Hawaiian Choice CBD€¦ · Batch 6613 View any other batch by scanning QR code on the box or visit...

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Accreditation # 92630 1150 S. KING STREET, HONOLULU, HI 96814 LICENSE #: 92630 CERTIFICATE OF ANALYSIS Nelson Lazaga, Ph.D Laboratory Director Date: 2/27/2020 The following results relate only to the samples tested and for the specific tests conducted. Steep Hill grants permission to reproduce this document in full only. © 2020 STEEP HILL, INC. ALL RIGHTS RESERVED CERTIFICATE #: HI82371 REVISION #: HI82371.1 Page 1 of 3 Sample Name: 6613 Steep Hill ID: HI82371 Batch ID: State ID: Sample Type: Tincture Date Received: 2/24/2020 Date Reported: 2/27/2020 Density: 0.930 g/mL Customer: Hawaiian Choice OVERALL BATCH SUMMARY: PASS Residual Pesticides Microbial Impurities Mycotoxins Heavy Metals Foreign Material Residual Solvents Pass Pass Pass Pass NT NT Total THC Not Detected Not Detected Not Detected Total CBD 2.73 % 27.3 mg/g 27.5 mg/mL Total Cannabinoids 3.16 % 31.6 mg/g 31.9 mg/mL Total THC = [THCA x 0.877] + [THC] Total CBD = [CBDA x 0.877] + [CBD] Accreditation # 92630 1150 S. KING STREET, HONOLULU, HI 96814 LICENSE #: 92630 CERTIFICATE OF ANALYSIS Nelson Lazaga, Ph.D Laboratory Director Date: 2/27/2020 The following results relate only to the samples tested and for the specific tests conducted. Steep Hill grants permission to reproduce this document in full only. © 2020 STEEP HILL, INC. ALL RIGHTS RESERVED CERTIFICATE #: HI82371 REVISION #: HI82371.1 Page 3 of 3 0 2 0 2 / 6 2 / 2 s t l u s e R d i o n i b a n n a C Standard potency analysis utilizing Ultra High Performance Liquid Chromatography (UHPLC; HI-SOP-024) Analyte % mg/g mg/mL LOD mg/g LOQ mg/g CBC NT NT NT NT NT CBD 2.73 27.3 27.5 0.00868 0.00912 CBDA ND ND ND 0.00868 0.0156 CBDV NT NT NT NT NT CBDVA NT NT NT NT NT CBG 0.152 1.52 1.53 0.00868 0.00999 CBGA NT NT NT NT NT CBN 0.278 2.78 2.80 0.00868 0.00868 THC ND ND ND 0.00868 0.00868 delta-8-THC NT NT NT NT NT THCA ND ND ND 0.00868 0.0200 THCV NT NT NT NT NT THCVA NT NT NT NT NT Total 3.16 31.6 31.9 Microbial Impurities Results Pass 2/27/2020 Microbiological screening utilizing PathogenDx and TEMPO (HI-SOP-008 + HI-SOP-007) - Limit units: CFU/g Analyte Pass/Fail Result Limit LOQ Aspergillus flavus Pass ND ND Not Detected in 1 gram Aspergillus fumigatus Pass ND ND Not Detected in 1 gram Aspergillus niger Pass ND ND Not Detected in 1 gram Salmonella Pass ND ND Not Detected in 1 gram Aerobic Pass <100 10000 1 CFU/g Coliform Pass <100 100 1 CFU/g Enterobacteria Pass <100 100 1 CFU/g General E. coli Pass <1 ND 1 CFU/g Yeast & Mold Pass <100 1000 1 CFU/g Terpenoid Results NT Standard terpene analysis utilizing Liquid Chromatography – Mass Spectrometry (LC-MS; HI-SOP-024) Analyte % mg/g mg/mL LOD mg/g LOQ mg/g -Bisabolol NT NT NT NT NT Camphene NT NT NT NT NT 3-Carene NT NT NT NT NT Caryophyllene Oxide NT NT NT NT NT -Caryophyllene NT NT NT NT NT Eucalyptol NT NT NT NT NT Geraniol NT NT NT NT NT Guaiol NT NT NT NT NT Humulene NT NT NT NT NT p-Isopropyltoluene NT NT NT NT NT Isopulegol NT NT NT NT NT Limonene NT NT NT NT NT Linalool NT NT NT NT NT -Myrcene NT NT NT NT NT Nerolidol NT NT NT NT NT Ocimene NT NT NT NT NT -Pinene NT NT NT NT NT -Pinene NT NT NT NT NT -Terpinene NT NT NT NT NT -Terpinene NT NT NT NT NT Terpinolene NT NT NT NT NT Total NT NT NT NT NT Moisture Results NT Moisture content analysis utilizing Moisture Balance (MB; HI-SOP-033) - Limit units: % Analyte Pass/Fail % Limit Moisture NT NT Foreign Material Results NT Foreign material analysis utilizing visual inspection with 10x magnification (HI-SOP-016) Analyte Pass/Fail Visual Inspection NT ND: Not Detected NT: Not Tested LOQ: Limit of Quantitation LOD: Limit of Detection Hawaiian Choice CBD Independant Lab Report Markings in RED are by Hawaiian Choice to highlight key findings Batch 6613 View any other batch by scanning QR code on the box or visit our website Manufacturing Date THC None Detected CBD 27.5mg per ml - Bottle 30ml = 825mg - Spray 0.4ml = 11mg Broad Spectrum CBG & CBN also detected in significant levels (beneficial non-psychoactive cannabinoids) Tincture Test Summary Microbial None Detected Bacteria, spores, molds, fungus

