ICP Test Report Certification Packet - Littelfuse/media/files/littelfuse/...2011/06/29 · Item No....
Transcript of ICP Test Report Certification Packet - Littelfuse/media/files/littelfuse/...2011/06/29 · Item No....
1
ICP Test Report Certification Packet
Company name : Littelfuse, Inc.
Product Series: FUSE - BF1 32V
Product #: 153.5631.xxxx Series
Issue Date: June 29, 2011
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the FUSE - BF1 RoHS-Compliant series products manufactured by
Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:.
Form 585-047 Rev. A 2/21/06
2
Table 1: List of Raw Materials covered by this report
Total Parts Raw Material Part
Number Raw Material Description Page(s)
1 355.1115.xxxx Element - Sn Plated Wire (50-200A) 3-9
2 353.1115.xxxx Melting Wire – Sn Plated Wire (30-200A) 11-13
3 353.1590.0001 BF1 Solder 14-17
4 326.2140.0000 Colorant – Amber 18-26
5 353.2140.1000 Cover Clear 27-31
6 325.7695.0110 Colorant Yellow 32-36
7 353.2131.4600 Body Yellow (60A) 37-45
8 353.1119.xxxx Melting Wire/ Element – Sn Plated Wire
(23A-30A) 46-49
9 353.2130.xxxx
Housing BF1 – 23A (Brown Colorant – 325.7692.0610
Base 325.2131.0001) 50-69
10 353.2131.4800 Housing BF1 – (80A) 70-78
11 325.7692.0000 Colorant Natural/ white – (80A) 79-87
Report No.: MX11-0928-04
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
RESULTS REPORT
INTERTEK TESTING SERVICES
DE MEXICO SA DE CV
LABORATORIO CD. DE MEXICO
DELIVER TO: Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila
ATTENTION: Ing. María Valdez
Report No.: MX11-0928-04
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
TEST REPORT
APPLICANT
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila
Ing. María Valdez
SAMPLE DESCRIPTION
One (1) group of submitted samples said to be :
Sample Description NP
Item No. 4) N/P 353.1115.6043
Country of Origin NP
Buyer's Name NP
Supplier's Name NP
Date sample received 2011-05-05
Testing period 2011-05-09 to 2011-05-13
********************************************************************************************
TEST CONDUCTED
As requested by the applicant, for details please refer to attached pages.
********************************************************************************************
CONCLUSION
Sample Number Testing item Conclusion Failed component Failed result
4
(Base) N/P 353.1115.6043
Pass
See Result summary --- ---
4
(Plated) N/P 353.1115.6043
Pass
See Result summary --- ---
********************************************************************************************
TEST CONDUCTED
Samples:
Report No.: MX11-0928-04
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
4) Base N/P 353.1115.6043
4) Plated N/P 353.1115.6043
TEST RESULT SUMMARY FOR RoHS DIRECTIVE :
TESTING ITEM
Ω RESULT (ppm) Limit (4)
Base
(4)
Plated
Cadmium (Cd) content ND ND 0,01% (100 ppm)
Lead (Pb) content 14,19 78,26 0,1% (1000 ppm)
Mercury (Hg) content ND ND 0,1% (1000 ppm)
Chromium (VI) (Cr6+
) ND ND 0,1% (1000 ppm)
ppm = parts per million based on dry weight of sample.
µg/cm2 = microgram per square centimeter.
mg/kg WITH 50cm2 = milligram per kilogram with 50 square centimeter.
< = less than.
ND = Not detected.
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω.
Prepared and checked by:
For Intertek Laboratory Manager
The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,).
NOTE : DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMENDMENT 2005/717/EC.
# =ACCORDING TO IEC 62321, A POSITIVE RESULT INDICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION AND SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX11-0928-04 WERE TESTED SEPARATED.
Test method:
Report No.: MX11-0928-04
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
4 Chromium VI (Cr
6+)
content With reference to USEPA 3060, by EPA 7196
QHU2010-61p73 2011-05-13 MELA 20,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
4 (Base) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 5,0
4 (Plated) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 41,67
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
4 (Base) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 2,0
4 (Plated) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 16,7
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
4 (Base) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 0,25
4 (Plated) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 2,5
Report No.: MX11-0928-06
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
RESULTS REPORT
INTERTEK TESTING SERVICES
DE MEXICO SA DE CV
LABORATORIO CD. DE MEXICO
DELIVER TO: Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila
ATTENTION: Ing. María Valdez
Report No.: MX11-0928-06
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
TEST REPORT
APPLICANT
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila
Ing. María Valdez
SAMPLE DESCRIPTION
One (1) group of submitted samples said to be :
Sample Description NP
Item No. 6) BFI SOLDER N/P 353.1590.0001
Country of Origin NP
Buyer's Name NP
Supplier's Name NP
Date sample received 2011-05-05
Testing period 2011-05-09 to 2011-05-13
********************************************************************************************
TEST CONDUCTED
As requested by the applicant, for details please refer to attached pages.
********************************************************************************************
CONCLUSION
Sample Number Testing item Conclusion Failed component Failed result
6
(Base)
BFI SOLDER N/P 353.1590.0001
Pass
See Result summary --- ---
6
(Plated)
BFI SOLDER N/P 353.1590.0001
Pass
See Result summary --- ---
********************************************************************************************
TEST CONDUCTED
Samples:
Report No.: MX11-0928-06
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
6) Base BFI SOLDER N/P 353.1590.0001
6) Plated BFI SOLDER N/P 353.1590.0001
TEST RESULT SUMMARY FOR RoHS DIRECTIVE :
TESTING ITEM
Ω RESULT (ppm) Limit (6)
Base
(6)
Plated
Cadmium (Cd) content ND ND 0,01% (100 ppm)
Lead (Pb) content 344,6 69,33 0,1% (1000 ppm)
Mercury (Hg) content ND ND 0,1% (1000 ppm)
Chromium (VI) (Cr6+
) ND ND 0,1% (1000 ppm)
ppm = parts per million based on dry weight of sample.
µg/cm2 = microgram per square centimeter.
mg/kg WITH 50cm2 = milligram per kilogram with 50 square centimeter.
< = less than.
ND = Not detected.
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω.
Prepared and checked by:
For Intertek Laboratory Manager
The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,).
NOTE : DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMENDMENT 2005/717/EC.
# =ACCORDING TO IEC 62321, A POSITIVE RESULT INDICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION AND SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX11-0928-06 WERE TESTED SEPARATED.
