wwwitquimaes

LABORATORY OF

CATALYSIS AND MATERIALS

Institute of Chemical and Environmental Technologies

wwwitquimaes

LABORATORY OF CATALYSIS AND MATERIALS Institute of Chemical and Environmental

Technologies (ITQUIMA)

University of castilla la Mancha

Avenida Camilo Joseacute Cela sn

13004 Ciudad Real

Tel +34 902 204100 (ext96322)

Responsible for laboratory

Joseacute Luis Valverde Palomino

Tel +34 926 295 3000 |Ext 5437

JoseLuisValverdeuclmes

ITQUIMA UCLMLABORATORY OF CATALYSIS AND MATERIALS

INNOVATION AND TECHNOLOGICAL

DEVELOPMENT

DIFFERENTIAL VALUE

Synthesis and characterization of

Graphene and other carbon and

inorganic nanomaterials (CNT

CNFCNS CrO ZnO Al2O

3 etc)

2

Calentamiento

(81 C) y agitacioacuten

Ultrasonidos(1h)

Mezclado y Agitacioacuten (1min)

Liofilizacioacuten- Tiempo de congelacioacuten6h-Presioacuten de vaciacuteo 008 mbar

-Temperatura de bandeja 35degC-Tiempo del proceso 6+27 h

AguaPVA

AguaMateriales Nanocarbonosos

Synthesis at lab and pilot plant scale

and characterization of polymer

composites and aerogels doped

with nanomaterials

AEROGELGRAFENE

Thermochemical valorisation of agro-industrial wastes and vegetable and

animal biomass (terrestrial and marine) through pyrolysis combustion and

gasification processes at lab and pilot plant scale

$

A SINGLE CENTER FOR ALL THE

TECHNOLOGICAL SERVICES

(SINGLE POINT LAB)

7

LABORATORY OF CATALYSIS AND MATERIALS

(UCLM)

Development of new materials

BUSINESS

Innovation and support

FROM INNOVATION TO MARKET IMPLEMENTATION

Products Ash biofuelgas

M

EnergyBIOMASS VALORIZATION

Thermochemical processesto pilot plant scale

Thermochemical processesat laboartory scale

Dried- Crushed

ITQUIMA UCLM

Chemical processes analysis and life cycle assessment (SIMAPRO)

Simulation modelling optimization and basic engineering of

chemical processes

Catalytic and electrocatalytic processes for the transformation of

alcohols ammonia synthesis gas and waste products (CO2) into

higher-added value compounds

Catalysis and Electrocatalysis

bull Synthesisofcatalystsat labandbenchscale

bull Spin-coaterandelectrodepreparationrobot

bull Physical-chemical characterization of catalysts (BET

TPDTPRTPOacidity chemisorptionoxidation by

pulses titrationsetc)

bull Electrochemical characterization of electrocatalysts

(rotarydisc ECSAanalysisTafelcurvesetc)

bull Different catalytic and electrocatalytic

configurations analysis of effluents (GC microGC

andHPLC)

PROCESSES AND PRODUCTS

FROM THE LAB TO THE INDUSTRIAL DEPLOYMENT

36

LABORATORY OF CATALYSIS AND MATERIALS

Biomass

Air

DRYER

Air

CRUSHER

Air

COMBUSTOR

CYCLONE

Ash

Gas

RANKINE CYCLE

BURNDECOMP

Q

InputGoods

Services

ResourcesProcess

CO2

CO

NOx

CH4

Wastes

4 5

ITQUIMA UCLM

SERVICES AND TECHNICAL ADVISORY SERVICES

Physical-chemical tests

bull Turbidity index (TSI)

bull Scanning electron microscopy

(SEM)

bull Fourier transform infrared

spectroscopy (FTIR)

bull Volume and density of

powders foams and bulk

solids

bull Pore size and pore distribution

(Hg porosimetryand BET)

bull Abrasion test of materials

bull Surface tension

bull Sound absorption analysis

Thermogravimetric and

thermal analysis

bull Differential scanning calorimetry

(DSC)

bull TGA-MS at atmospheric and high

pressure

bull Thermal conductivity of materials

bull Flash pyrolyzer coupled to GC-MS

Sample preparation

bull Extruder

bull Injection moulding

bull Sample cutting press

bull Powder and conductive samples for SEM

analysis

bull Centrifugation orbital mixing and

grinding

bull Solid V-Mixer

Mechanical tests and Rheology

bull Dynamic mechanical analysis (DMA)

bull Tensile flexural and compression

bull Shore D hardness

bull Rheology of liquids and suspensions

bull Curing of adhesives and resins

LABORATORY OF CATALYSIS AND MATERIALS

ITQUIMA UCLM

Chemical processes analysis and life cycle assessment (SIMAPRO)

