1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: Surface Mount Diode Array Product #: SP0503BAHTG (SOT-143 package) Issue Date: June 06, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Specialist>

(1) Parts, sub-materials and unit parts This document covers the Surface Mount Diode Array RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：.

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 NA Leadframe (A194 Alloy) 3-11 2 EMEG600 Epoxy Molding Compound 12-26 3 N/A 99.9% Tin Plating 27-33 4 N/A Gold (Au) Wire 34-42 5 84-1 LM1SR4 Adhesive 43-76 6 N/A IC Wafer 77-83

Test ReportHENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS92606 U.S.A.

SignatureFor Qu€Please with SGS

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No. : CEl201284041 Dale:2012lOBl3OP a g e : 1 o f 3 0

l:lllllt|rmtl|llMAIN OFFICE: 14OOO JAMBOREE ROAD, IRVINE' CALIFORNIA'

The followlng sample(3) wasrwere submitt€d and identified by/on behall ofthe cliont as:

Sampl6 De.criPtionStyle/ltem No.Sample Receiving DateTesting Period

ADHESIVE84-l LMtSR42c1A0812420121 08 t24 1 0 201 Z 081 30

T€6t R€6ult(e) : Please refer to next Page(s)

Cf-ttlc.l t|bottnlrt * TdPd

ffiffi

Test Report No. : CEI2O12J84O41 Date : 201208/30 Page : 2 of 30

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Teet R6ultlsl

PART NAIVIE No.l

lllllllllltlflflll14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA'

: SILVER COLORED PASTE

T€6t ltem(8) Unit il6lhod MOLRa6ultN o . l

Cadmium (Cd) mS/kS W;ifrEren-ce to IEC 62321 : 2oo8 andperfomed by ICP-AES.

2 n.d.

Lead (Pb) mg/Kg With referenc€ to IEC 6232 1 : 2008 andperfomed by ICP4ES

2 n.d.

Mercury Fg) mg/Kg Wth refeienc€ to IEC 62321: 2008 andperform€d bY |CP4ES.

2 n.d.

Hexavalent Chromium Cr(Vl) mg,/Kg WlifrErence to lEc 62321: 2oo8 andperformed by uv-Vls.

n.d.

Beryllium (Be) mgKg With r€ference to US EPA Method30508 for Beryllium Codent Analysiswas p€rfomed by ICP-AES

2 n.d.

Antimony (Sb) mg/kg Wittl reference to us EPA Method3052 for Antimony Contenl Analysiswas performed by ICP.AES.

2 n.d.

Bromochloromethane (CAS No :74-97-5)

figfr6-TWiGretere.nce to us EPA 5021lmethod. Analysis wa6 Perfomed bYlGc/lrs.

n.d.

mh refe.ence to US EPA 502'1nethod. Analysis was Perfofied bYGC/MS.

1 n.d.-uffur Hexafluodde (sFB) (CAsNo.:2551€2-4)

mg/Kl

Wiih reference to BS EN 1458212007.Analysis was Performed bY lC.

50 197Halogen-Chlorine (CD (CAS No :22537 -15-'l'l

mg/Kg

F;losen-Bromlne (Br) (cAs No :100€7-C-2)

mgKg WftfEference to Bs EN u5a2.2oo7Analysis \N€s performed bY lC

50 n.d.

'10 n_o.Pertluorooctane sulfonates{PFOS-Acid, Metal Salt, Amide)

mg/Kg With reference rc uu EPA Jccu\.:2007. Analysis was Perfomed bYLC/MS.Fiifarence to us EPA 355oci2007. Analysis was Perfom€d bYLC/MS.

' t0 n.d.PFoA (CAS No.: 335€7-1) mg/kg

n.d.2- (35ii-tert-butyF2-hydroryPhenyl)-2H+enzotiazole(CAS No.r 3846-71-7)

mgikS With rcforence to uu El'A rc4utmethod. Analysis wtss Performed bYGC/MS.

nffi':ffidu'*fmm.m-*Ti,.mffixW#romsi.,s*"te*mrffi"gl

.:;$ruil* rilHg*ffi {l*

I

SGSI

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS IIAIN OFFICE:92606 U.S.A.

Test Report No. : CE/201284041 Date : 20!2/08/30 Page : 3 of 30

Test ltom(s) unit Method r,DLResultNo.l

Polychlorinat€d Biphenyls (PCBS)(CAS No.: '133&36-3)

mg/Kg Wth reference to US EPA 3f,40cmethod. Analysis {ras performed byGC/MS.

n.d.

Polychlorinated Naphthalene(PCNs)

mg/kg r/vit-h reference to us EPA 3540cmethod. Analysis was Performed bYGC/MS.

5 n.d.

F6FychlorinatedTerphenyls(PcTs)

m9Kg With reference to US EPA 3540Cme4hod. Analysis was Performed bYGC/MS.

0.5 n.d.

with reference to us EPA 3540Cmethod. Analy6is was Performed bYGC/MS.

'100 n .d .nltanes, C10-13, chloo (ShortChain Chlorinated Paraffins) (CASNo.:85535-84-8)

mg/Kg

PVC Analysis was Pertormed bY FTIR andFLAITE Test.

Negative

Erornomahane (CAS No.: z+€3-e)

mgftg With reference to US EPA 5021method. Analysis was P€rforned bYGC/MS.

1 n.d.

HalonsFiton-tzr1 (CnS No.: :Sg+s-g) mg/Kg Wttr reference to Us EPn 502t

method. Analysis was Pedormed bYGC/MS.

n.d.

Halon-1301 (CAS No.: 7563-8) h!/l(gffi reference to us EPA 5021lmethod. Analysis was performed bylcc/t s.

I n.d.

Hal,cn-2402 (CAS No.: 124-73-2) mg/kg Fith reference to us EPA 5021method. Analysis was Perfomed bYGC/MS.

1 n,o.

0;qanic-{ln compounda0.03 n.d.

Tributyl Tin (TBT) mg/kg With reference to ulN J64u /_ rr'Analysis was performed bY GC/FPD

0.03 n.d.ariphenyl Tin (TPhT) m9Kg With €feren@ to lrlN 3!4ur-lr.

Analysis was Perfomed bY GC/FPD.n.d.

Ributytrin oxide (TBTo)"' (cAsNo.:56-35-9)

m9ftg with reference to ulN Jd'+rJ/_ rr'Analysis was Perfomed bY GC/FPD

ffifi

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I +e6@p,, nD !1!q!t!?43!9.:lI__,_l!!j!9:i1

Test Report No. : CE2Olz84O41 Oate : 2012/08/30 Page : 4 of 30

HENKEL CORPOMTIONHENKEL ADHESIVES-ELECTRONICS MAIN OFFICE:92606 U.S.A.

llllllllllllllllnl14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA,

Test ltem(s) Unit Meihod MDLR€aultNo.t

Asbe3to6Actinoliie (CAS No-: 77536€8-4)

%With reference to NIOSH 9000 methodAnaly6is was perfom€d bY )(RD

NegativeNeg€tiv€

{mosite (CAS No.: 12172-7}LAnthophyllite (CAS No.: 7753667- Negative

1 NegativeChrysotile (CAS No.: 12001-295)I Negativecroaidolite (cAs No.: 12001-28'4)

Tremolite (CAS No.: 77536€8€) 1 Negative

Sum of PBBS

mgKg Lwith reference to IEC 6232112008 andlperfomed by Gc/Ms.

n,o.

MonobromobiPhenyl n.o.n.d.

Diblomobiphenyl5 n.d.Tribrcmobiphenyl

n.d.TetrabromobiphenylPentabromobiPhenyl n.d.

5 n.d.ttexabrornobiptrenylHeptabromobiphenyl 5 n.d.

Octabromobiphenyl 5 n.d.

NonabromobiPhenyl 5 n.d.n.d.Decabromobiphenyl

Sum of PBDES n.d.

Monobromodiphenyl ether 5 n.d.

Dibomodiphenyl ether n.d,

fdbromodiphenyl ether 5 n.d.

Tetrabromodiphenyl ether n_o.

Pentabromodiph€nyl ether 5 n.d.5 n.d.Hexabromodiphenyl ether

Heptabromodiphenyl ether 5 n.d.

Octabromodiphenyl ether 5 n.d.

Nonabromodiphenyl ether 5 n.o.

Decabromodiphenyl ether 5 n.d.