Test method:
Report No.: MX11-0928-06
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
6 Chromium VI (Cr
6+)
content With reference to USEPA 3060, by EPA 7196
QHU2010-61p73 2011-05-13 MELA 20,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
6 (Base) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 5,0
6 (Plated) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 50,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
6 (Base) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 2,0
6 (Plated) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 20,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
6 (Base) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 0,25
6 (Plated) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 2,5
TEST REPORT NUMBER : TWNC00104294
AUTHORIZED BY: ON BEHALF OF INTERTEK TESTING SERVICES TAIWAN LIMITED
K. Y. LIANG DIRECTOR
THIS REPORT SHALL NOT BE REPRODUCED EXCEPT IN FULL, WITHOUT THE WRITTEN APPROVAL OF THE LABORATORY.
PAGE 1 OF 9
,
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APPLICANT: LITTELFUSE, INC. DATE : JAN 19, 2009 800 E. NORTHWEST HWY
DESPLAINES IL 60016
SAMPLE DESCRIPTION: ONE (1) GROUP OF SUBMITTED SAMPLES SAID TO BE : PART DESCRIPTION : COLORANT AMBER PART NUMBER : 326.2140.0000 FACILITY : DUNSEN DATE SAMPLE RECEIVED : JAN 14, 2009 DATE TEST STARTED : JAN 14, 2009 ***************************************************************************
TEST CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS PLEASE REFER TO ATTACHED PAGES. ***************************************************************************
NUMBER : TWNC00104294
TEST CONDUCTED
PAGE 2 OF 9
,
!"#$%&$$'%()(%*+!"#$%&$$'%'
() TEST RESULT SUMMARY : RESULT (ppm)
TESTING ITEM CLEAR AMBER PLASTIC BEAN
HEAVY METALCADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND
POLYBROMINATED BIPHENYLS (PBBs)MONOBROMINATED BIPHENYLS (MONOBB) ND DIBROMINATED BIPHENYLS (DIBB) ND TRIBROMINATED BIPHENYLS (TRIBB) ND TETRABROMINATED BIPHENYLS (TETRABB) ND PENTABROMINATED BIPHENYLS (PENTABB) ND HEXABROMINATED BIPHENYLS (HEXABB) ND HEPTABROMINATED BIPHENYLS (HEPTABB) ND OCTABROMINATED BIPHENYLS (OCTABB) ND NONABROMINATED BIPHENYLS (NONABB) ND DECABROMINATED BIPHENYL (DECABB) ND
POLYBROMINATED DIPHENYL ETHERS (PBDEs)MONOBROMINATED DIPHENYL ETHERS (MONOBDE) ND DIBROMINATED DIPHENYL ETHERS (DIBDE) ND TRIBROMINATED DIPHENYL ETHERS (TRIBDE) ND TETRABROMINATED DIPHENYL ETHERS (TETRABDE) ND PENTABROMINATED DIPHENYL ETHERS (PENTABDE) ND HEXABROMINATED DIPHENYL ETHERS (HEXABDE) ND HEPTABROMINATED DIPHENYL ETHERS (HEPTABDE) ND OCTABROMINATED DIPHENYL ETHERS (OCTABDE) ND NONABROMINATED DIPHENYL ETHERS (NONABDE) ND DECABROMINATED DIPHENYL ETHER (DECABDE) ND
HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) 1914 BROMINE (Br) ND IODINE (I) ND
REMARKS : ppm = PARTS PER MILLION BASED ON WEIGHT OF TESTED SAMPLE ND = NOT DETECTED
RESPONSIBILITY OF CHEMIST: IRENE CHIOU / KEVIN LIU / CATHY CHEN
DATE SAMPLE RECEIVED : JAN 14, 2009 TESTING PERIOD : JAN 14, 2009 TO JAN 17, 2009
******************************************************************************
NUMBER : TWNC00104294
TEST CONDUCTED
PAGE 3 OF 9
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() ROHS REQUIREMENT : RESTRICTED SUSTANCES LIMITS
CADMIUM (Cd) 0.01% (100ppm)LEAD (Pb) 0.1% (1000ppm)MERCURY (Hg) 0.1% (1000ppm)CHROMIUM (VI)(Cr6+) 0.1% (1000ppm)POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm)POLYBROMINATED DIPHENYL EHTERS (PBDEs) 0.1% (1000ppm)
() TEST METHOD : TESTING ITEM TESTING METHOD REPORTING LIMIT
CADMIUM (Cd) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
LEAD (Pb) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
MERCURY (Hg) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
CHROMIUM VI (Cr6+)CONTENT
WITH REFERENCE TO USEPA 3060A & 7196A, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER
1 ppm
POLYBROMINATEDBIPHENYLS (PBBs)
WITH REFERENCE TO IEC 62321-111/95/CDV IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY
5 ppm
******************************************************************************
NUMBER : TWNC00104294
TEST CONDUCTED
PAGE 4 OF 9
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() TEST METHOD : TESTING ITEM TESTING METHOD REPORTING LIMIT
POLYBROMINATEDDIPHENYL ETHERS (PBDEs)
WITH REFERENCE TO IEC 62321-111/95/CDV IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY
5 ppm
HALOGEN CONTENTWITH REFERENCE TO EN 14582:2007 BY COMBUSTION FLASK WITH OXYGEN AND DETERMINED BY ION CHROMATOGRAPHY
50 ppm
REMARKS : REPORTING LIMIT = QUANTITATION LIMIT OF ANALYTE IN SAMPLE TESTS WERE CONDUCTED WITH REFERENCE TO 111/95/CDV VERSION 2007-
10-12 WHICH IS STILL A DRAFT METHOD AND SUBJECT TO FUTURE CHANGES PRIOR TO PUBLICATION.
******************************************************************************
NUMBER : TWNC00104294
TEST CONDUCTED
PAGE 5 OF 9
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() MEASUREMENT FLOWCHART:
TEST FOR Cd/Pb/Hg CONTENTSREFERENCE STANDARD: IEC 62321 (111/95/CDV)
REMARKS:*1: LIST OF APPROPRIATE ACID
MATERIAL ACID ADDED FOR DIGESTION
POLYMERS HNO3,HCl,HF,H2O2,H3BO3METALS HNO3,HCl,HFELECTRONICS HNO3,HCl,H2O2,HBF4
******************************************************************************
SAMPLING/GRINDING OR CUTTING
FOR DIFFERENT MATERIAL, DIGEST THE SAMPLE WITH APPROPRIATE ACID*1
MAKE UP WITH DEIONIZED WATER
ANALYZED BY ICP-OES
CONFIRM THE TESTED SAMPLES ARE TOTALLY DISSOLVED
NUMBER : TWNC00104294
TEST CONDUCTED
PAGE 6 OF 9
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() MEASUREMENT FLOWCHART:
TEST FOR CHROMIUM (VI) CONTENTREFERENCE STANDARDUSEPA 3060A/7196A
******************************************************************************
SAMPLING/GRINDING OR CUTTING
WEIGH SAMPLE AND ADD EXTRACTION REAGENT
EXTRACT AT HOT PLATE BY APPROPRIATE TEMP.
