MedKoo Biosciences control data 13.09 INSTRUM spect PROBHD 5 mm PADUL 13C PULPROG zg30 TD 65536...
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12 11 10 9 8 7 6 5 4 3 2 1 ppm 2.501 2.506 2.510 2.514 2.519 3.358 3.626 3.671 3.839 4.330 4.375 6.434 6.886 6.908 7.007 7.014 7.036 7.043 7.288 7.310 7.881 7.888 7.893 7.906 7.910 7.917 10.977 1.02 3.02 1.00 1.02 1.03 2.03 1.00 2.02 1.02 Current Data Parameters NAME YK-4-279 EXPNO 1 PROCNO 1 F2 - Acquisition Parameters Date_ 20180911 Time 13.09 INSTRUM spect PROBHD 5 mm PADUL 13C PULPROG zg30 TD 65536 SOLVENT DMSO NS 8 DS 2 SWH 8012.820 Hz FIDRES 0.122266 Hz AQ 4.0894465 sec RG 158.27 DW 62.400 usec DE 6.50 usec TE 296.4 K D1 1.00000000 sec TD0 1 ======== CHANNEL f1 ======== SFO1 400.1324710 MHz NUC1 1H P1 10.00 usec PLW1 20.00000000 W F2 - Processing parameters SI 65536 SF 400.1300000 MHz WDW EM SSB 0 LB 0.30 Hz GB 0 PC 1.00 MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences www.medkoo.com [email protected]
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Transcript of MedKoo Biosciences control data 13.09 INSTRUM spect PROBHD 5 mm PADUL 13C PULPROG zg30 TD 65536...
12 11 10 9 8 7 6 5 4 3 2 1 ppm2.501
2.506
2.510
2.514
2.519
3.358
3.626
3.671
3.839
4.330
4.375
6.434
6.886
6.908
7.007
7.014
7.036
7.043
7.288
7.310
7.881
7.888
7.893
7.906
7.910
7.917
10.977
1.02
3.02
1.00
1.02
1.03
2.03
1.00
2.02
1.02
Current Data ParametersNAME YK-4-279EXPNO 1PROCNO 1
F2 - Acquisition ParametersDate_ 20180911Time 13.09INSTRUM spectPROBHD 5 mm PADUL 13CPULPROG zg30TD 65536SOLVENT DMSONS 8DS 2SWH 8012.820 HzFIDRES 0.122266 HzAQ 4.0894465 secRG 158.27DW 62.400 usecDE 6.50 usecTE 296.4 KD1 1.00000000 secTD0 1
======== CHANNEL f1 ========SFO1 400.1324710 MHzNUC1 1HP1 10.00 usecPLW1 20.00000000 W
F2 - Processing parametersSI 65536SF 400.1300000 MHzWDW EMSSB 0LB 0.30 HzGB 0PC 1.00
MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences www.medkoo.com [email protected]
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MedKoo Cat#: 406807 Name: YK-4-279 CAS#: 1037184-44-3 Lot#: C8R09B11 Chemical Formula: C17H13Cl2NO Exact Mass: 365.0222 Molecular Weight: 366.19
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YK-4-279 NMR Analysis, solvent DMSO-d6
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Injection Date : 10-Sep-18, 15:19:26 Tgt Mass(EZX) : Sample Name : YK-4-279 Location : Vial 17 Acq. Operator : 1 Inj : 0 Spec. Reported : Integration Inj Volume : 5 ul
min2 4 6 8
mAU
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DAD1 A, Sig=214,4 Ref=off
2.83
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4.29
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5.20
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Integration Results for DAD1 A, Sig=214,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 2.83 0.05 33.54 11.80 0.69 4.29 0.05 4775.88 1537.01 98.69 5.21 0.05 29.80 8.76 0.62
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MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected]
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MedKoo Cat#: 406807 Name: YK-4-279 CAS#: 1037184-44-3 Lot#: C8R09B11 Chemical Formula: C17H13Cl2NO Exact Mass: 365.0222 Molecular Weight: 366.19
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YK-4-279 HPLC Analysis
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Injection Date : 10 Sep 18 4:10 pm +0800 Tgt Mass(EZX) : Sample Name : YK-4-279 Location : Vial 25 Acq. Operator : D Inj : 1 Spec. Reported : MS Integration Inj Volume : 5 ul
min1 2 3 4
mAU
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1000
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DAD1 A, Sig=214,4 Ref=off
2.67
8
3.00
5
min1 2 3 4
200000
400000
600000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
2.70
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Integration Results for DAD1 A, Sig=214,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 2.68 0.08 10278.23 1976.87 99.45 3.01 0.05 56.51 19.30 0.55
LC/MS Report
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MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected]
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MedKoo Cat#: 406807 Name: YK-4-279 CAS#: 1037184-44-3 Lot#: C8R09B11 Chemical Formula: C17H13Cl2NO Exact Mass: 365.0222 Molecular Weight: 366.19
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YK-4-279 MS Analysis
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Ret. Time: 2.71 <<<< POSITIVE SPECTRA >>>>
LC/MS Report
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m/z100 200 300 400 500 600 700 800 900
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15000
20000
25000
30000
ES-API Positive
369
.0 390
.0
368
.0 3
66.0
60.
1
MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected]
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Bio
scie
nces
ww
w.m
edko
o.co
msa
les@
med
koo.
com
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MedKoo Cat#: 406807 Name: YK-4-279 CAS#: 1037184-44-3 Lot#: C8R09B11 Chemical Formula: C17H13Cl2NO Exact Mass: 365.0222 Molecular Weight: 366.19
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YK-4-279 MS Analysis
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![Certificate of Analysis - MedKoo · 2017-08-17 · Certificate of Analysis MedKoo Cat#: Product Name: Lot# 202250 Pixantrone Maleate TZC40615 Chemical name 6,9-bis((2-aminoethyl)amino)benzo[g]isoquinoline-5,10-dione](https://static.fdocuments.net/doc/165x107/5f9f51de7ab88e01124dceca/certificate-of-analysis-medkoo-2017-08-17-certificate-of-analysis-medkoo-cat.jpg)