Btli:,#y*f.,$Jf T i*rgef :""-"f'Ft'?! --'/,TI.*:'"'{ed I'tE'feeod,*dk:.:6d::.^:j:-

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Lil;iJiiii 'i.i;';i#* 4".m.: b'g.ry d d'r6tr or h oma o

.,t{fi'jlllUlrllr ri

SGSTest Report No. : CE201284041 Date: 2012/0e'/30 Page: 5 of 30

llllllltll0lll!I|[|14OOO JAIMBOREE ROAD, IRVINE, CALIFORNIA'HENKEL CORPOMTION

HENKEL ADHESIVES.ELECTRONICS MAIN OFFICE:92606 U.S.A.

Te3t ltem(s) Unit Method MDLResultNo.'l

,20 3 n.d.1). 4dMINODIPHENYL (CAS No.:c267-1)

mg/Kg With reference lo LFub bz ul_zAnalysis was performed bY GC/MS

BENZIDINE (CAS No r 92-87-2rl mg/Rg Wittr reterence to LPGB 82.02-2.Analysis was Perfomed bY GC/MS.

3 n.d.

3). 4-CHLORO-O-TOLUIDINE/cAS No : SSS9-2)

mg/kg W;ifrErenae to LFGB 82 02-2Anatysis was Performed bY GC/MS

3 n_o.

4). 2-NAPHTHYLAMINE (CASNo.:916$8)

mg,iKg W-h reference to LFGB 82 02-2.Analysis was Performed bY Gc/Ms.

3 n.d.

n.d.sx-E-AMt NoAzoroLUENE (cAsNo.:97-56-3)

mg/Kg with reference to Ll-ut dz.uz-zAnalysis was Perfomed bY GC/MS

5).. 2-AMrNo-4-NlrRoroLUENE/cAs No: 9S55-8)

mg/Kg Fith reference to LFGB 82 02-2Analysis was Performed bY Go/lllg

n.o,

t-: PcH-LoRoANlLlNE (cAs No.:10647-8)

mgKg With reference to LFGB 82 02-2.Analysis was P€rformed bY GC/MS.

3 n.d.

WiIh reference to LFGB 82-02-2Analysis was Perfomed bY GC/MS

3 n.d.8)2+DTAMINOANISOLE (CASNo.:615{5.4)

mg/Kg

WlGarence to LFGB 82.02-2Analysis was Performed bY GC/MS'

3 n.d.

3^o"1"oo,rrr*"r".r"o*.(CAS No.:101-77-9) _

mg/Kg

n.d.ibjFucHLoRoBENzlDlNE(CAS No.:91-941)

m9Kg With reiercnce to LFbtt oz,uz_z.Analysis w€s Performed bY GC/MS'

3 n.d.Tfil3l3 -onterHoxYeet'tzotHe(CAS No.: 11SgG4)

mo/ko f With refercnce to Lrvtl 62 uz-z- lAnalysis was performed by GCiMS

3 n.d.l-33LDtMETHYLBENZIDINE{CAS No.: 119-93-7)

m9Kg With refe€nce to LF9E 6z.uz-2.Analysis was Perfomed bY GC/MS.

3 n.o.13). 3,3'-D|METHYL4,4-DIAMINOOIPHENYLMETHANE(CAS No.;838€8{) -

mg/kg y'Vith rclerence to LFsl, oz uz-zAnalysis was Per{ormed bY GC/MS

3 n.d.I-).PcREslDlNE(2-METHoxY-$METHYLANILINE) (CAS No :

12G71-8)

mg/Kg wfh relerence Io LruD oz,v.-z'

Analysis wa6 Performed bY GC/MS

3 n,o.1-s):l '.lruemYtexe-gts-(z-CHLOROANILINE) (CAS NO.:101-1+4)

mg/kg With reterence to LFsn oz uz_zAnalysis was Performed bY GC/MS

ffii/! I -r iiri:"LTL" I rtlMri

i r\"{il ll luirii R

Test RePort No.: cEl2o1284u1 Date:2012108/30 Page: 6 of 30

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS MAIN OFFICE:92606 U.S.A.

llllllllllilllllll'14OOO JAI/IBOREE ROAD' lRVlNE, CALIFORNIA'

Test ltem(s) Unit Mothod MDLReaultNo.'l

3 n.o,i6). 46). 43loxYolANlLlNE (cAsNo.r '101€M)

mg/Kg With reference to Ll-ub 62 uz_zAnaly6is was Perlormed bY GC/MS

3 n.d.4,4.THIODIANILINE (CAS13965-1)

17\:No.:

mgKg with reference to Lf utt dz uz_Z.Analysis was Performed bY GC/MS.

3 n.d.18)r GTOLUIDINE (CAS No: 95-534)

mSikS With reference to LFUb uz.uz-r'Analysi6 was Perfomed bY GC/MS

WIF reference to LFGB 82 02-2Analvsis was Performed bY GC/MS

3 n.d.1 9): 2,4.TOLUYLENEDIAMINE(CAS No.r 9ffiG7)

mg/Kg

3 n.d.ZO). Z3,S-rnUetryUrutltt'tE(CAS No.: 13717-7)

mg/Kg With reference to LtGtt uz.uz_z-Analysis was Performed bY GC/MS

n.o.21-).. GAN|S|DINE (cAs No.: 9G044)

mg/Kg With releBnce to Lrsn oz uz-r'Analysis was Per{orm€d bY GC/MS

3 n.d.22F-AMINOAZOBENZENE(CAS No.:60-09-3)

mgKg with referen@ lo LroE dz.uz_Z.Analysis was Perfomed bY GC/MS.

3 n.d.23-)2r4xYLtDlNE (cAs No: 95-68-1)

mg/kg with ldelence to LFstt oz uz-zAnalysis was Pertormed bY GC/MS

Wth-reference to LFGB 82.02-2.Analysis was Perfomed bY GC/MS.

3 n.d.24):2,SXYLID|NE (CAS No.: E762-7)

m9Kg

F's(chlorof, uorocarbons)Group I n.d.:J orofluorocarbon-1 ! (CAS No.:rs694)

mgKg ruith reterence rc uo ErA ovz 'lethod. Analysis was Performed bY3C/MS.

1 n.d.Shlc,ro-hlc,rofl uoroca6onl2(cAsNo:75-71-8)

mgi Kg y'vith r€ference to u5 EPA 5uz Imethod. Analysis was Performed bYGC/MS,

1 n.d.dEl6-rottuorocaoon-rr:(cnsuo.76-13-1)

mg/kg with reference to u5 ErA ouz Imethod. Analysis was Performed bYGC/MS,

1 n.d.dfri66iii6rocarbon-114 (CAS No :7B-14-2)

mgKg with reference lo ul' ErA ouz Imethod. Analysis ',!as perform€d byGC/MS.

n.d.diiIofluorocarbon-1 1 5 (CAS No :76-15-3)

m9Kg With reference to uu El'A cuz Imethod. Analysis ',!as performed byGC/MS,

Fffiffi ,ffiffi$*ffiffiffiffiffi,,#trn#,ffi#,ffi iMi$ffi,G5a {o ! , r , s wucco to ,N ' r r t r ' r r l 4 t f f ! r { r f t f

:' l(:'i ii&iit r 't

Test Report No. : CE/201?J84041 Date : 2OlZO€l30 Page : 7 of 30

HENKEL CORPOMTIONHENKEL ADHESIVES-ELECTRONICS MAIN OFFICE:92606 U.S.A.

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Test ltem(s) Unit Method MDLReaultNo.'l

Group lllChlcrofl uorocarbon-1 3 (CAS No :75-72-9)

mg/kg Fith reference to us EPA 502 1method. Analysis w€s P€rformed bYGC/MS.

n.d.

fflooftuorocarbon-r 11 ICAS t'lo.:354-5+3)

mg./Kg Wifr reference to us EPA 5021method. Analysis was Performed bYGC/MS.

I n.d.

dfilorofluorocarbon-112 (CAS No :76-12-0)

mgikS With reference to US EPA 5021method. Analysis was Perfomed bYGC/MS.

I a.d.

Chlc,rofl uorocarbon-2l ! (CAS422-7e.$)

No.: m9Kg Wth refetence to US EPA 502 1method. Analysis was Peformed bYGC/MS.

,! n.d.

dEioroftuorocarton-2t z (CAS No.:3182-26-1'

mg/kg Witlr reference to US EPA 502'1method. Analysis was Performed bYGC/MS.

I n_o.

-hlorofl uorocarbon-21 3 (cAs No2354-06-5)

mg/Kg friifr reterenceio US ePA 50zlmethod. Analysis wEs Pedormed bYGC/MS.

n.d.

ehbrof luorocarbon-214 (CAS No.:29255-31-o)

m9Kg WlFE-ferenc€ to Us EPA 5021method- Analysis was Performed bYGC/MS.

1 n.d.

bywi[h reference to us EPA 5021method. Analysis was PertonnedGC/[rS.