MAKE UP WITH DEIONIZED WATERAND ADD DIPHENYL-CARBAZIDE SOLUTION
COOL AND FILTER THE EXTRACT
ANALYZED BY UV-VIS
NUMBER : TWNC00104294
TEST CONDUCTED
PAGE 7 OF 9
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() MEASUREMENT FLOWCHART:
TEST FOR PBBS/PBDES CONTENTSREFERENCE STANDARD: IEC 62321 (111/95/CDV)
******************************************************************************
SAMPLING/GRINDING OR CUTTING
WEIGH SAMPLE AND ADD ORGANIC SOLVENT
SOXHLET EXTRACTION OR SOLVENT EXTRACTION
CONCENTRATE THE EXTRACT AND MAKE UP WITH ORGANIC SOLVENT
ANALYZED BY GC-MSD
NUMBER : TWNC00104294
TEST CONDUCTED
PAGE 8 OF 9
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() MEASUREMENT FLOWCHART:
TEST FOR HALOGEN CONTENT REFERENCE STANDARDEN 14582
******************************************************************************END OF REPORT
ADD ABSORBENT IN A COMBUSTION FLASK & PLACE WEIGHED SAMPLE IN EQUIPMENT
FILL THE COMBUSTION FLASK WITH OXYGEN
IGNITE THEN LEAVE THE FLASK AT ROOM TEMPERATURE
TRANSFER THE ABSORBENT INTO A VOLUMETRIC FLASK
MAKE UP WITH DEIONIZED WATER
SAMPLING/GRINDING OR CUTTING
ANALYZED BY ION CHROMATOGRAPHY
NUMBER : TWNC00104294
TEST CONDUCTED
PAGE 9 OF 9
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PHOTO
Report No.: MX11-0928-08
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
RESULTS REPORT
INTERTEK TESTING SERVICES
DE MEXICO SA DE CV
LABORATORIO CD. DE MEXICO
DELIVER TO: Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila
ATTENTION: Ing. María Valdez
Report No.: MX11-0928-08
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
TEST REPORT
APPLICANT
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila
Ing. María Valdez
SAMPLE DESCRIPTION
One (1) group of submitted samples said to be :
Sample Description NP
Item No. 8) Cover Clear N/P 353.2140.1000
Country of Origin NP
Buyer's Name NP
Supplier's Name NP
Date sample received 2011-05-05
Testing period 2011-05-09 to 2011-05-18
********************************************************************************************
TEST CONDUCTED
As requested by the applicant, for details please refer to attached pages.
********************************************************************************************
CONCLUSION
Sample Number Testing item Conclusion Failed component Failed result
8 Cover Clear N/P 353.2140.1000 Pass
See Result summary --- ---
********************************************************************************************
TEST CONDUCTED
Report No.: MX11-0928-08
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
Samples:
8) Cover Clear N/P 353.2140.1000
TEST RESULT SUMMARY FOR RoHS DIRECTIVE :
TESTING ITEM Ω RESULT (ppm)
Limit (8)
Cadmium (Cd) content ND 0,01% (100 ppm)
Lead (Pb) content ND 0,1% (1000 ppm)
Mercury (Hg) content ND 0,1% (1000 ppm)
Chromium (VI) (Cr6+
) ND 0,1% (1000 ppm)
POLYBROMINATED BIPHENYLS (PBBs) Total ND 0,1% (1000 ppm)
Monobromobiphenyl (MonoBB) ND ---
Dibromobiphenyl (DiBB) ND ---
Tribromobiphenyl (TriBB) ND ---
Tetrabromobiphenyl (TetraBB) ND ---
Pentabromobiphenyl (PentaBB) ND ---
Hexabromobiphenyl (HexaBB) ND ---
Heptabromobiphenyl (HeptaBB) ND ---
Octabromobiphenyl (OctaBB) ND ---
Nonabromobiphenyl (NonaBB) ND ---
Decabromobiphenyl (DecaBB) ND ---
POLYBROMINATED DIPHENYL ETHERS (PBDEs) Total ND 0,1% (1000 ppm)
Monobromodiphenyl (MonoBDE) ND ---
Dibromodiphenyl (DiBDE) ND ---
Tribromodiphenyl (TriBDE) ND ---
Tetrabromodiphenyl (TetraBDE) ND ---
Pentabromodiphenyl (PentaBDE) ND ---
Hexabromodiphenyl (HexaBDE) ND ---
Heptabromodiphenyl (HeptaBDE) ND ---
Octabromodiphenyl (OctaBDE) ND ---
Nonabromodiphenyl (NonaBDE) ND ---
Decabromodiphenyl (DecaBDE) ND ---
Report No.: MX11-0928-08
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
|ppm = parts per million based on dry weight of sample.
µg/cm2 = microgram per square centimeter.
mg/kg WITH 50cm2 = milligram per kilogram with 50 square centimeter.
< = less than.
ND = Not detected.
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω.
Prepared and checked by:
For Intertek Laboratory Manager
The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,).
NOTE :DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMENDMENT 2005/717/EC.
# =ACCORDING TO IEC 62321, A POSITIVE RESULT INDICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION AND SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX11-0928-08 WERE TESTED TOGETHER.
Test method:
Report No.: MX11-0928-08
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
8 Chromium VI (Cr
6+)
content With reference to USEPA 3060, by EPA 7196
QHU2010-61p73 2011-05-13 MELA 20,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
8
POLYBROMINATE
D BIPHENYLS
(PBBs)
Determined by GC-MSD 2011-000274-PCL 2011-05-18
CONT 50,0
8
POLYBROMINATED DIPHENYL ETHERS (PBDEs)
Determined by GC-MSD 2011-000274-PCL 2011-05-18
CONT 50,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
8 Lead (Pb) content With reference to USEPA 3052, by EPA 6010 MET2010-40p128 2011-05-11 MARY 5,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
8 Cadmium (Cd) content With reference to USEPA 3052, by EPA 6010 MET2010-40p128 2011-05-11 MARY 2,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
8 Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p125 2010-05-10 RNC 0,25
Report No.: MX11-0928-01
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
RESULTS REPORT
INTERTEK TESTING SERVICES
DE MEXICO SA DE CV
LABORATORIO CD. DE MEXICO
DELIVER TO: Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila
ATTENTION: Ing. María Valdez
Report No.: MX11-0928-01
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
TEST REPORT
APPLICANT
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila
Ing. María Valdez
SAMPLE DESCRIPTION
One (1) group of submitted samples said to be :
Sample Description NP
Item No. 1) Colorant yellow N/P 325.7695.0110
Country of Origin NP
Buyer's Name NP
Supplier's Name NP
Date sample received 2011-05-05
Testing period 2011-05-09 to 2011-05-18
********************************************************************************************
TEST CONDUCTED
As requested by the applicant, for details please refer to attached pages.