Transcript of Hawaiian Choice CBD€¦ · Batch 6613 View any other batch by scanning QR code on the box or visit...

Page 1: Hawaiian Choice CBD€¦ · Batch 6613 View any other batch by scanning QR code on the box or visit our website Manufacturing Date THCTincture None Detected CBD 27.5mg per ml - Bottle

Accreditation # 92630

1150 S. KING STREET, HONOLULU, HI 96814 LICENSE #: 92630

CERTIFICATE OF ANALYSIS

Nelson Lazaga, Ph.DLaboratory DirectorDate: 2/27/2020

The following results relate only to the samples tested and forthe speci�c tests conducted. Steep Hill grants permission to

reproduce this document in full only.

© 2020 STEEP HILL, INC. ALL RIGHTS RESERVED

CERTIFICATE #: HI82371REVISION #: HI82371.1

Page 1 of 3

Sample Name: 6613Steep Hill ID: HI82371

Batch ID:State ID:

Sample Type: TinctureDate Received: 2/24/2020

Date Reported: 2/27/2020Density: 0.930 g/mL

Customer: Hawaiian Choice

OVERALL BATCH SUMMARY: PASSResidual Pesticides Microbial Impurities Mycotoxins Heavy Metals Foreign Material Residual Solvents

Pass Pass Pass Pass NT NT

Total THC

Not Detected

Not Detected

Not Detected

Total CBD

2.73 %

27.3 mg/g

27.5 mg/mL

Total Cannabinoids

3.16 %

31.6 mg/g

31.9 mg/mL

Total THC = [THCA x 0.877] + [THC]Total CBD = [CBDA x 0.877] + [CBD]

Accreditation # 92630

1150 S. KING STREET, HONOLULU, HI 96814 LICENSE #: 92630

CERTIFICATE OF ANALYSIS

Nelson Lazaga, Ph.DLaboratory DirectorDate: 2/27/2020

The following results relate only to the samples tested and forthe speci�c tests conducted. Steep Hill grants permission to

reproduce this document in full only.

© 2020 STEEP HILL, INC. ALL RIGHTS RESERVED

CERTIFICATE #: HI82371REVISION #: HI82371.1

Page 3 of 3

0202/62/2stluseR dionibannaCStandard potency analysis utilizing Ultra High Performance Liquid Chromatography(UHPLC; HI-SOP-024)Analyte % mg/g mg/mL LOD mg/g LOQ mg/gCBC NT NT NT NT NT

CBD 2.73 27.3 27.5 0.00868 0.00912CBDA ND ND ND 0.00868 0.0156

CBDV NT NT NT NT NTCBDVA NT NT NT NT NT

CBG 0.152 1.52 1.53 0.00868 0.00999CBGA NT NT NT NT NT

CBN 0.278 2.78 2.80 0.00868 0.00868THC ND ND ND 0.00868 0.00868delta-8-THC NT NT NT NT NT

THCA ND ND ND 0.00868 0.0200THCV NT NT NT NT NT

THCVA NT NT NT NT NTTotal 3.16 31.6 31.9

Microbial Impurities Results Pass 2/27/2020Microbiological screening utilizing PathogenDx and TEMPO(HI-SOP-008 + HI-SOP-007) - Limit units: CFU/gAnalyte Pass/Fail Result Limit LOQAspergillus �avus Pass ND ND Not Detected in 1 gram

Aspergillus fumigatus Pass ND ND Not Detected in 1 gramAspergillus niger Pass ND ND Not Detected in 1 gram

