980 (R3) E. C. B. Strong, Emergency Response and Hazardous Chemical Management:

Principles and Practices, CRC Press, Boca Raton, FL, 1996 (R4) Modes of Evaluation: Quiz/Assignment/ presentation/ extempore/ Written Examination Examination Scheme:


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Mass Transfer Equp. Design & Sepn. Process. Mass Transfer Equp. Design & Sepn. Process.


CHPD7011

Principles of chemical Process Safety

3 3 3

3


Name:

Enrolment No:

Course: CHPD7011 – Principles of Chemical Process Safety Programme: M.Tech. (CE+PD) Semester: II (2017-18) Time: 03 hrs. Max. Marks:100 Instructions: Attempt ALL four questions from Section A (60 marks) any Two Questions from Section B (each carrying 20 marks).

Section A ( attempt any two)

1. The following accident report has been reported:

Failure of a threaded 1%" drain connection on a rich oil line at the base of an absorber

tower in a large (1.35MCFID) gas producing plant allowed the release of rich oil and gas

at 850 psi and -40°F. The resulting vapor cloud probably ignited from the ignition system

of engine driven re-compressors. The 75' high X 10' diameter absorber tower eventually

collapsed across the pipe rack and on two exchanger trains. Breaking pipelines added more

fuel to the fire. Severe flame impingement on an 11,000-horsepower gas turbine-driven

compressor, waste heat recovery and super-heater train resulted in its near total

destruction.

Identify the initiation, propagation, and termination steps for this accident.

[15] CO1, CO2

2. Write detailed notes (hazard nature, chemicals involved, etc.,) on the following industrial

accidents by using neat schematics: (i) Flixborough, England (ii) Seveso, Italy

[15] CO2

3. Discuss in details the various possible routes through which the toxicants can enter the

biological organisms. [15] CO2, CO3


4. 1. Determine the mixture TLV at 25oC, 1atm pressure of a mixture derived from the

following liquid:

mixture of A, R and S leaves the reactor. Find CR, CS and τ for 90% conversion.

[15] CO2, CO4

SECTION B (Attempt any Two Questions) 4. Derive the expression for average vapor concentration for volatile vapors. [20]

CO3, CO4

5. Explain various ‘chemical plant control techniques’ in tabular form. [20]

CO4, CO5

6. Derive the design equations of sprinkler system. [20]

CO3, CO4


ELECTIVES

Course Objectives

17. To help solve simple problems involving optimization using traditional methods. 18. To help solve problems involving optimization using modern non-traditional/evolutionary

techniques. 19. To get a feel of optimization of large-scale industrial units. 20. To get the students to make simple computer codes for optimization. 21. To get the students to use library programs in MATLAB optimization using evolutionary

techniques. .

Course Outcomes On completion of this course, the students will be able to CO11. Understand the traditional techniques of optimization. CO12. Understand the modern, non-traditional (evolutionary) techniques of optimization. CO13. Solve simple problems in optimization using their own programs. CO14. Solve real-life optimization problems using codes in MATLAB.

Catalog Description Optimization is an integral part of life and is assuming considerable significance in Engineering. In this course, the focus is on covering both traditional and modern techniques of optimization. After the basic techniques are discussed, industrial units are optimized. Students get a hands-on exposure to optimize real-life industrial units using library codes in MATLAB. Course Content

Unit I: 7 lecture hours

Unconstrained single objective function optimization (traditional techniques)

Search techniques: Region-elimination: exhaustive search, interval halving, golden section search

Point estimation techniques: Powells’ method

Methods requiring derivatives: Newton’s method, bisection method, secant method

Unconstrained multi-variable techniques: general conditions for optimization

CHPD7012 Systems Analysis and Optimization L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure Undergraduate courses in Chemical Engineering, some

programming

Co-requisites --


Direct search techniques: simplex and Hooke-Jeeves pattern search; gradient search techniques: steepest descent/ascent, Newton’s techniques


Optimization with constraints, single objective functions (traditional techniques) Mathematical elimination, Lagrangian multiplier technique (including sufficiency

conditions), Kuhn-Tucker substitution, penalty functions

Other more general cases: two-variable golden section search, Box complex technique


Multi-objective Optimization


Non Traditional Evolutionary Techniques

SGA, NSGA-II, jumping gene and altruistic adaptations (09)

SA, NSSA, jumping gene adaptation (4)

Particle swarm optimization (PSO) (3)

Ant colony optimization (ACO) (2)


Equality constrained optimization/Pontryagins principle

Text Book Manojkumar C. Ramteke [ChE, IITD], D. N. Saraf [DITU, Dehradun] and Santosh K. Gupta, Optimization for Engineers, Chapters which are ready. Hard copy will be available for copying.

Reference Books G. S. G. Beveridge and R. S. Schechter, Optimization, Theory and Practice, McGraw Hill, New York, 1970 (Excellent text; Intl. Edn. was available, but is now out of print and dated). Asgar Hussain and K. Gangaiah, Optimization Techniques for Chemical Engineering, MacMillan, Delhi, 1976 (Has several lengthy, real life, Chemical Engg examples and problems; this book is now out of print). T. F. Edgar, D. M. Himmelblau and L. S. Lasdon, Optimization of Chemical Processes, 2nd Ed., McGraw Hill, New York, 2001 (Intl. Edn. is available) M. M. Denn, Optimization by Variational Principles, McGraw Hill, New York, 1969 (Excellent book in this specialized area; in fact, all of Professor Denn’s books are excellent)


W. H. Ray and J. Szekeley, Process Optimization, Wiley, New York, 1973 (Excellent book; in fact, all of Professor Harmon Ray’s books are excellent) G. V. Reklaitis, A. Ravindran and K. M. Ragsdell, Engineering Optimization, 2nd Edn., Wiley, New York, 2006

K. Deb, Optimization for Engineering Design: Algorithms and Examples, 2nd Edn., Prentice Hall of India, New Delhi, 2004 (Excellent text but at a more elementary level, ME oriented) A. E. Bryson and Y.-C. Ho, Applied Optimal Control, Hemisphere, New York, 1975 (an excellent compendium of advanced material)

Modes of Evaluation: Impression-Attendance/Written Examination Examination Scheme:





Programme Outcomes

CO1 Understand the traditional techniques of optimization. PO1, PO2

CO2 Understand the modern, non-traditional (evolutionary) techniques of optimization. PO1, PO2

CO3 Solve simple problems in optimization using their own programs.

PO3, PO4, PO5

CO4 Solve real-life optimization problems using codes in MATLAB.

