J57832-1 EnviroTest Level 2 Portrait Smp Sort Rev(1) …newtowncreek.info/docs2/2 Remedial...

ANALYTICAL REPORT

Job Number: 420-57832-1

SDG Number: L1213994

Job Description: Newtown Creek

For:

Alpha Analytical

8 Walkup Drive

Westborough, MA 01581

Attention: Mr. Chris Anderson

Renee Cusack

Lab Director

[email protected]

10/17/2012

Revision: 1

Lab Results Lab Resultscc:

The test results in this report meet all NELAP requirements unless specified within the case narrative. Pursuant to NELAP, this

report may not be reproduced, except in full, without the written approval of the laboratory. EnviroTest Laboratories Inc. certifies that

the analytical results contained herein apply only to the samples tested as received by our laboratory. All questions regarding this

report should be directed to the EnviroTest Customer Service Representative.

EnviroTest Laboratories, Inc. Certifications and Approvals: NYSDOH 10142, NJDEP NY015, CTDOPH PH-0554, EPA NY00049

315 Fullerton Avenue, Newburgh, NY 12550

Tel (845) 562-0890 Fax (845) 562-0841 www.envirotestlaboratories.com

Envirotest Laboratories, Inc.

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METHOD SUMMARY

Job Number: 420-57832-1Client: Alpha Analytical

Sdg Number: L1213994

Preparation MethodMethodLab LocationDescription

Matrix: Water

SM20 SM 5210B5 Day BOD test EnvTest

SM18 SM 9222BMembrane Filter Technique - Standard Total Coliform

Procedure

EnvTest

SM18 SM 9222DMembrane Filter Technique - Fecal Coliform Procedure EnvTest

SM21 SM5210B*M30 Day BOD Test EnvTest

Lab References:

EnvTest = EnviroTest

Method References:

SM18 = "Standard Methods For The Examination Of Water And Wastewater", 18th Edition, 1992.

SM20 = "Standard Methods For The Examination Of Water And Wastewater", 20th Edition."

SM21 = "Standard Methods For The Examination Of Water And Wastewater", 21st Edition

EnviroTest Laboratories, Inc.

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SAMPLE SUMMARY

Client: Alpha Analytical Job Number: 420-57832-1


Client Sample IDLab Sample ID Client Matrix

Date/Time

Sampled

Date/Time

Received

08/07/2012 0925 08/08/2012 0810NC034SW-A-20120807420-57832-1 Water

08/07/2012 1002 08/08/2012 0810NC034SW-C-20120807420-57832-2 Water

08/07/2012 1233 08/08/2012 0810EK014SW-A-20120807420-57832-3 Water

08/07/2012 1253 08/08/2012 0810EK014SW-C-20120807420-57832-4 Water

08/07/2012 1357 08/08/2012 0810EK022SW-A-20120807420-57832-5 Water

08/07/2012 1357 08/08/2012 0810EK1022SW-A-20120807420-57832-6 Water


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SAMPLE RESULTS


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Mr. Chris Anderson

Alpha Analytical

8 Walkup Drive


Job Number: 420-57832-1


Client Sample ID:

Analyte Result/Qualifier Unit Dilution

08/08/2012 0810

08/07/2012 0925

Date Received:

Date Sampled:

Lab Sample ID:

NC034SW-A-20120807

RL

Client Matrix: Water

420-57832-1

Method: SM 5210B Date Analyzed: 08/08/2012 1200

Biochemical Oxygen Demand 4.58 mg/L 2.00 1.0

Method: SM5210B*M Date Analyzed: 08/08/2012 1200



Coliform, Total 6300 CFU/100mL 100 100

Method: SM 9222D Date Analyzed: 08/08/2012 0900

Coliform, Fecal 4800 CFU/100mL 100 100

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Mr. Chris Anderson

Alpha Analytical

8 Walkup Drive


Job Number: 420-57832-1


Client Sample ID:


08/08/2012 0810

08/07/2012 1002

Date Received:

Date Sampled:

Lab Sample ID:

NC034SW-C-20120807

RL


420-57832-2


Biochemical Oxygen Demand <2.00 mg/L 2.00 1.0




Coliform, Total 630 CFU/100mL 10.0 10


Coliform, Fecal 340 CFU/100mL 10.0 10

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Mr. Chris Anderson

Alpha Analytical

8 Walkup Drive


Job Number: 420-57832-1


Client Sample ID:


08/08/2012 0810

08/07/2012 1233

Date Received:

Date Sampled:

Lab Sample ID:

EK014SW-A-20120807

RL


420-57832-3









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Mr. Chris Anderson

Alpha Analytical

8 Walkup Drive


Job Number: 420-57832-1


Client Sample ID:


08/08/2012 0810

08/07/2012 1253

Date Received:

Date Sampled:

Lab Sample ID:

EK014SW-C-20120807

RL


420-57832-4


Biochemical Oxygen Demand <6.00 mg/L 6.00 3.0







of 19

Mr. Chris Anderson

Alpha Analytical

8 Walkup Drive


Job Number: 420-57832-1


Client Sample ID:


08/08/2012 0810

08/07/2012 1357

Date Received:

Date Sampled:

Lab Sample ID:

EK022SW-A-20120807

RL


420-57832-5









of 19

Mr. Chris Anderson

Alpha Analytical

8 Walkup Drive


Job Number: 420-57832-1


Client Sample ID:


08/08/2012 0810

08/07/2012 1357

Date Received:

Date Sampled:

Lab Sample ID:

EK1022SW-A-20120807

RL


420-57832-6








Coliform, Fecal 260 CFU/100mL 10.0 10

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DATA REPORTING QUALIFIERS


Lab Section Qualifier Description


Biology

Duplicate RPD exceeds the control limitF


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Definitions and Glossary

Abbreviation These commonly used abbreviations may or may not be present in this report.