Salmonella Pass ND ND Not Detected in 1 gramAerobic Pass <100 10000 1 CFU/gColiform Pass <100 100 1 CFU/g

Enterobacteria Pass <100 100 1 CFU/gGeneral E. coli Pass <1 ND 1 CFU/g

Yeast & Mold Pass <100 1000 1 CFU/g

Terpenoid Results NTStandard terpene analysis utilizing Liquid Chromatography – MassSpectrometry (LC-MS; HI-SOP-024)Analyte % mg/g mg/mL LOD mg/g LOQ mg/g

-Bisabolol NT NT NT NT NT

Camphene NT NT NT NT NT3-Carene NT NT NT NT NTCaryophyllene Oxide NT NT NT NT NT

-Caryophyllene NT NT NT NT NTEucalyptol NT NT NT NT NT

Geraniol NT NT NT NT NTGuaiol NT NT NT NT NT

Humulene NT NT NT NT NTp-Isopropyltoluene NT NT NT NT NT

Isopulegol NT NT NT NT NTLimonene NT NT NT NT NT

Linalool NT NT NT NT NT-Myrcene NT NT NT NT NT

Nerolidol NT NT NT NT NT

Ocimene NT NT NT NT NT-Pinene NT NT NT NT NT

-Pinene NT NT NT NT NT-Terpinene NT NT NT NT NT

-Terpinene NT NT NT NT NTTerpinolene NT NT NT NT NT

Total NT NT NT NT NT

Moisture Results NTMoisture content analysis utilizing Moisture Balance (MB;HI-SOP-033) - Limit units: %

Analyte Pass/Fail % LimitMoisture NT NT

Foreign Material Results NTForeign material analysis utilizing visual inspection with10x magni�cation (HI-SOP-016)

Analyte Pass/FailVisual Inspection NT

ND: Not DetectedNT: Not TestedLOQ: Limit of QuantitationLOD: Limit of Detection

Hawaiian Choice CBD Independant Lab Report Markings in RED are by Hawaiian Choice to highlight key �ndings

Batch 6613View any other batch by scanning QR code on thebox or visit our websiteManufacturing Date

THC None Detected

CBD 27.5mg per ml- Bottle 30ml = 825mg- Spray 0.4ml = 11mg

Broad SpectrumCBG & CBN also detectedin signi�cant levels (bene�cial non-psychoactivecannabinoids)

Tincture Test Summary

Microbial None DetectedBacteria, spores, molds, fungus

Page 2: Hawaiian Choice CBD€¦ · Batch 6613 View any other batch by scanning QR code on the box or visit our website Manufacturing Date THCTincture None Detected CBD 27.5mg per ml - Bottle

Accreditation # 92630

1150 S. KING STREET, HONOLULU, HI 96814 LICENSE #: 92630

CERTIFICATE OF ANALYSIS

Nelson Lazaga, Ph.DLaboratory DirectorDate: 2/27/2020

The following results relate only to the samples tested and forthe speci�c tests conducted. Steep Hill grants permission to

reproduce this document in full only.

© 2020 STEEP HILL, INC. ALL RIGHTS RESERVED

CERTIFICATE #: HI82371REVISION #: HI82371.1

Page 2 of 3

Residual Pesticides Results Pass 2/27/2020Residual pesticide analysis utilizing Liquid Chromatography – Mass Spectrometry (LC-MSMS; HI-SOP-025) - Limit units: ug/g = ppmAnalyte Pass/Fail µg/g Limit LOD µg/g LOQ µg/g Analyte Pass/Fail µg/g Limit LOD µg/g LOQ µg/gAbamectin B1a Pass ND 1 0.251 0.761 Hexythiazox Pass ND 1 0.220 0.666

Acephate Pass ND 1 0.0718 0.218 Imazalil Pass ND 1 0.0492 0.149Acequinocyl Pass ND 1 0.00366 0.990 Imidacloprid Pass ND 1 0.0713 0.216

Acetamiprid Pass ND 1 0.119 0.361 Kresoxim-methyl Pass ND 1 0.0674 0.204Aldicarb Pass ND 1 0.0395 0.120 Malathion Pass ND 1 0.0616 0.187

Azoxystrobin Pass ND 1 0.0915 0.277 Metalaxyl Pass ND 1 0.0590 0.179Bifenazate Pass ND 1 0.106 0.320 Methiocarb Pass ND 1 0.100 0.304Bifenthrin Pass ND 1 0.207 0.628 Methomyl Pass ND 1 0.0391 0.119