PO3, PO4, PO5


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Course Code


CHPD 7012

Systems Analysis and Optimization

3 2 1 2 3

1 = weakly mapped 2 = moderately mapped 3 = strongly mapped



Name:

Enrolment No:

Course: CHPD 7012: Systems Analysis and Optimization Program: M. Tech. (CE-PD) Semester: EVEN-2016-17 Time: 03 hrs. (End Semester Exams) Max. Marks: 100 Open Book and Notes Exam Instructions: There are NO questions in Section A. Attempt ALL three questions from Section B (marks are indicated)

Section A (NO questions in this Section)

SECTION B (Attempt ALL THREE Questions) 1. Minimize the function

Min f(x1, x2) = (x1 ─ 30)2 + (x2 ─ 20)2

analytically (by using appropriate partial differentiations of f).

If you find this problem trivial, do not worry, it IS trivial.

[30]

CO4

2. Solve the following two-decision variable, single-objective minimization problem using

SGA (Note that f is the same as in Q. 1):

Min f(x1, x2) = (x1 ─ 30)2 + (x2 ─ 20)2

subject to (s.t.):

bounds: 0 ≤ 𝑥 ≤ 10

0 ≤ 𝑥 ≤ 10

and NO other constraints.

(a) Use three binaries each to represent x1 as well as x2, and use five chromosomes in the population, i.e., Np = 5. Use the sequence of random numbers given in your textbook to select the binaries. Use the binary number as zero if 0 ≤ 𝑅 ≤ 0.5 and as unity if 0.5 ≤ 𝑅 ≤ 1.0.

(b) Enter in the Table below: (5)

Parent chromosomes (binary):

Chromosome No.

x1 (binary) x2 (binary)

[35] CO2


1

2

3

4

5

(c) Complete the diagram below, then map the above chromosomes and fill up the Table:

0 0 1

0 0 1

0 1 1

|_________|_________|________|________|_________|_________|_________|

0 10/7 20/7 30/7 40/7 50/7 60/7 10

x1, x2 →

Calculate f(x1, x2). Enter these also in the Table (some entries are repeated): (5)

Mapped parent chromosomes (decimal system):

Chrom. No.

x1 (binary) x2 (binary) Mapped x1

(decimal)

Mapped x2

(decimal)

f(x1, x2)

1

2

3

4

5

(d) Now, use the further sequence of random numbers to select two chromosomes randomly. Use the values of f(x1, x2) of these two chromosomes to decide which of these is to be copied using tournament selection (without deletion from the parent pool so that they can be copied more than once) into the mating pool below. Repeat five times to get five chromosomes in the mating pool. (5)


Mating pool (binary):

Two chrom. selected

Chrom. selected

New No. for this Chrom.

x1 (binary) x2 (binary)

1

2

3

4

5

These chromosomes are identical (copies) to the ones in the original parent pool.

(e) Use the next two random numbers to select two chromosomes randomly from the mating pool. Using pcross = 1.0 (and consuming the next random number), find a crossover site (using yet another random numbers). Flip and get (initial) a pair of daughter chromosomes. Fill up in the table on the next page (NOTE THAT YOU WILL HAVE TO GENERATE SIX INITIAL DAUGHTER CHROMOSOMES WHILE YOU NEED ONLY FIVE. SO, DO CROSSOVER IN THE FIFTH AND SIXTH CHROMOSOMES, MAP AND THEN SELECT THE BETTER ONE OF THIS PAIR): CHOOSE ONLY ONE OF THE LAST TWO CHROMOSOMES TO MAKE FIVE. FILL UP THE TABLE ON THE NEXT PAGE. (5)

(Initial) daughter chromosomes (binary) after crossover:


Two

chromosomes selected from

the mating pool;

new No.

Location of the crossover

New Chrom.

No.

New x1 (binary)

New x2

(binary)

1

2

3

4

5

6

New

chrom.

No.

New x1

(binary)

New x2

(binary)

Mapped x1 Mapped x2 f(x1, x2)

5

6

(e) Do not do any mutation, i.e., pmut = 0 (AND SO DO NOT CONSUME ANY

RANDOM NUMBER). Use the further sequence of random numbers to do the a-

JG operation. Use paJG = 1.0 (i.e., CONSUME ONE RANDOM NUMBER FOR

THIS, EVEN IF paJG = 1.0). Use the number of binaries in the aJG as 2, and carry

out the aJG step:


Final Daughter chromosomes (binary) after the crossover and aJG

operations

Chrom. No.

x1

(binary, before aJG)

x2

(binary, before aJG)

aJG starting locn. (as

per diagram (pl

give)

x1

(binary, after aJG)

x2

(binary, after aJG)

1

2

3

4

5

Chrom. No.

x1

(binary, after aJG)

x2

(binary, after aJG)

x1

(real, after aJG)

x2

(real, after aJG)

1

2

3

4

5

Chromosome No.

f(x1, x2)

1

2

3

4

5


This completes one generation. (10)

(f) Compare with the lowest value of f in the starting set. (5) (35 Points)

3. We wish to develop a slightly modified EQP technique for a single objective

function (a non-linear function of the n decision n variables, x):

Min f(x1, x2, . . . xn) ≡ Min f(x)

subject to (s.t.) m equality constraints, also non-linear functions of the n decision variables, x) :

c1(x) = 0

c2(x) = 0

. . .

cm(x) = 0

The new algorithm quadritizes f(x) around a point, x(k), and also quadritizes all the ci(x) around this point, x(k).

Develop this algorithm in detail (and very carefully). (35 Points)

* * *

[35] CO5

CHPD 7013 Advance Process Control L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure Process control and Instrumentation at UG level

Co-requisites --


Course Objectives

Expose students to the advanced control methodologies used in industries and research. This course prepares the student to take up such challenges in his profession. Course Outcomes On completion of this course, the students will be able to

CO1.Estimate controller parameter settings CO2.Design of controllers for interacting multivariable systems CO3.Read and interpret the detailed P&ID

Catalog Description This course covers: the strategy of process control; controller tuning methods and frequency response; multivariable control theory; and construction of dynamic process models with control. The emphasis is on control problems in process engineering including Centrifugal Compressor/Steam Turbine Control, Fired Heaters/Boiler Control, Distillation Column Control (CDU also), Process Shutdown and Emergency Shutdown Systems, Reactor Control: Catalytic Packed Bed Reactors, Solution Polymerization, FCCU Control. Course Content

Unit I: 5 lecture hours BASICS OF INSTRUMENTATION, PROCESS DYNAMICS AND CONTROL

Basic Concepts and Definitions, Process Characteristics and Dynamics, The Feedback Control Loop–The Five Elements, Closed Loop Dynamics, Terminologies and Symbols Unit II: 8 lecture hours CONVENTIONAL CONTROL DESIGN AND MODERN CONTROL ALGORITHMS Degrees of Freedom and Control, Single Loop Control, PID Control Algorithms, Tuning of PID Controllers. Multi-variable Control and Controller Design, Model Predictive Control (IMC Control and DMC Control), Control Design for Non-Linear Systems, Concepts of Robust Control, Plant-wide Control