1 n,o.Chlorof luorocabon-215 (CAS No.:425943.2]

mg/kg

Chtorofluorocarbon-21o (CAS No :661-97-2)

mg/kg With reference to US EPA 502 1method. Analysis wa6 Performed bYGC/MS,

1 n.d.

Fhbrofl uorocaibon-217(cASNo:422-e6€)

mgKg wttr reterence to US ePA 50ztmethod. Analysis was P€rformed bYGC/MS.

n.d.

HCFCs(Hvd|ochlorofl uoocalbons)HCFC-21 (CAS No.: 75434) mg/Kg Wttr reference to uS EPA 5021

method. Analysis was Perfomed bYGC/MS.

I n.d.

HCFC22 (CAS No.r 754S) mg./Kg Wlifr reference to US EPA 5021method. Analysis was Perfomed bYGC/lis.

1 n.d.

ffitffiffiffiffi*ffi

Test RePort No. I CEaO1Z84O41 Date : 2OlZO8l30 Page : 8 of 30

HENKEL CORPORATIONHENKEL ADHEsIVES-ELECTRONIcS li4AlN OFFICE:92606 U.S.A.

Test ltem(8) Unit Method MDLResultNo.l

frm refe.ence to Us EPA 5021method. Analysis wEs Performed bYGC/MS.

n-o.fl-1 (cAs No.: 59&704) mSikS

FCFd1zt (cAs No.: 3s+14-3) mg/Kg Witth reference to uS EPA 5021method. Analysis ,,!as performed byGC/MS.

1 n.d.

i6Fe-tzz (cns No.: s54-zr-2) mdkg With reference to uS EPA 5021method. Analysis 'r/as performed byGC/MS.

1 n.d.

1 n.d.HCFC-'123 (CAS No r 3m-83-2) mg/Kg With reference to uu El'A iuz I

method. Analysis was perfonned byGC/MS,Wiifr reference to Us EPA 5021method. Analysis w€s Performed bYGC/MS.

n.d.HCFC-124 (CAS No.: 2837-Eg-0) mgKg

FteFcr3l (cAs No.: 35&284) mg/Kg w=rth reference to us EPA 5021method. Analysis was Perfomed bYGC/MS.

n.d-

HCFCj32b (CAS No.: '1649{8-7) mg/Kg With reference to US ePA 50Ztmethod. Analysis was Performed bYGC/MS.

1 n.d.

HCFo-1ii3a (cAS No.: 75-8&7) mg.i l(g Vvittr reference to US EPA 5021method. Analysis was Perfomed bYGC/MS.

'I n.d.

HCFG141b (CAS No.: 1717{0€) msikg Witlr reference to us EPA 5021m6thod. Analysis was Performed bYcc/Ms.

1 n.d.

HCFc-142b (cAS No.: 756&3) mgKg With reference to US EPA 5021method. Analy6is was Performed bYGC/MS.

n.d.

HCFC221 (CAS No.: 422-264) mg/kg r/Vith reference to US EPA 5021method. Analysis was Performed bYcc/Ms.

n.d.

HCFC-222 (CAS No.: 42249-1) mgKg With reference to us EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.

Nvh'Fcrv,l,w!i/,ri .i '.4{:4t I iiirr3![

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fffiffi!*'"'.ii,.i'."":#:i'+r&iii::iEililil-*liltsg;r"f::,#,e:5'*.";!p*i.t'"'tr;15-1iu.&'ir#ff.-'l,'"lfri"":lil',ilnXJH"d;frfJiiilS:9"9'**HI;#'J::"8',fii3:X;,i,+11i;;;b;;;'h"d@."d'.s"sdtrd^'o'-":""@nE*d;red'i'd$eco"1p'1vtidn$a'r. lne o,,E 'n,.Mdon r,y ard wm ne r.a.' u,'e"'. .*"6i" i.ll '* c"'oar's o" 'espos"''rv e ! n c dr ro rhh o@med dotsnt';{ili:'*'1"*i:"$:

i"^i1ii'dni'o.e,eg'oartrr'g'"g|Ba.ood'gdl9d3.dc'[^.hncsdons@ng$1h!ooc.-6rl@TL omen, Ary undd ro 'r'aion

"'0". "' '."'*"', ', '.JH;:-iiiiiiil' ar i**r a r*t' sd d'd'G ma h on,*-d b h

Test Report No.: cEI2O12J84o41 Date:2olz0&30 Page: I of 30

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS NIAIN OFFICE:92606 U.S.A.

Tost ltom(s) Unit lrethod MDLResultNo.1

ieFc-223 (cAs No.: a22-524) mg/Kg Fifir reference to us EPA 502'lmethod. Analysis was perfonned byGC/[IS.

n.d.

ICFC-224 (CAS No.: 422-54-8) mg/kg Wittr reference to US EPA 5021m€thod. Analysis was Perfomed bYGC/MS,

n.d.

HCFG22sca (CAs No.: 422-56{) mg/Kg With reference to US EPA 5021method. Analysis was Perfomed bYGC/MS.

1 n.d.

F225cb icAs No.: 507-55-1)mg/Kg Wii6 reterence to us EPA 5021method. Analysis \ras Pedormed bYcc/M6.

'I n.d.

FtcFG226 (CAS No.r 431-87-8) mg/Kg with reterence to us epA 50ztmethod. Analysis was Perfomed bYGC/MS.

1 n.o.

HCFC-231 (CAS No.: 421-94-3) mg/kg Wi h reference to US EPA 5021method. Analysis .|/as Pedorm€d bYGC/MS.

n.d.

HCFC-232 (CAS No.: ,16G89-9) mg/Kg With reference to US EPA 5021method. Analysis was P€rfomed bYGC/MS.

n.o.

ncrczgg (cns ruo.: zt25-84-0) | mgkg With reference to uS EPA 5021method- Analy6is was pertormecl byGC/MS.

1 n.d.

HCFC-234 (CAS No.: 42t94-5) mg/kg V',littr reference to US EPA 5021method. Analysis wtss Performed bYGC/MS.

1 n.d.

HCFC-235 (CAS No.: 460-92-4) m9Kg Wth reference to US EPA 502 1method. Analysis was Performed bYGC/MS.

1 n.d.

HCFC-241 (CAS No.: 666-27-3) m9Kg With reference to US EPA 5021method. Analy6is was Performed bYGC/MS.

1 n.d.

HCFC242 (CAS No.: 460-63-9) mg/kg With reference to US EPA 502 1method. Analysis \r€s Performed bYGC/MS.

n.d.

rlllllulllllllllll14OOO JAMBOREE ROAD, IRVINE' CALIFORNIA'

NryrrFicry,rdw:^/t l: :i I dt qUr mft$

Test RePort No. : CEI2o12l84u1 Oater 201210&30 Pagei 10of 30

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS92606 U.S.A.

llll ttllllLm ||l

MAIN OFFICE: '14000 JAMBOREE ROAD, lRVlNE, CALIFORNIA'

T€at ltem(s) Unit Method MDLResultNo.'l

Fiffi++g (cAs No.: 460-6+s) mgKg r'vith referenc€ to US EPA 5021method. Analysis was Pertormed bYGC/MS.

n.d.

HCFc244 mg/kg Wi-ith reference to us EPA 5021method. Analysis wEs Pe.formed bYGC/MS.

n.d.

FoFG251 (CAS No.: 421-41-0) m(yKg Wi-th reference to us EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.

HCFG252 (CAS No.: 81M0-1) mg/kg Wl-ith reference to Us EPA 5021method. Analysi6 was Performed bYcc/Ms.

'| n-d.

rcFc-2s3 (CAS No.: 460-35-5) mg/Kg With reference to US EPA 5021method- Analysis was Perform€d bYGC/MS.

1 n.d.

HCFC-251 (CAS No.: 420-97-3) mg/kg Vvillr refer€nce to US EPA 5021method. Analysi€ was Perfomed bYGC/MS.

n.d.

HCFC-262 (CAs No.: 421-02-03) mg/Kg With reference to US EPA 5021method. Analysis was Pedomed bYGC/[rS.

n.d.

HCFC-271 {CAS No.: 430-55-7) mg/Kg Wttr reference to US EPA 502 1method. Analysis was Performed bYGC/MS,

I n.d.

HBFCSrHv.lmhhd^fl tr.r.rcalbonsl

HBFC-2l82 (CHFBr2) (CAS No.:1868-53-7)

mgKg Wth reference to US EPA 5021method- Analysis was Pertormed bYGC/MS.

1 n.d.

HBFC-2281 (CHF2Bi) (CAs No.:151142-2]

mg/kg Wth raference to uS EPA 5021melhod. Analysis was Perfomed bYGC/MS.

1 n.d.