********************************************************************************************
CONCLUSION
Sample Number Testing item Conclusion Failed component Failed result
1 Colorant yellow N/P
325.7695.0110
Pass
See Result summary --- ---
********************************************************************************************
TEST CONDUCTED
Report No.: MX11-0928-01
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
Samples:
1) Colorant yellow N/P 325.7695.0110
TEST RESULT SUMMARY FOR RoHS DIRECTIVE :
TESTING ITEM Ω RESULT (ppm)
Limit (1)
Cadmium (Cd) content ND 0,01% (100 ppm)
Lead (Pb) content 12,76 0,1% (1000 ppm)
Mercury (Hg) content ND 0,1% (1000 ppm)
Chromium (VI) (Cr6+
) ND 0,1% (1000 ppm)
POLYBROMINATED BIPHENYLS (PBBs) Total ND 0,1% (1000 ppm)
Monobromobiphenyl (MonoBB) ND ---
Dibromobiphenyl (DiBB) ND ---
Tribromobiphenyl (TriBB) ND ---
Tetrabromobiphenyl (TetraBB) ND ---
Pentabromobiphenyl (PentaBB) ND ---
Hexabromobiphenyl (HexaBB) ND ---
Heptabromobiphenyl (HeptaBB) ND ---
Octabromobiphenyl (OctaBB) ND ---
Nonabromobiphenyl (NonaBB) ND ---
Decabromobiphenyl (DecaBB) ND ---
POLYBROMINATED DIPHENYL ETHERS (PBDEs) Total ND 0,1% (1000 ppm)
Monobromodiphenyl (MonoBDE) ND ---
Dibromodiphenyl (DiBDE) ND ---
Tribromodiphenyl (TriBDE) ND ---
Tetrabromodiphenyl (TetraBDE) ND ---
Pentabromodiphenyl (PentaBDE) ND ---
Hexabromodiphenyl (HexaBDE) ND ---
Heptabromodiphenyl (HeptaBDE) ND ---
Octabromodiphenyl (OctaBDE) ND ---
Nonabromodiphenyl (NonaBDE) ND ---
Decabromodiphenyl (DecaBDE) ND ---
Report No.: MX11-0928-01
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
|ppm = parts per million based on dry weight of sample.
µg/cm2 = microgram per square centimeter.
mg/kg WITH 50cm2 = milligram per kilogram with 50 square centimeter.
< = less than.
ND = Not detected.
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω.
Prepared and checked by:
For Intertek Laboratory Manager
The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,).
NOTE :DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMENDMENT 2005/717/EC.
# =ACCORDING TO IEC 62321, A POSITIVE RESULT INDICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION AND SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX11-0928-01 WERE TESTED TOGETHER.
Test method:
Report No.: MX11-0928-01
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
1 Chromium VI (Cr
6+)
content With reference to USEPA 3060, by EPA 7196
QHU2010-61p73 2011-05-13 MELA 20,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
1
POLYBROMINATE
D BIPHENYLS
(PBBs)
Determined by GC-MSD 2011-000274-PCL 2011-05-18
CONT 50,0
1
POLYBROMINATED DIPHENYL ETHERS (PBDEs)
Determined by GC-MSD 2011-000274-PCL 2011-05-18
CONT 50,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
1 Lead (Pb) content With reference to USEPA 3052, by EPA 6010 MET2010-40p128 2011-05-11 MARY 5,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
1 Cadmium (Cd) content With reference to USEPA 3052, by EPA 6010 MET2010-40p128 2011-05-11 MARY 2,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
1 Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p125 2010-05-10 RNC 0,25
TEST REPORT NUMBER : TWNC00104893
AUTHORIZED BY: ON BEHALF OF INTERTEK TESTING SERVICES TAIWAN LIMITED
K. Y. LIANG DIRECTOR
THIS REPORT SHALL NOT BE REPRODUCED EXCEPT IN FULL, WITHOUT THE WRITTEN APPROVAL OF THE LABORATORY.
PAGE 1 OF 9
!"#$%&$$'%()(%* +!"#$%&$$'%''$$'%'
APPLICANT: LITTELFUSE, INC. DATE : JAN 22, 2009 800 E. NORTHWEST HWY
DESPLAINES IL 60016
SAMPLE DESCRIPTION: ONE (1) GROUP OF SUBMITTED SAMPLES SAID TO BE : PART DESCRIPTION : BODY 60A YELLOW PART NUMBER : 353.2131.4600 FACILITY NAME : DUNSEN DATE SAMPLE RECEIVED : JAN 19, 2009 DATE TEST STARTED : JAN 19, 2009 ***************************************************************************
TEST CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS PLEASE REFER TO ATTACHED PAGES. ***************************************************************************
NUMBER : TWNC00104893
TEST CONDUCTED
PAGE 2 OF 9
!"#$%&$$'%()(%* +!"#$%&$$'%''$$'%'
() TEST RESULT SUMMARY : RESULT (ppm)
TESTING ITEMYELLOW PLASTIC
HEAVY METALCADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT 18 MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND
POLYBROMINATED BIPHENYLS (PBBs)MONOBROMINATED BIPHENYLS (MONOBB) ND DIBROMINATED BIPHENYLS (DIBB) ND TRIBROMINATED BIPHENYLS (TRIBB) ND TETRABROMINATED BIPHENYLS (TETRABB) ND PENTABROMINATED BIPHENYLS (PENTABB) ND HEXABROMINATED BIPHENYLS (HEXABB) ND HEPTABROMINATED BIPHENYLS (HEPTABB) ND OCTABROMINATED BIPHENYLS (OCTABB) ND NONABROMINATED BIPHENYLS (NONABB) ND DECABROMINATED BIPHENYL (DECABB) ND
POLYBROMINATED DIPHENYL ETHERS (PBDEs)MONOBROMINATED DIPHENYL ETHERS (MONOBDE) ND DIBROMINATED DIPHENYL ETHERS (DIBDE) ND TRIBROMINATED DIPHENYL ETHERS (TRIBDE) ND TETRABROMINATED DIPHENYL ETHERS (TETRABDE) ND PENTABROMINATED DIPHENYL ETHERS (PENTABDE) ND HEXABROMINATED DIPHENYL ETHERS (HEXABDE) ND HEPTABROMINATED DIPHENYL ETHERS (HEPTABDE) ND OCTABROMINATED DIPHENYL ETHERS (OCTABDE) ND NONABROMINATED DIPHENYL ETHERS (NONABDE) ND DECABROMINATED DIPHENYL ETHER (DECABDE) ND
HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) ND BROMINE (Br) 68298 IODINE (I) ND
REMARKS : ppm = PARTS PER MILLION BASED ON WEIGHT OF TESTED SAMPLE ND = NOT DETECTED
RESPONSIBILITY OF CHEMIST: IRENE CHIOU / KEVIN LIU / CATHY CHEN
DATE SAMPLE RECEIVED : JAN 19, 2009 TESTING PERIOD : JAN 19, 2009 TO JAN 21, 2009
******************************************************************************
NUMBER : TWNC00104893
TEST CONDUCTED
PAGE 3 OF 9
!"#$%&$$'%()(%* +!"#$%&$$'%''$$'%'
() ROHS REQUIREMENT : RESTRICTED SUSTANCES LIMITS
CADMIUM (Cd) 0.01% (100ppm)LEAD (Pb) 0.1% (1000ppm)MERCURY (Hg) 0.1% (1000ppm)CHROMIUM (VI)(Cr6+) 0.1% (1000ppm)POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm)POLYBROMINATED DIPHENYL EHTERS (PBDEs) 0.1% (1000ppm)
() TEST METHOD : TESTING ITEM TESTING METHOD REPORTING LIMIT
CADMIUM (Cd) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
LEAD (Pb) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
MERCURY (Hg) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
CHROMIUM VI (Cr6+)CONTENT
WITH REFERENCE TO USEPA 3060A & 7196A, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER
1 ppm
POLYBROMINATEDBIPHENYLS (PBBs)
WITH REFERENCE TO IEC 62321-111/95/CDV IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY
5 ppm
******************************************************************************
NUMBER : TWNC00104893
TEST CONDUCTED
PAGE 4 OF 9
!"#$%&$$'%()(%* +!"#$%&$$'%''$$'%'
() TEST METHOD : TESTING ITEM TESTING METHOD REPORTING LIMIT
POLYBROMINATEDDIPHENYL ETHERS (PBDEs)
WITH REFERENCE TO IEC 62321-111/95/CDV IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY
5 ppm
HALOGEN CONTENTWITH REFERENCE TO EN 14582:2007 BY COMBUSTION FLASK WITH OXYGEN AND DETERMINED BY ION CHROMATOGRAPHY
50 ppm
REMARKS : REPORTING LIMIT = QUANTITATION LIMIT OF ANALYTE IN SAMPLE TESTS WERE CONDUCTED WITH REFERENCE TO 111/95/CDV VERSION 2007-
10-12 WHICH IS STILL A DRAFT METHOD AND SUBJECT TO FUTURE CHANGES PRIOR TO PUBLICATION.
******************************************************************************
NUMBER : TWNC00104893
TEST CONDUCTED
PAGE 5 OF 9
!"#$%&$$'%()(%* +!"#$%&$$'%''$$'%'
() MEASUREMENT FLOWCHART:
TEST FOR Cd/Pb/Hg CONTENTSREFERENCE STANDARD: IEC 62321 (111/95/CDV)
REMARKS:*1: LIST OF APPROPRIATE ACID
MATERIAL ACID ADDED FOR DIGESTION
POLYMERS HNO3,HCl,HF,H2O2,H3BO3METALS HNO3,HCl,HFELECTRONICS HNO3,HCl,H2O2,HBF4
******************************************************************************
SAMPLING/GRINDING OR CUTTING
FOR DIFFERENT MATERIAL, DIGEST THE SAMPLE WITH APPROPRIATE ACID*1
MAKE UP WITH DEIONIZED WATER
ANALYZED BY ICP-OES
CONFIRM THE TESTED SAMPLES ARE TOTALLY DISSOLVED
NUMBER : TWNC00104893
TEST CONDUCTED
PAGE 6 OF 9
!"#$%&$$'%()(%* +!"#$%&$$'%''$$'%'
() MEASUREMENT FLOWCHART:
TEST FOR CHROMIUM (VI) CONTENTREFERENCE STANDARDUSEPA 3060A/7196A
******************************************************************************
SAMPLING/GRINDING OR CUTTING
WEIGH SAMPLE AND ADD EXTRACTION REAGENT
EXTRACT AT HOT PLATE BY APPROPRIATE TEMP.
MAKE UP WITH DEIONIZED WATERAND ADD DIPHENYL-CARBAZIDE SOLUTION
COOL AND FILTER THE EXTRACT
ANALYZED BY UV-VIS
NUMBER : TWNC00104893
TEST CONDUCTED
PAGE 7 OF 9
!"#$%&$$'%()(%* +!"#$%&$$'%''$$'%'
() MEASUREMENT FLOWCHART:
TEST FOR PBBS/PBDES CONTENTSREFERENCE STANDARD: IEC 62321 (111/95/CDV)
******************************************************************************
SAMPLING/GRINDING OR CUTTING
WEIGH SAMPLE AND ADD ORGANIC SOLVENT
SOXHLET EXTRACTION OR SOLVENT EXTRACTION
CONCENTRATE THE EXTRACT AND MAKE UP WITH ORGANIC SOLVENT
ANALYZED BY GC-MSD
NUMBER : TWNC00104893
TEST CONDUCTED
PAGE 8 OF 9
!"#$%&$$'%()(%* +!"#$%&$$'%''$$'%'
() MEASUREMENT FLOWCHART:
TEST FOR HALOGEN CONTENT REFERENCE STANDARDEN 14582
******************************************************************************END OF REPORT
ADD ABSORBENT IN A COMBUSTION FLASK & PLACE WEIGHED SAMPLE IN EQUIPMENT
FILL THE COMBUSTION FLASK WITH OXYGEN
IGNITE THEN LEAVE THE FLASK AT ROOM TEMPERATURE
TRANSFER THE ABSORBENT INTO A VOLUMETRIC FLASK
MAKE UP WITH DEIONIZED WATER
SAMPLING/GRINDING OR CUTTING
ANALYZED BY ION CHROMATOGRAPHY
NUMBER : TWNC00104893
TEST CONDUCTED
PAGE 9 OF 9
!"#$%&$$'%()(%* +!"#$%&$$'%''$$'%'
PHOTO
Report No.: MX11-0928-03
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
RESULTS REPORT
INTERTEK TESTING SERVICES
DE MEXICO SA DE CV
LABORATORIO CD. DE MEXICO
DELIVER TO: Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila
ATTENTION: Ing. María Valdez
Report No.: MX11-0928-03
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
TEST REPORT
APPLICANT
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila
Ing. María Valdez
SAMPLE DESCRIPTION
One (1) group of submitted samples said to be :
Sample Description NP
Item No. 3) Element Sn Plated Copper N/P 353.1119.4043
Country of Origin NP
Buyer's Name NP
Supplier's Name NP
Date sample received 2011-05-05
Testing period 2011-05-09 to 2011-05-13
********************************************************************************************
TEST CONDUCTED
As requested by the applicant, for details please refer to attached pages.