%R

DL, RA, RE

EPA

MDL

ND

QC

RL

RPD

Percent Recovery

Indicates a Dilution, Reanalysis or Reextraction.

United States Environmental Protection Agency

Method Detection Limit - an estimate of the minimum amount of a substance that an analytical

process can reliably detect. A MDL is analyte- and matrix-specific and may be

laboratory-dependent.

Not detected at the reporting limit (or MDL if shown).

Quality Control

Reporting Limit - the minimum levels, concentrations, or quantities of a target variable (e.g.,

target analyte) that can be reported with a specified degree of confidence.

Relative Percent Difference - a measure of the relative difference between two points.


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QUALITY CONTROL RESULTS


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Quality Control Results



WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

08/08/2012 1200

Method Blank - Batch: 420-58472

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 420-58472

Prep Batch: N/A

mL

mL

N/A

Units: mg/L

Method: SM 5210B

Preparation: N/A

N/A

No Equipment AssignedMB 420-58472/1

Analyte Result Qual RL

<2.00 2.00Biochemical Oxygen Demand

Water

1.0

08/08/2012 1200Date Analyzed:

Lab Control Spike - Batch: 420-58472

Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



N/A


Prep Batch: N/A

mL

300 mL

Units: mg/L

Method: SM 5210B

Preparation: N/A

N/A

No Equipment AssignedLCS 420-58472/2

Analyte QualLimit% Rec.ResultSpike Amount

198 213.0 108 85 - 115Biochemical Oxygen Demand

mg/LUnits:

Water

Dilution: 1.0

Date Analyzed:

Duplicate - Batch: 420-58472

Lab Sample ID:

Client Matrix:

Date Prepared:

08/08/2012 1200

Instrument ID:

Lab File ID:




Prep Batch: N/A

mL

mL

N/A

Method: SM 5210B

Preparation: N/A

N/A

No Equipment Assigned420-57832-1

Analyte QualLimitRPDResultSample Result/Qual

4.4804.58 2 20Biochemical Oxygen Demand


Calculations are performed before rounding to avoid round-off errors in calculated results.

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WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

08/08/2012 0900


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:


Prep Batch: N/A

N/A

Units: CFU/100mL

Method: SM 9222B

Preparation: N/A

N/A



<1.00 1.00Coliform, Total

CFU/100mLUnits:

Water

Dilution: 100

Date Analyzed:


Lab Sample ID:

Client Matrix:

Date Prepared:

08/08/2012 0900

Instrument ID:

Lab File ID:



Injection Volume:


Prep Batch: N/A

mL

mL

N/A

Method: SM 9222B

Preparation: N/A

N/A



52006300 19 20Coliform, Total



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WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

08/08/2012 0900


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:


Prep Batch: N/A

N/A

Units: CFU/100mL

Method: SM 9222D

Preparation: N/A

N/A



<1.00 1.00Coliform, Fecal

CFU/100mLUnits:

Water

Dilution: 100

Date Analyzed:


Lab Sample ID:

Client Matrix:

Date Prepared:

08/08/2012 0900

Instrument ID:

Lab File ID:



Injection Volume:


Prep Batch: N/A

mL

mL

N/A

Method: SM 9222D

Preparation: N/A

N/A



37004800 26 20 FColiform, Fecal



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WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

08/08/2012 1200


Date Prepared:

Instrument ID:

Lab File ID:




Prep Batch: N/A

N/A

Units: mg/L

Method: SM5210B*M

Preparation: N/A

N/A



<2.00 2.00Biochemical Oxygen Demand

mg/LUnits:

Water

Dilution: 4.0

Date Analyzed:


Lab Sample ID:

Client Matrix:

Date Prepared:

08/08/2012 1200

Instrument ID:

Lab File ID:




Prep Batch: N/A

N/A

Method: SM5210B*M

Preparation: N/A

N/A



20.2022.1 9 20Biochemical Oxygen Demand



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LOGIN SAMPLE RECEIPT CHECK LIST



Question T/F/NA Comment

Login Number: 57832

Samples were collected by ETL employee as per SOP-SAM-1 NA

The cooler's custody seal, if present, is intact. NA

The cooler or samples do not appear to have been compromised or tampered with. True

Samples were received on ice. True

Cooler Temperature is recorded. 5.4 CTrue

Cooler Temp. is within method specified range.(0-6 C PW, 0-8 C NPW, or BAC <10

C

True

If false, was sample received on ice within 6 hours of collection. NA

Based on above criteria cooler temperature is acceptable. True

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

There are no discrepancies between the sample IDs on the containers and the

COC.

True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True

VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. NA

If necessary, staff have been informed of any short hold time or quick TAT needs True

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

EnviroTest Laboratories, Inc. of 19

J57832-1 EnviroTest Level 2 Portrait Smp Sort Rev(1) …newtowncreek.info/docs2/2 Remedial...

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