CONTROL HARDWARE

Measurement of Process Parameters: Level, Temperature, Pressure, Composition, Measuring Instruments and Their Selection, Data Sheets–Performance Related Parameters for Instrumentation, Control Loop Hardware–Transmitters, Transducers, Pneumatic System, Hydraulic System, Electronic System, Final Control Elements: Control Valve–Types, Selection and Sizing, Inherent and Installed Characteristics, Dynamic Behavior, Actuators Unit IV: 5 lecture hours CONTROL PRACTICE–GENERIC CASE STUDIES


Centrifugal Compressor/Steam Turbine Control, Fired Heaters/Boiler Control, Distillation Column Control (CDU also), Process Shutdown and Emergency Shutdown Systems, Reactor Control: Catalytic Packed Bed Reactors, Solution Polymerization, FCCU Control. Unit V: 8 lecture hours OVERVIEW OF DCS, SCADA , P&IDS AND CONTROL

Definition, Application and Architecture, Performance Specification. Read a Simple P&ID,

Identify Control Loop Details, Read and Interpret a Detailed P&ID, Case Studies Specific to

Hydrocarbon Industry.

Text Books

1. Marlin, T., Process Control: Designing Processes and Control Systems for Dynamic Performance, McGraw Hill, New York, 1995.

2. Seborg, D., Edgar, T., and Mellichamp, D., Process Dynamics and Control, Wiley & sons, New York, 1989.

3. Stephanopoulos, G., Chemical Process Control: An Introduction to Theory and Practice, Prentice Hall, 1984.

Reference Books 1. Smith, C. and Corripio, A., Principles and Practice of Automatic Process Control,

Wiley & sons, New York, 1997. 2. Shinsky, F., Process Control Systems, McGraw Hill, New York, 1988. 3. Luyben, W.,Process Modeling, Simulation and Control for Chemical Engineers,

McGraw Hill, New York, 1990.


Components Seminar/Review Paper

Internal Assessment ESE





Programme Outcomes

CO1 Estimate controller parameter settings

PO2,PO3


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CHPD7013 Advanced Process Control

3 3 3 3

3


Course Objectives

1. To understand Concepts of Project Management for Planning & Execution of projects.

2. To know and use various optimization tools / techniques applied in Project

Management.

3. To introduce fundamentals of Contract Administration, Costing and Accounting of

Projects.

CO2 Design of controllers for interacting multivariable systems

PO3, PO4

CO3 Read and interpret the detailed P&ID PO1, PO12

LSCM 8001

Project management & Contract Administration

L T P C 3 0 0 3

Pre-requisites/Exposure Basic mathematical, analytical and comprehension skills.

Co-requisites Computer skills MS-Excel, MSP, Power Point, Web sources


4. To discuss, analyze and appreciate contemporary projects in Indian and international

context


CO1. Analyze issues & challenges in identification and selection of projects.

CO2. Develop skills required for project planning & formulation.

CO3. Apply optimization techniques in project management.

CO4. Learn processes for project execution, control and closing.

CO5. Appreciate the contracting process as applied in projects.

Catalog Description India is one of the fast growing and promising economy, aiming for an ambitious double digit GDP growth rate. The fulfillment of this aspiration calls for rapid growth in the transportation, communication, housing, storage, energy and power infrastructure. The target growth in the infrastructure sector cannot be achieved merely by substantial funding but also requires the professional capabilities of the highest order, in several aspects of effective planning and efficient implementation of the projects. This program presents a comprehensive framework for planning, executing, controlling and closing projects in the context of issues and challenges faced by Indian economy. Project management involves understanding the cause-effect relationships and interactions among the socio-technical-economic-environmental dimensions of the projects. Students will be encouraged to indulge in teamwork through participating in group assignments and presentations. Students will be given exercises involving applications of modern tools, such as, MS-Excel, MSP, MS-Power Point. Course Content

Module 1: THE PROJECT MANAGEMENT FRAMEWORK

(8 Lectures) Project Definition & Classification Project Management & its Relationship with Program Management and

Portfolio Management Project Manager PMBOK (Project Management Body of Knowledge) Project Life Cycle Project Organization Project Stakeholders Project Feasibility Study

Module 2: THE STANDARD FOR PROJECT MANAGEMENT OF A PROJECT

(6 Lectures) Project Management Processes for a Project Project Management Process Groups Planning Process Group


Executive Process Group Monitoring & Controlling Process Group Closing process Group

Module 3: THE PROJECT MANAGEMENT KNOWLEDGE AREAS

(10 Lectures) Project Integration Management Project Scope Management Project Time Management Project Cost Management Project Quality Management Project Human Resource Management Project Communications Management Project Risk Management Project Procurement Management Project Stakeholder Management

Module 4: EXECUTING, MONITORING & CONTROLLING

(6 Lectures) Integrated Change Management Acquire, Direct & Manage Project Team Earned Value Management

Module 5: CONTRACT ADMINISTRATION

(6 Lectures) Contracting Approach, Contractor’s role Types of Contracts Contract Planning, Contracting Schedule Contracting Procedure, Performance Guarantee Force Majeure, Liquidated Damages and Penalty

Text Books

1. Gray Clifford F., Larson Erik W.; Project Management – The Managerial Process, Tata McGraw Hill

2. Prasanna Chandra; Projects- Planning, Analysis, Selection, Financing, Implementation and Review’,VI Edition, Tata Mc Graw Hill.

3. Chaudhary S.; Project Management, Tata Mc Graw Hill

Reference Books 1. PMBOK Guide to Project Management, V Edition 2. Kerzner H.; Project Management, II Edition, CBS Publishers 3. Meredith Jack R., Mantel Samuel J.; Project Management, IV Edition, John Wiley & Sons 4. Patel Bhavesh M.; Project Management- Strategic Financial Planning, Education & Control,

Vikas Pub. House 5. Gopalakrishnan P., Ramamoorthy V.E.;Textbook of Project Management, Mac Millan Pub. 6. Maylor Harvey, Project Management, Mac Millan 7. Matheen A. Prof., Comprehensive Project Management, Laxmi Publications (P) Ltd.

Modes of Evaluation: Quiz/Assignment/ presentation/ extempore/ Written Examination


Examination Scheme:





Programme Outcomes

CO1 Analyze issues & challenges in identification and selection of projects.