********************************************************************************************
CONCLUSION
Sample Number Testing item Conclusion Failed component Failed result
3
(Base)
Element Sn Plated Copper N/P 353.1119.4043
Pass
See Result summary --- ---
3
(Plated)
Element Sn Plated Copper N/P 353.1119.4043
Pass
See Result summary --- ---
********************************************************************************************
TEST CONDUCTED
Samples:
Report No.: MX11-0928-03
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
3) Base Element Sn Plated Copper N/P 353.1119.4043
3) Plated Element Sn Plated Copper N/P 353.1119.4043
TEST RESULT SUMMARY FOR RoHS DIRECTIVE :
TESTING ITEM
Ω RESULT (ppm) Limit (3)
Base
(3)
Plated
Cadmium (Cd) content ND ND 0,01% (100 ppm)
Lead (Pb) content 36,10 148,1 0,1% (1000 ppm)
Mercury (Hg) content ND ND 0,1% (1000 ppm)
Chromium (VI) (Cr6+
) ND ND 0,1% (1000 ppm)
ppm = parts per million based on dry weight of sample.
µg/cm2 = microgram per square centimeter.
mg/kg WITH 50cm2 = milligram per kilogram with 50 square centimeter.
< = less than.
ND = Not detected.
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω.
Prepared and checked by:
For Intertek Laboratory Manager
The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,).
NOTE : DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMENDMENT 2005/717/EC.
# =ACCORDING TO IEC 62321, A POSITIVE RESULT INDICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION AND SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX11-0928-03 WERE TESTED SEPARATED.
Test method:
Report No.: MX11-0928-03
Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s).
The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150
www.intertek.com
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
3 Chromium VI (Cr
6+)
content With reference to USEPA 3060, by EPA 7196
QHU2010-61p73 2011-05-13 MELA 20,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
3 (Base) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 5,0
3 (Plated) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 50,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
3 (Base) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 2,0
3 (Plated) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 20,0
Sample Number
Testing item Ω Testing method Quality control
Batch: Analysis
Date:
Analyzed
By:
Reporting limit ppm
3 (Base) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 0,25
3 (Plated) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 2,5
TEST REPORT NUMBER : TWNC00104895
AUTHORIZED BY: ON BEHALF OF INTERTEK TESTING SERVICES TAIWAN LIMITED
K. Y. LIANG DIRECTOR
THIS REPORT SHALL NOT BE REPRODUCED EXCEPT IN FULL, WITHOUT THE WRITTEN APPROVAL OF THE LABORATORY.
PAGE 1 OF 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
APPLICANT: LITTELFUSE, INC. DATE : JAN 21, 2009 800 E. NORTHWEST HWY
DESPLAINES IL 60016
SAMPLE DESCRIPTION:
ONE (1) GROUP OF SUBMITTED SAMPLES SAID TO BE : PART DESCRIPTION : BODY 80A NATURAL PART NUMBER : 353.2131.4800 FACILITY NAME : DUNSEN DATE SAMPLE RECEIVED : JAN 19, 2009 DATE TEST STARTED : JAN 19, 2009 ***************************************************************************
TEST CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS PLEASE REFER TO ATTACHED PAGES. ***************************************************************************
NUMBER : TWNC00104895 TEST CONDUCTED
PAGE 2 OF 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) TEST RESULT SUMMARY : RESULT (ppm)
TESTING ITEM OFF-WHITE PLASTIC
HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT 26 MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND
POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MONOBB) ND DIBROMINATED BIPHENYLS (DIBB) ND TRIBROMINATED BIPHENYLS (TRIBB) ND TETRABROMINATED BIPHENYLS (TETRABB) ND PENTABROMINATED BIPHENYLS (PENTABB) ND HEXABROMINATED BIPHENYLS (HEXABB) ND HEPTABROMINATED BIPHENYLS (HEPTABB) ND OCTABROMINATED BIPHENYLS (OCTABB) ND NONABROMINATED BIPHENYLS (NONABB) ND DECABROMINATED BIPHENYL (DECABB) ND
POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MONOBDE) ND DIBROMINATED DIPHENYL ETHERS (DIBDE) ND TRIBROMINATED DIPHENYL ETHERS (TRIBDE) ND TETRABROMINATED DIPHENYL ETHERS (TETRABDE) ND PENTABROMINATED DIPHENYL ETHERS (PENTABDE) ND HEXABROMINATED DIPHENYL ETHERS (HEXABDE) ND HEPTABROMINATED DIPHENYL ETHERS (HEPTABDE) ND OCTABROMINATED DIPHENYL ETHERS (OCTABDE) ND NONABROMINATED DIPHENYL ETHERS (NONABDE) ND DECABROMINATED DIPHENYL ETHER (DECABDE) ND
HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) ND BROMINE (Br) 62313 IODINE (I) ND
REMARKS : ppm = PARTS PER MILLION BASED ON WEIGHT OF TESTED SAMPLE ND = NOT DETECTED RESPONSIBILITY OF CHEMIST: IRENE CHIOU / KEVIN LIU / CATHY CHEN
DATE SAMPLE RECEIVED : JAN 19, 2009 TESTING PERIOD : JAN 19, 2009 TO JAN 21, 2009
******************************************************************************
NUMBER : TWNC00104895 TEST CONDUCTED
PAGE 3 OF 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅱ) ROHS REQUIREMENT : RESTRICTED SUSTANCES LIMITS
CADMIUM (Cd) 0.01% (100ppm)LEAD (Pb) 0.1% (1000ppm)MERCURY (Hg) 0.1% (1000ppm)CHROMIUM (VI)(Cr6+) 0.1% (1000ppm)POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm)POLYBROMINATED DIPHENYL EHTERS (PBDEs) 0.1% (1000ppm)
(Ⅲ) TEST METHOD :
TESTING ITEM TESTING METHOD REPORTING LIMIT
CADMIUM (Cd) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
LEAD (Pb) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
MERCURY (Hg) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
CHROMIUM VI (Cr6+) CONTENT
WITH REFERENCE TO USEPA 3060A & 7196A, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER
1 ppm
POLYBROMINATED BIPHENYLS (PBBs)
WITH REFERENCE TO IEC 62321-111/95/CDV IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY
5 ppm
******************************************************************************
NUMBER : TWNC00104895 TEST CONDUCTED
PAGE 4 OF 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) TEST METHOD : TESTING ITEM TESTING METHOD REPORTING LIMIT
POLYBROMINATED DIPHENYL ETHERS (PBDEs)
WITH REFERENCE TO IEC 62321-111/95/CDV IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY
5 ppm
HALOGEN CONTENT WITH REFERENCE TO EN 14582:2007 BY COMBUSTION FLASK WITH OXYGEN AND DETERMINED BY ION CHROMATOGRAPHY
50 ppm
REMARKS : REPORTING LIMIT = QUANTITATION LIMIT OF ANALYTE IN SAMPLE TESTS WERE CONDUCTED WITH REFERENCE TO 111/95/CDV VERSION 2007-
10-12 WHICH IS STILL A DRAFT METHOD AND SUBJECT TO FUTURE CHANGES PRIOR TO PUBLICATION.