Simulation modelling optimization and basic engineering of

chemical processes

Catalytic and electrocatalytic processes for the transformation of

alcohols ammonia synthesis gas and waste products (CO2) into

higher-added value compounds

Catalysis and Electrocatalysis

bull Synthesisofcatalystsat labandbenchscale

bull Spin-coaterandelectrodepreparationrobot

bull Physical-chemical characterization of catalysts (BET

TPDTPRTPOacidity chemisorptionoxidation by

pulses titrationsetc)

bull Electrochemical characterization of electrocatalysts

(rotarydisc ECSAanalysisTafelcurvesetc)

bull Different catalytic and electrocatalytic

configurations analysis of effluents (GC microGC

andHPLC)

PROCESSES AND PRODUCTS

FROM THE LAB TO THE INDUSTRIAL DEPLOYMENT

36

LABORATORY OF CATALYSIS AND MATERIALS

Biomass

Air

DRYER

Air

CRUSHER

Air

COMBUSTOR

CYCLONE

Ash

Gas

RANKINE CYCLE

BURNDECOMP

Q

InputGoods

Services

ResourcesProcess

CO2

CO

NOx

CH4

Wastes

4 5

ITQUIMA UCLM

SERVICES AND TECHNICAL ADVISORY SERVICES

Physical-chemical tests

bull Turbidity index (TSI)

bull Scanning electron microscopy

(SEM)

bull Fourier transform infrared

spectroscopy (FTIR)

bull Volume and density of

powders foams and bulk

solids

bull Pore size and pore distribution

(Hg porosimetryand BET)

bull Abrasion test of materials

bull Surface tension

bull Sound absorption analysis

Thermogravimetric and

thermal analysis

bull Differential scanning calorimetry

(DSC)

bull TGA-MS at atmospheric and high

pressure

bull Thermal conductivity of materials

bull Flash pyrolyzer coupled to GC-MS

Sample preparation

bull Extruder

bull Injection moulding

bull Sample cutting press

bull Powder and conductive samples for SEM

analysis

bull Centrifugation orbital mixing and

grinding

bull Solid V-Mixer

Mechanical tests and Rheology

bull Dynamic mechanical analysis (DMA)

bull Tensile flexural and compression

bull Shore D hardness

bull Rheology of liquids and suspensions

bull Curing of adhesives and resins

LABORATORY OF CATALYSIS AND MATERIALS

4 5

ITQUIMA UCLM

SERVICES AND TECHNICAL ADVISORY SERVICES

Physical-chemical tests

bull Turbidity index (TSI)

bull Scanning electron microscopy

(SEM)

bull Fourier transform infrared

spectroscopy (FTIR)

bull Volume and density of

powders foams and bulk

solids

bull Pore size and pore distribution

(Hg porosimetryand BET)

bull Abrasion test of materials

bull Surface tension

bull Sound absorption analysis

Thermogravimetric and

thermal analysis

bull Differential scanning calorimetry

(DSC)

bull TGA-MS at atmospheric and high

pressure

bull Thermal conductivity of materials

bull Flash pyrolyzer coupled to GC-MS

Sample preparation

bull Extruder

bull Injection moulding

bull Sample cutting press

bull Powder and conductive samples for SEM

analysis

bull Centrifugation orbital mixing and

grinding

bull Solid V-Mixer

Mechanical tests and Rheology

bull Dynamic mechanical analysis (DMA)

bull Tensile flexural and compression

bull Shore D hardness

bull Rheology of liquids and suspensions

bull Curing of adhesives and resins

LABORATORY OF CATALYSIS AND MATERIALS