PO6, PO7, PO11, PO12

CO2 Develop skills required for project planning & formulation. PO3, PO6,

PO10, PO11

CO3 Apply optimization techniques in project management. PO3, PO6,

PO11

CO4 Learn processes for project execution & control and closing. PO9, PO10,

PO11, PO12

CO5 Appreciate the contracting process as applied in projects. PO9, PO11,

PO10


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Course Title PO1 PO2 PO3 PO4 PO5 PO6 PO7 PO8 PO9 PO1

0

PO11

PSO1

PSO2

LSCM 8001

Project Mgmt. & Contract

Administration 1 2 1 3 2 3 1




Name:

Enrolment No:

Course: LSCM8001 – Project Management & Contract Administration Programme: M.Tech. (PLE) Semester: EVEN 2016-17 Time: 03 hrs. Max. Marks:100

Note: Use of Calculators & Graph papers is allowed.

Section A Answer any six (o6) questions. Each carries 10 marks. 1. Define project & appreciate the role of projects in economic growth of a nation. 10 CO1 2. Discuss the various knowledge management areas applied to project management. 10 CO1 3. Describe various tools & techniques used for project cost estimation. 10 CO2 4. Write a detailed note on Cost Engineering and its application in projects. 10 CO2 5. Trace sequentially the activities involved in project procurement process. 10 CO4 6. What is a contract and mention its various types? Explain any one type of contract. 10 CO5 7. A simple Project involves preparation of 100 documents requiring equal time and

efforts. [Given that: Standard Cost / document: Rs. 1000; Work Rate: 1 document / day / executive; No. of Executives: 5]. After 5 days, only 20 documents were ready at an actual cost of Rs. 24,000. Calculate cost variance & schedule variance, also estimate the total cost and time required to complete the project if the efficiency remains same.

10 CO4

SECTION B Answer any two (02) questions. Each carries 20 marks. 8. What are the contents/format of a Project Audit report and responsibilities of project

auditor? Explain the various steps of Project Audit Life Cycle. 20

CO4

9. The following table gives the data on a project. ACTIVITY DESCRIPTION IMMEDIATE

PREDECESSORS DURATION

(WEEKS) TOTAL COST RS.

‘000

H Basic design - 10 100

I Hardware design for A H 8 64

J Hardware design for B H 6 96

K Drawings for B J 4 16

L Software specifications J 2 36

M Parts purchase for B J 4 84

N Parts purchase for A I 4 80

O Drawings for A I 5 50

P Installation drawings I,J 5 60

20 CO2


Q Software purchases L 5 80

R Delivery of parts for B M 5 0

S Delivery of parts for A N 3 0

T Software delivery Q 3 0

U Assembly of A O,S 1 14

V Assembly of B K,R 5 80

W Test A U 2 24

X Test B V 3 36

Y Final Installation P,W,X 8 104

Z Final system test Y,T 6 66

a) Draw the Gantt Chart for this project b) Prepare the cost baseline.

10. Consider the data of a project shown in the following table. Activity Immediate

predecessor(s) Time (weeks) Cost (Rs.)

Normal Crash Normal Crash

A - 8 6 4000 4300

B - 5 4 3000 3150

C - 10 8 6000 6800

D A 6 5 4000 4200

E C 7 7 5000 -

F D 9 7 7000 7550

G B,E 3 2 2000 2100

If the indirect cost per week is Rs. 350, find the optimal crashed result of the project network.

20 CO3


Course Objectives

To make the students aware of the overall industrial bioengineering so as to help them

to manipulate the process to the requirement of the industrial needs.

To endow the students with the basics of microbial kinetics, metabolic stoichiometry

and energetics.

To impart knowledge on design and operation of fermentation processes and basics of

bioreactor engineering with all its prerequisites.

To develop bioengineering skills for the production of biochemical product such as

commercially important modern Bioproducts, Industrial Enzymes, Products of plant

and animal cell cultures using integrated biochemical processes.

Course Outcomes On completion of this course, the students will be able to CO1. Apply engineering principles to systems containing biological catalysts to meet the needs of the

society.

CO2. Convert the promises of molecular biology and genetic engineering into new processes to make

bio-products in economically feasible way.

CO3. Interpret the kinetics of living cells and to develop a strategy to solve the issues emerging during

fermentation processes.

CO4. Enhance and modify the biological materials to improve its usefulness by finding the optimal

formulation materials to facilitate product production.

CO5. Apply the basics of microbial kinetics, metabolic stoichiometry & energetics and design of fermentation processes operation of with all its prerequisites Catalog Description

Biochemical designing incorporates sciences and building for the investigation of science, solution, conduct or wellbeing. It propels principal ideas, makes information for the sub-atomic to the organ frameworks levels, and creates imaginative biologics, materials, procedures, inserts and gadgets. Biochemical designing make informatics ways to deal with avert, analyze and treat infection, applying efficient, quantitative and integrative considering and answers for issues vital to science, restorative research and populace examines. The Biochemical building is called upon to configuration instruments, gadgets and programming, to unite learning from numerous specialized sources to grow new systems and to direct the examination expected to take care of clinical issues. This course additionally gives to Chemical Engineering

CHPD -7014 Biochemical Engineering L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure None

Co-requisites -


understudies with a prologue to the bioprocess business and its quick late development. Essential foundation in natural chemistry and science is given, including depictions of single-celled living beings, DNA translation and control. Bioreactor configuration is talked about, including cell stoichiometry and energetics, energy of cell development and passing, bioreactor outline and catalyst catalysis. Cases of procedures incorporate maturations, partition strategies, protein cleaning and monoclonal counter acting agent generation. The course incorporates a works visit in which a portion of the gear utilized as a part of the bioprocessing ventures will be displayed.

Course Content

Unit 1: 04 lecture hours Definition and Scope of Biochemical Engineering, Commercial Aspects of Biochemical Processes, Different Biochemical Unit Operations and Processes, introduction to microbiology Unit 2: 03 lecture hours Principles, Design of Batch and Continuous Sterilization Processes, air sterilization principles, Methods of Air Sterilization, Design of Air Filters, Stoichiometry and energetics of microbial growth Unit 3: 08 lecture hours Oxygen Transfer in Microbial Systems, Oxygen Demands, Mass Transfer Theories, Measurement of Volumetric Mass Transfer Coefficients, Power Requirements in Gassed and Un-gassed Bioreactors, Rheology of Fermentation Fluids Unit 4: 08 lecture hours Introduction and Scope, Mechanism of Enzymatic Catalysis, Allosteric Enzymes, Enzyme Kinetics, Production of Industrial Enzymes, introduction to Immobilization of enzymes and cells, Methods of Immobilization, Kinetics of Immobilized Enzyme Systems, External and Internal Diffusional Characteristics of Immobilized Systems, Kinetics of Microbial Growth, Substrate Utilization and Product Formation in Batch Reactors Unit 5: 07 lecture hours Scale-Up: Basic Concepts and Related Problems, Fed-Batch Fermentation, Principles and Applications, Aerobic and Anaerobic Fermentation: Kinetic Analysis, Comparison with Batch Fermentation, Applications and its Limitations. Enzyme reactors introduction and Performance, Operational Strategies, Carrier Life and Cycle Time, Industrial Applications. Unit 6: 06 lecture hours Aseptic Operations, Measurement and Control of Process Variables (pH, Dissolved Oxygen, Viscosity, Temperature, NADH), Agitative Power, Foam Control, On-Line Analysis and Computer Control of Fermentation Processes. Packed and fluidized bed reactors Analysis and


Applications. Non-mechanically agitated bioreactors such as Airlift and Bubble Column Reactors. Introduction to genetically engineered organisms Text Books

i. Shuler, Michael L. and Fikret Kargi, “Bioprocess Engineering “, Prentice Hall, 1992. ii. Doran M Pauline “Bioprocess Engineering Principles” . 2nd Edition, Elsevier, 2012.

iii. Sivasankar. B Bioseparations: Principles and Techniques, PHI, 2005 iv. Ghasem D.Najafpour, “Biochemical Engineering and Biotechnology”, Elsevier, 2007.