HBFC-3181 (CH2FBr) (CAS No.:373-524)

mgKg With reference to US EPA 5021method- Analysis was Performed bYGC/MS.

n.d.

HBFc-12184 {C2HFB14) mgikg Wittr reference to Us EPA 5021method. Analysis $ras Pedormed bYGC/MS.

n.d.

d;nirT'f.'115'6-'li:'cf xl"'jir'':riY'd*v,f rr""T* ":"1 " 1:i. l*:.'1::l:i:::*ji I';;|;;;:;;;-ddbd*{"'djFdi,h-''ndc-d**6'ii;;;D;;;ftajm'c9@sf€aie

* l " goo , s * . " - * " * i " - dYhdde ldmFdoe1d jgd i$diilii-.;.iir' ' i i.."lii*mno"-ow;tr"'.6olc..t' '*d;;', ';::'=;;c;;'ii!sh.@E''a

g6*do , * * * " " * , ; i ; d f dodm.nbFgodJT1 ' c . n .ocompd,, {ry u.,J,Tqr.d. b,,tr ' ' --,i!r-i' i j"p-t#ii o;;;;iitJn*' mo orrd'a r;bepm

NvrnFctrdwm/i I -t r. di qt'"r illrtlt

Test Report No : cEl201284041 Date: 2012108/30 Pase: 11 of 30

HENKEL CORPORATION , _. ,., |||ITUffiIIIII

iiEi.iiei lonesves-elEcrRoNtcs MAIN oFFlcE: 14ooo JAMBoREE RoAD' IRVINE' oALIFoRNIA'92606 U.S.A.

Teat ltem(8) Unit Method I'DLResultNo.1

HBFC-12283 (C2HF2B13) mSikg Wittr raference to uS EPA 5021method. Analysis was Performed bYGC/MS,

1 n.d.

HBFC-12382 (C2HF3812) mg/Kg Wth reference to US EPA 5021method. Analysis was Perfomed bYGC/MS.

n,o.

HBFC-12481 (C2HF4B0 mgKg l/Vith reference to US EPA 5021method. Analy6is was Performed bYGC/[rS.

n.d.

HBFc-13183 (C2H2FB13) mgkg With reference to US EPA 5021method. Analysis was Pertormed bYGC/MS.

1 n.d.

HBF C-1 3282 (C2H2F 2Br2l mg/kg With reference to uS EPA 502 1method. Analysis was Performed bYGC/MS.

I n.d.

HBFC-13381 (c2H2F3Br) mS/kS With reference to US EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.

HBFC-14182 (C2H3FBi2) mg/Kg With reference to US EPA 5021method. Analysis was perfomed bYGC/MS.

'I n.d.

HBFC-I4281 (C2H3F2Br) mg/Kg With reference to US EPA 502'1method. Analysi6 was perfomed bYGC/MS.

1 n.o.

HBFC-I5181 (c2H4FBr) mg/Kg With reference to US EPA 5021method. Analysis was performed bYGC/MS.

n.d.

HBFC-22186 (C3HFB16) msyKg With reference to Us EPA 5021method. Analysis was Perfomed bYGC/MS.

n.d.

HBFC-22285 (C3HF2815) mg/Kg With reference to US EPA 502 1method. Analysis was peformed bYGC/MS.

,! n.d.

HBFC-22384 (C3HF3B14) mgftg With reference to US EPA 502 1method- Analysis was pedormed byGC/tVS.

1 n.d.

f 1115 F3' '€ror der dry b trs !r'lpqs b5r9q l:!h!_pondda ; i m ; - . ; y . _ t l - r F + a _ f 4 , . _ _ _ . _ j . t l

i r i " i i . " 1 *ng , *o "# ' n "a .p - y *hdb "G* * | c -d fdds ; f , j 0 ' F i , o ; i ' eabdeo;;;;;*;;ffi;i;;ffiR';biaii6r"-"a{c@otoT,o,F|4rcn(oo6mdiRd|M'!s6fuinini in ni,i'i". '"oe- ,**" .- n d,6b' ,sa d.''d bs;it; ;* ti aiem.d ts-'d'sd o r d' co-Fa! ridhes ''; ; ; " i ; ; i : ; ; " ; ' ; ; d ; [ i i i . d t r dc |Gd rAMos , i r ' ' - - dnp j1 , t $s ' € ,pdgb |i"l.iii i j" i.- -e*'o,r."'

"ofs and db,€Ad\ '*' d. h;.d;i od* L -ns do@m'i't 6mioe Gpnd'cd "Go'

' '-

coi$tu M i&h zn dbdbn bma a rdsl€rcnd tp oieiio dd&tol"u€ {4 F doFrsd

- | ; ] ' 4 ! i ; . - ] } . i ' 1 ] 3 *" I 'i isiloiJrirzn r;oo@Pn r *".,;

Test Report No. : CE/201284041 Date : 2O1Z08il30 Page : 12 of 30

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS MAIN OFFICE:92606 U.S.A.

Test liem(s) Unit Method MDLResultNo.'l

HllFcr4B3 (caHF4Br3) mg/Kg Vvith reference to US EPA 5021method. Analysis was Performed bYGCiMS.

n_o.

HBFG22582 (caHFsB12) m9Kg With reference to US EPA 5021method. Analysis was Performed bYGC/MS.

n.d.

HBFC-22681 (CaHF6Br) mg/Kg Vviltr refer€nce to US EPA 502'1method. Analysis was Perfomed bYGC/MS.

1 n.d.

HBFC-23185 {CaH2FB15) m9Kg With reference to US EPA 5021method. Analysis was Per{ormed bYGC/MS,

,! n.d.

HBFG232U {cAH2F2Bi4\ mgikg With reference to uS EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.

HBFC-23383 (C3H2F3813) mgKg with referenc€ to us EPA 502 1method. Analysis was Perfomed bYGC/[TS.

1 n.d-

HBFo-2?/.82lc3H2F4Bt2) 6![g[wth reference to us EPA 502'1lmethod. Analysis was performed bytGc/Ms.

n.d.

HBFC-23581 (C3H2F5Br) m9Kg fVitfr reference to US EPA SO21method. Analysi6 was Perfomed bYoc/tus.

1 n.o.

HBFC-24'l 84 (C3H3FB14) mg/kg lrvith reference to US EPA 502 1method. Analy6is was Performed bYGC/MS.

1 n.d.

HBFC-24283 (C3H3F2813) mg/kg lwith refetence to US EPA 5021lmethod. Analysis $ras peformed bylGc/Ms.

1 n.d.

HBFC-24382 (c3H3F3812) mg/Kg with reference to us EPA 5021method. Analysis was Peafomed bYGC/MS.

I n.d.

HBFC-244B'1 (C3H3F4Br) mgKg With ref€rence to US EPA 5021method. Analysis was Performed bYGC/MS.

n.d.

rllllllllllllll|!14OOO JAMBOREE ROAO, IRVINE, CALIFORNIA'

u^esoh€N*@d[-66!rts3|lM -hr!4r€9o1!€'fryb$c\tnp6\6rres"d I' rFn "Fd6ub?c o s r y : ' ] ' ! ] ' 4 r l , 4 - : T ' - . ' : . ] . ] " ; ; : l . " } ; * " " i , ; ; ; ' * , | " b l " -

qe. '"-"""" "q "

'"" 'iiitid;i;6; ii{was @d'n"rsis*oo.o's*s"-*""..j";iiirir''iri.umaoe..ngm*eatan" o'' 'c d''*' '

"-';;; ; ai"-

-i"t"'oar "

-' ospa"'irv'' o'B c'€{'rd ih^ "*nent

d

e*"* oaarc""*".' * iii iai:ti:r'd'omats ri'mcr-d @Td!€ apmso 'dpr 'n $tiond

comD.Fv &vuraftlda''aror . Jl;;G;d;;;;' F'" d-'alr E i #n sddme6maho

krrp. cLv lr,ri / u l -ril!+t:{ I rrirllrlri

Test Report No.tCEaO1Z94c{| Date:2012108/30 Page: 13 of 30

HENKEL CORPORATIONHENKEL ADHESIVES.ELECTRONICS MAIN OFFICE:92606 U.S.A.

r ml|lllllllll14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA'

T.st ltem(B) Unit Meihod MDLReBultNo.t

HBFC-25183 (C3H4FB13) mg/kg With reference to US EPA 5021method. Analysis was Per{ormed bYGC/MS.

1 n.d.

HBF C -25282 (C3H4F 2B(2) mg/tg Wittr reference to US EPA SOZ lmethod. Analysis was Performed bYGC/MS.

I n.d.