Boscalid Pass ND 1 0.216 0.654 Methyl Parathion Pass ND 1 0.149 0.452Carbaryl Pass ND 1 0.0418 0.127 MGK-264 Pass ND 1 0.195 0.592

Carbofuran Pass ND 1 0.0293 0.0888 Myclobutanil Pass ND 1 0.0605 0.183Chlorantraniliprole Pass ND 1 0.0899 0.272 Naled Pass ND 1 0.0558 0.169

Chlorfenapyr Pass ND 1 0.0386 0.117 Oxamyl Pass ND 1 0.0389 0.118Chlorpyrifos Pass ND 1 0.0883 0.268 Paclobutrazol Pass ND 1 0.0394 0.119

Clofentezine Pass ND 1 0.167 0.505 Permethrin Pass ND 1 0.268 0.813Cy�uthrin Pass ND 1 0.415 0.990 Phosmet Pass ND 1 0.139 0.422Cypermethrin Pass ND 1 0.265 0.802 Piperonyl Butoxide Pass ND 1 0.0455 0.138

Diazinon Pass ND 1 0.0349 0.106 Prallethrin Pass ND 1 0.0826 0.250Dichlorvos Pass ND 1 0.177 0.538 Propiconazole Pass ND 1 0.0842 0.255

Dimethoate Pass ND 1 0.0491 0.149 Propoxur Pass ND 1 0.0308 0.0933Ethoprophos Pass ND 1 0.0933 0.283 Pyrethrins Pass ND 1 0.0394 0.119

Etofenprox Pass ND 1 0.241 0.732 Pyridaben Pass ND 1 0.210 0.635Etoxazole Pass ND 1 0.0497 0.151 Spinosad Pass ND 1 0.0330 0.0999

Fenpyroximate Pass ND 1 0.00147 0.00445 Spiromesifen Pass ND 1 0.0623 0.189Fipronil Pass ND 1 0.112 0.340 Spirotetramat Pass ND 1 0.0529 0.160

Flonicamid Pass ND 1 0.0959 0.290 Tebuconazole Pass ND 1 0.0804 0.244Fludioxonil Pass ND 1 0.0618 0.187 Thiacloprid Pass ND 1 0.0615 0.186

Mycotoxin Results Pass 2/27/2020Mycotoxin analysis utilizing Liquid Chromatography – MassSpectrometry (LC-MS; HI-SOP-025) - Limit units: µg/kg = ppb

Analyte Pass/Fail µg/kg Limit LOD µg/kg LOQ µg/kgA�atoxin B1 ND 5.14 15.6

A�atoxin B2 ND 4.71 14.3A�atoxin G1 ND 4.88 14.8A�atoxin G2 ND 7.06 21.4

Ochratoxin A Pass ND <20 9.10 27.6Total A�atoxins Pass ND <20 7.06 21.4

Heavy Metals Results Pass 2/27/2020Heavy metals analysis utilizing Atomic Absorption Spectroscopy(AAS; HI-SOP-015) - Limit units: µg/g = ppmAnalyte Pass/Fail µg/g Limit LOD µg/g LOQ µg/gArsenic Pass ND 10 0.00131 1.36Cadmium Pass ND 4 0.0000109 1.36

Lead Pass ND 6 0.00158 1.36Mercury Pass ND 2 0.00117 1.36

Residual Solvents Results NTResidual solvents and processing chemicals analysis utilizing Headspace Gas Chromatography – Mass Spectrometry (HS-GC-MS;HI-SOP-010) - Limit units: ug/g = ppm

Analyte Pass/Fail µg/g Limit LOD µg/g LOQ µg/g Analyte Pass/Fail µg/g Limit LOD µg/g LOQ µg/gAcetone NT NT NT NT Isobutane NT NT NT NT

Acetonitrile NT NT NT NT Isopropanol NT NT NT NTBenzene NT NT NT NT Methanol NT NT NT NT

Butanes NT NT NT NT n-Pentane NT NT NT NTChloroform NT NT NT NT Tetrahydrofuran NT NT NT NT

Ethanol NT NT NT NT Toluene NT NT NT NTHeptanes NT NT NT NT Total Xylenes NT NT NT NT

n-Hexane NT NT NT NT

Pesticides None Detected

Mycotoxins None Detected

Heavy Metals None Detected

Shelf Life Stability PassLow water activity (aW <0.86) and high acidity (pH <4.5)for improved anti-microbial shelf life and stability.

Hawaiian Choice CBD Independant Lab Report Markings in RED are by Hawaiian Choice to highlight key �ndings

Tincture