Reference Books 1. Bailey, James E. and David F. Ollis, “Biochemical Engineering Fundamentals”, 2nd

Edition. McGraw Hill, 1986. 2. Peter F. Stanbury, Stephen J. Hall & A. Whitaker, Principles of Fermentation

Technology, Science & Technology Books, 1995. 3. Jens Nielson, John Villadsen and Gunnar Liden, “Bioreaction engineering principles”,

2nd Edition, Kulwer Academic, 2002 4. Tapobrate Panda, “Bioreactors: Analysis and Design”, Tata McGraw Hill, 2011 5. Rajiv Dutta, “Fundamentals of Biochemical Engineering”, Springer, 2008






Programme Outcomes

CO1 Apply engineering principles to systems containing biological catalysts to meet the needs of the society.

PO1, PO2, PO3

CO2 Convert the promises of molecular biology and genetic engineering into new processes to make bio-products in economically feasible way.

PO1, PO2, PO5

CO3 Interpret the kinetics of living cells and to develop a strategy to solve the issues emerging during fermentation processes.

PO2, PO3, PO4, PO5

CO4 Enhance and modify the biological materials to improve its usefulness by finding the optimal formulation materials to facilitate product production.

PO7, PO6, PO11

CO5 Apply the basics of microbial kinetics, metabolic stoichiometry & energetics and design of fermentation processes operation of with all its prerequisites.

PO8, PO9, PO10, PO12


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Course Code


CHPD7014 Biochemical Engineering

3 2 3 1 1 1 1 1 2 2 2 1




Name:

Enrolment No:

Course: CHPD-7014 – Biochemical engineering Program: M. Tech. (CE+PDE) Semester: II (EVEN 2017-18) Time: 03 hrs. Max. Marks: 100 Instructions: Attempt any three questions from Section A (each carrying 10 marks); any Two Questions from Section B (each carrying 15 marks). Section C is Compulsory (carrying 20 marks).

Section A ( answer all the questions)

1. Determine the kinetic constant and maximum rate of velocity of an enzyme substrate reaction by Michaelis Menten method? [10] CO1

2. Differentiate between the structured and unstructured model for the growth of bacteria in a batch fermenter

[10] CO2

3. Describe the air lift bioreactor and packed bed bioreactor [10] CO3

4. Write a short note on enzyme classification? [10] CO1

5. What are the development stages of biotechnology and discuss in detail about the batch growth curve of bacteria. [10] CO1

SECTION B (Attempt any Two Questions)

6. Explain in detail about the selection of impellers for bioreactors [15] CO3 and CO4

7. What are the various methods of enzyme immobilization and explain in detail with its applications

[15] CO1

8. What is meant by sterilization? How it is helping to inhibit the growth of microbes in a batch system?

[15] CO5

SECTION C (answer any one question)

9.

The aerobic growth of S. cerevisiae on ethanol is simply described by the following overall reaction:

C2H5OH + aO2 + bNH3 cCH1.704N0.149O0.408 + dCO2 + eH2O

i. Determine the coefficients a, b, c, d and e where RQ = 0.66 ii. Determine the biomass yield coefficients (YX/S) and oxygen yield coefficient

(YX/O2) iii. Determine degree of reduction for the substrate and bacteria

[20] CO2

10.

(a) How intracellular and extracellular bio products are separated or recovered from the fermented broth? (10 marks)

(b) Explain briefly about the petroleum refinery waste water treatment process? (10 marks)

[20] CO4 and CO5


Course Objectives

22. To introduce the techniques required for analysis of biomass energy systems. 23. To describe gasification and the most common gasification technologies 24. To describe the most common gasification reactions and their dependence on temperature and

pressure and the kinetics of the reactions. 25. To select, size and model different gasifiers.

Course Outcomes On completion of this course, the students will be able to CO15. Understand and analyze the properties of various gasification feed stocks. CO16. Apply the basics of gasification, combustion and important chemical reactions in gasification

and combustion. CO17. Understand the processes that occur during biomass gasification and the operation of different

types of gasifiers. CO18. Describe and differentiate the basic approaches used for modeling of reactors. CO19. Apply the principles of gas clean up, the available types of separation equipment and their

respective capabilities and suitability and some approaches for over all clean up systems.

Catalog Description Gasification is a process that converts organic or fossil fuel based carbonaceous materials into carbon monoxide, hydrogen and carbon dioxide. This is achieved by reacting the material at high temperatures (>700 °C), without combustion, with a controlled amount of oxygen and/or steam. The resulting gas mixture is called syngas (from synthesis gas) or producer gas and is itself a fuel. The power derived from gasification and combustion of the resultant gas is considered to be a source of renewable energy if the gasified compounds were obtained from biomass. The course introduces the students the properties of biomass with specific relevance to gasification and pyrolysis of biomass. It also discusses the design methodologies for gasifiers, and selection of handling equipment for gas cleaning technologies. Course Content

Unit I: 6 lecture hours History, Current Status in Industry, Feed stock and Feed stock Characteristics, Coal, Petcoke, Biomass

Unit II: 8 lecture hours Fundamental Principles of Gasification, Gasification vs. Combustion, Gasification and Combustion Reactions, Stoichiometry, Thermodynamics of Gasification: Thermo-chemistry, Chemical Equilibrium, Reaction Kinetics.