HBFC-25381 (C3H4F38r) mg/Kg w h reference to Us EPA 5021method. Analysis wa6 Perfomed bYGC/MS.

n.o,

HBFC-26182 (CaHsFBz) mg/Kg With reference to uS EPA 5021method. Analysis wts6 perfomed bYGC/MS.

n.o.

HBFC-26281 (C3HsF2Br) m9Kg With reference to US EPA 5021method. Anaiysis was Perfomed bYGCA,tS.

1 n.d.

HBFC-27181 (C3HOFBT) mgKg With reference to US EPA 5021method. Analysis w€s Per{ormed bYGC/MS.

1 n.d.

HFCs (Hydrofl uorocalbon)HFC-23 (CHF3) (CAS No.:754&7)

mg/Kg With reference to US EPA 502 1method. Analysi6 was perfomed bYGC/MS.

1 n.d-

HFC-32 (CH2F2) (CAS No.: 75-10-5)

mgKg With reference to US EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.

HFC41 (CH3F) (CAS No.r 59953-3)

mg/kg With reference to US EPA 5021method. Analysis w€s Performed bYGC/MS.

n.d.

HFC-43-1omee (C5H2F10) mg/K9 With reference to US EPA 5021method. Analysis was performed bYGC/MS.

n.o.

HFC-125 (C2HF5) m!,/Kg With r€ference to US EPA 502'1method. Analysis was Performed bYGC/MS.

1 n.d.

HFC-13/ lC2H2F4t mS/kS With reference to US EPA 5021method. Analysis \ras pedormed bYGC/MS.

I n.d.

ow1 '1 rh6b3 ' r €eonF re !G la tu ' amoeF bebd r - !F l - pon* ' d' 4 | r & ! ' : r " - ' r

oaru-"*. ".*-,"..rori

'qf{o-€6se .*'3lsodeis "d

.m no'sr:m

ii'ir ri,ioiiii'i;; i;r oho*n $bld 6 rems md co d,b66; ri.imn. o@mo6 d 9N {s @tueMer:! n4cdo nmr€ - daeo

i;;#J;iih idmi'€t* .ad ilasd'dm '$fs ddtd rEc. Atui ^ i i i i n . , i t ' r g iwno " * " *o " ' t " s "1 . i so | c i - r . 'm ; ; ; i a ; ' i " comoaq .oeas f sDa1ii,1'l,]ito]iri..ii#*l"oar|o","g.s.rcou,g"**-oeru'n;;;i/orii.oiiti '**-g'--"itii'io"iiiii"i;;m;&-a'"*m.:'o,oor. r-"'r'*to. or m -'iiiiid;;;;;;;ir:" @nel" -' ""r' ala orend'6 ma' b' or'*'ad o r

Ntrri'Ficv,r!e?n/f I ./ ::4r{r'! rlii i3rlr:

Test Report No. I CE/2O1Z84M1 Date : 20'1208130 Page : 14 of 30

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS Ii4AIN OFFICE:92606 U.S.A.

lllllIllllffillnl14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA'

Test ltem(s) Unlt Method MDLResultNo.l

tFG134a (CH2FCF3) (CAS No.l311-97-2\

mgitg Wittr reference to US EPA s021method. Analysis w€s Perfomed bYGC/MS.

n.d.

Uvith reference to US EPA 5021method. Analysis was Perlormed bYGC/MS.

n.d.HFC-143 (CH3F3) mgKg

HFCl43e (CH3F3) mS/k0 With reference to uS EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.

HFC-152a (C2H4F2) (CAS No:75-37-6)

m!yKg Wttr reference to us EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.

HFC-227e4 (CaHF7) (CAS No l431-8S0)

mg/kg WiFtr reference to us EPA 5021method. Analysis was Perfomed bYGC/MS.

'I n.d.

HFC-236fa (C3H2F6) m9Kg Wlitlr reference to uS EPA 5021method. Analysis was Perfomed bYGC/[rS.

1 n.d.

HFC-236ea (C3H2F6) (CAS No :43'1-63-0)

mSikS With reference to Us EPA 5021method. Analysis v/as Pedormed bYGC/MS.

n.d.

HFC-24sca (C3H3F5) mg/kg WjG;;j;rence to us EPA 5021 I 1method. Analysis was performed by Icc/Ms. I

n_o.

HFC-245fa (C3H3F5) m9Kg With reference to US EPn S021method. Analysis was Perform€d bYGC/MS.

1 n.d.

HFC-365mfc (04H5F5) mg/Kg WiifrEr€nce to us taPA 5021 I 1method. Analysis wtss Perfomed bY IGC/MS. I

n.d.

PFC5 (Porfluorocarbon)

F14 (CAS No.r 7S73{) mg/Kg WlGEGEnce to us EPA 5021 I 1method. Analysis wEs performed by IcciMs. I

n.d.

Fluorocarbon 116 (CAS No.: 76-164)

mgKg with ieferenc6 to uS EPA 5021method. Analysis was Performed bYGC/lrs.

n.d.

(N .w r ;pd ' i q I : ! d r l ' : r r l L+ 9 * i I ' i : r ' { l

lHr.frrrrx"-r-f::,;'iT:::j:,:ry-:_q;::flr"'jH:;:::::i:::::THA":::];j:"tr:":HH"::;ft6 d&nmd 'e l6d bv !1. cotrrprnv 3ubieq ro G 6€!ea e ml. -.

"' - '.,"'' . ;:ii'ft;? 6i'i':nrJii"i* "s'

o*m"'gm!"oao*"9 i* ' ** ' i i ' i i i , i " |a ; 'd0 ' , ,o* ,g.6ad,*"h.. *'.'"

" -'-.','""'*;;:iii i; ;i;;i';rt;'i i;"o"bi

hr 50n6,{d o'mr! u'oe n" J;;;;;d;+d; r ' iaff iuft{aro:@ reYmuco&@p tr t

"ii.iii'iiP;* Ln o" oeo

Test Report No. : CE/20'1284041 Oale.2O12J08l30 Page: 15of 30

HENKEL CORPORATIONHENKEL ADHESIVES.ELECTRONICS92606 U.S.A.

ll [trlllfillllllrAlN OFFICE: l4OOO JAITBOREE ROAD, IRVINE' CALIFORNIA'

Test ltem(s) l,rnit lrethod MDLRaaultNo.t

Freon 218 (CAS No.: 7S1&7) m9Kg With reference to Us EPA 502 1method. Analysis wa6 Performed bYGC/MS.

1 n.d.

Decafluoobutane (CAS No.: 355-25-9)

mg/kg With ref€rence to US EPA 502 1method. Analysis was performed bYcc/Ms.

1 n.d.

Freon C318 (CAS No.: 115-25-3) mg/kg With reference to US EPA 502 1method. Analysis w€s Performed bYGC/MS.

n.d.

Pertluor- 1-butene (CAS No.: 357-2ffi)

mg/Kg with reference to us EPA 502 1method. Analysis was Performed bYGC/MS.

n.d,

perfluorisobutene (CAS No.: 382-21€)

mg/Kg Yvith reference to US EPA 5021method. Analysis was Perfomed bYGC/MS.

n.d.

1 .4-dihydroo6:taf luorobutane (CASNo.:377-3M)

mg/Kg With reference to US EPA 5021method. Analysis was Performed bYGC/MS.

1 n,o.

Nonaf luor-2- (trif luoromethyl)butane (CAS No.: 594-9'l -2)

mg/Kg With reference to US EPA 5021method. Analysis was Pedormed bYGC/MS.

1 n.d.

Perf luoro-n-pentane (CAS No.:67&26-2)

mg/kg lwith reference to us EPA 5021lmethod. Analysis was Performed bylGc/Ms.

'I n.d.

2-perfl uoromethylpentane (CASNo.:35S,9)

mg/Kg With reference to US EPA 5021method. Analysis was perfonned byGC/MS.

1 n.o.

Perfluorohexane (CAS No.: 35&42-0\

mgKg With reference to US EPA 502 1method. Analysis was Performed bYGC/MS.

n.d.

CHCS (Chlorinate hydroca6on)1,1, 1,2-Tetrachloroethane (CASNo.:630-206)

mgKg With reference to US EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.

1 , 1 ,1-Trichloroethane (CAS No. I71-556)

mg/Kg Wittl reference to US EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.

Nt!hrF civ,.rmrn/t I ;Jrlet{;: li:rl,\!!

oM '1 rnec$GeonEE!@v t Fc r . ' ! o . ( t b$d r - r r gd tpon6dc . . F n ' ' ' ' ' F . r ' - ' a ' | ] { l " , " " . . ' r - , : ' 1 " . . , ; - * ; ; ' " . ; ; - , " " " . " ' " " '; ;U;;Ero;;A; n! -,id,i'r.ftsd co.onom6iabd;i o;.ed" r *3!r @d"""rrs"o crd nd3"-\ 3 ooonm !