******************************************************************************
NUMBER : TWNC00104895 TEST CONDUCTED
PAGE 5 OF 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) MEASUREMENT FLOWCHART:
TEST FOR Cd/Pb/Hg CONTENTS REFERENCE STANDARD: IEC 62321 (111/95/CDV)
REMARKS: *1: LIST OF APPROPRIATE ACID:
MATERIAL ACID ADDED FOR DIGESTION
POLYMERS HNO3,HCl,HF,H2O2,H3BO3 METALS HNO3,HCl,HF ELECTRONICS HNO3,HCl,H2O2,HBF4
******************************************************************************
SAMPLING/GRINDING OR CUTTING
FOR DIFFERENT MATERIAL, DIGEST THE SAMPLE WITH APPROPRIATE ACID*1
MAKE UP WITH DEIONIZED WATER
ANALYZED BY ICP-OES
CONFIRM THE TESTED SAMPLES ARE TOTALLY DISSOLVED
NUMBER : TWNC00104895 TEST CONDUCTED
PAGE 6 OF 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) MEASUREMENT FLOWCHART:
TEST FOR CHROMIUM (VI) CONTENT REFERENCE STANDARD:USEPA 3060A/7196A
******************************************************************************
SAMPLING/GRINDING OR CUTTING
WEIGH SAMPLE AND ADD EXTRACTION REAGENT
EXTRACT AT HOT PLATE BY APPROPRIATE TEMP.
MAKE UP WITH DEIONIZED WATERAND ADD DIPHENYL-CARBAZIDE SOLUTION
COOL AND FILTER THE EXTRACT
ANALYZED BY UV-VIS
NUMBER : TWNC00104895 TEST CONDUCTED
PAGE 7 OF 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) MEASUREMENT FLOWCHART:
TEST FOR PBBS/PBDES CONTENTS REFERENCE STANDARD: IEC 62321 (111/95/CDV)
******************************************************************************
SAMPLING/GRINDING OR CUTTING
WEIGH SAMPLE AND ADD ORGANIC SOLVENT
SOXHLET EXTRACTION OR SOLVENT EXTRACTION
CONCENTRATE THE EXTRACT AND MAKE UP WITH ORGANIC SOLVENT
ANALYZED BY GC-MSD
NUMBER : TWNC00104895 TEST CONDUCTED
PAGE 8 OF 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) MEASUREMENT FLOWCHART:
TEST FOR HALOGEN CONTENT REFERENCE STANDARD:EN 14582
******************************************************************************
END OF REPORT
ADD ABSORBENT IN A COMBUSTION FLASK & PLACE WEIGHED SAMPLE IN EQUIPMENT
FILL THE COMBUSTION FLASK WITH OXYGEN
IGNITE THEN LEAVE THE FLASK AT ROOM TEMPERATURE
TRANSFER THE ABSORBENT INTO A VOLUMETRIC FLASK
MAKE UP WITH DEIONIZED WATER
SAMPLING/GRINDING OR CUTTING
ANALYZED BY ION CHROMATOGRAPHY
NUMBER : TWNC00104895 TEST CONDUCTED
PAGE 9 OF 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
PHOTO
TEST REPORT NUMBER : TWNC00104303
AUTHORIZED BY: ON BEHALF OF INTERTEK TESTING SERVICES TAIWAN LIMITED
K. Y. LIANG DIRECTOR
THIS REPORT SHALL NOT BE REPRODUCED EXCEPT IN FULL, WITHOUT THE WRITTEN APPROVAL OF THE LABORATORY.
PAGE 1 OF 9
Intertek Testing Services Taiwan Ltd. 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888 2797-8885 Fax: (+886-2) 6602-2410
APPLICANT: LITTELFUSE, INC. DATE : JAN 19, 2009 800 E. NORTHWEST HWY
DESPLAINES IL 60016
SAMPLE DESCRIPTION:
ONE (1) GROUP OF SUBMITTED SAMPLES SAID TO BE : PART DESCRIPTION : COLORANT WIHTE PART NUMBER : 325.7692.0000 FACILITY : DUNSEN DATE SAMPLE RECEIVED : JAN 14, 2009 DATE TEST STARTED : JAN 14, 2009 ***************************************************************************
TEST CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS PLEASE REFER TO ATTACHED PAGES. ***************************************************************************
NUMBER : TWNC00104303 TEST CONDUCTED
PAGE 2 OF 9
Intertek Testing Services Taiwan Ltd. 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888 2797-8885 Fax: (+886-2) 6602-2410
(Ⅰ) TEST RESULT SUMMARY : RESULT (ppm)
TESTING ITEM WHITE PLASTIC BEAN
HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND
POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MONOBB) ND DIBROMINATED BIPHENYLS (DIBB) ND TRIBROMINATED BIPHENYLS (TRIBB) ND TETRABROMINATED BIPHENYLS (TETRABB) ND PENTABROMINATED BIPHENYLS (PENTABB) ND HEXABROMINATED BIPHENYLS (HEXABB) ND HEPTABROMINATED BIPHENYLS (HEPTABB) ND OCTABROMINATED BIPHENYLS (OCTABB) ND NONABROMINATED BIPHENYLS (NONABB) ND DECABROMINATED BIPHENYL (DECABB) ND
POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MONOBDE) ND DIBROMINATED DIPHENYL ETHERS (DIBDE) ND TRIBROMINATED DIPHENYL ETHERS (TRIBDE) ND TETRABROMINATED DIPHENYL ETHERS (TETRABDE) ND PENTABROMINATED DIPHENYL ETHERS (PENTABDE) ND HEXABROMINATED DIPHENYL ETHERS (HEXABDE) ND HEPTABROMINATED DIPHENYL ETHERS (HEPTABDE) ND OCTABROMINATED DIPHENYL ETHERS (OCTABDE) ND NONABROMINATED DIPHENYL ETHERS (NONABDE) ND DECABROMINATED DIPHENYL ETHER (DECABDE) ND
HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) ND BROMINE (Br) ND IODINE (I) ND
REMARKS : ppm = PARTS PER MILLION BASED ON WEIGHT OF TESTED SAMPLE ND = NOT DETECTED RESPONSIBILITY OF CHEMIST: IRENE CHIOU / KEVIN LIU / CATHY CHEN