CHPD 7015 Gasification Technology L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure Basics of Heat Transfer, Chemical Thermodynamics and

Chemical Reaction Engineering

Co-requisites --


Different Types of Gasifiers and Gaseous fuels, Coal gasification technology, Biomass gasification, Pyrolysis. Unit IV: 8 lecture hours Modeling of gasification reactors, Downdraft, Fluidized and Entrained gasifiers. Unit V: 6 lecture hours Gas Clean-up Technology, Particulate removal, Gas conditioning, Integration of gasification technologies. Text Books

4. Gasification -Higman, Maarten Van der Burgt 5. Biomass Gasification and Pyrolysis- PrabirBasu

Reference Books 1. D. Bell, B. Towler and M. Fan, Coal Gasification and Its Applications, Elsevier, New

York, 2011. 2. J. Rezaiyan and N. P. Cheremisinoff, Gasification Technologies: A Primer for

Engineers and Scientists, CRC Press, New York, 2005. 3. M. L. de Souza-Santos, Solid Fuels Combustion and Gasification: Modeling,

Simulation, and Equipment Operation, 2nd Ed., CRC Press, New York, 2010. Modes of Evaluation: Quiz/Assignment/ presentation/ extempore/ Written Examination Examination Scheme:





Programme Outcomes

CO1 Understand and analyze the properties of various gasification feed stocks.

PO1,PO2, PO4,PSO1

CO2 Apply the basics of gasification, combustion and important chemical reactions in gasification and combustion.

PO1,PO2, PO3,PO4,PSO1,PSO2

CO3 Understand the processes that occur during biomass gasification and the operation of different types of gasifiers.

PO1,PO2, PO3,PO4, PSO2

CO4 Describe and differentiate the basic approaches used for modeling of reactors.

PO1,PO2, PO3,PO4,PSO1

CO5

Apply the principles of gas clean up, the available types of separation equipment and their respective capabilities and suitability and some approaches for over all clean up systems.

PO1,PO2, PO3,PO4,PSO1,PSO2


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CHPD 7015

Gasification Technology 3 2 3 3

3

3



Course Objectives

26. To help solve simple problems involving basic concepts of polymer science and engineering. 27. To help solve problems involving the morphology and crystallinity of polymers. 28. To help solve problems involving polymerization kinetics and average molecular weights. 29. To expose students to the design of industrial polymerization reactors. 30. To help solve problems involving polymer solution thermodynamics. 31. To help solve problems involving the viscosity of polymers and their processing..

Course Outcomes On completion of this course, the students will be able to CO20. Understand the basic principles and concepts of polymer science and engineering. CO21. Understand some principles of bio-polymers. CO22. Understand simple analytical techniques of polymer characterization. CO23. Solve simple design problems for polymerization reactors. CO24. Solve simple design problems for polymer rheology and processing.

Catalog Description Polymers are of great importance in Engineering. In this course, the focus is on covering both polymer science and polymer engineering (including bio-polymers). Research methods as well as industrial units are discussed. Students get a hands-on experience for the design of real-life industrial units. Course Content

Unit I: 1 lecture hour

Introduction to polymer science and engineering


Basic structure of polymers Unit III: 2 lecture hours

Polymer crystallinity and morphology


Polymer formation, kinetics and average molecular weights


Polymerization: concepts and industrial reactors

CHPD7016 Polymer Engineering L T P C

Version 1.0 3 0 0 4 Pre-requisites/Exposure Undergraduate courses in Chemical Reaction Engineering,

Chemistry

Co-requisites --


Unit VI: 10 lecture hours

Polymer solution thermodynamics (Flory-Huggins theory), phase diagrams, molecular

weight distributions


Viscous flow and elements of viscoelasticity of polymers

Text Books

1. Notes (to be purchased) 2. F. Rodriguez, C. K. Ober and L. A. Archer, Principles of Polymer Systems, 5th ed.,

CRC Press, Boca Routan, 2003 (used to be available in the Soft Edition once upon a time) (R)

3. A. Kumar and S. K. Gupta, Fundamentals of Polymer Science and Engineering, Tata McGraw Hill, New Delhi, 1978 (GK 1)

No single text is sufficient

Reference Books

a) S. K. Gupta and A. Kumar, Reaction Engineering of Step Growth Polymerization, Plenum, New York, 1987 (GK 2)

b) J. R. Fried, Polymer Science and Technology, Prentice Hall of India, New Delhi, 1995, etc.

Modes of Evaluation: Impression-Attendance/Written Examination Examination Scheme:





Programme Outcomes


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CHPD7016 Polymer Engineering 3 2 1 2 3 1 1 1 1 1 1

2

3

3

1 = weakly mapped 2 = moderately mapped 3 = strongly mapped

CO1 Understand the basic principles and concepts of polymer science and engineering. PO1, PO2

CO2 Understand some principles of bio-polymers. PO1, PO2

CO3 Understand simple analytical techniques of polymer characterization.

PO1, PO2, PO5

CO4 Solve simple design problems for polymerization reactors.

PO3, PO4, PO5, PO12

CO5 Solve simple design problems for polymer rheology and processing.

PO3, PO4, PO5, PO12



2016-17-II

Name: ____________________________ Roll No.: ___________________

UNIVERSITY OF PETROLEUM AND ENERGY STUDIES

End Semester Examination: May 2017

Program/Course: M. Tech. Chemical Engg. (spl. PD) Semester: II Subject: Polymer Engineering (Elective) Max. Marks: 100 Code: MREG 706 Duration: 3 Hrs No. of page/s: 0 + 5 In this OPEN BOOK and NOTES EXAM, you are allowed to have the class notes (by S. K. Gupta), all handouts provided, your own class-notes and your solutions to assignment problems

4. Show all intermediate steps of your answers (and not just the final answers) to earn marks

5. Please answer the questions in the sequence: 1, 2, 3. You can do this by assigning, a priori, a few pages to each question, in the correct sequence. You may then answer the questions in whatever sequence you wish to, all parts in one place

6. No student is allowed to leave the examination hall in the first hour of the exam 7. Please submit your question paper at the end of the examination. Try to use the

question paper and do not waste time copying Tables, etc., in your answer script

Section A: XXX No questions here

Section B: ALL THREE QUESTIONS ARE COMPULSORY [Total 100 Marks]

Q.1 Consider the following experimental data on the osmotic pressure, π, as a function of the polymer

concentration, c (for dilute polymer solutions):


No. c, (gm polymer)/

(deciliter solution)

π, cm solvent π/c

1 0.30 0.65

2 0.60 2.0

3 1.00 3.0

4 1.50 6.0

5 2.00 10.0

(a) Complete the third column (answer in the question paper itself) (5 Points)

(b) Plot appropriately on the graph provided on page 3 (of this question paper)

(10 Points)

(c) Use your judgment (take points 1 and 5) to draw a best-fit (by eye) straight line through the data

points (5 Points)

(d) Calculate the average molecular weight, M, for this polymer.

Since you may be uncomfortable with the cgs system, here are a few hints/data:

R = 1.986 cal/(gmol-K);

g = 980 cm/s2;

1 cal = 4.186 × 107 gm-cm2/s2

1 cm solvent (osmotic pressure) = ρsolventg×1 cm =980 gm/(cm-s2)

Take ρsolvent = 1 gm/cm3, T = 300 K (10 Points)

(e) Is your computed value of M the number-, weight- or z-average molecular weight,

𝑀 , 𝑀 𝑜𝑟 𝑀 . (5 Points)

(35 Points)

Continued….