Ms,6r ,$-' ** ".'i:-ii,t;#ft; #iliiGi;;;,y;d;+ii n.,imE or c,i.dx ndM;; ii.i ' i comat

" oa a*o'ui'v i b 6 c rr mo mE d@mrrd@

ors*" oo"sa'-" -*" ".

uiin;;;@m;B ri'doc-_'namoibe €pod'cd ecd 1a' *rd

tiliijiill i,i ijn'ain*i,io1lnm"i r",c",y u '.i'r-m" ot 0E offi-iiiiFiiiiii or ttc oomit s utamr 'na onendee mav be pres*d€d b $e rurb$ 'nenr or rhe r*

Test Report No.. CE^O1Z84O41 Date : 201208/30 Page : 16 of 30

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS ti4AlN OFFICEI92606 U.S.A.

trtllllllllllltllll14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA,

Test ltem(a) Unit Method MDLReaultNo.'l

i, 1,2,2-Tetrachloroethane (CAsNo-:79-34-5)

mg/kg With reference to uS EPA 5021method. Analysi6 w€s Performed bYGOMS.

1 n.d.

m-Trichloro€thane (CAS No.:79-00-5)

mg/kg Witlr reference lo US EPA 5021method. An€lysis \^/as performed byGC/MS.

I n.d.

1 ,1-Dichloroethane (CAS No.: 75-34-3)

mg/kg With reference to uS EPA 502'1method. An€lysis u/as performed bYGC/MS.

I n.d.

1 ,1-Dichloroethene (CAS No.: 75-3s4)

mgftg with reference to us EPA 5021method. Analysis was pedormed bYGC/MS.

n.d.

1 ,'l -Dichloropropene (CAs No.:563-586)

mgikg With reference to US EPA 502'1method. Analysis was performed bYGC/MS.

n.d.

1,2,3-Trichloropropane (CAS No. :96-184)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/|VS.

n.d.

1,2-Dichloroethane (CAS No.:107-0G2)

mgKg With reference to uS EPA 5021method. Analysis was perform€d byGC/MS.

1 n.d.

'1,2-Dichloroprcpane (CAS No.:78-87-5)

mgKg With ref€rence to US EPA 502 1method. Analysis was performed byGC/[IS,

1 n.d.

1,}Dichloropropane (CAS No.:142-24-9)

mgkg with reference to uS EPA 502 1method. Analysis vr€s per{ormed byGC/MS.

1 n.d.

2,2-Dichloropropane (CAS No.:594-20-7)

mS/kS with reference to us EPA 5021method. Analysis was performed byGC/MS.

I n.d.

Carbon tetrachloride (CAS No.:56-23-5)

mg/kg With reference to US EPA 502 1method. An€lysis $6s performed byGC/MS.

1 n.d.

Chloroethane (CAS No-: 75-0G3) mg/kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

e-s F.!qd r' 3 bs! tpo. s-d & Epd ud e'|@p 'i tJ'c o h s N l . l n / - t , l K ! , ! + l r - . : R - - E F l t - r { r -i ; " ; * d j d . d M h " f t @;;L;;;;ffi;i&;;;'.{bai'i""i'",ncdoto$,o,LFfuDo;manE.lM9g'omiriali:ii,]r"ur.

"0.* te"o" d." -*"di",io" 'g*r d. -& s.n akl Te or b6 i'odmpn 'iddred,h.

6 . i . ; " r6 'nk ;d - * r ' -d -h i i E i -Edc isnrs $ rado ls 'n , \ conpant ae camb I ' t v 6 o i3 'd ' 'nd rEdtumeid;#;;n;o"i;;-;;;;ll ;;s;:;jn ;;isa!o;ta*, h, btaairn mryd -tia ooem.irt smiii-*i ri.i'"i*d" +.*" 'ors..y rllrebibno't. @Gdo rrnol.@tst, Fnoseci.d o d

tN .w i rp . c i v , t u ! d r l , , l t t { { f , r E i f 331 i

Test Report No.: CEJzOlz84() 1 Oale' 2012108130 Page : 17 of 30

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS li4AlN OFFICE:92606 U.S.A.

Test ltem(s) Unit Method MDLRssultNo.1

Wittr reference to Us EPA 5021method- Analysis was Performed bYcc/Ms.

n.d.Chlrroform (CAS No.: 676+3) mgKg

Chlorornethane (CAS No.: 74-87-3)

mgftg Freference to us EPA 5021method. Analysis was Performed bYGC/MS.

n.d.

cisl,2-Dichloroethene (CAS No-:1s6-59-2)

m9Kg Vvith reference to US EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.

cis-1,3-Dichloropropene (CAS No :10061-01-5)

mS/kg V,,littr reference to uS EPA 5021method. Analysis was Performed bYGC/MS,

1 n.d.

FdEchloro6utadiene (CnS No.:87-68-3)

mg/Kg With reference to US EPA 5021method. Analysi6 was Perfomed bYGC/MS.

1 n.o.

Methylene Chloride (CAS No.: 75-o9-2)

mdkg With reference to US EPA 502'1m€thod. Analysis $ras Pedormed bYcc/Ms.

,l n.d.

Tetrachloroethen€ (CAS No.: 127-1H)

mg/k9 With reference to uS EPA 5021method. Analysis ! €s performed byGC/MS.

n.d.

tranel 2-Dichloroe'thene (CASNo.: 15&6G5)

mg/Kg With referenc€ to US EPA 502'1method. Analysis was Perfomed bYGC/MS.

n.o,

trans-t3-Dichloropropeno (CASNo.:10061-026)

m9Kg With reference to US EPA 5021method. Analysis was pertorrned byGC/MS.

1 n.d.

Trichloroethylene (CAS No.l 7$01€)

mg/kg Vvith reference to US EPA 5021method. Analysis w€s Performed bYGC/MS.

1 n.d.

[llllllllllllrllll14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA,

, / r'r! t:.r |r I !tr]]rlt

Test Report No. : CE/201?J84041 Date : 2OlZO8l30 Page : 18 of 30

Note i1. mg/kg = ppm ; 0.1M% =1000PPm

2. n.d. = Not Detected3. MDL = Method Detection Limit4 . " - "=No tRegu la ted5. " = Qualitative analysis (No Unit)

6. Negative = Undetectable / Positive = D€tectable

7. Asbestos : Negative = "< '1.0 yo", Positive = "> 1 0 yo"

8. 't': The sub$a;ce wEs calculated by the test €sult of Tdbutyl Tin The MDL was evaluated for Tributyl Tin'

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS IT4AIN OFFICE:92606 U.S.A.

lf,lll|lrnwflnl14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA'

PFOS Reference Intomation : POPS ' (EU) 7572010

Outlawing PFOS as substances or preparations in concentrations above O OOI0/6 (1oppm)' in semi-finished

proOuAs-or articf"s or parts at a level above 0.1%(lOOOppm), in teniles or other coated matedals above 1ug/m''

M '. tr'e '.s! tp!1 de: on'y! rr.i6 i i& , i i . i l ! , t :4 6 i?3 { r u l - \ }

I s'tu@ p"+' "*isa'

-"""' o' fdd o ̂ a!'93t d'-r {w's' 6n

",iliffir;n"i'6;n;;*;"'!bl.d6?tamco!d|td5b'E'ml<ou*samq'--gme"*go'***"*-j' ' iovh.loelo.tr'9ult1'jad'e'1$. dme o'6 'trt(4d6 onrv dd dnn m r-'u

" -'..' ' -*dis i;"Y- ii; c'^'pt;; *b Gemdi rv 5 b a cr'nt at r< d" i-sa dF

ohc.m d,€**'* .. ";.d;iooo*d

-'i6 d@"{ e-tiinFi +i -i" ;;;l;rr;ao'i t'qq

" raisr-'"" o u. o'ii"iii;;;;a+;r d;'d;;:c i'ddu aro otrosr -ai F i^scie 'o s

( { cw r i pdc i vLvd r r I + , r l +1 .31 ! r l i r r t { : t

Test Report No.:CE201284041Date : 20'12/0e'/30Page : 19 of 30

HENKEL CORPORATIONiEiriei noHesrves-eLEcrRoNlcs MAIN oFFlcE: 14000 JAIIIBoREE RoAD'92606 U.S.A.