DATE SAMPLE RECEIVED : JAN 14, 2009 TESTING PERIOD : JAN 14, 2009 TO JAN 17, 2009
******************************************************************************
NUMBER : TWNC00104303 TEST CONDUCTED
PAGE 3 OF 9
Intertek Testing Services Taiwan Ltd. 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888 2797-8885 Fax: (+886-2) 6602-2410
(Ⅱ) ROHS REQUIREMENT : RESTRICTED SUSTANCES LIMITS
CADMIUM (Cd) 0.01% (100ppm)LEAD (Pb) 0.1% (1000ppm)MERCURY (Hg) 0.1% (1000ppm)CHROMIUM (VI)(Cr6+) 0.1% (1000ppm)POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm)POLYBROMINATED DIPHENYL EHTERS (PBDEs) 0.1% (1000ppm)
(Ⅲ) TEST METHOD :
TESTING ITEM TESTING METHOD REPORTING LIMIT
CADMIUM (Cd) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
LEAD (Pb) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
MERCURY (Hg) CONTENT
WITH REFERENCE TO IEC 62321-111/95/CDV IN CLAUES 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES
2 ppm
CHROMIUM VI (Cr6+) CONTENT
WITH REFERENCE TO USEPA 3060A & 7196A, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER
1 ppm
POLYBROMINATED BIPHENYLS (PBBs)
WITH REFERENCE TO IEC 62321-111/95/CDV IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY
5 ppm
******************************************************************************
NUMBER : TWNC00104303 TEST CONDUCTED
PAGE 4 OF 9
Intertek Testing Services Taiwan Ltd. 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888 2797-8885 Fax: (+886-2) 6602-2410
(Ⅲ) TEST METHOD : TESTING ITEM TESTING METHOD REPORTING LIMIT
POLYBROMINATED DIPHENYL ETHERS (PBDEs)
WITH REFERENCE TO IEC 62321-111/95/CDV IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY
5 ppm
HALOGEN CONTENT WITH REFERENCE TO EN 14582:2007 BY COMBUSTION FLASK WITH OXYGEN AND DETERMINED BY ION CHROMATOGRAPHY
50 ppm
REMARKS : REPORTING LIMIT = QUANTITATION LIMIT OF ANALYTE IN SAMPLE TESTS WERE CONDUCTED WITH REFERENCE TO 111/95/CDV VERSION 2007-
10-12 WHICH IS STILL A DRAFT METHOD AND SUBJECT TO FUTURE CHANGES PRIOR TO PUBLICATION.
******************************************************************************
NUMBER : TWNC00104303 TEST CONDUCTED
PAGE 5 OF 9
Intertek Testing Services Taiwan Ltd. 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888 2797-8885 Fax: (+886-2) 6602-2410
(Ⅳ) MEASUREMENT FLOWCHART:
TEST FOR Cd/Pb/Hg CONTENTS REFERENCE STANDARD: IEC 62321 (111/95/CDV)
REMARKS: *1: LIST OF APPROPRIATE ACID:
MATERIAL ACID ADDED FOR DIGESTION
POLYMERS HNO3,HCl,HF,H2O2,H3BO3 METALS HNO3,HCl,HF ELECTRONICS HNO3,HCl,H2O2,HBF4
******************************************************************************
SAMPLING/GRINDING OR CUTTING
FOR DIFFERENT MATERIAL, DIGEST THE SAMPLE WITH APPROPRIATE ACID*1
MAKE UP WITH DEIONIZED WATER
ANALYZED BY ICP-OES
CONFIRM THE TESTED SAMPLES ARE TOTALLY DISSOLVED
NUMBER : TWNC00104303 TEST CONDUCTED
PAGE 6 OF 9
Intertek Testing Services Taiwan Ltd. 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888 2797-8885 Fax: (+886-2) 6602-2410
(Ⅳ) MEASUREMENT FLOWCHART:
TEST FOR CHROMIUM (VI) CONTENT REFERENCE STANDARD:USEPA 3060A/7196A
******************************************************************************
SAMPLING/GRINDING OR CUTTING
WEIGH SAMPLE AND ADD EXTRACTION REAGENT
EXTRACT AT HOT PLATE BY APPROPRIATE TEMP.
MAKE UP WITH DEIONIZED WATERAND ADD DIPHENYL-CARBAZIDE SOLUTION
COOL AND FILTER THE EXTRACT
ANALYZED BY UV-VIS
NUMBER : TWNC00104303 TEST CONDUCTED
PAGE 7 OF 9
Intertek Testing Services Taiwan Ltd. 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888 2797-8885 Fax: (+886-2) 6602-2410
(Ⅳ) MEASUREMENT FLOWCHART:
TEST FOR PBBS/PBDES CONTENTS REFERENCE STANDARD: IEC 62321 (111/95/CDV)
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SAMPLING/GRINDING OR CUTTING
WEIGH SAMPLE AND ADD ORGANIC SOLVENT
SOXHLET EXTRACTION OR SOLVENT EXTRACTION
CONCENTRATE THE EXTRACT AND MAKE UP WITH ORGANIC SOLVENT
ANALYZED BY GC-MSD
NUMBER : TWNC00104303 TEST CONDUCTED
PAGE 8 OF 9
Intertek Testing Services Taiwan Ltd. 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888 2797-8885 Fax: (+886-2) 6602-2410
(Ⅳ) MEASUREMENT FLOWCHART:
TEST FOR HALOGEN CONTENT REFERENCE STANDARD:EN 14582
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END OF REPORT
ADD ABSORBENT IN A COMBUSTION FLASK & PLACE WEIGHED SAMPLE IN EQUIPMENT
FILL THE COMBUSTION FLASK WITH OXYGEN
IGNITE THEN LEAVE THE FLASK AT ROOM TEMPERATURE
TRANSFER THE ABSORBENT INTO A VOLUMETRIC FLASK
MAKE UP WITH DEIONIZED WATER
SAMPLING/GRINDING OR CUTTING
ANALYZED BY ION CHROMATOGRAPHY
NUMBER : TWNC00104303 TEST CONDUCTED
PAGE 9 OF 9
Intertek Testing Services Taiwan Ltd. 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888 2797-8885 Fax: (+886-2) 6602-2410
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