Q.2 Consider Graessley’s molecular theory for the non-Newtonian (pseudo-plastic) viscosity of polymer

systems (concentrated solutions and melts) [script 𝓣𝟎 is 𝝉𝟎]

(a) Fill the Table below (HINT: Remember θ is in radians and not in degrees) and deduce a method to

evaluate 𝜼

𝜼𝟎 as a function of

�̇� 𝝉𝟎

𝟐

θ Cos-1 θ 𝛉(𝟏 − 𝛉𝟐)

(𝟏 + 𝛉𝟐)𝟐

F(θ) ≡ 𝜼

𝜼𝟎 �̇� 𝝉𝟎

𝟐


0.1

0.5

0.8

0.90

0.97

(15 Points)

(b) Plot 𝜼

𝜼𝟎 vs.

�̇� 𝝉𝟎

𝟐 on the graph provided on Page 6 (10 Points)

(c) Evaluate 𝝉𝟎 (with units) if:

c = 1 gm/cm3; R = 1.987 cal/(gmol-K): T = 325 K; η0 = 5 × 105 Poise; M = 105 gm/gmol and

1 Poise = 1 gm/(cm-s); 1 cal = 4.186 × 107 gm-cm2/s2 (05 Points) (30 Points)

Q.3 We are interested in evaluating the entropy of mixing of np,1 molecules of polymer, each having x1

subunits and np,2 molecules of polymer, each having x2 subunits (AND NO SOLVENT MOLECULES;

to keep the problem simple).

(a) Evaluate the number of distinct ways, N, in which you can place these molecules randomly in a lattice

having a coordination number (number of nearest neighbors), z. Solve this from first principles,

placing molecule by molecule. (20

points)

(b) In the absence of any solvent, how would you define x1 and x2. (5 points)

(c) What will be the total number of ways of placing np,1 molecules of pure amorphous polymer, 1, and

np,2 molecules of pure amorphous polymer, 2, before mixing (in appropriate lattices). (10 Points)

(35 Points)


* * *

End Sem Exam MREG 706 Polymer Engg 2016-17-II


Course Objectives 1. To understand the role of utilities in process plant 2. To learn in detail about the utilities system 3. To calculate fundamental physical quantities related to generation of utilities 4. To incorporate safety in use of utilities, and proper waste disposal 5. To understand role of CO2 emission Course Outcomes On completion of this course, the students will be able to CO6. To Understand the Role of Utilities system for smooth operation of Modern of Chemical Plants CO7. To Understand Equipment and systems needed to generate Utilities. CO8. To perform important calculations of size and energy requirement of Utilities System CO9. To Practice Safety as one of the prominent factors for Utilities and waste disposal CO10. To minimize CO2 emission in Utilities System Catalog Description Plant Utilities are very important for process plant because the non-stop operation of process plants is dependent on good management of utilities. The utilizes like water, steam, compressed air, refrigeration, etc. are extremely important. In this subject, the Master level will understand underlying principles related to generation and distribution of utilities with a modern and futuristic point of view. Safety in the Utilities System is of prime importance. CO2 emissions must also be minimized. Apart from class room lectures, students will be expected to gather knowledge from web resources, data banks, software, handbooks, etc. Course Content

Unit I: 4 lecture hours Utility & Offsite System Description Definition and Diagrammatic Description of various Utility Systems in a major Hydrocarbon Plant. Unit II: 6 lecture hours Raw Water & Cooling Water System Raw Water Sources and Analysis, Water Treatment Requirement for various Services, Design Basis and Sizing Cooling Water Header System, Cooling Tower Selection and Specifications. Unit III: 10 lecture hours Steam System Selecting Steam Pressure Levels, Treatment for Boiler Feed Water, Steam Network Design, Condensate Recovery and Recirculation, Steam Traps and their Application, Steam and Condensate Line Sizing. Unit IV: 6 lecture hours Fuel System Fuel Gas System for Fired Heaters, Gas Conditioning for Turbines, Pressure, Temperature and Quality Requirements.

Unit V: 6 lecture hours Instrument and Plant Air System

CHPD 7017 Plant Utility Equipment and Systems L T P C Version 1.0 3 0 0 0 Pre-requisites/Exposure Basic Fluid Mechanics, Heat Transfer, Thermodynamics Co-requisites --


Operating Conditions, Quality Requirements, Estimating Requirements and Specifying Air System.

Unit VI: 2 lecture hours Ancillary Facilities List and Description of other Offsite Facilities in a major Plant Complex, Storage and Handling of Raw Material, Products and Intermediates, Loading and Unloading Facilities.

Unit VII: 2 lecture hours Plant Layout Principles Basic Guidelines in Layout Preparation of a Complex with Process Pant, Utilities and Offsite Facilities, Typical Examples of Plant Layout. Text Books Process Plant Utilities, by Ashutosh Panday, Vipul Prakashan , Mumbai, 1999.

Reference Books

1) Eckenfelder, W. W, Jr. “Industrial Water Pollution Control” McGraw-Hill: New York, 1966.

3) Perry R. H. Green D. W. “Perry's chemical Engineer's Handbook”, McGraw Hill, New York, 2007.

4) P. N. Ananthanarayan, “Basic Refrigeration & Air conditioning”, Tata McGraw Hill, New Delhi, 2007.

5) Boilers Operator Handbook, Elonka



Relationship between the Course Outcomes (COs) and Program Outcomes (POs), Program Specific Outcomes (PSOs),


Course Outcomes (COs) Mapped Programme Outcomes, Program

Specific Outcomes

CO1 Role of Utilities system for smooth operation of Modern of Chemical Plants

PO 1, PSO 1

CO2 To Understand Equipment and systems needed to generate Utilities.

PO 2 PSO 1

CO3 To perform important calculations of size and energy requirement of Utilities System

PO 3 PSO 2

CO4 To Practice Safety as one of the prominent factors for Utilities and waste disposal

PO 9,10 PSO 1

CO5 To minimize CO2 emission in Utilities System PO 4

PSO 1


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CHPL 7002

Plant utility equipment & systems

3 3 3 3 3 3 3 3




Name:

Enrolment No:

Course: CHPD 7017– Plant Utility Equipment and Systems Programme: M.Tech. (Chemical) Semester: ODD-2017-18 Time: 03 hrs. Max. Marks:100 Instructions: Attempt any three questions from Section A (each carrying 10 marks); any Two Questions from Section B (each carrying 15 marks). Section C is Compulsory (carrying 40 marks).