Samole Material Dioestion Acid

geel, copper, aluminum, solder Aqua r€sia, HNO3, Hcl, HF, Hro,

Glass HNO3/HF

Gold, platinum, palladium, ceramic Aoua rcqraSilver HNO3

Plastic H,SO.. H,O,, HNO3, HCI

others Added appropriate reagent to totaldigestion

l llllllllrllllrIRVINE, CALIFORNIA,

1 )

2)3)

These 6amples w€re di$olved totally by pre-conditioning melhod according to below flow chart

( Cr& test method excluded )Name of the De6on who made measuaement Climbgreat YangName of the person in charge of measurement Troy Chang

lilote* : (1) For non-metallic material, add alkaline digestion reagent and heat to 90-g5t(2) Formetallic material. add pure water and heat to boiling

; f i ; i : -a i ; - : : n- i ; ;? : . .4 r a I , iE L r !?

i'ii 6iiiEii ii m;;irn "";Fdb'16*dc.r1dtu!"'b:itu:iDerdrcdri^k6s'dore-r.

m+cddmonsram4e oo"-dr A

"-'*; ;\,1v--;'or;;d.Boc-r' idieohd'nro@@nd*lodheRrdd!r-ecoMrv!hdhs34

"" "" .*

" -'-

" ,,,'"'.

";;;: i i"v ini cmp;'ii; -ta eo*'' q

bnsdo1 ' t r . f t s i !&h r r c " ra *ooamsu" . . . i i n i i u , doMml ; r : soau f t admds""

;;;6;;;;";;' d;;;n F '*i a- otu' @ 5 -a; M

Ndtrp. c! ldv:i/ ir l.f-i ri.4't ( 'r ii;tn$

Add appropriate amountof dig€stion reagent

Microwav€ digestion withHNO3/HCUHF

Acid digestion by suitable aciddepended on different samplematerial (as below table)

Heat to appropnatetemperature to e)dract

1) AlkaliFusion2) HClto di66olve

Add diphenyl-carbazidefor color development

measure the absorbanceat 540 nm by UV-VIS

Test Report No. : CE/20'12/8404'1Date.2112108130 Page : 20 of 30

HENKEL CORPORATIONiiEiiiiEi nonesrves-eLEcrRoNlcs MAIN oFFlcE: 14000 JAMBoREE RoAD'92606 U.S.A.

ItlllllllllllttllnIRVINE, CALIFORNIA,

1) These samples were dissolved totally by pr€-conditioning method according to below flow

chart.2) Name of the person who made measurementi Climbgreat Yang

3) Name of the person in charge of measurement Troy Chang

FlowChart ofdigestlon for the elemenb 'naly3is performed by ICP-AES

S-teel, copper, aluminum, solder Aqua regia, HNO3, Hcl, HF, H2O2

Glass HNO3/HF

Gold, platinum, Palladium, ceramic Aqua regia

Silver HNO3

Plastic HrSO., HrOr, HNO3, HCI

Others Mded appropnate reag€nt to total digestion

ffif---t N.wrapdcitvlawr$ r r; l +r r ir iiifrs'i

Sample Measurem€nt

Acid dig€5tion by suitable acid dependecl on

different sample material (as below lable)

Alkali FusionHCI to dissolve

r.s6rorrstE r+&ro?Prett @w

Test Report No. : CE/201284041Date : 201208/30 Page : 21 of 30

llll ltlllll llr

14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA'HENKEL CORPOMTIONiinxel noHesves-eLEcrRoNlcs MAIN oFFlcE:92606 U.S.A.

Analytical f,ow Ghart of halogen content

1) Name of the person who made mea6urement Rita Chen

2) Name of the person in charge of measurement Troy Chang

g31;;9,3.1.".1"1 r; -l: l.tT

*,r'm**Psml#*r**iii**rryrswsata,r;qlt#rlTi#d;iffi #;"$ri}:ffifihrffi i"fr T:"#q"{s."iffi l,Jfxigi:ilkri;"'*rx"-ti+riin$ill lnj.:lffi:?:-r:1':r

Sample Pr€treatm ent / Separation

Weigtfing and putting sample in cell

Orygen Bomb Combustion / Absorption

Diluton to fixed volume

Analysis was performed bY lC

r's602reerx ire6lo)aett

Test RePortHENKEL CORPORATIONHENKEL ADHESIVES.ELECTRONICS92606 U.S.A.

No.: CEl201Zuu1 Date:201208/30Page:22 ol 30

Itrtll llllllllllll

MAIN OFFICE: '!4OOO JAMBOREE ROAD, IRVINE' CALIFORNIA'

Analytical flow chart of volatlla organic compounds (vocs)

II

Name of the person who made measurement : Chun wu

Name of th€ pe6on in charge of measurement : Shinjyh Chen

lReference method : US EPA 5021 )

Nvr'ts]cq' lrwm/I I -ir i il{t'" I lli i i33int

'ffiiffi

Sample pretreatment

Take sample and Put it intoheadspace glassware

Analysis was Pertormed bY GC/MS

Test RePort No. iCEj2O12!84c41 Oale 2O12J08130 Page: 23of 30

HENKEL CORPORATIONHENKEL ADHESTVES-ELECTRONICS t\4AlN OFFICEI92606 U.S.A.

Itlllttllllllllllll14OOO JAMBOREE ROAO, IRVINE, CALIFORNIA'

II

Benzotrlazole analytlcal flovt chart

Name of the person who made mea€u€ment: Roman WongNem€ of the;erson in charge of measurement: Troy Chang

;lffi*vTdy l" **:s:h:xn F T'e jfs?rynT{ovf hsam?b'3 F3Eo %k"i@ndr"l":l:":.:::::"

ii;u;j,;r'* sd by tr" co^,p"r 'on" o. cs*' c*"i'osr'-*"I;fi,;fl*,f"','8ff"',ff;ftTl$ift".i:iiX'.#S"*"1f:lTT'q-"#;lf#ift"ill

i'i1rhHHilR:#ffiS'"*{'fts#"?i$Hffir:frljHi'siffii-s:;*lr'i'l1rriflr,j't'iff+rm:ff:?sr]';:TrPi"1Fl#i#;i##"'j,*';#*',:*#*:rs:"';p;t*ri#,"j*r.a'jir*e*J'"*rurr.r"x"::::""LTf''"Jrujir";til:r""rsirl'11;

- h j l 4 i i . r j ' d l r t t i

SamDle pretreatmenuseParation

Sample extraction by soxhlet method

concentrate/Dilute Exfacted 60tution

Dal,a

Test ReportHENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS92606 U.S.A.

No. : CE/201284041Dale:2012108/30 Page : 24 of 30

llfllll|Illlll[Il

IIIAIN OFFTCE: '14OOO JAMBOREE ROAD' IRVINE' CALIFORNIA'

Concentrat€/Dilute Extracted solution

Analysis was performed bY LC/MS

PFOA/PFOS analytlcal flowcha of lJlthsonic extractlon (LC/MS) proceduro

I Name ofthe person who made measur€ment: Roman l /ongr Name of the person in charge of measurement Troy Chang

'$r i i r i I r i I n t t i L I $ ! / ! l r l

-.r(&r:n*rl1)r:ri

Sample pretreatment

Sample ertraction by Ultrasonic extraction(Referenc€ method: US EPA 3550C)

HENKEL CORPORATTON lllllllllll llllllllHENKEL ADHESIVES-ELECTRONICS MAIN OFFICE: '14OOO JAMBOREE ROAD, IRVINE' CALIFORNIA'92606 U.S.A.

Test Report No. I CE|2O12JUU1 Date:201208/30Page : 25 of 30

Analysis flow chart for deiEmination of Asbestos1) Name of the DeBon who made measurement Victor Kao2) Name of the pe6on in ch€rge of m€asurement Wendy Wei

I Rete]ence mothod: NIOSH 9000 |

- Dtffr""ti"i-il"r<ot_lasbestos is present I

Diffraclion peak ofasbestos is absent-------r------

Asbestos identification byoptical microscopy

Asbestos fiber is present Asbestos fiber i6 absent

Containing A6bestos/Positive Not containing Asbestos/

Negative

a; ; f f ; . r : ' . r r ' i . : -

t i . ; ! r .8 . " . |1 ! , . ,s idL " . ? :^".""'*.*-"."'.-"*,"is"-ciptmo"ili'-J*aaueoa-qUsld.d@j'c*lM5{\6

i,ir ii,i.iniijnlc i(;a o;omns *tld 16 r.n a"d c-dfr*3io:aiea@ L Dnrdb ' dr;.g' der-\ md cot@n're-"Do*i,;;,;;i;ft d.^ncM.nu rhsac,s@o*mo tgin-ii'i" hdde'

"'hi3 dod-ed dadis rs 'is cosrI tdnsgd

i i ; ; ; ' ; ; ; ; ; ; ; f t ;d i . ; . t r " l .6dc ,d ! ' " * .d i fu i ;1 - i ' . cmp. l ry .$F!s@DH1'6biii,.''*.],iii..i;n.i"ga|h".,01Nmdqat9nsunde'hmnsf'doan.nGr,orJqi4n.oiiniii"v cv

"ne*r.z* auamr:ba.'v

" chd@r or h -;;i;iaF;;;; hE d@"d

" r a"' a oredd6 r'; b ot'ebd b b

N*ttrFctr.iw:d/r j :i: ett*lL r ilrr'll

Test Report No. '. CEl2O12l84O41 Date | 201 208r'30 Page : 26 of 30

HENKEL CORPORATIONHENKEL AOHESIVES-ELECTRONICS MAIN92606 U.S.A.

rlllll[lllllltllllllOFFICE: 14OOO JAMBOREE ROAD' IRVINE' CALIFORNIA,

Analytlcal flow chart of Org.nic-Tln content

I Name ofthe person who made measurement Ginny Chen

l Name of the pe6on in charge ofmeasurement Trcy Chang

Oata

ffiffiflk r4e ca ldw : i / ! l ) i r L4 i : qL ' l r j t f n l i

Test ReportHENKEL CORPORATIONHENKEL ADHESIVES.ELECTRONICS92606 U.S.A.

No. : CH2012luM1 Date ; 2012108/30Page : 27 of 30

llllllil|llllmli l

MAIN OFFICE: 14000 JAMBOREE RoAD, lRVlNE, CALIFORNIA'

Analysis flow chart for detonninatlon of Pvc in matedal

I Name oflhe person who made measurcment: Ginny Chen

r Name of the person in charge of meaEurement:Trcy Chang

Data

'$ffiffifii i: 6i:kL r iiL'!rr!

SamPle Pre-treatment

Flametest

Sample analyzed bY FTIR

Check wave-number of C-Clbonding

Test RePort No. : cE/201284041

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS ITAIN OFFICE:92606 U.S.A.

Date: 2012108/30 Page: 28 of 30

ll[lllllltlllllllul14000 JAI/IBOREE ROAD, IRVINE' CALIFORNIA'

Chlorinated Flam€ retardant analytical flow chart

1) Name of the person who made measurement Barry Tseng

2) Name of the person in charge of measuremenl Troy Chang

I Refeence method: US EPA 8270D, US EPA 3540

I Test ltems: PCBS, PCNS, PCTS, Mkex, CP' MCCP

Data

il

Test ReportHENKEL CORPORATIONHENKEL ADHESIVES.ELECTRONICS92606 U.S.A.

No. : CEJ2o12luu1 Date : 2012108/30 Page : 29 of 30

t\4AlN OFFICE: 14OOO JAMBOREE ROAD, IRVINE'Itrlll[lllllll ill

CALIFORNIA,

PBB/PBOE analytical FLOW CHART

r Name of the person who made measurement: Roman Wong

I Name of the pefson in chafge of measurement Troy Chang

First testing process -----'

Optronal screen Prccess ...'

confirmation plocess

: . . . . . . . . ' ' . . . . . . . . . ' ' . . . . . . 1| | - _ | ;: I Scre€n analvsis I :: t

' ' !

r - . . . ' . . . . 1 ' ' . . . ' ' . ' . . . r

Concentrate/DiluteExtracted solution

I Sample extraction/ II Soxhlet method I

Scre€n analysls

lssue Report

I Filter It--._-+

I Analysisbycc/Ms I

ffiewffih-! i n1 { i I c i l t l l

r+src).rs re |ie.a!/a!::,__jljg!--

Test Report No. . CEl2Ol2l&4(y1 Date : 20'12i08/30 Page:30of30

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS i'AIN OFFICE:92606 U.S.A.

lllllll lllllll ll14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA,

N€* i . ' t s i c i e r : iw ! t r / t l ' l L4 r r ' r l : ' : r n ! r

t The tested sample / pa b ma*ed by an anow if ifs shown on the photo '

" End of Repod "

84041

SignaturetidFor Question

with SGS

Test Report No. : CE/2012M036

Pleaseom

oate: 2012108/30 Page: 1 0f4

lflllllllllllmltl]lHENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICScALtFORNIA. 92606 U.S.A.

Sample DescriptionStyle/ltem No.Sample Receiving DateTesting Period

Test Roqu6tod

Test tlothod

Test Result(s)

[4AlN OFFICE: 14000 JAMBOREE ROAD' IRVINE'

Th. following sample(s) was/were submltted and identified by/on behalfofthe client as :

ADHESIVE8+lLtitsR42012,0er/242U2tOAt2410 2012n4/30

: With reference to BS EN 14582:2007

: Please refef to next page(s).

As specified by client, to test H€logen-Fluodne, Chlodne, Bromine' lodine 'n

the submitted sample.

Cft.dcalaotiory- P.aol.Nr I l|6qdEpgl erc mr r-olre q:41'\si Fsk- r!h' GsEd €f

trffixli'#*i#'ifi'*#'*I:i"er"{s*r"nx;i:;:r*t""mx,rr**:"+ry1!rxlTj#ir:ljsff":*"n';r.ilj.Trrjir;lni-.iriri,.i,ni,iirny "*-,reo*"- -'ab- ''!*' "".* r#:li#n""."t*#*:t E:"-tS;*'";$2";ruf ;l;**rT;:'l;:$'"%L'"lX'S"[iF#ffiil$ff"1i$:ilT',fijlT.ri$i'$iiqi;"!iji;"f#$'*ids-SJ'i;tr$r*ii'"rmisi**"1*';";;*"*ri"t"rr:5l""j"1r;i's';;

Test ReportHENKEL CORPORATIONHENKEL ADHESIVES.ELECTRONICSCALIFORNIA, 92606 U,S-A-

Test R€6ult{3)

PART |{AME No.'1

No. : CE201284036 Date : 201208/30 Page:2 ol 4

lt l[ulllll llll]lti4AlN OFFICEi 14000 JAMBOREE ROAD, IRVINE'

: SILVER COLORED PASTE

T€6t ltem(s) Unit Method MDLR6sultNo.1

HalogonFalogen-Fluorine (F)(CAS No.: 14762-94€)

mg/kgWith reference to BS EN14582:2007. Analysis wasperfomed bY lC.

50 n.d.

Halogen4hlorine (Cl)(CAS No.: 22537-1$1)

50 197

Halogen-Bromine (Br)(CAS No.: 10097-32-2)

5o n,o-

Halogenlodine (l)(CAS No.: 1436'2-4€)

50 n.o.

Itote :

1mg/kg=ppml 0 .1M% = 1000PPm

2. n.d. = Not Detected

3 MDL = Method Detection Limit

, f r : ! 1 : ! L r d i l t l i

Test RePort No : cE/20'1284036

HENKEL CORPORATIONHENKEL ADHESIVES.ELECTRONICS II4AIN OFFICE:CALIFORNIA, 92606 U.S.A.

Date : 2012108/30

14OOO JAMBOREE ROAD,

Page: 3 of 4

ll [lllllll]llllltlIRVINE,

Analytical flow chatof halog€n cont€nt

1) Name of the person wt1o made measurement: Rita Chen

2) Name of the pe6on in charge of measurement: Troy Chang

iitff ry:iff1Ti$$:m{tT;i'$ffi 5#Hnf.T:"ffi :liffii#""*L#ffi;:':;;:i:ffi ffiJd;*;lif#r;'#**,1*,*;*;*."%!i."{,';it'':"'"i:ii".";:lt-s'di;:"H-r:*H"#ffir"""i;:,*Pimxtirmrr, **lfiF,tii+'i1,ff#;Tru'r-S.t'',fririiffiflff;,flj$Hlifl-ffjffi:'Eft,Hf,*":+H{ir."l$a'i$liffi r"ftn{$i*l-$H$$:*:'*x#+q#'*it1*;"'s"'fi 'rlt#*{I#Sr},?fl #*#i#:"ffi illtr##i"rik"nl"lwir;[.*s*Tnmg"rurui'srl;

Sample pretreatment / Separation

Weighting and putting sample in cell

Oxygen Bomb Combustion / Absorption

Dilution to fixed volume

Analysis was Performed bY lC

iii6j"i erv,naumrz;o awmn. t'r'tv -

Test Report No. . CEi201284036 Dale:2012108130

HENKEL CORPORATIONHENKEL ADHESIVES-ELECTRONICS ti4AlN OFFICE:oALTFORNTA. 92606 U.S.A.

Page: 4 of 4

llmrrrfl l|lllta14OOO JAMBOREE ROAO, IRVINE,

' Th6 tested sample / pa.t is marked by an arrow if it's shown on the photo '

84036

" End of Report -'

Hqhr4 tu6ddh'! N'elapo''q raLd' r i r,-']: i /N rr!' ft ltr{t

=r/rh{lll*irN it!