Section A ( attempt any three)

1. [10] CO3 2. [10] CO1 3. [10] CO2 4. [10] CO4 SECTION B (Attempt any Two Questions) 4. [15]

CO4

5. [15] CO2 6. [15] CO5 SECTION C is Compulsory 7. [20] CO4

8. [20] CO4


Course Objectives

32. To provide the basic concepts of catalysis. 33. To introduce the role of catalysis in refining and petrochemicals. 34. To impart the principles of catalyst design for petroleum refining processes. 35. To impart the knowledge of various techniques of physico-chemical characterisation and

evaluation of activity of catalysts. 36. To give a glimpse of emerging trends in catalysis and new catalytic materials.

Course Outcomes On completion of this course, the students will be able to CO25. Understand the basic principles of catalysis CO26. Know the role of catalysis in refining and petrochemicals CO3. Design and develop catalysts for Petroleum Refining processes CO4. Characterize the physico-chemical properties and evaluate the activity of catalysts by various techniques. CO5. Get an insight into emerging trends in catalysis and new catalytic materials. Catalog Description Catalysis is the corner stone of petroleum refining, petrochemicals and chemical processing industries. Designing a chemical process it critically depends on the catalyst behavior and typical example is fluidized catalytic cracking which opened up new areas like fluidization. Concern for environment necessitated stringent specification for auto fuels and process modification which demands continuous effort in catalyst development and improvement. Therefore having an understanding of catalyst and catalysis is of key importance to be a successful chemical engineer. This course will provide the understanding of basic concepts of catalysis and the active centers for various processes employed in refining and petrochemical industries. It offers various techniques of physico-chemical characterization and evaluation of activity of catalysts and enable to relate them. It imparts knowledge on various unit operations and processes used in the general manufacture of industrial catalysts with specific emphasis for refining and petrochemical industries. Course Content

Unit I 4 lecture hours BASICS OF CATALYSIS

Historical Developments--a Tribute to all who Contributed in Building-up the Science of Catalysis to the Present Level, Actions and Classifications, The Arrhenius Rate Equation, Homogenous and Heterogeneous Catalysis Unit II: 4 lecture hours ROLE OF CATALYSIS IN PETROLEUM REFINING AND IN THE PETROCHEMICAL INDUSTRY

Catalytic Technologies for Petroleum Refining and Petrochemicals. Unit III: 4 lecture hours CATALYSIS BY ZEOLITES

CHPD 7020 Catalysis and Catalytic Materials L T P C

Version 1.0 3 0 0 3 Pre-requisites/Exposure Basic knowledge in Chemical Reaction Engineering

Co-requisites --


Chronology of Zeolite Catalyst Development, Zeolite Modifications for Various Catalytic Applications,

Cracking over Amorphous and Zeolitic Catalysts.

Unit IV: 9 lecture hours DESIGNING SPECIFIC CATALYSTS FOR REFINING PROCESS APPLICATIONS

General Assembly of Solid Catalysts, Preparation of Hydro-cracking and Hydro-treating Catalysts,

Effect of Support on Catalytic Functionalities of Mo and W Sulfide Hydro-processing Catalysts, Oxygen

Chemisorptions Support Effects, Designing Reforming Catalysts, Development of Fluid Catalytic

Cracking (FCC) Catalyst, Mechanistic and Thermodynamic Aspects of Catalytic Cracking, FCC Feed vs.

Product Slate Composition, Assembly of Specific Additives for Improving Catalyst Performance,

Catalyst Designing Alkylation and Isomerization Catalyst.

Unit V 10 lecture hours PHYSICO-CHEMICAL CHARACTERIZATION OF CATALYSTS

Determination of Specific Properties of Catalytic Materials, Commonly Used Techniques: Surface

Area, Acidity, Pore Size and Particle Size Distribution, Unit Cell Size, Pore Volume, Zeolite Area,

Crystalline, Elemental Analysis, etc., Spectroscopic Techniques used for Characterization of Catalysts:

an Overview of Various Techniques.

EVALUATION OF CATALYSTS USING VARIOUS TYPES OF REACTORS AND TECHNIQUES OF SIMULATION

TO COMMERCIAL UNITS

Unit V 5 lecture hours NEW CATALYTIC MATERIALS AND EMERGING TRENDS

Environmental Catalysis, Catalytic Distillation, Nano-catalysis. GLOBAL REFINING CATALYSTS

Catalysis Research in India, Catalysis in the 21st Century

Text Books 1. G. Ertl, H. Knozinger and J. Weitkamp, Handbook of Heterogeneous Catalysis (5 volume set), Wiley-VCH, 1997. 2. J. Lynch, Physico-Chemical Analysis of Industrial Catalysts (a Practical Guide to Characterization), Editions Technip, New York, 2003. 3. D. L. Trimm, Catalysts in Petroleum Refining 1989, Elsevier, New York, 1989. 4. A. W. Sleight and U. Chowdhry, Catalyst Design and Application: Applied Industrial Catalysis, Vol. 2, Chp. 1.Research papers 5. B.Viswanathan, S.Sivasanker and A.V.Ramaswamy, Catalysis Principles and Applications, Narosa Publishing House .

Reference Books 1. Applied heterogeneous catalysis: Design-manufacture use of solid catalysts by J.F.LE PAGE,

Technip Editions 2. Concepts of Modern Catalysis and Kinetics by I. Chorkendorff and J.W. Niemantsverdriet,

WILEY-VCH Verlag GmbH & Co.

3. Catalyst Preparation: Science and Engineering Edited by John R. Regalbuto, CRC Press Taylor & Francis Group

4. Thermal and Catalytic Processes in Petroleum Refining by Serge Raseev, Taylor & Francis Group

5. Principles of Catalyst Development by James T. Richardson, Springer US. 6. Nanostructured Catalysts edited by Susannah L. Scott, Cathleen M. Crudden and Christopher W.Jones, Kluwer Academic Publishers.


Modes of Evaluation: Test/Quiz/Assignment/ presentation/ Written Examination Examination Scheme:



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Course Code


Course Code



Programme Outcomes

CO1 Understand the basic principles of catalysis.

PO1 & PO2

CO2 Know the role of catalysis in refining and petrochemicals.

PO1, PO2 & PO4

CO3 Design and develop catalysts for Petroleum Refining processes.

PO1, PO2, PO3, PO4,

PO7, PSO1 & PSO2

CO4 Characterize the physico-chemical properties and evaluate the activity of catalysts by various techniques.

PO1, PO2, PO3, PO4,

PO7, PSO1 & PSO2

CO5 Get an insight into emerging trends in catalysis and new

catalytic materials.

PO1, PO2,PO3,

PO7, PSO1 & PSO2


CHPD 7020

Catalysis and Catalytic Materials

3 3 3 3 2 2 3 1 2 1 2 2 3 3


M.Tech (Chemical) PDE - UPES

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